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' 610 W. MAIN ST.. ROCKAWAY, NEW JERSEY 07866 cnvino ^ 5C!£nc£; inc. ^ ^ ^ - " ^ 19 COPELAND RD.. DENVILLE. NEW JERSEY 07834 ^^'^yyy. (201)366^256 f \ ~ s . ^ SDMS Document 115531 Apr II 1 7 , 1 9 8 6 M r . C h a r I e s D o I an U S E P A , E R R D 26 F e d e r a l P l a z a R o o m 7 4 7 , S I C B N e w Y o r k , N Y 1 0 2 7 8 R e : I s l a n d C h e m i c a l C o m p a n Y . U . S . v i r g i n I s l a n d s D e a r M r . D o l a n : As per o u r t e l e p h o n e c o n v e r s a t i o n , I am s e n d i n g the e n c l o s e d I n f o r m a t i o n c o n c e r n i n g E n v i r o - S c i e n c e s , I n c . w o r k at the I s l a n d C h e m i c a l C o m p a n y s i t e in S t . C r o i x , U . S . V . l . I t r u s t t h a t t h i s p a c k a g e will b e h e l p f u l in y o u r u n d e r s t a n d i n g of the a c t i v i t i e s w h i c h h a v e o c c u r r e d o n the s i t e d u r i n g the p r i o r o n e a n d o n e - h a l f y e a r s . A S w e d i s c u s s e d , I w i s h to m e e t w i t h y o u c o n c e r n i n g t h i s m a t t e r . If p o s s i b l e , I w o u l d p r e f e r to s c h e d u l e t h i s m e e t i n g for T h u r s d a y mor n 1 ng , A p r i I 24 t h . If y o u h a v e a n y q u e s t i o n s , c o n t a c t m e at 2 0 1 / 3 6 6 - 6 2 5 6 . V e r y t r u l y y o u r s . E N V I R O - S C I E N C E S , I N C . ^ izq (^7rJ^-nc/' y^Ol A l a n L. K y I e s , P h . D . V i c e P r e s i d e n t A L K / p o ( A K - 8 6 1 4 3 ) E n c l o s u r e s : P r o j e c t S u m m a r y w i t h a t t a c h m e n t s c c : ; R . M i I o s F. Cur t i s R . W i l l i s 1 . Ar s h e n S E N T V I A F E D E R A L E X P R E S S O N 4 / 1 7 / 8 6 . 100086 P r o l e c t S u m m g r y for I s l a n d C h e m i c a l C o m p a p y . Inc.. ( B e r l e x ) S t . C r o l y . V i r g i n I s l a n d s • ^ I n c l u d e d h e r e i n Is a s u c c i n c t s u m m a r y for the e n v i r o n m e n t a l c l e a n u p of I s l a n d C h e m i c a l C o m p a n y ( I C C ) , S t . C r o i x , V i r g i n I s l a n d s . D o c u m e n t a t i o n for all a c t i v i t i e s a r e I n c l u d e d as a t t a c h m e n t s . E n v i r o - S c i e n c e s , Inc. i n i t i a t e d a s i t e e v a l u a t i o n In S e p t e m b e r , 1 9 8 4 a n d c o n t i n u e d the I n v e s t i g a t i o n Into O c t o b e r . C o n t a m i n a t i o n w a s f o u n d at s e v e r a l l o c a t i o n s a n d a p r e l i m i n a r y c l e a n u p p l a n w a s d e v e l o p e d and d e l i v e r e d to M r . C o n r a d S i m o n , U S E P A R e g i o n 1 1 , N e w Y o r k d u r i n g D e c e m b e r , 1 9 8 4 . ( S e e A t t a c h m e n t A ) . M r . S i m o n a s s i g n e d M r . R o b e r t H a r r i s as the p r o j e c t o f f i c e r . A f t e r n u m e r o u s t e l e p h o n e d i s c u s s i o n s a n d I n f o r m a t i o n r e q u e s t s by M r . H a r r i s , an a d d e n d u m to the o r i g i n a l r e p o r t w a s s u b m i t t e d in A p r i l , 1 9 8 5 (At t a c h m e n t B ) . F o l l o w - u p c o n v e r s a t i o n s w i t h M r . H a r r i s i n d i c a t e d that the p r o p o s e d p r o g r a m w a s s a t i s f a c t o r y . I r e q u e s t e d a letter of a p p r o v a l f r o m h i m ; h o w e v e r , he s t a t e d that the U S E P A w o u l d not issue a l e t t e r . He did s t a t e that I s h o u l d send h i m a l e t t e r s t a t i n g our intent to c l e a n u p (At t a c h m e n t C ) . D u r i n g the a p p r o v a l p e r i o d , M r . H a r r i s r e q u e s t e d c o p i e s of h a z a r d o u s w a s t e m a n i f e s t s for m a t e r i a l s s e n t f r o m the f a c i l i t y by ICC in 1 9 8 2 ( A t t a c h m e n t D ) . B e t w e e n J u n e and A u g u s t , 1 9 8 5 s e v e r a l t a s k s w e r e p e r f o r m e d at the ICC s i t e . T a s k s p e r f o r m e d by d a t e s are summarizisd be I o w : 1 . J u n e 6 - 1 5 . 1 9 8 5 T o l u e n e C o n t a m i n a t i o n f O r v e r ) S o i l from e i g h t (8) of a t o t a l of 14 d r u m s of t o l u e n e - c o n t a m i n a t e d soil w a s put on d r y i n g t r a y s and p l a c e d in the d r y i n g o v e n . T e m p e r a t u r e r e a c h e d a p p r o x i m a t e l y 42 d e g r e e s C a n d c o n t i n u e d to i n c r e a s e as m o i s t u r e w a s l o s t . T w o ( 2 ) 2 0 - g a i l o n p i a s t i c - I i n e d p a p e r b a r r e l s w h i c h w e r e o n e - h a l f full of s o i l and w a t e r w e r e p l a c e d in the d r y e r intact in an a t t e m p t to e v a p o r a t e the w a t e r b e f o r e p l a c i n g the soil o n t r a y s . E x h a u s t f r o m the v e n t w a s m o n i t o r e d w i t h a F l a m e I o n i z a t i o n D e c t o r ( F I D ) for e m i s s i o n of T o l u e n e . P y r i d i n e C o n t a m i n a t i o n ( L a b o r a t o r y P i t ) All liquid w a s t e to the l a b o r a t o r y pit w a s r e r o u t e d ; n o n - c o n t a c t c o o l i n g w a t e r to the gut a n d l a b o r a t o r y r i n s e w a t e r to a s t a i n l e s s steel c o n t a i n e r . All l a b o r a t o r y w a s t e s ( r e a g e n t s , s o l v e n t s , e t c . ) w e r e c o l l e c t e d in 5 5 - g a l l o n d r u m s a l o n g w i t h f i r s t and s e c o n d r i n s e s . 100087 P o r t a b l e t o i l e t s w e r e p r o v i d e d to r e p l a c e the o f f i c e f a c i l i t i e s s i n c e it w a s s u s p e c t e d t h a t the s e p t i c t a n k m i g h t be In the I a b o r a t o r y p i t . C o n c r e t e w a s b r o k e n In an a r e a o u t l i n e d by t e s t h o l e s w h i c h e x h i b i t e d h i g h p p m e m i s s i o n s d u r i n g a b o r i n g p r o g r a m In O c t o b e r , 1 9 8 4 . S o i l w a s e x c a v a t e d and p l a c e d a r o u n d t h e o p e n e d p i t . The s i d e w a l l s a n d f l o o r of t h e e x c a v a t i o n w e r e e x a m i n e d w i t h the FID for o r g a n i c e m i s s i o n s . R e a d i n g s a l o n g t w o s i d e w a l l s w e r e In the 7 0 0 - 9 0 0 p p m r a n g e . T h e s e w a l l s w e r e e x c a v a t e d a n d r e c h e c k e d . F i n a l l y , a pit w a s e x c a v a t e d w h i c h d i d n o t e l u c i d a t e a p p m r e a d i n g o n the F I D . T h i s pit m e a s u r e s 3 0 x 3 0 f e e t a n d 9 feet d e e p . E x c a v a t i o n r e v e a l e d t h a t a p r e v i o u s o w n e r laid m a c a d a m o v e r the e n t i r e a r e a a b o u t t w o ( 2 ) feet b e l o w t h e p r e s e n t level of the c o n c r e t e . A later o w n e r c o v e r e d t h e m a c a d a m w i t h a b o u t o n e and o n e - h a l f f e e t of s o i l a n d p o u r e d c o n c r e t e to t h e p r e s e n t l e v e l . T h e l a b o r a t o r y w a s t e s f l o w e d into a p i t w h i c h w a s a b o u t 8-9 feet d e e p . T h e b o t t o m t h r e e ( 3 ) feet w e r e f i l l e d w i t h c o b b l e . W h e n l i q u i d f i l l e d the p i t , it w o u l d f l o w i n t o a f o u r ( 4 ) inch P V C p i p e and d r a i n to a n o t h e r c o b b I e - f 1 1 1 e d pit n e a r the r e a r f e n c e . T h i s pit w a s i n v e s t i g a t e d d u r i n g O c t o b e r ( s e e p r o g r e s s r e p o r t ) . D r a i n L i n e s T w o ( 2 ) s t o r m d r a i n l i n e s w e r e e x c a v a t e d to r e p l a c e the e x i s t i n g l i n e s w h i c h w e r e d e t e r i o r a t e d and c a v i n g in at s e v e r a l l o c a t i o n s . B o t h l i n e s w e r e c o n s t r u c t e d of 5 5 - g a l l o n d r u m s w h i c h w e r e w e l d e d . E x c a v a t i o n r e v e a l e d o n e line c o n t a i n e d a s l u d g y m a t e r i a l w i t h an o i l y t e x t u r e . T h i s m a t e r i a l w a s c o l l e c t e d and p l a c e d in 5 5 - g a M o n , o p e n top d r u m s ( 1 3 t o t a l ) a n d s t o r e d u n t i l a n a l y s i s I n d i c a t e d the c o n s t i t u e n t s . D r u m s f r o m the d r a i n line w e r e p l a c e d in a c o n t a i n e r for later d i s p o s a l . N o s l u d g e or r e s i d u e w a s p r e s e n t in t h e s e c o n d d r a i n l i n e . T h e b a r r e l s from t h i s line w e r e p l a c e d in a c o n t a i n e r for later d i s p o s a l . O n e line w a s r e p l a c e d w i t h 10 inch P V C p i p e . T h e e x c a v a t i o n and r e p l a c e m e n t of e a c h line w a s d i s c u s s e d w i t h P u b l i c W o r k s as to the n e e d for an " E a r t h C h a n g e " p e r m i t . A f t e r r e v i e w and i n s p e c t i o n , P u b l i c W o r k s d i d n o t r e q u i r e a p e r m i t for rep i a c e m e n t . P r o c e s s Pit • D u r i n g t h i s f i e l d v i s i t ( J u n e 6 - 1 5 ) s a m p l e s w e r e t a k e n f r o m v a r i o u s a r e a s and s e n t to s t a t e s i d e l a b o r a t o r i e s for a n a l y s i s . T h e s e l a b o r a t o r i e s a r e i n d u s t r i a l C o r r o s i o n M a n a g e m e n t , Inc. ( I C M ) , R a n d o l p h , N e w J e r s e y and Y o r k L a b o r a t o r i e s , I n c . ( Y o r k ) , M o n r o e , C o n n e c t i c u t . D u p l i c a t e s of m o s t s a m p l e s w e r e s e n t to e a c h l a b o r a t o r y as a q u a l i t y c o n t r o l , p r o c e d u r e . 100088 T h e f o l l o w i n g s a m p l e s w e r e t a k e n L o c a t 1 o n T y,ii.e. NP. A n a .1 y s I s D r y e r S o i 1 L a b o r a t o r y P i t S o i l D r a i n L 1 n e s P r o c e s s P i t 1 I - J u n e 31 - J u l y 3 L i q u i d 2 So S 1 u d g e 9 T o l u e n e P y r 1 d I n e V o lat 1 le O r g a n i c s V o I at i I e O r g a n 1 c s P r i o r i t y P o l l u t a n t s P l u s 4 0 C o m m e n t s T w o ( 2 ) s a m p l e s to e a c h l a b o r a t o r y F o u r ( 4 ) s a m p i e s to e a c h l a b o r a t o r y I CM on 1y T w o ( 2 ) s a m p les to e a c h l a b o r a t o r y I CM on 1y ; alt s a m p l e s c o m p o s i t e d to o n e s a m p l e T h e s i t e w a s r e v i s i t e d a n d s o i l s a m p l e s w e r e t a k e n f r o m the d r y e r ( 4 ) and the l a b o r a t o r y pit ( 8 ) . T h e s a m p l e s w e r e d i v i d e d e v e n l y b e t w e e n the l a b o r a t o r i e s . T h e r e m a i n i n g six ( 6 ) b a r r e l s of t o l u e n e - c o n t a m i n a t e d s o i l w a s l o a d e d o n t o t r a y s and p l a c e d in t h e d r y e r . In a d d i t i o n , l i q u i d s a m p l e s from the p r o c e s s pit w e r e t a k e n for P r i o r i t y P o l l u t a n t s p l u s 4 0 a n a l y s i s . H o w e v e r , t h e y w e r e lost in s h i p m e n t and h a d to be r e t a k e n at a l a t e r d a t e . I I I - J u l y 16 - 19 T h e s i t e w a s r e v i s i t e d a n d f o u r ( 4 ) s a m p l e s e a c h w e r e t h e d r y e r and the l a b o r a t o r y p i t . T w o ( 2 ) s a m p l e s of s e n t to e a c h l a b o r a t o r y . P r i o r i t y P o l l u t a n t s p l u s 4 0 s a m p l e s w e r e r e t a k e n f r o m the p r o c e s s p i t . IV - A u g u s t 6 - 9 t a k e n f r o m e a c h w e r e w a t e r A d d i t i o n a l c o n d u c t e d . s a m p l i n g of t h e l a b o r a t o r y pit and d r y e r w a s A n a l y t i c a l s h e e t s for the f i r s t t h r e e ( 3 ) s i t e s a m p l i n g p e r i o d s a r e in A t t a c h m e n t E w h i c h w a s a r e q u e s t of C o n s e r v a t i o n and C u l t u r a l A f f a i r s . A n a l y t i c a l s h e e t s for the A u g u s t v i s i t a r e in A t t a c h m e n t F. Nu.T.erous s a m p l e s b e t w e e n J u n e and A u g u s t w e r e d u p l i c a t e d and s e n t to a n o t h e r l a b o r a t o r y , Y o r k L a b o r a t o r i e s D i v i s i o n . T h e s e r e s u l t s a r e in A t t a c h m e n t G. 100089 D u r i n g S e p t e m b e r , the s i t e w a s v i s i t e d and s a m p l e s of all w a s t e s t r e a m s ( c o n t a m i n a t e d a r e a s ) w e r e c o l l e c t e d for s h i p m e n t to C h e m i c a l W a s t e M a n a g e m e n t . T h i s d a t a Is r e q u i r e d by them b e f o r e they can a c c e p t w a s t e s for d i s p o s a l . T h e m a t e r i a l p r o f i l e s h e e t s for e a c h w a s t e s t r e a m a r e l n A t t a c h m e n t H . O n S e p t e m b e r 1 7 , the s i t e w a s v i s i t e d by M r . L o u i s D i g u a r d i a , U S E P A R e g i o n 1 1 . He c o l l e c t e d s a m p l e s and d i s c u s s e d the s i t e a c t i v i t i e s w i t h M r . R a y m o n d H a y s . A f t e r C h e m i c a l W a s t e M a n a g e m e n t a c c e p t e d the w a s t e s t r e a m s for d i s p o s a l , the s i t e w a s v i s i t e d d u r i n g e a r l y O c t o b e r to d r u m all m a t e r i a l s for s h i p m e n t and d i s p o s a l . A t t e m p t s w e r e m a d e to d i s p o s e of w a s h e d d r u m s locally t h r o u g h a v e r b a l r e q u e s t to A u s t i n M c o r e h e a d . He s u g g e s t e d 1 call U S E P A R e g i o n ll. T h e a n s w e r from R e g i o n II w a s to send a l e t t e r . A c t i o n t i m e w o u l d h a v e b e e n 2-3 w e e k s . T h i s w a s not p u r s u e d d u e to c o s t s . tn a d d i t i o n , as per the r e q u e s t of M r . Bob M i l o s ( B e r l e x ) , p e r m i s s i o n w a s s o u g h t by letter ( h a n d w r i t t e n , A t t a c h m e n t I) to e v a p o r a t e , p r o c e s s pit w a t e r i n s t e a d of s h i p p i n g o f f Isiand. M r . M o o r e h e a d r e s p o n d e d to the letter v e r b a l l y that t h i s w o u l d r e q u i r e c o n s i d e r a b l e time for a p p r o v a l . At t h i s s a m e t i m e , 192 d r u m s of h a z a r d o u s w a s t e w e r e p a c k e d , a n i m a n i f e s t e d to C h e m i c a l W a s t e M a n a g e m e n t for d i s p o s a l ( A t t a c h m e n t J ) . o a d e d For U . S . C u s t o m s to r e l e a s e the d r u m s h i p m e n t in L a k e C h a r l e s , L o u i s i a n a a letter with s u p p o r t i v e d o c u m e n t s w a s s e n t to M r . Carl B e c n e l l ( A t t a c h m e n t K ) , c u s t o m s b r o k e r r e t a i n e d by ICC. On N o v e m b e r 6, r e s u l t s of the s a m p l i n g by the U S E P A ( L o u i s D i g u a r d i a ) w a s r e q u e s t e d ( A t t a c h m e n t L ) . At t h i s d a t e (April 1 6 , 1 9 8 6 ) the r e p o r t is not a v a i l a b l e . A f t e r a m e e t i n g with B e r l e x In W a y n e , it w a s d e c i d e d that I r e t u r n to t h e s i t e and s a m p l e the gut for v o l a t i l e o r g a n i c s and m e t a l s ( A t t a c h m e n t M ) . A n a l y s e s I n d i c a t e the p r e s e n c e of heavy m e t a l s at s e v e r a l l o c a t i o n s . A s u b s e q u e n t EP Tox test i n d i c a t e s that the l e a c h a b l e f r a c t i o n is well b e l o w U S E P A s t a n d a r d s ( d a t a s h e e t not a v a i l a b l e for t h i s s u b m i s s i o n ) . In a d d i t i o n , v o l a t i l e o r g a n i c s w e r e n o t d e t e c t e d . It w a s d e c i d e d that I r e t u r n on M a r c h 13 to take s p l i t s a m p l e s w i t h U S H P A R e g i o n 11 p e r s o n n e l . T h e r e s u l t s of t h i s s a m p l i n g are not a v a i l a b l e at t h i s t i m e . C o r r e s p o n d e n c e c o n c e r n i n g the e x t e n t of s i t e c l e a n u p was f o r w a r d e d to M r . S i m o n , U S E P A ( A t t a c h m e n t N ) . ( A K - 8 6 1 3 4 ) 100090 ATTACHMENT A i 100091 PROGRESS Kti'UKX ISLAND C.HE.'^.ICAL COMPANY, I N C . (BERLEX) S T . C R O I X , VIRGIN ISLAN'DS ATTACHMENT / 7^1^ yc ^^^- 'I / Env iro-Scie.Tces , Inc. 19 Ccpeland Read Denville, Nev Jersey G7o5- (201} 366-6256 December, 1?S4 100092 :.*:TRODUCTICN as contracted by Berlex Laboratories, nmental study cf their Island Erviro-Sciences/ Inc. (ESI) w I.'".c. (Eerlex) to ccncuct an envirc ^ __ _ Chemical Company, Inc. (ICC) facility in St. Croix, Virain Islands. Eerlex sold the facility to Virgin Island Chemical Ccnpany, Inc. (VICC) in September, 1984. Under the contractual agreement between Eerlex and VICC, ESI is responsible for certifying that the facility is environmentally clean and free of chemical contamination. The following discussion is a summary of the ESI site investigations and their results- SITE HISTORY Eerlex accuired the nine year old facility in St. Croix when it purchased Cooper Laboratories (Cooper) in 196G. At the time purchase the facility was in a non-operational mode. Both C of oope: of the _.id the original owner were in the pharmaceuticals area __ chemical industry. Exact manufacturing processes used by the original owner cannot be documented at this time. Cooper produced Neither owner was fully operational during this time. c u i n i d i n e :iped the f a c i l i t y and o p e r a t e d for about two of i t s sf o w n e r s h i p . The f a c i l i t y produced p r i m a r i l y . r , . . . ^ . . i r . i r . r . T Z l - . . . - ^ A . . ^ . . i r . . . . . . . . . . . 3 . . - . . . . . . • . • ; . . . . . ^ ^ . . U ... . . . . U . E e r l e x revam f o u r y e a r s o cuinidine from quinine rethodolocies used produced a .rethods used elsewhere in the industry. ^ than a year prior to purchase by vicC Production was drsccntinued more expensj.ve product than newer Th! plant did fcr more when the ew< not operate SITE EVALUATION .".r. Irving Cohen of ESI initiated the evaluation program on September 11, 1984 and was replaced by Dr. Alan Kyles on September 13. The initial phase continued through S<rptember 20, 19S4. A second phase was undertaken frcm October 22 through October 31, 1584. T.he entire property was walked and scrutinized for visible surface contamination. A backhoe was utilized to open trenches in areas where contamination might be expected. Most trenches were excavated to a depth of six feet. A portable Flame Ionization Detector (FID) was used to sense volatile organic compounds on the ground surface and faces of open trenches. (The FID has a detection range of 1 to 1,000 ppm.) As the program progressed a drilling rig capable cf boring concrete and split-spoon sampling fcr soil was broucht to t-he site. 100093 Scil samples were taken from all trenched areas showing volatile crganic contamination and from bore holes at various depths. All trenches were backfilled after investigations were completed. Trench and boring locations are shown in Figures 1 and 2. RESULTS The site evaluation procedures detected four areas of ccntamination. These are: 1) along trench number 4, under concrete slab number 3; 2) between tanks numbered 8 and 9; 3) along trench number 9: and 4) under the concrete surfaced loading dock. The contaminated area located along trench 4 is shown in Figure 3. T.he contaminant had a distinct odcr of toluene and exceeded a 280 ppr. reading on the FID. However, gas chromatography sample a.-.alysis (Sample numbers S4 through S4-4 ) did not detect the presence of toluene or indicated levels of <0.2 ppm. These analyses were conducted by two separate Eerlex laboratories. (See Appendices A and E, respectively.) The time lag between sample ta.^ing and analysis (3 weeks) may account for the difference between field readings and laboratory analytical results. A three- tc four-foot wide section was removed from slab 3 to determine the extent of contamination. Inspection with the FID i.ndicated that contamination was limited to this area and does not extend or penetrate the soil under slabs 2 and 4. Depth of cc.ntamination was restricted to the first two to three feet of scil. All contaminated soil (approximately 4 cubic yards) was placed in 55 gallon drums and stored in the warehouse for eventual disposal. The pit was backfilled with clean soil. T.-.e entire area between and in front cf Tanks 8 and 9 was ccntaminated with toluene which escaped frcm Tank 8 during cleaning. Laboratory analysis indicated that Tank 8 contained a 1.4 percent solution of toluene and water and the surrounding soil ar.d gravel mixture contained 694 ppm of toluene. (See Appendix A, Samples Tank 8 and Tank 6-1.) Due to rain the prior evening and i-pending for later in the day, the area was cleaned. Soil and gravel was removed down to a depth of about one foot. At this depth a hard clay layer is present. All material including water was placed in 55 gallon arums and removed to the warehouse fcr later disposal. Sample analysis of the clay soil indicated the absence of toluene (see Appendix E, Sample Tank 8-2). 100094 When opening trench 9 behin was broken (Figure 2 ) . Imm pyridine and the FID record broken pipe was probed. Th usage. Surface water settl 280 ppm. Further excavatio the fence containing stones emissions from the pit appr discontinued for about 4 we Surface samples (Figure 2) drains to the dry river bed nunbers D-1 through D-5; se were absent of pyridine: ho pps), D-2 (507 ppm) and D-5 a quinine sulfate were pres pyridine odcr was prevalent period. d the loading dock, a ediate odor indicated ed in excess of 1,000 is pipe was dry, indie ing in the open cut ha n and line tracing lea and covered with tin cached 800 ppm. Furth eks until the return v were taken in the erod and the excavated tre e Appendix A ) . Sample wever, pyridine was pr (3,014 ppm). Quinidi ent in these samples, during the excavation 4-inch PVC line the presence of ppm when the ating no recent d a reading of d to a pit near sheeting. Vapor er excavation was isit in October, ed trench which nch (sample s D-3 and D-4 esent in D-1 (920 ne gluconate and also. A strong and sampling Upon the return visit in October the pyridine odor was not noticeable. Probing the pit and PVC pipe did not elicit a response on the FID. The pit was excavated without detection of organic vapors especially pyridine. The presence of pyridine in the above discussed area lead to additional investigations; either the drain line was broken under t.he concrete, or another source of pyridine contamination was present. Discussions with personnel who have been at the facility fcr a number of years revealed the past history for the loading deck area. Originally, laboratory drains exited from the building and wastes flowed directly to an open pit. Occassionally, during the rainy season the pit would fill with water and overflow by a swale to the dry river bed beyond the fence. Later, the pit was filled and the area concreted for use as a loading dock. It was uncertain how the laboratory drain was rerouted to the pit near t.he fence. A total of 40 borings were made in the loading dock area: 22 curing September and 18 during October. Most borings were at least 6-feet deep with a few Ibeing 8-feet deep. Table 1 shows t.he FID readings for all samples taken during September. Soil texture indicates that contaminants are confined to sandy-clay material which was apparently used for fill. Samples taken from the dense clay below the sand were relatively free of contamination. 100095 t h e s i d e w a l l s A p p a r e n t l y e x p o s u r e t o a i r T h e r a p i d v o l a t i l i t y i s shown w i t h d a t a i n T a b l e 2 . FID r e a d i n g s f o r t h e b o r e h o l e s i n S e p t e m b e r show r a t h e r h i g h c o n c e n t r a t i o n s . Upon r e t u r n i n g i n O c t o b e r n o n e of t h e s e h o l e s e x h i b i t e d v o l a t i l e s u s i n g t h e F I D . P r o b i n g t h e b o r e h o l e a n d l o o s i n g w o u l d r e s u l t i n a s m a l l FID r e s p o n s e . A p p a r e n t l y ^ a l l o w s f o r o x i d a t i o n o r e s c a p e of t h e c o n t a m i n a n t s . T h e a d d i t i o n a l b o r i n g s made i n O c t o b e r f u r t h e r d e l i n e a t e d t h e c o n t a m i n a t i o n and p r o v i d e d i n f o r m a t i o n on t h e l a b o r a t o r y d r a i n r o u t i n g u n d e r t h e c o n c r e t e . I d e a s w e r e c o n f i r m e d u s i n g f l u o r e s c e i n d y e . A p p a r e n t l y t h e l a b o r a t o r y w a s t e s flow i n t o a p i t f i l l e d w i t h s t o n e n e a r b o r i n g s 20 and 20A. Once t h e p i t f i l l s , l i q u i d o v e r f l o w s t o a " t a n k " n e a r b o r i n g 1 6 . T h i s " t a n k " maybe t h e s e p t i c t a n k w h i c h s e r v i c e s r e s t r o o m s i n t h e o f f i c e p o r t i o n of t.he f a c i l i t y . Once t h i s f i l l s t h e n f l o w c o n t i n u e s o u t t o t h e p i t n e a r t h e f e n c e . S a m p l e s w e r e s e l e c t e d from t h e s e new b o r i n g s and i m m e d i a t e l y a n a l y z e d . The r e s u l t s a r e p r e s e n t e d i n Appendix D. A n a l y s e s s h o w s t h e p r e s e n c e of a t l e a s t 690 p p b t o l u e n e : 4 3 , 0 0 0 ppb p y r i d i n e : 6 4 , 0 0 0 d i p h e n y l m e t h a n o n e : a n d 600 t o t a l x y l e n e . A d d i t i o n a l m a t e r i a l s were p r e s e n t a t l o w e r c o n c e n t r a t i o n s . O i l e n d g r e a s e a n a l y s i s i n d i c a t e d c o n c e n t r a t i o n s up t o 1,500 ppm. PROPOSED CLEANUP PROCEDURES ESI i s p r o p o s i n g t o c l e a n t h e c o n t a m i n a t e d s o i l on s i t e i n s t e a d of s o i l r e m o v e d t o a c e r t i f i e d l a n d f i l l w h i c h i s p r o b a b l y l o c a t e d on t h e m a i n l a n d . We h a v e c o n s i d e r e d n u m e r o u s a l t e r n a t i v e s i n c l u d i n g c n - i s l a n d i n c i n e r a t i o n a t t h e H e s s R e f i n e r y . O n - s i t e d e c o n t a m i n a t i o n a p p e a r s n o t o n l y f e a s i b l e b u t c o s t e f f e c t i v e . 100096 The contaminated been cleaned up a drums. ESI propo equipment and ove emptied onto pans temperature tolue contaminated soil it to the site, site for soil dec temporary air emi areas around Tank 8 and at the end of slab 3 have nd the material is stored on site in 55 gallon s e s to decontaminate the soil using air drying ns on site. Drummed-contaminated soil would be and placed in the ovens. By raising the ne can be evaporated leaving non-toluene This soil would be analyzed before returning VICC officers will allow the use of equipment on ontamination. ESI will probably require a ssion permit from the EPA. ESI proposes to treat the contaminated area behind the loading dock while the soil is in place. This method will involve the following sequence: 1) All laboratory waste flows will be rerouted to a self contained unit thus preventing new contaminants and liquid from entering the area. 2) Portable toilets will be available to prevent the discharge of wastes and water to the area. 3) A shelter will be constructed over the area to prevent rainfall and runoff from entering the area. 4) All overlying concrete will be removed to expose the contaminated soil, laboratory drains, p:t, and septic tank. 5) A berm will be constructed around the -e.^posed soil to prevent inflow of water from rainfal.'.. These preliminary steps will allow for vaporization of volatile r.aterials to the atmosphere- Periodically, the soil will be turned using a backhoe to expose underlying soii; layers. Samples will be taken every 4-5 days to determine the rate of volatile release and confirm the success of the methodology employed. Discussions with Dr. Medhat Reiser of Nepara, Inc. (914-782-8171) indicate that pyridine will disappear upon exposure to air. He stated that although it is on the hazardous materials list it is biodegradeable in about 21 days if exposed to air and not in contact with water. The above precautions and methodology should allow for the biodegradation of pyridine. Also, other volatiles should disappear using this method. If this method is successful, the area will be rehabilitated to its prior condition. Acceptable ir.ethods for laboratory waste and septic discharges will be incorporated in the new design. ESI realizes that this method of treatment will require a temporary air emissions permit. Also, a tempor.3ry discharge permit maybe required if unexpected heavy rainfall should flood the pit area. Both permits will be requested from the EPA prior to initiation of the treatment method. 