USVI Public Records

Document text

SENT BY:I.T. CORP. KI\OXVlLLt~~7lu-25-S4 ~; : l.TTlOKr KI\OXVII i r- i Dl JL • - mTESNATIONAL TECHNOLOGY CORPORATION TELECOPY REQUEST TELECOPY SOMBER: TO: FROM: DATE: NUMBER OF PAGES REMARKS: i/i Cu_ fISCLODING COVER SHEET) ''A IT CORPORATION 312 DIRECTORS DRIVE KNOXVILLE, TN 37923 (615) 690-3211 DISCARD WHEN SEST PLEASE RETURN IF ALL PAGES ARE NOT RECEIVED, PLEASE ASK FOR EXTENSION 2221 AT THE ABOVE NUMBER. THANK TOO. IT XNOX7ILLE FAX NO. 615/690-3626 AND 615/690-4652 *64518* 64518 INTERNATIONAL TECHNOLOGY CORPORATION Project Name/No. ' ft Sample Team Members z. Profit Center No. ? Project Manager4 Purchase Order No.6 Required Report Date AIUALTSIB MCIMJEOI MRftJ CHAIN OF CUSTODY RECORD* P-'samptes Shpnqp* Date Page 1 of Leb Destination 1 JTT i Lab Contact LJ Protect Contact/Phone Cerrier/WaybiH *U-tJMi »( Special Instructions: ™ Ry* no fKp (?(uJ: m. UK //o^ ftut£*** In PiJ> / Possible Hazard identiftcation: 24 ^ . . Samb Possible Hazard Identification: 24 Non-hazard IJ Flammable J Skin Irritant J Poison B 'J Unknown flf Sample Dispose!: 2S Return to Client 'Jj I by Lab Arctitv*. •x (me Turnaround Time Required: Normal (A Rushl. evel:27 nJj iii.i 1. Relinquished by Time: v /^i Project Specific (spectfffcii *«/< 1. Received fly 28 ^/ J 2. Relinquished by Oete:. Time: 2. Received by 3. Relinquished by !Sigr>««urB/Aff*sUon) Date: Time: 3. Received by Comments: •CD uc.ro \_vra~. :liifK : J. I. CORF KNOXVILLE- IE 212 264 7611:*20/21 EPA SAMPLE W.I VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS T b Name*: ITAS- Lab Code: ITSTU Case No.: 54182 Matrix: (soi^water) WATER Sample wt/vol: 5.0 (g/mL) Level: (low/med) LOW % Moisture: not dec. ___ GC'Column: DB-624 ID: 0.530 (am) Soil Extract Volume: ______ (uL) Number TICs found: _Q Contract: SAS No. : TRIPBLANK SDG No.: MW1 Lab Sample ID: XX4805 Lab File ID: XX4805 Date Received: 05/28/93 Date Analyzed: 06/01/93 Dilution Factor: __ 1.0 Soil Aliquot Volume: CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L .(uL) CAS NUMBER COMPOUND NAME tf RT EST. CONC. Q FORM I VOA-TIC 3/90 SENT "BY: I. T. CORP." KNOXVILLE : 1 0-25-94 T~I: 42PM : I.T. CORP KNOXVILLE- 1A VOLATILE ORGAN I CS ANALYSIS DATA SHEET 212 264 7611:£19/21 EPA SAMPLE b Name*: Lab Code: ITSTU Case No.: 54182 Matrix: (soi^Jwater) WATER Sample wt/vol: 5.0 (g/mL) JJL,_ Level: (low/med) LOW % Moisture: not dec. ___ GC-Column: DB-624 ID: 0.530 (mm) Soil Extract Volume: ______ (uL) Contract: SAS No.: TRIPBLANK SDG No.: MW1 Lab Sample ID: XX4805 Lab Pile ID: XX4805 CAS NO. COMPOUND Date Received: 05/2B/93 Date Analyzed: 06/01/93 Dilution Factor: ____1.0 Soil Aliquot Volume: ____(uL) CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q 74-87-3-—————chloronethane___________ 74-83-9——————Bromomethane_____________ 75-01-4——————Vinyl Chloride__________ 75-00-3——————Chloroe thane_____________ 75-09-2——————Methylene Chloride________ 67-64-1——————Acetone_______________ 75-15-0———————Carbon Di*ulfid«__________ 75-35-4———————1,1-Dichloroethene________ 75-34-3——————1,l-Dichloro«thane________ 540-59-0——————1,2-Dichloroethene (total)__ 67-66-3—.