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SDMS Document 115549 ISLAND CHEMICAL COMPANY, INC REMEDIAL INVESTIGATION ST.CROIX, U.S. VIRGIN ISLANDS DRAFT WORK PLAN Volume II of II Appendices D through 0 Prepared For Island Chemical Company, Inc By Harding Lawson Associates Philadelphia, Pennsylvania March 17, 1994 w o IO 00 cn Appendix D Rainfall Summary • y . \WORK\24231\02\WORKPU^N.REP HARDING UXWSON ASSOCIATES 301286 TABLE 1 TEMPERATURE AND PRECIPITATION [Daia from Alexander Hamilton Field, St. Croix] Month January February--- March April ^lay.--- J :ne -•-ly f .:?ust £ ;ptenber-- C -.tober N :venber— Diceober— Year Temperature Average daily maximum °F. 83 83 84 86 86 sa 88 89 88 88 86 84 86 Average daily minimum "F. 70 70 71 73 74 76 76 76 75 75 73 72 73 Average maxiaun •F. 86 86 86 88 89 90 90 91 91 90 89 • l " ^92 Average minimum •F. 65 66 66 68 70 71 71 72 71 70 68 67 ^64 Precipitation Average total In. 2.23 2.19 1.73 2.83 4.31 3.10 3.51 4.58 6.65 5.45 4.65 3.34 44.57 One year in 10 will have-- Less than-- ' In. 0.50 .44 .40 .55 .60 , .58 .80 1.20 2.20 1.60 1.20 1.00 34.00 More than-- In. 7.2 s:8 4.6 7.6 8.2 6.0 6.6 8.8 11.0 10.2 9.0 8.6 53.8 Average number of days with more than one-tenth of an inch of rainfall 5 6 4 6 8 9 8 9 10 8 9 .9 91 Average annual highest temperature. Average annual lowest temperature. 301287 Appendix E Clean Air Act Correspondence \WORK\2423l\02\WORKPLAN.REP HARDING UVWSON ASSOCIATES 301288 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION II 26 FEDERAL PLAZA NEW YORK. NEW YORK 10007 i/9 Mr. Harry Sponnoble Vice President/General Manager Island Chemical Company, Inc. P.O. Box 6733 Christiansted, St. Croix U.S. Virgin Islands 00820 Dear Mr. Sponnoble: This Is to inform you that the United States Environmental Protection Agency ("EPA"), Region II Office, has completed its review of the information you submitted dated April 5, 1979, relative to the chemical plant Island Chemical Company, Inc. ("ICCI") recently purchased in St. Croix, Virgin Islands. Based upon a review of this material and information derived from subsequent telephone discussions with your representatives, it 1s the determination of the EPA that this project is not subject to Federal Prevention of Significant Air Quality Deterioration ("PSD") regulations. The PSD regulations apply to (among other sources) any new or modified chemical processing plant with pro- jected potential (uncontrolled) emissions (In the case of a modification, the Increase In potential emissions) of 100 tons per year or more of any pollutant regulated under the Clean Air >Act. From information contained in the Virgin Islands Department of Conservation and Cultural Affairs ("VIDCCA") permits to construct for this project, the increase in poten- tial hydrocarbon emissions were calculated to be less than 100 tons per year; therefore, your project is not subject to the PSD regulations. It should be mentioned that although this source is not now subject to PSO, it may be subject to the PSD regulations In the future; the potential emissions associated with this source will be added to the potential emissions of any subsequent modiflcation(s) in determining PSD applicability, Should you have any questions concerning the contents of this letter, please feel free to call Messrs. Kenneth Eng or Gerald DeGaetano at (212) 254-4711 and (212) 264-4726, respectively. Sincerely yours, Meyer Director Enforcement Division • cc: Mr. Donald C. Francois Virgin Islands Department of Conservation and Cultural Affairs 301289 II D€SCRIPTION OF EQUIPMENT - MAJOR AiND APPLICABLE ITEMS AJ Utility Building " 1 . Boiler: Primary Make: " York-Shipley Inc. Pressure: 150 Ib/in^ Blower: 5 H.P. Burner: York-Shipley Inc. FV-40 Fuel Consumption: #2 Oil 257.1 Ib/hr (19,700 Btu/lb) Sulfur Content: Q.1C% Sulfur Emissions: 0.41 Ib/hr 2. Boiler: Reserve Make: Llraberto-Girola-Milano Pressure; 16 kg/cm^ Btu Rating: 7,936,000 Btu/hr Blower Motor: 5.9 KH feed Water Puip: 7.5 KW Burner: Oertli Fuel Consumption:. #2 Oil 402.8 Ib/hr (19,700 Btu/lb) Sulfur Content: 0.16Ji Sulfur Emissions: 0.64 Ib/hr 8. Process Area 1. ._ •' V Reactor R-l Stainless Steel Volume: 1,500 gal. Dimensions: 6.5 Ft.die, 10 ft overall height Condenser R-l: 15 sq. meter surface area Reactor R-4 Stainless Steel Volume: 1,300 gal. Dimensions: 6.0 F t . d i a . , 9 ft. overall height 2. Reactor R-2 Stainleaa Steel Volume: 1,500 gal. Dimensions: 6,5 ft.dia., 10 ft. overall height Condenser R-2: 15 m^ surface area Flame Front Generator MFG. By : John Zink Co. Serial #X52932 Air Orifice: L-l Gaa Orifice: 5/64 3 012 90 Carrier: Propane 3. Reactor R-101» Volume: Dimepsions: Gloss Lined 2,000 gal. 6 ft.dia., 13 ft. overall height Condenser E-lOl: I6m^ surface area Reactor R-102: Volume: Dimensions: Glass lined 3,000 gallon 8 ft.dia., 15 ft. overall height Condenser E-102: 16m2 surface area 4. Storage Tank:- Volume: Dimensions: Reactor R-3 Stainless Steel Volune: Dimensions; Reactor ,R-5: Volume:' Dimensions: Stainless Steel 19 m^ 10 ft.dia., H.'z> ft overall height 1,500 gallon 6.5 ft.dia., 10 ft. overall height Condenser R-3: 15 m^ surface area Carbon Steel 1,300 gal. i' 6 ft.diQ.,'9.5 ft. overall height 301291 Appendix F Cooper Laboratories Geotechnical Investigations \WORK\2423l\02\WORKPLA.N.REP . HARDING LAWSON ASSOCIATES 301292 —I Car:::;'c-.in Drilling Services INCORPORATED Box A5 Kincshill St. Croix V.I. 00850 (809) 773-2737 General Engineering Corp. P.O. Box A59 Christiansted, St. Croix May 12, 1979 CDS Job 1119^12 ATTEN'TION: Mr. John HcCallum REFERENCE: Subsurface Investigation - Proposed Cooper Laboratories Plant Expansion, Estate Bethlehem, St. Croix Dear Sirs: Enclosed herewith please find our soil engineering report for the above project. Based on the available soils information it appears that footing foundations are feasible for the support of the proposed units. Specific recommendations are included in the body of the report. Should you have any questions with regard to this report, please do not hesitate to contact us. Very truly yours, CARiaSEAN DRIU-ING SERVICES, INC. Joseph M./Lasero Registered Professional Engineer' 260E JMC:fs / / 301293 ;and and water borinjs / diamond core drilling / soils / concrete / csphalt / chemical grouting / piezor-.e:er '.-::c!irtJcn SOIL REPORT SJcSURFACE INVESTIGATION - PROPOSED COOPER LA5JRATCRIES PLANT EXPANSION, ESTATE BETH^E.-iEM ST. CROIX, U.S.V.l, INTRODUCTION The subsurface investigation for the proposed Cooper Laboratories Plant Expansion, Estate Bethlehem, St. Croix has been completed. Three (3) soil borings were performed at the site and the results of these borings, to- gether with a location diagram are included in this report. It is our understanding that the proposed expansion will occupy an area of 33 ft. by 17 ft. with various units including a large class reactor having an estimated total weight (including internals) iof 35 tons. Other units will have minor loads. The purpose of this report is to describe the soil conditions as encountered in the borings, to analyze and evaluate the boring and test data obtained, and to submit recommendations regarding feasible foundation design and construction. SUBSURFACE INVESTIGATION PROCEDURES The soil borings were performed using a trailer-mounted drilling rig equipped with a hydraulic head used.in the drilling and sampling opera- tions. Also used was a truck mounted rig for deeper holes. The boreholes were advanced using continuous flight hollowstem augers and representatiive samples were obtained by means of split-barrel sampling procedures in accor- 301294 ; C A R I B a e A N D B I U L I H C S E R V I C E S . I N C . ^ CDS Job j^-795:2 dance with ASTM Specifications D-15S6. In the split-barrel sampling procedure, standard penetration resistance values (blows per foot of a 140 lb. hammer falling 30" on a 2" O.D. split-barrel sampler) were obtained. These resistance values are an indication of the relative density of predominantly granular soil in piace. All soil samples obtained in the field were labeled, sealed and forwarded to the laboratory for further examination and testing. TESTING PROGRAM Due to the nature of the soil's encountered a limited laboratory testing program was implemented.. The program consisted;of reclassification of the samples and determination of the natural moisture content. The ..re- sults of all tests performed are shown on the boring logs opposite the cor- responding samples. Careful boring logs were kept in the field, where the soil samples were classified in accordance with the Unified Soil Classification System. After completion of the testing program, the smaples were again examined and the field classifications revised where necessary. SOIL CONDITIONS The site is located in an alluvium valley formed on the Kings- hill Formation of Lower Miocene Age. Sediments were derived from the north range and consist of fine sands, sandy clays and silty gravels. Variable stratification is present indicating braided stream deposition. 301295 iziz^!nn;^i;izzzz^^^ni!^ziii^zrzr CARI6BCAM ORI>.I.INC SERVICES, INC.izi^zzmzziiizmz^ni^rirzz^z^r^^^iizzi CDS Job /;79512 From a sciis engineering viewpoint, the upper surface soils (below existing coricrete slab at B-I and B-2) at all boring locations consist of either stiff silty clay or silty sand with variable percen- tages of clay to an average depth of rom 1.5 to 2.5 ft. Below this surface layer, medium dense to dense silty sand and gravel or sandy silt (B-1) strata were encountered which extended to depth of from 5.0 to 7.5 ft., merging gradually into sandy silt or silty sand with numerous rock fragments. This latter stratum was interspersed with sandy clay seams of limited thickness. The lowest soil formation encountered (typically below 15 ft.) was a medium dense to very dense silty sand and gravel ,which extended to the maximum depths investigated (i.e. 25 ft.). WATER TABLE CONDITIONS Water level observations made after boring are shown on the boring logs. Based on the available information it appears that at the time the borings were performed, the hydrostatic water table was at approximately 20 ft.' below the present ground surface at all boring locations. The hydrostatic water table should be anticipated to fluc- tuate throughout the year depending upon variations in percipitation and surface runoff. 301296 ; C A R I B B E A N D R I U I - I N C S E R V I C E S , I N C . CDS Job ••'/79512 Paae ^ ANALYSIS AND RECCi-lMENDATiONS As described under soil conditions, the upper, near surface soils, consisting primarily of silty clay or loose silty sand and are not considered competent soils. We recommend footing type foundations be used deriving their support from either the medium dense silty sand and gravel or sandy silt typically encountered at 3 ft. below present ground surface. Footings may be designed for a maximum allowable total load soil bearing pressure of 3000 p.s.f., when established on the bearing soils noted above. If higher allowables are required, footings should be established below 5 ft., at which depth an allowable 'total load soil bearing pressure of 4000 p.s.f. or higher may be used. For footings located on the medium dense silty sand or sandy silt at 3.0 ft. (min.) below present ground surface, anticipated settle- ments should not exceed %". Differential settlements, however, should be negligible. Due to the nature of the bearing soils, (particularly at the location of boring B-1) we strongly recommend that excavations not be left open for an extended period of time. Saturation of the sandy silt or fine grained sand will affect bearing capacity adversely. If satu- ration does occur, it is recommended that the soil (saturated) be removed to full disturbed depth prior to steel placement and pouring the concrete. "No construction problems are anticipated for the smaller 301297 ; C A R I B B E A N O R I L 1 . I N C S E R V I C E S . I N C . • CDS JoD //79512 Pace 5 units, but some sloucning of the 53.~i-granular soils may occur in the excavations, which may not permit certain foundations to be poured neat. Again the longer excavations are left open the more sloughing is to be andicipated. Site drainage should be given careful attention to insure that surface waters are not permitted to stand near or seep into the foundation bearing soils. This report has been prepared in order to aid in the evalu- ation of the site soil parameters and to assist the engineer in the design of the project. The analysis and recommendations submitted in this report are based on data obtained from three (3) soil borings per- formed at the locations shown on the reference sketch 79512-D. This report does not reflect the variations between borings which may not become evident until the course of construction. If variations then appear evident, it will be necessary for the soil and foundation engineer to re-evaluate the recommendations of this report after performing on-site observations and noting the effect of such variations on the design of the structure. 301298 C A R I B B E A N D R I U U I N C S E R V I C E S . I N C . # SOIL BORING LOCATIONS 301299 C A R I B B E A N O R I U U I N C S E R V I C E S . I N C . ; ^ - 2 ^o/i. Bo/z/js/Q AOCyfT/oyy<s y - f t t t Y / / 13-1 s C A R I B B E A N O R I I . t . l N C S E R V I C E S . I N C . ; 301300 SOIL BORINGS 301301 ; C A R 1 B B E A N D R I U U I N C S E R V I C E S . I N C . •. O W N C R ! COOPER LABS, INC. L O G O " P O n i N C I^OM<3tR E - 1 j P R O J E C T N A M E PLANT EXPANSIJ". A R C H I T E C T - E N G I N E E R GENERAL ENGINEERING, IN'C, ' SITE L O C A T ! ESTATE I O N BETHL z 0 < 1 > h U 0. J itl U Q 0 Z u -I 2 < X l •" ! ^ I < U I y. C i tf. D E S C R I P T I O N O F M A T E R I A L > I 0 I u ,- j 5 I SURF-ACE E L E V A T I O N Ih I O V) T O N S / F T . * > 2 3 i 5 ^ L A t T t C W A T C » L I Q U I D L I M I T •/• C O N T C M T ' ^ L I M I T N X- o -A 0 S T « N O A • O ^ C N C T W A T I C*N 3 0 • t o W » / K T . * 0 5 0 SS I I • o L U N L K L H I 5L7^5" LD - I 1 I PA 1 ] SILTY CLAY, L t . Brown, S t i f f (CD i 2 iss! -5 1 IPAj SANDY SILT - TRACE CLAY, Lt. Brown, Med. Dense (ML) SS LC SILTY SAND AND GRAVEL, Lt. Brown, PA "i Dense (GM-SM) | SS PA \ SANDY SILT W/WEATHERED ROCK FGMTS, Lt. Brown, Dense (ML-GM) • i ^ 5 SS PA SS IJJ SILTY SAND - TRACE TO SOME GRAVEL, Lt. Brown, Dense (SM) Bottom of Boring I ! WL l A . O ' WS on WD BORING STARTED 4 / 1 7 / 7 9 WL B C R ACR j BORING COMPLETED 4 / 1 7 / 7 9 CARIBBEAN DRILLING SERVICES. INC. SOIL A N D F O U \ D A T l O H CONSULTANTS '^ 1 9 . 5 ' - A.B. RIC 4 5 _ C FOREMAN )(_Q£ , APPRO V ED B Y J ; . ; ^ C DS JO B N O. 7 9 5 ^ 2 3 013 0T O W N E R I COOPER LA3S, INC. i-OG o r p O s . N c s „ i . - I PROJECT NAME PLANT EXPANSION A R C H I T E C T - E N C i N C E R GENERAL E\uI\EE-.lNG, :\:. S I T E L O C A T I O N i ' ESTATE BETHLEHEM z 0 I- < X > t- u ^ _i Ui U O 0 z u J c 2 < V) I u i Z I < c ! tn j_ I D E S C R I P T I O N O F M A T E R I A L a u I u I w -I I J > c. I t. 0 2 I 2 U I * ^ I C I SURFACE ELEVATION 5' O in 1. o — _ — U X C P - . ' . - t o C C > " " t « « ' V C I T I . I - C T . TC % » . r j . • • L . S T I C W A T C H L ' C U l O L I M I T * . . C O t . y Z . H r ' . . L I M I T • . , X- 0 - - - - - - A i z I D h " U U N L K L T ^ 5L.4r ^«-> STA NO A « D > 0 ' r C N C T W A T l O H 10 ZO 30 • LOwt/rT. *0 5 0 PA 1 iSSi 2 SS P A i I i 3 Iss trace clay to 3' SILTY SAND AND GRAVEL, Lt. Brown, Med. Dense to Dense (SM-GM) ^ iPA 4 Iss PA SS PA 4 6 SS SANDY SILT W/WEATHERED ROCK FGMTS, Lt, Brown (ML) SANDY CLAY - SOME SILT, Lt. Brown, Very Tough to Hard (CD SILTY SAND AND GRAVEL, Lt, Brown, Very Dense (SM-GM) k®i ®' \ Nl ® ® ® Bottom of Boring I I W L WS on W D WU B C R A C R BORING STARTED 4 / 1 8 / 7 9 BORING COMPLETED 4 / 1 8 / 7 9 CARIBBEAN DRILLING SERMCES, INC. SOIL A N D F O U N D A T I O N CONSULTANTS WL 1 9 , 5 ' - A . t B l . : l RIC 4 5 - C FOREMAN KDE ! APPROVED BYJI-'ICI CDS JOB NO. 7 9 5 1 2 301303 Ovs N L M COuPER LABS, INC, L O G O F B O R I N G N U M B E R B-3 . P R O J E C T N A M E PLANT EXPANSION A R C H I T E C T - E N G I N E E R GENERAL ENGINEERING, INC. I S I T E L O C A T I O N I ESTATE BETHLEHEM S ^ > - U M c o N ' < > . c o e o M - » t T O N » / r T . * ! I : 3 9 , i v r f T O K N C T ^ t 5 0 z u -1 a. 2 < Vl u c > • - UJ J c 2 < V) u u z < w on U u J tL 2 < w D E S C R I P T I O N O F M A T E R I A L S U R F A C E E L E V A T I O N ! % • I V I c li L I M I T •». X - - W AT CN C O M T C N T 6 - L I Q U t O Vl L I M I T S» A • u so tn c - J X—K ST A N O A WD < > P < N C T « A T I 30 • L O W % t r r . AC , SO SS PA J 2 SS SS PA SS PA • J ^ 5 SS PA 6 SS PA SS SILTY CLAY - TRACE SAND, Lt, Brown, M'^ri. Dense (CD -5 1 I PAl I SILTY SAND AND GRAVEL, Lt. Brown, Med. Dense to Dense (GM-SM) SANDY SILT - TRACE CLAY, Lt. Brown,! I M f - ^ . . rs,...-.,.,-. I Very Dense (ML) SILTY SAND WA'EATHERED ROCK FGMTS, Lt. Brown, Med. Dense (GM-SM) SANDY CLAY, Lt. Brown, Tough ^p, ^ SILTY SAND AND GRAVEL (WEATHERED ROCK FGMTS), Lt. Brown to Tan, Med, Dense to Dense (SM-GM) P®^ IO 0 / / ® / 6 <S) \ - ^ . ® yf ® V ® Bottom of Boring W L W S o« WD I BORING STARTED 4 / 1 7 / 7 9 W L BCR ACR I BORING COMPLETED 4 / 1 7 / 7 9 CARIBBEAN DRILLLNG SERMCES. INC. S O I L A N D F O U N D A T I O N C O N S U L T A N T S WL 2 0 . 0 ' - A . B , RIG 4 5 - C FOREMAN KQE 1 APPRO V ED B Y J[.^Q CDS J O B N O. 7 9 5 1 2 301304" r O W N E R COOPER LABS, INC, L O G O F B O R I N G N U M B E R B-3 PROJECT N A M E PLANT EXPANSION A R C H I T E C T - E N G I N E E R GENERAL .ENGINEERING, INC. S I T E L O C A T I O N ESTATE BETHLEHEM. f - l ^ - U M C O N ' I N K D C O A - ' O t > I I V ( I T K C N S T . T O N » / r T . ' ' 1 2 J < 5 < Z > H UJ c J UJ U 0 o z u - I c 2 < Xi « u u z Ul I w -• i > 0. 0 2 U ' O E S C R I P T I O N O F M A T E R I A L * I g • S U R F A C E E L E V A T I O N )- I = > i l ^ L A f T l C W A T C * L l O U l O L I M I T tm C O N T K N T % L I M I T % X- o A ' ID 20 >CV ST A N O A » O < > * P C N C T f l ATIC i r n • L O w m f r r , t o ? o 3 0 4 0 s o SS SILTY CLAY - TRACE SANO, Lt. Brown, MoH. Dengp , (CD PA SS PAi SILTY SAND AND GRAVEL, Lt. Brown, Med. Dense to Dense (GM-SM) SS PA SANDY SILT - TRACE CLAY, Lt. Brown, I ^ " y ^^"=" (ML) ^H ^ SS PA • J ^ SS PA SS PA SS SILTY SAND W/WEATHERED ROCK FGMTS, Lt. Brown, Med. Dense (GM-SM) SANDY CLAY, Lt. Brown, Tough ^p, ^ SILTY SAND AND GRAVEL (WEATHERED ROCK FGMTS), Lt. Brown to Tan, Med, Dense to Dense (SM-GM) p® 1 — : - - l'-' '^i ®' ® / ^ y < ® I o ® - — \ \ ! ® Bottom of Boring W L W S O R W D BORING STARTED 4 / 1 7 / 7 9 W L B C R ACR BORING COMPLETED 4 / 1 7 / 7 9 CARIBBEAN DRILLLNG SERMCES. INC. SOIL A N D FOUNDATION CONSULTANTS WL 2 0 . 0 ' - A . B . RIG 4 5 - C FOREMAN KDE APPROVED BYJMQ CDS JOB N O . 