100097 ESI held a meeting with Mr. Alfred Williams and Mr. Austin Mcorehead of the Department of Conservation and Cultural Affairs, St. Croix (809-773-0565). The contents of this report were discussed in its entirety and they consider the proposed methods tc be suitable for the situation at the facility. They suggested that all work be coordinated through EPA Region II. 100098 TABLE 1 FID READINGS (ppm) FOR ISLAND CHEMICAL COMPANY (BERLEX) -1/ Boring No . 1 Foot Dent h 3 Feet Deoth 4 Feet D e o t h • 6 Feet D e o t h 8 Fee: Deoc h 1 2 3 U 5 6 7 8 9 10 1 1 12 13 \i* 15 16 17 18 19* 2 0 * * 2 1 * * * 22 B B B B 10 0 1 10 55 60 90 200 0 0 10 100 100 10 45 30 20 300 110 15 10 10 0 30 150 110 10 10 0 0 0 100 80 10 35 10 65 200 n / a 15 10 0 0 110 30 110 10 10 0 0 25 100 80 10 40 30 X 100 n/a 10 10 10 0 20 15 10 160 10 55 0 10 20 140 45 10 300 40 80 X SP 120 0 0 40 10 80 45 210 45 20 0 10 20 250 100 20 3 00 20 45 X SP 310 35 10 60 0 15 200 150 15 0 10 30 10 90 60 0 110 30 45 X SP 100 30 20 10 45 100 45 80 0 0 0 10 40 100 65 10 320 10 40 S? 130 0 20 0 25 120 15 60 0 0 0 0 10 15 100 100 15 160 10 15 20 SP 15 10 40 90 10 45 0 0 0 0 10 20 300 100 40 200 10 45 15 SP lOOC 680 0 0 30 40 0 10 0 0 25 25 0 10 0 0 150 55 0 10 15 B 10 10 10 \_l Sanpled during September. * X = No Sample **SP = Septic Pit ***At the 4 Feet Depth, Letter B should read 1000 plus 100099 TABLE 2 FID READING FOR BORINGS Dm Borina 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 60 35 40 270 40 550 0 0 350 200 280 240 1000+ 110 110 130 750 650 45 100100 TABLE 3 Inventory Items which have been at ISLAND CHEMICAL COMP.^Y. INC. (BERLEX) Quinine Sulfate Quinidinone Quinidine Base Quinidine Gluconate Quinacr Quinine Bisulfate THF (tetrahydrofuran) Toluene Pyridine (Karl Fisher Reagent) Isopropanol Sodium Chloride Ethyl Alcohol Benzvlphenone Chloroform Methylene Chloride Cinchona Bark 20% Dibah in Toluene Sodium Hydroxide (caustic soda) pellets and solution Gluccno-A -Lactone Liquid Ammonia Muriatic Acid Sulfate Acid Sodium Hypochlori"te Solution So'iium Bicarbonate Magnesium Sulfate Flourenone Potassium-t-Butoxide Acetone Calcium Hypochloride (H-T-H) Tetaric Acid Variquat Acetic Acid Soda Ash Gluconofin Carbon Black Kenite 7C0 Potassium lodo Platinate Butylated Hydroxy Toluene Ethylene Glycol Methanol Charcoal Castor Wax 100101 c y, Lh'w ex : OD CO i CU TANK FARM D I-IDA© ©:^ * 1@ (g) 0-! A i C c r t a ^ P . A 0 o crucrATnc nz \ 1.X5Q..J K (1. U«lT iMO Li ^"^«- C l l tTCi. Tr»wC» D ~^ i TRENCHES 3 1-12 50' _; SCALE r\.kiHr CMreiaHcr 100102 DRY RIVER BED O o O FIGURE 2 BORING LOCATIONS SCALE : f - 8- WAREHOUSE 2IA ' 2 1 LABORATORY DRAIN \ \ LOADING DOCK > o 21 > o -c FENCE -X X- FIGURE 3 v/yyyyyyy/yyy.i^ BACK FILLED TRENCH CONTAMINATION AREA 100104 FiGURE 4 P R C ^ ' ' . £ S FOR FID READINGS y j PROFILE A - A ' BORING NUMBER - 16 M - :-iir—•--!JB- -A7 .-JL. 4©— 190i- ^eO-—: i ^ f—36— DEPTH -<4- 20- -40— • A Q / i : . ' • — - 2 6 0 - — - 3 0 ^ -386—'• 3 3 ^ -te- : i ^- ' '. 1 1 '•• i ^ i ! j : !- ^ i •- y . • 1 i 1 ; ; ; • A B O 1 i : 1 i : • 1 1 : • n r 1 ! • i 1 • 1 0 1 ; ' 1 •. '• '• '. '• i • 1 • t • • : i • — ; — — . — • '; F ^ O f \ L ' E ' ~ B ' - ' 6 ^ ' BORVFTG' N'J 13 • Ifl • r* * 1 0 3D " D E P T H . "J" " *r ' ! M&i^R" I 13 ->«n "nn ,.. i l - n I ; i. ; i 1 i : i : : 1 ; ; ; 4- n " p - - — — - • ' . • L ^ . _ . : / E ' ' 70 ' 1 ; : ; ! '. 1 • : ! : • i ; . • • ' • . \ : ' : i ; '•. ; ' . • ' ' • - . •• \ •• : : 1 • ; : ! : : : ; : . ; • " •• ^ : " ; i i • " ! ; • "1 ; • I • ' ' : ' • • '' •• PROFILE C - C BORIMG NUMBER \ i i : : 1 : . a 2 : 5 : >*> DEPTH - ; : t ; : . • ; ! • I i ': : : ! • . : ; ' • • : ; : : ; . : ': . i • '. 1 " T ' . - - l i e — i - -"- — ; 1 •• ^ ' •W—:— : • ^ 1 i '. i i : ! 1 j i i : i . i ; — • — i ! ! j i i J : : : . 1 . i : 1 : 1 i ^ 1 1 • ; : : ! : • i 1 : • i ! • i 1 X I SEE FIGURZ 3 100105 FIGURE 5 PROFILE LOCATIONS WAREHOUSE C 11 B ° i o 12 .18. 19 LOADING 15 13 16 17 A' ' 2 1 LABORATORY DRAIN^ •20 22 DOCK 100106 APPENDIX A 100107 tCM/tOLI r K . To: From: Date: Subject: f i i v ^ \ » i II,. Laboratories Inc. Memorandum J. Beck D.W. McKennon October 15, 1984 ISLAND CHEMICAL ENVIRONMENTAL SAMPLES On 9/17/84, we received several samples from Irv Cohen of Enviro Sciences Inc. for analysis for various organic components. We agreed to examine the samples for volatile organics via GC techniques, and then for nonvolatile organics like quinidine using HPLC techniques. Our investigation is complete, and data is attached. DISCUSSION I. GC ANALYSIS Quantitable amounts of toluene were found in samples T8-1 and Tank-8. Also, quantitable amounts of pyridine were found in samples D-1, D-2, and D-5. Qualitatively, the chromatograms were examined for additional peaks. Samples S4-2, D-5, T8-1, and T8-2 contain an unknown peak eluting between the pyridine and toluene peak. Tank-8 had an unidentifiable peak which eluted shortly after toluene. II. HPLC Quantitable amounts of quinidine and/or quinine were found in D-1, D-2, D-5, T8-1, Tank-8, Tank-4, and Tank-9. Qualitatively, the HPLC chromatograms in many cases have some unidentified early eluting peaks which are not related to quinidine, quinine, or any of the other cinchona alkaloids. DEPOSITION OF SAMPLES On October 10, 1984, all samples were given to Al Kyles who is a representative of Enviro Sciences Inc. Note: Due to the extreme rush to analyze these samples, limited, precautions were taken to protect either GC or LC columns. Total replacement cost for columns is approximately $960. ^MZZZZ^-^i^z^^ 100108 D.W. McKennon DWM/hms Attachment cc: R, R. R. Willis Wohl Milos I.-Cohen/Enviro Sciences Inc G.C. ANALYSTS* SAMPLE IDENTIFICATION S4-1 S4-2 S4-3 S4-4 S4-surface D-1 D-2 D-3 D-4 D-5 -8-1 TS-2 Tank- Tank- Tank- Tank- •8 -4 -9 -7 ^4 Sample ^•4-High Cone. TOLUENE N/D N/D N/D N/D N/D N/D N/D N/D N/D N/D 694 ppm N/D 13,880 ppm - - - - - PYRIDINE N/D N/D N/D N/D N/D 920 ppm 507 ppm N/D N/D 3014 ppm N/D N/D N/D - - - - - L . C . ANALYSIS** VTTnrvr Q U I N I N E SULFATE QUINIDINE GLUCONATE N/D N/D N/D N/D N/D 452 ppm 96 ppm N/D N/D 170 ppm 274 ppm 47 ppm 4050 ppm 8227 ppm N/D N/D N/D N/D N/D N/D N/D N/D N/D 82 ppm N/D N/D N/D N/D 101 ppm N/D 1521 ppm 2594 ppm 354 ppm N/D N/D N/D N/D = None Detected *G.C. Reference Bk. 83-9, pp. 75-79, EGO •^L.C. Reference Bk. 83-11, pp. 22-30, MSM 100109 APPENDIX B 100110 liiiniy *Linumm0anomiimiii' / Laboratories Inc. To: W. C. Lumma From: R. A . Wohl Date: October 22, 1984 Subject: Soil Samoles from Island Chemical Comoanv Memorandum cc: A. Kyles/Enviro Scie.nces D. W. McKennon* R. Milos* A. Rudzik* Enclosed please find our Analytical Report (G. Rudd to W. B. Caldwell, dated October 19, 1984) on the three soil samples S4-1, 1' H-22 and 3' H-21. These three soil samples, originating from Island Chemical Company were received from A. Kyles of Enviro Sciences, Inc. on Oct. 12, 1984. Wohl RAW:cj E n c l o s u r e * 100111 • \ « — y I - Laboratories Inc. Memorandum To: Dr. W. B. Caldwell cc: W. Lumr.a R. Wohl From: G. Rudd Date: October 19, 1984 Suojsct; Analysis of Soil Samples from Island Chemical by - Headsoace•Gas - Chromatography Three soil samples received 10/15/84 from the Island Chemical site were examined by headspace gas chromatography for the prese.nce of toluene and pyridine. T.he results are listed in the table below. Chromatograms of the three samples are attached. The large pea.ks observed at t.he beginning of each chromatographic run are artifacts of the headsoace experiment. Samole S4-1 H-22 1 K-21 3 A B Toluene, ppm <0.2 none detected-^ none detected Pyridine, ocm <C0.2 none detected 1.2 (1) Limit of detection ca^. 0.1 ppm Quantitation was performed by standard addition (Ippm) to the sample and comparison to the unspi.ked si=..^ple. Chromatography Conditions A. Toluene Column: 6' x 2mm glass packed with 80/100 Carbooack C/ 0.1% SP-1000 Te.Tiperatures: Injector - 250°C Detector - 275^C Oven - 1 min (§ 100°C; 200°C & 16°C/min Carrier: Nitroge.n, 22 ml/min Detector: FID B. Pyridine Column: 4' x 2mm glass packed wit.h. 60/80 Carbopack 3/ 4% Carbowax 20.M/0.8% KOK 100112 -2- Temperatures: Injector - 250°C Detector - 275°C Oven - 130°C isothermal Carrier: Helium, 30 ml/min Decector: FID Assav Procedure 5.0 grams of sample were placed in a 50 ml serum bottle that was sealed with a Teflon lined septtun. The sealed serum bcttle containing the sam^ple was equilibrated at 90°C for 1-1.5 hours. With a previously heated gas tight syringe, 0.5 ml of t.he headspace volume from the serxim bottle was withdrawn a.-.d quickly injected into the gas chromatograph. McMeal, T. and Breder, C.V., JAOAC, 65, 184-187 (1982). Xc zebook Reference GI-l-1-143-146 G, I. Rudd 100113 " -iHnuimiH. S •Cl. • • '•ill. • i l i i - l l ' '.y-K -i..uiimitiinutMmitmimii' To: From: Date: Subject: o o o UJ a •X. Laboratories Inc. - 3 - Memorandum i:.:? _ SIX>A of- r^ifi^pttci. f^^i / . l 6 ^iDfr\ <r>.CS. 1C.S9 10.e« . 10.5: RT in minutes SAMPLE: l.lSFrM SPIK INJECTED AT 18:47:15 CN OCT 17. 1984 Heth: STD39 Ra>r, R2£c47 Prcc: P3S247 o 03 Ol C- (Q C UJ o o (j)' i 2'*"" I.'i. Ctz^rritr • /V/^ ^ Z ' 2 ^ fW^rM.n RT in Blnutss SAMPLE: S4-i*2 Heth: ST033 INJECTED AT 19:21:42 ON OCT 17. 1SS4 Ra»r. flaS249 Proc: P2924g 1 0 0 1 1 4 . ^ ^ • • ^ -••nitimimtj ..tMnummjTm.'1/mniMfi To: From: Date: Subject: CM a o C- fO o ca o UJ n ^ Laboratories Inc. -H " io.:iL Memorandum '5'CC^ C<- rstix.i.'spKiL T r Z Z T ' ^ 3 3 /'.'•'£» (ff 'f- 2.1^'^ 'A- 4.:0 RT in minutes SAMPLE; 3'B H21*2 INJECTED AT 19:08:50 CN OCT 17. 1SB4 Meth: STD29 Rax: R3£24a Ppoc: P2S24a ru O) c C Lu O o o s RT in minutes ? CsiK/^.. •BbfiCXO CAThoauO. C/O. 1% fP-OCT i ^ ' < 2rY\rv\ 1.4 fZ'f) . Zo.n,o '• ^J•^ a.^ J2roL/rw>»> " j r ^ . . : d.;: SAMPLE: IA H-C2 Heth: STD39 INJECTED AT IB: 41: £5 ON OCT 17. 1984 Raw: R3S242 . Proc: P29242 I 100115 ^w^ * • ' • % • ^ ^ • • h ."SBiHI "ffmaiutm,. B 'Stl.KU 'I'nem.mwm.t^.ui'- L a b o r a t o r f e s Inc. - S ~ To: From: Date: Subject: cn c IO o cs UJ C3 Memorandum 3.7? _ 3.:< _ B..:9L /ndiVvtf RT in minutes SAHPLL- Hetn: GC42 INJECTED AT 9: OB: 35 ON OCT 19. 1934 Raw: R42aB7 Proc: P42E57 o rrj c o o a Z3 3 . : : y 5.."3 .. i ? . ; /J^c^'^'^ Zoo6 A£wc9^c£ S^'^fsitf S**-' (;^'kx~»n • Carho^ci. Blf^o 0^rszc>..^t i? v^n • iSo :! UA:>''^' dvi«'' ,,.w> (< VP»") U ( ^ '/»p~) RT in minutes SAMPLE: Hetn: GC42 L.S. INJECTED AT 8: 2B: 00 ON OCT 19. 1984 Raw: R42EB2 Proc: P42B52 100116 •itHmuiirj, .I'mifiy To: From; Date: Subject: Laboratories Inc. " ^ ' Memorandum o er} 03 (O o tn o c ID c LU C3 O LU 1:2 •.:.9T 9.2< ^ f^^' U ^ ^ ' b Colu^ty l ' « 2 r . « Co.r'oofs.itcy.t h f o ^arfca-xf 2 0 / ^ / : .'S-fa t.0>^ .r: :.a: RT in minutes SAMPLE: Heth: EC42 INJECTED AT 8: 41: 40 ON OCT 19. 1934 Ra>r. R42S53 Proc: P42a53 ' . ? TOr-^ J o . ^ ^ <:<?H 100117 RT in minutes SAMPLE: Het.h: GC42 INJECTED AT 8: 47: 45 ON OCT 19. 1934 Raw: fl42E64 Proc: P^2=54 APPENDIX C 100118 ( (AT'yy/^^^j \^*0^0e0e^>^ 1% COPEL»*0 RO.. DEMVllXE. N€W JERSEY 07834 CHAIN OF CUSTODY RECORD I n s t a l l a t i o n : ^ ^ c c < /&SS, ^ ^ ^ , .Zr<.yA/o ^rv€yrt/ez<. da. . ^ c . JlZ ^^a^J( l///fs/^ /Zc»fOS S u r v e y N o . : r-l a E • iQ a V3 : c /s ^'£ rs S t a t i o n L o c a t i o n 2<s <tr /s <I><S 2 / R e l i n q u i s h e d b y : ( S i g n . ) R e l i n q u i s h e d b y : ( S i g n . ) R e . : . i n q u i s h e d b y : ( S i g n . ) R e l i n q u i s h e d b y : ( S i g n . ) D i s p a t c h e d b y : ( S i g n . ) D a t e / T i m e .Method of S h i p m e n t : S a m p l e r s : ( S i g n a t u r e ) D a t e yr-yfJrfir' // // // Time Sample Type Uomp . R e c e i v e d b y : ( S i g n . ) R e c e i v e d b y : ( S i g n . ) R e c e i v e d b y : ( S i g n . ) R e c ' d by L a b o r a t o r y f o r f i e l d a n a l y s i s ( S i g n . ) -IK "x L a b o r a t o r y A c ^ ^ G r a b X / / / No. of Contalnere / / / / D a t e / T i m e D a t e / T i m e D a t e / T i n e D a t e / T i m e D a t e / T i m e 100119 ; ; - t MFAOSPACF Ai •i'lVZA^'^ arr'.Ki'.; uanr/oaBteoater iabori ^rv INDUSTRIAL CORROSION MANAGEMENT INCORPORATED ns? m m lo RANOOIPH NF^T jt RSIT 07869 701 SB* 0330 V O L A T I L E O R G . ^ M C S BV PURGE AKD TR,^P GC/MS Compounde d e t e c t e d i n p a r t e per m i l l i o n ( m i l i g v a m a / k i l o g v a m s jOry Wgt.Basis SAMPLE SOURCE: ENVIRO SCIENCES SAMPLE ID: i' B Mole #20 Kcport Dale: Ociobcr 9. '08't Lab. * }h(>2k SAMPLE DATE: Sept. 18-19, 198'< TAKE.X BV: Alan l.Kvler -AT LAB DATE 9/27/8«» O O NJ O CHLOROMETHANE BROMOMETHANE DICHLORODIFLUOROMETHANE VI.WL CHLORIDE CHLOROETHA.NE METHVLE.NE CHLORIDE ACETO.VE T N I C I I L O R O F L U O R O M E T H A . X E . , 1 ,]-D1CHL0R0ETHVLE.\E 1 ,1-D1CHL0R0ETHA.\E t-1.2-DlCHL0R0ETHVLE\E. CHLOROFOR.M FKEO.N 115 , 1,2-DICHLOROETHANE t-BUTVL METHVL ETHER... 1 ,1 ,1-TR]CHL0R0ETHANE.. CARBON TETRACHLORIDE... BROMODICHLOROMETHANE... 1,2-DICHLOROPROPANE c-1,3-DICHLOROPROPENE t-l,5-DICHLOROPR0PENE TCE (TRICHLOROETHYLENE).. DlBRO^IOCHL01'.CMETiLANE BENZENE DlISOPROPYL ETHER Z-CHLOROETHVLVINVL ETHER. HEXANE BROMOFOR.M 1,1,2,2-TETRACHLOROETHANE PCE (TETRACHLOROETHVLENE) HEPTANE TOLUENE .. CHLOROBENZENE •. ETHYLBENZENE 0. 16 For the above listed volatile pollutants, nothing detected at O.Olppmsensitivity level X Other peaks detected. Fluorethyne ^ 0. *» 5 ; 2-me t hy I propano 1 0.20; pentane O.OI; LT = Less than, GT=Greater than, ND=Not detected '•'NOTE: Possibly from plastic bag H E A D S P A C E -'•:'l •i']^.\'A^° driKkiy; ujiev/waetejater Labora. y INDUSTRIAL CORROSION MANAGEMENT INCORPORATED us? ROUit 10 RANDOLPH. NC* jCRSfT 07869 ?oi 58.0330 V O L A T I L E O R G A N I C S BV PURGE AND TR.AP GC/MS Compounds d e t e c t e d in p a r t e per m i l l i o n (miligrams/kilograma )Ory Wgt.Basis S.AMPLE SOURCE: ENVIRO SCIENCES SAMPLE ID: i, • Q nole H ^ Report Date: October 9, 198'« Lab. n 3'«625 S.AMPLE DATE: Sept. 18-19, 198'* TAKEN BV: Alan L.Kyler AT LAB DATE 9/27/8'« I-* o o lO CHLOROMETHANE BR0M0.^1ETHANE DICHLORODIFLUOROMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE TRICHLOROFLUORO.NIE THANE. 1,1-DICHLOROETHYLENE... 1,1-DICHLOROETHANE t-l,2-DICHL0R0ETHVLENE. CHL0ROFOR.M FREON 115 1,2-DICHLOROETHANE t-BUTVL METHVL ETHER... 1,1,1-TRICHLOROETHANE.. CARBON TETRACHLORIDE BROMODICHLOROMETHANE... 1 ,2-DICHLOROPROPANE c-1,5-DICHLOROPROPENE t-l,5-DICHL0R0PR0PENE TCE (TRICHLOROETHYLENE).. DI EROMOCHLOP.OMETH.ANE BENZENE DIISOPROPYL ETHER 2-CHLOROETHVLVINVL ETHER. HEXANE BRO.MOFOR.M , 1,1,2,2-TETRACHLOROETHANE PCE (TETR.ACHLOROETHVLENE) HEPTANE TOLUENE CHLOROBENZENE.. . .: ETHYLBENZENE J^ For the above listed volatile pollutants, notlung detected at 0. 01 ppnsensi t ivity level _X Other peaks detected. Fluorethyne •'0.38; 2-methyl propanol 0.16 LT = Less than, GT^Gieater than, ND=Not detected ••'•NOTE: Possibly from plastic bag '"t'i -i1\\'A^° criKKv.: ii3ier/waeteoater Labot^, ,y INDUSTRIAL CORROSION MANAGEMENT ' 1'^^?5P^CE_ lU-port Date: October 9, 198'« INCORPORATED Lab. n 3,^626 us? ROUU )0 RM-ooiPH NfW JCRSIY 07S69 701S84 0330 V O L A T I L E ORGANICS BV PURGE AND TR.AP GC/MS Compounde d e t e c t e d i n p a r t e p e r m i l l i o n fmt Zigrama/ki iograma )Ory Wgt .Basi s S.AMPLE S O U R C E : ENVIRO SCIENCES SAMPLE ID: 3- D-Mole I M SAMPLE D A T E : S e p t . 18-19. 198'< TAKEN BY: Alan L.Kyler AT LAB DATE: 9/27/B'( O O to to CHLOROMETHANE BROMOMETHANE DICHLORODIFLUOROMETHANE \INYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE TR1CHLOROFLUOR0.^1ETHANE. , 1,1-DICHLOROETHYLENE 1,1-DICHLOROETHANE t-l,2-DICHLOROETHYLENE., CHLOROFOR.M FREON 115 1,2-DICHLOROETHANE t-BUTVL METHYL ETHER 1,1,1-TRICHLOROETHANE. . , CARBON TETRACHLORIDE BROMODICHLOROMETH.ANE. . . 1 .2-DICH LOROPROPANE c-l,5-DICHL0R0PR0PENE t-l,5-DICIiL0R0PR0PENE TCE (TRICHLOROETHYLENE).. DIBROMOCHLOROMETHANE BENZENE DIISOPROPYL ETHER 2-CHLOROETHYLVINVL ETHER. HEXANE BROMOFOR.M 1,1,2,2-TETRACHLOROETHANE PCE (TETR.ACHLOROETHVLENE) HEPTANE TOLUENE CHLOROBENZENE ; ETHYLBENZENE J< For the above listed volatile p o l l u t a n t s , notliing detected at O.Olppmsensitivity level J( Otlier peaks d e t e c t e d , f i nnrp.i hynp, ''< Q . l l : 2-methyl propanol 0.16 LT = Less t h a n , G T = G i e a t e r than, ND=Not detected ANOTE: Possibly from plastic bag ^ w-r..:^- . e m : tea ^irn.rut.: uater/uaetewater Labor jru INDUSTRIAL CORROSION MANAGEMENT ' l-'^^?^?^^^- Report Date: October 9, 198't INCORPORATED Lab. i ^ken ns? ROUU 10 RANDOiPH NfW jfRSfY o?B69 ?oi 584 0330 V O L A T I L E O R G A N I C S BV PURGE AND T R A P G C / M S Compounds d e t e c t e d in p a r t s per m i l l i o n (miligrame/kilograms)Ory Vgt.iasi S.AMPLE SOURCE: ENVIRO SCIENCES SAMPLE ID: /^ . Q Hole 21 SAMPLE DATE: Sept. 18-19, 198'* TAKEN BY: Alan L.Kyler AT LAB DATE: 9/2 7/8'< H o o to LO CHLOROMETHANE BROMOMETHANE DICHLORODIFLUOROMETHANE VINYL CHLORIDE CHLOROETHANE MEniYLENE CHLORIDE , ACETONE TRICHLOROFLUOROMETHANE. , 1,1-DICHLOROETHYLENE I,1-DICHLOROETHANE t-l,2-DICHLOROETHYLENE., CHLOROFOR.M FREON 115 1,2-DICHLOROETHANE , t-BUTVL METHYL ETHER 1 ,1 ,1-TRICllLOROETHANE. . , CARBON TETRACHLORIDE BRO.^IODICHLOROMETH.ANE. . . 1 ,2-DICIILOROPROPANE c-1,5-DICHLOROPROPENE t-l,5-DlCHLOROPROPENE TCE (TRICHLOROETHYLENE).. DIBROMOCHLOROMETHANE BENZENE DIISOPROPYL ETHER 2-CIILOROETHYLVINVL ETHER. HEXANE BROMOFOR.M 1,1,2,2-TETRACHLOROETHANE PCE (TETRACHLOROETHYLENE) HEPTANE TOLUENE CHLOROBENZENE ; ETHYLBENZENE For the above listed volatile pollutants, noiinng detected at o.Olppm sensi t ivi ty level. _X Otlier peaks detected, fluorethyne- 0.06; 2-methyl propanol 0.^)7. 2-me t hy I - I-hep t ene 0.21; pyr I d I ne 0.02 \ LT = Less than, GT=Creater than, ND=Not detected. NOTE :-''Pos s i b 1 y from plastic bag. APPENDIX D 100124 November 12, 1984 30850-145 ENVIRO-SCIENCES, INC. 19 Copeland Road Denville, New Jersey 07834 Artention: Mr. Irv Cohen PURPOSE Nine (9) soil samples were submitted to York Laboratories for determination of toluene and pyridine on a quantitative basis. 0~her compounds found in the samples were also indentified and are reported on a semi-quantitative basis. The samples were also analyzed for oil and grease. METHODOLOGIES The samples were analyzed for toluene using the dynamic headspace Gas Chromatograph/Mass Spectrometry method in accordance with Chemical Analysis of Sediments and Elutriate Testing, EPA 1979. A Tekmar Model LSC-3 Purge and Trap iiiterfaced with an HP 5995C GC/MS/DS were used ' for the analysis. Tbe samples were analyzed for pyridine and oil and grease in accordance with EPA/CE-81-1 Procedures for Handling and Chemi- cal Analysis of Sediments and Water Samples, May 1981. An HP 5S95C GC/MS/DS was used for the pyridine analysis. RESULTS The results are listed in the following tables. Prepared by: "") C ^ - J ^^ S|^.,^ Gail 0. Sprio Senior. Chemist Approved by GDS/JCC/mz CJhilet'X;htemist 100125 YWC. INC • 2C0 Mof ,rc- 'ni-ior-- - ^'|••"•• - TABLE 1 ENVIRO-SCIENCES, INC. TOLUENE AND PYRIDINE RESULTS Sample Identification 20 Septic 20 A-2' 21 A-2' 21 A-4' 25 - 2' 27 - 2' 32 - 2' 35 - 4' 36 - 2' (Auger) Toluene ug/kg (pDb) 540 690 15 43 210 16 15 8 7 Pyridi ne ug/kg rppb) <1,000 <1 ,000 <1,000 <1,000 13,000 26,000 43 ,000 <1 .000 <1,000 100126 i'vC" Sample Identification 20 Septic (Auger) 20 A - 2' 21 A - 2 21 A - 4 2 5 - 2 2 7 - 2 ' 3 2 - 2 ' 35 - 4' 36 - 2' TABLE 2 ENVIRO-SCIENCES, INC. Compounds Found 1 ,1-methylene bis-benzene diphenyl methanone methylene chloride chloroform benzene methylene chloride chloroform benzene ethyl benzene total xylenes methylene chloride chloroform trichloroethylene benzene tetrachloroethylene ethyl benzene methylene chloride chloroform benzene methylene choride chloroform benzene methylene chloride chloroform benzene methylene chloride chloroform 1,1,1-trichloroethane benzene methylene chloride chloroform 1,1 ,1-trichloroethane benzene methylene chloride chloroform benzene C o n c e n t r a t i o n * 8,400 64,000 <5 12 <5 <5 5 <5 68 600 <5 <5 <5 <5 <5 7 <5 <5 <5 <5 5 <5 <5 19 <5 <5 <5 <5 <5 <5 13 11 <5 <5 <5 <5 1.5) 0.5) 2 . 3 ) 0.9) 2.4) 3.8) 0.8) 0.6) 0.9) 2 . 2 ) 2 . 6 ) 0 . 4 ) 1.7) 0.4) 2 . 2 ) 0.6) 4 . 4 ) 4 . 2 ) 0 . 8 ) 0 . 8 ) 2 . 4 ) 0 . 4 ) 1.6) 1-4) 0.2) • R e s u l t s a r e r e p o r t e d on a s e m i - q u a n t i t a t i v e b a s i s . 1 0 0 1 2 7 wc,INC • 2r,r, r/,.-,'rr.r ATTACHMENT B 100128 ATTACHMENT B nnno m sasfKis mc. 19 COPELAND RO.. DENVILLE. NEW JERSEY 07834 (201)366-6256 Mr. Robert Harris USEPA Region II 26 Federal Plaza New York, NY 10007 Dear Mr. Harris: Enclosed is the addendum to the progress report submitted to Mr. Conrad Simon In December. I hope that the information therein will answer the questions and concerns expressed by you during our numerous telephone conversations. Please review this information as soon as you can. If you have any question, please contact me at 201-366-6256. I sincerely appreciate your help during the past several months. Very truly yours, ENVIRO-SCIENCES, INC. Alan Kyles, Ph.D. Vice President AK/po Enclosure 100129 ^I^J)»W¥0 5Ct£nC£5irK. ^ ^ V ^ ^ W 19 COPELAND RD.. DENVILLE. NEW JERSEY 07834 ^ % % ' m N ^ (201) 366-6256 A p r i l 2, 1985 Mr. Conrad Simon USEPA Region II 26 Federal Plaza New York. NY 10007 Reference: Island Chemical Company, Inc.. St. Croix Virgin Islands Dear Mr. Simon: Er.closed is an addendum to the progress report submitted to you In December for Island Chemical Company, Inc. (Berlex), St. Croix, Virgin Islands. E-viro Sciences, Inc. (ESI) has prepared this addendum as the result of numerous telephone conversations with Mr. Robert Harris of your office. The enclosure addresses questions which were raised by Mr. Harris in his efforts to fully u-derstand ESI's efforts to cleanup toluene and pyridine spills at the facility. It is our hope that the addendum will help your staff to grant ESI the necessary permits to pursue the cleanup in an orderly and timely manner. If you have any questions concerning the addendum or desire a meeting with ESI, please contact me immediately. '«" Very truly yours, ENVIRO-SCIENCES, INC. <Z^-^yZ/p^^' Alan L. Kyles, Ph.D. Vice President ALK/po Enclosure cc: Mr. Robert Harris, USEPA Region II Mr. Robert Milos, Berlex Mr. Frank Curtis, Berlex 100130 1 3 3 3 1 3 1 f I I .1 I I i ADDENDUM TO PROGRESS REPORT ISLAND CHEMICAL COMP.'iNY. INC. (BERLEX) ST. CROIX. VIRGIN ISLANDS Enviro-Sciences, Inc. 19 Copeland Road Denville, New Jersey 07834 (201) 366-6256 A p r i l A, 1985 100131 V W > 3 d l KdACUi 1---V ADDENDUM PROGRESS REPORT U-J---.: Islanc3 Chemical Comoanv, • Inc. ( Berlex ) m n St.Croix, Virain Islands Prcaress Report Summary BackaroDnc3' Information - * — — — • • - • - — Tl^.e facility is located on the island's south side and near the west e.nd (Figure 1) at Latitucae 17 42*26" and Longitude 64 47*25". It is situated approximately 6.1 miles equidistant from the two major towns: Frederiksted to the west and Christiansted to the east. Facility access is via Route 66 which traverses the island east and west. As seen in Figure 2, it is about 0-5 miles north of Alexander Hamilton Airport. Elevation is approximately 40 feet mean sea level- An intermittant stream which originates near the north side of the island and empties i.nto the Caribbean Sea on the south side borders the north side of the property. Flow occurs generally during the wet season (September through December) and only during heavy runoff (Table 1 ) . The lower portion of the drainage lying beyond the facility is flowing and is utilized aa sewage outfall Wind direction is frora the east and southeast (trade winds) with velocities ranging from 5-15 miles per hour. Closest residences are located about 0.1 miles east of and upwind of the facility. As shown in Figure 3, the facility is situated on soils of the Coamo Series. These are gently sloping, well drained soils which occur as alluvial fans and terraces. They formed in sediments derived from volcanic and limestone rocks- They range in texture frora clay to sand. The upper layer is typically grayish-brown clay loam which is uncferlain by numerous layers of yellowish-brown clay and clay loam. Permeability is slow to moderate, and the shrink-swell potential is 100132 n r f f a moderate. These soils are commonly associated with San Anton, Glynn and Fraternidad soils. potable water for distribution is supplied from both ground water (30 percent) and desalted water (70 percent). However, the island is very dependent on storage (cisterns) to cope with water demands. Most private dwellings have their own roof/cistern systems for water supply- There are eight major well fields on St. Croix and they are located as shown in Figure 4. The quality is generally poor due to mineralization and oil contamination from pump lubrication. These contaminants are often pumped into the supply system. The location of the three closest well fields in relation to the facility are shown in Figure 5. The three fields contain 14 of the 37 total well field wells. Field•Study Results The original field investigation detected contamination in four locations (Figure 6 ) : 1) along trench number 4, under concrete slab number 3; 2) between tanks numbered 8 and 9; 3) along trench number 9: and 4) under the concrete surfaced loading dock. Analysis indicated that areas 1 and 2 above were primarily ccntaminated with toluene. As stated earlier, the toluene ccntaminated areas were cleaned and the contaminated soil placed in drums (25) and stored in the facility's warehouse. The pyridine contamination is still in place. Based upon analytical results (see Progress Report) the pounds of contamination were calculated as follows: Scil•in"Drums 3 a I 1 Contamination•Concentration 10,000 ppm 1,000 ppm x X Soil•(Tons) 4.5 Tons = 99 lbs. 9.0 Tons =19;81bs; Soil Under Concrete-Pad ( 60-x'35-=-f oof area) Ccntamination Concentration 9000 ppb 3C0 ppb CleanuD Procedures X X Soil (Tons) 6,000 tons = 119 lbs. Pyridine 6,000 tons = 4 lbs. Toluene ! ESI proposes to clean the contaminated soil using the following 100133 1 1 f 1 I I 1 i 1 methodology: Toluene contaminated soil will be placed on trays in a dryer which is at the facility. The location is shown in Figure 7. Prior to beginning the drying operation, calculations will be made using the and stack diameter to insure During the handling of contaminated soil, protective clothing and an appropriate breathing apparatus will be used by all personnel (t.he breat.hing apparatus used is discussed later). The pyridine contaminated area will require rerouting existing laboratory discharges to a self-contained unit (probably 250-500 gallon stainless steel vessel) and providing portable toilets in place of existing restroom facilities. These changes will eliminate sources of water which are presently entering the contaminated area and would prevent the degradation of pyridine. The pyridine contaminated area will be prepared as follows: 1. A structure will be built over the area which will be exposed to prevent soil saturation from rainfall. 2. The concrete will be cut and removed using a backhoe. The concrete will be hauled to a landfill, or used to stabilize the bank along the dry river bed. The Department of Public Works will be contacted for permission to do the latter. 