———chloroform______________ 107-06-2——————1,2-Dichloroethane_______ 78-93-3——————2-Butanone______________ 71-55-6——————1,1,1-Trichloroethane______ 56-23-5---————Carbon Tetrachloride______ 75-27-4——-——Bromodichloromethane______ 78-87-5—•—————1,2-Dichloropropane_______ 10061-01-5————cis-1,3-Dichloropropene____ 79-01-6——————Trichloroethene__________ 124-48-1—————Dibronochloroaethane______ 79-00-5——————1,1,2-Trichloroethane_____ 71-43-2-—-———Benzene_________________ 10061-02-6———trans-l,3-Dichloropropene__ 75-25-2—————Bromoform_______________ 108-10-1—————4-Methyl-2-Pentanone______ 591-78-6—————2-Hexanone_____________ 127-18-4——————Tctrachloroethene_________ 79-34-5——————1,1,2,2-Tetrachloroethane___ 108-88-3—————Toluene________________ 108-90-7——————Chlorobenzen*____________ 100-41-4 ——————Ethylbenzene 100-42-5—————Styreno 1330-20-7—————Xylene (total)____________ 10 10 10 10 8 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 uuuu BJ uuu uu uu uuuuuuu uuuuuuuuuuuuuu FORM I VOA 3/90 MWAT IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS J Name: _ w Lab Code: ITSTU Case No.: 54182 Matrix: (soiVvater) WATER Sample wt/vol: 5.0 (g/aL) ML Level: (low/med) LOW % Moisture: not d«c. ___ GC'Column: DB-624 ID: 0.530 (mm) Soil Extract Volume: ______ (uL) Number TICs found: Contract: SAS No.: zo-i EPA SAMPLE NO. MW4DL SDG No.: MW1 Lab Sample ID: XX4609 Lab File ID: XX4809DL Date Received: 05/28/93 Date Analyzed: 06/03/93 Dilution Factor: ____2.0 Soil Aliquot Volume: CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L .(uL) CAS NUMBER COMPOUND NAME w RT EST. CONC. Q FORM I VOA-TIC 3/90 rvrrvm" T 1A VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE T -b Name: jTAS-KNOXVILLE________ Contract: Lab Code: ITSTU Case No.: 54182 SAS No.: Matrix: (soii/vater) WATER Sample wt/vol: 5.0 (g/aiL) ML Level: (low/med) LOW % Moisture: not dec. ___ GC' Column: DB-624 ID: 0.530 (am) Soil Extract Volume: ______ (uL) MW40L SDG No.: MW1 Lab Sample ID: XX4809 Lab File ID: XX4809DL CAS NO. COMPOUND Date Received: 05/28/93 Date Analyzed: 06/03/93 Dilution Factor: ___2 .0 Soil Aliquot Volume: CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L 74-87-3———————Chlorome thane__________ 74-83-9—————-Bromome thane__________ 75-01-4——————Vinyl Chloride________ 75-00-3———————Chloroe thane___________ 75-09-2———————Methylene Chloride______ 67-64-1———————Acetone_______________ 75-15-0———————Carbon Disulfide________ 75-35-4——————1,1-Dichloroethene_____ 75-34-3———————1,1-Dichloroethane______ 540-59-0——————1,2-Dichloroethene (total) 67-66-3——————Chloroform___________\ 107-06-2—————1,2-Dichloroethane______ 78-93-3——————2-Butanone____________ 71-55-6——————1,1,1-Trichloroethane___ 56-23-5———————Carbon Tetrachloride____ 75-27-4——————Bromodichlorome thane____ 7B-87-5——————1,2-Dichloropropane_____ 10061-01-5————cis-l, 3-Dichloropropene__ 79-01-6———————Trichloroethene___________ 124-4 8-1——•——-Dibromochloromethane____ 79-00-5———————1,1,2-Trichloroethane____ 71-43-2—————Benzene______________ 10061-02-6————trans-l,3-Dichloropropene_ 75-25-2———————— Bro»ofor»________________ 108-10-1——————4-Methyl-2-Pentanone____ 591-78-6—————2-Hexanone___________ 127-18-4——————Tetrachloroethene_______ 79-34-5——————1,1,2,2-Tetrachloroethane_ 108-88-3—————Toluene_____________ 108-90-7—————Chlorobenzene__________ 100-41-4—————Ethylbenzene__________ 100-42-5——————Styrene_______________ 1330-20-7—————Xylene (total)_________ 20 20 20 20 6 20 20 20 20 25 20 20 20 20 20 20 20 20 23 20 20 20 20 20 20 20 210 20 20 20 20 20 20 U u UuJuuuu uuuu uuuu uuuuuuu uuuuuu .