7 9 5 1 2 a i . : l 301305 "^ SUBSURFACE INVESTIGATION PROPOSED FIREWATER TANK COOPER LABORATORIES PLANT FREDERIKSTED, ST. CROIX U.S. VIRGIN ISLANDS 301306 ICARIBSCAN DRILLING SERVICES. INC. r n SOIL REPORT SUBSURFACE INVESTIGATION - PROPOSED COOPER LABORATORIES PLANT EXPANSION, ESTATE BETHLEHEM ST. CROIX, U . S . V . l . L • • . J 301307 J Caribbean Drilling Services INCORPORATED Pnon« 809-773-6162 EnglnMrIng Analyili ^ Rtoorti — Construction Quality Control lniD«ctlon — Ttsting — D««lgn Address Reply To: P.O.BOX 4S, KINSSHILL ST. CROIX, U.S. VIRGIN ISL. OOiSO Cooper Laboratories Inc. Frederiksted, St. Croix U.S. Virgin Islands Reference; Dear Sirs: Subsurface Investigation Proposed Firewater Tank Cooper Laboratories Plant Frederiksted, St. Croix August 19, 1980 CDS Job No. 81501 We are submitting herewith, our engineering report on the subsurface investigation for the above project. Based on the information obtained from the soil borings and laboratory test data, it appears that adequate support for the proposed tank may be obtained vdthin a reasonable depth at the proposed site. Specific recommendations are discussed in detail in the body of the report. Should you have any questions with regard to this report, please do not hesitate to contact us. Very truly yours, CARIBSEA5%?K,LING SERVJCK, INC. 301308 S O I L R E P O R T SUBSURFACE I.N-VESTIGATION FOR THE PROPOSED FIREWATER TAN'K COOPER LABORATORIES PLA.Vr, FREDERIKSTED, ST. CROIX, U.S.V.l. CDS Job No. SlSOl August 19, 1980 INTRODUCTION The subsurface investigation for the Proposed Firewater Tank to be located at the Cooper Laboratories Plant in Frederiksted, St. Croix, U.S. Virgin Islands, has been completed. A total of three C2) soil borings were performed and the results of these borings together with a location diagram are included with this report. It is our understanding that the Proposed Tank will be approxima- tely 57.0 ft. in diameter and approximately 58.0 ft. high. The tank is contemplated as a Firewater Reserve and is designed with a tank ring on a • compacted and treated fill. Foundation requirements stipulate a bearing capacity of approximately 2,000 psf with minimal settlement. Finished grade has not been established at this time but is expected to be slightly higher than existing plant grade, for ease in piping. The purpose of this report is to describe the soil conditions as encountered in the borings, to analyze the field and laboratory data and to submit recommendations regarding feasible foundation depths for the project requirements. SUBSURFACE INVESTIGATION PROCEDURES The soil borings were performed with a trailer-mounted drilling rig equipped with a hydraulic head used in the drilling and sampling ope- rations, the boreholes were advanced using continuous flight augers and 301309 ' C A R i a a E A N DRILLING SERVICES. INC. CDS Job No. 51301 representative samples were obtained by means of split-barrel samplers in accordance with ASTM Specification D-1S86. In the split-barrel sampling procedure, standard penetration re- sistance values (blows per foot of a 140 lb, hammer falling 50 in. on a 2 in. O.D. split-barrel sampler were obtained). These resistance values (SPT) are an indication of the relative density of the soils in place. All soil samples obtained in the field were sealed and forwarded to the laboratory for further examination and testing. LABORATORY TESTING PROGRAM Due to the nature of the soils encountered, a limited laboratory testing program was implemented. The samples were carefully examined and re-classified and the natural moisture content of representative portions was determined. The results of all laboratory tests are plotted graphi- cally opposite the corresponding samples on the boring logs. Careful boring logs were kept in the field where the soil samples were classified in accordance with the Unified Soil Classification System (USCS). At the completion of the testing program, the samples were again examined and the field classifications revised, where necessary. SOIL CONDITIONS The specific soil conditions at each boring location are detailed on the pertinent boring log. Typically, a medium dense browTi sandy silt, approximately 2.0 ft. in total thickness, blankets the site. This stratxjm is in a loose to medium dense state. 301310 ;CARIBaCAN DRILLINQ SERVICES. INC.^ - \ CDS Job No. 81501 # Below this surface veneer, medium dense light brown clayey silts or sandy clayey silts were encountered which extended to depths ranging from 5.0 ft. at boring B-5, to a maximum of 8.0 ft. at boring B-2. The clayey silts in turn are underlain by tough to very tough silty sandy clays which continue to the bottom of the boring B-1, and to approximately 12.0 ft. in boring B-5. Silty clays are absent in boring B-2 and the clayey silts previously mentioned extend to approxiaately 15.0 ft. The lowest soil formation at borings B-2 and B-5, was a dense silty sand with varying percentages of gravel which continued to the maximum depth investigated (15.0 ft.). Typically, below the surface veneer, density and strength increase with depth and moisture content decreases significantly below 7.0 ft. WATER TABLE CONDITIONS Water level observations made after boring are shown on the boring logs. Based on the available information, it appears that the hydrostatic water table was below the maximum depths investigated. The hydrostatic water table should be anticipated to fluctuate throughout the year depending upon variations in precipitation and surface runoff. Due to the possibility of occasional silty sand seams or gravel seams within the various formations, a perched water table may occur at the site during certain parts of the year. This condition would become evident during the time of construction. 301311 ; CARIBBEAN DRILLING SERVICES. INC.: # CDS-Job No. 81-501 A.NALYSIS AND RECOMMENDATIONS Based on an analysis of the soil profile and the results of the laboratory tests, we recommend that the site be excavated to approximately el. 102, and the footing for the tank ring be excavated further to el. 101. For footings so located, we recommend an allowable total load soil bearing pressure of 2,000 psf. Anticipated settlement for this load criteria should not exceed %". Differential settlements are not expected to exceed V . For the in- terior of the tank we recommend select backfill, preferably quarry screen- ings, between el; 102 and el. 105.5, be used. All backfill should be placed in 8 in. lifts Qoose thickness) and compacted "to a minimum of 93% of the maximum density as determined by ASTM Specification D-1557. We also recommend that the upper 6 in. consist of either oiled salt free sand or preferably oiled quarry screenings to preserve the inte- frity of the tank bottom steel (i.e. reduce moisture migration and oxida- tion to the bottom plates). GE?}ERAL RECOMMENDATIONS It should be noted that the proposed bearing soils are moisture sensitive. We therefore recommend that excavations not be left open for any extended period to minimize the possibility of saturation or overdrying. If saturation of the bearing soils should occur, it will be nece- ssary to remove the disturbed soil to full depth prior to pouring the concrete or backfilling within the tank ring. This precaution is necessary in order to prevent unduly high differential settlements upon imposition of load. 301312 ' CARIBBEAN DRILLING SERVICES. INC. CDS Job No. 81501 Due to the presence of silty clays and clayey silts relatively close to the bottom of the foundation system, it is imperative that mois- ture migration to the foundation elements be minimized. This may be accom- plished by sloping the site away from the tank in all directions. Further, we suggest paving an annulus around the tank ring with asphaltic concrete so that sheetwash from the tank sides will not penetrate the ring founda- tions or create erosion gullies. A 10.0 ft. annulus should be adequate. Needless to say, positive drainage away from the tank pad area to avoid local ponding is absolutely essential. Additionally, we recommend that the.excavation and backfill i operations be inspected by a qualified soil technician to verify that the proper bearing soil has been reached and to insure that the compaction re- quirements are met. The technician should perform in-situ density tests and the necessary proctor tests to establish compliance with these speci- fications. This report has been prepared in order to aid in the evaluation of the foundation soil parameters of this site and to assist in the design of this project. In the event that any changes in the design or location of the tank pad. , as outlined in this report are planned, the conclusions and recommendations contained in this report shall not be considered valid unless the changes are reviewed and conclusions of this report modi- fied or approved in writing by the soil and foundation engineer. 301313 ' C A R I B B E A N O R I U L I N C S E R V I C E S . I N C . SOIL BORING LOCATIONS 301314 [ C A R I B B E A N D R I L L I N G S E R V I C E S . I N C . -m 301315 S O I L B O R I N G S 3 0 1 3 1 6 -:?3 ; CARIBBEAN DRILLING S F R V l ' ' ^ S I N r OWNER- COOPER 'LABORATORIES PROJECT NAME PROPOSED FIREWATER TANK L O G O F B O R I N G N U M B E R B-1 A R C H I T E C T - E N G I N E E R S I T E L O C A T I O N FREDERIKSTED, ST. CROIX, U.S.V.l. 0 z u -J < Ift D E S C R I P T I O N O F M A T E R I A L SURFACE ELEVATION 108.7 - ( ^ U N C O N F I M C D C O M P a S l S I V K ( T K C N Q T M I T O N l / r T . ' I I 2 3 i 5 ! i - . Q V) Z 3 P L A S T I C W A T a a L I Q U I D L I M I T "r. C O N T C N T S L I M I T "T. X- • -A 10 to <0 90 ® ST A N O A ft O F C H K T U A T I C N • t O w i / r y . 40 50 SS See Note #1 PA SS TO SANDY CLAYEY SILT, Light Brown to Brown, Medium Dense (ML-CL) SS LL PA 2 4 4 ^ SS SAJXDY SILTY CLAY, Light Brown to Brown, Tough to very Tough CCL) \ \ A / ® ® Bottom of Boring Note #1; SANDY SILT W/ LIMESTONE FRAGMENTS, Brown to Dark Brown, Medium Dense (^^L) W L WS OR W D W L BCR A C R BORING STARTED 7 / 2 1 / 8 0 BORING COMPLETED 7/21/80 CARIBBEAN DRILLING SERVICES, INC. SOIL A N D FOUNDATION CONSULTANTS WL NONE - A J . RIC45-C FOREMAN KDE APPROVED B"|JMC( CDS JO^B NO._31501 "3 01317 OWNER COOPER LABORATORIES LOG o r BORING NUMBER B-2 PROJECT NAME PROPOSED FIREWATER TANK ARCHITECT-ENGINEER SITE LOCATION FREDERIKSTED, ST. CROIX, U . S . V . l , z 0 H < I > I- J Ul U Q 0 Z bJ .J a. < in DESCRIPTION OF MATERIAL SURFACE ELEVATION , Q y y -(^y- UNCONPINCO C O M P K K l f l V K «TR«NOTM T O N i / r T . * 1 2 3 i 5 i ' . >\: I t ' O V) t3 Z D ^UAiTIC klMlT •»• W A T I " COMT«NT LlOUlO UIMIT % X- • -A /C>, (TANOIkRO ' O ' PCNCTWATI CN 10 B L O W t / r T . 40 30 40- SS PA SSI PAi SANDY SILT, Brown to Dark Brown, Medium Dense (ML) SS PA SS PA SANDY CLAYEY SILT, Light Brown, Medium Dense C^tL-CL) trace gravel CLAYEY SILT W/ LIMESTONE FRAGMENTS, Brown, Dense (ML-CL) . ^ SILTY SAND § GRAVEL, Brown, Dense (SM-GM) \ ®. \ \ \ I Vi W L BCR A C R xtPiVTC « tr- BORING STARTED 7 / 2 1 / 8 0 BORING COMPLETED 7 / 2 1 / 8 0 I CARIBBEAN DRILLING SERVICES, ENC. SOIL AND FOUNDATION CONSULTANTS _ . — 4 C n 301318 OWNER COOPER LABORATORIES L O G O F B O R I N G N U M B E R P R O J E C T N A M E PROPOSED FIREWATER TANK B-5 A R C H I T E C T - E N G I N E E R S I T E L O C A T I O N FREDERIKSTED, ST. CROIX, U . S . V . l , z 0 ? < I > H liJ 0. J U UJ Q 4 9 - • a - 0 z UJ J a. 2 < Ifl UI J a. Z < Ift SS PA SS "PAT^ LC D E S C R I P T I O N O F M A T E R I A L S U R F A C E E L E V A T I O N 110.5 SANDY SILT W/ LIMESTONE FGMTS, Dark CLAYEY SILT - SOME SAND, Brown, Medium Dense (ML-CL) SS LD PA SS PA SS SILTY SANDY CLAY, Light Brown to Brown, Tough to very Tough (CL) . SILTY SAND - SOME GRAVEL, Brown, Dense (SM-GM) Q V) Z 3 - ^ - U N C O N r i N C S COMr T O N » / r T . ' I 2 3 ' L A I T i e LIMIT * l . X-- WAT«I» CONTENT ' - - • - • UOUIO LtMiT % --A u >0. JTAWOAKO *<> PCMCTKATI Bottom of Boring W L W L BCR WS OR WD A C R vnvc _ A~D BOR.NG STARTED 7 / 2 1 / 8 0 | CARIBBEAN DRILLING SERVICES, INC. B O R I N G C O M P L E T E D 7 / 2 1 / 8 0 ' SOIL AND FOUNDATION CONSULTANTS 301319 . 1 ^ . 1 % - — / ? \ 1 - • Appendbc G Report Concerning Small Quantity Generator Status of Island Chemical \WORK\24231\02\WORKPLAN.REP HARDING LAWSON ASSOCIATES 301320 IVnO • KKSK£S UK. 19 COPEUVND RD.. DENVILLE. NEW JERSEY 07834 (201)366-6256 May 7, 1985 Mr. Robert Harris U.S.E.P.A. Region II Room 1000 26 Federal Plaza New York, NY 10007 Reference: Island Chemical Co., St. Croix, U.S.V.l. Dear Mr. Harris: Enclosed is inforination concerning the manifesting of hazardous material at Island Chemical Co. when operations ceased and prior to its,sale by Berlex to Virgin Island Chemical Co. Included are eight (8) manifests. In addition/ there is an explanation as to why activities at the facility would classify it as a small generator. We are anticipating a meeting in the immediate future with USEPA staff members to discuss this project. If you have any questions, call me at 201-366-6256. Very truly yours, ENVIRO-SCIENCES, INC. Alan L. Kyles, Ph.D. Vice President ALK/po (AK-8531) Enclosure cc: Mr. Robert Milos Mr. Frank Curtis Ray Willis, Ph.D, 301321 REPORT CONCERNING SMALL QUANTITY GENERATOR STATUS OF ISLAND CHEMICAL The Island Chemical Company (ICC) was incorporated in Delaware on July 21, 1978. All of the shares were then owned by Cooper Laboratories, Inc. ICC stock has never been publicly traded on any exchange. The land currently under consideration, comprised of three acres more or less and situated at St. Croix, U.S.V.l. (the "leasehold") is owned by Charles H. Steffey, Inc. On May 1, 1969 Steffey leased the property to Houston Chemical Industries, Inc. Houston Chemical assigned the lease to Caribe Chemical Co., i Inc. (subsequently known as Pierrel America, Inc.) on March 20, 1972. On June 30, 1978 Pierrel America assigned the ground lease to Cooper Laboratories, Inc. On October 30, 1979 Cooper Laboratories assigned the lease to its subsidiary, ICC. On November 1, 1979 Cooper Laboratories sold all of the stock of ICC to Berlex Laboratories, Inc. (then known as ASAG Pharmaceuticals, Inc.) Prior to the acquisition of the leasehold by Cooper Laboratories, it is believed the prior owners used the site to manufacture phenacetin and ethoxyquin. Shortly before Berlex - 1 - 301322 m acquired Island Chemical, and with it the leasehold and improvements, the facility was being used by Cooper to perfect a four-step process licensed frora a French company to convert quinine, a relatively inexpensive compound, to its dextrorotary isomer quinidine, a far more expensive product. Cooper halted its work on the French process in mid-1979. Quinidine is the active ingredient ' in Berlex's product QUINAGLUTE* (quinidine gluconate) DURA-TABS* (sustained release tablets). After the acquisition of the facility in late 1979, ICC began preparation for the use of a quinidine process being developed by a West German concern. A single pilot batch was run with the French process, but the resulting product was not pure enough. It was not until October 198O that sufficient planning and research had been done on the German process to warrant full staffing and personnel training at the St. Croix facility. It was thus not until the end of I98O that production of pilot size, batches was begun. In addition, after that time the plant also was used to reclaim quinidine from rejected lots of final product. From the end of 198O until the end of I982 the St. Croix plant continued to experience production problems related to the purity and yield of the product and only during the last few months of 1982 were anything "more, than pilot batches produced. Early in 1982, Berlex made a strategic decision that - 2 - 301323 its backward integrating of the supply of quinidine was ill- advised since it caused Berlex to enter the chemical processing business with which it did not possess enough technical expertise. Consequently, the plant was permanently closed at the end of 1982. During its period of ownership, the plant was required only to convert quinine to quinidine or reclaim quinidine from final product. In both of these processes, toluene was used. In addition, quanitities of pyridine were used in the French process. Two laboratories were present at the St. Croix facility. An analytical laboratory was maintained to test raw materials, and to conduct in-process and' final product testing. A process laboratory was also present at the site for product development functions, primarily the small scalfe duplication (1-5 liter quantities) of steps in the process to work out problems and test improvements. Toluene. The German process in use for the conversion of quinine to quindine involved neutralization, oxidation, and reduction. At several points of the process, toluene was used. This toluene was recovered at every step. The entire amount recovered in every case was stored and reused when the process was run the next time. The same is true for the process used to recover quinidine from finished product. The toluene used in the process was recovered and reused when the process was run again. - 3 - 301324 Thus, the approximately 28,600 gallons of toluene on the site during ICC's use of the facility constantly was used in the two processes. At the time of the shut-down of the plant in December of 1982 by ICC, there was ho further useful purpose for this material and it was manifested (see attached manifests IC-01 through IC-06) and shipped to Inland Chemical of Puerto Rico, Inc. of Manati, Puerto Rico, where it was burned. Pyridine. Pyridine was used only in the French process, which was run only once by ICC. In addition, extremely small quantities of pyridine were on the ICC site for use as'a reagent in the analytical and process laboratories. Unfortunately, some of this material found its way down a sink drain in the laboratory, giving rise to the pollution described under point 4 on page 2 of the Addendum of Progess Report submitted by Enviro-Sciences, Inc. As you can see from the extent of the contamination described in this report, only small quantities were involved. Xylene. At the time ICC acquired the St. Croix site, approximately 6,900 gallons of xylene mixed with p-phenetidine was present. This substance was a raw material used by a former owner. It was at no time used by ICC. After the plant shut- down, it was shipped to Philipp Brothers Chemcials, Inc. in New York for sale. The sale unfortunately was not consummated and since no other purchaser could be found, the material was - 4 - 301325 thereafter manifested as a hazardous waste and shipped to Inland Chemcial in Puerto Rico for burning. See manifests IC07 and IC08 attached. Other Chemicals. As noted above, ICC maintained analytical and process laboratories on the site. Small quantities of laboratory chemicals were present in each. These included toluene; methyl chloride; alcohols, alkaloys and acids; benzophenone; and Dibah. These chemicals were for laboratory use only and were in containers.of the pint, quart, liter and gallon sizes frequently seen in the laboratory. Only very small quantities would be used at a time in laboratory procedures, e.g., a half pint or less at a time. Conclusion. Thus, as you can see from the foregoing, during the period of approximately two years when ICC operated the St.Croix site, the only wastes regularly generated were those stemming from the process and analtical laboratories. These would total no more than a few gallons or so a quarter. Thus, ICC was a' small quantity generator during this period. - 5 - 301326 UTTPe C N V i H U N M t N T A L Q U A U T Y B O A R D HAZARDOUS WASTE MANIFEST <r o 2 i ART A: CtKIUTM W M oocuMEPrr w . («0t) 77^X300 s m UXMEU Tiwie;ra<niRiio.t niDI« anuxMs TTWMSJWHH 110.2 T r * o « ^ « r t « D i d PMOK sn«)o«ss n U T M N T . STOMGt Ofl " ^ • l ^ ^ «5*-ICO0 rzii^'' f. R. |f,l|»,«,«,fi,*,J,),9,»!' |f^,5,»,»,0,4,<,*,3,r,' ^ ^ , a , » , « , « , j , : , 4 , J | i j ^ f|ti>«,<,0,!,»,•,7,11.: F UOfif W W TWO inwSPSRTfRS AR£ TO K UTU.HO. f l l OUT T « FOOOWUfi AS A l f f l O m T t TH15 F 0 » " 1^ > " '• f i f i T m i i n f TxKiBST u n w r - n nnoMJifT nn i<j P R 1, ..J ,,! 1 1 i 1 t f O f i H US OOT SHIPf>(MG HtMl 1 T o l « « n e V3 p. US OOT HA2*W)CUSS ri'.c-.. Li^ni-? UN mutm .:9A FORM L OUWOTTf 1 I ^ l ' l ' l * 1 , , , .0 UMTS k»!. OMfTWCIB . HO. i 1 | ) | l l l l TY?£ ^1^1 L-J—1 1 , 1 1 I 1 I I I 111 M 1 1 1II 1 1 nxi cnni. tl !QB/TF» WASTtTI \'\A' 1 1 1 1 1 1 1 1 1 1 1 •! 1 1 1 1 SKQAl HM«UNG WSTRUCTVWS MUUDING COMTAINER EOf MPTXJN ( I L IDEWTinCATION OF AOOmONAl WASTtS WCIUOEO IN $HK>M{VT OF X NONHUAROOUS UTU« VVXICH 00 WT K * « TO B U w r n t l D ) ^ I M B ^ N w t a Moa M n « 4 n a r u a v i proculr cJautixL iaunbai. ttmUi tni labiHta «i< * • n ptiwtf csnauon iw lanwonaiion Kttttmi " ' t jtl^MipilBiiiii IXS. EPX aid UM Ccmoranitth ol P.R Thi w n i i i a a i b t i ttmt v t i i onigntd u a< Ttmsooiv luntd. T)ii tl ^irdaus m e t . •>< Ixi i iilid pann« u do to. I cmitr f"> >^ (ortgomf a m »d tcnta ig I M bet si nr TTIU i JWlia) «l «r t — i l i i ^ IM o n i n n ol TIM jflitaOll iWii»ii»i • oil BkMidBi.' ..Z-'fW^-''- UU. O i l jTi TUNSraRTIR NQ. 1 VlHltU D. MO. I ' l ' i ' i ' i ' i ' i ' i •^^r^y OATl MCEIVtO 1_LJ L_L_l l_i MO OAT '?• TUS AT TKIS PERFORATION GEN Ers-s, S » ' — I — ' — ' — I — I — I — I — I — I — I SIGlUTUfSnoWihfttafniM r w u ^ K t O w m o c m a m i i r ,-) Z^ TBUItfOKIEfl NO. 2 SIGNATURE l o IA> test ol mr kmxiidgi iht = n i t n u ol Uu I twv« K£iOtc4 tw siRxpon contofmi wim t M dnchption vt tNt mamitit." ^ t W U S P o i T T l ?WNS?ORTIR NO. 2 VEHICU 10 NO y / y ^ ^ OATl O d l V t R t O j , , _ 11 1 -!_L DATE SiCllVlO I I I l_L_ NO. 2 SHjNATUIt -Ittttit-f I^ll I ttatt net Ivnptrid r t h of mjttiMili kkzLzmk T W T M a r STORAGE OR OISTOSAI f AUITY BMlUTWN 0 ^ ANY OIFf E«NC£S BflWtEN NUNIFEST ANO SHIPMENT OR LISTING Of RUSONS m A i O O U n s m O N OF REJECTED MATIRUIS 301327 t tTOMGf OR OlSPONSAl f ACUIIT SIGNATURE "Upon m u j i xipiciion. I r M U t r • * * • eoniimi «l Dia tk«mt<n conlaim onh iiu d n o i o i i v O" il>s mimleii •0 dJiatOMKie Actt4 on tnu (o«in" HANOUNG METXQO t>^/"^-V • y . 