3. The soil will be tilled using a backhoe at 2 - 3 day intervals. Soil turning will allow exposure of the contaminated soil to ambient air- The release of pyridine and minor amounts of toluene to the ambient air cannot be controlled. However, the interval between the soil turning can be lengthened to decrease the release rate. 100134 «-o-««,«c Samples will be taken at the beginning of the cleanup operation and continue at weekly intervals until acceptable pyridine contamination levels are reached. It is expected that this level will approach a very low level rather quickly, since half-life is about seven days- During all phases of cleanup, workers will be provided protective clothing and a breathing apparatus. As mentioned earlier, sampling will occur on a weekly basis beginning when the area is fully exposed. Samples will be taken at 3 to 4 locations from three different levels: surface, mid-depth and bottom. In addition, one sample will be taken from the clay layer underlaying the contaminated area. All samples will be sent state-side to a certified laboratory for analysis. When the pyridine level has decreased to zero or an acceptable level, the area will be restored and resurfaced according to the owner's requirements. The existing septic system will be used as is, replaced in Che same location or relocated elsewhere on the property. All laboratory effluent will be containerized until plans are made by the owner for disposal. Disposal procedures under consideration include sewerage, pretreatment and sewerage, or disposal in accordance with St. Croix Island authoratative guidelines. Safety Procedures To ensure the health of all personnel involved in the cleanup procedures, disposable protective clothing, including shoe coverings and hats will be provided. The breathing apparatus will be NIOSH approved masks with filters for organic vapors, acid gases and dust. The Scott part numbers and descriptions are listed below: Respirator (half face) Cartridge Dust Filter Dust Filter Holder TC-23C-174 642-OA 642-F 642-FR Monitoring The program will be monitored by weekly sampling and analysis. Samples will be taken by ESI personnel or qualified persons presently cn site. Proiect Timina The cleanup of pyridine using the above described degradation procedures requires that water is prevented from entering the exposed area. This will be facilitated by rerouting of laboratory effluent, supplying portable toilets, and construction of an overhead shelter. This concept is further enhanced by conducting cleanup operations during May and June when rainfall is minimal. It is expected that the pyridine contamination can be cleaned in 30 - 45 days. The drying of 100135 Kunajnc We would appreciate your timely review of this request and a determination as to the disposal location of each item listed above. I will contact you next week as to your progress. If you have any question, please call me collect at 919/499-5182. Very truly yours/ ENVIRO-SCIENCES, INC. 'X iZkzy Alan L. Kyles, PhD. Vice President AK/po (AK-8 5225) cc: Mr. Greg Rhymers Dept. Conservation & Cultural Affairs P.O. Box 4399 S t . T h o m a s , U . S . V . l . 00801 100136 • I.KDUSTRIAL CORROSION MANAGEMENT !NC0RPCPJ2,TED 1152 ROUTE ;C. .RANDOLPH, NEW JERSEY 07869 '201 53<03;0 m L CLIENT: ENVIRO SCIENCES. INC SAMPLE SOURCE: ICC (BERLEX). PKOJECT !iata Sheet 1 NJD.EP Cartified Drinking Water/ Wastewater Laboratory ID i*14116 REPORT DATE: August 15.1985 LAB If 42882 SAMPLE ID: Drain Line Ifl SA."^LE DATE: 6/7/85 SAMJ-'LED SY: A. Kyles SOIL SAMPLE LABORATORY ANALYSIS REPORT AT LAB DATE: 6/18/85 Idencificacion of Black Soil; Paranecer Result ienzene Ethylbenzene M-Xylene ' 0,?-Xylene 0.10 0.25 0.33 0.27 Sample has "Toluene like or solvent odor. UNKNCU-N PE.-UCS ?..T. 6.89 ac 40 mg/kg R.I.30.81 -c 2 mg/kg All results reported in mg/kg. Ve thank you for this opportunity to serve you. If you have any questions, please do not hesitate co call. nroUSTRLAL CORROSION MANAGEMENT, INC. ET/jmg •cl. ^^pLess Than Edwin Tichenor Vice President 100137 M O O W 00 :ffl INDUSTRIAL CORROSION MANAGEMENT INCORPORATED \M1 IWUII 10. MMOMID. WW XKU.10'MI 101 M« 0)10 CLIENT; ENVIRO SCIENCE - ICC (Berlex) NJDEP Certified Drinlcing Uater/Wastewat4^P^ Laboratory ID IIUIS SOIL SAMPLE REPORT DATE; July 31. 1985 LAB f /|?861 SAMPLE ID; Drain Line SI SAMPLE DATE: blllQb SAMPLED BY; A. Kyles VOLATILE ORGANICS BY PURGE AND TRAP By GC BTX/HEADSPACE ^AT LAB DATE; 8/18/85 Compounds detected In parts per million (ml 11 igrams/lcilograms) dry weight basis. CHLOROMETHANE • BROMOMETHANE • VINYL CHLORIDE - CHLOROETHANE • METHYLENE CHLORIDE ACETONE • 1,1-DICHLOROETHYLENE - 1,1-DICHLOROETHANE **-• t-l,2-DICHLOROETHYLENE CHLOROFORM 1,2-DICHLOROETHANE t-BUTYL METHYL ETHER -• 1,1,1-TRICHLOROETHANE - CARBON TETRACHLORIDE -• BROMODICHLOROMETHANE -• 1,2-DICHLOROPROPANE --- 1,240 M! 68 10 "^Compounds co-elute (could be either material) LT«Less Than, GT-Greater Than dwb-Dry Weight Basis. X-Not Detected rC-1,3-DICHL0R0PR0PENE t-I,3-DICHL0ROPR0PENE — TCE (TRICHLOROETHYLENE) X_ ^rl,l,2-TRICHLOROETHANE ^DIBROMOCHLOROMETHANE BENZENE X_ DiISOPROPYL ETHER X 2-CHLOROETHYLViNYL ETHER X_ BROMOFORM X_ 1,1,2,2-TETRACHLOROETHANE X_ PCE (TETRACHLOROETHYLENE X. TOLUENE CHLOROBENZENE ETHYLBENZENE - M-XYLENE • *rO-XYLENE P-XYLENE 5.600 **Tetrahydrofuran ( Phosgene also elute at this point. Numerical results are calculated for I,l-Dichloroethane only. For the above listed Volatile Pollutants, nothing detected at a sensitivity level of: _X ^Unknown peaks detected (retention time,estImated amount); Xylenes 16; 10 unknown hydrocarbon peaks ranging from 2 to 10 tng/kg. _ _ _ _ _ _ ^ NOTE;Compound Identification Is based upon retention time matches with specific known standards. Confirmation of anaiysis using GC/MS is required to positively identify any material and/or amount detected. 11 rt Dl n n n in Tichcftor, Vice Presf^Jm^ H O O l-» OJ vo Pi INDUSTRIAL CORROSION SOIL SAMPLE MANAGEMENT L'j 1 I I INCORPORATED ))•>> KMU to MNtXHnt. WW JIHUT OrMI NI U4<I}N CLIENT; ENVIRO SCIENCE ICC (Berlex) NJDEP Certified Drinking Water/Wastewal Laboratory ID IUII6 REPORT DATE; July 31.1985 LAB I /.2889 _ _ _ _ ^ SAMPLE ID: Dryer SAMPLE DATE: 6/14/85 SAMPLED BY: A. Kylea VOLATILE ORGANICS BY PURGE AND TRAP By GC BTX/HEADSPACE _AT LAB DATE; 6/18/85 Compounds detected in parts per million (milligrams/kilograms) dry weight basis. CHLOROMETHANE BROMOMETHANE • VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE 1,1-DICHLOROETHYLENE - 1 ,1-DICHLOROETHANE **-• t-l,2-DICHLOROETHYLENE CHLOROFORM 1,2-DICHLOROETHANE t-BUTYL METHYL ETHER -- 1,1,1-TRICHLOROETHANE - CARBON TETRACHLORIDE -- BROMODICHLOROMETHANE - 1,2-DICHLOROPROPANE --- *[ c-l,3-DICHL0R0PR0PENE t-l,3-DICHL0R0PR0PENE "' TCE (TRICHLOROETHYLENE)- ^,I,1,2-TRICHLOROETHANE „ ^DI BROMOCHLOROMETHANE "' ' " ' — 4.0 340 4.2 ^Compounds co-elute (could be either material) LT-Less Than, GT-Greater Than dwb-Dry Weight Basis. X-Not Detected BENZENE • DlISOPROPYL ETHER 2-CHLOROETHYLVINYL ETHER • BROMOFORM --T 1,1,2,2-TETRACHLOROETHANE PCE (TETRACHLOROETHYLENE • TOLUENE • CHLOROBENZENE ETHYLBENZENE M-XYLENE *rO-XYLENE P-XYLENE 6.6 A. 000 16.1 ILL 15.1 A^Tetrahydrofuran & Phosgene also elute at this point. Numerical results are calculated for I,1-Dlchloroethane only. For the above listed Volatile Pollutants, nothing detected at a sensitivity level of; 1 mg/kg dwb. Unknown peaks detected (retention t ime,est imated amount): • NOTE:Compound identification Is based upon retention time matches with specific known standards. Confirmation of analysis using GC/HS Is required to positively identify any material and/or amount detected. INDUSJ J? rf m n n u> (-> o o l - » o i INDUSTRIAL CORROSION MANAGEMENT INCORPORATED lit; Rouif 10. lUNoarH wA j(HS(r oiut nuti-oix NJDEP Certified Drinking Water/Uastewater Laboratory ID n h W d REPORT OATE:_ LAB H i^'il'^1 AuniMt n.l9H5 CLIENT: CNVIRO SCIENCES,INC. - ICC (BERLEX) PROJECT SAMPLE DATE: 7/1/85 SAMPLED BY: Enviro Sciences SAMPLE ID; Dryer AT LAB DATE: 7/11/85 VOLATILE ORGANICS BY PURGE AND TRAP GAS CHROMATOGRAPHY/ HEADSPACE Compounds detected in parts per million (milligrams/kilograms) dry weight basis CHLOROMETHANE BROMOMETHANE , VINYL CHLORIDE • CHLOROETHANE • METHYLENE CHLORIDE ACETONE • 1 ,1-DICHLOROETHYLENE -• 1,1-DICHLOROETHANE ** • t-l,2-DICHLOROETHYLENE CHLOROFORM 1 ,2-DICHLOROETHANE t-BUTYL METHYL ETHER -- 1 ,1,1-TRICHLOROETHANE - CARBON TETRACHLORIDE -- BROMODICHLOROMETHANE -- M *[ 1,2-DICHLOROPROPANE c-1 ,3-DICHLOROPROPENE t-l,3-DICHLOROPROPENE TCE (TRICHLOROETHYLENE) -- 1,1,2-TRICHLOROETHANE DIBROMOCHLOROMETHANE BENZENE DlISOPROPYL ETHER 2-CHLOROETHYLVINYL ETHER - BROMOFORM 1,1,2,2-TETRACHLOROETHANE • PCE ( TETRACHLOROETHYLENE) TOLUENE • CHLOROBENZENE • ETHYLBENZENE • JL sua JL ••Compounds co-elute (could be either material) LT"Les5 Than dwb«Dry Weight Basis. GT=Greater Than X-Not Detected **Tetrahydrofuran & Phosgene also elute at this point. Numerical results are caluclated for 1,l-Dichloroethane only. For the above listed Volatile Pollutants, nothing detected at a sensitivity level of mg/kg dwb. n If _X Unknown peaks detected (retention time, estimated amount) numerous other hydrocarbon peaks, 0.02 to 0.1 mn/kg NOTE: Compound identification is based upon retention time matches with specific known standards. Confirmation of analysis using GC/MS is required to positively EJ/ identify any material and/or amount detected. INDUSTRIAL CORROSION MGMT.,INC. r. Vice President H O O M M u INDUSTRIAL CORROSION . MANAGEMENT INCORPORATED NJDEP Certified Drinking Water/Wastewater Laboratory ID n k W S i M K U n tc. IWNOOini. WW XRSET 071(9 20l!l4-0)]0 REPORT OATE; LAB # August 13.1985 A3752 Dryer CLIENT; ENVIRO SCIENCES,INC. - ICC (BERLEX) PROJECT SAMPLE ID; SAMPLE DATE: 7/1/85 SAMPLED BY: Enviro Sciences ^AT LAB DATE; 7/11/85 VOLATILE ORGANICS BY PURGE AND TRAP GAS CHROMATOGRAPHY/HEADSPACE Compounds detected in parts per million (milligrams/kilograms) dry weight basis CHLOROMETHANE BROMOMETHANE- VINYL CHLORIDE • CHLOROETHANE • METHYLENE CHLORIDE ACETONE • 1,1-DICHLOROETHYLENE - 1,1-DICHLOROETHANE ** • t-l,2-DICHLOROETHYLENE CHLOROFORM 1,2-DICHLOROETHANE t-BUTYL METHYL ETHER -- 1,1,1-TRICHLOROETHANE - CARBON TETRACHLORIDE — BROMODICHLOROMETHANE -- .2.JL *( *I 1,2-DICHLOROPROPANE c-l,3-DlCHL0R0PR0PENE t-i ,3-DICHLOROPROPENE TCE (TRICHLOROETHYLENE) — 1,1,2-TRICHLOROETHANE DIBROMOCHLOROMETHANE BENZENE DlISOPROPYL ETHER 2-CHLOROETHYLVINYL ETHER - BROMOFORM • 1,1,2,2-TETRACHLOROETHANE • PCE ( TETRACHLOROETHYLENE)- TOLUENE • CHLOROBENZENE - ETHYLBENZENE • JLui. ••'Compounds co-elute (could be either material) LT-Less Than dwb-Dry Weight Basis. GT-Greater Than X-Not Detected Ai^Tetrahydrofuran & Phosgene also elute at this point. Numerical results are caluclated for 1,l-Dichloroethane only. For the above listed Volatile Pollutants, nothing detected at a sensitivity level of J( Unknown peaks detected (retention time, estimated amount) 34.07 g 15 mg/kg mg/kg dwb. NOTE; Compound identification is based upon retention time matches with specific known standards. Confirmation of analysis using GC/MS is required to positively EJ/ identify any material and/or amount detected. INDUSTRIAL CORROSION MGMT.,iNC. n n rt /in Tichenor, Vice President • toluene ladened soils will be ongoing during this time period. Summarv Over 6,000 tons (estimated) of soil has to be cleansed of about 245 pounds of hazardous materials (125 lbs- of toluene; 120 lbs. of pyridine). ESI proposes to clean the soil on site since proper equipment is available, the materials are conducive to on site cleanup, and the total amount is rather small (245 lbs.). Release of these materials to ambient air will not have an adverse effect on nearby residence (0.1 miles away) since the release rate will be low, 5 - 15 mile per hour winds are normally present, and nearby residents are upwind from the facility. Safety precautions will be employed during all phases of the operation. It is the contention of Berlex and ESI that the above described cleanup procedures are the most cost effective and efficient methods which can be utilzed. Literature Sources Consulted Black, Crow, and Eidsness, Inc. 1976. A Water Management Plan for St, Croix, U.S. Virgin Islands. Project No. 540-72-51. Department of Conservation and Cultural Affairs. 1983. Comprehensive Water Resources Management Plan for the U.S. Virgin Islands. Environmental Research and Technology, Inc. 1984. The Land Treatability of Appendix VIII Constituents Present in Petroleum Industry Wastes. API Publication 4379. Washington, D.C. 1983. Land Treatment Practices in the Petroleum Industry. American Petroleum Institute, Washington, D.C. Soil Conservation Service. 1970. Soil Survey: Virgin Islands of the United States. USDA. Washington, D.C. 100142 TABLE I TE.MPERATURE AND PRECIPITATION [Data from Alexander Hamilton Field, St. Croix] 3 1 3 a a Month January February March . April 1 May ' June July August September-- October November December Year Temperature Average daily maximum •F. 83 83 84 86 86 88 88 89 88 88 86 84 86 Average daily minimusi "F. 70 70 -1 73 74 76 76 76 75 75 73 72 73 Average maximum ... r . 86 36 66 88 89 90 90 91 91 90 89 j87 92 Average minimum •F. 65 66 66 68 70 71 71 72 71 70 68 ^67 Precipitation Average total In. 2.23 2.19 1.73 2.83 4.31 3.10 3.51 4.58 6.65 5.45 4.65 3.34 44.57 One year in 10 will have-- Less than-- In. 0.50 .44 .40 .55 .60 .58 .80 1.20 2.20 1.60 1.20 1.00 34.00 More than-- In. 7.2 5.8 4.6 7.6 8.2 6.0 6.6 8.8 11.0 10.2 9.0 8.6 53.8 Average number of days with more than one-tenth of an inch of rainfall 5 6 . 4 6 8 9 8 9 10 8 9 9 91 Average annual highest temperature. Average annual lowest ternperature. 100143 FIGURE 1 FACILITY LOCATION MAP 5.000 10.000 FEET FACILITY LOCATION H O o SOURCE: COMPREHENSIVE WATER RESOURCES MANAGEMENT P L A N FOR THE UNITED STATES VIRGIN I S L A N D S . 1983. V: ; ».^,^ •, '• -...•„ \ > ^-i ' ' . ' ' '• - K ' • ' ' - i ' -' " J e t " ' ! - " ' • ZSZ) V-TTT',' i J / \ ^ J (xli va I'A», O U • I ritt;». Z VT^- ^ ^'Cs •^:i^v;--.r r r - y i % - • \ /~-'r_.v.v.- B i i \ i * t •x ••: i»" • V*' *' ' ^ « • ' B'«inl«t>tm Old Work ;• '' \ / .b . \ \ • - : ;-r^?>U. 1> y^i'»y-' \ ' VbM —"^ ^y^ifcli ; — - [ . B"_^ . • • r ^z: :; \ at .tinir—j T./ • ~ ~ li—..^—: -v.- — l/E^AAf-y^E E\^A^'>\Z--'Z'''EZ^ \.Z • iy.A-^\ ID ^-—\ o l - ^ _ • ^ ^ ^ 1 ' •' AdvMltun \ \ % .^•••-^Tl <r\yTi J ib3;ii:%\ 'i""4i^> S " ZxmAz' "'EzZyT^^^^ ..J-Zzz^r~-^H.[ cT^vP ,:...„'v^-V V "..::^5''^'v>>^v-:-^^;-A -/i I 1--:^^- y y , / \ ..::.y \ ,i ^i A--- ' * r ' ^ — - • • " ' I ' V ^l '^—' Z U . y-AM:)^^"-- Cz> • z \ ' ^ ' :A \A H'' ' "S - -y .EZ z ~z^ V ...~^ 'h ' % 0 V .:^~.^:<7 y . y C:3 •rlo'<^* . ^ /2 C o o H FIGURE 3 SOILS R N F. £ . . . . « . , . . . . . . . . . . . , . . . . . . . I - ' « « » •..., il Z . . . . . . . SOUnCE: SOIL SURVEY: VIHGIN ISLANDS OF THE UNITED STATES . 1970. USDA - SCS. ;.#S^;i;^-^-;;:;fMV/':7r"i-.'"-x \ •Z^-zEzi'.z^Z-^. \AEA''AzE!^z"yzm • •.-P-K.-y^/)) ^ ^•'Zrf^Z- Z--^.'y^Zr ^ . \ •.•.-••.W ^ (\ I =•' 'K IV..:N f-^ , -• - V V-f" - - I'^.^^:/^v;:^'%....••-»•,: J^^-^^^JVTTT^JM -li'^ • sii v*^'**" >"..>.•• •. ••V.:k A ) -. -. y y y — \ 'r^~^z%^^^yztz'"'^p^ - 'E. vy:iyyi:^'yz^y~^'>y- r-fzyr- -v fi-N IVsWV-'^-t • v;>^".--.;/-•^•••. ' - -^i-^JZ^'- ^ - y - \ \ •• V ^y^y^Z^^b^-^^-^^^'^:A'''-yi.^^ .. ••.-=•'-.-- l^kM^Nf r •r/^zZ:A'y ^z^^iAClS A<:/.-^^'E,^ ^ : ; | •y, '~y-A>yE'yz i • r '•^. -^-^'-3 . 3uot GMcn ^ : i l ..;:; ^ •. , Muis«u»iri f" r_"^' .^Mounuia •'.3 . 3uit GMc«n 'Y ' I - - " * ' " ' .. ' : ' ^ o " - ^ ^ *• I - T ; - , V. i ' •I:H-,.-.I'...'} •- •MC'i. cx> i -'J* H O O H I I v.::ori;z ^ FACILIT. LOT PLAN SHOWING AREAS OF CONTAMINATION CONCRETE PADDING ± n 7 6 4 2 1 T 3 " TT an cm CO. OD CZD T A N K F A R M wmmm LOADING DOCK^ft'.;^?^,-'^, •m.-z^ri'j.ii^.-i OKTCI kKtk k l * . c r i M p . COOLIMC i m t A C Z . T * - c s A i c n t l A « -•- * - P M.TCC. / • L O C . ' / * a U«iT AMD - ^ " • % « c-XD L J e n o t Q "7 • / * ^ — - IV C t M C C A r n c / , f i t . c r u M t r TRENCHES 3 1-12 50' 100' r\~»iHT CHTZkucr ISLAND CHEMICAL PLOT PLAN SCALE 100149 CONCRETE PADDING V n 7 6^ 5 4 3 2 1 CUD CUD an cm CJD •CZD o O D ^C!D TANK FARM FENCED STORAGE LOADING DOCK w * a t « « n u t c i~ i__i-rxi r 1 rri^ C A / . A « . £ A AfC C O M R COOLIMC ^ o i c x t * D ., (CACTO« - , , i«.«A cruccAinc iO'O'Oio,,,^. —. ^OOO CAL (^ vmexcz. T»««5 DRYER •+• CtWTtirUiC > A-O M.TII. / BLOC. ^ / CiA<« t t A c T n v . e.n. uMiT AHO Li «""«• e ~7 • TRENCHES I.. ^ 1-12 0 50' 100 -=^-H- ^ A K T eMTCJk»4Cf ISLAND CHE>v1ICAL PLOT PLAN SCALE 100150 ATTACHMENT 100151 ATTACHMENT C .;iRo • KicncEJ inc. %<^W<^|^%« 19 COPEUVND RD., DENVILLE. NEW JERSEY 07834 ^ ^ ^ ^ ^ ^ (201)366-6256 Mav 1 5 , 1985 Mr. Robert Harris U.S.E.P.A. Region II 26 Federal Plaza NY, NY 10007 Re : Island Chemical Co. (Berlex) St. Croix, U.S.V.l. Dear Mr. Harris: A" As per our telephone communication on May 9, 1985, Enviro-Sciences, Inc. (ESI) will begin the cleanup of pyridine and toluene contamination at Island Chemica^l Co., U.S.V.l. This cleanup will commence on June 6 and be conducted as described in documents submitted to you in December, 1984 (Progress Report Island Chemical Company, Inc. St. Croix Virgin Islands) and April 4 ;Addendum to Progress Report...). I r.ave briefed Mr. Carlos O'Neal in San Juan as to our plans and will forward to him the above documents. In addition, these same Gccuments will be sent to Mr. Austin Moorhead of the Conservation and Cultural Affairs office in St. Croix. ESI will take all samples which will be sent with a chain of c'jstody to independent laboratories stateside for analysis. All samples will be handled in accordance with U.S. Department of Agriculture permits which are in the possession of the laboratories. ESI will adhere to the restrictions of the permits when shipping soil samples. Attempts will be made to isolate all contamination (especially pyridine odor) to the site. If odor is excessive after concrete re:noval , release of contamination from the exposed area will be daripened using plastic sheeting. However, ESI does not think that excessive odor release will be a problem. 100152 ATTACHMENT D 100153 AITACHMENT D ^cnvmoBlKicnaiinc. ^ M ^ S ^ y W 19 COPELAND RD., DENVILLE. NEW JERSEY 07834 (201)366^256 May 7 , 1985 Mr. Robert Harris U.S.E.P.A. Region II Room 1000 26 Federal Plaza New York, NY 10007 Reference; Island Chemical Co., St. Croix, U.S.V.l. Dear Mr. Harris: Enclosed is information concerning the manifesting of hazardous material at Island Chemical Co. when operations ceased end prior to its sale by Berlex to Virgin Island Chemical Co. Included are eight (8) manifests. In addition, there is an explanation as to why activities at the facility would classify it as a small generator. We are anticipating a meeting in the immediate future with USEPA staff members to discuss this project. If you have any questions, call me at 201-366-6256. Very truly yours, EKVIRO-SCIENCES, INC. Alan L. Kyle's, Ph.D. Vice President ALK/po (AK-8531) Enclosure cc: Mr. Robert Milos r/- Mr. Frank Curtis ^ Ray Willis, Ph.D. 100154 I a p p r e c i a t e your continual a t t e n t i o n to t h i s project over the past months and w i l l keep you informed as to our progress. Very t r u l y yours, ENVIRO-SCIENCES, INC. ^ • < ^ ; Alan L. Kyles, Ph.D. Vice President ALK/po (AK-8554) cc: Bob Milos Frank Curtis Ray Willes, PhD. 100155 H O O cn o^ 1.1 •f tti»e* Imi u nrt i l l b b cnM*0NwrAHM or i . / « t o (ii;o tNVinoNMENTAl OUALMV BOAHD HAZARDOUS WAgfE MANIFEST II oocuMiNT 10 3 2 2 ^ r. 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ONWEALttI 0» rUlKTO H, O ENVlnONMENTAl OUAUTY BOARD HAIARDOUS WASTE MANIfEST H O O H cn •~j / t V / l n c e r » o r a t a d — «» r r « U It « V I . T r a l l t r K a r l n a T r a n i p e r t C o r p e r t t l o n OOCUMtl i n wo<a f 8 0 f ) n B - } } 0 0 ( 8 0 9 ) 7 2 1 - 1 3 1 ) I c U C i a n d < « P u c t t o K l c o T r a n i p e r t * D i a i • t l a v o n n Z o n a P o r t u a r i a , P u a r t e N u a v o , I a n J u a n , P u a r l e m f t n f l * t . 1 < « M U « a e « F « M r w i « « i ' n I f l l M d C h c n l c a t o f P . « . , I n c . ( • O f ) ? 9 2 - 7 9 f 9 R i c o ( 8 0 9 ) 8 ) « - l 0 9 0 t n « M « t i i K « . ) l . n l R h u a y 9 2 t H a n a t i , P u e r t o l U n • HOW ( M t rwo i M « i * w n R t oaf • • m w n v i a f i i fut « • i « i t « M « at ap*ao^n m u t r w a a s • • • • « « • • na i»iiMa>HtiitotuM(ii f m n * «t H I » TotutHt nq 1 1 • 1 I f » » a i NaMao c u l t na». ttquld WMMa I J 9 * •0 a ail MMann k i a a s i 1 I . I . . 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I tur y u u u u II t O i t r a m t f i (M I'.-, I M l_Li_ h . l l . l l . t n r u i M a H e i M B i t i a u c i « a i M a u o M C a « t a M a i t t H r t O T i i « « a w < a t M O i a w r n « M m j n i a « i t i m a * M n a i i i O i a « i w B M ^ m •« M l Mi>l la M u a M i i n O I I M A« •«w««(V»>(yJ*>vi( •! AtflMVMkMt •< It•>*••>• <*«• a l I'a *>4 *4 CaHMMHM* W P a K* • n i * tf>«««.4 M^tswt WM^ii*«*> • • t>«N*«<« i M t ^ K« KXI rrtjI.I.M (MMttMliaWI H f . a * ! * ^ n i » * Wf>*'-vt'M<.«|<r^i*M«*t>l<l>« aaii pi^pfa '»*' mp o#J iaaoi*aariai« i l ' ^ ' fiCW i;!utinr.«iii l*P1ti|naM.»uBitt D*.| HdnfS l|Ba«) fM| ptMCaaima h.Z-A'^^- lZ<Jf..3/f iC- ,. l!LiULiii_c_m:'.Mi-'.: ' 'yyyy-J:^]_:t^y'lczL yAz^Z<AXkuL i M k i ' M M a n a I i-(.ii>iiii . \.^t*tOfs tfc> .-H««n »• twj i M V i t i * | l . Vb I *...,H«*«....^..« I ^-^it -^ M i l I I I lai^'.rV"*)**^ l l ' . ^ t l V ^ ),,»•, ik.ilkh.>>«iMw*<i< uip L ^ iL;. •-iJ '.A.^ S'. r a i s i M « > i i O V U M a i i r 9 t a t rata<ttMO<*f««ai •<rt«ai|««tttMtMt*<**<Mllt*aaiHi»wi«i aailiNC a« «atO>l i«a»-iar>'i*«:i*>Miti «i n t n a v * " * * ' ^ lAdii'xiJn'- J. M n ntin>*» Docuumi ittsjiilS r • Cv. i M O N W l A l T t l 0 1 f i l l RTO .iICO I N V I R O N M t N T A l Q U A I I I V HOARO HALAROOUS WASTE MANIFEST niN.irMIKI ND f II I r 06 l l l a n d Chcwirol t n . , I ' . ' . imil) 77I1-J7IH1 j ^ , t , | « I X l I K I I I U - n r l l . l r l i i ^ . S>. I t . . ! ' . . l l . S . »lr.)W. | " ^ " J ; ^ li*»i.mni ..» ~ T'i"''"' I t n l U t •*!lll'«_"i'"T?.'' CotliotnU... _ | (nill) 111 1)11 riiiZ.^^. ~ *• ' ~ I n l n C t i t . l i , r.HTllii n i r . i . . . • • I . v : . , '. • l r i n ; ^ . . . i l i - OIn/ T^ i:?m.\ / . . . 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LL. \A- • '••'- -'•''VEZ.nr(.'7^'./.^...\'' \ , Z''\Z'Z', y/<Am.Z<. iZzi.ut Al i'...i.i.^.i I >^ii-' i!-."^' "VJ • • • - • • • * y - • • - - - — V—} • • • • ( , ' * ; " " , " " " " • " • — • ~ ^^^r o -——i:;:^:^ 5 " " Ll-L'Jll'JIii'.llj _9iL.4fcii: tl'.H • I I MP l ' j * U i i iS i.\i/^.:.^y^,- y, "zyy-'z'i^l.^^\ /Z^-JZ<.:r.-s-z.,. -jfT^iy/A- t/yfyykj/v/M •:^/y/^y L- I ! ; ' I L_.: L L o o Ul ! -SAi ,'/<^..^./ 1. ! I O O H Ol O t f i KT A : ^ I ' I * " ' / C » l ' ' I..11 CO. ^ O N W f A l T M Of P l l f R T O I . . t o I N V I R O N M C N T A l O U A I I I V DOARO HArAROOUS WASTE MANIFEST OKUUIKI n » • IC 0) . i t t r n v t i l»l»ncl e i . t » l c » l C o . , I n c . (eu») M B - l l O T m i9r.u t»l»le l y l . [»t«l» BethlehCT, 51. Crol», U.S, virgin l»l«m)!i w«^.««n* m t " ~ 1*5',.' I r . l l t r H » r l n t I m n t p o r t Coipor»Uon | (807) 7 1 1 - m ) • I I MMMItl t a l l d i v i d e . T u e r l o Rico tuavH.ia M l I r i n e p o r l e Plot <mi')> Tll-lm I t f i . r p l V i > m l » , T u g r l o Huevo, St»» Junn. Tuarlo Ulco IMItlMai. l.OMCI •• . rmmt fvnMpiaiir»>ii Inlmwl C h w l f l of P . H . , I n c . (liny) ll'*4-l(W0 « • . 5 1 , lllif'm.Y I 1 , H o n o l l , Puerto Hlco | v | l | D | T | l ) | ' ' | t | > , I . O | < i ' k l l P l T l O . n . t . * . « . } . > . ! [r,n,D,;iii,o,>,i,«,»,),. |l-,B|l)|0,7,n,3|»,»i 7,1,1 • MOW 1M» imr tuairwnu i t 10 f onoit. IM out m laiiowoo i i l/rwrwil WM W ^ i — M l»ll MWiti ootlMtvl of a KO"* nm. TMO tuairoonu «« 10 . I i i i o » a > e - - J . - » > i i iMiriainooi CilMI l o l u t t i e nr) f Ion. l l q i i l r l w ftUM«it 179a l O M 1. f « lui-iS-lii Ml vatsvni* 1 I'l't'l'l L.r.'j 1.... i I I . M I l l M . I .M.I i;..r — I.I I. u. I I L J LLL I I-LJLI aw • n. h«J 1,1 LJ U LJ UJ rren ••I ICItt LJ U U U Ll li Li=iJ L_Li aa aoi •••« la • M*iMii'iai « «. v^«»'« •*»4N«>i fl ** #••»»-«• •> fc*>i«^^«> a I If a » L'a;i * i . . ^,.:^—:n.^r- f / Jerome Ti:^lw>>«lq ^ nnt P r e s l d m l TUkiroaiiaaft'l rT»an« !• * . »*H •!•* k*«>H«|t iMswtw •**• I III , n | ) | llu«tfMiiaitn ) Mjj ^nyi ty* J-^J' S C « »|1H|1|0|5|I|7, im(ii| amrii eai ^ ^ ^ ' 1<>IIJ lajl i£li . . lVi'1',»i°i.'i^i'i''i''i> ua IP* tip I . tMAVaanaaa I tn.a*iuat ltM^(A«i*M^tw^r(4*« •••'•••««t .... •^yyZd^jx/'i /:ic 'cZfc lu^vaanaae I K * S I ( M I * * * » I I I •••«bw>*4V*^t«^*nu*.l <*'«lfO*tt««) t . * , > ^ , s > . . . . . , . . f W . ^ » , M > % ^ ^ * , a M > ^ > a . . . . . ^ w I ; " ^ ' M I l l I I I iftAas/oaiiaao i\KU*\\m liM^piMiaa.*i«t)«wMpak»aa*M^ tiitiMai|ioMCioa0'iPaiaii«c«iit»ounoaaii*«eaiiN<tiiiirMia«iMitia<«v*u(«ia»i>iiait,i« • roaawvinmio^oi "Mtna laanaiail 1C:iiM«( |la%iU&-itU>Uiiaia7i iik^ttA vi^l^i.ar,.,:i mi'i» *^tt (M^M>4t atatt *>a>« l>-m Ikll RttlxMB blcLiiri-bk^ Zk'ArAZZ^ ••\tnrt(, t'l'i^in I^W// .i'y-'^pi^ *(»/fO o o cn c m l O N W F A U M 0 ) I ' I M I I l n . . n E N V i n O N M E N T A l O U A I I I V ( l O A I I D H A Z A R D O U S W A S T E M A N I F E S T iimiiMiht mi (riii'i) 7 ; M . / / I N I •• " 11 IK. Oil 100*111 t » l » U l y n , t o l o l o B o l l . M . w i , S I . C t o l « , U.S. V l r . i h . ^ L . - . l - . tMaVOOMI M l I r o l l e r H o r i n o lr•n!^»ot^ C o r p o r o t i o n tei t i l aMiaill t a l a Cnaidff, P u a r l o R I c o wauoaiia aat I r n n a p o r t e D l u t - -JlPiri) vn-.'L" y» 100.011 Irw.n P o r t u n r l i , P u e r t o Huevo, Son > i o n , Puerto Rico mtiiMoi. iioMU oo ovttM p m i i c t r n l n l n » j Choolcol o f P . " . . I n c . [fKiR) 054- Koi. 5 1 , HIglMoy I 1 , H o n o H . Puerto B l c o t «MM iwA rwo nwiiv««nu ft« i t • fiollont.oo 1 . I k l ' l " l 7 l " l " l ' ' l ' ' l ' . " l ' ' l MIUDJa iU .U U. l A . ' A l i l l i : Li!Li«i2i'L!LLijiilLiliii! t',B|n,0|7|0,)|7|7|>,l,l III WI na miVWVA t\ arriCP«lt - na insT Hiaam focuMwi at a i ' . ^ " . ' . • • I roonotftoor tM*«|NCIlUM . l o h i c r . r nn otoot Mowvni' l l n « . t l q i i l r i L'j^iy.! I - L L L J L L H J I L L L L I I J . 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J — I 1 ' I • iM*l*ra^aB9 t fir.^<tua> I . ^ I A M ,ia wo t atwiP* 1* •( w<i •(*• w«a^tV"*<^*Mitf »t| •••^^rnatu «.« ) fc..M..»...^H.. r * " " « llw.a ••ii«K>«lv*«oi**tfa>^»a.#i*.faMMMW«ia».»H.t I * I I I I I I I I iM^iroail z± iaiaiMai|io-aUOaO<'^iaiiatima«<anea«iilfat|iaKl|MrMiatuwiu*wv«^«'aainiMCia«auN; ita«*«»yaiitBtte>«lJl[nD Han«ail ' . i i y p . I t ! ' • ' ; ' ' ' tkalMkl llfuCl a* Nrroaiai Kofif K*iM tkalMkl llfuCl a* Nrroaiai Kofif |««MHM| «*» ,te« kiwidJT' «• tot* r «• M a« (^.tM) • • ' — M^oni».-»—•-rti.*'**.** lan Ife Jii-!j£L!^ •Ti'i nii>^n _3r!_izn_i 4 1iitliivt«il \i (' l o / i 1 «MlfUfttwtl C i V t U ( rAKT Al '.'fTVv IWIAITH OF rUlRfs. HICO * ^ ^ XMfNTAl OI'AIMV BOAflO A\ t l ^ l [D0U5 WA6TE Mf<H\ftSL^ir^j/\r^ ' _ x T " / v ^ » ^ ' ^ ^ ^ ^ POCWllil^RQ PR IC 0 ' U l a r t d CM*a c a l X o . , (009) ;7Q-720O C » t a U j > 9 . C a t a t t B e l h l a ^ e o , S t . C t o l a , U-S-Vliqln l a l a n d t A u r v n t M l ' L ) . V. i " " »*D»i u w n t a a i '^1 . V. i f r a i l t r HaMn».lran'aport C o r p o r a t i w i (U09) 7 z i - n n BU tae«n l o l a Cranda. Fuarto Rico \M«VtanaMI Itaoaporto D i a l naHM (0119) 192-7999 i| aoMU l . l - . 1 Zona P o f t u a t l a , Puerto Nuevo', San Juan, Puerto Blco •'- • • I - - - ' \ T Z Miiniiat. iiMiU m »tf>wmai*cvw I n l t n d Cheailcal of P . B . , Inc im taoam i I Ti i Ka>. 5 1 , l l l g l t o y i l l , H « > . t l , P u o i l o Rlc no?) 054-1090 | y | l , D , 9 i » | 0 , < | 5 i l . 0 , 7 , 5 | p , l l , D . ? i B . O , t . 