(UL) FORM I VOA 3/90 IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS 74 EPA SAMPLE NO. Mb Name: JTAS-KNOXVILLE _______ tab Code: ITSTU Case No.: 54182 Matrix: (soi^water) WATER Sample wt/vol: 5.0 (g/nL) ML Level: (low/med) LOW % Moisture: not dec. ___ GC'Column: DB-624 ID: _0.530 (am) Soil Extract Volume: ______ (uL) Number TICs found: _0 Contract: SAS No.: MW4 SDG No. MW1 lab Sample ID: XX4809 Lab File ID: XX4809 Date Received: 05/28/93 Date Analyzed: 06/01/93 Dilution Factor: ___i.o Soil Aliquot volume: ___ .(uL) CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L CAS NUMBER COMPOUND NAME * RT EST. CONC. Q FORM I VOA-TIC 3/90 "SENTBY'r.T: CORF. KNOXVTLLET ;iO-2o-3<3 r 1A I . J . IDKP KXOXVILLZ- 212 264 7611:«15-'21 EPA SAMPLE VOLATILE ORGANICS ANALYSIS DATA SHEET Name: TTAS-KNOXVILLE Lab Code : ITSTU Case No . : 54182 Matrix: (soiiyvater) WATER sample wt/vol: 5.0 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. ___ GC' Column: DB-624 ID: 0.530 (mm) Soil Extract Volume: ______ (uL) Contract: SAS No.: MW4 SDG No.: MW1 Lab Sample ID: XX4809 Lab File ID: XX4809 Date Received: 05/28/93 Date Analyzed: 06/01/93 Dilution Factor: ___1.0 Soil Aliquot Volume: ___ CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L 74-87-3 ——————Chlorone thane_________ 74-83-9——————Bromomethane_____________ 75-01-4——————Vinyl Chloride_________ 75-00-3——————Chloroethane__________ 75-09-2——————Methylene Chloride______ 67-64-1—-——--Acetone______________ 75-15-0——————Carbon Disulfide_______ 75-35-4 —————— 1,1-Dichloroethene______ 75-34-3—-———-1,1-Dichloroethane______ 540-59-0—————1,2-Dichloroethene (total) 67-66-3——————Chloroform____________ 107-06-2——————1,2-Dichloroethane______ 78-93-3——————2-Butanone___________ 71-55-6———————1,1,1-Trichloroethane____ 56-23-5———————Carbon Tctrachloride_____ 75-27-4——————Bromodichloronethane____ 78-87-5———————1,2-Dichloropropane_____ 10061-01-5————cis-l,3-Dichloropropene__ 79-01-6——————Trichloroethene________ 124-48-1—————Dibromochloromethane____ 79-00-5——————1,1,2-Trichloroethane___ 71-4 3-2-————-Benzene______________ 10061-02-6—•———trans-1,3-Dichloropropene_ 75-25-2—————•—Bromofom______________~ 108-10-1—————4-Methyl-2-Pentanone____ 591-78-6——————2-Hexanone_____________ 127-18-4—————Tetrachloroethene_______ 79-34-5——————l,l,2,2-Tetrachloroethane_ 108-88-3-——————Toluene________________ 108-90-7—————Chlorobenzene_____________ 100-41-4—————Ethylbenzene__________ 100-42-5——————Styrene______________ 1330-20-7—————Xylene (total)_________ 10 10 10 10 2 10 10 10 10 25 10 10 10 10 10 10 10 10 26 10 10 10 10 10 10 10 240 10 10 10 10 10 10 uuuu BJ U U U U Uu D U Uuuu uuuuuuu Euuuuuu FORM I VOA 3/90 'itJM C T - I . T . LUKT. R1WXYTLLT TIU-Z5-31 1E OJKT VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS 212 264 761l:*14/21 EPA SAMPLE N0>." b Name: Lab Code: ITSTU Case No.: 54182 Matrix: (soi^water) WATER Sample wt/vol: 5.0 (g/»L) ML_ Level: (low/med) LOW % Moisture: not dec. ___ GC'Column: DB-624 ID: 0.530 (ma) Soil Extract Volume: ______ (uL) Number TICs found: _Q Contract: SAS No.: MW3 SDG No.: MW1 Lab Sample ID: XX4808 Lab File ID: XX4808 Date Received: 05/28/93 Date Analyzed: 06/01/93 Dilution Factor: ____i.o Soil Aliquot Volume: CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L .