0 » n RECEIVED kl cai> «< xtaiincr o< ipij iatn,tii„rf o i l Ilu Eim/onminljl OuaMf 9o«o |t09l nS-U92 DOCUMENT N O . - ^ J , P n HAZARDOUS WASTE MANIFEST OQCUMEffT NO. P. K Chemical Cocroanv• Incorporated PHOMt (809) 778-??nr c a r p n n F . r a r p aprhlphgn^, Cr. r r n i - r 11. <; . V i - r f ^ n T . l . n ^ . IRnRNO.I T r a i l e r Marine Tranaport Corporation PHOM (809) 721-1313 sm AooKss l a l a Grande, Puerto Rico TMNSraRTlR NO.2 Tranaporte Diaz PHOFC (809) 792-7999 s n AOORtSS Zona Portuaria, Puerto Nuevo, San Juan, Puerto Rico TKUTMENT. STORAGE OR OiSPOSAt fTSO) FACIUTY I n l a n d C h e m i c a l o f P . R . , I n c , PHONE (809) 85A-1090 STTE AOORESS Km. 5 1 , Highway *2, Hanati, Puerto i i c o EPA -IMl. tlllMlil^LiLlillii! 0 M. ilu 1 P I R I D I 9 I 8 , 0 , 6 | A , A , 5 I 7 L :R|D|9|8|0|5|2|6|8|3 P ' R I D 10 | 9 | 0 | 3 l 9 i9l7 l l f MORE THAN TWO TRANSPORTERS ARE TO BE UTXKED. F U OUT T « FOUOWING AS A^PROfWn 1 1 THIS FORM IS NO. Of A TOTAl Of THE fIRST MANIFEST OOCUVEtfT NO. IS. PROPER US OOT SHIPPING NAME P. R. ^.^ 1° .2 . US OOT KA2AR0CUSS UN NUMBER fORM K T OUANTTH UMTS COtfTAINERS NO. TTPE Eia Itk KA2 £001 EQS/i WASTE I TOLUENE RQ Flara. Liquid 1294 a q 51 :ai I I I 1 I I I I I k. u o u U Ll- U U L^ U Li_ UL. U L_ SPEDAl HANOUNG INSTRUCTIONS I.NCIUOING CONTAINER tXE.MPTlON l i t lOENTlflCATION Of AOOITIONAl WASTES INCIUOEO IN SHIPMENT OF A N0NHAi4RO0USNATURE WHICH DO NOT HAVE TO BE MANIFESTED) GE NCRATOfT S CE RTIFICATIOtI: Tta a u n r t i t f Uu lAc U o t nanod n i t B i a t i « i piopcrtr d a u i t i o l i a i a t b t i . n a r t i d ind labtUtd M a i n propn u n a u o n tot iiim«on<non K u i a o q te D M •vpliuUo i i g u l i i o u ol K M O n a m n t n i l Tiansponnioo. U.S. EPA n d iKi CanvnonmNh ol PR. Tht w i s t i d t u r i b i d a b n i w i n conv^rud lo thi T i a n u c n v luniid. The Tif Mffltni. Slo'>9e or Onoosil f i o i i r t c m md will i c t i p t tht shipfflini ef h u vdous w n t t . and has 3 vsJid ptrnui to do u . I ctnilr thtt thi lofcqotnf is Tut »nd cocrta ta i M best elrnr knoMfftdgt^ G E K U T O R S SIGNATURE r^-T-rVw^ T i l Tnu Preaident OATE SMPPtO 1 11 11 I 71 Q I I fll •>{ UU." I j i f " 'JS " EXTECTED ARRVAl OAH ^ ANSPORTER NO. I SIGNATURE T o iln ttst oVu^ kntMritdqt tht antfnis ol tht sh«intra I h>v« sccepMtftoi irsrfcson cnlorms with Iht diioipiisfl on this mamltsl." TJUNS?ORTER NO. 1 VEHICU c r v T T 10. NO. ^ ^ ^ " I ? ! " " ^^nl^^l ii oi OATE RECEIVEO 1/ 1/ I \^Y^\ l£ MO OAT TEAR A I THIS PERFORATION PART B CEN EPA 10 a VI TiT^i oiRinifeisnini TRANSPORTER NO t SIGNATURE 1 u n i N l h « I h n t nol i i n p n i d M h o t m t i t r u l l Y Jdtttd Iht tonunis ol lh"» Ihiomnil • OATE OEIIVEREO TRANSPORTER NO 2 SIGNATURE "To iht Ptsi ol my knmliOqt Iht nnitnis ol Iht thvpmtnt I havt acctplcd foi liansoon conlofms w>ih ir>« dciciiption on ihii miniltsi." IRANSPORTER NO 2 VEHICIE 10 KO I I I I I ' I I OATE RECEIVEO I I I I I I L T U N S f ORTER NO 2 .^ir.NATURF n ;;nit> i V i U t x ' . ' r t txnpirid »<n oc n t i n i i l l r i ^ t r i d Iht contttits ol Ihl, ihioiMni " «n 4fr" TRUTVENT STORAGE OR OISPOSAI f ACSITY INOICATION Of ANT OlfFERENCES BETWEEN MANIFEST ANOSHIPtmENI OR LISTING Of REASONS FOR ANO DISPOSITION OF REJECTED MATERUIS TRATMENT STORAGE OR OlSPONSAl f ACIIITT SIGNATURE Uoon t i U H nsoitlion t ctnihr I h n tht u n i t n i i ol ihii ih«mtni eonloini wiih tht dciaiotiofl on ihit msniltsi B u o l Ihdsi OocieDsncifS nolld on this term" In c j i t ol tffltrgincy or ipi.l >mmediitilT c**! 'ht EnvMonmenial Quilirr Soiid 18091 !)2Ma92 301328 DOCUMENT NO HANOUNG METHOO DATE RECEIVEO L-L-l L , ^ L P R. - y y E / ^ V I R O N M E W f A L QUALITY O O A n o O^ZARDOUa WASTE rjANirJ^T OOCUM£>(T NO. P.R. y-'—i 1^>'\ "taynyi" liXvr^-ft'HeJ PHONE L.-.;:, vi.llfl ti'i" • '• • ' ^ t . .. I i-iiuiiE .< Ariiia.':<; .-.•niiini).-ICJ TnJfic y---rvV) !•- AIMIRESS _•_. r . ; r r - . i ' l r ^ r n - V - ' n . ':-.:z. .V--:, li.l.Ml.l'NI. SlUIMGC OR '•••••""-•' OS--I FACIUTY ) . - v - . ^ , i o ; , , . . . , v . . ; r ' '• V I. ..Ml Aiiiiws; mm. (•- ' ' ."-•-Tr-^-> ' \ ,1:.--rl. ^u EPA •.:nm ^y^M• r\vu IIIANSCORTERS A K TO BE UTIQID. fm OUT nn FOUOWIHC AS APPROIIAJE ' ' — OF A TOTAl Of — 1 — THE FIRST MANIFEST OUCUMENT NO. IS. 1111$: luiVA IS no • P.R. >U llll. LLLLLinillULLxLL .Mr iy-lo.Ki._L.; .'.JLi; iJidxd!jJL_L_l:.J..J;.L.! • f - l i t i j ? ,1-; L-J.. J ^ i r J . I" lit !• rr.iirtR US COT SlliniNU NAAU us OOT HA2AR0aASS 'A.-:. T,-;-iu.LL UN NUMOER FOfiM NET OUANTTTf .,L..Ld l l l l I I l l l l t. ) .1 I UWIS J i . zhrrZ. CONTAIWHS ^0. Li_.J TTPt L J L L J I I I I LJ ZZ II-.: IIM I r;:it U I!l0- •i:i.v. 1_L L.L LLiiU.lL LJ ILI ill . I > <»l K>\' .'\ii"<- Q S i m c n O N S MaUOWG CONTAINER EXEMTTKM )li. DENTiriCATKM Of AEIOmOHAl WASTES HauOCD M SMPMEKT Of ANOmAZAfnoti':>l«I<)::i 7/:r •11 ---.m HJ\=. TO Bt MAWfESTEOl ' ;• ii;.iuii • I" liTlFiCMION: Ihs a t» nnitir Uu ihi aten uiwd Kmuvii ait pio^itilr dssilnA UKIIUCU, ouakid andlabettd aid « i n pii>9« conamai ka i.-T>s,i.i Jil^ >.. ..m.. i;». Mvlirt Jc rrwiUiom »J tarn P«»«>iien »l TrxspaubK US. EPA m i INt Camnonttitli el f l l The watt d e o i M itiart m n tamnffi w tkt Titwi-:.* i.in>ii T -ini.'ni. Sii*'<r" (laroidftoHqaa an^ «4i ecupt the leieHeni e^liaiydanw.isJt. Mti lias i valid pamit la dese. l o i t i ^ lliai ih#> fortyMiqisinManitfanttM'iiHr h"-*"i> ».Mr«ion'.;siuvMius£ THU • .'iSnJRTt-'i NO 1 SlGNATUff "T« » • fc««l •* trt ta—UP^t Dw t M t n o tl Iht TRANSTORTER Na t VEHKIE «. NO. .•; OATE SMlfED 4 y y y y y ) 1 1 V 1 -1 1 1 •• - 1 •.' -• 1 . /xncTio inaii.i. n« LJ_J l.L.i OArEiaci:yin 1.J-' I. L.l ' MO |..i HAR AT TWS PEItfOKAIlUN :y-k-. %y---^ •/- .!IT ••! GEN EPA DJ» L J_LJ_L-UI-.I ••..••.tnjKIIHKO. I : - .1 Ih:: |..nlrTirt SHNATimE iaryiVi>*'ii>*n'*"'*'*"^.<'<***M<su')r \ .1 ,.„.''^^/^^,<^-7/kz,:-''..y\,.t .„-.y ylky.-y. \ IH :.'.rOn'l R NO 2 SONATUK ~7« Kw kwt ti mt >i«i«ii^. I M wntMs tl Iht j •>,),iw«l Liw t r t i > i t d l a r t n > a p « i E B ^ a s ; ± ± : t = ; ; ^ a I k i s s a « l t s l ' TRANSTOHtER NO. 2 vtwaE B NO. I I I I I I I I DATE Ot','•.•»:> ;i L L J L •• OAII ir.iii.' I L-l_) I..I. «X1 .I;'. I \t.y4snm\.*. n i BEUTUK •\^f*t kii i kM m U>«B«d « M « wda>u*r k^kk ri(.\ W « i SIOMfi M g e r a t M ^ ^ a i n W C t T n IF MtTOFFERCNas I H M i N UMVESTAM SIPMEirT W U T K OF l U ^ rv, 301329 TRAiMEin siuHAg OH annmi^ twam awuiat -u>.» tamd t-tieom t:«<«t fce-.t dBcinawn «»<•< «* » • > » • ' •_ l l t « d (tOSI " C/n Mfl'iOO 5^/ ».' S*TF Kcimo J^_ilfe tWCUMEKT M. _ P. H i.*E A^PilORNAME ^ i . : ' ...; ciio-iiciti Co., i f w . UUCUMlNi N U . PHONE (I.U9) 7711-2201) P sm AOORESS 1. :<: 13 'J Cctuto flc'ihlchcn, St. Croix, U.S. Vir.nin Irjlcndj IIUNjrORIIR NO 1 r, - l . l - ''..rinn Trmqiort Cnrjinrntlnn PHONE (!;<iy) 721-1313 SITE AOORISS TRANSPORIER NO } 1, Lo ':;i;iz PHONE (•JU7) 792-7999 SITE AOORISS /... ;• M-Lui^rtn, Puerto Nuavo, S:in Ju.jn, Fuorln \\\ca TRUTMENT. STORAGE OR oisPOSAUTSoiFACIUTY I n l . - n d Clim.i.lcal o f P . H . , I n c . PHONE (i;;j9) nw-iii90 SITE AOORESS .. . y., lll.MU.iy J 2, M-nncitl, Puorto Rico f R. ir '3 EPA 0 mi V,I,D,9,a,Q,C,,!.,l,n,;, p,n,D,9,Q,n,6,i,A,3,/, P|R,D,9,U,0,5,:;,--,,:'.,^ p,R,i),n,9,n,3,9,y,7,i, IF MORE THAN TWO TRANSPORTERS ARE TO BE UTUIZED. f U OUT THE fOUOWlNG AS APPROPIATE THi^ (npM IS nn nf A TOTAl O f — J — T H F FiH<n MANiFFrrnnriiurifTiin is P R I | C , 0 | 3 ) i i PROPER US OOT SHIPPING NAME ,Ti:>T-..-v:: . . : 2 3 4 5 6 SPECUl HANOUNG INSTRUCTIONS INClUOING C 00 NOT HAVE TO BE MANIFESTED) US OOT HAZARD ClASS Flcin. Llc^iitl UN NUMBER 1294 FORM L • Mr QUANTITY lA|7lfi|3 UWTS Ccil, CCNTAJNERS no. TYPE 1 11 illtX I.Jil, I n II J ! 1 : 1 1 1 . . 1 I 1,1 L J . IdB- iPA KAi cirtf Li EQB/EPA WASH h In.', !- 1 1 I I L. 1 ! 1 . 1 1 M i l }NTAINER EXEMPTION r i L DE.NTIFCATKIN Of AOOmONAl WASTES INCIUOEO IN SHIPMENT Of A NONHAZARDOUS NATUKE WHICH I GENERATOR'S CERTIFICATION: This a to unilY tha ih< aboti namtd aaiinals u t piopirtr dassilitd. disoibtd. inarttd and labtlltd and > i n propv onoiuen io> i r n p o n a i a n x u r o i n g le Iht applicaMt rtqulaiions ol tht Oiavimtnt ef Trarupontfton U . l E?A and tht Cemaicrwtahh of P.R Tht w m a dtsnihtd a^ovf w t r t conijfntd le dit TiamoonB eamtd. Tht Trtaimtnt Sieragt er Oisoosal f acilbr can and will accept ilM shipottm ef haiirdous wasia. and has a vafid ptfmii te do sa. I canifr thai i h t fort^oir^ is n a *^d csnta le ibt best of mr inawliiliit GENERAIOirS SIGMATURt '. - .-. . ; / •, / • f V ' ' , ; Z •Je3:tjnQ H . l u c h v l t ] ^ TlTlE P r c j i d c n t DATE SHIPPED CUII L ^ dJZJ *HJ D A Y \-\ ex?ECTIO JUWVAL DAT! 1 ^ q.if' c TRANSPORTER NO 1 SIGNATURE "Te the btsi el H Y kKMi<ti«9t the o n i m s el the sJiiprntnl t li>ie Kceplcd lor liarissert anlerms with Ihe dtsoplion on iSs maniltst." TRANSPORTER ND. 1 «Hn:u SCXU P. l3 l l i n r> lO 13 DATE RECEIVED llLJ Liil MO DAY TEAR AT THIS PERfORATION yz-zs// 5c- _ = PART B y / k GEN EPA IDS |v ll 0 |9 h3 0 n 6 1 0 IRi';;?ORT'-^IC ' S;GNt:uRE "Icini>y i(iail>ijyr^int»rn:t't4.<?ihorm>itiijilY Witrrd the cuflienil o' !hil i n i o m t n i ' k ^ — ' ^ . f ^ - 7 i -i . '. • • y y ' ' • / / .f/1<. rS )(o. 2 ^z^L ' \ j k A ^ ^ . TRANSPORTER NO 2 SIGNATURE "In iht b t i t ol my knowlidjt ihi camtnii ol i « ^ shifpmcnl I h^ve .ccipicd lor iraniporl conlorms wilhihe desuioiion en this manilesi TRAHSPORTtfi/o. 2 VEHICU 10 NO I ' I 1 I t ) I OATE RECEIVEO I I 1 l _ L J TRA.'JSPOflrrn NO 7S'CNAruPE t eini^y thai I na-/c not lamot'cd •..rftor ffijitnallT alltfcd Ihr Lunlenl, ol Ihn shipment ' I I I I ; L _ l IKJATiiJJJT STGSiC; S" SISrOSAl fACniTY INDICATION 0? ANY DKfESENCtS BETWEEN MANIFEST ANO SHIPMENT OR USTING Of REASONS FOR t n u OiSPOSIIinN Of REJECTED MAIERIAIS HA.MUlitJC H'll'U.'O :5 TRATMCWr ::onACE Ofl O I S P O N S I L U C a i l t S I C W A T U W -Ueon m u x .Aiptction. I ctnity rhat iht contents ol ttiii thipmim conlofm wnh th« dtiuipitononiht] nuntlisi i « t i m ilioie dtNd'iuncni ftontj Oft thn •»!(«" -'• Ci'.t ul c M \r" < •ituitftit.iifiv LJM int EnvKonmrniii GuixiT n m i j lUDOl DOCUMENT H ( y p : < i 3 p fl 301330 H A Z A R D O U S WASTE M A N I F E S T nnciiMEKi NO PR IC W TOI NAM land Chemical f n , , liu:. Mlii/.l (Om) 770-2200 AOCWSS E s t a t e 13n Estutt- Bcthlehefn, St. Cniix, U.S. Vinjin Inlunth IPA o IC |V|I|D|9,n,n,6,5|1 (1 iiuNSPfwnR itl) I T r a i l e r Marine Trunnport Corporation IH'IM (ni)9) 721 1313 sill APimi.sr. I3ln GrantlR, Piu|£to Rico 1 rnnriportr Dia.'. [a\Y)) 7')2-7'.>99 s;ii i.MRt.^S 'loiMi Portuaria, Puerto Nuevo, San Juan, Puerto Rico i K i i r ~ ••,:( l•^Cf i.ii ij'.i•?!»:•'•••• "-citi:' Inland Chemical of P.R. , Inc. i-ll/i:.' . (009) 034-1090 Km. ' ' 1 , Highway SI, Manati, Puerto Pico JP.R,0,9,0.0,6,^4,5 P|R|D,9,0[0,5|2|6,I1 P|R,D|0,9,0|3|9,9,7 n i i i lii.'iM l i ?.•! •.;l IIL-.:..^.|il i - a t l ! M H Uif.lZlO, U l OUl IHE 101llii\.«'.i AS A l T l i ' T U l ! 1 .. _ 1 l-l l lOIAl 01 TW l.'RIT MAMILSI DilCl.'Mi:,! NO IS r R II |C 1° 1^ I J L I'.^-inn ll.S Dui - , !•:•.: .ViVt l o l l l f d f P'I US OOT MA.Uf ;i HASS U l vvmK riam. Lic;uiri 12''ii i I l..„ N i l IIRINIIIT l-.UL-l.4r-J L-Li-Ll Gal CONIAlMRS. ± J Z 1 i T f l TiK LjJiU j _ i JIU t p i HA2 bi U U |L_1;...LJJ_J ; i i 1 1 . . I l . J - I . I i I • 1 • ' .1 ; '. il^lLJiU Ih.JlliJiLl II :...!:'.Jlu V.A". U L L l.l. . J :.-..-» . .• I ; •••f IM-. e.jl tiitytt. •.. 1 -.^l. .*. ;.li- J • • 1 . . I - . . : . ,: .• I . • •• : J . 1 ^ 1 . 1 , - . - .-.-. .M<, •tM • . - r . : . .:;:,*:..!"• t l . . > 1 :• »••» Il .r.in.e.-a.f- - . . = • • ^ I ! •a I U * ; • •! • ir-t-.: * . • , . l - " . . ' • z^m ; . : i l !:Mi : J : . I I : I \l\il lllfll liii! I 'I'ir.iiu ...'nvAi i.Aii Jerome II. Ludwiq ^ \ .Prc;3ident '-T.'T^ S.*?.-' _ H .,-..I<:,...^.i.,....,.,.,.^,_,^.„iii.,,».-,.„., |;f,"--;;' scxu i2i3ninisn |9, | ijZx u[il * ' ' I ' ••0 1 -Ml RAW 1 WrmW i-'Mr.in i iLl^! Li I r.Mi n n .•AHT D i V i I . | D | 9 , 0 | 0 ^ | 1 lO [ y IJ • L dj'a^ L.1..J L_L.: \ - - I . . . . . . I ismc -. m.S • I V : ^ r . - : ! ! [ ''S/kZ 301331 v . - , : ' . u i r • 1 1./ : ' . ' H I ' ' * . i i ' . • : • . » .HirJ r-* ' • • • _ • ' , , , . , _ ^ , _ ^ - . ^ — _ _ .furr r »;• I «. •-.' A O^t •z/. Ih 'kh m ^ H T A; ^ P aVRATOIIM ^ r Ialanc ^ BnAOoxu n**d_«n»-iwt-io t i ' A O I C M A N I F E S T OOCUMJKT NO. aVRATOIKAMf l a l a n d Chemical Co., I n c . P fl IC 05 PNOMI (809) 778-2200 on Aooxu Estate 130, Estate Bethlehem, St. C r o i x , U.S. V i r g i n Islands TUNsmmRao.i T r a i l e r Marine Transport Corporation P1<IINf (809) 721-1313 snt Aoonss lala Grande, Puerto Rico IRANSPORIIR NO.2 Tranaporte Diaz P1IIINI (009) 792-7999 SmAOMCSS Zona Portuaria, Puerto Nuevo, San Juan, Puerto Rico TREATMENT. STORAGE OR , DisnSAi(TSDifAoun Inland Chemical or P.R., Inc. riiUNE (n09) 0 54-1090 Sin AOORESS Km. 5 1 , Highway i 2, M a n a t i , Puerto Rico f MORE THAN TWO TRANSPORTIKS A K TQ K UTUZEO. I U OUT T K (OUOWMS AS AnROPUU " A 0 HO | V | I | D | 9 | 8 ,0,6,5,1 Q, | P | R l O i 9 i a , 0 , 6 , a . 4 , 5 ILU | P | R | D | 9 , f l , 0 , 5 , 2 | 6 , 8 , | P | R | D | 0 | 9 i O , 3 i 9 , 9 , 7 , THIS fORM IS NO- 1 Of i TOTAl Of — ^ — PROPEIl US DOT SHIPPJNG NAME I Toluene RO T W f S S T UAJWEST DOCUMENT NO IS P.R. II iC lO l5 US DOT HAZARD CUiS Flam. L i c u i d UN NUMBER 1294 fORM KT UUANTIIT I'i 7|3|1 J _ L J _ L J L UNI IS Gal CO»IIAiI»RS I |1 I I .J L TiK LJ iPA lu; £011, hJ U u u Q IJ EOS. \YAST liii Li- Lu LL Li- L^ Si iLiAi HANUiir.c tfiSisuciicw iKauoiNG CUNIAWIR lUMPncN ai IUENIIFCAUON ot Aniiiiuiii.M .v/.siis iNcimifii :H simr.a:;; m A .';;i.'jL-..v.r{):.:is;yruRi v.lllc^ so NOT HAVt TO EE MANIiESIEOI CJ Nl RAlOfi i CE Rllf ICATIOri l>«s a te ctnih, tha >he tbcwt T»ai«td main«s ar i eroptilr cijtsilitd tir-i niirH mjikeii jnd labcUtd i i m . . . « i - . i , . : , i i»i.i..« i.., :i..r.p.ii.d.oi xiuromij to IIM appliciblt.rtpulatioru el Iht Otearuntnt ol Tiartspodairtn. U.S EPA and the Connmwtalih ol I' R Tlir wjsir dnnibcd jtic.-e .^-.tp iiirr.4')i.r.(i -t* ii. - ii-.i-.fl:.-.ti ivencd Iht TitauMni. Sioiajeer Disposal I acUtti u n a « d » 4 acttpi ihe shipiitM i l h j / i b a j s want, aidhas j \ J i d | i n i i „ i i u do le I cRiilt ih.i it-- lunKri'iilis n w c o i t u ' i t i i i o i h i l . n i t t i T . r Uawltdpt GEkERATOfTS SIGNA Jerome tf7^Luc>wig TTUNSt^RTlR Nfr-1 SICNAIURE H e UM b t i i el r r biewltd9e the csntars t l the •Aipmeei Ihakf x c i p i c d br Brupon c o n b m i wkh ihe desof lioa ta ;as luriiltsL' imE President OAiE sini-pin I .1,11 M l O l | 8 | 3 i TRANSPORTER NO I T m ^ ^ ^ U | 2 | 3 | 1 | 0 | 5 | 1 | 9 | IIPICIIO ARAYAl OAIE G i l l nEI.rl-.10 I £ L U ICLZi l i VII QAT PART B r.iN EPA V| I [ D | 9 | B | 0 | 6 | 5 | 1 | 0 | TMNSPORHR NO I SIGNATURE 1 ahtrvd Iht cviltnis el Ihii aot W t ^ t t l i v O • auithai>f " • ' ^ v y y ^ ^ y ^ J'y^^o^, TRANSPORTER NO } SIGNATURE l i Ott b u t al n r k m r i t d ^ the c a i n i s t l n t l^ipqnicnl I ha.a acceplad tor trtRs^en cartoms wifit the desstptiort e« ?«s c»*nil*^L'' OAn DEllVtRUl TRANSPORIER NO 2 VlHiat D NO ^ ^ ^ I I I ! I I I I lUNSPORIER NO 2 SIGNATURE 1 canir aa< I Iwri m laagered wtn m a a i r i ^ afl«td Ilia aautnis el this IN TWATUENT STORAGE ORBIS?DSAi F A n m fCCATION Of ANT OJflHNCES BETWEEN MANIfEST ANOSHIRMENI OR USIINC 01 Kl AS11N5 F M ANO DISPOSITION Of REJECTED UAHRUIS 301332 OilE RECEIVED I I ] L-1_J L IRAIMENI STORAGE OR D1S?3NSAI lACJinr SICNAIURI "Uoon r u a .mppciion. I candy that dit o n i i M i ol ihu ih^mtni (onljim with iht descupiioi en that mjii.iit, t i t t e l llioit d'lcrcttancnt neic^ tn Ais term' In cast el imfipffnry or ipij ..-mfilia*«>r (III Ih. |n*"«»imeni,l [Vj»J.r, ^•....l , M I " l i ' i 199? M.MtOUNG , kl d 2 t.iV, l l f •.vill •'4T.fyy....A.Z:z^'- / , i i ( ; j : . : i ' i ; •.»••. j i ^ ^ - c S '•' >ART A: UOCllMfKI NU I- I! IC U6 «NIUT0«NAM« . . _ I s l a n d Chemical C o , , I n c . SIIE AC0MS3 E s t a t e 13Q, Estate Bethlehem, St. C r o i x , U.S. TIlANSMmiXN0.1 T r a i l e r Marine Transport Corporation VtlllM (niv) 7711-22(10 V i n ] i n Islands 1 PHIINI |(,009) 721-1313 I STE AOORESS 1 I s l a Grunde, Puerto Rico TRANSPORTER NQ 2 1 T r a n s p o r t e Diaz riil;M i(fin9 1 SIK AOOMSS Zona P o r t u a r i a , Puerto Nuevo, San J u a n , Puerto Rice TlttATMEJfT. STORAGE OR - „ „ . 1 oiswsAirsoif*cwrr I h l v > d Chemical o f P.R., I n c . .myji')!..... 3 \ I W ) ) 854-1090 sm AOORESS Km. 5 1 , Highway # 2 , M a n a t i , Puerto Rico 11' ^ 11) xo L l \^yA<}h I'-JCin'q'.niOi 1 6,'.,1 U, i i i ' i l U . | ' , l f : U | 9 | 0 | l l , ' . , 2 | 6 | U , ^ | R , D | 0 | 9 , 0 | 3 , 9 | 9 , 7 , 1 » MORE THAN TWO TMKS^OIIIEra A « TO K i n i a a , f U OUT TW f OUOVWC AS AWROfWIE 1 THIS fORM 8 NO. 1 Of A T O T A l O f - i - ^ THEflRSTMAMfESTOOCUUINTlin K P B | 1 | 1 I | | 1 PRflPtRilSOOI SMPHMGIUME 11 T o l u e n e RO us DOT HA2AROCUS3 riara. L i q u i d NUUSEI 1294 _ lORM L Nil QUANTITT I l3 |7 |2 |4 1 I l l l l I I l l l l I I l l l l I I l l l l I I l l l l I 1 ' . n c i i HANUiivmsTRuc'noHSDitiuDisi;CG:;;i^UR£MM?Tioi«ti» loi.'iiiiiCATuwoi AWI.I:.;II.-II v.;.-.:isi"iin;:i 00 NOT HAVE TO BE MANtfESnO) UMIS Cal . - - • r.IWIAlMKS . no LLI'I ITft |TIK| LUIU l l l l 1 1 1 l u i EPA HAJ cpfr bJ 1 1 I -L1 11 Lui 1 LJ l l l l IL,,,I • * . • / 1.1 • , • ; . . 1.1..J L 1 , ll[J 108/ WiSTi | F | 0 .".•.;iwn; ij^jiiutil v.-iitv CI W IU lOfl S CE NTIf ICA1I0>I. Tin a Id ctniir tha n.t ahiKt ear*to aainaa ao propillf cussiWil dir4.iiiiril. •i.»kril .>id UirKrii .^ii..'m i^n^^^^TTT^ld^^ td like i^htaWt irQulaturu el the OrvViuwid ef Trarnpenaioa U.S EPA and ihe Cemmonnetaiih ol I' H Ii-r iiii.nie drsailird .^c... m,.. .. .-sup^d to 'Ur ;i.^r.^u-;n s^.ea !: K Iitainitni. Sierat;t or Otspdsal f a c ^ on and wtU xctpt the ihjpei«« ef h^adous w^itt. and Kai j».4i;i ti-.n'r.i in ao in i ct^iiK ih.j :IIF •... ..^i^i., n irnr jn.: r..irrn:«'-' t t v <.i :., CIWRAIORS S I G N A T U I « W ' ^ ' ) Y V » U . / 7 I /Jerome H. Ludwig (^ iini Preaident IIAII a'liTiii 1RANSP0RUR NO ) SfCNATURE Te the k«st o< en trpite»,i xu eeiinis e< the Oi^ntv I hart accepted lor uans^art csrilorma weft tht desaipi«ii ee i ^ mamiul.*' TRANSPORIlH Nil I VfHiai _4tLiM?L!^ r S ' scxu I2|3|1|0|5|0|3, ijiIllllI ;.!fltvAi llin mn SI r.l p.ln 1£JJLI 1^1?! £ un OAT Q . A ^ Z ^ K ^ y h j / ' y ' t ' " *' '"'S f'IRiiiiiAlii'M y ^ - 3/J^9 PART B CtN ITA ,„. |V|l,D|9,n|0|6,5,1|0,' IfUNSPORTER NO 1 SIC NATURE T emitr I ^ t r i d tht (oniems dl this ihi«iMii. IRANSrORIER NO 2 SIGNATURE Te ihi hesi ol e^ bioiidt^ Die c^timti s( tht ahippeiiri I h m acCKiitd lor trmqen cdxteira rMi the »aa«lr9i at d u Ranfwt." lUNSPORTER NO 2 SIGNATURE 1 tariit t u l I kare u l i m ^ w t l a a m a a e r i ^ aiint* Iht ceoieeit el il»t sfcpwiaB.- . | ! ; ' . | | i ' 1 TRANSPORTER Nil 2 VEHIQE 10 NO I ! I I ! I IRIAIUENT STORAGE BR D1S?0SAI f ACtTTY KOCATXU Of AKT 9TOUCU J lETWlEN UAWI (ST ANIISllirwi NI OR USIINC Dl fll A.lliNS E OR AND DISTOSJllON Of REJECTED VUTIRUIS Z ^ i Z Z \ \W..- 301333 UAIE DEUVlREn LJL) gjgi i Qiit pfcfivtn I J I. I I L WT'SIIT^ ^ "ANniixr. wniibo zb c'ZL TRAIMENT STORAGE OR OlSPONSAl fAOKTT StCNAIURE "U»a> M a * telaediin. Iltiiilf ihei the nnienii oliliiiih«mtfno3nloi>nw<<Kihetaa^iaianlhiitienjleit iitipi ihoai diicitpenoti neiid en lAis I o n ' In c u t ol fmrigtncr ff i p i j inunidult^r tall Iht E/v.iionmmlii Ok«L/T Aoara iCCJ. 72i 1197 l u l l n i r i M U 2f.^.^__J-^..:4ri^ jiir.'.i.v.lM \-i; H -.1 umunttM I aland Che»a. - t ^ - c T ^ OOCUMEjttNO. PR. IC 07 (809) 778-2200 Eatate 13Q , Estate Bethlehem, St. Croix, U.S.Virgin Islands Triilor Marine,Tranaport Corporation PHONE (009) 721-1313 SItifiONU ,, Isla Gr^ide, Puerto Rico IP» 0 NO V|1|D|9|8,0,6,5| |P,R|Di 9,8,0,6,4, I H A N S M M I R M J Transporte Diaz pmiNi (U()9) 792-7999 Slit Aoocn , : , I..,. Zona Portuaria, Puerto Nuevo', San Juan, Puerto Rico P|R|D|9|8|0|5|2|, TRuiMin. SToua OR - | Drtyoau.(Ttci fAOJTr Inland Chemical of P.R., Inc. "^^009) 054-1090 tm*oo«a , • |- . ' Km. 51, Highway. # 2, Manati,:Puerto Rico P,R,0|0,9,0, 3|9,' I MORE TMAN nvO T M N S P O n i J B i K TO S U T l u a , H I OUT TW fOUOWNE AS APfflOPIAIE 1 1 " 1 • THIS t o x B » 0 - - • 0 » * TOTAl » TW f W T WAJgfST >OCUMENI P. R. Li Cl 0 , 7 ffuni us OOT %iaerm HAW t ; «BOT M i l R O C U S IM NIMMR fORM NET QUANtllT UMIS COXIAJNERS M Tm ToT EPA KA2 I Xylene RQ riam. Liquid 1307 3l 3i 2| 0| gal I | 1 T /< _I l l l l -UL I I I I U I I I I I L _ L l l l l J_L 1 1 1 ' -L_L i l 1 ciAi MiicniiMG wsTPvcnCNSINCIUOIHG CONUWEREHWTic* lit. lOiNTtflaiiON ot AnnniMNAi w.xsiis wciuuiuIN SIHPW.'II UI ANONiiAaBoousNAiuM•. 