4 | 4 , 5 , 7 , > | p i P ) D l 9 i e i O | 5 | l | t i e i 5 i 4 JP, P. 0,0,9, 0,5, 9, 9, 7, I. »i 0 ooo IHU MO IOUf#00>l« Ul 10 • VWaa Ml OUl nt IIUOWOO 11 Yfomoiii l - l " . ' Miio.wi|oa—It. oroiom - M I M I MlHItl fOClMIO, 00 O PH I ' l C i O l ' l I • I I Hylent m 1(1 oti Mojmcull r i M . (.quid M a^Mit 1)07 lOaai I J J I J I O L J L - I I 1 L . . . I .1 L l . L Ll I .1 ,. LL,,a=J gal -LL - L L J _ L J L L L_J Ltl U Ul LJ L.,i[UUU li»/tra •Min m t lii-ia. 1 . 1 ) I I . , Lx ^Uiai Hiti''<'T(P)ll*Ufl'0«lMliMitI««iama|MiWM>aK> «N*taaat««H AIMIHISM «*k'l1'«lt«tNa*'..iar«.«<il W (*iOH>iatai«iOtkaaiuai ai^Ot •sMv «pi«j»i>o.^^*« •! *• a*•«vri •« tojwi.i—i «• |ra «n<».c«—*w*«»*'rp iw.t.it *«*«** AM> »••*(•-<'«•«*ta*« ••••.•VI^.^O^B tw t.rrtatt | l * > r * a n p « > l « * 4 < M • ^ • « » M » l * • * • - • * » * fc-l-fc-t-"'* ••«»M • . J.'**«M o* * M |,W»,^ •.« ok. »..•«•-« d kM aM I w t l l •••« Mol .>•( I 1 1. Jeto*«* H. t o t ^ l g mil Pfealdenl •.1.^-t-. tk»« •.l*f<»<*» t ^ " * ^ »^W—••*!«* • . ( • « i « • I M ••U.ol 1 ii*MWii|a «u 1 •••1 »»mit» MiJ 4i?' V J l?.?l»ll|l|»,0) luMtuf aanvu oiif sail -atiMS O O t l . . . . |t.| la.o.....* 110 iro « • |>ii|D|9|nin|t|5|i,0|9|5| mVOanaM I V.mtiM 1rM-*,lh»t«»o**«> a iw^l/aaitaao I IciullM-T luhvaanaM ivcikiiM ^^ iu«voaiiako I •l"Ut O a« i M M I U (uanM«i*muaaot!nu4fKlintCKAr>a«tf rowwiTCatn^facrtfi^ it-.*iw<-\i-f Wiritli^ *T i.*«D tMiM i-*J« J J ia«^p>l«4>« «>aw^Vl%MAiM »,.^ fc,. a.wifwfc.Uw »N »»V»-' '•'''• ' ; ' •__ b,*M «l •»(><•( «t«J»M>H^#t 1^*1 l>.n—*MI».tf*|ll** (Il<| i ; i i n i I UiarMiaMaaiiimiwwaiaaiKlMWMiaimi nan «iiMi) iicLbbLbti -bbiiiLycL aa't udMa -bif-btUrti ••iMiATiiit tm r H U/ko :^i'i INDUSTRIAL CORROSION SOIL SAMPLE MANAGEMEf/T INCORPORATED IIW IWtni 10 MMXHFH. MIW JUUT OfMI K l M4«l)0 CLIENT: ENVIRO SCIENCE ICC (Berlex) NJDEP Certified Drinking WaterA/aslewate Laboratory ID l l \ k \ \ e REPORT DATE; July 31.1985 LAB / /*2H89 __ SAMPLE ID; Dryer SAMPLE DATE; 6/1A/85 SAMPLED BY: A. Kylea VOLATILE ORGANICS BY PURGE ANO TRAP By GC 'BTX/HEADSPACE _AT LAB DATE; 6/18/85 m H o o H Compounds detected In parts per million (milligrams/kilograms) dry weight basis. CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE 1,1-DICHLOROETHYLENE - 1,1-DICHLOROETHANE **-- t-l,2-DICHLOROETHYLENE CHLOROFORM 1 ,2-DICHLOROETHANE t-BUTYL METHYL ETHER - 1 ,1,1-TRICHLOROETHANE - CARBON TETRACHLORIDE - BROMODICHLOROMETHANE -- 1,2-DICHLOROPROPANE — *[ c-l,3-DICHL0R0PR0PENE t-l,3-DlCHL0R0PR0PENE ' TCE (TRICHLOROETHYLENE) ^f1,1,2-TRICHLOROETHANE „ 'DIBROMOCHLOROMETHANE ' A.O 340 A.2 ^Compounds co-elute (could be either material). LT-Less Than, GT-Greater Than dwb-Dry Weight Basis. X-Not Detected BENZENE DlISOPROPYL ETHER 2-CHLOROETHYLVINYL ETHER - BROMOFORM --T 1,1,2,2-TETRACHLOROETHANE PCE (TETRACHLOROETHYLENE - TOLUENE CHLOROBENZENE ETHYLBENZENE M-XYLENE *r O-XYLENE , P-XYLENE 6,6 A. 000 16.1 ALd. 15.1 **Tetrahydrofuran & Phosgene also elute at this point. Numerical results are calculated for I,l-Dichloroethane only. For the above listed Volatile Pollutants, nothing detected at a sensitivity level of; 1 mR/kR dwb. Unknown peaks detected (retention time,estImated amount); NOTE:Compound identification Is based upon retention time matches with specific known standards. Confirmation of analysis using GC/MS Is required to positively Identify any material and/or amount detected. INDUS! rf n Rrm~^ l\ INDUSTRIAL CORROSION MANAGEMENT INCORPORATED lli2M)UI£ 10. RANOO.N. N(* JiAS(r07M> 20l'il4-0]]0 NJDEP Certified Drinking Water/Wastewater Laboratory ID /?U116 REPORT DATE:_ LAB # 437A7 Aui'.u.st 15.1985 CLIENT: CNVIRO SCIENCES.INC. - ICC (BERLEX) PROJECT SAMPLE ID; Dryer SAMPLE DATE: 7/1/85 SAMPLED BY: Enviro Sciences AT LAB DATE; 7/11/85 VOLATILE ORGANICS BY PURGE AND TRAP GAS CHROMATOGRAPHY / HEADSPACE Compounds detected in parts per million (milligrams/kilograms) dry weight basis CHLOROMETHANE BROMOMETHANE- , VINYL CHLORIDE CHLOROETHANE • METHYLENE CHLORIDE ACETONE — — • 1,1-DICHLOROETHYLENE - 1,1-DICHLOROETHANE ** • t-l,2-DICHLOROETHYLENE CHLOROFORM I,2-DICHLOROETHANE ;-BUTYL METHYL ETHER - 1,1,1-TRICHLOROETHANE - CARBON TETRACHLORIDE -- BROMODICHLOROMETHANE -- X i. X_ 1,2-DICHLOROPROPANE . ^,c-1,3-DICHLOROPROPENE ' 't-l,3-DICHLOROPROPENE TCE (TRICHLOROETHYLENE) ^ ^rl,l,2-TRICHLOROETHANE 'DIBROMOCHLOROMETHANE ^ BENZENE DIISOPROPYL ETHER ' 2-CHLOROETHYLVINYL ETHER " BROMOFORM " 1,1,2,2-TETRACHLOROETHANE " PCE ( TETRACHLOROETHYLENE) " TOLUENE " CHLOROBENZENE ' ETHYLBENZENE ' K. X HJil ••'Compounds co-elute (could be either material). LT-Less Than dwb-Dry Weight Basis. GT-Greater Than X»Not Detected **Tetrahydrofuran & Phosgene also elute at this point. Numerical results are caluclated for 1,l-Dichloroethane only. KO rH O O H For the above listed Volatile Pollutants, nothing detected at a sensitivity level of mg/kg dwb. _X Unknov^/n peaks detected (retention time, estimated amount) numerous other hydrocarbon peaks, 0.02 to 0.1 wf./kg. ID m rr NOTE: Compound identification is based upon retention time matches with specific known standards. Confirmation of analysis using GC/MS is required to positively £-^/ identify any material and/or amount detected. INDUSTRIAL CORROSION MGMT.,INC. Cdwin Tichenor, Vice President 01 :i;'i'i INDUSTRIAL CORROSION MANAGEMENT INCORPORATED lib? win( IC. KAWxuftt. m w x K i i otitt loi-stt-oijo NJDEP Certified Drinking Water/Wastewater Laboratory ID /^'i'tllS REPORT DATE:_ LAB ff A3752 August 15.1985 CLIENT; ENVIRO SCIENCES,INC. - ICC (BERLEX) PROJECT SAMPLE DATE: 7/1/85 SAMPLED BY: Enviro Sciences SAMPLE ID: Dryer VOLATILE ORGANICS BY PURGE AND TRAP GAS CHROMATOGRAPHY/ HEADSPACE AT LAB DATE; 7/11/85 Compounds detected in parts per million (milligrams/kilograms) dry weight basis CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE • CHLOROETHANE • METHYLENE CHLORIDE — • ACETONE • I,1-DICHLOROETHYLENE - 1,1-DICHLOROETHANE ** - t-l,2-DICHLOROETHYLENE CHLOROFORM JL X XJL X X 1,2-DICHLOROETHANE --• t-BUTYL METHYL ETHER - 1.1,1-TRICHLOROETHANE CARBON TETRACHLORIDE - BROMODICHLOROMETHANE - X 1,2-DJCHLOROPROPANE ^,c-l,3-DICHL0R0PR0PENE 4-1 ,3-DICHLOROPROPENE TCE (TRICHLOROETHYLENE) -- ^e1,1,2-TRICHLOROETHANE 'oIBROMOCHLOROMETHANE BENZENE DIISOPROPYL ETHER 2-CHLOROETHYLVINYL ETHER - BROMOFORM 1,1,2,2-TETRACHLOROETHANE • PCE ( TETRACHLOROETHYLENE)' TOLUENE • CHLOROBENZENE • ETHYLBENZENE • J . ^ •'•Compounds co-elute (could be either material) LT-Less Than dwb-Dry Weight Basis. GT-Greater Than X-Not Detected **Tetrahydrofuran & Phosgene also elute at this point. Numerical results are caluclated for 1, l-Dichloroethane only. For the above listed Volatile Pollutants, nothing detected at a sensitivity level of J5 Unknown peaks detected (retention time, estimated amount) 34.07 g 15 mg/kg mg/kg dwb. NOTE; Compound identification is based upon retention time matches with specific known standards. Confirmation of analysis using GC/MS is required to positively ET/ ^^entify any material and/or amount detected. INDUSTRIAL CORROSION MGMT.,INC. . 3w.n Tichenor, Vice President IT) vo H o o H :y n n rt tn >j'i INDUSTRIAL CORROSION MANAGEMENT INCORPORATED 1)2 MMII .0. MNOOIPH. WM J(U(T 071(9 201 il4«lH CLIENT: ENVIRO SCIENCES,INC. - ICC (BERLEX) PROJECT NJDEP Certified Drinking Water/Wastewater Laboratory ID jCI'<ll6 REPORT DATE: August 15.1985 LAB # AA629 SAMPLE ID: Dryer SAMPLE DATE: 7/17/S5 SAMPLED BY: Enviro Sciences AT LAB DATE: 7/25/85 VOLATILE ORGANICS BY PURGE AND TRAP GAS CHROMATOGRAPHY / HEADSPACE Compounds detected In parts per million (milligrams/kilograms) dry weight basis CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE I , I-DICHLOROETHYLENE -- I ,1-DICHLOROETHANE * * • t - l ,2-DICHLOROETHYLENE X CHLOROFORM I ,2-DICHLOROETHANE --- t-BUTYL METHYL ETHER • 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE - BROMODICHLOROMETHANE - X X X X 1.2 X X X X X X X X X *i " I * I 1,2-DICHLOROPROPANE c-1,3-DICHLOROPROPENE t-l,3-DICHLOROPROPENE TCE (TRICHLOROETHYLENE) -- I,1,2-TRICHLOROETHANE DIBROMOCHLOROMETHANE BENZENE DIISOPROPYL ETHER • 2-CHLOROETHYLVINYL ETHER -• BROMOFORM • 1,1,2,2-TETRACHLOROETHANE • PCE ( TETRACHLOROETHYLENE) TOLUENE • CHLOROBENZENE • ETHYLBENZENE • 0.07 0.36 "Compounds co-elute (could be either material) LT-Less Than dwb-Dry Weight Basis. GT-Greater Than X-Not Detected **Tetrahydrofuran S Phosgene also elute at this point. Numerical results are caluclated for 1,l-Dichloroethane only. For the above listed Volatile Pollutants, nothing detected at a sensitivity level of mg/kg dwb. ^Unknown peaks detected (retention time, estimated amount) numerous other hydrocarbon peaks O.OI to 1 ms/kg vo — vo H — o o t-t — O i NOTE; Compound identification Is based upon retention time matches with specific known standards. Confirmation of analysis using CC/MS is required to positively EX/ identify any material and/or amount detected. INDUSTRIAL CORROSION MGMT.,INC. t r, Vice President INDUSTRIAL CORROSION sI^LE MANAGEMENT INCORPORATED i t a Sheet 7 NJDEP C e r t i f i e d D r i n k i n g W a t e r / W a s t e w a t e r L a b o r a t o r y ID # l ' 4 l l 6 REPORT DATF: J u l v 3 1 . 1985 LAB » ^2886 & ^2887-COMPOSITE 1152 ROlHE 10. RANDOLPH. NEW JERSEY 07869 201 584 0330 CLIENT; ENVIRO SCIENCES SAMPLE SOURCE:. SAMPLE DATE: 6 / 1 A / 8 5 ICC (Berlex) SAh'.PLED BY: A . K y l e s AT LAB DATE: 6/18/85 PRIORITY POLLUTANT VOLATILE ORGANICS + AO by GC/MS t 15 PEAKS Pararrieter R e s u l t P a r a m e t e r R e s u l t a c r o l e i n * a c r y l o n i t r l l e * benzene b r o o o f o r m c a r b o n t e t r a c h l o r i d e c h l o r o b e n z e n e c h l o r o d ibrcxTKjmethane c h l o r e t h a n e 2 - c h l o r o e t h y l v i n y l e t h e r c h l o r o f o r m d l c h l o r o b r o m o m e t h a n e 1 , 1 - d i c h l o r o e t h a n e 1 , 2 - d i c h l o r o e t h a n e 1 , 1 - d i c h l o r o e t h y 1 e n e _Z2IL 1,2-dichloropropane 1,3-dichloropropylene ethylbenzene methyl bromide methyl chloride methylene chloride 1 ,1 ,2,2-tetrachloroethane • tetrachloroethylene toluene •,---- 1 ,2-trans-dichloroethylene 1 ,1,1-trichloroethane 1,I,2-trichIoroethane trichloroethylene vinyl chloride Results reported in mg/kg (ppm), dry weight basis. *Detection Limit LT-Le5s than X=Not detected 100 ppm OTHER COMPOUNDS DETECTED APPROXIMATE CONCENTRATIONS 125 1.560 benryl acetate — 22 chloromethyl benzene 1430 l-chloro-2-methyl benzene 40 ET/jmg INDUSTRIAL CORROSION MANAGEMENT, INC. dwlnV \Ar^<?r> EdwinVTichen'cvc Vice President 100167 INDUSTRIAL CORROSION MANAGEMENT INCORPORATED 1152 ROOTE 10. RANDOLPH. NEW JERSEY 07869 201 5M 0330 CLIFNT: ENVIRO SCIENCE " ^ t a Sheet 8 NJDEP Cert led D r i n k i n g Water/ WasLewate.- Laboratory ID #1^116 REPORT DATE: July 31, 1985 LAB I 42886 & 42887 COMPOSITE SOIL SAMPLE SAMPLE SOURCE; ICC (Berlex) SAMPLE DATE: ft/U/fiS SAHPLFD BY: A. Kvles .AT LAB DATF.; 6/18/fi5 PESTICIDE 6 PCB EXTRACTABLES PRIORITY POLLUTANTS + kO • by GC/MS Pa rameter Result Aldrin LT 2- a-BHC LT 2 b-BHC LT 2 d-BHC - LT 2 S-BHC - LT 2 C.hlordane LT 12 '»,^'-DDD LT 3 ij.^'-DDE LT 3 i^.A'-ODT - - LT 3 O i e l d r l n LT 3 E.-idosulfan I L T 3 Endosulfan II LT 3 Endosulfan Sulfate LT 3 E.-idrin LT 3 Endrin Aldehyde LT 3 Heptachlor LT 3 Heptachlor Epoxide LT 3 Tcxaphene • LT 12 PCB-10'16 - - — — LT 45 PCB-1221 - LT 45 P^B-^232 - LT45 PCB-12A2 LT 45 P^B-12A8 - - - LT 4-7 PCB-125A LT 45 PCB-1260 LT 45 All r e s u l t s are reported in mg/kg (ppm), dry weight b a s i s . INDUSTRIAL CORROSION MGMT, Edw i V*^ T i ch^xior — / , E T / j m g V i c e P r e s i d e n t / d ^ L T » L e s s Than X=Not D e t e c t e d 100168 INC INDUSJ. ..AL CORROSION ^°'^ ' ^ ^ ^ ti.ivKf (,«•'I I 1 • ' u r m k l i x ) M.wr.r/ Data Sheet 9 Wastewater L. . l a t o r y ID #14116 MANAGEMENT INCORPORATED nS2 R0U1E 10. RANDOLPH. NEW JERSEY 07869 201 5«4 0330 CL I ENT: ENVIRO SCIENCES REPORT DATE: Julv 31,1985 LAB # 42886 & 42887-COMPOSITE SAMPLE SOURCE; ICC (Berlex) SAMPLE DATC; 6/14/85 SAMPLED BY: A.Kyles .AT LAB DATE; 6/13/85 BASE/NEUTRAL EXTRACTABLES PRIORITY POLLUTANTS + ««0 by GC/MS •» 15 PEAKS Parameter Result acenephthene X acenaphthylcne X anthracene • X benzidine X benzo (a)anthracene X ben2o(a)pyrcne X S.'l-benzof lucranthene X benzo(ghl)perylene X benzo(k)fluoranthene X bls(2-chloroethoxy)methane X b l s ( 2 - c h l o r o e t h y l ) e t h e r X bl s ( 2 - c h l o r o l s o p r o p y l ) e t h e r X b l 5 ( 2 - e t h y l h e x y l ) p h t h a l a t e X '»-bror>ophenyl phenyl ether X b u t y l benzyl phthalate X 2-ch1 oronaphthalene X *»-chl orophenyl phenyl ether X chrysene. X dlbe.izo(a,h)anthracene X 1,2-dIchlorobenzene X 1,3-dlchlorobenzene X 1 ,l»-d Ichlorobenzene X ' 3,3-dichlorobenzIdlne . X Parameter Result diethyl phthalate dimethyl phthalate dl-n-butyl phthalate 2,'»-dln i tro to luene 2,6-d ini trotoluene di-n-octyl phthalate 1,2-dI phenyl hydrazine(as azobenjene)' fluoran thene fluorene hexachlorobenzene hexachlorobuladlene • hexachtorocyclopentadiene -- hexachloroethane lndeno(l,2,3-cd)pyrcne isophorone naphtha Icne ni trobenzene N-ni trosodlmcthylamine N-nltrosodi-n-propylamine N-ni trosodiphenyl aminc phenanthrene pyrene 1 ,2,'<-trIchlorobenzene A - _ X None of the above listed Priority Pollutants detected at a sensitivity level of 450 ng/kg (ppm) dry weight basis. ** . LT-Less Than X=Not Detected **Large dilution necessary due to high concentration of benzyl acetate. APPROXIMATE CONCENTRATION OTHER COMPOUNDS DETECTED benzyl acetate — ,/Se/r^ benzene methanol _ 170,000 15,000 l,l'-[oxybi8 (inethylene) bis Jbenzene Chloromethyl benzene diphenyl methanone — 9H-fluorene-9-one — 4,400 30,000 4,000 All results reported in mg/kg (ppm), dry weight basis. E T / - - f 3,000 100169 INDUSTRIAL CORROSION MGMT.,INC. INDUSTRIAL CORROSION fAAHAGEMEKT L ' J I 1 I INCORPORATED IDIMUIIIO.MMKIirHWWJIRMTO/IM H I U 4 01N NJDEP C e r t i f i e d Drinking Water/Wastewa Laboratory ID #I<<I16 arer SOIL SAMPLE REPORT nATP; July 3 1 . 1965 LAB I A2886 & 42887 COMPOSITE CLIENT: ENVIRO SCIENCE.^ SAMPLE SOURCE; ip.r. rRprl.v^ SAMPLE DATE: 6/14/»S SAMPLED BY: A yyi^g AT LAB DATE; 6/lS/fl5 ACID EXTRACTABLES PRIORITY POLLUTANTS + kO bv qC/MS-H 10 PEAKS O O M -J O ACID EXTRACTABLES PRIORITY POLLUTANTS + 1 0 Peaks 2-chlorophenol 2-nitrophenol phenol 2,'<,-dimethylphenol 2,'<,-dichlorophenol pentachlorophenol 2,'i-dlnl trophenol '•,6-dlnl tro-o-cresol — '•-ni trophenol 2,'»,6-trichlorophenol -- '•-chloro-3 methyl phenol OTHER COMPOUNDS DETECTED APPROXIMATE CONCENTRATIONS X None of the above listed Priority Pollutants detected at a aenistivity level of 450 mg/kg (ppm) dry weight basia No other Phenolic compounds detected at a sensitivit} of 500 mg/kg (ppm) dry weight basis. ** INDUSTRIAL CORROSION MANAGEMENT, INC ** Large dilution necessary due to high concentration of benzyl acetate. ET/jmg LT-Less Than X-Not Detected Edwifr- Tich Vice President rt tu n n rt ca Sheet Ll INDUSTRIAL CORROSION „ MANAGEMENT INCORPORATED lis? RWJll 10. RANOOIPH. NEW XRStT 0;tl£9 ?0l M< 0 IVI n IFMT. ENVIRO SCIENCES SOIL SAMPLE NJDEP Ceriified Drinking Water Wjslewater Laboratory ID #14116 REPORT DATE: Julv 31. 1985 LAB # 42886 & 42887 Composite SAMPLE SOURCE: ICC (Berlex) SAIPLE DATE L_1ZAAZ85___ SAMPLED BY: A. Kyles AT LAB DATE:6/18/85 — - ^ PRIORITY POLLUTANTS-H 40 TOXIC POLLUTANTS: Metals, Cyanide and Total Phenols PARAMETER Tot a Tota Tota Tota Tota Tota Tcta Tota Tcta Tcta Tcta Tota Tcta Tota Tcta Antimony - Arsenic -- Be ryI Ii um Cadmium -- Chromium - Copper — Lead -- — • Mercury -• Nickel --• Selenium • S iIver — ThaI Ii um • Zinc RESULT LT 118. 40.0 LT 2.87 22.8 592 327 688 2.73 134 LT 1.08 LT 7.48 LT 66.2 3.594 Cyan ide Phenol - ZL.^U 9^01 All r e s u l t s are reported in mg/kg (ppm)', dry weight b a s i s . We thank you for this opportunity to serve you. If you have any q u e s t i o n s , please do not h e s i t a t e to c a l l . Very truly yours, INDUSTRIAL CORROSION MGMT., INC. ET/jmg LT=Less Than X=Not Detected dwin TicheWor — / 6^ Edwin TicheWo Vice President 100171 ;>ata ineet L^ INDUS Ml AL CORROSION MANAGEMENT INCORPORATED NJDEP Cc.tified Drinking Water/ Wastewater Laboratory ID #14116 REPORT DATE: August 15.1985 LAB # 44418 1152 ROUTE 10, RANDOLPH, NEW JERSEY 07869 2QI 584 0330 CLIENT: ENVIRO SCIENCES. INC. SAMPLE SOURCE: ICC (BERLEXI PROJECT SAMPLE ID; St.Croix SAMPLE DATE: -w^wova- SAMPLED BY: Al Kyles .AT LAB DATE: TI22J%5 WATER Parameter PRIORITY POLLUTANT VOLATILE ORGANICS by GC/MS acrolein* acrylonitrile* benzene brornoform carbon t e t r a c h l o r i d e chlorobenzene chlorodibromomethane chlorethane 2-chloroethy1vinyl ether chloroform dichlorobromomethane I , I - d i c h l o r o e t h a n e I ,2-dIchloroethane 1 ,1-dichloroethylene Result 0.04 Parameter I,2-dichloropropane I,3-dichloropropylene ethylbenzene methyl bromide methyl chloride methylene chloride I,1,2,2-tetrachloroethane - tetrachloroethylene toluene I,2-trans-dichloroethylene I,1,I-trichloroethane I,I,2-trichloroethane trichloroethylene vinyl chloride - Results reported in mg/l (ppm). Detection limit 0.001 mg/l (ppm) Resui t .Q.3g JL *Detection Limit: Q.l mg/i E T / j m g I N D U S T R I A L C O R R O S I O N M G M T . , I N C J Edwin T i c h e n o r V i c e P r e s i d e n t LT=Less Than X=Not Detected 100172 INDUS'i..iAL CORROSION MANAGEMENT INCORPORATED ..V.UUI ».<.i Lll I tz- II idKing wa L t r/ Wa stewater Laboratory 10 ,116 Data Sheet 13 REPORT DATE: August 15.1985 LAB » ^^^^8 ; 1152 ROUTE 10. RANDOLPH, NEW JERSEY 07869 201 584-0330 CL I FMTf FNVTi;n < ; r T E N r E S . I N C . SAMPLE cniiRrP- ICC(BERIEX) ; St. Croix SAMPLE nATg: u n l r — - <;AMPI FD BY: A l Kyles AT LAB OATE: /9y/^d<ryr'jyi— WATER PESTICIDE & PCB EXTRACTABLES PRIORITY POLLUTANTS , by GC/h? Parameter Result Aldrln - - LT 0.01 a-BHC LT 0.01 b-BHC LT 0.01 d-BHC : LT 0.01 g-BHC — - LT 0.01 Chlordane - LT 0.02 4,i*'-DDD LT 0.01 1*,4'-DDE - LT 0.01 1»,'»'-DDT LT 0.01 Dieldrin LT 0.01 Endosulfan I - LT 0.01 Endosulfan II LT 0.01 Endosulfan Sulfate - — LT 0.01 Endrin - LT 0.01 Endrin Aldehyde - - LT 0.01 Heptachlor - ^ - LT O.OI Heptachlor Epoxide LT 0.01 Toxaphene - LT 0.02 PCB-I 016 - LT 0.01 PCB-1221 - -— LT 0.01 PCB-1232 - LT 0.01 PCB-1 2^*2 - LT 0.01 PCB-12'»8 - LT 0.01 PCB-125A - - LT 0.01 PCB-1260 - LT 0.01 A l l r e s u l t s reported in mg/l (ppm). INDUSJRIAL^CJia&i)SI/ Edwin T i c h e n o r ET/jmg Vice P r e s i d e n t LT=Less t h a n X=Not d e t e c t e d 7/22/85 MGMT. , INC 100173 INDUSTRIAL CORROSION MANAGEMENT INCORPORATED i l » ; ROUTE 10. MNOOlfN, NEW JUSEr tJU9 » l M4-03M CLIENT: ENVIRO SCIENCES, INC, NJDEP C e r t i f i e d Drinking Water/Wastewater Laboratory ID #11«I16 REPORT DATE: August 15,1985 LAB # 44418 l-« o o l-» •J 1^. SAMPLE SOURCE; SAMPLE D A T E L ICC (BERLEX) PROJECT unknown-' /^y^^yyftJ&— SAMPLED BY: Al BASE/NEUTRAL Parameter Result acenaphthene X acenaphthylene X anthracene • X benzidine X benzo(a)anthracene X ben2o(a)pyrene X 3 .'i-benzof luoranthene X ben2o(ghl)perylene X benzo(k)fluoranthene X bis(2-chloroethoxy)methane X bis (2-chIoroethyl)ether X bis (2-chloroisopropyI)ether X bis(2-ethyihexyl)phthalate X 4-bromophenyI phenyl ether X butylbenzyl phthalate X 2-chloronaphthalene X 4-chlorophenyl phenyl ether X chrysene X diben2o(a,h)anthracene X I ,2-dlchlorobenzene X I ,3-dichlorobenzene X I ,'4-dlchlorobenzehe X 3,3-d'chloroben2ldlne X None of the above Priority Pollutants detected **Other compounds see Addendum I LT-Less Than X-Not Detected C T / I mr* SAMPLE ID: ST. Croix Kyles AT LAB DATE: 7/22/85 EXTRACTABLES PRIORITY POLLUTANTS bv GC/MS Parameter diethyl phthalate dimethyl phthalate di-n-butyl phthalate -; 2,4-dinitrotoluene 2 ,6-dini trotoluene di-n-octyl phthalate I,2-diphenylhydrazine (as azobenzene) fluoranthene fluorene --- hexachlorobenzene " hexachIorobutad iene hexachlorocyclopen tadiene hexachloroethane indeno(l,2,3-cd)pyrene i sophorone naphthalene n i t robenzene N-n11 rosod imethy I amIne N-ni trosod i-n-propyI amine N-ni t rosodI phenyl amine phenanthrene pyrene 1,2,'•-tr Ichlorobenzene at a sensitivity level of 0.03 mg/l (ppm) INDUSTRIAL CORROSION MANAGEMENT, INC. Result rr 0) n n rt Edwin Tichenor Vice President ''CI 'Hta Sheet If NJDEP Certified Drinking Water/ Wastewater Laboratory ID ii'14116 REPORT DATE; August 15,1985 LAB H 44418 CLIENT: ENVIRO SCIENCES, INC. SAMPLE SOURCE; ICC (Berlex) SAMPLE ID: St. Croix SAMPLE DATE; wkriuwir SAMPLED BY: Al. Kyles AT LAB DATE; y9yZZZEZyys~~ BASE/NEUTRAL EXTRACTABLES PRIORITY POLLUTANTS ADDENDUM I _0THER_C0MP01JNDS DETECTED by~Gc7MS~ ~ Parameter Result 7/22/85 benzaldehyde chloromethyl benzene benzene methanol phenyl acetate diphenyl methane 1-1'-[oxybis(methylene]bis benzene All results are reported in mg/l (ppm). 3.0 0.3 24.0 26.0 0.4 0.4 We thank you for this opportunity to serve you. If you have any questions, please do not hesitate to call. INDUSTRIAL CORROSION MANAGEMENT, INC. ET/jmg end. LT=Less Than Edwin Tictfenor Vice President 100175 Jata Sheet 16 INDUSTRIAL CORROSION MANAGEMENT INCORPORATED 11S2 ROUTE 10, RANDOLPH, NEW JERSEY 07869 201 584-0330 NJDEP Certified Drinking Water/ Wastewater Laboratory ID #14116 REPORT DATE: August 15.1085 LAB # 44418 CLIENT: ENVIRO SCIENCES. INC. SAMPLE SOURCE ICC (BERLEX) PROJECT ST. Croix SAMPLE DATE: unKuuwir SAMPLED BY: Al Kvles y9J7rcy/9crr^ AT LAB DATE: ACID EXTRACTABLES PRIORITY POLLUTANTS bv GC/MS l l l H ^ ' ^ WATER Parameter Result 2-chlorophenol X 2-nitrophenol X phenol X 2,4-dimethylphenol X 2,i4-dichlorophenol X 2, i( ,6-trichlorophenol X pentachlorophenol X 2 ,i<-din i trophenol X A.^-dinitro-o-cresol X '•-n i trophenol X '4-chloro-3 methyl phenol X None of the above P r i o r i t y P o l l u t a n t s detected at a s e n s i t i v i t y level of 0.01 mg/l (pp: OTEZR PEAKS DETECTED: benzoic acid (? 3 mg/l INDUSTRIAL CORROSION MGMT.,INC ET:j mg LT=Less Than X^Not Detected ZZZE^ Edwin T i c h e n o r V i c e P r e s i d e n t 100176 jata Sheet 17 INDUSTRIAL CORROSION MANAGEMENT INCORPORATED u s ? RLvll 10. RANOOlPH, NtW JERSEY 07S69 201 W4 OI"«l CL1ENT: ENVIRO SCIENCES INC. NJDEP Certified Drinking Water Wastewater Laboratory ID #14116 REPORT DATE: A»yn«;t 15.1985 LAB I 44418 SA.-.PLE SOURCE-^ SA.-.PLE DATE: ICC (BERLEX) PROJECT SAIQ'LE ID: St. Croix • uitknumr* <;AMPI rn BY: Al Kyles y^jZrc^/rp/j— PRIORITY POLLUTANTS AT LAB DATE: 7/22/85 TCXIC POLLUTANTS: PAt^AMETER Metals, Cyanide and Total Phenols Tota Tota Tota Tota Tota Tota Tota Tota Tota Tota Tota Tota Tota Tota Tota All Antimony - Arsenic -- Beryl Iium Cadmium -• Chromium • Copper Lead ----- Mercury -• Nickel --• Selenium • S iIver — Thai 1ium ' Zinc Cyan i de Phenol • WATER SAMPLE RESULT LT LT LT ],T 0. 0- fi- 0. 0. 0 0 n 0 0 0 0 4 0 0 m6 005 013 003 027 JJ.3 nn nm 080 Jlil5 sm SOS 85 053 061 results are reported in ng/l (ppm). We thank you for this opportunity to serve you. do -lot hesitate to call. If you have any questions, please Very truly yours, INDUSTRIAL CORROSION MGMT., INC. L. E T / > q LT=Less Than X=Sot Detected Edwin Tichenor Vice President 100177 1» COPtLANO TO.. DEMVILLt NEW JERSCT 07a>4 CHAIN OP CUSTODY RECORD I n s t a l l a t i o n : ICC (Berlex) S u r v e y N o . : S a m p l e r s : ( S i g n a t u r e ) (ULtXyU^t^. *>fc^jZo> o. B «o c Vi Z S t a t i o n L o c a t i o n Date Analysis Time Sample Type Comp G r a b vr u c «»-l - r i o n u • c o o 2 U Drain Line ^ t Z l ^ S ' l Toluene 6/8/85 Identify the contents bf^the black soil sample.] 2 3 4 5 6 Laboratory P i t ^ ^ S ^ P 3 Pyridine 6/14/85 Laboratory Pit-duplicate ^ ^ ^ VGA /^(^/, 6/14/85 Time limit may have expired, if so do not run.] 7 7 7 F S Plt--diinHe3re niniHd^ P r l n r i t v Pollutants 6/14/8! y: Pit-duplicate (liquid) Priority Pollutantb 6/14/85 4m ^F^mrs Pit-Interface(liquid/sludge)\ combine and run 6/14/85 T A T F T i p r i o r i t y Pit-3ludge v a f g ^ -^ p o l l u t a n u t a n t s 6/14/85 /pyo X [* One container has a white lump, segregate ^ it and an; lyze for qulnid ne. ] Drver Relinquished by: (Sign.) CC- ifs 'A^^f'f Toluene 6/14/85 Relinquished by: (Sign.) R e c e i v e d by:. ( S i g n . ) JZLi / R e c e i v e d b ^ : ( S i g n . ) D a t e / T i m e D a t e / T i m e r e l i n q u i s h e d b y : ( S i g n . ) R e c e i v e d by: ( S i g n . ) D a t e / T i m e R e l i n c m i s h e d by R e c ' d by L a b o r a t o r y f o r f i e l d a n a l y s i s ( S i g n . ) !M D a t e / T i m e ^7i'^s' /x'/.r Dispatched by: (Sl/^n.) Date/Tlra^ Rec'd for Laboratory by: D a t e / T i m e .Method of S h i p m e n t : Express Air Freight / T L ClcAAEtAy^ 1 0 0 1 7 8 LAB NO. 42885 Pit duplicate (liquid),Priority Pollutants +40 (Process Pit) Samples not analyzed because sample volume too small. 100179 I t COPtLANO TO., DEMVnOJL MEW JEWCY 07»M CHAIN OP CUSTODY RECORD '3f^^ 3'4^^ i3-|H^ (^1-^ ;^,-^5l # ^ - • I n a t a l l a t l o n : /dd/'/S^e/r/^:.^) Survey N o . : a a ' 19 C to a - - -s# • "^ " - W ^ S t a t i o n L o c a t i o n _ 2 ^ y V > e , /-itrtff^. y^titf A T /^JZ few>/</ "' * ^ ^ <- >^S ' •• f ^ ' j / ) / t t / ^ / ^ ' A'Ut{-T'.t R e l i n q u i s h e d by: ( S i g n . ) R e l i n q u i s h e d (^y: ( S i g n . ) R e l i n q u i s h e d by: ( S i g n . ) R e l i n q u i s h e d by: ( S i g n . ) D i s p a t c h e d by: ( S i g n . ) Date/Time Samplers: ( S i g n a t u r e ) date ' /iAr^Y ZiAyc^/ A/^JcY ^J^rV '<%S-/ / A i ^ ^ / w i i y Time A^rff^r-r 'f <• * • 'r f . Sample Type Comp . Received by: ( S i g n . ) R e c e i v e d / l ^ : ( S i g n . ) • Received by: ( S i g n . ) Rec'd by Laboratory for f i e l d a n a l y s i s ( S i g n . ) Rec'd for Laboratory by: G r a b V v V y y-. \ • w • c o « u • e o o / / / / / / Date /Time Date/Time D a t e / T i m e D a t e / T i m e D a t e / T i m e Method of Ship^nenXi, y , / ^ / ^ ^ •}>! 100180 CHAIM OP CUSTODY RECORD I t CJDflUMO TO, O e f V U l . NEW J C W l OTtM I n . t . l U t l o n : ^ ^ ; ^ ^ Survay Mo.: ^ ^ i c ^ 9 ^ 4 0 ^ 3 c -<A-<^62I CO Station Location Samplers: (Slgnatur*) /)/e</€y2, (^7a'y('^^<yzA) /^S^/^ / Z / " J a ^ T ^ ^ c J / ^ / ^ / l y x ^ ) y/ Z ^ f /ty/Zyy/i^iC,^ /d. - ? » - ' /y/e/ry y^c^'yys^/T -A-^^ y^^rt:/^ / ^ ^iyis^cZ. \ tyyar' /=~<fu^a a^r/c- /)/r/zyZ-^ rp/zr/>cxy r/ /r ry //^y> t^^y/ke^. /<ej^>rfrp<sy> / ' ^ / ^ c y / h ^ Rirlinqulahed by:, ( S i g n . ) Rezlinquished by: (Sign//) Relinquished by: (Sign.) Relinquished by: ( S i g n . ) "X > ^ / ^ Received by: (Sign. ) fZZ Ji ^-i~Lcyr^-'.-.-<-!JL^ Received by: CSlgn. ) Dat«/TiB* Received by: (Sign. ) Dispatched by: (Sign.) Date/Tim* Rec'd by Laboratory for field analysis (Sign.) Dat«/TiiBa Data/Time Date/Tim* Rec'd for Laboratory by: Dattt/Tima Method of Shipment cZziyuc^ zZ^/oC /^^^ly^ay/y' 100181 anwio S Ksncsi nc CHAIN OP CUSTODY RECORD I t C O m > M O TO.. O e M L L I k M n r JEMKY OTVM i^/g In.t.llation: y ^ ^ ^ / f < r Survey No.: • a S ' « c Vi 2 • Station Location /Z^y/^y/y/^^y//?*;/! -A- ^ ^ /"^^-^^^^ /<y^ A4/C<^ RelAnquished by: (Sign.) Relinquished by: (Sign.) / Kelinquiahed by: (Sign.) Relinquished by: (Sign.) Dispatched by: (Sign.) Date/Time Samplers: (Signature) Date /^yf! / • Time ^ 2 cc Sample Typoj Comp. Received by: (Sign.) Received by: J Sign.) Received by: (Sign.) Rec'd by Laboratory for field analyais (Sign.) Rec'd for Laboratory by: -tirab V No. of Containeri <y. Date/Time Date/Time Date/Time Date/Time Date/Time Method of Shipment: ^ y / 100182 ATTACHMENT 100183 u^ T &i till INDUSTRIAL CORROSION MANAGEMENT INCORPORATED iis?nuuiE 10.RANOGLPii.Niv.'jEnsEr07669 roistt-oajo NJDEP Ceiiificd Drinking Water/Wastewater Laboratory 10^14116 REPORT DATE: Septeml.cr 12.1985 LAB 45362 CLIENT: ENVIRO SCIENCE - ICC RERLEX PROJECT SAMPLE ID: Lab Pit //5965 SAMPLE DATE: August 7, 1985 SAMPLED BY: Enviro Science AT LAB DATE: August 9. 