(UL) CAS NUMBER COMPOUND NAME RT EST. CONC. Q FORM I VOA-TIC 3/90 SLM BfU.T. COKF. KTCUXVTLLET I. 17 COKP tCVOXVILLE- 1A 212 264 751i:S13'21 EPA SAMPLE VOLATILE ORGANICS ANALYSIS DATA SHEET , Name: 3;TAS-KNOXVILLE_________ Contract: Lab Code: ITSTU Case No.: 54182 SAS No.: Matrix: (soiV&ater) WATER Sample wt/vol: 5.0 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. ___ GC Column: DB-624 ID: 0.530 (mm) Soil Extract Volume: _______ (uL) KW3 SDG No.: MW1 Lab Sample ID: XX4808 Lab File ID: XX4608 Date Received: 05/28/93 Date Analyzed: 06/01/93 Dilution Factor: ____ 1.0 Soil Aliquot Volume: CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L 74-87-3 ————— /•i oj y 75-01-4 —— —— 75-00-3 ————— 75-09-2 ————— 67-64-1 ————— 75-15-0 ————— 75-35-4 ————— 75-34-3 ————— 540-59-0 ———— 67-66-3 ————— 107-06-2 ———— / D ^ _> -J 71-55-6 ————— 56-23-5 ————— ^ C ^ ^ A t O O 1 3 10061-01-5 —— 79-01-6 ————— 124-48-1 ———— 79-00-5 ————— 71-43-2 ————— 10061-02-6 —— 75-25-2 ————— 108-10-1 ———— 79-34-5 ————— 100-41-4 ———— 100-42-5 ———— 1330-20-7 ——— — — Chloromethane —— Bromomethane —— Vinyl Chloride —— Ch 1 or oe thane —— Methyl ene Chloride —— Acetone —— Carbon Disulfide —— 1, l-Dichloroethene —— 1. l-Dichl oroe thane —— 1,2-Dichloroethene (total) __ —— Chloroform —— 1, 2-Dichloroethane —— 2 -But anone —— 1,1 , 1-Trichioroethane —— Carbon Tetrachloride —— Bromodichloromethane —— 1,2-Dichloropropane - — cis-1, 3-Dichloropropene —— Trichloroethene —— Dibromochloromethane ——1 , 1 , 2-Trichloroethane DCfliCJlo —— trans-l, 3-Dichloropropene ___ —— Bromoforv —— 4-Methyl-2-Pentanone — — 2-Hexanone — . -Te trachl oroethene —— \, 1,2, 2-Tetrachloroethane ___ —— Toluene —— Chlorobenzene —— Ethylbenzene —— Stvrene —— Xylene (total) 10 10 10 10 1 10 10 10 10 7 10 10 10 10 10 10 10 10 3 10 10 10 10 10 10 10 6 10 10 10 10 10 10 uuuu BJ U U UuJuuuuuuuuJuuuuuuuJuuuuuu FORM I VOA 3/90 IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS J»b Name*: TTAS-KNOXVILLE________ Contract: __ L~5b Code: ITSTU Case No.: 54182 SAS No.: EPA SAMPLE ND.C MW2 SDG NO.: MW1 Matrix: (soil^ater) WATER Sample wt/vol: 5.0 (g/»L) ML Level: (low/raed) LOW % Moisture: not dec. ___ GC'Column: DB-624 ID: 0.530 (mi) Soil Extract Volume: ______ (uL) Number TICs found: _a Lab Sample ID: XX4807 Lab File ID: XX4807 Date Received: 05/28/93 Date Analyzed: 06/01/93 Dilution Factor: ____1.0 Soil Aliquot Volume: CONCENTRATION UNITS: (ug/L or ug/Kg) OG/L .(UL) CAS NUMBER COMPOUND NAME - RT EST. CONC. Q FORM I VOA-TIC 3/90 SENT BY: I . T . CORP. KNOXVILLh :lU-25-94":"T:-ilMH : i . I . CORf KMJAV I LLt- 1A VOLATILE ORGANICS ANALYSIS DATA SHEET 212 204 /Oil -£ EPA SAMPLE N37 Lab Code: ITSTU Case No.: 54182 Matrix: (soil>yater) WATER Sample wt/vol: 5.0 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. ___ GC Column: DB-624 ID: 0.530 (mm) soil Extract Volume: _____ (uL) Contract: SAS No.: MW2 SDG No.: MW1 Lab Sample ID: XX4807 Lab File ID: XX4807 Date Received: 05/28/93 Date Analyzed: 06/01/93 Dilution Factor: ____i.o Soil Aliquot Volume: ___ CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L 