00 NOT HAVE TO K MANffESTlOJ | - CSNiRAT0ITSCERII'CkT)OtJ.T)iusBC»ti>rtf>«Riea6aetUB*daacinaaatpn9tityclanilMl 4 e s u i b t d . i n a k > d a n d l a e « « ( d i d ' i i n p r i i e t r iaie>iienre<uansp«rtai.cnKiu ,0 Ihr «p<ica«it i i i u l a s K s el the O w a n e n i e4 Tiaraptnaie*. U.1 (PA a>d Die CemMratialiS el P K The waste d n o i h t d A n t w n t conii^vd to the Tiampenn nvnel l i i a i m t n i . Siaa^t oi Dopee J f i e * H o « a<d wi« ace w t the i l i r a n e l t a t a d o i a want, and t u t a <aii4 peiiwt te de sa I ceiitt that thi inr^joinqtssueindcancuieiiiebeMi inowttdje • I I • GIWRATOITS SIGNATURE Jerome H, LucVig TlUE President IKANSPORTER NO I SIGNATURE T e m t ten el n r k n a t e ^ Ble caaiaMi el I N .i!4<iiitni lha%r i K i p i t d I a uausencsnlDiira wentht d i s s v i a a eaOBBanilesL" OAIE SHIPHU kULMk^ TTWNSTORURNU I «""^^ SECS O. NO. 19|2|8i2n |9i0i EJPECTEO ARHVAl 0 OAII KICEIVEO I OAT iiAK AI mis .'IHIOIIAIU:N PART B GIN IPA 10» V|I|D)9,8.,0,6|5|1 lIUISPORnjRNO. I SC»(AIUR£Tt»1i^lh*l»at»n«Uie»«td«*»tiaetuih, .Hrtd i>« eontents el ilei - > — — ' • - ' ' IKANSPORIIR NO 2 SCNATURt T » I»a » « el ixj Uiippmtei I iMrt tceaeied la r»«»«1 eoiihrM ««h it^e iNe CMtenci of ihtj atttiteiaaltsi.' IHAHS^ORURNO 2 W H t a i 10 NO 1 I I I I ' ' I iRANsyoRTER a. J saiuien Bni«t ftdii h*e« iKiiad l*e cenitnss i ^1i^- TFEATMENT STORAtE 0 * t X T B t U f f C U r t M O U T T O M 1 ^ (OR « D OtSrOSmON Of RLXCTffl j ^ T l M U ' \ • [ l\ I K T M E l l M M T EST ANO SHIPMENT OR USTING Of REASONS •Ml,i..jl-'i'# i.JilgM Z <M 301334 THATmn! vwttt Uims*i..tJivn ^av.^m--ifmjMmih ai-"^IZt, ' it^tfti^^amtmaa'itfAititMmemiwna^mtakm^lmmmaUwi «>CM tkme t m n a t M a m a a m *m hn.-^ ' -'^^'•-•n.. • O i U DUMPED OAII HECIIVIO L4.J J4U ±1 ^ U r - ' WittM «f u r n t n r y a tp.) knnidvjltfrtxl IM Invr-HinaMi XaMi lead |I0?: 7:i t r t } '• I • I I I C o f / l N T .'IU H A I O U K MEIHflO OAIE RtCli-VtD ^AA P i: FART ,C. ^ (Uirn 771: DOCUMINT fJQ p H IC 08 770-221)11 • j M v a , ' 1,1 I -" I • •,» [ E«tit« 13Q'| Eatite Bethlehem. St. C roix, U.S.Vinjin IslamJ;-. Trailer Marine Trahaport Corporatic TlWJ) 721-1313 BTt lOONSi , ! lala Grande', Puerto Rico IMANSrORTER NO 2 Tranaporte Diaz nii'.ii (iu!M) in-Trj'.i JITt AOOMSS ' ' I 1 ' Zona Portuiatia, Puerto Nuevo, San Juan, Puerto lUim TRIAIWW. n o M W M 1 |- j 1 , oorosAtnai>*a"TT Inland'Chefflical of P.R., Inc. m AOORin 1 , 1 : " i Km. 51.'Highway: t\:2, Hanati,; Puerto Rico PllUfll IU!II (Ofl')) 11 54-109(1 r u n « .THW T W TKMsrainiK M C ro • U T U O I L r u OUT TNE rouowNC AS AAPRUJTA H ' ' ^ - - — Of A TOTAl J -J THE fH«T MANlftSIJ^OCUMlM Ml li ^OOT . HAZARGCUSS IPA H) no Vil|l),9,0,0,r.,5|1 ( PiPiOiVifiiOi fi|4,4^; l'lH|O|9|Q|0|5)2)6iE l't^l"'^'t'-^|0|3|9|9,: THIS f O M B M . ' !• II I |C ,0 .0 J L_L PMfWWDOT j l ) . sumw iuMi i '.'. I Xylene RQ' ii I il!i riam. Liquid UN U I M I l l l rr.iiM 1307 1. N(l .l.iAMlilr 131612I£ _.L.l I U l l l l l l l l .1 U U L . I.I I ' IJ111-. I.WI.'.I S.l 1 111 i..uJ 1 1 1 1 LLI_ ' 1 Irl-l .T!K 1 1, 1 i . , J _ . IPA r';nf Ll 10 WA: lii 1 _ i 1 1 - 1 r i U a i M A N D I i K G l S S T I f j C T i O N S i i a U O W C CONTAINER I I I W r O N M i O £ N I l l i a i u : N n i s|i|.i;::i:;-.i •.V.VWI.'SIM:!!;;:!!! Cl . i i i l - v i . M i . ; A:aji.ii.-.//.h:;CIISNiIUIIt'/»;iK UO NOI KAVl TO K M A W E S T E ^ : !: i! •jjjrjjygif^^(ireSSi5i'n5lMa'«mIt»»7u^^ ll. the ictilcaaa i t i K l a M •* * • •eteruaaM el TitAsponsiaa. I l l EPA and O M Caei>eim<Nih ei I' K llic wiMt dcsoikid i i m n • c c cuuivncd le ihr Ii>n:,penci itatiid Th' t i i a i n t n i S t a a ^ v O i t p e t i t r i E i i i ^ a i a W a d l accept the iKV'aan e f U i a dais w a i t , a i d h i i a.J>.i|i.iin.i m i i e i o l i n n t i 'ii.i iii.. I>«i.ij<v<j<i our . o d i i - i i i i i i H i c t i M i d n . If*wttd9d I • " I I • ' ' I r.lNlRATO»rSSChAIU« i :!llt : i JeroBB H. Luciwiq TlUE iiAir jjnniii President I h ^ ^Tj^^ ^ ^ U ^ 'rJvU tll-iCIEU ARHYAl DATE IliillSPORirR W I SIGKATURE T e Ita k»»l el «ij krawlad^ tfie e o t c n a ol ih« s:itfiiH>i I h » t a.'(fP'ed l a ktrasen cailonra with ih< dcsoyioe at t h i a t n i l i i i . " IIUNSPOflllil Ml : vTiiiQi SECS I9i2|8i2i2i3i 111 KO ' — ' ' OAI! H;i.1l'rtO i LJ-J I I. I L 1 ll.VH.M I'iS • y - - i : : \ . PART B : I I I A i:ii: : iV|I|Dl9|0|Q|6|5)1 |0 -.•S^'^IIfRNO I SGNAIWn Ji,.t4 Ihe ctniK.ls el ttu lh>aai t ••' I • lllAhSJ-ORUR NQ J SeiUI^.-llihljeWldi., ^,^f...,n\ktf.Ktiataatairma^Jataai0mwaki>n I al Oe IRANSyURIERNO ? S ) O a T U « n A j i i c i r t the o r t i w i el I iMAtuiKT STORAGE OR o a r a « I OR tJtO DISriiSTXM Of KJICTU IRANSPURtill Ml VlhlUl 10 NO M M II.MI iiii.vimii I 'jAif laciivin L J U I, I •.' I 2h usr lissaU; I t p a |CT>MtNNWMESIAK Bii Hp a. W'^'l^ nsiiirwuiimusiwcof iiu'infc 301335 ^Ar^ U T ^ ' KANOIIflG UtlKW t 3 i OAIE L. HiliE -1.J r.io J 4 t 4r i J L . i : C u v i ; ; ' •::. P :l • Appendix H May 17, 1983 RCRA Inspection Form \VVORK\24231\02\WORKPLAN.REP HARDING LAWSON ASSOCIATES ^0133^ -±.>. 6^^— ^ s RCRA INSPECTION FORM I a . Report Prepared For: Generator Transporter HVJM (TSD) F a c i l i t y Copy of Report Sent t o t h e F a c i l i t y Z'w k 7 IZZJ C J F a c i l i t y Information Name! Address EPA iD#: 1/rp 7 ? r o / 5 7 M S ^ - Date of I n s p e c t i o n : t ' ^ . " ' ^ ^ ' / ^ '4^ A * ^ ^ ^ f- 4 ^ -d, P a r t i c i o a t i n a Personnel *A Personne. 511 KZ%efryZu^../.^^c,^f',. Co.cy.s. Dyy^ ^ D ^ Z S ^ Facility Personnel: y ^ ^ . y^/Qm^Z.^ u . y / ^ y ' ^ ^ A • Report Prepared by (Name) : /1 . \ / k C^"/^ /r Agency: C^6ykp//)^y^^/D ^ ^ / J ^ L Telephone Numb«r: ^ K l Z ^ - T ^ - ^ ' ^ ^T^O Jefom« H. Ludwvj. Ph.D. fratiaant JslafKl Chtfnical Co., lf>c P.O. Bo« 6733 OiriitMfMlad, St. C'Oix U.S. Virqin I t l j n d i 00820 (8091 778-2200 V\ AUc B. Smith Plant Erigirve*< liland Ch«mic«l Co.. Inc. P O . Boee733 C h r i i t x n i l t d . St. C'On U.S. V i r f i n i m r y j i 00120 IBOfi) 778-2200 s.be.«.«y c( eej?t§x ''^o rcZ^ykaJlfi/U. V V t v M . N . J. 07470 ( 2 0 1 I 6 W - * 1 0 0 SubdidU fY Of BgJUjLliX CaiiM Knolli. NJ 07927 (201) &40.a700 301337 -C- l3 there reason to believe that the facility has hazardous waste on- site? a. If yes, what leads you to believe it is hazardous waste? Check appropriate boxes: / / Company admits that its waste is hazardous during the inspec- tion. / / Company admitted the waste is hazardous in its RCRA notifica- tion and/or Part A Permit Application. / / The waste material is listed in the 'regulations as a hazardous waste from a non-specific source (261.31). / /. The waste material is listed in the regulations' as a hazardous waste from a specific source (261.32). / / The material or product is listed in the regulations as a dis- carded commercial chemical product (261.33). / / Testing has shown characteristics of ignitability, corrosivity, reactivity or extraction procedure toxicity, or has revealed hazardous constituents (please attach analysis report). / / Company is unsure but there is reason to believe that waste materials are hazardous. (Explain). 301338 1 V -A- Susaarr of Flncdinsza Ui o tjJ Ui vo ^:?^ Facility Deacripcion and Operaeiong nZ<Z^r^ J rI^^:.y.:[P..ySTQrr^ / f \ U f . . . r ' - ^ ^ e A 4 r h r c . - ^ / C^y^^^yOy.^^^^y> ^ ^ - X s A c ^ J ^ ~ ^ u - ^ c : ^ ^ JT^^-r-^ 'Ml.^Z/k^/r^^l^ ^ T ^ . / ^ f., g<>-^;^^ y k ^ y i -3- (^^•^Wf vlcles chac result in ctie generacion 6Z lUitH-S^Ms^ ( & . ^ ^ . - r ± Ic^jfe.-::^ -^ y A. k^^y^—y<L. (i HOT FOR RELEASE TO CDMP.\trf. PROTECTED INFROHAIION -C- Sueaaarv, Conclugiona ^nci Racotanendations Z. /^^^r- JAAy^-tkkZ~lT7Zt——77nP. \ •, NOT FOR RELE.\SE TO COMP.\NY. PROTECTED INFROHAIION - C - Susxjar'i', Concluaiona and Reconmendations . ^^>M '-X'--^-----<f^,^^* f i ^ Z yyZt^^-kg cLmty/ , ^ - ( ^ ^ y i ^ lXaJ_£. 9hrA * - . .^-••.—,-<:.-.T.^. Pump" ' ^ re ISO 100 KVA Cer.cr.Ttor Dryer Building' , , Cooling Tower U.S.V.l. Guard IIQU.SC "'•^^^-*^l Reverse Osmosis Chlorine ^ ^ ,.,^Stnrai;c 350 KVA Cone r.l tor Glaas Plant • Stainless Steel Plant • Hot Air y . Drying Roon ^itainlcsa Steel Storaso Tanks :!•"••; i^P-£S>«Hng i, •'•''' • Tower>><."- ' : Utility Building I . - .;..•'S iiJ.:""; " ": Paved Parkin;;/Rond Arna M- unch Uocra — roiaing Roora Storage Shipping; : '•••' Aro.T Finishing Area Office AriM Ljbi)rJCory Arra Warehouse Area Truck Dock -Truck Dock I • I I .• v l i •• I i I k, I ' l IJccure Storage Area :-. I 301342 , , , .11 •Oato Tank Fam . y ' '-•.. y •^ ^/^ . . y v^ v.: f Drum' Storage Aren • J Ll M •': I -1- GENERATOR INSPECTION CHEC.XLIST \ 40 CTR 262 Subpart A ~ General YES }K) N/A 262.H - Hasardoua Waaea Determination 1) Old t.ha generator test Its waste to deterraln* whether It Is hazardous? Is the waste hazardous? 2) Is the generator detenalning thht Its waste erhihlts a hazardous waste characteristic(s) based on its knowledge of the naterial(s) or processes used? 40 CFR 262 Subpart B - The Manifest - - K Has hazardous waste b««n shipped off-site since November 19, 19607 If yes, approxiaately how many shipoents, off-site, have bi«en aade and describe the approximate size of an average shipment made on a nonthly basis.. If fa- cility i>Na saAlI quantity generator, please" explain. Llity ^»^* saAlI quantity generator, please explain. ^^ . - / ^ / 262.21 Does each Rajiifett (or representative sample] have the following information? Please circle the aissinq elements. - a manifest docoaent nuaUser? - t h e generators name, mailing address, telephone nuaber and I.D. Nusiber? - the transporters naste and EPA I.D. Nuaber? - the naae, address -and EPA I.O. Number of the desig- nated facility? -. a description of the wastes (DOT) - the total quantity of each hazardous waste by units of weight or volume, and the type and number of con- tainers as loaded into or onto the transport vehicle? - a certification that the materials are properly classified, described, paclcage, marXed and labeled, and are In proper condittion for transportation under regulations of the DOT and EPA? (obtain a copy of the incomplete manifests] vaa&.3i.n a t^upy oc ci 5/7-^ CUJJ-5^ f^^jk k 301343 I • ^ 40 CFR 252 - Subpart 0 - Recordkeeping and Reoortlno YES NO N/A 262.40 Has the generatoraaintalned facility records since November 19, 19807 (manifest, exception report and waste analysis) 262.42 Has the generator received signed copies (frcm the TSD facility) of all the manifests for waste shipped off-site more than 35 days ago? If not, have Exception Reports been submitted to EPA covering any of these shipments made aore than 45 days ago? 40 CFR 262 - Subpart C - Pretransportation Require- ments 262.30 Before transporting or offering hazardous -33 waste for transportion off-site does the generator: 1) Pac)cage the waste in accordance with appli- cable DOT regulations (i.e., 49 CFR Parts 173, 178 ( 179) 2) Label each package according to DOT i i . . ^ . ; 49 CFR 172) 3) Mark each package according to DOT (i.c-., CFR 172) 4) Mark each container of 110 gallons or less with the words "HAZARDOUS WASTE - FEDERAL LAW PROHIBITS I.MPROPER DISPOSAL. IF FOUND, CONTACT THE NEAREST POLICE OR PUBLIC SAFETY AUTHORITY OR THE U.S. EPA', and Include the generators naae, address and manifest docu- ment nuaber. (i.e., 49 CFR 172.304) 262.34 Accumulation Time 1] How ia waste accumulated on-site? / / Containers / 7 Tanks / / SurfaoB iitpsundnents (carplete SV*5" checJclist) / 7 Piles (cotpleto SS*T ciiecklist) 2) I s w a s t e accumulated for more than 90 d a y s ? If y e s , complete SVfl-lF c h e c k l i s t . 3) Is each c o n t a i n e r c l e a r l y d a t e d wit.h each p e r i o d of a c c u m u l a t i o n so as to be v i s i b l e for i n s p e c t i o n ? 4) Is eac.i c o n t a i n e r c r tank marked or l a b e l e d w i t h the words "HAZARDOUS WASTE" or i n c o n - p i i a n c e with t h e DOT l a b e l i n g r e q u i r e m e n t s ? STOP HERE IF-THE HAZARDOUS WASTE .MGT FACILITY (TSD) CHECKLIST IS FILLED CUT 301344 -<fflkj<:s t e^kzi •,-3- i / i y C ^ ^ s S L r ^ 262.34 - Short Ter:n Accumulation Standards (For generators who accumulate waste i.i tanks or containers for 90 days or less) . 40 CFR 265 - Suboart I Containers YES NO N/A 265.170 - What type of containers are used for storage. Describe the size, type and quantity and nature of waste (e.g., 12 fifty-five gallon druau of waste acetone). 265.171 - Do the containers appear to be in good condi- tion, not in danger of leaking? If not, please describe the type, condition and nuaber of leaking or corroded containers. Be detailed and specific. 265.172 - Axe hazardous waste stored in containers made of compatible awiterials? . If not, please explain. 265.173(a) - Ara all containers closed except those in use? • i^ . , 265.173(b) - Do containers appear to be properly opened, handled or stored in a manner which will minimize the risk of the container ruptu- ring or leaking? 265.174 - Is tha storage area inspected at least weekly? 265.176 - Are containers holding ignltable and reactive waste located at least 50 feet (15 meters) away frca the facility's property line? 265.177 - Ara incompatible wastes stored separate froa each other? 40 CFR 265 Subpart J - Tanks 265.190 1) What ara t.ha approximate nuaiber and size of tanks containing hazardous waste? 2) Identify the waste traatad/storad in each tank. 265.192 - General Operating Requirements 1) Are the tanks maintained so that there is no evidence of past, present, or risk of futura leaks? If no, please explain 301345 l i ) • b YES SO N/A 2) Are there leaking tanks? 3) Ara all hazardous wastes or treataent rea- ' gents being placed in tanks compatible with the tank material so that there is not dan- ger of ruptures, corrosion, leaks or other failures? 4) Do uncovered tanks hava at least 2 feet of freeboard or an adequate containment struc- ture? 5) If waste is continuously fed into a tank, is the tank equipped with a means to stop the inflow from the tank? e.g. by^ss system to a sandby tank 265.194 - Inspections 1) Is the tahk(s) inspected each operating day for: a) discharge control equipment b) aonitoring equipment ; c) laval of waste in tan)c 2) Ara tha tanks and surrounding areas (e.g., dike) inspected weekly for laaks, cncro- sion or other failures? 265.198 3) Ara there underground tanks? If yas, how many and can they be entered for inspection? - Are ignltable or reactive wastes stored in a manner which protects there from a source of ignition or reaction? If no, please explain. 265.199 - Does it appear that incompatible wastes are being stored separate from each other? 265.16 - Personnel Training 1) Have facility personnel successfully com- pleted a program of classroom instruction or on-the-job training within 6 months of having been employed? If ve:^, have facility personnel taken part in an annual review of training? ' • 301346 \ \ YES ao N/A 2) Is there written documentation of the following: -job t i t l e for each position at the f a c i l i t y r e l a t e d to hazardous waste management and the naae of the esiployee f i l l i n g each job? -type and aaount of t r a i n i n g to be given to personnel in jobs related to hazardous wasra management? - a c t u a l training or experience received by personnel? 3) Are training records kept on a l l employees for a t l e a s t 3 years? 40 CFR 265 - Suboart C - Preparedness and Prevention - 265.32 Does the f a c i l i t y cooply with preparedness and prevention raquiraaents including" maintaining: -an i n t e r n a l coaoiunlcations or:alann system? -a telephone or other device to siJmaon emergency assistance from local a u t h o r i t i e s ? - p o r t a b l e fira aquipswnt? -water at adequate volume and pressure to supply watar bose streams, foam producing equipaent, e t c . 265.33 Is equipeaent tasted and maintained? 265.34 Is t h e r e inmediate access to comraunications or alara systems during handling of hazardous waste? 265.35 Adequate aisle spaca? If no, please explain storage pattern. In your opinion, do the types of waste on-site require all of the above procedures, or are some not needed: Explain. 301347 -6- ai YES NO N/A 40 CFR 26S - Suboart D - Contingency Plan and Emergency Procedures Does the facility have a written contingency plan for emergency procedures designed to deal wtch fires, explosions or any unplanned release of ha- zardous waste? 1) Does tha plan describe arrangements made with tha local authorities? 2) Has the contingency plan been submitted to the local authorities? 3) Does tha plan list naaes, addresses and phone nuabers of Emergency Coordinators? 4) Does the plan have a list of what emer- gency aquipiant is'available? 5) Is there a provision for evacuating, fa- cility personnel? ' 6) Was there an awergency coordinator present or on cal:at -f- 301348 Appendix I Waste Classification Analyses and Disposal Profiles \WORK\24231\02\WORKPLAN.REP HARDING LAWSON ASSOCIATES 301349 Laboratories, Inc. Subsidiary ol Schering AG, West Germany REPORT APPROVAL FORM TITLE OF REPORT: Analysis of Material from Bulk Storage Tanks 17, #8, #9 and 113, Island Chemical Company, St. Croix, Vircir. Isla.nc£ DEPARTMENT/TESTING FACILITY: M e d i c i n a l C h e m i s t r y STUDY NUMBER(S): DATE OF REPORT: November 1 0 , 19S2 REPORT PREPARED BY: D a n i e l S z e t o SUBMITTED BY: APPROVED BY. APPROVED BY: RECEIVED BY •2. •y^^^-^ -^zt^o^r y/. cy^' Study Director/Mortitor . ^ ; y / / ' / A ^ ^ ^ Departmeni.^Di rector. Corji'.' V i c ^ President, R t D ..yik^</H Vice P r e s i d e n t , R ^ ( T D Admin. BERLEX REPORT NUMBER: 5^/6 7 DATE: ^ ' / / / r ' / i A ' ^ DAT: /-' DATE : c . < I I DAT ,. ////c/^2^ REPORT DISTRIBUTION: R t. D ADMINISTRATION/ARCHIVE ( O r i g i n a l ) / M e d i c i n a l C h e m i s t r y (Org ina t i n g Deot.) ^ ' Operations Department _3 Island Chemical Co., I n c . 301350 770 East Hanover Avenue, Cedar Knotls. New Jersey 07927 (201) 540-8700 Telex 13635'! BERLEX LABORATORIES INC RESEARCH REPORT jY) CHEMISTRY Q PHARMACOLOGY [n PHARMACEUTICAL DEVELOP, DEPT. REPORT NO. DATE: BERLEX REPORT NO. fp/6 7 PAGE OF 1 PAGES 5 CHARACTERISTIC BIOLOGICAL EFFEC1 TITLE OF REPORT: Analysis of Material from Bulk Storage Tanks #7, 18, 19 and 113, Island Chemical Company, St. Croix, Virgin Islands KEYWORDS (3 t o 5) : Storage Tank Analysis. Island Chemical, chemical composition PROTOCOL NO. GROUP/SECTION: Medicinal Chemistry Department Analytical Chemistry Section STUDIES WERE CONDUCTED FROM: TO: 10/25/82 11/02/82 EXPERIMENTS CONDUCTED BY: J. Traina, E. Nisperos, M. Johnson and D. Szetc AUTHOR 5IGNATURE: y^AzAy SECTION HEAD SIGNATURE: -zyf^^ COMPOUNDS STUDIED CK NO.: GENERIC NAME: Toluene, xylene, p-phenetidine, 9-fluor- enone FOR.".JLATIDf.' NO. PURPOSE OF STUDY: To determine the composition and identify the contents of material from bulk storage tanks in St. Croix. 301351 SUM.HARY AND SIGNIFICANCE DEPT. REPORT NO, PAGE OF 2 PAGES 5 Material from bulk storage tanks in St. Croix were fractionated by simple vacuum distillations. Fractions and residues were identified by NMR and IR. The results are as follows: Tank «7 Tank S8 Tank US Tank ^13 xylene mixture p-phenetidine toluene 9-fluorenone p-phenetidine p-phenetidine ca. 14% ca. 80% c c . 29% c a . 50% ca. 95% ca. 95% -2- 301352 Analysis of Material from Bulk Storage Tanks #7, S8, S9 and S13, Island Chemical Company, St. Croix, Virgin Islands All four samples Tank S7, 18, #9 and #13 were received in 10 ml screw cap vials. These samples were analyzed as described below and the results are summarized in Ta'z-ls.- :, I I and I I I . Tank 17 This sample was analyzed by semi-micro distillation. Two volatile fractions collected at the ranges of 75-100°C and 100''C-120°C were both identified by NMR and IR as mixed xylene. The residue was also identified by NMR and IR as p-phenetidine. Tank #8 This sample was analyzed by semi-micro distillation. Two volatile fractions collected at the ranges of 75-100''C and 100-120''C were both identified by NMR and IR as toluene. The residue was analyzed by NMR and IR. The spectral data indicated that the residue was mainly composed of 9-fluorenone. Tank #9 No volatile fraction distilled from the sample when heated. The sample was fractionated by semi-micro vacuum distillation. Practically 1 fraction was obtained by vacuum distillation. The fraction and a small amount of material left in the distilling flask were identified by NMR and IR as p-phenetidine. Tank #13 No volatile fraction distilled from the sample when heated. The sample was fractionated by semi-micro vacuu.Ti distillation. Practically 1 fraction was obtained by vacuum distillation-. The fraction and a small amount of material left in the distilling flask were identified as ;-pheneticine by NMR and IR. -3- 301353 Tcbl-: 1: Comoosition and P h v s i c a l Aooearance of Samoles Composition #7 xylene mixture ca. 14% p-phenetidine ca. 80%* Tanks »8 #9 113 toluene ca. 39% 9-fluorenone ca. 50%* p-phenetidine p-phenetidine ca. 95%* cz'. 