1985 VOLATILE ORGANICS BY PURGE AND TRAP GAS CHROMATOGRAPHY/ HEADSPACE CHLOROMETHANE.. BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE --- ACETONE 1,1-DICHLOROETHYLENE - I ,1-DICHLOROETHANE *^ t-I ,2-niCHLOROETHYLENE CHLOROFORM 1 ,2-OICHLOROETHANE --- t-BUTYL METHYL ETHER - 1 ,1 ,1-TRlCHLOROETHANE CARBON TETRACHLORIDE - BROMODICHLOROMETHANE - Compounds detected in parts per million (milligrams/kilograms) dry weight basis - X X X X X 0. 32 X 0. 0. 02 02 X X X X X X M 1,2-DICHLOROPROPANE c-1,3-DICHLOROPROPENE t-I,3-OICHLOROPROPENE'" TCE (TRICHLOROETHYLENE) 1,1 ,2-TRICHLOROETHANE DIBROMOCHLOROMETHANE BENZENE DIISOPROPYL ETHER --- • 2-CHLOROETHYLVINYL ETHER -• BROMOFORM • 1,1 ,2,2-TETRACHLOROETHANE • PCE ( TETRACHLOROETHYLENE)- TOLUENE • CHLOROBENZENE ETHYLBENZENE • 0.34 0.08 0.01 "Compounds co-elute (could be either material) LT=Less Than dwb=Dry Weight Basis. GT=Greater Than X=Not Detected ••'••"Tetrahydrofuran £ Phosgene also elute at this point. Numerical results are caluclated for 1,1-Dichloroethane only. For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 0.01 mg/kg dwb. H o o H 00 (1^ JJ Unknown peaks detected (retention time, estimated amount) Xylenes approx 0.06 mg/kg dwb NOTE: Compound identification is based upon retention time matches with specific known standards. Confirmation of analysis using GC/MS is required to positively identify any material end/or amount detected. ;:SI.: INDUSTRIAL CORROSION MANAGEMENT, INC. zMyZjl^ 'iJichard SyLevi'he/P lii chard S./Levi'he/President > o H ni INDUSTRIAL CORROSION MANAGEMENT INCORPORATED 1157HOurt l i WNDOLPli, Nf* Jt«5tro?<69 ?0I 58<-O330 NJDEP C e r t i f i e d Drinking Water/Wastewater Laboratory ID H k W i , REPORT DATE: September 12.1985 LAB ff 45363 CLIENT: ENVIRO SCIENCE - ICC BERLEX PROJECT SAMPLE ID: Lab P i t //5966 SAMPLE DATE: Aufiust 7, 1985 SAMPLED BY: E n v i r o Science VOLATILE ORGANICS BY PURGE AND TRAP GAS CHROMATOGRAPHY/ HEADSPACE AT LAB DATE: August 9 . 1985 CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE HETHYLENE CHLORIDE - — ACETONE - - 1,1-DICHLOROETHYLENE - 1 ,1-DICHLOROETHANE '^* t-l,2-DICHLOROETHYLENE CHLOROFORM I,2-DICHLOROETHANE - - - t-BUTYL METHYL ETHER - 1 ,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE - BROMODICHLOROMETHANE - Compounds d e t e c t e d in p a r t s per m i l l i o n ( m i l l i g r a m s / k i l o g r a m s ) dry w e i g h t b a s i s X 1,2-DICHLOROPROPANE - X X X X 0. 27 X 0. 0, 02 01 X X X X X X ,rc-l,3-DICHLOROPROPENE "'t-l,3-DICHLOROPROPENE" M TCE (TRICHLOROETHYLENE) , 1 , 2 - T R I C H L 0 R 0 E T H A N E _ _ DI BROMOCHLOROMETHANE BENZENE DIISOPROPYL ETHER 2-CHLOROETHYLVINYL ETHER - BROMOFORM 1,1,2,2-TETRACHLOROETHANE • PCE ( TETRACHLOROETHYLENE)' TOLUENE CHLOROBENZENE • ETHYLBENZENE JL A.OL X X . "Compounds co-elute (could be either material). LT=Less Than dwb=Dry Weight Basis. GT=Greater Than X=Not Detected ••"^••'Tetrahydrofuran 6 Phosgene also elute at this point. Numerical results are caluclated for 1,1-Dichloroethane only. For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 0.02 mg/kg dwb. o Unknown peaks detected (retention time, estimated amount) M 00 tn NOTE: Compound i d e n t i f i c a t i o n is based upon r e t e n t i o n time matches w i t h s p e c i f i c known standards. Confirmation of analysis using GC/HS is required to p o s i t i v e l y i d e n t i f y any m a t e r i a l and/or amount d e t e c t e d . INIJUSTRIAL CORROSION HAf.'AGEMENT, INC. 'ilichorci S ./Lev i-ne/Pres i d e n t INDUSTRIAL CORROSION MANAGEMENT INCORPORATED ll5?H0UIt 10. RfNOOini. NtW jenSCV 0»«69 30) 5»«-0330 NJDEP Certified Drinking Water/Wastewater Laboratory ID n ^ \ 16 REPORT OATE: .^e pi ember 12.1985 LAB /f 45364 CLIENT: ENVIRO SCIENCE - ICC BERLEX PROJECT SAMPLE ID: Lab Pit //5967 SAMPLE DATE: August 7, 1985 SAMPLED BY: Enviro Science AT LAB DATE: August 9. 1985 VOLATILE ORGANICS BY PURGE AND TRAP GAS CHROMATOGRAPHY/HEADSPACE Compounds detected in parts per million (milligrams/kilograms) dry weight basis "Compounds co-elute (could be either material) LT=Less Than dwb=Dry Weight Basis. GT=Greater Than X=Not Detected X CHLOROMETHANE X BROMOMETHANE X VINYL CHLORIDE 211 CHLOROETHANE HETHYLENE CHLORIDE - — ACETONE I,1-DICHLOROETHYLENE -- 1,1-DICHLOROETHANE AA t-l,2-DICHLOROETHYLENE - CHLOROFORM - - --- - — 1 ,2-DICHLOROETHANE - t-BUTYL METHYL ETHER 1 , I , 1-TRICHLOROETHANE - CARBON TETRACHLORIDE BROMODICHLOROMETHANE -- --- -- 0.23 0.03 0.11 ,2-DICHLOROPROPANE .,rc-l ,3-DICHLOROPROPENE "'t-l,3-DICHLOROPROPENE'" TCE (TRICHLOROETHYLENE) ^rl,1,2-TRICHLOROETHANE "'0 IBROHOCHLOROMETHANE BENZENE DIISOPROPYL ETHER 2-CHLOROETHYLVINYL ETHER - BROMOFORH 1,1,2,2-TETRACHLOROETHANE • PCE ( TETRACHLOROETHYLENE)- TOLUENE CHLOROBENZENE ETHYLBENZENE X X X 0. 01 X X X X X 0. 05 X 0. 04 ••"^Tetrahydrofuran 6 Phosgene also elute at this point. Numerical results are caluclated for 1,1-Dichloroethane only. For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 0.01 mg/kg dwb. XUnknov;n peaks detected (retention time, estimated amount) o 00 -. o\ , NOTE: Compound identification Is based upon retention time matches with specific known standards. Confirmation of analysis using GC/HS is required to positively identify any material and/or amount detected. ;.SL: Xylene —0.02 mg/kg dwb INDUSTRIAL CORROSION MANAGEMENT. INC. Kichard S ./Lev IT ine/President CHAIM Of CUSTODY RECORD V5-'J^V .'i-3<i J ^ ^ / / .z:}co- V • -. • • i«cofCLAMOno.DefvmxNIWjcwr OTVM I t i . t a l U t i o n : / ^ ^ j ^ . ^ Survey Mo.: a • « c CO a r-2.-3 s-^L/ 't\ S t a t i o n L o c a t i o n ^ ^ / ( ^ < ^ //^^^y<>*^) / ^ ^ ( ^ r Z Z ^ d h o y ^ y^^/^yZ^ f/ZU^-aZZAic, / i n q u i s h e d by: ( S i g n . ) \^.A^^\t^.y\, c L ^ - /^ie\AX>\.>k-A^ K e i i n q u i a h e d by: ( S i g n . ) | K e i i n q u i s h e d by: ( S i g n . ) R e l i n q u i a h e d by: ( S i g n . ) D i a p a t c h e d b y : ( S i g n . ) Date/Time Samplera: ( S i g n a t u r e ) (y Date 7^^1^ // Time ' y^.'Arry tZP.yx?^ ^ • * % V r f Sample Type Comp. G r a b ^ \ \ • Received by: ( S i g n . ) Received by:(j(Sign.) Received by: ( S i g n . ) Rec'd by Laboratory for f i e l d a n a l y a i s ( S i g n . ) Rec'd for L a b o r a t o r y by: 1 No. of Container! / z ^ D a t e / T i m e D a t e / T i m e D a t e / T i m e D a t e / T i m e D a t e / T i m e Method of Shipment: ^ ^ 1 0 0 1 8 7 ATTACHMENT G 100188 YORK LABORATORIES DIVISION ATTACHMENT G /^.f-^ CERTIFIED REPORT TRANSMIHAL REPORT NUMBER 3 0 8 5 0 - 1 4 5 DATE_ November 12, 19 8 4 CLIE.NT Enviro-Sciences, Inc- 19 Copeland Road Denville, New Jersey 07834 AHENTION ]ZZ^ Ir^j Cohen • The above referenced report is enclosed. Copies of this report and supporting dctc will be retained in our files in tfie event ttiey are required for future reference. If ttiere are any questions conceming ttiis report, please do not hesitate to contact us Any samples subnnitted to our Laboratory will be retained for a maximum of sixty (60] days from receipt of this report, unless other arrangemenrs are desired. Naturally, cs in the pest, our staft will be pleased to quote on any future requirements you may have. 'n addition to the sen/ice provided, we also offer the following: Hazardous Waste Analyses Product Evcluction'R&.D Water and Wastewater Analyses Air and Process Gcs Analyses Industrial Hygiene Surveys fvletallurgical Analyses fvlicrobiologicci Analyses Mass Spectrometry Services ruly Y o u j s ' / ^ Robert Q. Bradley Vice President C. .NC. 100189 November 12, 1984 30850-145 ENVIRO-SCIENCES, INC. 19 Copeland Road Denville, New Jersey 07834 Attention: Mr. Irv Cohen PURPOSE Nine (9) soil samples were submitted to York Laboratories for determination of toluene and pyridine on a quantitative basis. Other compounds found in the samples were also indentified and are reported on a semi-quantitative basis. The samples were also analyzed for oil and grease. METHODOLOGIES The samples were analyzed for toluene using the dynamic headspace Gas Chromatograph/Mass Spectrometry method in accordance with Chemical Analysis of Sediments and Elutriate Testing, EPA 1979. A Tekmar Model LSC-3 Purge and Trap interfaced with an HP 5995C GC/MS/DS were used for the analysis. The samples were analyzed for pyridine and oil and grease in accordance with EPA/CE-81-1 Procedures for Handling and Chemi- cal Analysis of Sediments and Water Samples, May 1981. An HP 5995C GC/MS/DS was used for the pyridine analysis. RESULTS The results are listed in the following tables. Prepared by .ZJl^ Gail D. Sprio Senior, Chemist oenxor v..neraisx A Approved by: U/>/^^../ C • IAAJ.UZC' J^ejzitey C. Curran Ghiigt'X:hleraist ^ GDS/JCC/mz 100190 TABLE 1 ENVIRO-SCIENCES, INC. TOLUENE AND PYRIDINE RESULTS Sample Identification 20 Septic 20 A-2' 21 A-2' 21 A-4' 25 - 2' 27 - 2' 32 - 2' 35 - 4' 36 - 2' (Auger) Toluene ug/kg (pob) 540 690 15 43 210 16 15 8 7 Pyridine ug/kg (ppb) <1,000 <1 ,000 <1 ,000 <1 ,000 13,000 26,000 43 ,000 <1 ,000 <1,000 100191 Samole Identification 20 Septic (Auger) 20 A - 2' 21 A - 2 21 A - 4 2 5 - 2 - 2' 3 2 - 2 35 - 4' 35 - 2' TABLE 2. ENVIRO-SCIENCES. INC. Compounds Found 1,1-raethylene bis-benzene diphenyl methanone methylene chloride chloroform benzene methylene chloride chloroform benzene ethyl benzene total xylenes methylene chloride chloroform trichloroethylene benzene tetrachloroethylene ethyl benzene methylene chloride chloroform benzene methylene choride chloroform benzene methylene chloride chloroform benzene methylene chloride chloroform 1,1, l-trichloroethane benzene methylene chloride chloroform 1 ,1 , l-trichloroethane benzene methylene chloride chloroform benzene Concentration* 8,400 64 ,000 <5 12 <5 <5 5 <5 68 600 <5 <5 <5 <5 <5 7 <5 <5 <5 <5 5 <5 <5 19 <5 <5 <5 <5 <5 <5 13 11 <5 <5 <5 <5 1.5) 0.5) 2.3) 0.9) 4) 3) S) 6) 9) 2.2) 2.6) 0.4) 1-7) 0.4) 2.2) 0.6) 4.4) 4.2) 0.8) 0.8) 2.4) 0.4) 1.6) 1.4) 0.2) ^Results are reported on a semi-quantitative basis 100192 TABLE 3 ENVIRO-SCIENCES, INC. OIL AND GREASE RESULTS Oil And Grease Sample Identification mg/kg (ppm) 20 Septic (Auger) 20 A - 2' 21 A - 2' 21 A - 4' 2 5 - 2 ' 2 7 - 2 ' 3 2 - 2 ' 35 - 4' 36 - 2' 241 566 1 ,500 27.9 89.6 137 50.6 39 .5 965 100193 YORK LABORATORIES DIVISION (^yy/rr^ CERTIFIED REPORT TRANSMIHAL REPORT NUMBER 30850-1195 DATE Septe:nber 25, 1985 CUENT E n v i r o s c i e n c e s , I n c . 19 Copeland Road D e n v i l l e , NJ 07834 ATTENTION Dr. A. Kyles The above referenced report is enclosed. Copies of this report and supoorting data will be retained in our files in the event they are required for future reference. If there are any questions conceming this report, please do not hesitate to contact u i Any samples submitted to our Laboraton/ will be retained for a maximum of sixty (60) days from receipt otthis report, unless other arrangements are desired. Naturally, cs in the past, our staff will be pleased to quote on any future requirements you may have. In addition to the service provided, we also offer the following: Hazardous Waste Analyses Product Evaluation/R&D Water and Wastewater Analyses Air and Process Gas Analyses Industrial Hygiene Surveys Metallurgical Analyses Microbiological Analyses Moss Spectrometry Services V^y Truly Yourv/' Robert Q. Bradley . Vice President ^ 100194 ,c.-.-ce ;;.^6 • :ViC.' September 25, 1985 30850-1195 ENVIROSCIENCES, INC. 19 Copeland Road Denville, New Jersey 07834 Attention: Dr. A. Kyles PURPOSE AND RESULTS Eight (8) soil samples were submitted to York Laboratories for analysis. The samples were prepared and analyzed in accordance with Procedures for Handling and Chemical Analysis of Sediment and Water Samples, EPA/CE-Sf-I. The results are reported in the following Tables. Prepared by; ZII^xv^x^^-^-6^ Daniel F. Ott Laboratory Manager Approved by: ^ i J o , u., C ^ - (z/U<y,^ •J^fr^y/C. Curran /Cftikf Chemist D?0/JCC/md 100195 TABLE 1 30850-1195 ENVIROSCIENCES, INC. Sample Identification Toluene, ug/kg Drainline #1, 6/7/85 4 p.m. 140,000 Drainline #2, 6/7/85 4 p.m. 310,000 Dryer SI, 6/14/85 10 a.m. 1,500,000 Dryer #2, 6/14/85 10 a.m. 150,000 100196 Y'.VC. !\'C. • 2ZZ McP'CS T^.TCi'<e • ••Acr.rce. Cznr.zrzr.es. C6^6£ •i2Z2'; 2z'-^z3. TABLE 2 30850-1195 ENVIROSCIENCES, INC. Sample Identification Pyridine, ug/kg Lab Pit #1, 6/14/85 3,900 Lab Pit #2, 6/14/85 <150 Lab Pit #3, 6/14/85 510 Lab Pit #4, 6/14/85 180 100197 >VC. '->^IC. • 222 */'c.~'c-? '^rrz.'<e • Mc^rce. 2zr.r.ecz.z'z: C;6-c; • !2-3' 26'-—53 YORK LABORATORIES DIVISJON '/zyrr CERTIFIED REPORT TRANSMIHAL REPORT NUMBER 30850-1283 DATE September 2 5 . 1985 CLIENT E n v i r o s c i e n c e s , I n c . 19 Copeland Road D e n v i l l e , NJ 07834 ATTENTION Dr. A. Kvles The above referenced report is enclosed. Copies of this report and supporting date will be retained in our tiles in the event they are required for future reference. If there are any questions conceming this report, please do not hesitate to contact us. Any samples submitted to our Laboratory will be retained for a maximum of sixty (60) days from receipt of this report, unless other arrangements are desired. Naturally, c% in the past, our staff will be pleased to quote on any future requirements you may have. In addition to the service provided, we also offer the following: Hazordous Waste Analyses Product Evaluatioa'R&.D Water end Wastewater Analyses Air and Process Gas Analyses Industrial Hygiene Surveys Metallurgical Analyses Microbiological Analyses Mass SpectTometr/ Services Robert Q. Bradley Vice President / 100198 r.vr Mc-rce rw.-rc:.;3 • ^icrrce. Cc: September 25, 1985 30850-1283 ENVIROSCIENCES, INC. 19 Copeland Road Denville, New Jersey 07834 Attention: Dr. A. Kyles PURPOSE AND RESULTS Six (6) soil samples were submitted to York Laboratories for analysis. The samples were prepared and analyzed in accordance with Procedures for Handling and Chem.ical Analysis of Sediment and Water Samples, EPA/CE-81-1. The results are reported in the following Tables. 'repared by; ^^^.y,^' ^ - t : Z ^ Daniel F. Ott Laboratory Manager Acoroved bv C. Curran hemist DFO/JCC/md 100199 T.VC. :NJC • z r : Mcr-ca :'jrT.-z: ••/crrce. :nr.:?c TABLE 1 3 0 8 5 0 - 1 2 8 3 ENVIROSCIENCES, INC. Sample I d e n t i f i c a t i o n T o l u e n e , ug/kg 5434 - D r y e r , 7 / 1 / 8 5 7,700 5435 - D r y e r , 7 / 1 / 8 5 920 100200 •.VC, :.''JC. • 2C3 ''/ic."ro3 Tc.rc:/e • 'Vlcnrce. Cc-r,ecr:c-: Cd-ic; • '22;'. 25'-—;£i TABLE 2 30850-1283 ENVIROSCIENCES, INC. Sample Identification Pyridine, ug/kg 5436 - Lab Pit, #1, 7/1/85 1,100 5437 - Lab Pit, #2, 7/1/85 3,400 5438 - Lab Pit, #3, 7/1/85 <150 5439 - Lab Pit, #4, 7/1/85 <150 100201 n v c . :NC. • 22C .Mcrrce 'u.-Ci^e • !'Azr.rzs. Czrr.Bczz-s: 06Ui5 • •22;', 2i'--^£3 YORK LABORATORIES DIVISJON 7Z7zrj- CERTIFIED REPORT TRANSMIHAL REPORT NUMBER 30850-13^3 DATE September 26, 1985 • CL'ENT AHENTION Envirosciences, Inc. 19 Copeland Road Denville, NJ 0783A Dr. A. Kvles The above referenced report is enclosed. Copies of this recort and supporting data will be retained in our files in ihe event they ore required fcr future reference. If there are any questions conceming this report, please do not hesitate to contact us. Any samples submitted to our Laboraton/ will be retained fcr a maximum of sixty (60) days from receipt of this report, unless other arrangements cre desired. Naturally, as in the past, our staff will be pleased to quote on any future requirements you may have. In addition to the service provided, we also offer the following: Hazardous Waste Analyses Product EvaluatiorvR&D Vv'ater and Wastewater Analyses Air and Process Gas Analyses Industrial Hygiene Surveys Metallurgical Analyses Microbiological Analyses Mass Spectrometry Services Very Truly Yoi Robert Q. Bradley Vice President 100202 •^vvc. : N C .-"JC '-A- : e •.•W.T.C:J<^ September 26, 1985 30850-1343 ENVIROSCIENCES, INC. 19 Copeland Road Denville, New Jersey 07834 Attention: Dr. A. Kyles PURPOSE AND RESULTS Four (4) soil samples were submitted to York Laboratories for analysis. The samples were prepared and analyzed in accordance with Procedures for Handling and Chemical Analysis of Sediment and Water Samples , EP.A/CE-8 1-1 . The results are reported in the following Tables. Prepared by: —^^U. ..> r-cSH Daniel F. Ott Laboratory Manager Approved by: Q - y ^ ^ C-- ( , / U ^ ^ . yjffk-p^ fZ. Curran /^'hA^r Chemist DFO/JCC/md "X/ 100203 TABLE 1 30850-1343 ENVIROSCIENCES, INC. Sample Identification Toluene, ug/kg 5753 - Dryer 600 5754 - Drver 660 100204 /'.VC. :.NC. • 222 r/cr.,'ce Tu.—.ciiee-Mc,".rce. Ccr;r.ec:;c'jt 26^:63 •1,2031 261-^-^53 TABLE 2 30850-1343 ENVTROSCIENCES, INC. Sample Identification 5751 - Lab Pit #2 5752 - Lab Pit #1 P y r i d i n e , uc/kg <150 <150 100205 'V.'C. INC. •222.Mcr,rc j.T-.cike • v.orrce, C; JT 06^65-'2231 261-0453 YORK LABORATORIES DIVISJON W.'f^ CERTIFIED REPORT TRANSMITTAL REPORT NUMBER 30850-14AA DATE. September 25, 1985 CUENT Envirosciences, Inc. 19 Copeland Road Denville, NJ 0783A AnENTION Dr. A. Kvles The above referenced report is enclosed. Copies of this report and supporting data will be retained in our files in the event they are required for future reference. If there are any questions concerning this report, please do not hesitaie to contact us. Any samples submitted to our Laboratory will be retained for a maximum of sixty (60) days from receipt of this report, unless other arrangements are desired. Naturally, as in the past, our staff will be pleased to quote on any future requirements you may have. In addition to the service provided, we also offer the following: Hazardous Waste Analyses Product Evcluation/R&D Water and Wastewater Analyses Air and Process Gas Analyses Industrial Hygiene Sun/eys Metallurgical Analyses Microbiological Analyses Mass Spectrometry Sen/ices Roberto. Bradley Vice President ^V/C.. ' 2C2 N'tCT-'cs 'w.T.ci-^3 • "'icrrcs. Ccrr.s-cTicui Ji—o'j • 100206 September 25, 1985 30850-1444 ENVIROSCIENCES, INC. 19 Copeland Road Denville, New Jersey 07834 A-ttention: Dr. A. Kyles PURPOSE AND RESULTS Five (5) soil samples were submitted to York Laboratories for analysis. The samples were prepared and analyzed in accord- ance with Procedures for Handling and Chemical Analysis of Sediment and Water Samples, EPA/CE-81-1. The results are reported in the following Tables. Prepared by: ....j P' c x ^ Daniel F. Oct Laboratory Manager .^y.:i C - (yCc^^y,. ^proved by; v^,^^/.-.. v_ - -.^c^v./., ^fifrey* C. Curran :hemist CFO/JCC/md 100207 '^•VC. i.NC. • 222 i'vic.Tce "u.T'.CKa • Mcrrcs. CcrnecT;c'_t Zt~tZ • '^O;' 261-—ici TABLE 1 30850-1444 ENVIROSCIENCES, INC. Sample Identification Toluene, ug/kg ICC Berlex, 8/7/85 1:00 360 100208 ",VC. ;MC. • 222 Mcr.rce Turoike • -V.cr.rce, Ccr,nec:;cuT C i ^ i ; • i222-, 26V^c = TABLE 2 30850-1444 ENVIROSCIENCES, INC. Sample Identification Pyridine, ug/kg ICC Berlex - Lab Pit, 8/7/85 12:00 2,700 ICC Berlex - Lab Pit, 8/7/85 12:00 <150 100209 '•''.VC. ' C. • 222 V'cr^'cs TL.'.'HC--'? •-'vicr'c^ O—~'^?CT;c'j.'Ci«c£ "'2221 Z-i-*—--53 TABLE 3 30850-1444 ENVIROSCIENCES, INC. VOLATILE PRIORITY POLLUTANTS All results reported in ug/l. Sample Identification Compound chloromethane bromomethane vinyl chloride chloroethane methylene chloride trichlorofluoromethane acrolein acrylonitrile 1,1-dichloroethene ",1-dichloroethane trans-1,2-dichloroethene chloroform * ,2-dichloroethane "•4,1,1 -trichloroethane carbon tetrachloride bromodichloromethane 2-chloroethylvinyl ether ',2-dichloropropane trans-1,3-dichloropropene trichloroethylene benzene cis-1,2-dichloropropene c ibromochloromethane *,1,2-trichloroethane bromoform tetrachloroethylene ', , 1 ,2-2-tetrachloroethane toluene chlorobenzene erhyl benzene ICC B e r l e x Lab P i t 8 / 7 / 8 5 3:00 <10 <10 <10 <10 <10 <10 <100 <100 <10 <10 <10 <10 <1G <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 22 <10 <10 ICC B e r l e x Lab P i t 8 / 7 / 8 5 3:00 <10 <10 <10 <10 <10 <10 <100 <100 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 21 <10 <10 ICC B e r l e x Lab P i t 8 / 7 / 8 5 3:00 <10 <10 <10 <10 <10 <10 <100 <100 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 360 <10 <10 100210 '.^VC..^JC.•222 Mc _rrc.'<s • 'V^cr'cs. Ccr.r.ectlcjT 26—63 • '222". 2i1-«i'i£r. ATTACHMENT H 100211 h A GENCKiU. jNrOTlMATIOM C E N E R A T O A I ITI AOOnESS .ZF<zz>y^ <^p^J' o ^ . t n i M i . r t t U M L t SHEET * ^ ATTACHMENT H •iOH l _ U VJ v-i U ^ Z'^^'t^-"/^. y^-^-'yo*<, /yi<7.»-.-y>c^/ , C^^^yyT-rfSrir/z-t _l^»NSPORTE«PHONE.i'r'<^'^/'r'r.z.-ytyt^T/tfZ"^ -, :^NE«*To«usEP*,o. y , i DP.9n^::),)p.<?5. J GENESATOB STATE l.O. l_ I TECHNICAL CONTACT: - 5 ; .. ' i^^..t r.. i^.trt. yyjr^y.*^ r!<y*^yc /Zrn^^ ^ ^ - ? ^ TITLE: L lA' <i AZt.fi"^^r-' _l PHONE 1 ft/<^yZf<rrp-s'zym taoy/SiSi: . ^ ^ . y i PnOCESS C E N E n A n N C WASTE: U f ^ / • PHYSICAL CHA.HACTEJHSTICS Of WASTE COLOR ^ C i y> •«t^^ - / < ^ c ooon ^ ^ NONE LJ uiLO D STRONG DESCRIBE L. PHYSICAL STATE O 70*F / S SOLID L J SEMISOLID D LIQUID U POWDER LAYERS C MULTILAYEREO L J 8IL>TERE0 / Q SINGLE PHASED FREE LIQUIDS D Y E S ^ y VOLUME I ' P H : D < 2 I a ' • M-IO • 10.1-12.5 ft • EXACT i_ • N/A SPECIFIC D < » GRAVITY ; s ; i . i . i j Q EXACT D 1.3.,.. Qi.s...? D > '•'> FLASH D < " • ' ' POINT • > W5"F Q 7 0 - F - 1 0 0 - F ^ ^ NO FLASH • 101 -F • l.'«-F Q EXACT , Q 1 4 0 - F . 2 W F Q CLOSED CUP Q OPEN CUP C CHEMICAL CCMPOSJTJIJN (TOTALS MUST ADO TO 1 « ' / . | :A 'atLiyr yy^^^yZ^f^yZi ( ^ ^ • ^ ^ - ^ ) -r>,tfL ( ^- ' ^ y ' Z * ' ^ z^^. -y^y L. ' r ^ ^ ' - ^ o / fl. <ra. exiy ^ ^ v . -T*' J \ 0 METALS • TOTAL (PPMI G ARSENIC (A«) 1 y y ^ yiy/} EPA EXTRACTION PROCEDURE (mg;L) , < BARIUM iBai CADMIUM (Cd) CHROMIUM (Cr) MERCURY (Hg) LEAD (Pbl SELENIUM (S«IL. SILVER (Ag) i_ y ^ ^ y ? COPPER (Cul I . yyy^ yr/" yyy^ yt//f^ NICKEL (Nil L ZINC (Znl \_ yyy^ Ay9 ^ \ CHROMIUM.HEX (Cf • «l L. yC//il TKALUUM(TI) L. y/y!^ OTHER COMPONENTS - TOTAL (PPM) CYANIDES I NQK£ F SHIPPING INFCRMATION O.O.T. HAZARDOUS MATERIAL? " y O ''ES D NO /^^-^/<i.off<ij (ZZ^'i^/z. J^^/zi y^y<ry , ^ .-jSONi^ CROPER SMIPf»1NG NAME I HAZARD CLASS I t s y y ^ y ^ ' t ^ J ID. NO, METHOD OF SHIPMENT: D BULK UOUIO S0RUM(TYP£(SI2E) L. tyr^y'-pyrfiant'^^/^t \ZZ\ BULK SOUD ANTICIPATED VOLUME; L. - I GALS. L. J CUBIC YARDS PE.SL- > S ' o N E TIME D QUARTER ..• ' OTHER L_ D WEEK D YEAR f^ray/j^ L J MONTH D, SULFIDES G HAZARDOUS CHARACTERISTICS PCB-S PHENOLICS R E A C T I V I T Y : S NONE D EXPLOSIVE D PYROPHORIC L J WATER REACTIVE D SHOCK SENSITIVE U OTHER \ ^ftiP OTHER HAZARDOUS CHARACTERJSTJCS; ^ I NONE - G RADIOACTIVE D ETIOLOGICAL U PESTICIDE MANUFACTURING WASTE D OTHER \ USEPA HAZARDOUS WASTE7 D YES O NO USEPA HAZARDOUS CODE/S) I I r ^ ^ * — t I j STATE HAZARDOUS WASTE? D YES " ^ ^ N O yyy< STATE COD£(S) L. H SPEQAl. H A N S U H O INFORMATION y^s > > t - Alt (XUy^ cf'. KLjOf(jLa7 ^ Hl^^&,r> •iryr-'- n ADDITIONAL PACEIS) ATTACHED (EST CEBTIF* THAT ALL INFORMATION SUBMITTED IN THIS AND ALL ATTACHED DOCUMENTS IS COMPLETE AND ACCURATE, AND THAT ALL KNOWN OR bwoPtCTED M A i A t O S HAVE BEEN DISCLOSED. l U ^ d i t o i ^ D SIG^'^TURE TTTLE OATE 100212 i GENERATOR'S WA« MATERIAL PROFILE SHEET Z-1 -r ^^ v^ 'w i_ < dENCRAI. IMf.SnMATION GENERATOR N TY ADDRESS AUE. 1 -^Z£p.ui> C/vyy^oj ^^^^^^'/rav//'j^'^yii^ yZs>^v) * I ' — • ' _l TRANSPORTER "y^^^uA. y*f^x.»Jc "yZzarfsy^T J TRANSPORTER PHONE: , ' <ZZyyy/73r)*/yrz.t Jfr . < 0 < i / ^ ^ 2 . - / < l . € 7 / ^ ^ ; , / ) J . GENERATOR USEPA AT-, ^ j t e / i y y / y f <i?o/2o.{ ID. y A ^ t ' ^ / p . ^ . s - y o , 9 r . TECHNICAL CONTACT: L. .p<c^.cT. • /f^yCooaS £y/^fS. y^^a/c rVoS Z/ / c J GENERATOR STATE ID, L. • ^ c U / y - yZxty /dffy/>ty Jct^cM) , T,TLE, , kycri. ^^A^/?^A/r—' J PHONE: , f/9yit<>9-r//2.. ?^y.ri \t P*»OCESS GENERAT-.NG WASTE; L Ir^jtATc^ / w y ^ ^ . / ^ ^ ^ y ^ /^^ffr-C yntAo,^ y ^ ^ y j ' f g . c ^ n : J I < PHYSICAL CHARACTERISTICS OF WASTE COLOR ) S i OOOfl U NONE ' ' a j MILD D STRONG / ^ t y a / i DESCRIBE L. PHYSICAL STATE e JO-F D SOLID D SEMl-SOLIO ^ S LIQUID D POWDER LAYERS G MULTILATERED D^l-LAYEREB rSJ SINGLE PHASED FREE LIQUIDS ' ^ Y E S ^ VOLUME L yas NO %J PH: D * 2 • 7.1.10 • 10.1.12.5 D> ' " • EXACT i_ D N/A SPECIFIC D < GRAVITY ^ ^ .81.0 G ' - i - ' - j G EXACT L Q 1.3-1.4 D '5-1.7 CHEMICAL CCMPOSITION (TOTALS MUST ADD TO 100%) t^<y<7£/c^ - J L _ ^ f ^ v . FLASH 0 < 70'F POINT G'0-F.100*F /^^3fV > y « ^ 22 O < / 0 f * ^ ^ > 5 a X ^ ^ t T / t V W ^ _ r / i . Q t o / • tr Z^f j < . S d A / S i A / ^ \ "^. IF r r ^ .t^-^tSTvrK'ec- >y4wc- y^£;frz. z^. / ^ v c ^ c / g - • ^ y g ' / ^ y a n ^ Z ^ r ? . c / , ,<ro.or -,. ETALS ARSENIC (Aa BARIUM |B« O O M I U M (Cd) Q > 200-F ^ Q NO FLASH • 101 -F . I39-F Q EXACT , G 140-F-200*F Q CLOSED CUP G OPEN CUP TOTAL (PPM) L C C o f EPA EXTRACTION PROCEDURE img/U < / yi^ g . c o , ^ CHROMIUM (Cr) L. MERCURY (Hg) |_ LEAD (Pt» L. <::». ^ J J 7 If. o t r MATERIAL? F SHIPPING I N F C R M A T I O N D O T . HAZARDC PROPER S H I P « > I N 3 N A M E L HAZARD CLASS I - ^ ^ ^ ' ^ X YES *•, G NO ^ . ' C O / / CHROMIUM.HEX ( C r . S l L . THER COMPONENTS - 'CTAL (PPM y Z ^ l . SELENIUM (S«)L_ SILVER (Ag) l _ COPPER (Cu) l _ NICKEL (Ni) 1 ZINC IZtw L_ THALLIUM f r h ) l _ ^ r a. ear's a . o o f , a . r r j , a . 9tfo , ^./r-, i y . o z f , PCBS y < y a ^ ^ PHENOLICS L a. y£f METHOD OF SHIPMENT:' Q BULK UOUIO GoRUMfTYPE/SIZE) I J 1.0. NO. ^ / < ^ - < ? ^ , P.O. t * ^ ^ ^ . G BULK SOLID ^y^9*t^ ^ ^ ^ ANTICIPATED VC»L.ME: L. J GALS. L _1 CUBIC YARDS €?t: ^ S o N E TIME Q QUARTER J OTHER l _ G WEEK G YEAR ^ooa /Af Q MONTH G, AZAROOUS CHARACTERISTICS REACTIVITY>SJ NONE Q G EXPLOSIVE'' PYROPHORIC U WATER REACTIVE G SHOCK SENSITIVE Q OTHER I OTHER HAZARDOUS CHARACTERISTICS: y S NONE U RADIOACTIVE Q ETIOLOGICAL U PESTICIDE MANUFACTURING WASTE G OTHER i USEPA HAZARDOUS WASTE? ^ S YES G NO USEPA HAZARDOUS COOES) 1 ^ ^ ^ • i ^ ^ ^ f , ^ A ^ V , STATE HAZARDOUS WASTE? Q YES ^ S NO STATE CO0E(S) i / y ' T ' -•• SPECIAL HAA SLING INFORMATION yyyit^^. yy:^^//e^:fi -u-T" ALL TUa/X^ J • hUjLO^ Q ADDITIONAL PAGE(S) ATTACHED JEREBY C£HT-=^ THAT ALL JNFORMATION SUBMITTED IN THIS ANO ALL ATTACHED DOCUMENTS IS COMPLETE AND ACCURATE, ANO THAT ALL KNOWN OR j M K C T E D H A Z A R D S : H A V ^ M I N OISCISSEO. |R1Z£P SK^HATUR( TTTLE DATE 100213 J * • ^ • - - ^ ^ ^ ..-3 I -^..^M.^^^^—^^^—.^ • I = ORM WMl-600C-e. : e i S U WASTE MANAGEMENT, INC v ^ GENERATOR'S WAS .MATERIAL PROFILE SHEET u ^ c o u ^ OTENERAL ^ O A M A T I O N GENERATOR zP/^y^/<:6 c (Z^^Tf^^ ( S x . /<4^ y ^ j j ) 4 J TRANSPORTER U y^?<tji yfyrcu^ yyz^jA^r-^ . r r ADDRESS L. ;Pa 2 ^ <i77S _| TRANSPORTE»» P M O N E : L C^A^/e/rr^^setsnifi ^ d / ^ r z - y ^ < 7 ( ^ ^ „ / ) TECHNICAL CONTACT r r . ^ j i ^ y / S / . f . rya/2o _l GENERA ^/yi/r> y / P 9 P 9 ^ r / f > ^ 9 r J GENERATOR STATE I D . _l TITLE: L y/cz, ytu'j'j^r' _I PHONE. L NAME OF WASTE.!. y,^-B/eM^m ^^/&frt tj^'xi •»«/• 9^9/f9? -<V2- ^'<, y ' j Y ^ - ^ a r i PROCESS GENERATING WASTE: L yc^rjjy^ 5 Q . 1 • PHYSICAL CHA*ACTERISTICS OF WASTE COLOR y y ^ r t ODOR G NONE i j i MILD G STRONG t* - rf mi-m y DESCRIBE L. PHYSICAL STATE O 70*F ^ S SOLID G SEMLSOLID G LIQUID Q POWDER LAYERS D MULTILAYEREO G B I . I A Y E R E O ^ SINGLE PHASED FREE LIQUIDS G YES * S NO VOLUME L. OH: G < i G <•'•«•» I I 10.1-12.5 • > 12.5 ; I EXACT I GN(A SPECIFIC G < •' GRAVITY G »-'-o g ] i . i . i j G EXACT G '-3 G'.5- G>' 14 1.7 7. FLASH G < ' f ' ' G > » < ' ' ^ POINT Q T O ' F I O O - F ' ^ g NO FLASH Q 101 'F . 139'F Q EXACT , G 140*F. 200-F G CLOSED CUP G OPEN CUP C CHEMICAL CCMPOSITION (TOTALS MUST AOO TO 1W%I Sa/c • rf/trm>^4cCt4Ae^ (^^yiay^u)^ WF "pjeiia^ yer'£s><:jYci)4/£)^ v>:Vv«. - i v y y ^ e S ' y i ^ ^ ^ / C ^ j a r w /A/C/iozZtJ^rU ^9.3 ... ^ ^ ^ v . a.fZ. yy.e/ -r.*/ -r.