74-87-3——————Chloromethane _________ 7 4-83-9-——————Bromoaethane_____________ 75-01-4——————Vinyl Chloride__________ 75-00-3————— -Chloroethane_____________ 75-09-2——————Methylene Chloride________ 67-64-1———————Acetone_________________ 75-15-0——————Carbon Disulfide__________ 75-35-4———————1,1-Dichloroethene________ 75-34-3——————l,l-Di chloroethane________ 540-59-0——————1,2-Dichloroethene (total)__ 67-66-3————•——Chloroform_______________ 107-06-2—————1,2-Dichloroethane________ 78-93-3———————2-Butanone_______________ 71-55-6——————1, i, l-Trichloroethane______ 56-23-5———————Carbon Tetrachloride_______ 75-27-4———————Bromodichloromethane_______ 78-87-5——————1,2-Dichloropropane_______ 10061-01-5————cis-l,3-Dichloropropene____ 79-01-6—————Trichloroethene__________ 124-48-1——————Dibromochl or ome thane_______ 79-00-5———————1,1,2-Trichloroethane______ 71-43-2———————Benzene _______________ 10061-02-6————trans-l,3-Dichloropropene___ 75-25-2——————BroB»oform_______________ 108-10-1——————4-M*thyl-2-Pentanone_______ 591-78-6——————2-Hexanone_______________ 127-18-4—————Tetrachloroethene_________ 79-34-5———————1,1,2,2-Tetrachloroethane___ 108-88-3——————Toluene_________________ 108-90-7——————Chlorobenzene____________ 100-41-4——————Ethylbenzene_____________ 100-42-5——————Styrene_________________ 1330-20-7—————Xylene (total)____________ 10 10 10 10 1 10 10 10 10 20 10 10 * -g- 10 10 10 10 10 35 10 10 10 10 10 10 10 200 10 10 10 10 10 10 u u uu BJ Uuuu uu U U U U U U Uuuuuu u uuuuu .(uL) FORM I VOA 3/90 SEN! BY: I. T. CORF. KiNOXVILLh i :-lurM • l . i . LUKr KMMV !U_t- 1E VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS 2i<i 20-1 (DJ.1 -~1U ^i EPA SAMPLE N2.1 Contract: Lab Name: ITAS-KNQ> Code: ITSTU Case No.: 5418? SAS No.: Matrix: (soiV*»ter) WATER Sample wt/vol: 5.Q (g/mL) ML Level: (low/med) LOW % Moisture: not dec. ___ GC'Column: DB-624 ID: _0.530 (mm) Soil Extract Volume: ______ (uL) MW1 SDG No.: MWl Lab Sample ID: XX4806 Lab File ID: XX4806 Date Received: 05/28/93 Date Analyzed: 06/01/93 Dilution Factor: ____1.0 Soil Aliquot Volume: ___ .(UL) Number Ties found: _Q CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L CAS NUMBER " COMPOUND NAME • RT EST. CONC. Q FORM I VOA-TIC 3/90 SENT BY:|.T. CORP. KINOXVILLE ;ll)-25-b4 : l:3bPM : 1 . 1 . COKr hiNOXVILLt- 2L2 zD4 /DH-S. ^.tl INTERNATIONAL TECHNOLOGY CORPORATION October 25, 1994 Ms. Caroline Kwan Project Manager New York/Caribbean Superfund Branch 2 United States Environmental Protection Agency Region II Jacob K. Javits Federal Building New York, NY 10278-0012 Groundwater Samples From O'Henry Laundry. St. Thomas. US VI Dear Ms. Kwan: This letter is a follow-up to our phone conversation yesterday concerning groundwater data included in the Risk Assessment for the Tutu Wells site, St. Thomas, performed by CDM. From our conversation yesterday and from the fax you sent me indicating which samples are in the data package used by CDM, it appears that CDM only has one of the data packages. Groundwater samples were collected from the four monitoring wells at the 0' Henry Laundry on two occasions in 1993, March and May. There were a variety of associated QA samples collected with these samples as indicated in Table 1 (attached). Analytical data packages from both rounds