95%* Physical Appearance slightly heavy; black liquid slightly heavy; black liquid slightly heavy; black liquid slightly heavy; black licuid Total Nitrogen Content (by Galbraith Lab.) 7.56% 1 . 8 3 % 9 . 4 9 % 9.54% T o t a l C h l o r i n e C o n t e n t (by k>raith Lab.) m C-...orinated hydrocarbon content (by Beilstein test) 0 . 0 8 8 % Not d e t e c t a b l e (N.D.) 0.081% N.D. 0.24% N . D . 0.24% • E s t i m a t e d by NMR. - 4 - 301354 Identification and Pronerties of Volatiles Tanks # 17 #8 #9 =1 Boiling Point Mixed xylenes Toluene volatile Lit. 137-140°C Lit. 110°C Flash point xylene Toluene Lit. 17°C(o-) Lit. 4.4°C Lit. 25°C(/n-&p-) Identification NMR, IR NMR, IR Identification and Prooerties of Non-Volatiies Tanks l l ii il =13 Boiling point p-phenetidine 9-fluorenone p-phenetidine :-pheneticir non-volatile Lit. 250''C Lit. 342°C 95°C (O.OSmmHc) 95-105°C (760mmHg) Lit. 250''C (0.05.T.mHc) (760mmHg) Lit. 250°C (7 60mm.Hg) I d e n t i f i c a t i o n NMR, IR NMR, IR NMR, IR NM?., I." - 5 - 301355 - t t^wao 19 COPELAND RD. DENVILLE! NEW JERSEY 07834 (201)366-6256 August 15, 1985 Mr. Austin Moorehead Department of Conservation and Cultural Affairs Division of Natural Resources Management 14F Building 111 Water Gut Homes Christiansted, St. Croir, U.S.V.l. 00820 Dear Mr. Moorehead: As per our telephone conversation on August 9/ Enviro-Sciences, Inc. is requesting perinission to dispose- of contaminated materials on St. Croix. The materials are on the Island Chemical Company site (now known as Virgin Island Chemical Company) and have been collected and stored in drums" or will be collected for disposal. The collection and clean up of these materials has been described previously in documents submitted to your office. The location and description of materials are as follows: Location Type Amount Major Contaminents 1) Drain line 2) Dryer (soil collected from a spill) Soil Soil Water 18, 55 gal. drums 14, 55 gal. drums 2, 55 gal. drums Toluene, see Data Sheets 1 & 2 Toluene, see Data Sheets 3-5 The Data Sheets are inclusive of a four week drying period. Note that toluene concentrations decreased from 4000 ppm to 1.5 ppm during this time interval. Drying continued for an additional week after the last sampling period. 3) Process Pit Sludge 2,000 gals. Toluene, zinc, see Data Sheets 7-11 4) Process Pit Water 6,-000 gals.- Data Sheets 12-17 301356 We would appreciate your timely review of this request and a determination as to the disposal location of each item listed above. I will contact you next week as to your progress. If you have any question, please call me collect at 919/499-5182. Very truly yours, ENVIRO-SCIENCES,. INC. ^ . ^ z ^ ^ "^ ' (7 Alan L. Kyles, PhD. Vice President AK/po (AK-85225) cc: Mr. Greg Rhymers Dept. Conservation & Cultural Affairs P.O. Box 4399 St. Thomas, D.S.V.I. 00801 301357 INDUSTRIAL CORROSION MANAGErvlENT INCORPORATED IIS2 RQUre 10. RANDOLPH. NEW JERSEY 07869 •201-584-03:0 CLIENT: ENVIRO SCIENCES, INC SAMPLE SOURCE: ICC (BERLEIQ, PROJECT Data Sheet I NJDEP Certified Drinking Wacer/ Wascewacer Lahoratory ID i^l^llS REPORT DATE: August 15.1985 LAB II 42882 SAMPLE ID: Drain Line ^1 SAMPLE DATE: 6/7/85 SAMPLED BY: A. Kvles SOIL SAMPLE LABORATORY ANALYSIS REPORT AT LAB DATE: 6/1S/85 Identification of Black Soil; Parameter Benzene Toluene Ethylbenzene M-Xylene Q,P-Xylene Resul 0- c 10 233 0. 0. 0. 25 33 27 Sample has "Toluene like" or solvent odor. Lf^'rCS'0'-'N ?£^\KS R.T. 6.89 ac 40 mg/kg R.T.30.81 -c 2 mg/kg All results reported in mg/kg. We thank you for this opportunity to serve you- If you have any quescions, please do noc hesitate co call. INDUSTRIAL CORROSION MANAGEMENT, V.:C. m. jmg • 1 Edwin Tichenor Vice President n = L e s s Than 301358 Ui o l-» Ui Ul vo f a ] 1 ^ INDUSTRIAL if CLIENT; ENVIRO SCIENCE - ICC (Berlex) ^Jlil CORROSION MANAGEMENT INCORPORATED SOIL SAMPLE NJDEP Certlticci Urinking Waier/w<i:>iuw<iLcr Laboratory (0 #14116 REPORT DATE; July 31. 1985 LAB #_12M1 •SAMPLE. ID; Drain Line 112 •SAMPLE DATE: 6/7/85 SAMPLED BY: A. Kylea VOLATILE ORGANICS BY PURGE AND TRAP By CC BTX/HEADSPACE AT LAB DATE; 6/18/85 CHLOROMETHANE • BROMOMETHANE • VINYL CHLORIDE • CHLOROETHANE • METHYLENE CHLORIDE ACETONE - • 1,1-DICHLOROETHYLENE - 1,1-DICHLOROETHANE **- t-l,2-DICHLOROETHYLENE CHLOROFORM 1,2-DICHLOROETHANE t-BUTYL METHYL ETHER -• 1,1,1-TRICHLOROETHANE - CARBON TETRACHLORIDE - BROMODICHLOROMETHANE - I.2-61CHLOROPROPANE — Compounds detected In parts per million (milligrams/kilograms) dry weight basis X X 1,240 *rC-l,3-DICHL0R0PR0PENE 't-l,3-DICHLOROPROPENE ~ TCE (TRICHLOROETHYLENE) X rl,I,2-TRICHLOROETHANE 'DIBROMOCHLOROMETHANE '"" ~ 68 10 BENZENE • DIISOPROPYL ETHER 2-CHLOROETHYLVINYL ETHER • BROMOFORM I,1,2,2-TETRACHLOROETHANE PCE (TETRACHLOROETHYLENE - TOLUENE CHLOROBENZENE ETHYLBENZENE M-XYLENE • *f O-XYLENE 5.600 ^Compounds co-elute (could be either material). LT-Less Than, GT-Greater Than dwb-Dry Weight Basis. X-Not Detected P-XYLENE AATetrahydrofuran ( Phosgene also elute at this point. Numerical results are calculated for I,]-Dlchloroethane only. For the above listed Volatile Pollutants, nothing detected at a sensitivity level of:_ _Unknown peaks detected (retention tIme,estImated amount): Xylenes 18; ]0 unknown hydrocarbon peaka ranging from 2 to 10 mR/kg. _J NOTE;Compound Identification is based upon retention time matches with specific known standards. Confirmation of analysis using GC/MS Is required to positively Identify any material and/or amount detected. I NDUSIiUAt:i:ORR0S ION^ win TTcheKor, Vice PresJ^rrrt-- n rt rti r t N) o Ui o Pi irtuubiHlAU CORROSION MANAGEMEhfT INCORPORATED t u ; ROUIE lO.IWMOOLtN. WW jCMSfYOrui MI-U4.0U0 CLIENT; ENVIRO SCIENCE ICC (Berlex) SOIL SAMPLE • '- 1 i • » • ''• HJDEP Certified Drinking Water/Wast ,^^«r Laboratory 10 ||i«li6 REPORT DATE:_ LAB # 42889 July 31.1985 SAMPLE ID: Dryer •SAMPLE DATE; 6/14/85 SAMPLED BY: A. Kylea VOLATILE ORGANICS BY PURGE AND TRAP By GC BTX/HEADSPACE _AT LAB DATE; 6/18/85 CHLOROMETHANE • BROMOMETHANE • VINYL CHLORIDE • CHLOROETHANE • HETHYLENE CHLORIDE ACETONE - — 1,1-DICHLOROETHYLENE - 1,1-DICHLOROETHANE **- t-I, 2-DICHLOROETHYLENE CHLOROFORM 1,2-DICHLOROETHANE t-BUTYL METHYL ETHER - 1,1,1-TRICHLOROETHANE - CARBON TETRACHLORIDE — BROMODICHLOROMETHANE -- 1,2-DICHLOROPROPANE — Compounds detected In parts per million (milligrams/kilograms) dry weight basis. TCE (TRICHLOROETHYLENE) X jkfC-l,3-DICHLOROPROPENE 't-l.3-DICHLOROPROPENE M 1,1,2-TRiCHLOROETHANE X 4.0 340 4.2 '^Compounds co-elute (could be either material). LT-Less Than, GT-Greater Than dwb-Dry Weight Basis. X-Not Detected 'DIBROMOCHLOROMETHANE BENZENE DIISOPROPYL ETHER 2-CHLOROETHYLVINYL ETHER BROMOFORM 1,1,2,2-TETRACHLOROETHANE PCE (TETRACHLOROETHYLENE TOLUENE CHLOROBENZENE ETHYLBENZENE - ' M-XYLENE - *rO-XYLENE P-XYLEME **Tetrahydrofuran ( Phosgene also elute at this point. Numerical results are calculated for I,1-DlchIoroethane only. X • X X 6.6 X X X X X 4.000 X 16.1 17.7 15.1 For the above listed Volatile Pollutants, nothing detected at a sensitivity level of; 1 mg/kR dwb. Unknown peaks detected (retention tIme,estImated amount): NOTE:Compound identification Is based upon retention time matches with specific known standards. Confirmation of analysis using GC/MS Is required to positively Identify any material and/or amount detected. INDUSJ win Tlchefior, Vice Presf^trrt-- rf It rt JDUSTRIAL CORROSION MANAGEMENT L ' J I I I INCORPORATED 111} ROOK 10. tUtUDCLfii. WW JCRSEr 07Mt 20l-Si4.O]}0 NJDEP Certified Drinking Water/Wastewatf Laboratory ID #1M16 REPORT DATE:_ LAB a 43747 August 15.1985 CLIENT; EKVIRO SCIENCES,INC. - ICC (BERLEX) PROJECT SAMPLE DATE; 7/1/85 SAMPLED BY: Enviro Sciences SAMPLE ID: Dryer AT LAB DATE; VOLATILE ORGANICS BY PURGE AND TRAP GAS CHROMATOGRAPHY/HEADSPACE 7/11/85 Compounds detected In parts per million (mi 11tgrams/kllograms) dry weight basis CHLOROMETHANE- BROMOMETHANE VINYL CHLORIDE CHLOROETHANE HETHYLENE CHLORIDE — - ACETONE ],1-DICHLOROETHYLENE - 1,1-DICHLOROETHANE ** • t-l,2-DICHLOROETHYLENE X X CHLOROFORM • 1 ,2-DICHLOROETHANE - - t-BUTYL METHYL ETHER - 1 ,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE - BROMODICHLOROMETHANE - 1,2-DICHLOROPROPANE c-r,-3-DICHLOROPR0PENE t-l,3-DICHL0R0PR0PENE"' TCE (TRICHLOROETHYLENE) - - 1,1,2-TRICHLOROETHANE DIBROMOCHLOROMETHANE BENZENE DIISOPROPYL ETHER 2-CHLOROETHYLVINYL ETHER - BROMOFORM 1,1,2,2-TETRACHLOROETHANE • PCE ( TETRACHLOROETHYLENE) TOLUENE - - CHLOROBENZENE • ETHYLBEHZENE — • X SLM '••Compounds co-elute (could be either material). LT-Less Than dwb-Dry Weight Basis. GT-Greater Than X-Not Detected **Tetrahydrofuran & Phosgene also elute at this point. Numerical results are caluclated for 1 ,1-DichIorocthane only. o M Ui a\ For the above listed Volatile Pollutants, nothing detected at a sensitivity level of mg/kg dwb. rt (t rt JJ Unknown peaks detected (retention time, estimated amount) numerous other liydrocnrbon peaks, 0.02 to 0.1 mg/kg NOTE; Compound Identification Is based upon, retentIon time matches with specific known standards. Confirmation of analysis using GC/HS Is required to positively £y/ identify any material and/or amount detected. INDUSTRIAL CORROSION MGMT.,INC, iwin Tichenor, Vice President I i'i I INDUSTRIAL JORROSION MANAGEMENT INCORPORATED iisiMxm IC. RAMoam. wwjdisfYorui toi-iu-oao NJDEP Certified Drinking Water/Wastewat Laboratory ID tl\h\\(> REPORT DATE;_ LAB # 43752 August 15.1985 CLIENT; ENVIRO SCIENCES,INC. - ICC (BERLEX) PROJECT SAMPLE ID: Dryer SAMPLE DATE: 7/1/85 SAMPLED BY: Enviro Sciences AT LAB DATE: 7/11/85 VOLATILE ORGANICS BY PURGE AND TRAP GAS CHROMATOGRAPHY/HEADSPACE Compounds detected In parts per million (milligrams/kilograms) dry weight basis CHLOROMETHANE—- BROMOMETHANE VINYL CHLORIDE • CHLOROETHANE • HETHYLENE CHLORIDE — • ACETONE • 1,1-DICHLOROETHYLENE - 1,1-DICHLOROETHANE ** • t-I,2-DICHLOROETHYLENE CHLOROFORM X X JLH 1,2-DICHLOROPROPANE - — ^rc-1,3-DICHLOROPROPENE 't-l ,3-DICHLOROPROPENE" TCE (TRICHLOROETHYLENE) . , 1,1,2-TRICHLOROETHANE 'DIBROMOCHLOROMETHANE " " X 1,2-DICHLOROETHANE —• t-BUTYL METHYL ETHER • 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE - BROMODICHLOROMETHANE - X X BENZENE DIISOPROPYL ETHER — 2-CHLOROETHYLVINYL ETHER - BROMOFORM 1,1,2,2-TETRACHLOROETHANE PCE ( TETRACHLOROETHYLENE) TOLUENE • CHLOROBENZENE • ETHYLBENZENE •Ixi '•'Compounds co-elute (could be either material). LT-Less Than dwb-Dry Weight Basis. GT-Greater Than X-Not Detected **Tetrahydrofuran i Phosgene also elute at this point. Numerical results are caluclated for 1,1-Dlchloroethane only. u> o oji X For the above listed Volatile Pollutants, nothing detected at a sensitivity level of mg/kg dwb. Unknown peaks detected (retention time, estimated amount) 34.07 3 15 mg/kg NOTE: Compound Identification Is based upon, retentIon time matches with specific known standards. Conflrmatlori of analysis using GC/HS Is required to positively ^ j / identify any material and/or amount detected. INDUSTRIAL CORROSION HGHT.,INC, win Tichenor, Vice President n (u rt> rt * I iU \i ^ ^ i i I, I .•JDUSTRIAL CORROSION MANAGEMENT L'J I J I INCORPORATED CL I ENT; ENVIRO SCIENCES. INC. - ICC (BERLEX) PROJECT SAMPLE DATE; 7/17/R5 SAMPLED BY; Enviro Sciences NJDEP Certified Drinking Water/Wastewat Laboratory ID #11(116 REPORT DATE: LAB i 44629 August 15.1985 SAMPLE ID; Dryer AT LAB DATE: VOLATILE ORGANICS BY PURGE AND TRAP GAS CHROMATOGRAPHY / HEADSPACE 7/25/85 Compounds detected in parts per million (milligrams/kilograms) dry weight basis CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE • METHYLENE CHLORIDE —-• ACETONE • 1,l-DiCHLOROETHYLENE - 1,1-DICHLOROETHANE ** • t-l,2-DICHLOROETHYLENE CHLOROFORM 1,2-DICHLOROETHANE t-BUTYL METHYL ETHER - 1,1,1-TRICHLOROETHANE - CARBON-TETRACHLORIDE — BROMODICHLOROMETHANE — X X 1,2-DICHLOROPROPANE — - X^ ^rC-1,3-DICHLOROPROPENE 't-i,3-DICHLOROPROPENE — TCE (TRICHLOROETHYLENE) X 1.2 ^r1,1,2-TRICHLOROETHANE 'DIBROHOCHLOROMETHANE — ~ X X BENZENE - DIISOPROPYL ETHER 2-CHLOROETHYLVINYL ETHER - BROMOFORM 1,1,2,2-TETRACHLOROETHANE PCE ( TETRACHLOROETHYLENE) TOLUENE CHLOROBENZENE • ETHYLBENZENE • 0.07 0.36 '•'Compounds co-elute (could be either material). LT-Less Than dwb-Dry Weight Basis. GT-Greater Than X-Not Detected **Tetrahydrofuran & Phosgene also elute at this point. Numerical results are caluclated for 1,1-Oichloroethane only. Ui o Ui o^ CO For the above listed Volatile Pollutants, nothing detected at a sensitivity level of mg/kg dwb. Unknown peaks detected (retention time, estimated amount) niimeroug other hydrocarbon peaks 0.01 to 1 mp/kg NOTE: Compound Identification is based upon retention time matches with specific known standards. Confirmation of analysis using GC/MS is required to positively £j/ identify any material and/or amount detected. INDUSTRIAL CORROSION MGMT.,INC rt Itl f t ^ fn Tichenor, Vice President INDUSTRIAL CORROSION sI^L MANAGEMENT INCORPORATED 1152 ROUTE 10. RANOOtPH. NEW JERSEY 07869 201-5^-0330 CL I E N T : EKVIRO S C I E N C E S , NJDEP C e r t i f i e d Drinking Water/ Wastewater Laboratory ID # m i l 6 REPORT DATE: Julv 3 1 , 198.S LAB i 42886 & 42887~C0MP0SITE SAMPLE SOURCE:. SAMPLE DATE: 6/14/85 ICC (Berlex) SAMPLED BY: A.Kyles AT LAB DATE; 6/18/85 PRIORITY POLLUTANT VOLATILE ORGANICS + AO by GC/HS + 15 PEAKS Parameter a c r o l e i n * a c r y l o n i t r i l e * benzene bromoform carbon t e t r a c h l o r i d e chlorobenzene chlorodibromomethane chlorethane 2-chloroethylvlnyl e t h e r chloroform — dIchlorobromomethane - - - • 1,l-dlch1oroethane 1,2-dlchloroethane 1,1-dIchloroethylene Result X Parameter Result X 22SL X 1,2-dichloropropane 1,3-dichloropropylene ethylbenzene methyl bromide methyl chloride methylene chloride 1,1 ,2.,2-tetrachloroethane - tetrachloroethylene toluene — • : 1,2-trans-dlchloro«ithylene 1 , 1 , 1 - t r i c h l o r o e t h a n e 1 , 1 , 2 - t r i c h l o r o e t h a n e t r i c h l o r o e t h y l e n e vinyl chloride Results reported in mg/lcg (ppn), dry weight basis. •Detection Lii»it LT-Less than X=Not detected 100 ppm OTHER COMPOUNDS DETECTED APPROXIMATE CONCENTRATIONS 125 1.560 X benzyl acetate 22 1430 l-chloro-2-iaethyl benzene 40 chloromethyl benzene ET/jmg INDUSTRIAL CORROSION MANAGEMENT, INC. dwlnVTichen&r- v-- / EdwlnVTichent Vice President 301364 l1 , , J I INDUSTRIAL y ,! I CORROSION P l ' j MANAGEMENT 9 1 I I INCORPORATED OUTE 10. RAMDOIPH, NEW JERSEY 07869 201 •5ft4-0330 11£NT; ENVIRO SCIENCE NJDEP Certified Drinking Water/ Wastewater Laboratory ID #1^116 •il REPORT DATFrJuly 3 1 . 1985 LAB I 42886 & 42887 COMPOSITE SOIL SAliPLE AMPLE SOURCE: ICC (Berlex) AMPLE DATE:fi/14/8S SAMPLED BY: A. Kvles .AT LAB DATF.; 6/18/8S PESTICIDE S PCB EXTRACTABLES PRIORITY POLLUTANTS -K AO • by GC/MS arameter Result . Idrin • LT 2- -BHC - — LT 2 -BHC — - LT 2 -BHC - - LT 2 -BHC ^- LT 2 hlordane LT 12 ,i»'-DDD — LT 3 ,^-DDE LT 3 ODX LT 3 'drln LT 3 iiaosulfan I ' LT 3 ndosulfan II LT 3 ndosulfan Sulfate .- — LT 3 ndrin LT 3 :ndrin Aldehyde LT 3 eptachlor LT 3 eptachlor Epoxide LT 3 oxaphene • LT 12 'CB-10'16 LT 45 'CB-1221 ^ - LT 45 CB-1232 — - T.T 45 'C8-12'»2 - — T.T 45 'CB-I2A8 - T.T 45 'CB-1254 - - - T.T 45 'CB-1260 - LT 45 vll r e s u l t s are reported In mg/kg (ppm), dry weight b a s i s . INDUSTRIAL CORROSION M G M T . , I N C . EdwiH^ T i c n ^ o r ^ - 7» iT^mg Vi-ce P r e s i d e n t /(jJZ) r - L e s s Than <-Not D e t e c t e d 3 0 1 3 6 5 3 U •J u Data Sheet 11 ^1 INDUSTRIAL CORROSION SOIL SAMPLE MANAGEMENT INCORPORATED NJDEP Certified Drinking Water Wjsiewater Laboratory 10 lUllS REPORT DATE: j u W 31. 1985 LAB » 42886 & 42887 Coouosite US? ROUll IU. RANOOiPH. N£W XRSIT 0;il69 ?QI ^ 4 0 l\(l CLIENT ENVIRO SCIENCES SAMPLE SOURCE: ICC (Berlex) SAMPLE DATE: 6/14/85 <;&MPI cn BY: A. Kvles AT LAB DATE:6/18/85 -'"'^^ PRIORITY POLLUTANTS-f 40 TOXIC POLLUTANTS: Metals, Cyanide and Total Phenols PARAMETER Total Antimony - Total Arsenic — Total Beryllium Total Cadmium -- Total Chromium - Total Copper — Total Lead ;-• Total Mercury — Total Nickel — Total Selenium • Total Silver -- Total Thai 1ium Total Zinc RESULT T,T 118 40.0 LT 2.87 22.8 592 327s 688 2.73 134. LT 1^08 LT 7^48 LT 66.2 3,594 Total Cyanide Total Phenol • A4.44 ^ 0 1 A M results are reported in mg/kg (ppm)',' dry weight basis.. We thank you for this opportunity to serve you. If you have any questions, please do not hesitate to call. Very truly yours, INDUSTRIAL CORROSION MGMT.,1HC. ET/jm<3 LT-Less Than X-Not Detected Edwin" TicheWor Vice President 301366 aw # INDUSTRIAL CORROSION MANAGEMENT INCORPORATED NJDEP Certified Drinking Water/ Wastewater Laboratory ID HlkWS REPORT DATE: August 15.1985 LAB # 44418 1152 ROUTE 10. RANDOLPH. NEW JERSEY 07869 201-584-0330 CLIENT: ENVIRO SCIENCES. INC. SAMPLE SOURCE: ICC (BERLEX) PROJECT SAMPLE ID; St.Cro-tx SAMPLE DATE: -W«^WHW»- SAMPLED BY: Al Kyles .AT LAB DATF- 7/22/85 WATER Parameter PRIORITY POLLUTANT VOLATILE ORGANICS by GC/MS acrolein* acryloni t r i l e * benzene : bromoform carbon tetrachloride chlorobenzene chlorodibromomethane chlorethane 2-chloroethylvinyl ether chloroform dichlorobromomethane I ,l-dichloroethane 1,2-dlchloroethane 1 ,1-dichloroethylene Result X 0.04 _X X X X X Parameter Result X X X X X X 1 ,2-dichloropropane I,3-dichloropropylene ethylbenzene methyl bromide methyl chloride methylene chloride 1,1,2,2-tetrachloroethane - tetrachloroethylene toluene ^ 1,2-trans-dichloroethylene I,1,1-trichloroethane I,1,2-trichloroethane trichloroethylene vinyl chloride Results reported in mg/l (ppm). Detection limit 0.001 mg/l (ppm). •Detection Limit: Q.l mz/1 Q.3S JL ET/jmg INDUSTRIAL CORROSION MGMT.,INC. Edw i n T i c h e n o r V i c e P r e s i den t LT=Less Than X=Not Detected //"A 'yyyr /z^-^ 301367 INDUSTRIAL CORROSION MANAGEMENT INCORPORATED . ' - o c r ^ci t i 1 . CO Ul I nn, I ng wa cer/Was t e w a t e r (^(^ L a b o r a t o r y ID #li»116 Data Sheet 13 REPORT DATE: August 15.1985 LAB if ^^^18 1152 ROUTE 10, RANOOLPH. NEW JERSEY 07869 201-544.0330 CL I FNT: FNVTT^n «;rTFNrES. TNC. ICC(BERLEX) SAMPLE SOURCE:_ SAMPLE DATF; TinVnnT.nw SAMPLED BY: St. Croix Al Kvles AT LAB DATE: /yy/a'atyyr'ji'S'^ WATER PESTICIDE & PCB EXTRACTABLES PRIORITY POLLUTANTS bv GC/HS Parameter Result Aldrin • LT 0.01 a-BHC LT 0.01 b-BHC LT 0.01 d-BHC LT 0.01 g-BHC - - — - :- LT 0.01 Chlordane • LT 0.02 A,if'-DDD 7 LT 0.01 1»,I»'-0DE — LT.O.