^/ D METALS Q j ARSENIC (At) BARIUM (Bal CADMIUM (Cd) CHROMIUM (Cr) MERCURY (Hg) LEAD (Pt» TOTAL (PPM) Q EPA EXTRACTION PROCEDURE (mg(U SELENIUM (Sail yj/y y / t ^ _i SILVER (Ag) i_ Az:^ yy/^ COPPER (Cu) L. yyy yyy^ yyy? NICKEL (Ni) L ZINC iZnl I ri//f y y y yy/A THALUUM(Th).L. yyyp CHROMIUM-HEX ICl • «)(_ E OTHER COMPONENTS - TOTAL (PPM) r f SHIPPING INFCRMATION ! I D.O.T. H A Z A R O O L S MATERIAL y y y y y y _i PCBS y y y yyy J PHENOLICS L y y y 1 PROPER SHIPWNG NAMEL ,? y B YES G NO HAZARD C l > S S L. METHOD OF SHIPWENT: G BULK UOUIO 7 C \ DRUM (TYPE/SIZE) J 1.0. NO. y < ^ ' 9 / < r 9 , pQ , < : A f ^ G BULK SOLID ANTICIPATED VOLL.-VE;L. i « ( L : . r r ^ 2or /7y/ S. L. J CUBIC YARDS PE . ^ L _ i .OTHER l _ ONE TIME G WEEK G QUARTER Q YEAR y/jooe /£s Q MONTH G. L C HAZARDOUS CHARACTERISTICS R E A C T I V I T Y ' S NONE G PYROPHORIC G SHOCK SENSITIVE G E X P L O S I V E ' Q WATER REACTIVE G I I OTHER i_ OTHER HAZARDOUS CHARACTERISTICS: X NONE G RADIOACTIVE Q ETIOLOGICAL G PESTICIDE MANUFACTURING WASTE G OTHER I 'XI YES 1 STATE HAZARDOUS! WASTr? G YES .'NO STATE COD£(S) I H SPEOAL H A N C J N C INFORMATION yirinr<. AZe^ 7 ^ V t C ^ < K < _) USEPA HAZARDOUS WASTE? . ^ YES G NO USEPA HAZARDOUS COOES) ^ ^ ' • < ^ ^ * - • • ^ ^ ' ^ • ^ ^ ' ^ • < •T-^ • - ' , •'T^ ^ 1 .G ADDITIONAL PAGE(S) ATTACHED / J 8 I ^ I ^ ^ ^ ^ ^ B Y CEHTIFT JHAT *LLiIwi=(JJ(M»f ION SUBMITTED IN THIS AND ALL ATTACHED DOCUMENTS IS COMPLETE AND ACCURATE, AND" THAT ALL KNOV^U-OR: ; • 1 ^ ^ B T C T E D MAZAF»3S'TtAVE~BEEN-DISCLOSED. - ' \ ' • S R l r t D 6 i P > * n » n E -vi « • i « ! i r » _ . . » • TITLE •OATE . . y l k Z^y2:!/-'{^^d'yy^^^y^^/^ . = ORM wMi-«aoo-e'e.^ C 1S&3 WASTE MANAGEMENT. INC. 100214 v<sy GENERATOR'S WASTE iTERIAL PROFILE SHEET T l i ^ ^ D 48603 M: QCMrHAL IMFOAW.ATION . E N E R A T O R N A M E . I ADDRESS 2 : ^ : ^ ^ ^ ^ > r ^ c C ^ ^ . ^ ^ ^ c c ^ y . ' ^ y r ) , ,«,^3^,,E, . / ^ P ^ c r ^ x ^ . ^ / - ^ ' 7 ^ ; w » , ^ , ;?<7. . ^ ^<^?y _ — , TRA^.PORT.:, PHON. • - ^ y K J ^ j t ^ - y < f < 7 / ^ Z t r ^ , . ( Z A y y ^ y ^ r / > i ^ j r C £ > - • ' ' - ' ^ ' ^ ' - - - ^ " " ^ . yr. Cyi^^ / y X K r <xy92<y - I GENERATOR USEPA 1.0 yy.byy0^frp<?' E C H N I C A L CONTACT. I <AM£ OF WASTE. I ^ ^ s ^ y . y^ccr /<e:^A>o JL-^aftfi/) J GENERATOR STATE I.O. l_ J TITLE: L yyei y ^ PHONE I Py9/^<?>9 -J^grS, 'OOCESS GENERATItaS WASTE: L ^^A}ocf /WPA^. y^t*t^^yv^zj2/A^^ t^/sryz /"/ytra^v' ^^of/sree- C3SZ. PMYSiCAi. OtAAACTERISTICS OF WASTE » L O « ODOR G NONE G MILO ® STRONG , 8 ^ t y y e t » r € . DESCRIBE I PHYSICAL STATE O W F G SOLID O SEMLSOLID JcQ LIQUID G POWDER G3?-'-'0 G * " ' \ 1 10.1-12.5 T l E X A C T . ^ ^ . SPECIFIC G < •• CRAvmr G-»-'-o G ' - i - ' - j Q lJ-1.4 G'•»•'•? G > 1-'. G EXACT , 1 ^ = - LAYERS ^ S J MULTILAYEREO C l d Bl^ LAYERED 1 SINGLE PHASED •; FREE LIQUIDS ^ Y E S G VOLUME 1 ^ ^ HO FLASH G < ">*^ POINT Q T O - F - I O O - F C H p l l C A L COMPOSITION (TOTALS MUST ADD TO 100%) So/c. ^JyiTzyA. & ^ f j c y / /VC^JE, t TZf _i i^yfL^Z-ei. .3 i / ^ g r. £ e 0 7 y / y ^ y ? i ^ 4 t i J ^ _J L. A C jri. ''»>roy /^/.^C?.*e*«F' S.O 9Ay^ y 7 a » , ^ a ^ ^ - ^ - a ^ . ^ , , C-£ iZ^c^Me^oA^*yi7o p^ur))y(:vn/ci,^yi>/^'tie(arj^<».«4 f,. 0 METALS ARSENIC (As) BARIUM (Ba) CADMIUM (Cdl CHROMIUM (Cr) MERCURY (Hg) LEAD (POI s i > 20O'F ^ CLOSED CUP G NO FLASH Q OPEN CUP Q 1 0 1 ' F • i3»'F Q E X A C T y ^ e ^ G " 0 * ^ •2O0'F TOTAL (PPM) L i EPA EXTRACTION PROCEDURE img/U ^ ^ I SELENIUM fs.li / y y . c G SILVER (Ag) . Z r % y p y y / ^ /Z2.e ^^z J?.7S 6^0 COPPER (Cu) L. NICKEL (Nil I ZINC (Znl I 3 J S Y ^ THALLIUM m i l i y ^ T ' ^ ^ - ^ CHROMIUM.HEX (Cr • 61 u. E OTHER COMPONENTS - TOTAL |PPM) / < t < - SHIPPING INFCRJMAT10N O T . MAZAROOfS M A T E R U L ? < CYANIDES L SULFIDES ^yf- PCBS x^&y«r J PHENOLICS L. ROPER S H I P ^ N G MAME A2AR0 CLASS I ^ ^ y ^ X J YES G NO _| I.D. NO, t yvyp 9 y f 7 , ^n r ^ : ^ G BULK SOLID ETHOO OF SHIPW£,VT: Q BULK UOUIO P S DRUM (TYPE/SIZE) t ^ S j ^ y / t t v / / y y r t^PS'exj N T I O P A T E D V O L L . ' W E . L . _l GALS. U J CUBIC YARDS PER < S J ONE TIME Q QUARTER I OTHER l _ G WEEK G YEAR G OL. MONTH G SHOCK SENSITIVE 0 OTHER \ ^ ^ ^ ^ ^ < 9 C hAZARDOUS CHARACTERISTICS R E A C T I V I T Y : X J N O N E G PYROPHORIC Q EXPLOSIVE G WATER REACTIVE OTHER HAZARDOUS CHARACTERISTICS: ^ C NONE D PESTICIDE MANUFACTURING WASTE G USEPA HAZARDOUS WASTE? Ka't/y^4a>e.^ S o a t f r n ^ G RADIOACTIVE G ETIOLOGICAL - ^ OTHER L. s NO A f^<^y^ ^ e ^ ' 2>ooe /xx>e USEPA HAZARDOUS CODECS) ^ 2 * - ^ • / > O e C - , . / ^ ^ g ? , . £>CO <^ l-l «n /'"^f* STATE HAZARDOUS WASTE? L J YES ^ NO . A/y STATE CODEfS) I SPEOAL KANOLJHC INFORMATION . y j / f v ^ y^^,ttey> E M M .G AOOmONAL PAGE/S) ATTACHED . 1 ^ ^ ^ CERTIFY --i»cT-ALL i-rtORM^TWH SUBMITTED IN THIS AND ALL A H ACHED DOCLMENTS IS COMPLETE ANO ACCURATE AND THAT ALL KNOWN OR U S ^ ^ P I E D M A Z A ^ o s ' i u v a f e i N afccLOSED. ^ ••«•.-: . .,,.. ^ . . . j T B W t t O ^ S i G N A T J R E . , • . , .» ^ - , . , TITLE OATE 1 0 0 9 1 * ^ ; :• >-A- . , y^u. '^a^^y/^cC^ ' / ^ / t \ J ^ /^'r/S^ . 'M wMi-6000-e.ej it:i»a3 WASTE MANAGEMENT, INC. ATTACHMENT I 100216 ATTACHMENT I w ^ ^ ' / ^ S ^ z . z^c,t^^^:ut^ aZt^^^^y^ ^ ^ ^ ^^^- ^^.-. i-'^s^J _^ . y- yiy^^^^-'^^y.^ z^^ cyZ7ZZZzr:.;t;yZZ^ y Z . y . Z^ /^^^^-<. . . ^ J ^ ^^^/^y^^^yrz2),cz^,^ ' ^ ' U - y;ccT£ V ^ ^ ^ - ^ ^ ^ Z Z . . . ^ ^ ^ ^ ^ . . ^ ^ y r ^ 'ji<2yiC', ^ u.,^-yrsc .^.^ ^^,,,2;;^ ^ ^ ^ 100217 ' z- r ^ y ^ / ^ ^ ^ ^ ay^^^^iO!^ ^^,y,^(Z:^^ ^ Z Z / U i ^ u i ^ ^ ' 1 4 U ^ ^y,.c.ny.>d:zy6 yiy^,:^^^^ / ^ / ^ ...:««.^> ,,c^^,c.j^ ^ ^ Cz*^f<^y4ty — (/rt4i4=**'<s<^ C^'ty^ . 100218 ATTACHMENT 100219 ^ y ^ (As Required By The Alabama Depanment of Environmental Management) Kt««fr« orint or TtP* ( f o r m a t s i g n e d for usm on eliit 113-piitni l y p a w i i i t t I U N I F O R M HAZARDOUS W A S T E MANIFEST .er>vr»icr & Name ana .VAamng Acarc&& ^ S i S ^ A C ^/»'Cy:>/C<3.<, ^ o / i - r / V - v y ^ / . v » v ^ y y e a / < ^ £ r t r y a ^ H f ^ f r O I ' t Z T O G « n e r i i O ' ' s Phone ( / « / ) i 9 t t ' ' • * ^ 0 0 1. Ceneraior s u b t P A lO No. Manii«(i / i / / > . ^ . g i g i ^ r ' / ' ( 3 ^ i r ] / ^ ' y " < ? ' ^ i form Approvat , res 7 31-16 2 p.g, ,—r ATTACHMENT J ct 7 . t d 4ie<s F a c a r a i T r a i l e r Number RTMZ 251880 A. S u i a Manifact D o c u m a n i NurrU>ar .-CWMA ••243031 B. S u t a G a n a t w o r ' a (O S. I r a n s o c . e r 1 Comoanv Name T^^fS^o^r-ryryC^ I. I r a r u p o n a r 1 CompaoY Nama 6. LIS EPA 10 Number C S u t a .Tranaponar's 10 O. Trartaoonar* . f h o n a M. l>as>cr^>*0 raciliiY Nama a r ^ iiiie A<ldrau~ C H E M I C A L W A S T E M A N A G E M E N T . I N C . E m e l l t F a c i l i t y A l a o a r n a i - i i ^ m a y 17 at Mile Marker 163 E m e l l e . A J a a a m a 3 5 4 5 9 ~8^ US EPA 10 Numoar | / = ^ / e ! ^ l 9 l ^ l < ? i * ! « l g i r i 7 '<? E. S u i a Tranaponaf » 10 F, T r a n s o o n a f ' i Pnona 1 ^ * l L, US EPA 10 Numoar 0| Oj 0 { 6 i 2 I 2| 4 , 6 r 4 Ca.Suia FaciKTya 10 H. Facilrty • Phona 205/652-9721 1 1 . u s DOT Dvscriplion llnclyding Piopar Stuppmg Name. H a i a t d ClatM. a n d ID Numtserl 12. Coniairtar* No. I Type 13 Total Quaniiiy 14. Unit Wl/Voi 7. W B S U N O . •• //szs^/-c<Ai '^^cJZZi, y^^iy/tO /ycjr^TociytyyytL ^^^ryi/£c^/Bj ^ CIWM Profile NurYioer y O O J i i V ^ < & G ^ iMk ck TZ yyp<ry:yz<pc-:rs U'y^^ yr'^rjcy' ^ c ^ CyoaytWC f c^rc/zc^yj^-/ < ? > f x S > ; ' C - < f " y y y ? 9 r ^ C W M Prof.le N u m b e r ^ r ; ^ ^ g ^ ^ dS^/A '• y i / ^ y y ^ o o j C^y^f^Sac^ ,i/sJ^7^c</^^t^Cfrc^^y^ayeyn) ff/Cr^-^ y - ^ y ^ 9 / / 9 C W M Prodle ^ u m l x r y C y ? ^ 4 ^ 6 ^ * ^ \ ') mz/!A C W M Profile N u m b e r I I Addr.ional Descnpnons for M n e n a i t Listea Atiove ~2 / / / f m Z t M / ^ ^ y - r > / • 7 e ^ ^ * ^ C t , ^ * - ^ r r j S W C •;•:- xiy^y/r" <fjoeu«t. a*^^^^z<yi. yscir^rz:' •'• y/4. ^yyti^^c^y^^f^oy &^ 'A tiy<4:-s.d/£.^y='iyzy^^«^^^y ^ryi^yc^cc^rc hZZ//^. Zdsx //is^o / ^ ' / 7&<uy*^^ z*****? ."^"^ •'-*^ CA/ox^/4t»^ty I I I I I ti. HarKjIinj) CoOes lor W a s t e s b s i e d AJx7v» ..OS-/ 15. Spectai r a n o i m g instruciions ano Aooinonai J r l o r m a n o n 3. apectai r a n o i m g instruciions ano Aoomonai ( r i o m a i t o n / ^ * z^4:^&ri7isiey /^f>t^z?- <z!y^' /u^^^^^-cyi^y^' \ 6. G E N E R A T O R ' S C E R T I F I C A T I O N : ! nereov ceciare Thai ihe contents o^ inis consignmeni are 'uiiv anc accu^aieiv Oescrioeo aoove Oy prOD«r s n i ^ ^ n g name end aro classi*icO. oackeo. markefl. anO laoele^. anO are m ai( respects m proper condition <or transpon by htghway aceofCif>y to applicaDle international and national government regulations. Unless I a m a small Quamity generator wno has ^t%r\ exempted by statute or regulation from the dury to make a waste minimization cenificauon undaf S e c t i o n 3002tb) of RCRA. l also cenify that 1 have a program m place to reduce the voiume and toxicity ol waste generated lo the degree I have d e t e r m i n e d to be economically practicable and I have selected the method o' irearment. storage, or disposal currently available to me wnich m.-mmires rrie present and future threat to human health and tne environment Prim»c- T y ^ d Name ^ - ^ y . /Zyy^ Signaiur ^'3^^z^^ M o n t h Dsy Year ./,«?,/<? ^ff•J\ '. T 17,Trenjco.Ta' 1 Actcnowiadgement ol Raceipi ol Maierials • R ' A I N s o'S-KiTI T, Jt ;me .ransport Inc I Signature signature . d m /OM.: M o n t h Day rear I 1! n i l 7 b t^ Ifi.Transpone.' 2 Acknowledgement of Receipt of Materials P ^ » d / T i r p « < 3 Name / / A/^XAO^ yEtyy/^yy Stgr^^ure < y . 7 iS^.Discrepancv inOication Space • / / M o n t h Oar ^tar O x^/3 lIR / 100220 O.Facility O w i e r or Operator: Cenilication ot receipt of najardous materials coveraA by this mairficsi f t t ^ t / as noteo m Item 19 •""•^^.W^. PrmiBO/TyT^wO N a m e _ _ - — - ^ " T EPA F « r m B7CX>-Z2 (Rev. 4 - 8 5 ) Previous efl -r<g^ M o n t h D»r Year ^ ^ ^ Mion„Obsolete. STATE OF ALABAMA (Mu^Accompony Shipnnent) J / l l ^ Z ' j O L ^ « « ^ orint o* rvpa (Form aeygtieo for Liif or' f i i ' t n : pitcM ivDewnier I ' 21 .Generator s J o E P A I D No. y r D 9 80 6 s'yo gs^ Manliest Documani No U N I F O R M H A Z A K U g U i . WASTE M A N I F ^ T (Continuatio&'SheeT) 23.Gererator. N.n>e y^^^p^ Trailer Nu.Tjber r<x> y r ^ y y - ^ ' i ^ ^ ^ ^ ^ d>9<;f7o 54 Traniponer ilompany Name ^ ^ ^ •yfi ^ l a n % o i M ^ : , CP"'P«"y Name 25^ US EPA ID Number \ y e. y>yf g<^ ff o s 9 'J 7 . f - o p f t M r : c p u s EPA ID Number 27 form Aop.evffl QMB ^o ^QCW 0404 dp.let 7 31 22.^aj« ' " ' o " " a i i o n in me snaoeo areas 1$ n o i requireo t>y f o o e r a l L Stale Mantleil Oocumsnt Numoar CWMA J y 4 3 ^ 3 / M.State Ganeisioi's ID " N. Slate Trantponar't ID 0 . Trarttooner'i. Phone P. State Trantponer't 10 U.Trantponer't ^ ' l o " ^ 7 1 P _ / l ' ? O C ' 5 / l O 28 US DOT Description (Including Proper Shipping Nome. Haiard Class, a n d ID Numberi Profile Numtier y ^ L S ' 2 ) < ? / 6 £ ' Z J ~ ' ^ ^ 29. Containers Type ^ 30 Total Quantity J l . Unit \A\/\iti Watte No.' t>- '^^Zi^zZv/^/icuS ^ S V / S y^^c/r/i y\y<zj^7z;c</6^<re^cyyccfrcr/>i^ 0^C>^-C^^^vyt_jyX. • CWM Profile Number / C c T f l > ^ P C o . ? '- y^a<y^ z^^'Zc. o5^2 yy^ /^cy/<MCy fd^ir/zffiiie^ ^yyf^iCycy/r9y/y CWMprotiieNumoer^^;/?^ 9 ^ 6 0 9 ^ CWM Profile Number CWM Profile Number CWM Profile Number h. CWM Profile Number CWM Profile Number S. A6C.;.cnal Descriotions for Materials LijtetJ Above fA<r. /<•<(- Vn-( ^ ' ^ F^- Ttfr«grw>ri'— 32. S: TZy. 7y^^^ 'i^izy^jS:,^^^ T. Handling Cooes (or Wastes Lilted Above b. c. 9- h: »<;^^—Hanc :no instructions ana Aoomonai i">r"'a'.f>n t i y . _ , , ' . ' - . y ^ • x - ^ ^ ^ j ^ ^ • y ^/c .^^<y^^j^^^^<<y^^<^^ ^y^^^-y^^^^^t^^c^^ ^ -/yjyy-yyp^yz^.c^/e ^^^/^ZuA^tyyfC^<^ dP^ (ir^<^ . yZyltfu^^.^'^^iy^y^^^, 33. T r e n i c o n e r Acknovvfe<3gemenI of Receipt of Materials 3^ Date Printe<:/Typ«d Nerne i^r7".r. u TiuubpuiL inc" -au:: - & ^ ^ U i Month Day Year 1 t o l 1 ? ! « < 34. Tf»ns;>onef " ^ AgknowleOgement or Receipt o< Meionals Printei3/Typ*d Name /-> / / Simiature ' j ^ ^ Date Month Day Year 35. Oiacfeoancy Irxlicstion Space rx%^ 100221 nAZ.A.iUUU5VVASTL IVlAN!^tb! ^ ^ (As Required By The Alabama Department of Environmental Management) ^l«4k« print or rvp* f f o r m designed for use on ehie 117-pitch) lype^^rner } f o r m Approvet) OMB f^o iOOO-OaOa t i o i r t i 7 31 86 UNIFORM HAZARDOUS WASTE MANIFEST M a n i i a i t 1. Oenoiaior s US fcPA 10 So / • / ' ^ • 9'ff' c<^ • / , I a.9 ir]j^°tWi>'*-l. 2. Page 1 of X intormaiion in tne snaoeP areas I t n o t r e q u i r e d b y F e o e r a i law ~3. {jeneraior s .Sarr^e ano Mamng Aooia&s ZZZsiS*J.C ^r/CyJfC^^ Cf^i^Ol^t^ 4, Generators Phone ( Z d / ) ^ f d ^ ^ ^ O O T r a i l e r Number RTMZ 251880 A Stata Manitast Oocumani Numoar .-CWMA-.. 243031 S. S u i a {janaraior a 10 . . ' . " • • ' ' . • • • . - • . - Iransponer 1 Comoany Name 6. US EPA 10 Numoar C S u i a ..Tranapooar a IO 0 . Tranaponar'a f t K m a / . i r a n t p o n a r ^ Company Nama y. Uesignaiaa Facility Nama anC \stl9 A d O r a u ~ ~ C H E M I C A L W A S T E M A N A G E M E N T , I N C . E m e l l e F a c j i i t y A l a o a m a H i T i m a y 17 at Mile M a r k e r 1 6 3 Emelle. A l a b a m a 3 5 4 5 9 T USiPfi 10 Numoar E. SiBia Tranaponat > IO J^^li£lfj£i£_lf_!.li*i£I2-l£. f. Tranaportar'a Phona ia u s EPA 10 Number C S i a i a Faciiitya 10 ) A | L| D| 0| 0 , 0 , 6 ) 2 , 2 | 4 ) 6 | 4 H. Faciiny'a Piyjna 205/652-9721 1 1 . u s OOT 0«scription (Including Proper Shipping N%m». H a t a r d Clata. antI ID N u n ^ a r l 12. Coniainars No. I Type 13. Total Quantity 14. Unit I W t / V o l '• \ . • • Wane No. »• yysZr^yyrZco^ ^-^ycjy/i, yyi^u/y^ yycs^Toccriyyrz:. ^yZry</^t^/^ CWM Profile Number /<?i>?.2J V S 6 d 2 . . M L / ^ I I I I yy?cy:yZ£>Ct:rs u^y^r^ x/^r^/y^^ yy<^^rc^c^tiyyc fC^rc-^'i^yzi^i <^yy-''tr^ yyy?9'^9^ CVJM ?tou\t uumott x^^^^ < y ^ ^ ^ ^Sd/A ! I I /ya^yCyt/)cas OySJfC. SCC^a ,i/C<Z/y^c4/-*id, tjZCf^ce/ecy^ajejn) ^ / C r ^ ~ ^ y-ryJ 9 y y 9 CWM Prodlc Number/^^^ t / / 4 ^ 4 ^ 1 Ij mm I I I I t C W M Profile N u m b e r A<lailional ^^escnptiora for M s t e n a l i Listed Above ^ ///9. Z c s i / ^ - < / y-a 'yi Tet-erd^c x<Wi> ^ ^ J ^ c . / / / . /fyy^e^^/^rifsc/ st> 'A *'/<<: -P^^j /:>i^^KAycy ^rZ^^yc, y c y : ^ r ^ Z/re.. y££T / ^ ^ / ' ^ y 7'S<i^UM€m / ^ x ^ >S.«jP*-c-. (Z/yejtay^Z^^ I I ! K. Hendling Cooes for Wastes Ljsiea Above <y&] .OS I 15. Special nervciing Instructions and Additional Inlormaiion D. dpeciai narvcnno instructions ano Aociiionai i r i o r m a n o n ^ / g- y ^ //c. i ^ Z y . / , y y d ^ z t ^ K ^ 2 Z u < ^ . y/uy/^y^. ^ ^ . . ^ ^ y ^ y ^ r y r ^ . y ^ ^ , ^ ^ ^ 1 6. G E N E R A T O R ' S C E R T I F I C A T I O N : I nereoy ceciare inai tne contents of mis consignment are fully ana accurately oescriPeO above by proper srtipping name aT\t are classified, packed, marked, and labeled, and ara m all respects in proper condition for transport by highway iccordir>g t o applicable international and national government regulations. Unless I a m a small quantity generator w h o has been exempted by statute or regulation Irom the duty to make a wasie m i m m u a i i o n cemfication under Stc-.ion 3002(bl of RCRA. I also cenify that I have a program m place to reduce the volume and toxicity of waste generated to the degree I have d e t e r m i n e d to be economically practicable and I have selected the method of treatment, storage, or disposal curreritiy available to me which m:nimi2es t ^ e present ana futur'e threat to h u m a n health and the environment P t i m a c / T y r ^ Name •.t'tft^^ Name y i - i ^ y. yZy/yt " ^ ^ ^ z ^ f f ^ M o n t h Day Yaar \ / yP\/ C \ 0 t S ' ' T 17.Transponar 1 Acknowieogement of Receipt of Materials R _ frifited<;Tvae<: N j m e 0 N e a l e s Trai Tt .ransport Inc Signature (L- m /Q^ M o n t h Day Year ' 1! nl 17 ^ "s IS.Trensponer 2 Acj^nowleogement of Receipt of Materials rr;*Med/Typ«< Name y / /^ocyiy yytyyy^yy S i g n ^ u r * /^'yyyrdoc. yzyy / y y ] / I L ' M o n t h Day Year 1 /-:^x^i^s 13.Discrepancy indication Space / ^ /^y5 100222 S.Facility O w r * r or Operator: Certification of receipt of haiaroous materials coverail by this maii<lest e i c e ^ as noted in Item 19 :rei!l PTimoQ/Typ«c Name Signature Jti:=. M o n t h Day Year A i2^gi3i?<5'i iPAPtKH, 8700-22 ,'flev. 4-86) Previous edition ..Obsolete. STATE OF ALABAMA ( M u ^ Accompony Shipment) J / U ^ J I ^ Q u . I F n r m aesipneo f p r m e pr- H . t t (12 o . t c M t y r e w t i t e r I ^ " * ' • > " " ' ^ ^ - ^ ^ — ^ 2 1 . ! . e n c , a . o . s U S e P A l b N O " D M FORM HAZARDOUS ^ WASTE M A N I F ^ ^ . (Continuatioc^rte^l! M a n l i e s t • D o c u m e n t N o y r /) 9 ffo 6 s^/to <ps\ r o r m Aoo'n»»0 O M B No rO>J 0 4 0 * E»D"e» 7 3 I S . ^ a g e i n l o r m a i i o n i n t h e s n a o e o aree is n o i r e o u i r e d Oy F e o e r ^ l a w Zc/z, 2 3 G e n e r a t o r ' s N o m a T r a i l e r Ntx-nber RTMZ 251880 5 4 T r a n t p o n a r C o m p a n y N a m e - ; p - m ? ^ W » « « r / J ' p m p a n y N a m e r-'-r^f:^, o/\Mr:rB 25^; u s E P A ID N u m b e r yycfiZ? g c S O J 9 9 7 2 7 . u s E P A ID N u m o e r L. S t a t e M a n i f e s t O o c u m e n i N u m o a r - CWMA Jy4'^<^s/ M . S l a t e G a n e r a i o r £ ID \ . S t a t e T r a n t p o n a r ' t ID 0 . T r a n t p o n a r ' t . P h o n a P. S t a t e T r a n t p o n a r ' t ID U . T r a n t p o n e r ' t P ^ o n a T T p _ £ | ' 2 0 C 9 / i C 2 8 U S D O T D e s c r i p t i o n ( I n c l u d i n g P r o p e r S h i p p i n g N a m e . H a i e r d Class, a n d I D N u m b e r ) 2 9 . C o n t a i n e r s P r o f i l e N u m b e r / J C c ^ A ^ < f / S ^ i 0 / C y ^ - ^ ^ ^ J V ^ J [ Z y S ^ ~ ' c ^ M " p " r o < . l e N u m t i e r / C c T t / > ^ f £ o 3 ^ y y > ^ ' ^ ' ' y i y ^ y / V . . . C W M p r o f i l e N u m t s e i y ^ ^ y ) 9 ^ 6 0 9 — 3 0 T o t a l O u a n i i i y 3 1 U n i t U M A W R. • - W a t t e No.- • y - i - f . . C W M Profile Numtaer C W M P r o f i l e N u m t i e r , , V : . ~ZZZ:J':. ZAzZZAzzA^: • 'XZ'yA'ZZ^'^'~ h. C W M P r o f i l e N u m t j e r ••'':^Z^>iZ^Z-- C W M P r o f i l e N u m t j e r . ~ . • . ' . ' - • ^ - « ' - S . A d c j i t i o n a l D e s c r i p t i o n s for Materials Listed A b o v e -//a,*^ / y* f ^ ' ^ f t i C C ) T . H e n d l i n g Codes f o r Wastes Listed A b o v e . a . d . . - B - -'—•"• i ^ ^ - t - ^ - y i - j i ^ < ^ - ^ j ^ y / r Z y ^ / j i E y - e. h;..'. 3 2 . S o f c c e — r t a n d l i n g I n s t r u c t i o n s a n d A e a i t i o " B i ' - ^ y r - ^ a f n n AJf^Hdr^ \ ^ ' ' r i ^ ^ ( / L ^ . ^yj^^-y^^^^yu^Zi^y^ -'/yyz>y-yyp^y2A.c^y4' ^y^J^o^yyi^-Mty d?^ y^y<^ . yZyLZatr^>*'^^/^ 3 3 . T r e n a o o n e r A c k n o w l e d g e m e n t of Receipt of M a t e r i a l s Date P r i n t n i / T y p o d N a m e p^o—: . ^ l "" ..ii.'.nnr! inr" S i g n a t u r e i g n a t u r e i gry: m -A^^A. M o n i h D a y Yeer I, A I I 7|R = fi 3 4 . T r a n t p o n e r ' ^ A e f c n o w l e < ^ e m e n t or Receipt of M a t e r i a l s I . ^''^ T / ^ y T ^ E)oAo<j..i-^l^\m':^yZEm M o n t h D a y Year 0-1 ^ If/" 3 5 . D i a c r e - p a n c Y I n d i c a t i o n S p a c e rxTT- 100223 ^ ^ ^ / (As Required By The Alabama Department of Environmental Management) f-ieasa print or tvp« (Form designed for usa on elite 112-pitchl typemrriier.) <i" U N I F O R M HAZARDOUS W A S T E MANIFEST f o r m Approved OMB No 20O0-0tO4 Ctpires 7 31-86 1. Generator s US EPA 10 No. Maniiest t^i / 1^ I ^ i f l o i g if^ ^ 1^1 P I T I /^°&V''h'*^ oeneratc-' s Name and Mailing Aodress JZZrce-'t* C/^i/v^cBc coy>t,^A/c/ £>co y ^ y ^ ^ y r r ^ ^ " ^ ^ e7a-x> 4. Generator t Phone ( ^ O / ) 6 9 d - ^ / O O 6, Iranspor-.t--"! Company Name 7 y ^ S * t U / S Q X f - . g ' ^ C / g . . . / . iranspor-.6/ 2 Company Name T7fS/c^/i. /(»7/«/*/</e' rAa*iyyo^rjjwf~ T r a i l e r Number TMTZ 680365 u s EPA 10 Number \P\i&\Z>\9\9\o\i,\^\<i.\S'\79 8. US EPA ID Numper | / > ^ | 2 > | ^ | g 1^71 gig \<i.\S'\7\9 2. Page ) of Z . (niormaiion m (n« snaoec i r t a IS n o t r e g u > r « d b y F e d e r a l law A. Siaia Manifest Document Numoer CWMA 243032 8. Stata Ganaraior's ID C. State T r a n t p o n e r ' t 10 0 . Transponar t Phone £. State Trantponet t 10 F. Transponer's Phone < - / / ( / . ' / I C - \ — i U U 9. b a s i g r u i e c Faciiiry Name and Site Address C H E M I C A L W A S T E M A N A G E M E N T . I N C . E m e l l e F a n l i t y A l a b a m a —:ighv«ay 17 at Mile M a r k e r 1 6 3 Ernelle, A ataama 3 5 4 5 9 10. US EPA 10 Numoer G. State Facility t ID , A , L| D, 0| 0 | 0 | 6 | 2 | 2 | 4 | 6 | H. FaciliTy's Phone 205/652-9721 1 1 . u s DOT Description (Including Proper Shipping Name. H a i a r d Class, a n d ID Number I yyS-&yj/Z/)CcyJ ur9/rz, Z/po/y) yycs(7hcr/e»i y ^ ^ z i ^ 12. Comamers No. Type 13. Total Quantity 14. Unit Wt/Vo I. Waste No. - T - ^/€^'<r y//?9y/9 C W M Profile Utitntset y ^ y ^ ^ ^ 0 ^ 0 2 . . //ff3/:ycy?ays c<yBJrc yy^£/yo yyriy(y^^^^^, ^(Zyy-ujedyoKy) ^yiyii^&^ / y ^ ^ / / ^ C W M Profile N u m b e r , , < t : ^ ^ 6 0 S \ l ^ £>\/'i •= //•ffSryQyLerxAf U^BsyS Jcyy/} yucf //rf£:&c />K^<jfrJ) r P ^ y ^ ^ ^ ^ y y 9^<^ C W M Profile N u m b e r / O C y f ^ ^ f f ^ < ^ m/h/E. I ^ y : I I I I d . C W M Profile N u m b e r I I I I I I Aoainor.£. Descriptions tor Matenals Listed Above ~ / r i : , . y * a ^ rya*<y / o y -yU/Zejxc e^ruyi ^^^^^c^^* / / 6 ' y^^M-erj^^^lZy ^ o ' y tTyi^o^acti^, yi,cu^A<Zy^ r^^^^Tf^^.^ y / c ' yU4^»ia,3 C r v T ! ^ yaoK^tey y^/<^«».<*^r^/'«<nny e v / / ^ ^ ^ ^ —-•• — • - M B i - t M i . r s A I n c T r • ir-v m n r s n M a r t H i ? m r \ a l I r A A r m 9 * • A n * K. Handling Codes for Wastes Listed Above ,.De< d. IS. Special —.andiing Instructions and Additional Irtormation / / a . ^k<«*«:<t uyZcij .yyu^<m> Tio/LcjiZ/yuiCy «5<*/^><s«i*i-''^>r»«<L.^lZt^ y ^ Cuyy9fy9 15. G E N E R A T O R ' S CERTIFICATION: I nereoy declare mat tne contents ot tnis consignment are tully ano accurately described apove by proper s.-:sping name ano are classified, packed, marked, and lat)€led. and are in all respects in proper condition for t r a n s p o n by hignway a c c o r d i r ^ t o applicable international artd national government regulations. Unless : a m a small quantity generator w h o has been exempted by statute or regulation from ihe duty to make a waste minimization cenificetion under S e c t i o n 3002(b) of RCRA. I also cenify lhat I have a program in place to reduce the volume and toxicity of waste generated to the degree I hava c e t e r m i n e d to be economically practicable and I have selected the method of treatment, storage, or disposal currently available to me »*hich m i n i m c » 3 i n e present and future threat to human health and the environment 7 Pnniefl. . v p e d Name y^-oiAy y yyyyid Signatun Z ^ ; ^ ' ^ Month Day Year \ / r ? \ / \ y y . S ' T 17.Tr»nspc.—sr 1 Acknowieogement of Receipt of Materials R A N S V Priniec, " vpsd Name ~ Oneale s Transport Inc Norton 1 . M. Burt Signature i •y^ e . - m -A..^lr . ^ • Month Day Year 18.Tr»nsoc-^»r 2 Acknowledgemen;^ of Receipt of Materials Pri;>»ec. ~ vped Name 7 y tjnaxtuy , / . ^ Month Day Year zy ^ys 19.0iScrec.a''.CY Indication Space / P ^ 2 0 . F a C i l i t y Crwner or Operator; Cenrfication of receipt of hazardous materials ca'vered by tlyiymaTtifa^t except as noted in Item 19. ^ Nam* I f .'. J Z- / • Prinie<i. fT>ed N a n i e ^ ^ClS- Signatijre Month Day Yeer E P A F o r m e 7 0 C ^ 2 i (Rev. 4 - 8 5 ) Previous edition is obsolete. S T A T E D P A l A R A ^ / . A / M . • c + ^ A . r - r o m r ^ n n v . « ; h i t D m e n t ) i . ^ ^ , ^ 100224 Pi»»»« pr.ot or NT» (Form designed for use on elite ( i S o n c n ) tvpewr.ter I UNIFORM HAZARDOUS WASTE MANIFEST (Continuation Sheet) 2 1. Generator s US c ?A iD No" Mannest • Document No y r /) 9 / 0 ^ s-y a 9 s \ X C Q o S f p i n Aoofo»ea 0>^a No 7000 0404 E.D.rrs : 31 86 « 23.Generator s Name .Z2x.P^^ (Z^^ry'tisc Ca^^-vy T r a i l e r Number Sots /^y>^'^''rtu> ^dS£ gyc7o "^^^ 680365 24. Transporter Q C o m p a n y Natrta /?5/i/£~C/if yy/irraA/M/fO,*, 26. T>aneaeRei '\ Compgny Narrsw, 25. US EPAIO Numoer 27. US EPA ID Numoer fsTage iniof rr^aiion .n tne snaoeo a.eas IS not required by Federal law L. State Manifest Document Number CWMA y ^ S D e / U.Slate Generators lO N. State Transponar s ID 0. Trantportat t Pf>on6 P. Stata Ttaniporter $ lO 28. US DOT Description (Including Proper Shipping Name. Haiard Class, a n d ID Number, « ^^y^fe/pi(>£M f//:iry;r. yypc//y] yyay/7oc:/a^^^j^m^^jmj^) CWM Profile Number y^zzT^-^^AA 29. Coma No. Type U . T r a n t p o n a t t Phone:;; j ^ ^ _ / j ^ q _ p ^ ^ 7 7 j t T inert I 3 0 | 3 1 . 1 b. yi'^p^yiK^oedi '6(/ajrz. yrpcyy/) yvar/yhcceja,^ (Titf %,.IK " V f ^ / ^ ^ " ^ - - ~ i y A ^ ^ » "^LTT 1 vf'i C'l't"! fMi''ini"_i,f _ i , i i j i j , / V f f i - i L ^ zfca2r62^e== =. y / a ^ - ^ I l A r A ^ MAejTSr t/dCiD • g ^ g . ^ l ^ ^ l ^ / g ^ /^AZCt^t*/} CW\B Pfefill> • ' i i m h ( l f ^ < 7 f ^ V ? ^ ^ < g ^ ^ f ^ ^ . / CWM Pro file Number /./\^/f /.y. CWM Profile Number % CWM Profile Number CWM Profile Number CWM Profile Number /VA d/y vyf^ Total Quantity Unit R. Waste No. CWM Profile Number . Addmona. DesCTiptionsVor Materials Listed Above ^ p .^jy^..yiM^f<^'^'yzc^yr^r?y "yi i , • iiyzd^j^fAZs^syViZyz ^ ^ ^ . . ^ ^ ^ ^ ^ ^ - . ^ ^ ^ t / j e K / ^ ^ s Z i Z ^ < ^ ^^'uJJeZ yuy0t^iy/yiya/,iy-\~ c T. Handling Codes for Wastes Listed A b o « a. d. g. e. h. f. i. onai Information 32. Special Hjja^nnqlnstr '^-^ithSa^ZZTi^^ZZ^^fZy:^!^^ Cr^cEyy. V 33. Tran&c>on»r Acknowieogement of Receipi of Materials Date PTy\te<3.fIyp»d_ Name •& i . C u ^ l . G ...L'di' ar: sport—me crzcr. C^M—Bur: Signatura j f Month Day Year r > , ( \ ' I Date 34. Trantpor.ar < Acknowledgement or Receipt of Materials P r i p » K l / T r p « d Name / - \ ' Z^ I Siigniiiure f l \ C ^ / ] DiaCrapartcY Indication Spaca S Month Day. Yeeu 100225 £ ? A F o r m 8 7 0 C - 2 2 A (3-84) STATE OF ALABAMA (Must Accomoanv Shioment) HAZAHDOiiS-WASYb MANIFEST (As Required By The Alabama Department of Environmental Management) l-lea^e onnt or tvo« iform designed for use on elite 112-piichl lypei^riter t f o r m A o p r o t e d O M B No 20CX) 0 * 3 4 e.p.tes 7-31 Sf # U N I F O R M HAZARDOUS W A S T E MANIFEST J. vjaneraicr s Nam« and •'•tauino Aooress XZrcs^'U C/<^£/»'COt, co/rsf^ti/r/ 4. Ganaraior's Phone ( • S ^ / I ^ ^ ^ - t f / ^ b. Iranvporrcr 1 Company Name 1. Ganaraior s US EPA 10 No. Mannest .Pocpr^j^n\ No i . Page ) of Z . inlormaiion m tne snaoeo areas IS not reouireo by Feoeral law Trailer Nunber TMTZ 680365 7 ' ^ 5 4 J U ^<g>€(r- T T y y c . us EPA 10 NumtHir /. iransponer 2 Company Nama \P\£'l>^?' e\ gig I ^'ti.\£'\7'9 A StBle Manileet Documani Number CWMA_243032 6. State Car\araior'i lO C Slaia Transpoaar t ID 0. Trantponer't Phona US EPA 10 Numoer rx-fftrcxA./»7/«>g/vc r«s*trye>jtr^jwe.' \P'^\Z)i9i0\O\^><f-s^^^\7\9 •?! uiastgnatcj raciliiy Name ar<d Siie Address C H E M I C A L WASTE MANAGEMENT. INC. Emelle Facility Alabama Highway 17 at Mile Marker 163 Emelle. Aabama 35459 to. US EPA 10 Numoer 1 A, L, D) 0, 0, 01 6 I 2 I 2| 4 I 6 1 4 E. State Traruponer't 10 F. Transponar I Pnona G. Stata Faaliryt 10 ^CAE'Lt^ZA-fqUX ^izjui H. Feciliry't Pnona 205/652-9721 11. u s OOT Description (Including Proper Shipping Name. Haiartl Class, end ID Number) /yp^y/z^cyj ur5^rz, /y^c/ro y^rys(7ecr/^c yZ/^^-eu/e) 12. Conumars No. I Type . 13. Total Quantity 14. Unit iWiA'o • \ . • - - Wane Na"-. c^eyp?'€' y/y?9yrr9 CWM Profile Number y ^ / J ^ ^ f f / S c Z . I l^l/^l/*/ I ' l l ' yyffSyrycy>ayys ryyajro yy^c/yo yrcy(7^.y^A€.. frcZy^coeityo^ ( P r i y V ^ ^ yf/y 9'y/9' ' ^ ^ ' ^ ' ' ^ ° ' " ' N u m b e r / < ^ ^ ^ ^ 6 < D 3 XzQjiiy, /yVSry^rt^icrys UfBSrS Jccy/) yucf //r^r^xfc i>j^u^j) O^/V-S" ^yy 9 y ^ C W M Prodle Number / C c y 9 ^ ^ f f ^ ^ \H]D\A\ I ! 1 d. CWM Profile Number I I I I ! I I I J. Aaiitittrja. Deacriptions ior Materials Ijsied Apova ~Z • ' y y / a , , ytacy / 9 / a ^ / o y y^ni^jKC. At-*^ ^if^fe^t^^ yZ/y£.y^y^4.