of sampling were transmitted to you in August 1993 and again in February 1994. For you information, I have enclosed Form Fs for the package that CDM seems to be missing (May 1993 sampling). If you need me to transmit the entire data package again, please let me know. Sincerely, Belinda K. Price, R.P.G. Project Manager cc: N. D'Anna, Esq. Regional OUice 312 Directors Drive • Knoxville. Tennessee 37923 • 615-690-3211 KNWOCTVWUCUU /T Coj.pwoHon j, o wftofly owned subsidiary 01 International Tbcftno/ojry Corpora* SEINTBY'l.T. CORP. KINOXVILLh :lU-25-b4 : I.I. LOKr IMVJA.V i (Oil -~ O- _j Table 1 Summary of Groundwater Samples Collected by IT Corporation. 1993 O'Henry Laundry, Tutu, St. Thomas March 1993 Sample * MW-01 MW-02 MW-03-OR MW-03-FD MW-04 MW-03 MS/MSO DRM01 May 1993 Sample # MW-01 MW-02 MW-03 MW-04 Trip Blank PW-1 Samples (7 Water Samples) Sample Description Sample From MW-01 Sample From MW-02 Sample From MW-03 Field Duplicate From MW-03 Sample From MW-04 Matrix Spike/Matrix Spike Duplicate from MW-03 Purge Water Samples (6 Water Samples) Sample Description Sample From MW-01 Sample From MW-02 Sample From MW-03 Sample From MW-04 Trip Blank Purge Water Analysis CLP VOCs CLP VOCs CLP VOCs CLP VOCs CLP VOCs CLP VOCs 601/602 Analysis CLP VOCs CLP VOCs CLP VOCs CLP VOCs CLP VOCs 601 /G02 SENT B Y : I . T . CORP. KM)XVILLE~": 10-25-94 : l:39PM : l . T . CORP KMXVILLfc- 212 2b4 7bli:s 4- CORPORATION SERVICES ft CERTIFICATE OF ANALYSIS IT Corporation June 23, 1993 312 Directors Drive KnoxviUe, TN 37923 Ann: Belinda Price Job Number: I IKK Ml 82—————————————————————————————P.'OrNumber: 490440.003 This is the Certificate of Analysis for the following samples: Client Project ID: St. Thomas Date Received by Lab: 05/28/93 Number of Samples: Six (6) Sample Type: Water-five (5); Trip Blank-one (1) 1. Introduction On 05/28/93, five (5) water samples and one (1) trip blank arrived at the ITAS-Knoxville, Tennessee, laboratory from IT Corporation, Knoxville, Tennessee, in support of the St. Thomas project. The list of analytical tests performed, as well as date of receipt and analysis, can be found in the attached report. / n. Analytic^ Results/Methodology The analytical results for this report are presented by analytical test. Each set of data will include sample identification information and the analytical results. Please note that the data are not blank corrected. The samples were analyzed for Target Compound List (TCL) volatiles by gas chromatography/mass spectroscopy (GC/MS) in accordance with the EPA CLP 3/90 Statement of Work. The samples were analyzed for halogenated and aromatic volatile organic compounds by gas chromatography based on EPA methods 601 and 602. Reviewed and Approved: Alyce R. Moore Laboratory Manager American Council ol Independent Laboratories International Association ol Environmental Testing laboratories American Association IOT laboratory Accreditation ,•; , , IT Analytical Services, 5*15 Mlddlebrook Pik». Knorville. TN 37921 am* S E N T B Y : | . T . CORP. KMXVILLh :lU-25-34 : l^ShM '• I . I . LUKr KiNOAVlux- kik ^o^ / O I L - 0^.1 FT Corporation IT ANALYTICAL SERVICES June 23 1993 5615MIDDLEBROOKPIKE ' KNOXVILLE. TN j» Henl Project JD: St. Thomas__________________________Job Number: ITEK 