-Ol ^,if'-DDT LT 0.01 Dieldrin — r '• LT 0.01 Endosulfan I LT 0.01 Endosulfan 11 • LT 0.01 Endosulfan Sulfate : LT 0.01 Endrin LT 0.01 Endrin Aldehyde LT 0.01 Heptachl or LT 0.01 Heptachlor Epoxide LT 0.01 Toxaphene LT 0.02 PCB-1016 LT 0.01 PCS-1221 LT 0.01 PCB-1 232 r LT 0.01 PCB-12A2 LT 0.01 PCB-12^8 LT 0.01 PCB-1 25A LT 0.01 PCB-1260 LT 0.01 All r e s u l t s reported in mg/l (ppm). INDUSTRIAL CJUUlgSI /-o ,-• Edwin Tichenor ET/jmg Vice President LT=Less than X=Not detected 7/22/85 M G M T . , I N C 301368 m hUSTRIAL 'RROSION MAHAGEMEFfT INCXtRPORATED NJDEP Certified Drinking Water/Wastewater Laboratory ID #IA116 n i l R O i n i IO.IUMX)LrH.N£WJEJa{r07Mt »n-S»4-01)0 REPORT DATE:. LAB # August 15,1985 44418 CLIENTL ENVIRO SCIENCES, INC, SAMPLE S O U R C E L - .SAMPLE DATE: -^xnkxuiUfi^ ICC (BERLEX) PROJECT /yjZ'^yyi^jir^ SAMPLED BY: Al BASE/NEUTRAL Parameter Result acenaphthene X acenaphthylene X anthracene X benzidine X benzo(a)anthracene X ben2o(a)pyrene X 3,^i-benzof luoranthene X ben2o(ghl)perylene X ben2o(k)fluoranthene X bls(2-chloroethoxy)methane • X bls(2-chloroethyl)ether X bis(2-chlorolsopropyl)ether X bis(2rethylhexyl)phthalate X ^i-bromophenyl phenyl ether X butylbenzyl phthalate X 2-chloronaphthalene X 4-chlorophenyl phenyl ether — X chrysene X dIben2o(a,h)anthracene X 1 ,2-dichlorobenzene X I ,3-dlchlorobenzene X to'I,^-dichlorobenzene X <=> 3,3-dichlorobenzldlne -- - X ^ None of the above Priority Pollutonts detected vo **Other compounds see Addendum I LT-Less Than X-Not Detected FT/Imo SAMPLE ID; ST. Croix Kylea AT LAB DATE; 7/22/65 EXTRACTABLES PRIORITY POLLUTANTS t?Y GC/MS Parameter diethyl.phthalate dimethyl phthalate dl-n-butyl phthalate ; 2,^l-dini trotoluene ; -- 2,6-dinitrotoluene dl-n-octyl phthalate I,2-diphenylhydra2ine (as azobenzene) fluoranthene . fluorene hexachlorobenzene hexachlorobutadiene hexachlorocyclopentadiene hexachloroethane indeno(l,2,3-cd)pyrene Isophorone naphthalene nitrobenzene N-nitrosodimethy lamine N-nItrosodi-n-propyI amine N-nltrosodiphenyl amine phenanthrene pyrene 1,2,'•-trichlorobenzene at a sensitivity level of 0.03,mg/l (ppm) INDUSTRIAL CORROSION MAIjAGEHENT, INC. ' ••'' C " c T " : ^y. Edwin Tichenor Vice President Result rt (0 (t) rt ^i'l i NJDEP Certified Drinking Water/ Wastewater Laboratory ID #14116 REPORT DATE: Augiist 15,1985 LAB # 44418 CLIENT: ENVIRO SCIENCES, INC. SAMPLE SOURCE: ICC (Berlex) SAMPLE ID: St. Croix SAMPLE DATE: uatereirtr SAMPLED BY:_ y9A^yy9/'J-' Al. Kvles AT LAB DATE: 1I22I%5 BASE/NEUTRAL EXTRACTABLES PRIORITY POLLUTANTS ADDENDUM I OTHER COMPOUNDS DETECTED by GC/MS Parameter benzaldehyde Result 3.0 chloromethyl benzene benzene methanol — — phenyl acetate diphenyl methane — — 0.3 24.0 26.0 0.4 0.4 l-l'-[oxybis(methylene]bis benzene All results are reported in mg/l (ppm). We thank you for this opportunity to serve you. If you have any questions, please do not hesitate to call. INDUSTRIAL CORROSION MANAGEMENT, INC. ET/jmg end. LT=Less Than Edwin TicK'enor Vice President 3 0 1 3 7 0 ^m. # INDUSTRIAL CORROSION MANAGEMENT INCORPORATED 1152 ROOTE 10. RAHOOLPH. NEW JERSEY 07869 201-584-0330 NJDEP Certified Drinking Water/ Wastewater Laboratory ID #U116 REPORT DATE: August 15.1985 LAB # 44418 CLIENT: ENVIRO SCIENCES. INC. SAMPLE SOURCE ICC (BERLEX) PROJECT ST. Croix SAMPLE DATE: uukiiuwu' SAMPLED BY: Al Kvles /9j:ycy/9fr^ AT LAB DATE: ACID EXTRACTABLES PRIORITY POLLUTANTS bv GC/HS 7(171^^ WATER Ji Parameter 2-chlorophenol 2-nitrophenol phenol Result 2,4-dimethyIphenol 2,'l-dlchlorophenol 2,'»,6-trichlorophenol --• pentachlorophenol 2,^-dinitrophenol 4 , 6 - d I n I t r o - o - c r e s o l '•-nitrophenol 4-chloro-3 methyl phenol X X X None of the above P r i o r i t y P o l l u t a n t s detected a t a s e n s i t i v i t y l e v e l of 0.01 mg/l (p OTHER PEAKS DETECTED: benzoic a c i d (§ 3 mg/l INDUSTRIAL CORROSION MGMT.,INC ET:jmg LT=Less Than X»Not Detected Edw i n T i cheiio r V i c e p r e s i d e n t *** 3 0 1 3 7 1 ^ Data Sheet 17 Cfc T i l I I INDUSTRIAL NJDEP Certified Drinking Water U . I j CORROSION Wostewater Laboratory ID ^1M16 . P I I MANAGEMENT REPORT DATE: A,,^,,,^ is.igRs L'J I I 1 INCORPORATED ^AB » 44418 IS? ROUli 10. RANOOlPH. N[W JERSEY 07»69 201 58< O.IV) r-LIFNT; ENVIRO SCIENCES INC. SAMPLE SOURCE: ICC (BERLEX) PROJECT SAMPLE ID: St. Croix SAMPLE DATE: .unlma<rf=* <;AHPI Fn BY: Al Kyles . AT LAB DATE: 7/22/85 PRIORITY POLLUTANTS WATER SAMPLE TOXIC POLLUTANTS: Metals, Cyanide and Total Phenols PARAMETER RESULT Total Antimony LT 0.016 Total Arsenic LT fa.005 Total Beryllium • LT &.013 Total Cadmium '-— 0.003 Total Chromium '• 0.027 Total Copper ; 0.153 Total Lead ---. n.O'n Total Mercury n.001 Z Total Nickel — 0.080 Total Selenium '• T.T 0.005 Total Silver- 0.008 Total Thallium --' o.o29 Total Zinc •_ 4.85 Total Cyanide 0.053 Total Phenol 0.161 All results are reported In mg/l (ppm). We thank you for this opportunity to serve you. If you have any questions, please do not hesitate to call. Very truly yours, INDUSTRIAL CORROSION MGMT.,INC. Edwin Tichenor ET/jm<3 Vice President LT=Less Than X=Not Detected 301372 CHAIN OP CUSTODY RECORD 19 COPtLANO RO.. DENVIUi NCW JERSET 07O4 Inatallation: ICC (Berlex) Survey No .: V a B tz c to 2 Station Location Analysis S a a p l e r s : ( S i g n a t u r e ) Date Time Sample Type Comp Gra b BT Ui V c u-l ..-I o <0 u • c o o 2 U Drain Line A / A ^ S ' I Toluene 6/8/85 2 3 4 5 6 ^y2tSv'>- Identify the contents of^the black soil sample.] Uboratory Pit ^ 5 cP<F3 Pyridiw 6/14/85 Laboratory Pit-duplicate ^ ^ « ^ V VOA k ^ 6/14/85 Time limit may have expired, if so do not run.] Z?57?3 Pit-duplicate (liquid) Priority Pollutantb 6/14/85 ^,3,Pf-i.\ combine and 4iAJl Pit-Interface(liquid/slidgeTN ^un 6/14/85 Pit-sludge "K priority ''^ pollutants 6/14/85 /P^^o X One container has a white lump, segregate it and anc lyze for quinid .ne.] U Drver i k k ^ ' ^^ ^^^^^ Toluene Relinquished by: (Sign.) 6/14/85 Relinquished by: (Sign.) Received JyJLy A (Sign.) Date/Time Received by: (Sign.) Date/Time Relinquished by: (Sign.) Received by: (Sign.) Relinquished by:/-6Sign.) Dispatched by: (Sl/^n.) Date/Time Rec'd by Laboratory for field analysis ( S i g n . ) Date/Time y vytfs /:x!/.r Date/Tim^[Rec'd for Laboratory by: Date/Time Method of Shipment: Express Air Freight O 301373 LAB NO. 42885 Pit duplicate (liquid) Priority Pollutants +40 (Process Pit) Samples not analyzed because sample volume too small. 301374 cnwio • foaKu VK. CHAIN OP CUSTODY RECORD I i O0«I>«0 TO.. DCNVIUX N€W JEBSEY 0T»4 I n s t a l l a t i o n : /CC (^/f&€yftA Survey No.: a a nj C tn a y > ^ ^ Station Location ^ /y^ytf/^ /fia^ifr-e-' ykt;^ Tzr /^JZ fe^-"^ <,yy!y/iyj/.ry ^ a ^- >l/. Samplers: (Signature) date Time Sample Type Liomp .( Cirao /iyycy A/iyti.y y^.-f^yayrj / / ^ ^ ^ /J^y.y \ BT u V a o m u • c o o V / y ^ ^ ky/^'-. 'tL .-y-. -^ 2 ^/^yA^ yv-iztiT*.<.. /yt^y \ / Relinquished by: (Sign.) y^:^,y^rzyy-y Relinquished (^y: (Sign.) Received by: (Sign.) Date/Time HhLLzZzzdzi^yii=zir^''y-' y'^l'"^ '^''^• Relinquished by: ^Stgn.) Relinquished by: (Sign.) Dispatched by: (Sign.) Received/by: (Sign.) Date/Time Received by: (Sign.) Date/Time Rec'd by Laboratory for field analyais (Sign.) Date/Time Date/Time Method of Ship|aen£_^ ky yA , • - j ^ 5 / Rec'd for Laboratory by: Date/Time 301375 •WHO tM KttncMS WKm CHAII OF CUSTODY RBCOID ItCOraAMO n o . O e M U X NCW J ^ K T 07B« Instaiiacion: Survsy No.: ZZiiL. Ol • « ci j - ^ 4 6 3 1 S t a t i o n Location Saaplars: ( S i f n a t u r a ) 7)/ev<^ ( T a ' / ^ ^ yA^-S'/S / y k ' J ^ m y f ^ J AA^zyyy^, Data "T:^—7 / ^ Vy/eyry /ali^/Sf^yX T ^ ^ ^ 7^^ru^ '^ ^SM^Zy ZA'' "IT y/ \ y\yar' /=^4t^/3 yyi^rrc y^y=y^yi-.^ r^yTT/^cxy ^/ /VSU) <^^y^£^. /Ce./i^frPiyzj) y < ^ c y y h ^ \ Rfl^inquishad by:, (Si^n.) - • Ra/linquiahad by: (Signj/) Ralinquiahad by: (Sign.) Ralinquiahad by: (Sign.) ^ < ^ 1 Racalvad by: (Sign.) Racalvad by: flSign.) Data/Tiaa Data/Tima Racalvad by: (Sign.) pata/Tiaa Dispatched by: (Sign.) Data/Tiaa Rac'd by Laboratory for field analyaia (Sign.) Rac'd for Laboratory by: Data/Tiaa Data/Tiaa Method of Shipaent: cSyZ^y<iaA <kiU^ /^Zi^^i^ 301376 m CHAIl OF CUSTODY RBCOID It cofCUMO w}< ocMvaii. amn Installation: y ^ ^ ^ ^ Survay No.: a • <« d Vi Station Locatioa Saaplars: (SIgnatura) Data T/ Til Saapla Typ< UoapTF^TrTB" —a- a o m w • a o o o z rj:t.2> fSi./ I ^ ^gd-^ /y^t^^ya»^, i y ^ ^ ( ^ l ^ a Z 2 ^ ^^<»a^, 7y^4^i^'Aa/. T / I ^ • ^ ( f y ^ <^-'^^A^ >r \ ^ \ ^ R ^ i n o u i s h e d by: ( S i g n . ) Racalvad by: ( S i g n . ) RacaiVad by :(jT5ign. ) D a t a / T i a a Raiinquishad by: ( S i g n . ) Relinquished by: ( S i g n . ) Data/Tiaa Received by: (Sign.) Data/Tiaa Ralinquiahad by: (Sign.) Diapatched by: (Sign.) Data/Tiaa Rac'd by Laboratory for f i e l d a n a l y a i s (Sign.) Daca/Tlaa Rac'd for Laboratory by: Data/Tiaa Method of Shipaant: ( Z ^ C ^ a ^ j * ^ / 4 l ^ k ^ 301377 CHAII OF CUSTODY RECORD It COfOMO MX. OOMUI. MCW JCMCr ortM Installation: _72r(L ! ^ ^ 1 ^ u-yy. Survay No.: Saaplars: ( S I g n a t u r a ) '•4^/g 03 Station Location Data /^/f/^/Ay yi^^-^z^/^^/zz -f <^o y^^<^:^i*^ y ^ ^ /^yL^ckk Tiaa Saapla Typa (Joap.t'<>rao /^jS^y/^ '^t2-^o T Relinquished by: (Sign.) u fi 144 tr^ O « • fl o o 2 U ^ c ^ Relinquiahad by: (Sign.) / Kaiinquishad by: (Sign.) Racalvad by: (Sign.) (ZZi. L • — L J ej>y—U^.-~yit..y-L. Data/Tiaa l i s 2 J - I S Received by: ciSign.) Data/Tiaa Received by: (Sign.) Data/Tiaa Ralinquiahad by: (Sign.) Diapatched by: (Sign.) Data/Tiaa Rac'd by Laboratory for f i e l d a n a l y s i s ( S i g n . ) Data/Tiaa Rac'd for Laboratory [Data/Tiaa b y : Method of S h i p a a n t : ^ ' y ^ (£yeyy^ ^^^y^r^ 301378 - • * » £nv«io 19 COPELAND RD.. DENVILLE. NEW JERSEY 07834 (201) 365-5256 iOBKiSVK, 32 EAST 39 STREET. NEW YORK. NEW YORK 10016 (212) 697-9450 November 15, 1985 Mr. Carl Becnell G. A. Becnell, Customs Brokers 150 Marine S t r e e t Lake Charles, Louisiana 70601 Dear Mr. Becnell: As per a telephone request from Mr. Frank Curtis of Berlex L a b o r a t o r i e s , I n c . , I am sending the enclosed laboratory a n a l y t i c a l sheets which d e s c r i b e the chemical contents of hazardous wastes which o r i g i n a t e d in St. Croix, USVI. I t i s my understanding t h a t U. S. Customs w i l l not r e l e a s e .the material for shippment to Chemical Waste Management, I n c . i n Alabama xmtil they know the contents of the shippment. •• Below i s a l i s t i n g of data sheets and to which drums they are a p p l i c a b l e . DATA SHEETS 1 and 2 3 - 6 7 - 11 1 2 - 1 7 * CHEM. WASTE MANIFEST NO. ALA D 48604 ALA E 68803 ALA D 48603 ALA D 48602 ALA E 68804 MATERIAL Soil Soil Sludge Water Pieces of Metal Dnrni.s NO. OF DRUMS 24 15 45 94 14 * Pieces of washed drums which contained materials in items 1 and 2 above, I t r u s t . t h a t this information will suffice for release of the material. If you have any questions, contact me at 919/499-5182 or 201/366-6256. Very truly yours, Alan L. Kyles, 4hD. Vice President enclosures 301379 S & W WASTE, INC. 15 JACOBUSAVE. . SOUTH KEARNY. NJ. 07032. (201)344-4004 GENERATORS WASTE MATERIAL PROFILE SHEET APPROVAL COOE TECHNICIAL REP. INITIALS . GENERAL INFORMATION ZZ^l'-lo-'^l JENERATOR NAME ~/^SC'5>ff£ C Z ^ f f f r f / i ^ C ^ / Z ^ i " 7 ^ 7 ? r > ^ GENERATOR EPA LD. NO. '^O 9 P a ^ r y a ( ? r - ADDRESS, [Sx:^ ^'7'PS Cyy^.ys/7?^jrz£ _ Jr-. /Z-^yr-^. tyJ^Zf C c f Z o TECHNICIAL CONTACT ^ ' ^ • ^ ^ / Z ^ t U ^ k c ^ t - ' y / ^ /g.A'CiMy) /ASTE NAME /4y^^i^^ ^U^tZ Zpyyo yTy^j:, TITLE. V ^ PHONE ^<r.<^dy<g'-^-^"C" PROCESS GENERATING WASTE. zy—r—*^— B. PHYSICAL CHARACTERISTICS OF WASTE PHYSICAL STATE @ 7 0 " F J ° ° ° " yyfr<.,y3 Z SOLID V-'Q'J'O I C / L C SEMI-SOLID D POWDER «t. LIOUID %H20 COLOR r'ORGANIC ^INORGANIC C CHLORINATED ORGANIC BTU VALUE PER G A L . "b C L _ BS4W_ Ob ASH. % S LAYERS a MULTI LAYERED G BI-LAYERED ^ S I N G L E PHASED TOC. COO. % S C L : y y m ^ PH: DO-2 D 2.1-4 C 4.1-6.9 C 7 • 7.1-10 G 10.1-12.5 G>12.5 G E X A C T _ • N/A v.-t^*^ SPECIFIC GRAVITY I <-8 : J-.9 : .5-.95 : .95-1.0 : 1.0-1.1 C 1.1-1.24 C 1.25-1.4 G 1.5-1.7 C>1.7 G EXACT.£L 7S/9 • FUVSH • POINT GCF) GCC QOC CEXACT. Q<90 • <100 a 100-140 • 140-200 n <2oo VISCCSiTY (Centipoise) g l - l O O G 100-1000 C 1000-10000 G >iaooo C EXACT C. CHEMICALCOMPOSITION(MUSTTOTALioo%) % -rr- D. Ag As Ba Cd Cf Cu OTHER. METALS V. C TOTAL ZZE. yjfi AJy. y/z G EP TOX Hg Ni Pb Se 2n Te y F. HAZARDOUS CHARACTERISTICS: TOXICITY RATINGS INHALATION DERMAL ORAI C EXPLOSIVE G WATER REACTIVE C MSDS ATTACHED NFPA RATING yt/c^c' q. PYROPHORIC G SHOCK SENSITIVE G. MANIFEST INFORMATION PROPER DOT SHIPPING NAME / ^ " ^ ^ ^ i t ^ u J . y y y ^ Z ^ yZi^^ey.r, / t / g ' : DOT HAZARD CLASS _ UN/NA NO. y ' Z ^ (^yeyu-^ ^yy^ EPA/STATE WASTE TYPE _ EPA/STATE HAZARD CODE. A)€kp/ ydAdL XJA. y^y/i yy/l y//> JilAL E. G G G G G G G G G OTHER COMPONENTS PCB'S* PESTICIDES/HERBICIDES* CYANIDE OR CYANIDE PRODUCING . SULFIDE OR SULFIDE PRODUCING . PHENOLICS J RADIOACTIVE INFECTIOUS "1 y/yd '2K. y/yf y y y ! y < ^ y/i^ ELEMENTAL METALS*_ OTHER. ,^M^ •ATTACHED DISCLAIMERS MUST BE SIGNED k M H. SHIPPING INFORMATION G BULK LIQUID G BULK SOLID >g DRUMS COTrlE SHIPPING FREQUENCY: nUANTlTY / Y.'=.r\. PER. I. SPECIAL HANDLING INFORMATION/COMMENTS: I HEREBY CERTIFY THAT ALL INFORMATIl ARE REPRESENTATIVE OF THE WASTE. SUBMrrTHD ABOVE AND ALL ATTACHMENTS ARE COMPLETE ANO ACCURAT DATE TITLE SAMPLES SUBMITTED 301380 GENERATOR'S SIGNATURE Polychlorinated Biphenyl (PCB) Warranty This disclaimer is to all persons who generate and dispose of chemical waste. The terms PCB and . ;B'S are used in this disclaimer to refer to any chemical substances and combinations of substan- Jjes that contain 50 ppm orgreater of PCB's as defined in 40 CFR 761.3 (s), including any byproduct, in a process which contains less than 50 ppm PCB because of any dilution; again, these latter shali be included as PCB and PCB's. Substances that are regulated by this rule include, but are not limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and other chemical substances or combination of substances, including impurities and byproducts. It is unlawful for S&W Waste, Inc. to receive PCB's. Any generator and/or transporter who knowingly or willfully Ships PCB's to our facility will be subject to civil penalties or criminal prosecution. hereby warral^ts that materials transferred by it to S&W Waste, Inc. for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl (PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby agrees to idemnify and hold S&W Waste, Inc. harmless from any costs, damages or other liability resulting from the breach of this warranty. DATED; BY:. WITNESS: Herbicide/Pesticide Warranty l^i^^rNtv^ CorrA(r Pr^ roX^tfershy warrants that material transferred by it to S&W Waste, Inc. for transportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level greater than 0.001% when measured in eSch container or vessel transferred to S&W Waste, Inc., and hereby agrees to indemnify and hold S&W Waste, Inc. harmless from any costs, damages or other liability resulting from the breach of this warranty. Z£S=L?^Z^ Qj^^r^iCRp.^ GSl ~iOC. nAT.n. 3 - 3 ^ ^ RV. VcUk iVAyy^ ^e.c\tii^.j WITNESS; yy^2fy<-'^•^:P\ y \ yyy^tZ^- Aluminum and Reactive Metal Warranty k - ^ z y N ^ OyZ^^i(^':'^CQ:)^^Z>zZ./L hereby warrants that material offered to S&W Waste, Inc. for transportation, treatment and/or disposal does not contain elemental aluminum or reactive metal paste, powderor pigment and hereby agrees to idemnify andholdS&WWaste, Inc. harmless ^rom any costs, damages, or other liability resulting from breach of this warmnty. ~ . v ^ xsLf^Ai^ ctt^t^MusL co,y^k ..... '^-^'-^^ ..-.k^rkAJkL-^ <^^yjCy WITNESS; 301381 TABLE 1.4 30870-0705 EITVISOSCIEHCSS Sajnple Identification: ALAB 64570 FC3 Isomer Result .-E • .U FC3 1016 <0.20 PC3 1221 <0.20 PCB 1232 PCB 1242 PCB 1248 PCB 1254 PCB 1260 <0.20 <0. <0. <0, <0 20 ,20 .20 .20 301382 YWC. INC. • 200 Mcnrce Turnpike • Monroe. Connecticut 06468 • (203) 261-4458 "INDUSTRIAL '^- . CORROSION .MANAGEMENT INCORPORATED NJDEP,.Cercified Dri.-.kins Vacar/ ...Wascewacer LabqricWy..IDi^ 14116 '•.REPORT :,DATE; j ^ ^ j ^ T T ^ _/-7_c 5 5 1152 ROurt 10. RANOOLPH. NfiV JERSEY 07869 iOl-584-0330 CLIENT: E>TVIRO SCIENCES -.. Island Cheaical Proiecc SAMPLE SOURCE: SamDle ')3' SAMPLE DATE: February g5.--19S6 SAMPLED BY: \_ Kvles _AT LAB ..DATE: ^ria-zr. 7. 193 6 LABORATORY ANALYSIS REPORT Parameter **Pecroleuzi Evdrocarfaon — Result 220"' ' tug./lXppia) We chank you for chis opporrunicy to'ser-/e you.' If you have any questio.r.s-',''please. do noc hesicaca co call. Sincerely, •-•- INDUSTRIAL-.CORROSION .MAKAGIiHENT',-, 1NC%' " yky lichard S. /Levijie Presiden RSL: dlh LT=iess Chan **This cesc employs arialycical mechodology which can-give false posicive readings. •SimpI scaced, chis cesc is .measuring che Carbon-Hydrogen linkaga ia...-.c.tganic molkcuies.;- Wiile Pecroleum Hydrocarbons mosc cercainly possess chis link, a-^nujabar of organic molecules ^(H'.imus, Lignin ecc.) noc considered pecroleum based, also p_os.sess it as wellv Therefora in order Co more correcdy confirm a high reading, iC is suggesced chac a GG run ba additionally performed. The above Tocal Pecroleum Hydrocarbon con•cehc^acion•^ffl!ay'•^_QOC^•reJ5Ee•sen cRf-r hydrocarbon value'as ."ihdicaced by an incerference at-.;.i745 cm-1.'' 301383 / } t ^ ^ 6 ¥1/0 INDUSTRIAL CORROSION MANAGEMENT INCORPORATED NJDEP Carcified Drinking Wacer/Vastavace: Laboracory IDi^ 14116 REPORT DATE; April 14. 1986 _ ^ ^ LAB H 52956 1152 ROUTE 10. RANOOLPH, NEW JERSEY 07869 201-534.0330 CLIENT: ENVIRO SCIENCES - Island Chemical Proiecc SAMPLE SOURCE: Samnle il2 SA:-I?LE DATE: Februarv »28, 19S6 TAKEN BY: A. Kvles AT LAB DATE: LABORATORY ANALYSIS REPORT PARAMETER .RESULT Flashpoint GT 95"C boiled 'I 95'C Specific Gravity ~ .0.9319 pH(uni.ts) 7 . 44 If you should have any questions, please do not hesitate co call. INDUSTRIAL CORROSION MANAGEMENT, INC. I Richard S. Zervtn Presidenc RSL:dlh GT=Greacer Than 301384 y^y.yit^ciyy7a S & W WASTE, INC. 115 JACOBUS AVE. . SOUTH KEARNY. N.J. 07032. (201)344-4004 GENERATORS WASTE MATERIAL PROFILE SHEET APPROVAL CODE TECHNICIAL REP. INITIALS I.A. GENERAL INFORMATION C ^ GENERATOR K.AMP J ^ C ^ ^ ZPyr<^^iI^ <^ k - S ^ 'juL'*^ I c y . , '/^-^7 ADDRESS. ^ ^ ! ^ C^y^ kyyy.ys/r7^^^zz> Jr. ZZw-^ c/S'lZT ergfzo GENERATOR EPA LD. N Q . / ^ ' . ^ '^Z^ZTyp-y.T- TECHNICIAL CONTACT »VASTE NAME_ - / y < . V t * ' y^ /f^-^ko cyvif/£yJCi»*'ti-- ftt*^ti-'jk / ^ r y - d Z u ^ ot'^sATZ^ /k'Qy/x> ( y A c ^ TITLE, V/^" PROCESS GENERATING WASTE. yXAcTTT^ PHON E ^ c y j i 6 - f = : z S X B. PHYSICAL CHARACTERISTICS OF WASTE PHYSICAL STATE «> 70°F C SOLID ' ^ I Q U I D C SEMI-SOLID C POWDEH % LIQUID % H20 ODOR \^^ COLOR AA{£u>>ryy /P*r ORGANIC INORGANIC : CHLORINATED ORGANIC BTU VALUE PER GAI «<. CL. 9SiW_ «(>ASH. % S . LAYERS a MULTl LAYERED ^ii'BI-LAYERED D SINGLE PHASED ; TOC. I COD. •>. SOLIDS • t / g ^ ^ - PH: CO-2 C 7.1-10 C 2.1-4 C 10.1-12.5 C 4.1-6.9 0 1 2 . 5 C7 C EXACT _ C N/A ^. / / SPECIFIC GRAVITY : <.S : .a-.9 : .9-.95 ; .95-1.0 : ;.o-i.i G 1.1-1.24 G 1.25-1.4 C 1.5-1.7 G >1.7 G EXACT. / : 0 & D FLASH C POINT acc DOC GEXACT. D <90 C <100 C 100-140 D 140.200 O <200 '(iSCOSmr (Cemiooiiei G 10O-1000 G 1000-10000 G > 10.000 G EXACT CHEMICAL COMPOSITION (MUSTTOTAL100%) % /Atysy^/Tcy/yz. Z3,L y7.£> y/. yuAy/TZZ. F. HAZARDOUS CHARACTERISTICS: TOXICITY RATINGS INHALATION DERMAL ORAL G EXPLOSIVE • WATER REACTIVE C MSDS ATTACHED y//? NFPA RATING D PYROPHORIC C SHOCK SENSITIVE G. MANIFEST INFORMATION^ PROPER DOT SHIPPING NAMF //2^7*:0C^.i:r C ' ^ / Z / . J C W / C D. METALS Ag As Ba Cd Cr Cu G TOTAL Zy/yZ y j y ) yZTT y y / l OTHER. C EP TOX Hg Ni Pb Se Zn_ Te /v'/f ^z^yL y / / : y ^ / l . DOT HAZARD CLASS C / ^ L y ^ - ^ UN/NA NO. y V y ^ - 9 r f ^ EPA/STATE WASTE TYPE EPA/STATE HAZARD CODE. <P=^^ / A £ r < i - / . .A. H. SHIPPING INFORMATION G BULK LIQUID O BULK SOLID 7:$)RUMS "OTHER SHIPPING FREQUENCY: QUANTITY / PER Ji2L£i:_ ^ E. G G G G G G G G G OTHER COMPONENTS PCB'S' / / ^ PESTICIDES/HERBICIDES*. yZiC CYANIDE OR CYANIDE PRODUCING y ^ ' ^ SULFIDE OR SULFIDE PRODUCING / ^ ^ PHENOLICS / Z A Z RADIOACTIVE INFECTIOUS yyyi_ ELEMENTAL METALS^ OTHER. y ^ •ATTACHED DISCLAIMERS >*US1 8£ SIGNED yz>^ I. SPECIALHANDLING INFORMATION/COMMENTS: J . I HEHEBY CERTIFY THAT ALL INFORMATION SUBMITTED ABOVE AND AL'L ATTACHMENTS ABE COMPLETE AND ACCURATE. ANO THAT ALL S-»MPLES SUBMlTTcD ARE REPRESENTATIVE OF THE WASTE. DATE CyQ.zj] TITLE GENERATORS SIGNATURE '^^ZL-f- 301385 Polychlorinated Biphenyl (PCB) Warranty ""Ms disclaimer is to all persons who generate and dispose of chemical waste. The terms PCB and JB's are used in this disclaimer to refer to any chemical substances and combinations of substan- ces that contain 50 ppm orgreaterof PCB's as defined in 40 CFR 761.3 (s), including any byproduct, in a process which contains less than 50 ppm PCB because of any dilution; again, these latter shali be included as PCB and PCB's. Substances that are regulated by this rule include, but are not limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and other chemical substances or combination of substances, including impurities and byproducts. It is unlawful for S&W Waste, inc. to receive PCB's. Any generator and/or transporter who knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal prosecution. hereby warrants that materials transferred by it to S&W Waste, Inc. for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl (PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby agrees to idemnify and hold S&W Waste, Inc. harmless from any costs, damages or other liability resulting from the breach of this warranty. DATED: : BY: WITNESS: Herbicide/Pesticide Warranty jSurrivi?) ^rtn^.lrpn_r^^ -J^^iMnereby warrants that material transferred by it to S&W Waste, Inc. for transportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level greater than 0.001% when measured in each container or vessel transferred to S&W Waste, Inc., and hereby agrees to indemnify and hold S&W Waste, Inc. harmless from any costs, damages or other liability resulting from the breach of this warranty. X^'\J^ZiZ> CH^HlC/'tL. Q.C^~i^<Z. DATED:. 3-3i-n sr.Vs:LXSkiAn ^^^\?xr--n WITNESS:. Y?/y^ykky^'-k Aluminum and Reactive Metal Warranty ^Si\z?yZ^C^AAM\'{Z^ ClCl^f^cL hereby warrants that material offered to S&W Waste, Inc for transportation, treatment and/or disposal does not contain elementa! aluminum ot reactive metal paste, powderorpigment and hereby agrees to idemnify and hold S&W Waste, Inc. harmles.