^^^^^^ i?e'y cy^o^otLr//o^^*<Z^ d0y^*r%f^^ " • / / € , . £U40m3 c * ^ 7 ^ ^ ya<>t<Zjy^yrd^Zti^yum%f iU//yj^'dir iructipns and AodHional Ir^orma K. Handling Codes for Wastes Listed Above ! b.D0( ^D3l Z d. 15. Special r\andiing instructipns and Acdilional inoTmatton / / a . Si^u**vcd. t4.AZz^ ,^<^uvc. yv yx.yyriny^ ^-^^y/..^yy^y^.. MJCA & (Ic</y»f/7 16. GENERATOR'S CERTIFICATION: I hereby declare tnai tne contents o< this consignment are luiiy and accurately oescnbec aoove by proper sr.^ping name eno ar© classified, packed, marhec. ond labeled, and are m all respects in proper condition for transpon oy highway according :o applicable international and national government regulations. Unless I am a small quantity generator who has been exempted by statute or regulation from the duty to make a waste minimization cenification under Section 3002(b) of RCRA. 1 also certify that 1 have a program m piace to reduce the volume and toxicity of waste generated tp the degree I hava determined to be economically practicable and I have selected the method ol treatment, storage, or disposal currently available to me which mmimces tne present and future threat to human health ar\C tne environment PrimecyTyped Name y ^ ' P / y y / y y y £ i / Signatur ^ ^ ^ ^ ^ c y ^ ; ^ ^ Month Day Year \ / i ? \ / y \ / r \ T 17.Transoor-.e- 1 Acknowledgement of Receipt ol Materials R A N s A..d- i I T PrinteoTypjd Name .T O n e a l e s T r a n s o o r t I n c Norton C. M. Biirt Signaiuf« i Month Day Year h i n h i7ifi 'Si ' 6.Tf»ns3or:«r 2 Acknowiedgemeoj^ ol Receioi ot Materials Ptipt^c^^.rz^a Name / / M o n t h Day Year S l Q n a i u r a ^ / / / ^ > r ^ i u m n ^ a j t e a r .yZAfyt. /cE^j/.- CyZy y y ^ ^ y y /^<j 1S.0iscrepar.cv Indication Space t T 20.FaciliT;r Crwmer or Operator: Certification of receipt of hazardous materials covered by iiyi/manilust excepi at noieo in Item 19. 10022G Prin^a/T I'ped Name_ Month Day Year l / i Z j ^ ? i r : 3 " -..EPA Form 870C-22 (Rev. 4-86) Previous edition 1. Obsolete. < ; T A T P D ^ A l A R A \ / . A / ^ / r . c t ^ A r - ^ n m n n n v < ; h i n m e n t ) I -! ^ O / ^ (Form rtftioned for ute on eliie (1? pitchl tvocv»r.tcr I U N I F O R M H A Z A R D O U S W A S T E M A N I F E S T fCor-:inuation Sheet) Jl.uenerjlor s uS C?A iD No. I CTanTToIi d Document No y Cr>oj foi*!. Hooio.re OMB No 70OO Oarn E . O . ' H ' 3' 86 J.Generator J "xame .^scp^tMi {ZA^ryf'CSc C^^'^'^y T r a i l e r Nunber S o o ^y^'^^rtU) y^d9J> ^yayo " ^ ^ ^ 680365 Ctr^ie/yytr, ^£u> Ji:yj<iy <9ayi:»s r t c Ho^-^Ptji. .<^/y>o 24. Tranaponer ^ C o m p a n y Name ^rtrnpary Namn 26. T'»a»>f>onei 25. US EPA ID Number X^i. z> 9 9 o 8 o 3 'Y'7 7 •^AtinrR- 27. US EPA ID Numoer 28. US DOT Deacription (Including Proper Shipping Name. Haiard Class, and ID Numberi ^ ^ ^ - ^ y : ^ i : ^ E = y { / y f ^ y ^ CWMProtileNum^T'T^^Z^igry^^-tJ 22.r'ag« Intoir^aiion in ine shaoed areas IS not required by Foderai law C. State Manifest Oocuyn^nt Numoer CWMA M.Slate Generator's ID N. Slate Transponar s ID 0. Trantponar't Pttone P. State Transponer's ID U. Transponar 1 Phone'2' 29. Containers No I Type 30. Total Quantily Unit Av^^3f ^-U'^Q-f^vaa ' Waste No. Mfz^tCZ)oda cystsrz, yrpcry/) yyar(yocuja^ f. M t^vvi^i Piuiiiy mjiTiuei^a{*£vy ^ / ^ ^ r^s€7zc.e>6*td u/ejFZ> /dczp yyOfry^iysc yi<.cim<^) ^ =-—^^— i—ZT oyy7f::j. ^ m C W M Profile Number (.y// /.y. CWM Profile Number ' CWM Profile Numtjer CWM Profile Number h. CWM Profile Numt>er CWM Profile Number S. Additional DeicripttonsJor Materials Listed Above ' ^ j f ^ M . . y j ^ j M a f ( / y p y y^y,yjdci.y ^ y i * i ^ < ^ ' z ^ ^ . ^ ^ w a » » u ^ ••^'*y^ O iTl r z / A / f J ^^^^Z^,'^^^^.^t-~6^^0^K?yOyy<yix^ * ^ ^ ^ ' u y ^ sZce^dKd^^ylw'i T. Handling Codes for Wastes Listed Above a. d. g. b. e. h. ^^^^^stzz^czcE^zy^fzy^^^i<y^^ <ZZy:yy^. 33. Tranaponer AcJcnowleOflement of Receipt of Materials Date Rf^>i»d/Ty"?*d Name " " -rr^—9—rrsTTSTJo-rr—me V o,...-»• Signaiura ^{yyit ^ ^ <•• i'^{ — f ^ l ' A^" Month Day Year I 34. Tran»t>on»r < Acknowiadgement or Receipt of Materials Prip««d/Trp*d Name / - ~ \ ' Z) I signjlture t ] \ <Zy / ] Date Dia£r»p«rwc-< Irtdicaiion Spaca ^i Month Day., f t / i — 100227 ?A Form 8700-22A (3-84) STATE OF A L A B A M A (Must Accomoanv Shioment) t-Xat - ^ HAZA,^UUUS WAS TL MAf^lFEbT (As Required By The Alabaina Department of Environmental Management) (Porrri aesignaa Por usa on ahta 112 pitch) typewriter ) ^ f o r m A p p r o v a l OMB No 2 0 O 0 0 4 0 4 e i p t r e i 7 31 86 # UNIFORM HAZARDOUS V»'ASTE MANIFEST 1. Generator s uS EPA 10 No Manirest u«n*.-a'.^' s .Name ana Mamng Aooress .ZZju^^t^ C/JCyfCSt, <Z»rrry«4/y eoo y^/^^f^£^y>/^osy) cvyrryyy^ A/ery sXtiyjiy a ^ f p <^ ?<2 ^ 4 G a n r e - . y s Phona ( J ! c / ) ^ ^ ^ - ^ / O O b. ;rarspc-'".er 1 Company Name t^i/ugifi^-g'^^.^'g?if 4-LZ^r'g>y/ 2. Page I of ^ intormaiion m tne snaoeo areas IS n o t r e q u i r e d b y F e d e r a l T r a i l e r Number RTMZ;274676 A Siaie Mannest Oocumam Numoar CWMA 243033 B. State Ganaraior's 10 6. US EPA 10 Number l/'i/* U> I ^iJ^io **'itfi <iS'\7.9 •rrAS.yryhy.7-. yy/d.. ^ iraru<icr-.er 'i. Company Name 6 US EPA ID Numper y. Uesigru'.ed hacitiiv Name and Site Aooress C H E . V l C A L W A S T E M A N A G E M E N T . I N C . E m e l l e - a c i l i t y Alaaarr-a H i ^ w a y 17 at Mile M a r k e r 163 ErT>e:!e. A . ' a b a m a 3 5 4 5 9 10. US EPA 10 Numoer A , L| D, 0, 0 , 0 | 6 , 2 I 2] 4 | 6 ) 4 C Stata Tranaponer s 10 O. Transponar'* Ptvina E. Slate Transooner s ID P. Transponer's Phone G. State FaciliTy's 10 H, Pacilitv s Phona .205/652-9721 1 1 . u s DOT Description /Including Proper Shipping Name. Hatard Class, and ID Number/ '• /y^2yp/ey>0ffJ c^y)sr£ j-acyx> y / ^ s (7o<-^^'^ fy^er&rje) 12. Containers No. ! Type 13. Total Quamiiy 14. Unit W t / V o I. • Weate No. ^/?xy-<£- y/y^ 9 / ^ CWM Profile Number / ^ C / } ^ ^ 8 S ^ l / ! / l i g l / ^ I '' /iy/TzytJtoce/S £</9Jrs: ser.y/^ yiyo^(/0a/iyrc (i:cy/^yo/^ayiy>i^ < ^ ^ - ' ^ ^ y 9 / < f 9 „ '—ycyi></fi,o4^ C W M Profile N u m b e r 'Z'3'/>y^ I 1 ! I ayyyy^ yy/J ^ / f f CWM Prome Number ycyy> ^^OZ, Z^J^Utl C W M Profile Numtjer I I A o o i i i o r Z Descriptions lor Materials Listed Above ~ y y , y/di^. y'ess Mats / o ' A 7<"yr-*^» a^y/fcJZi^ Z-r'-, / / ^ . /ej-J ;5^a*» / . o / . "TetyjtfTC. AfiaC <!^<£eyprsAry7 y/ca /csJ ^Odo y ^ ' / i /iLat*iey a y t y . £ d ^ J i ^ I I I I K. Handling Cooes for Wastes Listed APove a.DeJ •J>&1 15. Spec-^* —andiing instruciions and Aaainonai iriormaiion y/<^€'/^.yZ7:Zki yy<y.^ Oy/6. ji^'A,. yfty.^r'/1?<, y-yr^/rrT^ ySy r y j t C y - y y f y y y c y y y o ^r/^>f/r/.tV. yycK-:7 sr. ryyykz. yZ'y^y^y/rryyyy^/:^ • ^ i . G E N ^ f i A ' T O R ' S C E R T I F I C A T I O N ; 1 hereDy oeciare xtsax the coniems oi inis consignmeni are :uiiy ano accurately oescnbeo at>ove by proper v*-c3ping name and ere clBSSifi«d, packed, marked, and labeted. and are m ad respects in proper condition lor transpon by highway • c c o r f i i r ^ to applicable international and national government regulations. Unless ' «rn a small guaniiry generatof who has been exempied by siaiuie or regulation from the duty lo make a waste m m i m i r a i i o n ceriiflcation unoer S e r t i o n 3002ib) o* RCSA. 1 also certify that I have a program rn place to reduce the volume and toxicity of waste generated to the degree i have Ce'.e—Ttinod to be economically practicable and I have selected the method ol treatment, storage, or disposal currently available to me whicn mrnimi2«^ r*ie present and future threat to human health and the environment. !l 7 Primec. 't-yan Name ycoAy y. /z/itT Signature '^a^^y^^k^r^ M o n t h Day Year \/yr>\yi\Q\F.r' T 1 T.Transpcr-.e* 1 Acttnov^iedgement of Receipt of Materials Prmtec.'~«ped Name O ' N e a l e s T r a n s o o r t I n c Nortcr. C .M. Burt Signature i 2 itm A nicyvlcZ\ rl.. m. /Z}y>u yH. M o n t h Day Year I I ' O I I I 7 I 8 ' 5 16.Transpor-.e- 2 Acknowieogement of Receipt of Materieis ignaiuiE-^' f , y y j M o n t h Day Yeer Printec/"" *^«K3 Name l^y . ^~^tra narrie . / /z<JO^ y ^ y y j e a 1S.Di»cfeo*.-«cv Indication Space ^ffp] (yr^^y3 1 0 0 2 2 8 X zD^Faeility C^wner or Operator: Cenification ol receipt of riazaroous materials coveced by this manifest enoepi as noted m item 19 PrimeOy/ 'vw^l Nama //:yyAey? /yE?7^c^ Sionature M o n t h Day Year i/i'2r^>.3iS'^ PA Fcrm 8700-22 (Rev. 4-86) Previous edition is opsoi.te. S T A T E O F A L A B A M A ( A \ u S t A c C O m ^ O n y S h i p m e n t ) / ^ / . y / ^ or rvTie (Porm designed for me on ene 11? oitcri) typewriter > 21.Ciuner3lor t uS c r A iD ,Mo. UNIFORM HAZARDOUS WASTE MANIFEST 'Continuation Sheet) Manifest Document No y / ^ 9 0 o 4 s- / o 9 s^Z'yoCi / r o " " »DD'0.ea O M 8 No JOOO 0«O« E ' D . ' H 7 3t 8 f ;:.?a9e Z ' / Z iniorrnation in tne snadec areas 1$ not required by f e d e r a l law 23 Qtr>tti\ot \ Name . JTy^.o^Mi <Z^yyfy<!at. Ct^frf/>a<// Trailer Number S a o jC^/tey^/icO ^rOLD o'7tx7o RTMZ; 274676 dyy^^€^ yyt^^ yryi/tcy o> rt ^a- rrc yio^.6?tx. ^yoo L State Manifest Document Numt)er M. State Ganaraior'» ID ' 24. T r a n a p o r t e r ^ Company Heme 26. Tranaponer i^ Comruuiy Name 25. US EPA ID Number \r^r. a 9 0 t9 ff a 3 9 7 7 N. State Transporters ID 0. Transoonar't Phone / . , 27. US EPA ID Number ^ \ n n nn7P,99q7^ p. State Transponar « ID Q. Tranaponer s Phoni 2S. US DOT Oescriplion (Including Proper Shipping Name. Haiard Class, end ID Numberi sPyy>i>-r^ , / l K ^ 9 y / f omivunitNumot, ^<^.^i<g^;,gBJ: / y \ / > / f 29. Containers No Type 3D. Total 'j}q-a59-62i!9 Quantity WiytJci Unit R. Waste No. ^ yz2!^.£/'(uy^ inr^/z / o r r n Afnrfr^<ydaf, ^cxirsfy^tyyjjgj/fZL ^ ^ ^ y ^ ^ yyy) <yyP^ - e w w v r o i . l e Number 'yi^^^ ??722^~2E£i^ ^us^<L fyU^£Ar€j~Al ypfix^^z^—s^w/>f CWM P'ofile Numoer d. CWM Pro file Number ^Vs,,/'*--' ACy i Zx 'yyi-yyp''- CWrul Profile Number # CWM Profile Number CWM Profile Number CWM Profile Number CWM Profile Numoer S. Additiorvai Descriptions for Materials Listed Above - —4— '72Z^ZEZZ^i=iZZZ/^^^ r/=-7Stf^^ty/ y f c z y ^ — j T. Handling Codes for Wasters Listed Above { a. d . g. b. e. h. c. f. i. 32. Soe^.j IlJ JJliiiy instructions and Additional Information J^/c y^^^-^yy^ TA^^rts /^it yf/^. yy^yjj^ ^ 6 yy/i/y^cytj) yfcyy/yy^A^/^ yy^<py:^ -77^ yy£ppy?ry/ec y='y^a^ rEZcyay/c yyye^K'y^ y^^oc^^^ Tc yiP^^^^^^ /='y<'^ y^rZf^yZyyy ycy^pyyj— T 33. Transponar Acknowledgement of Receipt of Materials Dale Signature \ ^ J ~ ^^Tyzyz^/^^zm. JLJA^y^. ^ ^ ^ n ^ r ^ tfajna —--- ^ ' nspn. -r T ac 34. T r a n a p o n e r ^ Acknowledflement or Receipt of Materials l/Trt>^ Narne Month Day Year .\\ Q!I 7[R S T P^ftnad/Trffha Name ^ — , '•^y/rrht j / y / /C laucZ= '"t^/r.,,..///^ y ^ y ' Date Month Day Year - Diacrepar>CY Indication Spaca 100229 PA F o r m 8 7 0 0 - 2 2 A (3-84) C ; T A T F n p A l ARAA.AA ^ M . i e t Ar-i-r^r cu:. .1. hAZA::UUUS"WAbii: >^ y-u y-^ ^bbi l e print or tVD* ' (As Required By The Alabama Department of Environmental Management) (Forrritletigned tor u s e o n e l i t e l H - p i i e h l i y p e r r r i i e r I f o r m Approved OMB No 30O0 0 a 0 4 Eioires 7 31 SB F U N I F O R M HAZARDOUS W A S T E MANIFEST J . u e n a r a t o r s Name ano Mamnq Aooress . Z j - t P - ^ i^rueyr^St, <Zdyrty«4/y £cyn/yy^ yyecy ^Ti/Uiy 4 G e n a r a t w s Phone ( ^ O / ) £ 9 « - a. I r a n s p c ' . e r 1 Company Name 1. Generator s US EPA ID No. (/| /'•/> I f i^.g 1^ .s-^r ,g If >r ^ ^ ^ f g ^ y / O^t^TIO ^yoo T r a i l e r Number RTMZ;274676 o '/%y^^£4T rK.utJCfi/C' ^ r m / u ^ I Name 6. US EPA ID Numoer \/>\/e 'j> I ^ij=^to :^!tf I ^ S ' \ 9 ' 9 8. u s EPA ID Numper / . I r a n s o o o e r i Company 7''^s.'C£/t. rrrj^/uA^ /7eavCf>>%a<r;'.gVO |/'i>gi.<gi f / ; ^ ig'i<^i^i>ri7 !?> T U e s i g n a i s o Facility Nama ano Sua Address 10. US EPA ID Numoer C H E M I C A L W A S T E M A N A G E M E N T . I N C . E m e l l e F a c i l i t y A l a b a m a r-iighway 17 at Mile Marker 163 Errielle. A l a b a m a 3 5 4 5 9 [ A , L| D| 0 | 0 | Oj 6 | 2 I 2 | 4 | 6 | 4 2. Page I ol ^ I n l o r m a i i o n m tne snaoeo areas IS n o t r e Q u i r a d by F e d e r a l taw A Stale Manifest D o c u m o n i Numper CWMA 243033 B. State Gertarator's ID C. State Transporter's ID 0 . Transporter's Pnone E. S u i e Tratuponer's 10 F. Transponer s Phone (j. Sieta Facility's ID M. Faeilriy's Pttona 205/652-9721 1 1 . u s DOT Description (Including Proper Shipping Name, H a i a r d Class, a n d ID Numbarl 12. Containers No. I Type 13. Total Quantiry 14. Unit W t / V o 1. Waste No. / / ^ z yS'yeJXfe/j c*^r9sr£ J'ocyz> yiy£?s (7h<-^^''y^ f y c e r ^ ^ e ) c y ^ ^ ~ G ^ ^ 9 / ^ CWM Profile Number / ^ y f ^ 6 8 8 ^ ''• //y7Zy}/ty>cxJ:s toSJiZ Teiyzi /t/fe\r^/b<^tC<c i^cy/6oyor^a^y>f) a^y=^ -<r y^y) 9 m CWMProtHe Number y i y D 4 S ' < £ y > 4 - A^y\o/^ \i'S^y>! }lyL ^ ^ I I C W M Profile N u m b e r •7^ A o t u t i o r . ^ Descriptions I I I I I I I lor Ma Met .^arerials Usted Above / / i t . , y^ss M&d] / o ' / . Tocy/ytida ef^y/fciZASvij / / 6 . A-*^^ T^oyr / o Y 7cU/t*tc. Ottyy. Cyr^fiTfrvfiyi y/Ca / o s j f^Odo A - ^ y i TZiiio^c a^yy Si^ffSidrK^ n e t r a i f > 4 m n p «Mf4 A ^ r a i i i n n a l \9^irt.rrfi.-mm,r.». K. Handling Codes for Wastes Listed Atxive a.i/Bi c D B l bPsA • d. I s . Special —.anoling Instruaions and Adcitionai Information y i / < ^ £ ' y j Z / y k i yyo^ *Z/y6. Jo.-c,. y f t y . r r - y ^ yZ/yryCcycy> / S y cyijyyy-y^<} y^/ercyy ^ y~e? z>rr=Pyrr/.i'Z- ^Z^^-^v ZT. ^rv^^vr. y^AZycy^vr'zCyyc'<:tyy:t<p 16. G E N E R A T O R ' S C E R T I F I C A T I O N ; I herebv oeciare tnai trie contents ol this consignment are lully ano accurately cescribeo above bv proper f r p p i n g name and are classified, pacired. mariied. and labeled, and are m all respeas m proper condition for transpon by hignway a c c o r d i r ^ t o applicable international and national government regulations. Unless •' a m a small quantiry generator wno has been exempted by statute pr regulation from the duty to make a waste minimization certification under S-ection 3002(b| of RCRA. I also cenify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I have d e t e r m i n e d to be economically practicable and I have selected the method of treatment, storage, or disposal currently available to me which m i n i m i r e s the present and future threat to human health and the environment. V P r i n t e c " y p e d Name /^coAy y . y / < € j - '•^..iyy^y^ M o n t h Day Yea \/y>\n\-7\!A\ A 17.Transoci-:er 1 Acknowledgement of Receipt of Materials Prmtec. "yped Name O'Neale s Transport Inc Nortor- C.M. Burt Signature i 2 i ^ A M o n t h Day Year 11 10 11'7 18^5 18.7ransocr-:er 2 Acknowledgement of Receipt of Materials Prtrttjc. ~ y p e d Name iTi^c- .ypeu raamo , y -rV/yjrzziy yyyyjec/ SignatuiiE^';'^ » y / * M o n t h Day Year 1 9 . D i * c r e c * ^ C Y Indication Space (j-yyy3 ff 20,FacilitY ^Fwner or Operator'. Certification of receipt of haiardous materials coveted by this maiS'ifesi eioeot as noted in Item 19. Primeo--- iT>«d Name / - / : ^ y / i r s ^ / ^ n > ^ c y % i . M o n t h Day Year EPA Form 87o^2i (Rev. 4-85) Previous edition IS Obsolete. STATE OF ALABAMA (A\ust Accom^Qny Shipment) u i l I J y 100230 ':»t*m r-int or rvoa (Form desioned for use on e'ltf (IJoitch) typewriter i ferr" Aoo'o.pfl QMB No 2000 040a t ' c r s 7 2' P' t UNIFORM HAZARDOUS WASTE MANIFEST (Continuation Sheet) n .>3ooeraior s US lirA O No Man.lest n.r'age Document No d urocumeni nts z o/Z iniorrnaiion in tne sn^OtC d'«ras L State Manifest Document Num&er CWMA Z^s^^y^ 23.Generator s Name . ZTsc^^u} ^y^yyfrCot^ C^-rrpy:^/ Sd^o y'^i'£y^^(cy:> ^(JSZ) O 7tr?o cjyuyyy^y y / t ^ AZe/^y 24.Transponet»..g Company Name y A * / g . £ 4 _ X ^ T'AOtl/cti/'XI^ 26. Transporft-4 Cornpany Name • TYPFr! V\'^\<yT^y ..Trailer Number RTMZ; l l k b l h T'rc j!<}/-^9^ €./oo •5! u s EPA 10 Number L M.State Caneraior s ID N. State Transponer s ID \ r t. e> 9 S o 9 d> 3 9 7 7 27. US EPA ID Numoer I n n nn7riT257n 0. Transponer's Phone P. Stata Transponar s ID U. Transponer s Phon 28. US OOT Description (Including Proper Shipping Nerne. Haiard Class, and ID Number, 29.Containers No. Type 30. Total Quantity i'3;LS-a?9-52^-!9 Unit AWol R Waste No / z ^ A^-f g ' / g / g g ^ < f y \ / y 9 f ^ y l S . «W(rt^rol,le Numoer / ^ ^ y l > i > / U y f - ^=>z^ J>/iy Zsye, i r ^ U ^ l A ^ — CWM Profile Numoer y^tfy^zZ—^v- r CWM Profile Number Z y y ^ / ( / / ' ^ />/>) Zx CWM Profile Number CWIul Profile Number CWM Profile Number CWM Profile Number CWM Profile Number S. Additior-.ai DesCTiptions for Materials Listed Above ^ ml - '^^lZ^^xA=y^y^i-Tci^taycr. ^^fu^ & / ^ ^ ^ ^ * ^ T. Handling Cooes for Wastes Listed Abov? a. d. g. h e. h. f. 32. St>*til^i 11I..UIll-It) ihslructipns and Additional Information JZ-/C /^-^^''^fy^EryfTt! /ya, iZ y/^. /y^^jy ytz. yrytfyx£c/Cj> ^ y cyj/z/yy>y^ yy/cy:^ 7 5 yey'^yTTf/^^, /='y^a^ rTZCyoyy ytC^?.=pfyy ^ ^ o c ^ r ^ r ^ y ^ ^ - y y y Z / y y y r y ^ p / ^ j — J I 33. Transponer Acknowledgement of Receipt o< Materials * I ^ r ^ ^ ^ r j . ' r ; ^ Nerne J -<ivl.\ g - • ^ " ^ '^-r^rMz.r.cTr T n r P I v=- - - -,,- r> V •a..X^' ° I 34.Trans{>orter-7^Acknowledaemenl or Receipt of Materials Sionature ) / l y y ^ y ^ 'E.Tn. iSZZZc ^ 5 Date Month Day ' • tr I 1 n! 1 7I 1; ^ f i3. Diacreparkcy Indication Space ~ — - ^ I Date I SiOT^turi * y y, y Z Z y E Month Day Y-ar Urf..a. /{f. 4.^.uW I / L l AJ • ^ i?A Form 8700-22A (3-84) < ; T A T P D P A I A R A K A A ( M i K i t Ar , , Cklr.— ^ . - * . ! 100231 ATTACHMENT K 100232 ATTACHMENT K snviio Ki scisDc^ inc. 19 C0P5LAND RD.. DENVILLE. NEW JERSEY 07834 ^ ^ ^ ^ ^ i ^ 32 EAST 39 STREET. NEW YORK. NEW YORK 10016 (201) 366-6256 ^ ^ ^ ^ » ^ ^ (212) 697-9450 November 15, 1985 Mr. Carl Becnell G, A. Becnell, Customs Brokers 150 >iarine Street Lake Charles, Louisiana 70601 Dear Mr. Becnell: As per a telephone request from Mr. Frank Curtis of Berlex Laboratories, Inc., I a=. sending the enclosed laboratory analytical sheets which describe the chemical consents of hazardous wastes which originated in St. Croix, USVI. It is my understanding that U. S. Customs will not release the material for shippment to Chemical Waste Management, Inc. in Alabama until they know the contents of the shippment. Below is a listing of data sheets and to which drums they are applicable. DATA SHEETS 1 and 2 3 - 6 7 - 11 12 - 17 * CHEM. WASTE KA.NIFEST NO. ALA D ALA E ALA D ALA D ALA E 48604 68803 48603 48602 68804 M.^TERLA.L Soil Soil Sludge Water Pieces of Metal Drums NO, OF DRL-MS 24 15 45 94 14 * Pieces of washed drums which contained materials in items 1 and 2 above. I trust that this information will suffice for release of the material. If you have any questions, contact me at 919/499-5182 or 201/366-6256, Ver-^ truly yours, Ala- L. Kyles, '^hD, Vice President enclosures 100233 ATTACHMENT L 100234 ATTACHMENT L ic:£fK2i inc. Ci-LjVijXjnir 19 COPELAND RO.. DENVILLE. NEW JERSEY 07834 ^ ^ * * ^ ' " * ' (201)366-5256 November 6, 1985 Mr. Louis Diguardia DSEPA Environmental Services Division Woccbridce Avenue Edison, NJ 08837 Re: Island Chemical Comoanv, St. Crcix, U.S.V.l. Dear Mr. Diguardia: T.hrough the Freedom of Information Act, I am requesting a copy of the analytical results for samples taken by you on September 9, 1985 at the Island Chemical Company site in St. Croix, U.S.V.l. Berlex Laboratories, Inc., the company responsible for site cleanup, wishes to finalize t.heir responsibilities to the new owner. Virgin Island Chemical Company. Your immediate response to this request would be appreciated. Very truly yours, ENVIRO-SCIENCES, INC. Alan L. Kyles, Ph.D. Vice President ALK/po (AK-85391) 100235 ATTACHMENT M 100236 ATTACHMENT .". Heavv .Metal Analvses For "Gut" Sarr.Dles Loca G-1 G-2 G-3 G-4 G-5 G-6 G-7 G-8 G-9 G-10 G-11 tion 1) 2) 3) 3) 4 ) Cadmium LT 0.24 LT 0.2 3 LT 0.2 2 LT 0.2 2 LT 0.2 3 1.0 2.4 LT 0.23 LT 0.2 3 LT 0.30 LT 0.5 4 Chromium 14.5 16.4 16.7 12.0 17.1 46.4 71.1 20.4 19.8 30.6 41.1 CoDoer 37.3 38.3 33.8 25.3 36.1 40.0 51.4 32.8 34.9 62.7 69.7 Lead • 21.0 22.0 14.5 13.2 20.2 32.9 46.4 19.4 21.4 16.5 12.8 Mercury LT LT LT LT LT LT LT LT LT LT LT 0.092 0.103 0.101 0.102 0.105 0.122 0.121 0.093 0.113 0.106 0.194 •Zinc 63.1 57.8 129 37.1 57.2 349 861 76.2 75.7 66.5 871 Volatile Organic Analyses All sa~ples appear to be clean (verbal from ICM 6 Mar, 4:00 p.m.) 1) G-1: Background - above plant site. 2) G-3: Just below Laboratory pit outlet to the gut. 3) G-5 and G-7: At point of drain line discharge. 4) G-11: Setting "basin" area in gut 250-300 feet beyond drainline discharge point. 100237 Q ^ / z - 100238 : ,1 1 i I i. ; 4 i INDUSTRIAL CORROSION MANAGEMENT INCORPORATED ns?i)ixiiti> «A«:)OL)^. NfWjiH^tr o/abs ?ui^a4.u.i.iu NJDEP Certified Drinking Vacer/Wastewace: Laboratory ID //14116 REPORT DATE: March 5. 1986 LAB If •52i63 PRIORITY POLLUTANT LABORATORY A.N'ALYSIS CLIENT: ENVIRO SCIENCES INC SA.MPL SA.MPL UNITS SOURCE: Tsland Cheynical Co. ID: G-1 SAMPLE DATE: February 19. 1986 SAMPLED BY: Al.-^n Kvles !r.p/kg''ppm') dry weight basis AT LAB DATE: Fphru.-^ry 21. 1986 MATRIX: S Q U NC = 2;on-calcuable RPD due to value(s) less than detection limit. dwb = Dry Weight Basis X = N"ct Analyzed LT = less Than INDUSTRIAL CORROSION MANAGEME.NT. INC. RPD = Relative percent difference. RSL/dlh (This report form contains Parameter Ant ir.env Arser.ic Bervllium Cac-.iu3i Chro-ium Coooar Lead Mercurv Nickel Selenium Silver Thallium Zinc Phenol Cvar.ice Sample Result X X X LT 0.24 U.S 37.3 21.0 LT 0.092 X X X X 63.1 X X both the ori Sample Duplicate X X X LT 0.26 17.9 63.5 25.7 LT 0.093 X X X X 67.8 X X ginal sample RPD X X X NC 20% 15% 20% NC X X X X 7% X X result and Control Limits X X X NC .20% .20% ±20% NC X X X X 120% X ' X the duplicate result.) Minimum Detection Limit X X X LT 0.2-!. LT 0.22 LT 0.62 LT 1.3 LT 0.092 X X X X LT 2.28 X X Method Blank Analysis X X X LT 0.24 LT 0.22 LT 0.62 LT 1.3 LT 0.092 X X X X 1.03 X X ' 1 1 1 1 ! ! i 1 1 RMenard S. L^vj P r e s i d e n t 100239 INDUSTRIAL CORROSION MANAGEMENT INCORPORATED iti^HouTE!: fANOOuv. KEwjeRSEr 07ttt :ai'M443w NJDEP Certified Drinking Water/Wastewater Laboratory ID <I14116 REPORT DATE; March 5. 1986 LAB It 52466 PRIORITY POLLUTANT LABORATORY ANALYSIS CLIENT: ENVIRO SCIENCES. INC. SA.HPLE SOURCE: Island Chemical Co. SA.MPLE ID: G-2 UNITS: mg/kg(pPTn) drv weight basis • SAMPLE DATE: February 19. 1986 SAMPLED BY: Alan Kvles AT LAB DATE: February 21. 1986 MATRIX: Soil Para-eter A.ntirrnv Arsenic Bervllium Cadni-m Chro-ium CoDoer Lead Mercurv Nickel Selenium Silver Thallium Zinc Phencl Cyanide Sample Result X X X LT 0.22 16.4 38.3 22.C LT 0.103 X X X X 57.8 X X Minimum Detection Limit X X X LT 0.23 LT 0.21 LT 0.59 LT 1.3 LT 0.103 X X X X LT 2.1 X X Method Blank Analvsis X X X LT 0.23 LT 0.21 LT 0.59 LT 1.3 LT 0.103 1 X X X 1 X 0.97 X X 1 dvb = Dry Weight Basis X * Net Analyzed LT » Less Than INDUSTRIAL CORROSION MANAGE.MENT, INC. RSL/clh 100240 95?hardS President yyyyy- INDUSTRIAL CORROSION MANAGEMENT INCORPORATED I I M WulE IC. MU1OCH.PH. NEW JERSEY 0>tb9 201'i>t44;)]u NJDEP Certified Drinking Water/Wastewater Laboratory ID tfl4116 REPORT DATE: March 5. 1986 LAB it 52465 CLIENT: ENVIRO SCIENCES, INC PRIORITY POLLUTANT LABORATORY ANALYSIS SA.MPLE SA.MPLE UNITS: SOURCE: Island Chemical Co. ID: G-3 m^/ke(ppm) drv weight basis ' SAMPLE DATE: February 19, 1986 SAMPLED BY: Alan Kvles AT LAB DATE: February 21, 1986 MATRIX: Soil dwb " Dry Weight Basis X « Not Analyzed LT » Less Than Parameter Antimony Arsenic Bervllium Cadr-ium Chromium Cooper Lead Mercurv Nickel Selenium Silver Thallium Zinc Phenol Cyanide Sample Result X X X LT 0.22 16.7 33.8 14.5 LT 0.101 X X X X 129 X X Minimum Detection Limit X X X L"^ n.22 LT 0.21 LT 0.58 LT l.-i ^ T 0 1 r>i X X X X LT 2.1 X X Method Blank Analysis 1 X X TT 0.22 LT 0.21 LT 0.58 TT 1.^ 1 1T n ini 1 X i X X 1 X 0.96 X X INDUSTRIAL CORROSION MANAGEMENT,INC. RSL/dlh lievirie <. 100241 I^fchard S President ' th I'I INDUSTRIAL CORROSION MANAGEMENT INCORPORATED nSIKWIE 10. *A«00l.PH. N£WJtRSE»0?t»li 7<>l-i>tt<l'iXi NJDEP Certified Drinking Water/Wastewate: Laboratory ID tfl4116 REPORT DATE: M.qrch 5. 1986 LAB II 52466 PRIORITY POLLUTANT LABO.^MORY ANALYSIS CL IENT: FNVTRO SCIENCES INC. SAMPLE SOURCE; Island C: emical Co. SAMPLE ID: G-4 UNITS: mg/ke(pom) drv weight basis • SA.MPLE DATE: February 19, 1986 SAMPLED BY: Al^n Xv^^t, AT LAB DATE: Fehrii.nrv !> i . 1986 MATRIX: Soil Parameter Antimony Arsenic Bervllium Cadmiur: Chromium Conner Lead Mercurv Nickel Selenium Silver Thallium Zinc Phenol Cvanlde Sample Result X X X LT 0.22 12.0 25.3 13.2 LT 0.102 X X X X 37.1 X X r • — - ' — - a s — . 1 . 1 Minimum Detection Limit X •X X LT 0.2 2 IT 0.20 LT 0.5 7 LT 1.3 LT 0.102 X X X X LT 2.1 X X ^ Method Blank Analvsis X X X LT 0.22 LT 0.20 LT 0.57 LT 1.3 LT 0.102 X X X X 0.94 X X dwb « Dry Weight Basis X - Not Analyzed LT - Less Than INDUSTRIAL CORROSION .MANAGE.MENT, INC. 100242 RSL/dlh lithard S. LeV: 'resident / • Si'i INDUSTRIAL CORROSION MANAGEMENT INCORPORATED iii;MiurE 10. fUNOOiPti. NEwxRStr o/ibt ni-iiH-orju NJDEP Certified Drinking Water/Wastewater Laboratory ID tfl4116 REPORT DATE; March 5. 1986 LAB II 52467 PRIORITY POLLUTANT LABORATORY ANALYSIS CLIENT: ENVIRO SCIENCES INC. SAMPLE SOURCE; Island Che-^ical Co. SAMPLE ID: G-5 ' UNITS: mg/kg(ppm) drv weight basis ' SAMPLE DATE: February 19, 1986 SAMPLED BY: AT LAB DATE: Alan Kvlp.. Februarv 21. 1086 MATRIX: So^l dwb » Dry Weight Basis X - Not Analyzed LT « Less Than Parameter Antimony Arsenic Bervllium Cadmium Chromium Copper Lead Mercurv Nickel Selenium Silver ' Thallium Zinc Phenol Cyanide Sample Result X X X LT 0.23 17.1 36. 1 20.2 LT 0.105 X X X X 57.2 X X Minimum Detection Limit X X X LT 0.23 LT 0.21 LT 0.60 LT 1,3 LT 0.105 X X X X LT 2.2 X X Method Blank Analysis X X X LT 0.23 LT 0.21 LT 0.60 LT 1.3 LT 0.105 X X X X 0.98 X X 1 RSL/dlh INDUSTRIAL CORROSION MANAGEMENT.INC. 1 0 0 2 4 3 lichard S./Le^<t-ne President C rii( INDUSTRIAL CORROSION MANAGEMENT INCORPORATED Wit MUIC IC. fW«iX>l.f>H. HlW JLfViir OltiH n\-SH-03M NJDEP Certified Drinking Water/Wastewater Laboratory ID tfl4116 REPORT DATE: March 5. 1986 LAB H_52AM PRIORITY POLLUTANT LABORATORY ANALYSIS CLIENT: ENVIRO SCIENCES INC. SAMPLE SAMPLE UNITS: SOURCE: ID: G- Is -6 mg/kgCripm") land dry Chemic£ weight ll Co. basis • SAMPLE DATE: February 19. 1986 SAMPLED BY: Alan Kvles AT LAB DATE: Fehri'.T-" 21. 1QP6 MATRIX: SQVI # dwb » Dry Weight Basis X » Not Analyzed LT - Less Than RSL/ dlh Parameter Antimonv Arsenic Bervllium Cadmium Chromium Copper Lead Mercurv Nickel Selenium Silver Thallium Zinc Phenol Cyanide Sample Result X X X 1.0 46. 6 40.0 32.9 LT 0.122 X X X X 349 X X Minimum Detection Limit X X X LT 0.28 LT 0.25 LT 0.71 LT 1.6 LT 0.122 X X X X LT 2.6 X X Method Blank Analysis X X X LT 0.28 LT 0.25 LT 0.71 LT 1.6 LT 0.122 X X X X 1.2 X X INDUSTRIAL CORROSION MANAGELMENT, INC. 100244 Ri(ihard S President I.I i I INDUSTRIAL CORROSION MANAGEMENT INCORPORATED NJDEP Certified Drinking Water/Wastewater Laboratory ID #14116 I I M M X i U >0 k«> jOlPH. New JtH^LT U'B6t TOIMt-UjJU REPORT DATE: .March 5. 1986 LAB It 52469 PRIORITY POLLUTANT LABORATORY ANALYSIS CLIENT: ENVIRO SCIENCES INC. SA.MPLE DATE: February 19, 1986 SA-MPLE SOURCE: Island Chemical Co. SA.MPLE ID: G-7 SAMPLED BY: Alan Kvles AT LAB DATE:February 21. 1986 UNITS: mg/kgrppm.-') H^v weipht basis MATRIX: Soil (This report form contains both the original sample result and the spike recovery.) Para-erer Antimcnv Arsenic Bervllium Cadiiiun Chromium Copper Lead .Me r cur-.' Nickel Seler.ium Silver Thallium Zinc Phenol Cyanide Sample Result X X X 2.4 71.1 51.4 . 46.4 LT 0.121 X X X X 861 X X Spike Added X X X 1 1 1' 1 0.004 X X X Y 1 X X Spiked Sample Result X X X 1.13 4.04 2.89 2.92 1 0.0035 i X 1 X i X i X ': 1.72 ' X i X X X X 103% 119% 83% 1 1 106% 1 88% ! X X X ! X 103% 1 1 X X Control Limits for %R 75-125 Z 75-125 % 75-125 % 75-125 2 75-125 % 75-125 % 75-125 7. 