54182 HI. ftyaKtv Control Routine laboratory level I QC was followed. The volatiles analyses were performed by purge and trap with a J&W DB-624 megabore column on a Finnigan GC/MS/DS unit. The sample analyses went well. Elevated levels of tetrachloroethene in MW-4 required a two-fold dilution. There were no problems seen in final data review. Data were reported with qualifiers as follows: U - Compound analyzed for but not detected; value given is quantitation limit. E - Compound exceeded calibration range. D - Compound analyzed at a secondary dilution factor. J - Compound detected but below quantitation limit; value estimated. S • Spiked compound. B - Compound found in method blank. A - Suspected aldol condensation product. Y - Indistinguishable isomer in tentatively identified compounds. V - Presumptive evidence of compound presence. The samples were analyzed for halogenated and aromatic volatile organics by gas chromatography/photoionization and electrolytic conductivity (Hall) detection in series using an RTX 502.2 column on a Varian 3400 GC. No problems were encountered. M?<M SENT BY: I. T. CORP. KiNOXVILLt ;lU-25-b4" IT Corporation June 23, 1993 Client Project ID: St. Thomas . i. Cukr / G i 1 • "• 0 • _ i IT ANALYTICAL SERVICES 5615 MIDDLEBROOK PIKE KNOXVILLE. TN Job Number: ITEK 54182 HALOGENATED AND AROMATIC VOLATULJE ORGANIC ANALYSIS Result! in jig/liter (ppb) Sample Matrix: Water Client Sample ID: PW-1 Lab Sample ID: XX4810 Compound dichlorodifiuoromethane chlorometbane vinyl chloride bromometbane chloroetbane iricbJorofluoromethane 1,1-dichJoroethene s methyleoe chloride trans-1,2-dicbJoroetheoe 1.1 -dichloroethane cis-1,2-dichJoroetbeoe trichlorometbane (chloroform) I . I , J-trichJoroethane carbon tetrachloride benzene 1.2-dichloroethane tricbJoroethene Analysis Date: 06/03/93 Result Compound 1.8 U [,2-dichloroDiooane 0.8 U bromodicbJoromethane 1.8 U 2-chJoroethylvinyl ether 1.2 U cia-lt3-dichloropropene i 5.2 U toluene 2.0 U tran8-l,3-dicbJoropropcoe 1.3 U 1,1,2-trichloroethaac IS U tetrachloroetbetie 1.0 U dibromochloromethane 0.7 U chJorobearcnc 15 ethyl benzene 0.5 U xylenes (total) 0.3 U bromofonn 1.2 U 1.1,2.2-tetrachloroetbwDc 2.0 U 1,3-dichlorobenzcne 0.3 U 1,4-dichlorobenzenc 8.8 1,2-dichlorobenzene Result 0.4 U 1.0 U 1.3 U 3.4 U 2.0 U 3.4 U 0.2 U 49 0.9 U 2.0 U 2.0 U 1.0 U 2.0 U 0.3 U 3.2 U 2.4 U 1.5 U U - Compound was analyzed for but not detected. The number is the detection limit for the sample. IM SEM B Y U . T . COKP. KiNOXVILLt ;lu-25-b4 : i-4urM • 1 . 1 . KMM.V i 20-i /DJLJL •" IT Corporation June 23, 1993 Client Project ED: St. Thomas IT ANALYTICAL SERVICES 5815 MIDDLEBROOK PIKE KNOXVILLE. TN Job Number: ITEK 54182 HALOGENATED AND AROMATIC VOLATILE ORGANIC ANALYSIS Results La /(g/liter (ppb) Sample Matrix: Water Client Sample ID: Method Blank Lab Sample ID: B3297 Compound dichlorodifloorometbane chJoromethane vinyl chloride bromo methane chloroetbanc tricbJorofluoro methane 1.1-dicbloroethene s methyleoe chloride trails-1,2-dichloroethcoc l.l-dicbloroetbane cis-1.2-dichloroethene trichloronoetbane (chloroform) 1,1,1 -tricbJoroethanc carboo teirachloride benzene 1,2-dichJoroethane trichlorocthcoc 1.8 U 0.8 U 1.8 U 1.2 U 5.2 U 2.0 U 1.3 U IS U 1.0 U 0.7 U 1.0 U 0.5 U 0.3 U 