< Vom any costs, damages, or other liability resulting from breach of this warranty. y:^J^-/^j^^ — ^ v ' z 301386 DATED: WITNESS m TABLE 1.3 30870-0705 MYTROSCIENCBS Sample Identification: ALAE 64869 PCB Isomer Resiilt. -g'K:? PCB 1016 <3.0 PCB 1221 <3.0 PCB 1232 '3.0 PCB 1242 ' <3.0 PCB 1248 <3.0 PCB 1254 <3.0 PGB 1260 <3.0 301387 YWC. INC. • 200 Monroe Turnpike • Monroe. Connecticut 06^8 • (203) 261-4453 INDUSTRIAL CORROSION MANAGEMENT INCORPORATED 1152 ROUTE 10. RANDOLPH, NEW JERSEY 07869 201-;34-0320 J August 13, 1986 Mr. Al Kyles ENVIRO SCIENCES INC. 610 we: Main Street Rockavay, NJ 07866 RE: Island Chemical Project - Flashpoincs Dear Mr. Kyles: Upon your request three samples fron Island Chemical( Sanple data: 2/2S/86) have been reanalyzed for Flashpoint using a Pensky-Martens Closed Tester. Saapla v5 (Labv 52958) and Sanple •t'V-s.bi.- 52960) were composited and analvzed on .V. 1986. The conoosita boiled a- 98°C. The :us; il results reportad(Re:;or: cata: March 7, 1936) were Sample =5 - 40°C duplicate 41°C and Sample it 7 - 45'c. Sample Y5 and iH were originally analyzed separately. There was insufficient samoie remaining to reanalyze sample i'S and -17 individually. Sample H i l a h i f 52957) was also reanalyzed on August 7, 1986., The original Flash- point reported for this saaale was 50''C. The reanalysis resulted in a flashpoint of 5^'C. We do not feel that the results of these reanalyses are as reliable as possible since the samples have been held for over five months from the date of collection. As stated in the method erroneously high flashpoints may be obtained due to loss of volatile material. These saaples were-n^ox stored in volatile organic bottles and therefore volatiles may have been lost. We are also unsure as to the correctness • of compositing hazardous waste for analysis. Enclosed please find a page from the NJDE? Field Procedures Manual, November 1985, cautioning against this practice. I have also enclosed a copy of the procedure for determining flashpoint by Pensky- Martens Closed Tester. If you have any further questions, please do not hesitate to call. Sincerely, INDUSTRD^ CORROSION MANAGEMENT, INC. Susan Richardson Quality Assurance Coordinator SR:dls enclosures 301388 yii.A^€<S61 STATE CERTIFIED DRINKING WATER/WASTEWATER LABORATORY I.D. #14116 INDUSTRIAL CORROSION MANAGEMENT INCORPORATED 1152 ROUTE 10. RANOOLPH. NEW j£J?SEir 07859 201-584.0320 NJDE? Certified Drinking Wacer/ Wastewater Laboratory ID-/ Uli6 REPORT DATE: .a,nril U . 198c LAB Q 52957 CLIENT: ENVIRO SCIENCES - Island Chemical Proiect SAMPLE SOURCE: Samnle •f^- SAMPLE DATE: February 2S. 1956 SAMPLED BY: A. Kvlas AT LAB DATE: \t^~.-- 1936 LABORATORY ANALYSIS REPORT Parameter **Petroleum Evdrocarfaon Result 176.000 mg/l(ppm) We chank you for chis oppo: do not hesitate to call. . to serve you. If you have any questions, please j Sincerely, INDUSTRIAL CORROSION MANAGEMENT, INC. ..,,, ,,zyy Lcnard S./LaviXe ichard S.A. resident/ RSL:dlh LT=less Chan **This test employs analytical mechodology which can give false positive readings. Simp' stated, this test is measuring the Carbon-Sydrogen linkage in organic molecules. While Petroleum Hydrocarbons most certainly possess this link, a number of organic molecules (Humus, Lignin etc.) noc considered petroleum based, also possess it as well. Therefore in order to more correctly confirm a high reading, it is suggested that a GC run be additionally performed. The above Tocal Petroleum Hydrocarbon concentration may noc represenc crue peer hydrocarbon value as indicated by an interference at 1745 cm-1. 301389 ,cyi'^6<'f^'^ INDUSTRIAL . CORROSION MANAGEMENT INCORPORATED 1152 ROUTE 10. RANOOLPH. NFiV JERSEY 07869 201-534-0230 NJDEP Certified Drinking Wacer/Vastewaca- Laboratory IDi? 14116 REPORT DATE: April 14, 1986 LAB ? 52957 CLIENT: ENTIRO SCIENCES - Island Chemical Proiect SAMPLE SOLTICE: Samnle fM SA>£PLE DATE: Februarv 28, 1986 TAKEN BY: A. kvles AT LAB DATE: March 7, l = i LABORATORY ANALYSIS REPORT • PARAMETER RESULT Flashooin; 50' Specific Gravity 1. 0565 pH(units) • 6.81 If you should have any questions, please do not hesitate to call. INDUSTRIAL COI^ROSION MANAGEMENT, INC. [/v^y---e^ President RSL:dlh 301390 .^cyiei"/*''' S & W WASTE, INC. 1 5 JACOBUS AVE. . SOUTH KEARNY, N.J. 07032. (201)344-4004 GENERATORS WASTE MATERIAL PROFILE SHEET APPROVAL CODE TECHNICIAL REP. INITIALS GENERATOR EPA I.D. NO. V / C ^ t f ^ ^ ^ - / ^ 3 r - /GsTfZ. (^"^"^.^ k'yy/?/srr:i*fj7^, J r - dyie<^ , / / n Z T c c p z . 0 GENERAL INFORMATION '.ENERATOR NAMP JlTctT^^? k k y y ^ / C a c k J ' ( / , - P . ^ - ^ - , 5 . y i ^ ^ ADDRESS- TPrHNiriAi r.nNTAP.T yZZ^z^ Z- /Zy^U^ Ckyfl-'/yUS Jczy^yj^ TiTi P ^A^ //jy-Zyfoz^u^ <Z^y^rz, y^/pu/.ei y y ^ ^ i - ^ ASTE N A M E . P R O C E S S GENERATING W A S T E . y'^<r?f^ PHONE . ^ ^ J z k t l l k ^ ^ ^ B. PHYSICAL CHARACTERISTICS OF WASTE 'HYSICAL STATE » TCFi °°°"y<^/'<Lp : SOLID ^ L I Q U I D C SEMI-SOLID 3 POWDER "b LIQUID . H 2 0 _ o/<.^ j ' ^ O S G A N l C I J ~ INORGA.NIC COLOR "Z CHLORINATED ORGANIC BTU VALUE PER GAL • • > * • • • • - ' _ ^ % C L _ BS4W_ ""b ASH. % S . LAYERS C MULTI LAYERED •:; BI-LAYERED 2<SiNGLE PHASED ] TCC i COO I i a^ SOLIDS Vt'-Ty<g" pH: • 0-2 G 7.1-10 C N/A C 2.1-4 G 10.1-12.5 G 4.1-6.9 0 1 2 . 5 ^ . y C 7 G EXACT ZZZZ— SPECIFIC GRAVITY :• <.3 ; .5-.3 : .9-.95 : .95-1.0 : 1.0-1.1 C 1.1-1.24 G 1.25-1.4 G 1.5-1.7 = >'-7 / . e r ' G EXACT _ 1 _ _ I _ _ D FLASH G POINT CCF) • CC • • OC • EXACT. • <90 • <100 C 100-140 G 140-200 G <200 9/'<^ iN(lSyOSrrY (CentiDoise) ^ 1 - 1 0 0 G 100-1000 G 100O-10000 G > 10.000 G EXACT C. CHEMICALCOMPOSIT10N(MUSTTOTALioo%) % zR. / : & : ^ i y M * - ^ /4c/y.yr^-y < ^ o . ( j ^ : , 0 / D. METALS Ag y ^ As Ba Cd Cr yZA. Cu ^ Z : D TOTAL zz>y ~zzyr y//^ O T H E R . A/y; C EP TOX H g . N i . P b . S e . Z n . T e . AJ^ y y y ; y j y . ~/yyr yyyi yZZZ F. HAZARDOUS CHARACTERISTICS: TOXICITY RATINGS • INHALATION D F R M A l ORAL G EXPLOSIVE G WATER REACTIVE C M S D S ATTACHED yA/f-- NFPA RATING G P Y R O P H O R I C D S H O C K SENSITIVE G. MANIFEST INFORMATION PROPER DOT SHIPPING NAME ^r.A.cAt«^ oAy^T^ yZca/cyi/y DOT HAZARD CLASS _ UN/NA NO. yJy} OyCyff-€' ^yA^ EPA/STATE WASTE TYPE _ EPAySTATE HAZARD C O D E . ^ Z ^ - ' t Z y y t z f y H. SHIPPING INFORMATION C 3 U L K L I Q U I D C B U L K S O L I D " ^ D R U M S G O T H E R SHIPPING FREQUENCY: QUANTITY S r ^ j ? ER g*^cy E. G 0 C Q G G G n OTHER COMPONENTS PCB'S* PESTICIDES/HERBICIDES* CYANIDE OR CYANIDE P R O D U C I N G . SULFIDE OR SULFIDE P R O D U C I N G _ P H E N O L I C S RADIOACTIVE INFECTIOUS y y ^ yZAT y/r / j y t E L E M E N T A L M E T A L S * . O T H E R . •-ZA4- yyy^ vTTACHED DISCLAIMERS MUST BE SIGNED I. SPECIALHANDLING INFORMATION/COMMENTS: I HEREBY CERTIFY THAT ALL INFOF^^lOflON SUBMIfTEp|ABOVE ARE REPRESENTATIVE OF THE WAS • 3 - I b ^ ^ T DR^OriON SUBMIfTEplABOVE AN» ALL ATTACHMENTS ARE COMPLETE ALL ATTACHMENTS ARE COMPLETE AND ACCURATE. AND THAT ALL SAMP'.ES SUBMlTTcD DATE TITLE GENERATOR'S SIGNATURE 301391 Poiychiorinated Biphenyl (PCB) Warranty •' '-^ disclaimer is to all persons who generate and dispose of chemical waste. The terms PCB and _ 3's are used in this disclaimerto refer to any chemical substances and combinations of substan- :es that contain 50 ppm orgreaterof PCB's as defined in 40 CFR 761.3 (s), including any byproduct, in a process which contains less than 50 ppm PC3 because of any dilution; again, these.latter shall be included as PCB and PCB's. Substances that are regulated by this rule include, but are not limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and other chemical substances or combination of substances, including impurities and byproducts. It is unlawful for S&W Waste, Inc. to receive PCB's. Any generator and/or transporter who knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal prosecution. hereby warrants that materials transferred by it to S&W Waste, Inc. for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl (PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby agrees to idemnify and hold S&W Waste, Inc harmless from any costs, damages or other liability resulting from the breach of this warranty. DATED: EY: WITNESS; Herbicide/Pesticide Warranty T^Lf^^JD r'-tfcl'^-lC/>?P^ca.'DK4ifirphy warrants that material transferred by it to S&W Waste, Inc. for transportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level greater than 0.001% when measured in each container or vessel transferred to S&W Waste, Inc., and hereby agrees to indemnify and hold S&W Waste, Inc. harmless from any costs, damages or other liability resulting from the breach of this warranty. ^jiSL-fVJi^C n^.tC^'tV- OJC aTfXl DATED:. V/ITNESS: Aluminum and Reactive Metal Warranty " I ^ V , < V ^ rngTAiTftu ( ^ . A>f3T . hereby warrants that material offered to S&W Waste, Inc. for transportation, treatment and/or disposal does not contain elemental aluminum or reactive metal paste, powderorpigment and hereby agrees to idemnify and hold S&W Waste, Inc. harmless ''om any costs, damages, or other liability resulting from breach of this warranty. — ^ :P3U.VJO ctKwMC/?u06\<^^c DATED:_?±il^3 PV- ^ . . W . ^ C ^ WITNESS: 301392 TAHLB 1.0 30S70-0705 ENVTROSCIENCES Samule Identification: KARB 64980 PCB Isomer P.es'a.1' PCB 1016 <0.20 PCB 1221 <G.20 PCB 1232 <0.20 PCB 1242 . <0.20 PCB 1248 ' <0.20 PCB 1254 <G.20 PCB 1260 <0.20 301393 YWC. INC. • 200 Monroe TL^npske • Monroe. Connecticut 06d6& • (203) 261-'U58 p' INDUSTRIAL CORROSION MANAGEMENT INCORPORATED .1152 ROUTE 10. RANOOLPH. NEW JERSEY 07863 201-534^330 August 13, 1986 Mr. Al Kyles ENVIRO SCIOCES INC. 610 West Main Screec ..... Rocks.way, NJ 07866 RE: Island Chemical Project - Flashpoinrs Dear Hr. Kyles: Upon your request three saaples from Island ChemicaK Sanple date: 2/2S/86) have been reanalyzed for Flashpoint using a Pensky-Martens Closed Tester. Sancie ?5 (Lab/f 52958) and Sample i-7(Lab# 52960) were composited and analyzed on Aurust 7, 1986. The composite boiled at 9S°C. The original results reported(Re::ort date: March 7, 1986) were Sanple -75 - '^O'C. duplicate 41°C and Samule -f 7 - ^'s'C ianaie 115 and were origina si LVZ: setjar; :eiv. There was insufficient sansle remaining to reanalyze sanple ^5 and 117 individually.- Sample ill4(lab# 52957) was also reanalyzed on August 7, 1986. The original Flash- point reported for this sasrole was 50'C. The reanalysis resulted in a fashpoint or 54°C. We do not feel that che results of these reanalyses ara as reliable as possible sines the samples have been held for over five months from the dace of collection. As stated in Che method erroneously high flashpoints may be obtained due co loss of volacile material. These sanples were"."n'ar stored in volatile organic bottles and therefore volatiles may have been lost. We are also unsure as'to the correctness of compositing hazardous waste for analysis. Enclosed please find a page fron the NJDE? Field Procedures Manual, November 1985, cautioning against this practice. I have also enclosed a copy of the procedure for determining flashpoint by Pensky- Martens Closed Tester. If you have any further questions, please do not hesitate to call. Sincerely, INDUSTRIAL CORROSION M.'^AGEMZNT, I N C . y SR:dls enclosures Susan Richardson Quality Assurance Coordinator 301394 STATE CERTIRED DRINKING WATE.R/WASTEV/ATER LABORATORY I.D. S14115 /*^yiyzcc^9S^0 INDUSTRIAL CORROSION MANAGEMENT INCORPORATED NJDEP Certified Drinking Wacer/Wastavate: Laboratory ID# 14116 REPORT .DATE: .^oril 14. 1986 LAB H 52960 1152 ROUTE 10. RANDOLPH. NEW JERSEY 07£o5 201-584-;3330 CLIENT: ENVIRO SCIENCES - Island Chenical Project SAMPLE SOURCE: Samole -fH SAMPLE DAIE: Februarv .28, 1986 lAKZM SY: A. Kvles AT LAB DATE: March ?86 LABORATORY ANALYSIS REPORT PARAMETER RESULT F l a s h p o i n t S p e c i f i c Gravi p H ( u n i t s ) 45°C 1.0836 5.05 If you should have any questions, please do not hesitate to call. INDUSTRIAL CORROSION MANAGEMENT, INC. RSL;dlh glchard S. I^vWe President r y»l y,yci.4'/i^ 301395 INDUSTRIAL CORROSION MANAGEMENT INCORPORATED 1152 ROUTE 10. RANDOLPH. NEW JERSEY 07865 201-534.0330 NJDE? Certified Drinking Wacar/Wastevate: Laboracory IDi* 14116 REPORT DATE; April 14. 1986 LAB# 52958 CLIENT: ENVIRO SCIENCES - Island Chenical Proiect SAMPLE SOURCE; Samnle •'/5 SAMPLE DATE: Februarv JS, 19S6 TAKEN BY: A. Kvles AT LAB DATE: March LABORATORY ANALYSIS REPORT PARAMETER RESULT Flashpoint Specific Gravit; pHCunits) ^0°C 1.0206 4.51 — 1 U V .-ur; If you should have any questions, please' do noc hesicace to call. INDUSTRIAL CORROSION MANAGEMENT, INC. V ^ ' / y j y ^ y - - ^ RSL:dlh Richard S. LfevThe Presidenc / 301396 y y ^ ^ £ 6<tl<' ..INDUSTRIAL CORROSION MANAGEMENT INCORPORATED 1152 ROUTE IQ. RANOOLPH. NEW JERSEY 07863 201-584-01-0 NJDE? C e r c i f i e d Drinking Water/ Wastewater Laboracory IDi/ 14116 REPORT DATE; A p r i l 14. joRf, LA3 i 52953 CLIENT; ENVIRO SCIENCES - Island Chenical Proiect SAMPLE SOURCE: Sample •?5 SAMJ'LE DATE: February 28. 1986 SAMPLED BY; A. Kvles AT LAB DATE: ^'=- LABORATORY ANALYSIS REPORT Parameter **Pecroleum Evdrocarbon Result LT 5 mg/l(ppm) We chank you for this opportunity to serve you. If you have any questions, please do noc hesicace co call. Sincerely, INDUSTRIAL CORROSION MANAGEMENT, INC. lichard S. /Levi^e Presidenc k RSL;dlh LT»less than **This Cesc employs analytical mechodology which can give false positive readings. Sinp stated, chis cesc is measuring che Carbon-Hydrogen linkage in organic molecules. While Pecroleum Hydrocarbons mosc certainly possess chis link, a number of organic molecules (Humus, Lignin ecc.) noc considered pecroleum based, also possess ic as well. Therefore in order to more correctly confirm a high reading, ic is suggesced chac a GC run be addicionally performed. The above Tocal Pecroleum Hydrocarbon concentration may noc represenc crue peer hydrocarbon value as indicated by an interference at 1745 cm-i. 301397 ^ y j / l . e ' 6 ^<lfO INDUSTRIAL CORROSION MANAGEMENT INCORPORATED NJDEP C e r c i f i e d Drinking Water/ Wascewacer Laboracory ID') 14116 RZPORT DATE; April 14. 1986 L ^ ^ 52960 1152 ROUTE 10. RANOOLPH, NEW JERSEY 07869 201-584.0330 CLIENT; prVIRO SCIENCES - Island Chenical Proiect SAMPLE SOURCE; Samole ••?7 SAMPLE DATE: February 28. Icge SAMPLED 3Y: A. Kvles _AT LAB DATE: Manr. 7. 19S5 LABORATORY ANALYSIS REPORT Paramecer **Pecroleun Hydrocarbon Resulc 100 ng/1(ppm) We chank you for chis opportunicy to serve you. If you have any questions, please do not hesitate to call.. • " Sincerely, INDUSTRIAL CORROSION MANAGEMENT, INC. Aichard S./Levi^e President RSL; dlh LT-less than **This Cesc employs analycical mechodology which can give false posicive readings. Simpi scaced, chis cesc is measuring che Carbon-Hydrogen linkage in organic molecules. While Pecroleum Hydrocarbons mosc cercainly possess chis link, a number of organic nolecules (Humus, Lignin etc.) not considered pecroleum based, also possess ic as well. Therefore, in order Co more correcdy confirm a high reading, it is suggested that a GC run be additionally performed. The above Total Petroleian Hydrocarbon concentration may not represenc crue peer hydrocarbon value as indicaced by an incerference at 1745 cn~l-. 301398 ^ ^ A : ^ £ < ' 7 y ^ ^INDUSTRIAL ••^•- JCORROSION 1 MANAGEMENT INCORPORATED .^^- 1152 ROUTE JO, RANDOLPH. NEW JERSEY 07869 r01-5M-033O CLIENT; EN\'IRO SCIENCES - Island Ihemical Proiect NJDEP Certified Drinking Water/ Wastewater Laboratory ID# 14116 REPORT DATE; Apr-;i 14, iofl<^ LAB } 59ot;6 y ' ^ " -t ^ SAMPLE SOURCE: Samole il3 SAMPLE DATE; February 18.- 1986 SAMPLED BY: A. Kvles AT LAB DATE; March 7. 1986 LABORATORY ANALYSIS RZPORT Parameter **Petroleum Evdrocarbon Resulc 22£L mg/l(ppm) We chank you for chis opporcunicy to serve you. If you have any quescions, please do noc hesicace to call. Sincerely, INDUSTRIAL CORROSION MANAGEMENT, INC. iichard S./L P r e s i d e n c / evi;(e RSL: dlh LT-less Chan **This Cesc employs analycical mechodology which can give false posicive readings. Simp.' stated, chis cesc is measuring che Carbon-Hydrogen linkage in organic nolecules. While Pecroleum Hydrocarbons mosc cercainly possess chis link, a number of organic nolecules (Humus, Lignin ecc.) noc considered pecroleum based, also possess iC as veil. Therefore in order co more correcdy confirm a high reading, iC is suggesced chac a GC run be additionally performed. . . The above Tocal Pecroleum Hydrocarbon concentration may noc represenc true peer hydrocarbon value as indicaced by an incerference ac 1745 ca-1. 301399 /o^ytT^ ¥!/o ^ S & W WASTE, INC. 115 JACCBUS AVE. . SOUTH KEARNY. N.J. 07032. (201)344-4004 GENERATORS WASTE MATERIAL PROFILE SHEET m A P O R O V A L COOE TECHNICIAL REP. INITIALS . GENERAL INFORMATION CA^'^'/DSI GENERATOR NAME - Z / g g ^ ' ^ (ZkytfyrryC/M:, k A k ^ . - ^ - ^ -'kt<^J GENERATOR EPA I.D. NO lyyoP(ft>(^ryPrS ADDRESS 2r-r. <^7'73'^ CZyyPy^rys^^MyCy) J h C c ^ . ^ < y r y r ' g^>5£gt7 " " ^ - ^ " ^ ^ ^ - , . — ^ 1 — _ , — - ^ - — ; TECHNICIAL roNTArT ^ t p ^ yZ/- /tycs.^yZZ-yy/ig J 2 a ^ i j < i j WASTE NAME /A^f^Py^^StK^ y U / ^ X . y r y c - y y O A - TITLE. l^P PROCESS GENERATING WASTE. ^ 'y=*-cc.. PHONP.^'/'/ykvg- - g ^ i B. PHYSICAL CHARACTERISTICS OF WASTE PHYSICAL STATE @ 70°F XSOLID D LIQUID C S E M I - S O L I D G POWDER % LIQUID % H 2 0 ODOR y t y t r f f C COLOR y / y f G ORGANIC ! ) r INORGANIC 1 I u CHLORINATED ORGANIC BTU VALUE PER GAI «b Cl % S B S i W % A S H L A Y E R S y < y > ^ • MULTI LAYERED D BI-LAYERED D S I N G L E PHASED T O C . C O D . yVA! ««. SOLIDS. pH: DO-2 D7.M0 y^Hlti. C 2.1-4 C 10.1-12.5 D 4.1-6.9 0 1 2 . 5 D7 D EXACT SPECIFIC GRAVITY c ca D i ; - . 9 C .9-.95 D.95-1.0 • 1.0-1.1 D 1.1-1.24 D 1.25-1.4 D 1.5-1.7 X > 1 - 7 D EXACT_ D F L A S H • POINT O r F ) • cc DOC D < 9 0 • < 1 0 0 D 1 0 0 - 1 4 0 D 14C-200 D < 2 0 0 D EXACT ' ^ C y Z t ^ J ^ VISCOSITY (CentipoiM G 1-100 C 100-1000 G 1 0 0 0 - 1 0 0 0 0 D > 1 0 . 0 0 0 C E X A C T . y C 4 n ^ e . . C. CHEMICAL COMPOSITION (MUSTTOTAL100%) % yzyye^y:!..^/' (Z^ <!^'0 / o y ^ y i j ^ ^ l ^ y Z ^ ^ y k • " C g g . y > C F C Y D. M ETALS ^ D TOTAL y y y A.<; Ba Cd Cr Cu yyy; yyy: y / y : yyy} /y'y^ OTHER. y y y ! D EPTOX H g . Ni. Pb. Se. Zn. Te. yjy! y y y : ~yyZr y y / / z y y ^ ^ i Z ^ E. D D D D O D D D D OTHER COMPONENTS PCB-S* PESTICIDES/HERBICIDES* CYANIDE OR CYANIDE PRODUCING . SULFIDE OR SULFIDE PRODUCING _ PHENOLICS RADIOACTIVE INFECTIOUS ZMZ ZM. .A/^ _^4f£_ yyA yz^ ELEMENTAL METALS'. OTHER. : ^ •ATTACHED DISCLAIMERS MUST 8E SIGNED '^K. F. HAZARDOUS CHARACTERISTICS: TOXICITY RATINGS INHALATION DERMAL ORAl D EXPLOSIVE D WATER REACTIVE D MSDS ATTACH ED NFPA RATING y / a < y ^ - D PYROPHORIC D SHOCK SENSITIVE G. MANIFEST INFORMATION / / /- • PROPER DOT SHIPPING NAME y^'^PjTTJiej-'ic^ .j^Jr^Ty. JZxy^? - DOT HAZARD CLASS (ZPyfy^-rS' UN/NA NO y j y y f ' 9yrP7 , EPA/STATE WASTE TYPE. EPA/STATE HAZARD CODE. ^ y t S ^ ' D H. SHIPPING INFORMATION /'^'^^ k^r^CC O / / D BULK LIQUID D BULK SOLID ^TDRUMS G OTHER SHIPPING FREQUENCY: QUANTITY / O P F R ^ ^ C e 1. SPECIAL HANDUNG INFORMATION/COMMENTS; yi/t-rrtr.t C<yry-yy> ^ y y c c^ ^-g y / y J ^ /)yuy*^fi-' . ^ y < L t ^ ^ y ^ t y ^ ' i - y r T r y y ^ y - / ^ y - ^ i / < - y > ' y ^ ^ . ^ e ^ y y y^mi^nyiu^r- C^i (Z£.t:-:i*f yyyir^ZZ^ " ^ ^ • ^ . I HEREBY CERTIFY THAT ALL INFORMATION SUBMITTED ABOVE AND ALL AHACMMENTS ARE COMPLETE AND ACCURATE. AND THAT ALL.£AMPXES SUBMITTED ARE REPRESENTATIVE OF THE WASTE. y \ TITLE DATE BMITTED ABOVE AND ALL AHACMMENTS ARE COMPLETE AND ACCURATE. AND THAT ALL.£AMP ily€^^' AAy.iA.kLI GENERATOR'S SIGNATURE THZZZZ 301400 Polychlorinated Biphenyl (PCB) Warranty •^his disclaimer is to all persons v/ho generate and dispose of chemical waste. The terms PCB and r'CB's are used in this disclaimerto refer to any chemical substances and combinations of substan- ces that contain 50 ppm orgreaterof PCB's as defined in 40 CFR 761.3 (s), including any byproduct in a process which contains less than 50 ppm PCB because of any dilution; again, these lattershall be included as PCB and PCB's. Substances that are regulated by this rule include, but are not limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and other chemical substances or combination of substances, including impurities and byproducts. It is unlawful for S&W Waste, Inc. to receive PCB'a Any generator and/or transporter who knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal prosecution. Ooyy /.