75-125 7. 175-125 % I75-I25 7. 175-125 % 175-125 % I75-I25 7. 175-125 7. b5-125 % Minimum Detection Limit X X X LT 0.28 LT 0.25 LT 0.72 LT 1.5 ! LT 0.121 1 i X i X X ! X •' LT 20.1 i X i X i l i ! i 1 1 1 1 j 1 1 -^- ' ——' — Method Blank Analysis X X X LT 0.28 LT 0.25 LT 0.7 2 LT 1.5 LT 0.121 X X X i i X 1.17 X i X %R = Percent Spike Recovery NR = .\'ot required. Standard addition performed. dwb » Dry Weight Basis X * Net Analyzed LT = less Than INDUSTRIAL CORROSION MANAGEMENT,INC. The spiked sample result is based on the soil / rt in solution. It does not directly reflect the ^1 / (J / ^ C 100245 final -g/kg dry weight basis result of the y / r - J A I Li sar-.pie. ALUiy^yiyJ hyiAyy^ ^:i'i L INDUSTRIAL CORROSION MANAGEMENT INCORPORATED Mil HUUIE 10. S A M O O U ^ . MEW JEHSET U / S M 2UI'&(<.UJ30 NJDEP Certified Drinking Water/Wastewater Laboratory ID *14116 REPORT DATE; March 5. 1986 LAB if 524 70 PRIORITY POLLUTANT LABORATORY ANALYSIS CLIENT: ENVIRO SCIENCES INC. SAMPLE SOURCE: Island ChcTnical Co. SA.MPLE ID: G-8 UNITS: mg/kgCppm') drv weight basis ' SAMPLE DATE; February 19. 1986 SAMPLED BY: Alan Kyles AT LAB DATE: Feb'-u.Tv ''i. 1986 MATRIX: Soil para-eter Antimony Arsenic Bervllium Cadriun Chror:ium Copper Lead Mercurv Nickel Selenium Silver Thallium Zinc Phencl Cvanide Sample Result X X X LT 0.23 20.4 32.8 19.4 LT 0.093 X X X X 76.2 X X 1 Minimum Detection Limit X X X LT 0.23 LT 0.21 LT 0.60 LT 1.3 LT 0.093 X X X X LT 0.4 4 X V Method Blank Analysis X X X LT 0.23 LT 0.21 LT 0.60 LT 1.3 LT 0.093 X X X X 0.99 X X dwb = Dry Weight Basis X " Net Analyzed LT » Less Than INDUSTRIAL CORROSION MANAGE-MENT, INC. RSL/dlh 100246 Ri6hard S. L^vin^ President K40n^ INDUSTRIAL CORROSION MANAGEMENT Fi I. ^ • . INCORPORATED I I M OOUll 10. >IA*XK.PH. HEW JlRSlt OObB JOl >»»-UJJO NJDEP Certified Drinking Water/Wastewater Laboratory ID ^14116 REPORT DATE; March 5. 1986 LAB tl 52471 PRIORITY POLLUTANT LABORATORY ANALYSIS CLIENT: ENVIRO SCIENCES INC. SA.HPLE SA-MPLE UNITS: SOURCE: ID: G- 7.2/k£( Isl -9 ?yn]. and d^^ Chemical Co. we .7ht hs'?-' t; "SAMPLE DATE; February 19. 1986 SAMPLED BY: Alan Kvles AT LAB DATE: Fehrn?-^v 21 . 1986 MATRIX; Soii dwb » Dry Weight Basis X " Not Analyzed LT - Less Than RSL/dlh Parameter Antimonv Arsenic Bervllium Cadmiun Chromiur: Copper Lead Mercurv Nickel Selenium Silver Thallium Zinc Phenol Cvanide Sample Result X X X LT 0.23 19.8 34.9 21.4 LT 0.113 X X X X 75.7 X X Minimum Detection Limit ' X X X LT 0.23 LT 0.21 LT 0.61 LT 1.1 LT 0.113 X X Y X LT 0.44 X X Method Blank Analvsis X X X LT 0.23 LT 0.21 LT 0.61 LT 1.1 LT 0.113 X X X X 0.99 X X INDUSTRIAL CORROSION .MA.NAGE.MENT, INC. 100247 Ri^ard S. Lawine^ President m INDUSTRIAL CORROSION MANAGEMENT pi L J t 1 INCORPORATED IIMMXITE 10. fiA«r3C4.f>H. NEWJERSEr 0/tlia 20l'ia4-03]0 L NJDEP Certified Drinking Water/Wastewater Laboratory ID tfl4116 REPORT DATE; M.arch 5, 1986 LAB H 52472 PRIORITY POLLUTANT LABORATORY ANALYSIS CLIE.NT: ENVIRO SCIKNCFS. INC. SAMPLE SA.MPLE UNITS; SOURCE ID: G- : Is 10 -s/^?(rpni) land drv Chemical weight JL Co. ?si? . SAMPLE DATE: February 19, 1986 SAMPLED BY: Alan Kvles AT LAB DATE: Fehru.Tv 2' 1986 MATRIX; Sn--i Parameter Antimonv Arsenic Bervllium Cadciu- Chromium Copper Lead Mercur-.- Nickel Selenium Silver Thallium Zinc Phenol Cvanide Sample Result X X X LT 0.30 30.6 62.7 16.5 LT 0.106 X X X X 66. 5 X X Minimum Detection Limit X X X LT 0.30 LT 0.27 LT 0.77 LT 1.4 LT 0.106 X X X X LT 0.56 X X Method Blank Analysis X X X LT 0.30 LT 0.27 LT 0.7 7 LT 1.4 LT 0.106 X X X X 1.3 X X dwb « Dry Weight Basis X • Net Analyzed LT - Less Than INDUSTRIAL CORROSION MANAGEMENT,INC. RSL/dlh 100248 (A^2^^ f-,^ ; INDUSTRIAL *' t i CORROSION MANAGEMENT INCORPORATED iib7Nuu:i lu iu>.«_™ NLW AKiir o/ubs yui sm u.i.u; NJDEP Certified Drinking Water/Wastewater Laboratory ID #14116 REPORT DATE: March 5. 1986 U\B It 52473 PRIORITY POLLUTANT LABORATORY A.N'ALYSIS CLIE.NT: ENVIRO SCIENCES INC. SAMPLE SAMPLE UNITS: SOURCE: Island Chemical Co. ID: G-11 m^/kg(ppm) drv weight basis ' SAMPLE DATE: February 19, 1986 SAMPLED BY: Alan Kvles AT LAB DATE: February 21, 1986 MATRIX: Soil Parameter Antimonv Arsenic Bervllium Cadmiu- Chromiur Copper Lead Mercurv Nickel Seleniu- Silver Thalliu- Zinc Phencl Cyanide Sample Result A X X LT 0.54 41.1 69.7 12.8 LT 0.194 X X X X 871 X X Minimum Detection Limit X X X LT 0.54 LT 0.49 LT 1.4 LT 2.5 LT 0.194 X X X X LT 5.1 X X Method Blank Analvsis X X X LT 0.54 LT 0.49 LT 1.4 LT 2.5 LT 0.194 X X X X 2.3 X X 1 i dwb = Iry Weight Basis X = Net Analyzed kLT = Less Than INDUSTRIAL CORROSION .MANAGEMENT, INC. 100249 RSL/dlh Vichard S. L^vi'i 'resident / J L'J N I IN DUSTRIAL CORHOSION MANAGEMENT INCORPOnATED 1152 ROUIE 10, HANOOLPll. NEW JCRSET 0rt69 201 S X OJJO O O Ul O NJDEP Certified Drinking Water/Wastewater Lahoralory ID n h \ \ f > REPORT DATE: March 10. 1986 LAB ff 52A63 Z CLIENT; ENVIRO SCIENCES. INC. - Island Chemical Company Prolect: SAMPLE ID: G-1 , ; SAMPLE DATE: February 19. 1986 SAMPLED BY: Alan Kvles ^AT LAB DATE; Fchruarv 21. 1986 VOLATILE ORGANICS BY PURGE AND TRAP ; By GC/MS - HEADSPACE Compounds detected in parts per million (milligrams/kilograms) dry weight basis, CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE ---• METHYLENE CHLORIDE ACETONE 1,1-DICHLOROETllYLENE -• 1,1-DICHLOROETHANE t-I ,2-DICHLOROETHYLENE CHLOROFORM 1,2-DICHLOROETHANE t-BUTYL METHYL ETHER -- 1,1,1-TRICHLOROETHANE - CARBON TETRACHLORIDE -- BROMODICHLOROMETHANE -- -ND— -NIL- -NIL- -Nil— JJt NI) ND NI) NI) NI) Nl) NI) Nl) NI) 1,2-DICHLOROPROPANE c-l,3-DICHL0R0PR0PENE t-l,3-DICHL0R0PR0PENE TCE (TRICHLOROETHYLENE)--- 1,1,2-TRICHLOROETHANE DlBROMOCHLOROMETHANE BENZENE --- DIISOPROPYL ETHER • 2-CHLOROETHYLVINYL ETHER • BROMOFORH - I,1,2,2-TETRACHLOROETHANE PCE (TETRACHLOROETHYLENE) TOLUENE CHLOROBENZENE - ETHYLBENZENE -- - ND ND ND _ N ! L U\L Nl) JUL JIIL JUL JJD JUL JilL Jin LT=Less Than, GT=Greater Than, ND=Not Detected dwb=Dry Weight Basis SURROGATE RECOVERIES; dj methylene chloride - 69Z d_ toluene - 125Z BFB - 13IZ For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 0,02 mg/kg(ppm) dwb. Other compounds detected: ' ^ • I •-^-: INDllTlRlAL COB^OBION MANAGEMENT, INC. [ nil?1 RIAL COBl^^ION MAN; 115 I'I INDUSTRIAL CORROSION MANAGEMENT INCOnPOnATED n s ; ROUTE 10. RANOoini. KEW JERSEY 07ec9 ;oi s x 0330 l-» O o to Ul NJDEP Certified Drinking Water/Wastewater Laboratory ID l l ] k \ \ f i REPORT DATE: March 10. 1986 LAB # 5246A CLIENT: ENVIRO SCIENCES INC. - Island Chemical Company Prolect SAMPLE DATE; Fcbrnnrv 19. 1986 SAMPLED BY; Aldn Kvles SAMPLE ID: G-2 VOLATILE ORGANICS BY PURGE AND TRAP By GC/MS - HEADSPACE AT LAB DATE; February 21. 1986 Compounds detected in parts per million (milligrams/kilograms) dry weight basis, CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE 1 ,1-DICHLOROETHYLENE -• 1,1-DICHLOROfTHANE t - l ,2-DICHLOROETHYLENE CHLOROFORM 1 ,2-DICHLOROETHANE t-BUTYL METHYL ETHER - - 1,1,1-TRICHLOROETHANE - CARBON TETRACHLORIDE - - BROMODICHLOROMETHANE - - NIL n[L NIL NIL NIL NIL NIL NIL i\y NIL NU. NIL N NIL NIL 1,2-DICHLOROPROPANE c-1 ,3-DICHLOROPROPENE t-l,3-DICHL0R0PR0PENE TCE (TRICHLOROETHYLENE)--- 1,1,2-TRICHLOROETHANE DIBROMOCHLOROMETHANE BENZENE - -- • DIISOPROPYL ETHER 2-CHLOROETHYLVINYL ETHER • BROMOFORM 1,1,2,2-TETRACHLOROETHANE PCE (TETRACHLOROETHYLENE) TOLUENE CHLOROBENZENE --- ETHYLBENZENE JUL JIIL JIL — NIL IL HIL JUL IL JUL Nn_ NIL LT=Less T h a n , GT=Greater T h a n , ND^Not D e t e c t e d dwb=Dry Weight B a s i s SURROGATE RECOVERIES; dj methylene chloride - 6«Z tiene BFB - 126Z d toluene - ll<iZ X For the above l i s t e d Volatile P o l l u t a n t s , nothing detected at a s e n s i t i v i t y level of 0.02 mg/kg(ppm) dwb. Other compounds detected: _ ^ 'y ' INDn^TIOAL COj^O^ON MANAGEMENT, INC. INDUSTRIAL CORROSION MANAGEMENT INCORPOnATED l»2 ROUIE 10. RANKOIPII. NEW JdlSir 0/(69 201 Ae4 0330 NJDEP Certified Drinking Water/Wastewater Laboratory ID l l \ k \ \ ( , REPORT DATE: March 10. 1986 LAB # 52465 CLIENT; ENVIRO SCIENCES. INC. - Island Chemical Company Project SAMPLE ID: G-3 SAMPLE DATE: February 19. 1986 SAMPLED BY: Alan Kyles _AT LAB DATE: February 21. 1986 VOLATILE ORGANICS BY PURGE AND TRAP By GC/MS - HEADSPACE Compounds detected in parts per million (milligrams/kilograms) dry weight basis. CHLOROMETHANE -• BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE 1,1-DICHLOROETHYLENE -- 1,1-DICHLOROETHANE t-l,2-DICHLOROETHYLENE CHLOROFORM 1,2-DICHLOROETHANE t-BUTYL METHYL ETHER -- 1,1,1-TRICIILOROETHANE - CARBON TETRACHLORIDE -- BROMODICHLOROMETHANE -- NI) NI) ND m Nl) ND ND JIQ. ND JilL JIIL JI!L Nl) JIIL JIIL 1,2-DICHLOROPROPANE c-1,3-DICHLOROPROPENE t-l,3-DICHL0R0PR0PENE TCE (TRICHLOROETHYLENE)--- 1,1,2-TRICHLOROETHANE DlBROMOCHLOROMETHANE • BENZENE - - DlISOPROPYL ETHER 2-CHLOROETHYLVINYL ETHER - BROMOFORM 1,1,2,2-TETRACHLOROETHANE PCE (TETRACHLOROETHYLENE) TOLUENE CHLOROBENZENE ETHYLBENZENE JIIL JIIL JUL JIIL JIIL JIIL JIIL JUL JIIL JIIL JIIL Nl) LT=Less Than, GT=Greater Than, ND=Not Detected dwb=Dry Weight Basis SURROGATE RECOVERIES; dj methylene chloride - 98Z d_ toluene - 61Z BFB - 57Z o o tJl IO J. For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 0.02 mg/kg(ppm) dwb. Other compounds detected: I CSION MANAGEMENT, INC. I ,..• (,,,• ' \ < t , - • • l . l . INDUSTRIAL CORROSION MANAGEMENT INCOnPORATED 115? ROUIE to. RANDOlfH. NEW JERSEY 07«69 201 5B< 0330 O O IO U l CO NJDEP Certified Drinking Water/Wastewater Laboratory ID n h W d 't • .J. { - REPORT DATE: March 10, 1986 ''v'^ ' • LAB H 52466 ' ':''-' ' CLIENT: ENVIRO SCIENCES. INC. - Island Chemical Company Prolect SAMPLE DATE: February 19. 1986 SAMPLED BY: Alan Kvles SAMPLE ID:_G-4 VOLATILE ORGANICS BY PURGE AND TRAP By GC/MS - HEADSPACE _AT LAB DATE; February 21. 1986 Compounds detected in parts per million (milligrams/kilograms) dry weight basis. CHLOROMETHANE --- BROMOMETHANE VINYL CHLORIDE CHLOROETHANE --- METHYLENE CHLORIDE ACETONE - 1,1-DICHLOROETHYLENE -• 1,1-DICHLOROETHANE t-l ,2-DICHLOROETIIYLENE CHLOROFORM 1,2-DICHLOROETHANE t-BUTYL METHYL ETHER -- 1,1,1-TRICHLOROETHANE - CARBON TETRACHLORIDE -• BROMODICHLOROMETHANE -- -NO- J l l l _ ND JIU _m J)U_ JIIL JIIL Jill Nl) NI) NI) Nl) 1 ,2-DICHLOROPROPANE c-l,3-DICHL0R0PR0PENE t-l,3-DICHL0R0PR0PENE TCE (TRICHLOROETHYLENE)--- 1 ,1,2-TRICIILOROETHANE D I BROMOCHLOROMETHANE BENZENE - - -• DIISOPROPYL ETHER 2-CHLOROETHYLVINYL ETHER - BROMOFORM - 1,1,2,2-TETRACHLOROETHANE PCE (TETRACHLOROETHYLENE) TOLUENE CHLOROBENZENE --- -- ETHYLBENZENE ND ND ND Nl) ND ND ND ND NI) NO NO JUL ND ND ND SURROGATE RECOVERIES; dj methylene chloride - lOOZ LT=Less Than, GT=Greater Than, ND=Not Detected dwb=Dry Weight Basis cl_ toluene BFB - 63% 70Z For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 0.02 mg/kg(ppm) dwb, Other compounds detected: INDUSjrRLAL COKKpiON MANAGEMENT, INC. //y/Zjt<yA(H.ylAi'^ • 'INDUSTRIAL CORROSION MANAGEMENT INCORPORATED l l j ; ROUIE to, RANDOLPH. NEW JERSEY a;a69 ; 0 I 584 0330 NJDEP Certified Drinking WaterVWaslewater Laboratory ID #l'tn6 t y ' . ! • •! o o lO (Jl REPORT DATE; March 10, 1986 ••."'•' LAB # 52467 CLIENT: ENVIRO SCIENCES. INC. - Island Chemical Company Project SAMPLE DATE; February 19. 1986 SAMPLED BY: Alan Kyles SAMPLE ID: G-5 VOLATILE ORGANICS BY PURGE AND TRAP By GC/MS - HEADSPACE AT LAB DATE: February 2 1 . 1986 •-'',- j : • Compounds detected in parts per mi 11 ion (mil 1igrams/kilograms) dry weight basis. CHLOROMETHANE BROMOMETHANE -- VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE 1,1-DICHLOROETHYLENE -• 1,1-DICHLOROETHANE t-l,2-DICHLOROETHYLENE CHLOROFORM 1,2-DICHLOROETHANE t-BUTYL METHYL ETHER -- 1,1,1-TRICHLOROETHANE - CARBON TETRACHLORIDE -- BROMODICHLOROMETHANE -- ND ND JUL ND JUL JIIL ND JUL_ JUL JUL JUL JUL Nl) JUL JIIL 1,2-DICIILOROPROPANE c-1,3-DICHLOROFROPENE t-l,3-DICHL0R0PR0PENE TCE (TRICHLOROETHYLENE)--- 1,1 ,2-TRICHLOROETHANE Dl BROMOCHLOROMETHANE BENZENE -- Dl ISOPROPYL ETHER 2-CHLOROETHYLVINYL ETHER • BROMOFORM - 1,1,2,2-TETRACHLOROETHANE PCE (TETRACHLOROETHYLENE) TOLUENE --- CHLOROBENZENE ETHYLBENZENE -- ND ND NO ND JiD_ JUL NO JUL JUL NO NIL JUL J&\L Nl) JUL LT=Less Than, GT=Greater Than, ND-Not Detected dwb=Dry Weight Basis SURROGATE RECOVERIES; dj methylene chloride - 97Z d„ toluene - 67Z o BFB - 66Z j( For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 0.02 mg/kg(ppm) dwb. Other compounds detected: • t MANAGEMENT, INC. I I I I I I ' l l l INDUSTRIAL CORROSION MANAGEMENT INCORPORATED NJDEP C e r t i f i e d Drinking Water/Wastewater Laboratory 10 iCltjIie Its; ROUIE to. RANDOini. NEW JERSEY 0/gS9 ?0I 5t« 0330 M O O to Ul tn CLIENT; ENVIRO SCIENCES. INC. - Island Chemical Company Project SAMPLE DATE: February 19. 1986 SAMPLED BY; Alan Kyles REPORT LAB H SAMPLE DATE: March 10. 52468 ID: G-6 1986 ' VOLATILE ORGANICS BY PURGE AND TRAP By GC/MS - HEADSPACE AT LAB DATE: February 21. 1986 Compounds detected in parts per million (milligrams/kilograms) dry weight basis. CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE --- 1,1-DICHLOROETHYLENE -• 1,1-DICHLOROETHANE t-l,2-DICHLOROETHYLENE CHLOROFORM • 1,2-OICHLOROETHANE t-BUTYL METHYL ETHER -- 1 ,1,1-TRICHLOROETHANE - CARBON TETRACHLORIDE -- BROMODICHLOROMETHANE - - ND NO ND JIIL JUL JUL JIJ) J I l i _ J U L - JID J ^ I I _ JID .NIL JID ND 1,2-DICIILOROPROPANE c-l,3-DICHL0R0PR0PENE t-l,3-DICIIL0R0PR0PENE TCE (TRICHLOROETHYLENE)--- 1 ,1,2-TRICIILOROETHANE DIBROMOCHLOROMETHANE BENZENE DlISOPROPYL ETHER --• 2-CHLOROETHYLVINYL ETHER • BROMOFORM • 1,1,2,2-TETRACHLOROETHANE PCE (TETRACHLOROETHYLENE) TOLUENE - CHLOROBENZENE -- ETHYLBENZENE JUL M - JUL Nl) JUL JUL JUL JUL JID ND JUL JUL JUL LT=Less Than, GT=Greater Than, ND=Not Detected dwb=Dry Weight Basis SURROGATE RECOVERIES; dj methylene chloride - 84Z d„ toluene BFB - 59Z d„ toluene - 66Z o For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 0.02 mg/kg(ppm) dwb. Other compounds detected: _ _ _ _ ^ 1 U, COIiVjKJON MANAGEMENT, INC. '-y./iff/zPz^z^ r 1 13 INDUSTRIAL CORROSION MANAGEMENT INCORPORATED lis? ROUIE to. RAND0iril.NEWJlllSEY0/eb9 ?0I )g« 0330 H O O lO Ul o^ NJDEP Certified Drinking Water/Wastewater Laboratory ID ll\k\\(> REPORT DATE; March 10, 1986 LAB ff 52469 CLIENT: ENVIRO SCIENCES. INC. - Island Chemical Company Project SAMPLE ID: G-7 SAMPLE DATE: Fphmnrv 19. 1986 SAMPLED BY: Alan Kvles ^AT LAB DATE: February 21. 1986 VOLATILE ORGANICS BY PURGE AND TRAP By GC/MS - HEADSPACE Compounds detected in parts per million (milligrams/kilograms) dry weight basis. CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE 1,1-DICHLOROETHYLENE -• 1,1-DICHLOROETHANE t-l ,2-DICHLOROETHYLENE CHLOROFORM 1,2-DICHLOROETHANE t-BUTYL METHYL ETHER -- 1,1 ,1-TRICHLOROETHANE - CARBON TETRACHLORIDE -• BROMODICHLOROMETHANE -- NIL NIL JUL JID- JUL JUL JJIL JUL ND_ ND_ ND NO ND Nl) ND 1 ,2-DICIILOROPROPANE - c-l,3-DICHL0R0PR0PENE t-I,3-DICHL0R0PR0PENE TCE (TRICHLOROETHYLENE)--- I,1,2-TRICHLOROETHANE DIBROMOCHLOROMETHANE BENZENE - DIISOPROPYL ETHER 2-CHLOROETHYLVINYL ETHER • BROMOFORM -- -- 1 ,1 ,2,2-TETRACHLOROETHANE PCE (TETRACHLOROETHYLENE) TOLUENE -- CHLOROBENZENE --- ETHYLBENZENE ND ND ND Nl) ND ND ND ND ND ND ND NI) ND ND ND LT=Less Than, GT=Greater Than, ND=Not Detected dwb=Dry Weight Basis SURROGATE RECOVERIES: 62 methylene chloride - IllZ dg tol BFB - do toluene - 126Z o j( For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 0.02 mg/kg(ppm) dwb. _X Other compounds detected: hydrocarbon RT 44 min. approx. 0.5 me/kR(possIbly octane) I CQRK^^IPI^ MANAGEMENT, INC. INDUSTRIAL CORROSION MANAGEMENT INCOnPORATED 11)2 ROUIE 10. RANDOLPH. NEW JERSEY 07)69 ?0I )«< 0330 NJDEP Cert if led Drinking Water/Wastewater Laboratory ID iflMl6 o o to Ul -J CLIENT; ENVIRO SCIENCES. INC. - Island Chemical Company Project SAMPLE DATE: February 19. 1986 SAMPLED BY: Alan Kyles REPORT DATE; March 10, LAB # 52470 1986 - : SAMPLE ID: G-8 '' VOLATILE ORGANICS BY PURGE AND TRAP By GC/MS - HEADSPACE AT LAB DATE; February 21, 1986 CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE --- ACETONE 1,1-DICHLOROETHYLENE - 1,1-DICHLOROETHANE --- t-l,2-DICHLOROETHYLENE CHLOROFORM 1,2-DICHLOROETHANE --- t-BUTYL METHYL ETHER - 1,1 ,1-TRICHLOROETHANE CARBON TETRACHLORIDE - BROMODICHLOROMETHANE - Compounds detected in parts per million (milligrams/kilograms) dry weight basis. ^p NI) ND .NIL Nl) JUL ND MIL NEL NIL ND ND JO. Nl) JUL 1,2-DICHLOROPROPANE - c-1 ,3-DICHLOROPROPENE l-l,3-DICHL0R0PR0PENE TCE (TRICHLOROETHYLENE)--- I .1,2-TRICHLOROETHANE DIBROMOCHLOROMETHANE BENZFNE DIISOPROPYL ETHER • 2-CHLOROETHYLVINYL ETHER • BROMOFORM - • 1 ,1 ,2,2-TETRACHLOROETHANE PCE (TETRACHLOROETHYLENE) TOLUENE -- CHLOROBENZENE ETHYLBENZENE ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND SURROGATE RECOVERIES; LT=Less Than, GT=Greater Than, ND=Not Detected dwb=Dry Weight Basis d2 methylene chloride - 104Z d_ toluene BFB - 55Z d_ toluene - 72Z _X For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 0.02 mg/kg(ppm) dwb. Other compounds detected: • I INDIia^fUAK CORWKJCN MANAGEMENT, INC, '//y\ / ( y / i yA/,iy)y.^ *y INDUSTRIAL CORROSION MANAGEMENT INCORPOnATED W i l ROUIE to, RANDOLPH. NEW JERSEY 07J69 JOI 584^330 H O O to Ul CO NJDEP Certified Drinking Water/Wastewater Laboratory ID #1'|116 REPORT DATE: March 10. 1986 LAB If 52471 CLIENT: ENVIRO SCIENCES INC. - Island Chemical Company Project SAMPLE DATE: February 19. 1986 SAMPLED'BY: Alan Kyles SAMPLE ID: G-9 VOLATILE ORGANICS BY PURGE AND TRAP By GC/MS - HEADSPACE AT LAB DATE: February 21. 1986 Compounds detected in parts per million (milligrams/kilograms) dry weight basis, CHLOROMETHANE BROMOMETHANE • VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE 1,1-DICHLOROETHYLENE -• 1,1-DICHLOROETHANE ---• t-l,2-DICHLOROETHYLENE CHLOROFORM 1 ,2-DICHLOROETHANE t-BUTYL METHYL ETHER -• 1,1 ,1-TRICHLOROETHANE - CARBON TETRACHLORIDE -- BROMODICHLOROMETHANE -• ND ND ND ND JUL JUL JUL Nl) • JID_ NI) ND JO.- .NU_ .Nl)_ JU1_ 1,2-DICHLOROPROPANE c-1 ,3-DICHLOROPROPENE t-l,3-DICHL0R0PR0PENE TCE (TRICHLOROETHYLENE)--- 1,1,2-TRICHLOROETHANE DIBROMOCHLOROMETHANE BENZENE • DIISOPROPYL ETHER 2-CHLOROETHYLVINYL ETHER • BROMOFORM -- - 1,1,2,2-TETRACHLOROETHANE PCE (TETRACHLOROETHYLENE) TOLUENE - CHIORODENZENE ETHYLBENZENE ND ND ND ND ND ND ND ND ND ND ND ND ND -NIL NI) LT=Less Than, GT=Greater Than, ND=Not Detected dwb=Dry Weight Basis SURROGATE RECOVERIES; dj methylene chloride d- toluene - 76Z o BFB - 68Z 102Z For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 0.02 mg/kg(ppm) dwb. Other compounds detected: INDUSTRIAL CORROSION MANAGEMENT INCORPORATED IIS? ROUIE 10. RANOOlPH. NEW JERSEY 07869 201 $640330 CLIENT: ENVIRO SCIENCES. TNC. - Island Chemical Company Project SAMPLE DATE: February 19. 1986 SAMPLED BY: Alan Kyles NJDEP Cert ified Drinking Water/Wastewater Laboratory ID ll\k\\f> REPORT DATE: March 10. 1986 LAB H 52473 SAMPLE ID: G-11 VOLATILE ORGANICS BY PURGE AND TRAP • By GC/MS - HEADSPACE AT LAB DATE: February 21. 1986 Compounds detected in parts per million (milligrams/kilograms) dry weight basis. o o to Ul vo CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE • METHYLENE CHLORIDE ACETONE 1,1-DICHLOROETHYLENE -• 1,1-DICHLOROETHANE t-l,2-DICHLOROETHYLENE CHLOROFORM 1,2-DICHLOROETHANE t-BUTYL METHYL ETHER -• 1 ,1 ,1-TRICIILOROETIIANE - CARBON TETRACHLORIDE -- BROMODICHLOROMETHANE -- JUL .mi J U 1 _ J U L — J I U _ JUL JUL JUL JIO_ JI ND JUL ND NI) LT=Less Than, GT=Greater Than, NI)=Not Detected dwb=Dry Weight Basis 1,2-DICHLOROPROPANE c-1 ,3-OICHLOROPROPENE t-I,3-DICHL0R0PR0PENE TCE (TRICHLOROETHYLENE)--- 1,1,2-TRICHLOROETHANE DIBROMOCHLOROMETHANE BENZENE - • DlISOPROPYL ETHER 2-CHLOROETHYLVINYL ETHER • BROMOFORM - - 1,1,2,2-TETRACHLOROETHANE PCE (TETRACHLOROETHYLENE) TOLUENE -- CHLOROBENZENE ETHYLBENZENE --- ND JUL JUL JUL JUL JUL JUL JUL JUL JUL JUL ND ND ND ND SURROGATE RECOVERIES; -WATER dj methylene chloride - lOIZ d toluene I 7 3 Z HKB 163Z For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 5 ug/l(ppb)-water 0.1 mg/kg(ppm) - soil Other compounds detected: 657. INDUSMd/y. COURCf^UJN MANAGEMENT, INC. MACi/<y,yi ynAZb^zz-^ tnvToo t ^ fotnctJ m-c 19COrtl>NORO CHAIN OF CUSTODY RECORD ,,, R. \ r) i. DE^fVILLE. NeWJ€nS€Y078M -jr^ T" v ! ^ r\ [ \ / t l t~\ \ \ I n s t a l l a t i o n : _y.(<rA//> ('.:yy<r.y,->c /yr-Ky^'y Su rvey No.: Samplers: (Signatur •e) y-Z/ rf y-Z/^,.^ V .—" CL 1= •3 C CO sr S t a t i o n L o c a t i o n Date Time Sample T y p e Corap.j o r a b rr u c O tti l-l • c o o .'.<?.-/V .y<'/rr.. /'//yyz <"/ • ? - y / y /.'7 yc - > ^ ^ ' i ' y ,- />/-.' zZ I • / - • • - • C y, ./^z. ..' Az/^--y//;-f7,/ V i ^ yz.t^^f y Z / ' r y / A .-. e l i n q u i s h e d b y : ( S i g n . ) • . y ^ . . y . y y . y y y ^ r . y i _ A c 1 i nqu i s llefl hy : ^^ 1 jj n . ) .-.e linquished by : ( Sign . ) Received by: (Sign.) Date/Time Received by: (Sign.) R e c e i v e d b y : ( S i g n . ) Ua L e / T i m e U a c e / T i m e r e l i n q u i s h e d b y : ( S i g n . ) 'Ispatched by: (Sign.) Rec'd by Laboratory Date/Time for field analysis (Sign . ) Date/Time '.ethod of Shipment Rec'd for Laboratory by:^ • ,1 ' Date /Tim"? / / • " 7-" I 100260 EnvffKS t£a 5a&K£i inc. 1« COPEUkNO RO.. 0€HV1LL£. HEW JtRSCY 07834 \br ?\\ Kvf(L€- /Chgn^Co^o, CHAIN OP CUSTODY RECORD In8tallatlon:_^^^ ^^^Cucyr^ y Z U y ^ Survey No.' Samplers: (Signature) ^ Z/ w - l o. B « C t/3 S t a t i o n L o c a t i o n D a t e Time Sample Type Uomp G r a b o 2 ZZk /A^yE,^/ y?E^s/^ r9^//y ' / I r ^ V ^ ^ ^ A"^ /V /v > o- y/en^ y^yiy \ c^^V ^-^ N; -f y<et^r<Y y ^ r r t ^ / f V .<^,<?r ya (^•^ y^<fy4;^J \ y y yo o \ y/0 /yyttiy y^e/Tys -y X :^^ - ^ ^ ' i ^ Relinquished by: (Sign. ) Reilnquished by: (Sign . ) Received by: (Sign.) Date/i Relinquished by: (Sign. ) Received by; (Sign. ) Da te /: Received by: (Sign.) Date/' Relinquished by: (Sign.) Rec'd by Laboratory for field analysis (Sign.) Date/ dispatched by: (Sign.) Dace/Time Rec'd for Laboratory b y : I L D a t e , .2 - Method of S h i p m e n t : 100261 • EnvmO E£4 JC&KZi IOC. 19 CXJPtLAND RO.. DEWVILLE. NEW JERSEY 07834 CHAIN OF CUSTODY RECORD I n s t a l l a t i o n : _ ^ ^ ^ ^ ^ ^ ^ ^ Survey No . : w . — t o. s fO o eo C S » , ^ 6« Station Location yy^^yy^^z^ i ^ / /£> Relinquished by:(Sign.) y^*^ Rellnquisheii by: (Sign. ) Relinquished by: (Sign.) Relinquished by: (Sign.) Samplers: (Signature) zy Date yA/^y^ Time .ZzzZZ^ y y Sample Type Comp .1 Grab y 1.1 0) c Lu T * O <TJ i.1 • C o o 2 U / A^ Received by: (Sign.) Date/Time Received by: (Sign.) Date/Time Received by: (Sign.) Date/Time Rec'd by Laboratory for field analysis (Sign.) Date/Time Dispatched by: (Sign.) Date/Time Rec'd for Laboratory by: Method of Shipment: f^ D a t e / T i m e q -^> /*- 100262 METALS Pit Slud' Cadmium Chromium Copper Lead Zinc ge 22.8 592 327 688 3594 Samole Points (Avg.) 1. 7 58. 9 45. 7 39.7 605 G--6& G--J_ % Of 7.5 10.0 14.0 5.8 16.8 100263 O o IO I 5 L A . ^ n c u ILKr\ I C A L : ^ O T ^ P L A M CJD CZD r~—IT ( "i 3 ( 3 ) r 1 } TAfJK FARM COOktMC^ * i » e n w i ^ . o «l<5t •l/N i.xia.j C i v r t i » u t t , ' <y •'"- e l | »ni. D ^fl TRENCHES / 7 i k V 0 - 50- y . \ :X « z z._, r,/ cnvino B fCicncEJ inc. • " ^ " ^ ^ ^ ^ ^ 19 COPELAND RD.. DENVILLE, fEW JERSEY 07834 * ^ ^ ^ ^ i ^ (201) 366^256 February 1, 1986 Mr. Conrad Simon USEPA Region II 26 Federal Plaza New York, N.Y. 10007 Dear Mr. Simon: Enviro-Sciences, Inc. (ESI) has completed the proposed scope of work for on site cleanup of the Island Chemical Company (Berlex) facility in St. Croix, U.S. Virgin Islands. The cleanup program and methodology were presented to Mr. Robert Harris of your office in December, 1984 and ammended in a subsequent report dated April 4,1985. Briefly, the cleanup involved decontamination at several locations. These are: 1) soil around above ground storage tanks - Toluene; 2) soil around a concrete pad - Toluene; 3) soil along a collapsed drain line - Toluene, Heavy Metals; 4) water and sludge in a process pit - Toluene, Heavy Metals, Benzyl Acetate; and 5) soil in a laboratory waste pit - Pyridine. All materials from the first four (4) locations listed above were containerized in proper 55-gallon steel drums, manifested and shipped as hazardous wastes to Chemical Waste Management, Inc. (CWM) Emelle, Alabama. CWM acknowledged receipt of these materials for disposal. The laboratory waste pit soil was treated on sire to decrease pyridine contamination level from above 1000 ppm to less than 2 ppm. ESI considers this level of contamination to be below levels which would require any additional cleanup efforts. 100265 February 7, 1986 Paoe -2- Tho collapse of the drain line and subsequent an.nlysis of soil has initiated the need to conduct additional sampling off-site in the "gut" or dry creekbed. ESI will undertake this sampling program immediately to ascertain the presence of contamination and, if present, concentration levels. We would appreciate any comments relating to our cleanup program at the Island Chemical Company site. You may contact me or Mr. Irving Cohen at (201) 366-6256. Very truly yours, ENVIRO-SCIENCES, INC. Alan L. Kyles, Ph.D. Vice President ALK/ak cc: Robert Milos Frank Curtis 100266 tZ cy*'^*y- yC^cL A. ^A "CHAIN orcul yTRKtJiiD tnrlroiMi n f 1 Servlcti DlTtilon '• •Z'TLfi. - ^ • - ' ^ ^ • • • t m ' ' - l f 7J-C 'p:et\t'r-'u>- .:V:. . (^01. a ^ - -»J ^ ml \ :^ 1 \ . , ' V ' * : y ^ ^ ^ C-. DA - »^ v i ^ A ~ ) y. --\ « J.. V . . ^ . . S . ] - C . ~ r ^ ( .'•*-^ f « n « * A«>«wia« la«»**Ubi S'.-'^L ^••' ar ••i«<»«<ri*k«d ar-. t»hmn9ttkmd ^w* K»K««*i«4W tr* i»t«n»mi< %n lM«i*«4 »r: ! • • • • • i9d C^*»a» •< C»«*4f • M M « tmr Ck« *--| lar Gk«»9« W C«w« f t t««a»B 4«* Clk«*a» •< < * • • # ! LOUIS DIGUARDIA G*o<ogiit (809) 773-6257 EXPERT H O M E REPAIRS No job i» too small WooODr.O^ A»»no« Eaiton. N«.» Je'i«v 06i37 12011321.6712 Rayniond Hay* lgC>it>«"« B»». u.s.v.1. 0 0 8 : : 100267 ATTACHMENT N 100268 ATTACHMENT N ' 610 W. MAIN ST., ROCKAWAY, NEW JERSEY 07866 MnviRO ^ sczncti inc. ^ y . - y y - y ^9 COPELAND RD.. DENVILLE. NEW JERSEY 07834 i i i i i i (201)365-6256 April 21, 1986 Mr. Conrad Simon USEPA Region II 26 Federal Plaza New York, N.Y. 10007 Dear Mr. Simon: This letter is to follow up on certain matters raised in our letter of February 7, 1986, a copy of which is enclosed. As we advised, Enviro-Sciences has sampled the "gut" area adjacent to the site. Analyses of these soil samples disclose the presence of the metal described on Exhibit A, at the levels set forth on the Exhibit. Subsequent EP Toxicity tests conducted on a composite of sample numbers 6, 7 and 11 indicate concentration levels do not exceed the maximum permissible concentration levels ser forth in 40 CFR, Part 261.24 (Exhibit A, page 2). Operations personnel at Berlex Laboratories, Inc. (the corporate parent of Island Chemical) have reviewed the processes in use by Island Chemical at the site. The metals listed on Exhibit A were not involved in the processes run by Island Chemical. While we do not know for sure, it is likely that these elements are present in the anti-rust paint used on the buildings on site (and many other buildings on the island). In addition, volatile organic analyses for soil samples at these same locations indicate that none are present. 100269 m April 21, 1986 Page -2- In view of the relatively low leachability of metals found and the likely source of the material involved, no further action is planned. Very truly yours, ENVIRO-SCIENCES, INC. Alan L. Kyfes, Ph.D. Vice President ALK/ak (86-13) CC: Charles Dolan, USEPA B. Kilos, Berlex R. Willis, Berlex F. Curtis, Berlex I. Arshen, Berlex 100270 G - 1 H O O to •J i GUT SOIL SAMPLING PROGRAM ISLAND CHEMICAL PLOT PLAN