1.2 U 2.0 U 0.3 U 1-2 U Compound 1,2-dichJoropropane broroodichloromcthane 2-chloroethylvinyl ether cis-1 ,3-dichioropropene toluene trans-l,3-dicbJoropropeoe 1,1,2-tricbJoroethanc tetrachloroetbeoe dibrotnochloromethane chlorobenzeoe ethyl benzene xylenes (total) bromoform 1,1,2,2-tetnchloroethane 1.3-dichlorobenzeae 1.4-dicb]orobearene 1 ,2-dicblorobenzene Result 0.4 U 1.0 U 1.3 U 3.4 U 2.0 U 3.4 U 0.2 U 0.3 U 0.9 U 2.0 U 2.0 U 1.0 U 2.0 U 0.3 U 3.2 U 2.4 U 1.5 U Analysis Date: 06/03/93 U - Compound was analyzed for but not detected. The Dumber is the detection limit for the sample. M71M SENT B Y U . T . CORF. K1NOXV1LLE :lU-25-94 IT Coiporation June 23, 1993 Client Project ID: St. Thomas l . i . LOKr Ki\OXV I LLt- / O i l . £ 0- IT ANALYTICAL SERVICES 5815 MIDDLEBROOK PIK£ KNOXVILLE. TN Job Number: ITEK 541K2 WATER SURROGATE PERCENT RECOVERY SUMMARY Client Sample ID PW-1 PW-1 Method Blank I -«h Sample ID XX4810 XX4810 (Dl:5) B3297 BCM 110 82 99 VOLATILE OCFB 111 78 93 ffi 112 - 117 QFCB 113 - 117 BCM - broroochloromethue OCFB - ortbo-chJorofluorobf)<ua«je FB - fluorobouene OFCB - ortho fluoro chlorobeozeoe PC LIMITS (60-127%) (65-126%) (64-126%) (73-128%) ~SENTBY:l.T. CORP. KNOXV1LLE : "10-25-94 : 1A . COKP KiNOXVTLLt- 212 204 / O i l • " 3< EPA SAMPLE VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Nam€: ^—'tab Code: ITSTU Case No.: 54182 Contract: SAS No.: MW1 SDG No.: MW1 Matrix: (soi^*/ater) WATER Sample wt/vol: 5.0 (g/mL) ML_ Level: (low/med) LOW % Moisture: not dec. ___ GC Column: DB-624___ ID: Q.S30 (mm) Soil Extract Volume: ______ (uL) Lab Sample ID: XX4806 Lab File ID: XX4806 CAS NO. COMPOUND Date Received: 05/28/93 Date Analyzed: 06/01/93 Dilution Factor: ____1.0 Soil Aliquot Volume: CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L 74-87-3——————Chloromethane___________ 74-83-9——————Bromomethane____________ 75-01-4——————Vinyl Chloride____________ 75-00-3——————Chloroe thane.____________ 75-09-2——————Methylene Chloride________ 67-64-1——————Acetone_______________ 75-15-0———————Carbon Disulfide ~ 75-35-4———————1,1-Dichlorocthene________ 75-34-3——————1,1-Dichloroethane________ 540-59-0——————1,2-Dichloroethene (total)__ 67-66-3———————Chloroform_______________ 107-06-2 —————— 1,2-Dichloroethane________ 78-93-3———————2-Butanone_______________ 71-55-6——————1,1,1-Trichloroethane______ 56-23-5——————Carbon Tetrachloride______ 75-27-4——————Bromod ichloromethane______ 78-87-5——————1,2-Dichloropropane_______ 10061-01-5———-cis-l,3-Dichloropropene____ 79-01-6——————Trichloroethene__________ 124-48-1——————Dibromochloromethane_______ 79-00-5——————1,1,2-Trichloroethane______ 71-43-2———————Benzene__________________ 10061-02-6————trans-i,3-Dichloropropene 75-25-2———————Broao£orm________________ 108-10-1——————4-Methyl-2-Pentanone_______ 591-78-6——————2-Hexanone_______________ 127-18-4——————Tetrachloroethene_________ 79-34-5———————1,1,2,2-Tetrachloroethane___ 108-88-3——————Toluene_________________ 108-90-7——————Chlorobenzene____________ 100-41-4——————Ethylbenzene____________ 100-42-5——————Styrene________________ 1330-20-7—————Xylene (total)___________ 10 10 10 10 1 10 10 10 10 22 10 10 10 10 10 10 10 10 6 10 10 10 10 10 10 j) 10 10 10 10 10 uuuu BJ Uuuu uuu uuuuu J u uuuuuu uuuu uu .(uL) FORM I VOA 3/90