^ A -. ,. f Z \'z:xz^-r-'-r=r:r^=^/ hereby warrants that materials transferred by it to S&W Waste, Inc. for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl (PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby agrees to idemnify and hold S&W Waste, Inc harmless from any costs, damages or other liability resulting from the breach of this warranty. J ^ L f ^ O CthiA^ UZb-^ Qyj J I M <=- DATED:. g - ( / - ^ ? .v ^ y V ^ C k f M - - QeeyJuP^ WITNESS: ( ^ y ^ ^ ^ Herbicide/Pesticide Warranty hereby warrants that material transferred by it to S&W Waste, Inc. for transportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level greater than 0.001% when measured in each container or vessel transferred to S&W Waste, Inc., and hereby agrees to indemnify and hold S&W Waste, Inc. harmless from any costs, damages or other liability resulting from the breach of this warranty. X ' - ^ L P ^ ^ Cff-^O^^^^TV ^ ^ ^ ^ ^ ' DATED: wn..... k^^<ky^/^yzCy Aluminum and Reactive Metal Warranty ^ hereby warrants that material offered to S&W Waste, Inc for transportation, treatment and/or disposal does not contain elemental aluminum or reactive metal paste, powder or pigment and hereby agrees to idemnify and hold S&W Waste, Inc. harmless from any costs, damages, or other liability resulting from breach of this warranty. ^ ^ DATED: ' S ^ ^ I S l BY: ^ j ^ rJA^/i/K/V-^ ^ U ^ A s J ^ ^ wnt^F'^.- / ^ k ^ . * < J ^ y ^ c ^ L y ^ 301401 S & W WASTfc, INC. 15 JACOBUSAVE. . SOUTH KEARNY. N.J. 07032. (201)344-4004 GENERATORS WASTE MATERIAL PROFILE SHEET CODE TECHNICIAL REP. INITIALS GENERAL INFORMATION _ GENERATOR M A I ^ P ^ S C ^ ^ <Z^yy<Zy^yCc^ d . / ^ 0 ^ W/^/^7 GENERATOR EPA LD. NO. 'iZl/l2J^^i£lyC>?r' ADDRESS ^ ^ ^-A?.^, ZAt^yfyZTTi^T^iZj Sr. C^^yry </yjiT £>afz2,y} i . -.1 V ; -y ; TECHNICIAL r n i ^ T A P T ^ ? - ^ ^ - i^VC^ky^yyy^ J t O ^ i ^ ) vASTE NAME //^Z7yyx>ci6 / > y ^ 7 ^ SZcyp y ^ c S - TITLE. V/=' P H O N E ^ g / - J ' g t g " - J Z S J C PROCESS GENERATING WA.'^TF X l > ^ g . J / y ^ A - o . ^ . J J ^ J B. PHYSICAL CHARACTERISTICS OF WASTE PHYSICAL STATE @ 70°F _XSOLID D LIQUID 3 SEMI-SOLID C POWDER «b LIOUID •*>H20 OOOH . S<.y<?.ryr- . y ^ ^ a . ' ^ ^ y < i y £ > COLOR y < / A D ORGANIC X. INORGANIC D CHLORINATED ORGANIC BTU VALUE PER GAL y^y? *, r i % s R.t^W <»»A.<;H LAYERS y y A D MULTI LAYERED D BI-LAYERED D SINGLE PHASED TOC. COD. y^'y/ ">|>S0LIC£. pH: c o - 2 n 7.1-10 V N / A D 2.1-4 C 10.1-12.5 ^ C 4.1-6.9 D>12.5 C 7 D EXACT SPECIFIC GRAVITY D < 8 C3-.9 C .9-.95 D.95-1.0 D 1.0-1.1 • 1.1-1.24 C 1.25-1.4 G 15-1.7 n EXACT. D FLASH D POINT • CF) DCC • OC G EXACT. D < 9 0 D <100 O 100-140 D 140-200 I <200 /o, viSCOSmr (Ceniipoise) C 1-100 D 100-1000 • 1000-10000 oiaooo D EXACT_ /v/i CHEMICAL COMPOSITION {MUSTTOTAL IOO%) % y / y ^ kkua»^ <Zo / ^ ^yjeDrrr" (L t^yZi y^AcAZZZa /^'rjL Zky^:^^ if.c,^'/ D. Ag As Ba Cd Cr Cu O T H E R . METALS . D TOTAL y / \ I W I ~ y 7 ^ zzzy yzz^r i E P T O X Hg Ni Pb Se Zn Te /zy^ / V A ~Z(Zyr yyyt y y y E. D D D a D D a D D OTHER COMPONENTS PCB'S* / ^ PESTICIDES/HERBICIDES* CYANIDE OR CYANIDE PRODUCING . SULFIDE OR SULFIDE P R O D U C I N G , PHENOLICS RADIOACTIVE ! INFECTIOUS y / T ^ ~7Z7r /vy y/A ~Z(7/r ELEMENTAL METALS*_ O T H E R . ^ • w •ATTACHED DISCLAIMERS MUST BE SIGNED F. HAZARDOUS CHARACTERISTICS: TOXICITY RATINGS INHALATION DERMAL ORAL D EXPLOSIVE D WATER REACTIVE O MSDS ATTACHED NFPA RATING y / C y ^ ^ a PYROPHORIC D S H O C K S E N S m v E G. M A N I F E S T I N F O R M A T I O N PROPER DOT SHIPPING NAME /AriT-yyjyijjL! ^JyyJi. Jr:ApyJ::}L- DOT HAZARD CLASS, UN/NA NQ. y ^ y ^ n y f y i ^ - ^ ^/f? EPA/STATE WASTE T Y P E . EPA/Sfjiffe HAZARD C O D E . ^ C X ^ Z - - / - H. SHIPPING INFORMATION C BULK LIQUID G BULK SOLID X ' D R U M S SHIPPING FREQUENCY: QUANTITY y7y6^A~r*:C^ £fyjy O O T H E R 5 PER,i!25£*-' I. SPEplALHANDLING INFORMATION/COMMENTS: y y ^ < ^ : k/y^jy/^ i^/t^^t;^ ^/=- / ^ rr<L. /7/iyo J)<U<yMy^, gC^fZ-e, yyvU^, TTiyiftu:, /Z,yy!/^o tz.^ _ ^ g/7/f/gJ £>£r£ie/ac:}rz£> • /y]cyct.x> /y/yrry I HEREBY CERTIFY THAT A.LL INFORMATION SUBMITTED ABOVE AND ALL ATTACHMENTS ARE COMPLETE ANO ACCURATE. AND ARE REPRESENTATIVE 0= THE WASTE. A>'ID-3 7 DATE czy,y-. TITLE GENERATOR'S SIGNATURE lAT ALL SAMPLES SUBMITTED 301402 Polychlorinated Biphenyl (PCB) Warranty T - disclaimer is to all persons who generate and dispose of chemical waste. The terms PCB and F-^^B's are used in this disclaimer to refer to any chemical substances and combinations of substan- ces that contain 50 ppm org reater of PCB's as defined in 40 CFR 761.3 (s), including any byproduct, in a process which contains less than 50 ppm PCB because of any dilution; again, these lattershall be included as PCB and PCB's. Substances that are regulated by this rule include, but are not limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and other chemical substances or combination of substances, including impurities and byproducts. It is unlavi^ul for S&W Waste, Inc to receive PCB's. Any generator and/or transporter who knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal " 4 ^ ^ ^ ^ -^—^^'^£r^S hereby warrants that materials transferred by it to S&W Waste, Inc. for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl (PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby agrees to idemnify and hold S&W Waste, Inc harmless from any costs^ damages or other liability resulting from the breach of this wan-anty. XSLl*rAJD CtrtC^'-<^/'^~>- CO ZP^^ 3-f(-S? RY- ^ S k A r v y - ^ c y j - ^ wiTNF.';.^- /z2iz^^y^^zk^iyu/ -% ^^ Herbicide/Pesticide Warranty KZ y A i • -y 1 . " ^ hereby warrants that material transferred by it to S&W Waste, Inc. for transportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level greater than 0.001% when measured in each container or vessel transferred to S&W Waste, Inc., and hereby agrees to indemnify and hold S&W Waste, Inc. harmless from any costs, damages or other liability resulting from the breach of this warranty. JTx-^A-IAJO QtPiyA^CATi C ^ Z ^ <^ DATED:. DATED: WITNESS: Aluminum and Reactive Metal Warranty ? £ ^ hereby warrants that material offered to S&W Waste, Inc. for transportation, treatment and/or disposal does not contain elemental aluminum or reactive metal paste, powderorpigment and hereby agrees to idemnify and hold S&W Waste, Inc. harmless '•om any costs, damages, or other liability resulting fr©ffl±)reach^fihisw^n^i;^^ ^ ^ _ . DATED:_Ojl/_|2i2 . Ry. I ^ W ^ j C L ( ^ I V \ , Scg^^-/^ WITNESS: c^ty^'^^^..rr<. y \ <yU ^ 301403 S & W WASTE, INC. 115 JACOBUSAVE. . SOUTH KEARNY. N.J. 07032. (201)344-4004 GENERATORS WASTE MATERIAL PROFILE SHEET GE NERATOR NAME J ^ g ^ < ^ : ^ A ^ ^ / ^ ^ APPROVAL CODE TECHNICIAL REP. INITIALS A. GENERAL INFORMATION ADDRESS ' ZZZtZ " ^ a . . , j^^i. GENERATOR EPA I.D. NO. fAZ^^JlZ^J/.y'^ TECHNICIAL CONTACT ' ^ ^ ' ^ ' y ^ / < ^ ^ ( ^ ^ y / f c c .J/Ziyyy-kl WASTE MAK.c / y ^ - ^ j y ^ ^ / y / y A ^ k k - y j s y < / < ^ ' 0 £ f ^ TITLE. yp PROCESS GENERATING WASTE yZy^/fy/Chc^rrj PHONE ^ / / W - g . ^ B. PHYSICAL CHARACTERISTICS OF WASTE PHYSICAL STATE @ TCF! ^ S O L I D 12 LIQUID • SEMI-SOLID D POWDER % LIOUID "fcHZO ODOR Sc<y-i^' A k / e ^ COLOR yZA'yCyjy/ 'fX*'»< "^ORGANIC C INORGANIC D CHLORINATED ORGANIC BTU VALUE PER GAL _ £./yf^Ai^e:ynif 'ft C L _ BS«W_ % ASH. SbS. LAYERS y i / y r a MULTI LAYERED G BI-LAYERED O SINGLE PHASED TOC. COD. y y y Ob SOLIDS. pH: a 0-2 D 7.1-10 D N/A D 2.1-4 D 10.1-12.5 C 4.1-6.9 0 1 2 . S ^ C 7 D FYAr.T 6 ' « g SPECIFIC GRAVITY • <.8 D.fi-.9 C .9-.95 C.95-1.0 D 1.0-1.1 D 1.1-1.24 a 1.26-1.4 D \£r\.l D>1-7 0 EXACT. 2/.?^ C FLASH C POINT = CF) CCC • OC CEXACT. D<90 D <100 C 100-140 • 140-200 5f>S00 VISCOSITY (Centipoisel C 1-100 C 100-1000 C 1000-10000 O10.000 y V y C n EXACT _ _ l _ _ l _ 0. CHEMICAL COMPOSITION (MySTTOTAL 100%) % '^uriy.'yt^ayrfffa /fdi^ruWC K O S I T I U N d v i y j x2^.^>^ (y^y<0(D^^^yyk zSO y f c - C i S i / D. A g . A s . Ba. Cd. Cr_ Cu. METALS a TOTAL y y A y / A D EPTOX yM J14. yZ/T OTHER. ZZUTT Hq Nl Pb Se -Zn Te yyA yyyj yyyj y j / i yi/yj y/yi F. HAZARDOUS CHARACTERISTICS: TOXICITY RATINGS INHALATION DERMAL ORAL D EXPLOSIVE D WATER REACTIVE D MSDS ATTACHED yj/^ NFPA RATING a PYROPHORIC D SHOCK SENSITIVE G. MANIFEST INFORMATION^ PROPER DOT SHIPPING NAME / A ^ r ^ o C ^ / y ^ y r z J y ^ / K .^> DOT HAZARD CLASS ZZ)/Cy^-<S ^ UN/NA NO y^AA 9<^f7 EPA/STATE WASTE TYPE. EPA/STATE HAZARD CODE. y y ^ Z t c H. SHIPPING INFORMATION D BULK LIQUID D BULK SOLID " ^ D R U M S SHIPPING FREQUENCY: QUANTITY. COTHER / p=a (yrf^i." E. a a n D a n D D D OTHER COMPONENTS PCB'S* y//l PESTICIDES/HERBICIDES* CYANIDE OR CYANIDE PRODUCING . SULFIDE OR SULFIDE PRODUCING. PHENOLICS RADIOACTIVE INFECTIOUS yUA y / i yAi ZZK ZM. zyAz ELEMENTAL METALS*. OTHER. AM. •ATTACHED OrSCLAIMERS MUST BE SIGNED ZZM. I. SPECIALHANDUNG INFORMATION/COMMENTS: y ^ y a o u t y ^ ^ . y t y y / Z : y ^ y ^ ^ y i y ^ ^ y 7 y y j y ^ < . y y y A i ^ 1 HEREBY CERTIFY THAT ALL INFORMATION ARE REPRESENTATIVE OF THE WASTE. DATE lACHMENTS ARE COMPLETE AND ACCURATE. AJ<D THAT AU. fAMPl.ES SUBMITTED / C^^.iA. TITLE GENERATOR'S SIGNATURE 301404 Polychlorinated Biphenyl (PCB) Warranty is disclaimer is to all persons who generate and dispose of chemical waste. The terms PCB and rCB's are used in this disclaimerto refertoany chemical substancesand combinations of substan- ces that contain 50 ppm orgreaterof PCB's as defined in 40 CFR 761.3 (s), including any byproduct, in a process which contains less than 50 ppm PCB because of any dilution; again, these lattershall be included as PCB and PCB's. Substances that are regulated by this rule include, but are not limited to, dielectric fluids, contaminated solvents, oils, waste oils,* heat transfer fluids, hydraulic fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and other chemical substances or combination of substances, including impurities and byproducts. It is unlawful for S&W Waste, Inc to receive PCB's. Any generator and/or transporter who knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal PtQsecution. o,o-x _ y k r > , Av^.O^r^TT^lO^ (^<) -P^J"^ ireby warrants that materials transferred by it to S&W Waste, Inc. for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl (PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby agrees to idemnify and hold S&W Waste, Inc harmless from any costs, damages or other liability resulting from the breach of this warranty. JkS\.f\^k) C^'^A^Ur^ (ZO or/^o. DATED:. 3->(-^V PY- \^\od^(3J^fhy^rSey^^i{^^y WITN i Z ^ ^ ^ _ Herbicide/Pesticide Warranty 17_1-^•ll y z . --fz. Kr=^ L'-rr-r-TT': v:::rT hereby warrants that material transferred by it to S&W Waste, Inc. fortransportation, treatment and/or disposal is not contaminated by herbicide/pesticide ata level greaterthan 0.001% when measured in each container or vessel transferred to S&W Waste, Inc., and hereby agrees to indemnify and hold S&W Waste, Inc harmless from any costs, damages or other liability resulting from the breach of this warranty. jpTS {.^f\T>ZO> C ti^r^C^rh^Cl U DATED: ^ - )/-^7- py. ^l>vtC|/alAv— iQzc^Jz-^^ WITNESS: /M^^k^jy ^Aluminum and Reactive Metal Warranty \ \^^^—^ .^-P-TTSI^* hereby warrants that material offered to S&W Waste, Inc. for transportation, treatment and/or disposal does not contain elemental aluminum or reactive metal paste, powder or pigment and hereby agrees to idemnify and hold S&W Waste, I nc. harmless -om any costs, damages, or other liability resulting fronoLbreach of this warranty., ^ . n yr. T yU.^f\/y^y) ol^^^^j^icn- ^ y ^ ' \ i - y ._ ... ^i^^ciMy— ^^o^ DATgP- ; „ . ^ WITNESS: _ 301405 :^i'i PRIORITY POLLUTANT VOLATILE ORGANIC ANALYSIS LABORATORY ID IU116 LAB # 5295^ CLIENT: ENVIRO .SCIENCES-I.siand Chemir::! V-ni SAMPLE SOURCE Sample n ... .-..-:. ec; GC/MS Method 624* Tier II Deliverables PARAMETER Chloromethane Bromomethane -• Vinyl Chloride • Chloroethane Hethylene Chloride 1 ,1-Dichloroethene 1 ,1 -Dichloroethane Trans-l ,2-Dichloroethene • Chloroform 1,2-Dichloroethane 1 ,1 ,1-Trichloroethane Carbon Tetrachloride Bromodichloromethane 1,2-Dichloropropane • -- Trans-1,3-Dichloropropene Trichloroethene Di bromochloromethane 1,1 ,2-Trichloroethane Benzene — cis-1", 3-Dichloropropene — 2-Chloroethyl vinyl ether Bromoform Tetrachloroethene 1,1 ,2 ,2-Tetrachloroethane Toluene • Chlorobenzene Ethyl benzene Total Xylenes *Dichlorobenzenes noc analyzed under chis mechod. RESULT ug/l u u u u u u u u 8.2B U U U U U u • " i u u u u u u u u 3.900B U 6. 7J U HtiHOD BLANK ug/l u u u u 7 = ' U u u ".8 J U U U U IT U u u D 2.0J U D U U U ^.9J U U HDL 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 • 10 10 10 Analyzed by GC/MS Method 625. y<is^^</iyf 301406 INDUSTRIAL - CORROSION ^MANAGEMENT INCORPORATED NJDEP Certified Drinking Wacer/Vascewac« Laboracory IDtf 14116 REPORT DATE: April 16. 1986 LAB i 5295A .1152 ROUTE 10. RANOOLPH. NEW JERSEY 07869 201-584.0330 CLlENT: ENVIRO SCIENCES - Island Chemical Project SAMPLE SOURCE: Samnle #1 SAMPLE DATE: February 28... 1986 TAKEN BY: A. Kvles AT LAB DATE: M.arch 7, 19S6 LABORATORY ANALYSIS RZPORT PARAMETER RESULT Benzoohenone Neat Benzoohenone If you should have any questions, please do not hesitate,to call. INDUSTRIAL CORROSION MANAGEMENT, INC, Ritf^ard S. L^v President RSL:dlh y<^£(.4s^i' 301407 INDUSTRIAL CORROSION MANAGEMENT INCORPORATED NJDEP Certified Drinking Water/wasravace: Laboracory IDif 14116 . .... ' RZPORT DATE: April 14. 19^6 LAB 9 52954 .1152 ROUTE 10. RANOOLPH. NEW JERSEY 07869 201-584-0330 CLIENT:-ENVIRO SCIENCES - Island Chemical Project SAMPLE SOURCE: Samole #1 SAMPLE DATE: Februarv.28, 1986 TAKEN BY: A. Kyles AT LAB DATE: M.arch 7. 1986 LABORATORY ANALYSIS REPORT P.ARAMETER Ignitability Specific Gravity — pH(units) RESULT Ignites without persistent burr 21.97 8.06 ng If you should have any questions, please do not hesitate co call. INDUSTRIAL CORROSION MJ^AGEMZNT, INC. lichard S President RSL:dlh 301408 ynyc'n^/i!' S & W WASTE, INC. 115 JACOBUSAVE. . SOUTH KEARNY, N.J. 07032. (201)344-4004 GENERATORS WASTE MATERIAL PROFILE SHEET APPROVAL COOE TECHNICIAL REP. INITIALS GENERAL INFORMATION C£iZ)^-lo-'Sn GENERATOR NAME - / ^ S ^ " ^ ^ Cyr<*ff''e/i£.. C t J ^ ^ i id"^'/ GENERATOR EPA LD. NO. Y'^/Z 9P(/>&r/a<?r ADDRESS ^fcg? (Z77S- <Zyyy.ysr>?y*jTZD _ J r - . ^ ^ ^ , ^ y j l j ^ C o / ^ o MuuMtsa ' — ^ ~ :^_ - ^ / : •- ^ i — r : TECHNICIAL CONTACT / ^ A Z . A t S l - ^ Jc^cy/c^ J c ^ ^ ^ c ^ . y . ^ y - y - y • • . . WASTE NAME, Af^y^^^y-*"!^ ^ t y c * ! " ^ yZptyye . ^ / C S - ' — — i — — TITLE. vr PROCESS GENERATING WASTE /ZZ-Z'^Ki'^i^ ^ ^ Z ) a PHONP ^ C / / ^ 6 - < Z : ' B, PHYSICAL CHARACTERISTICS OF WASTE PHYSICAL STATE @ 70"F C SOLID "^LIQUID • SEMI-SOLID C POWDER t LIQUID %H2D ODOR y ^ , t . ^ C/y.. COLOR G'ORGANIC ^INORGANIC n CHLORINATED ORGANIC BTU VALUE PER GAL. % CL_ BS4W. %ASH. % S, LAYERS D MULTI LAYERED D BI-LAYERED "^SINGLE PHASED TOC. COD. •H. SOUPS y y r n ^ pH: • 0-2 D 7.1-10 n N/A D 2.1-4 D 10.1-12.5 D 4.1-6.9 D>12.5 ^ ^ ^ f i , 0 7 n C5rArT ' • ~ ^ • EXACT. SPECIFIC GRAVITY C <.8 D J-.9 0 5 5 D .95-1.0 • 1.0-1.1 • 1.1-1.24 D 1.25-1.4 D 13-1.7 D>1.7 • EXACT. c. 9S/9 OFLASH G POINT am OCC • OC G EXACT. • <90 • <100 G 1OO-140 O 140-200 "D <200 .VlSCOSmr (Centipois S'l-ioo • 100-1000 • 1000-10000 • >iaooo C EXACT C H E M I C A L C O M P O S m O N (MUSTTOTAL 100%) % y ^ • ^ 7 ^ ^ D. METALS Ag As A ^ ' D TOTAL y ./Ay^ Ba C(j Cr Cu OTHER. yA/\ y A y ZML JiAL D EPTOX Hg. Ni yyy^ Pb r / A Se / / f l . 2n y y / l TP yyy^ E. D D D a D D D D D OTHER COMPONENTS PCB'S* ' PESTICIDES/HERBICIDES* _ _ _ _ _ CYANIDE OR CYANIDE PRODUCING . SULFIDE OR SULFIDE PRODUCING _ PHENOLICS ^ RADIOACTIVE INFECTIOUS \ZK. Z^Z yK. A ^ y A ELEMENTAL METALS*_ OTHER. yK. •ATTACHED DISCLAIMERS MUST BE SIGNED AJA^ F. HAZARDOUS CHARACTERISTICS: TOXICITY RATINGS INHALATION DERMAL ORAL . D EXPLOSIVE D WATER REACTIVE • MSDS ATTACHED NFPA RATING y ^ O T l / E ' D PYROPHORIC D SHOCK SENSITIVE G. M A N I F E S T I N F O R M A T I O N j . j . PROPER DOT SHIPPING NAME / ^ l ^ - ^ ^ g ^ A y / y x . A/t:cy,r, Ay DOT HAZARD CLASS _ UN/NA NO y'AA- < p / ^ y ~ ^ WJ? EPA/STATE WASTE TYPE. EPA/STATE HAZARD CODE. "25^Z _y_ H. SHIPPING INFORMATION D8ULKL/0UID DBULKSOLID "JXDRUMS SHIPPING FREQUENCY: QUANTITY DOTHER / p g R c-*<y^— I. SPECIAL HANDUNG INFORMATION/COMMENTS: I HEREBY CERTIFY THAT ALL INFORMATIl ARE REPRESENTATIVE OF THE WASTE. DATE L ATTACHMENTS ARE COMPLETE ANO ACCURAT, SAMPLES SUBMITTED TITLE GENERATOR'S SIGNATURE 301409 Poiychiorinated Biphenyi (PCB) Warranty •^his disclaimer is to all persons who generate and dispose of chemical waste. The terms PCB and CB's are used in this disclaimerto refer to any chemical substances and combinations of substan- ces that contain 50 ppm orgreater of PCB's as defined in 40 CFR 761.3 (s), including any byproduct, in a process which contains less than 50 ppm PCB because of any dilution; again, these lattershall be included as PCB and PCB's. Substances that are regulated by this rule include, but are not limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and other chemical substances or combination of substances, including impurities and byproducts. It is unlawful for S&W Waste, Inc. to receive PCB's. Any generator and/or transporter who knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal prosecution. hereby warrants that materials transferred by it to S&W Waste, Inc. for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl (PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby agrees to idemnify and hold S&W Waste, Inc harmless from any costs, damages or other liability resulting from the breach of this warranty. DATED: BY: WITNESS:. Herbicide/Pesticide Warranty T ^ r V s i T ^ Ccmv.(r(TL rPi:<.tferehy warrants that material transferred by it to S&W Waste, Inc. fortransportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level greaterthan 0.001% when measured in each container or vessel transferred to S&W Waste, Inc., and hereby agrees to indemnify and hold S&W Waste, Inc. harmless from any costs, damages or other liability resulting from the breach of this warranty. ' X ^ L N Z } ) (Zd^Q^iZRp.^ ( j l ~fOC. 3-5^^^ . . . ^ U [LlZy,.t DATED:. WITNESS: Aluminum and Reactive Metal Warranty J - S l j f V J ^ C[inZ)\(C(^ CfpyTy^C hereby warrants that material offered to S&W Waste, Inc. for transportation, treatment and/or disposal does not contain elemental aluminum or reactive metal paste, powder or pigmentandherebyagreestoidemnify and holdS&WWaste, Inc. harmless *''om any costs, damages, or other liability resulting from breach of this warranty. _ ^^ xsLf^isit^ ctt^Hcrj^ co,/-roc DATED: _ i l _ _ _ " nv ^ r A x J i A u U ^ T ^ Ak^yy^ze:^^ WITNESS: 301410 TABLE 1.4 30870-0705 ENVISOSCIHNCBS Saaple Identification: ALAE 64S70 PCB Isomer Res--ilt. v.^.^': PCB 1016 <0.20 PCB 1221 " <0.20 PCB 1232 <0.20 PCB 1242 , <0.20 PCB 1248 ' <0.20 PCB 1254 <0.20 PCB 1260 <0.20 301411 YWC. INC. • 200 Monroe Turnpike • Monroe. Connecticut 06468 • (203) 261-iU58 S & W WASTE, INC. 115 JACOBUSAVE. . SOUTH KEARNY. N.J. 07032. (201)344-4004 GENERATORS WASTE MATERIAL PROFILE SHEET APPROVAL CODE TECHNICIAL REP. INITIALS A. GENERAL INFORMATION C/kyl) ^ - - A d S "> GENERATOR K..MC Z Z I c ^ ^ k ^ ^ ^ ^ i ^ ^ J S ^ - J ^ ^ j ) _ ^ GENERATOR EPA I.D. UO.lA'J> ' ^ f i ^ T / a ? ^ ADDRESS ^^ZSK^ (Z'y'yi^ ky^y^S/T^^J^^^ , J r . (Zk^-yy (y^KT jfofZO TECHNICIAL CONTACT A Z ^ - ^ ^ ^ / ^ - ^ / ^ t - ^ > / C > ^ g ^ - - ^ WASTE NAME A f 4 . T y . y f ^ ^ u T s y ' ^ A k ' s V / P ( A / c f ^ TITLE. VA' PHONE _ £ C y ^ 6 2 5 ^ r X PROCESS GENERATING WASTE y l ^ i T T i ^ B. PHYSICAL CHARACTERISTICS OF WASTE PHYSICAL STATE @ 7 0 T D SOLID ' ^ I Q U I D a SEMI-SOLID D POWDER % LIQUID %H20 ODOR ,y>fy<~o COLOR ^ORGANIC D INORGANIC D CHLORINATED ORGANIC BTU VALUE PER GAI (/yy:/<C/.An<.nr) % CL_ BS4W_ %ASH, % S . LAYERS a MULTI LAYERED X'BI-1-AYERED D SINGLE PHASED TOC. COO. <»> SOUDS y y < ' ^ < - ' pH: nO-2 D 7.1-10 D N/A D 2.1-4 C 10.1-12.5 • 4.1-6.9 0 1 2 . 5 . p , D 7 n P Y a r r G - ' ' SPECIFIC GRAVITY n <.8 • .fl-.9 • .9-.95 D .95-1.0 D 1.0-1.1 D 1.1-1.24 • 1.25-1.4 D 1.5-1.7 0 1 . 7 D EXACT_ y. e 6 D FLASH • POINT • CF) DCC • OC • EXACT. • <90 • <100 • 100-140 • 140-200 • <200 yiSCOSmr (Centipoise) X'-ioo C 100-1000 G 1000:10000 OI'OOOO C EXACT C. CHEMICAL COMPOSITION (MUSTTOTAL 100%) % AA/cZAac/^rL O r L y 7 . 6 ~Z7ZZkJ. /Zi/'ATT^ F2tf^ D. Ag As Ba Cd Cr Cu OTHER. METALS n TOTAL A m — yZ/Z y j A yZTT yZ/iZ^ : ^ ZUTT D EPTOX Hg Ni Pb . Se Zn Te Ai/A ^/K. y y y y/£- yjA. A ^ F. HAZARDOUS CHARACTERISTICS: TOXICITY RATINGS INHALATION DERMAL ORAL D EXPLOSIVE D WATER REACTIVE Q MSDS ATTACHED yA//? NFPA RATING D PYROPHORIC D SHOCK SENSITIVE G. MANIFEST INFORMATION PROPER DOT SHIPPING NAME AA?'- :7/:ocu:. c','=-/rz yucw/c DOT HAZARD CLASS C / ^ y f f - ^ UN/NA NO. y A y : - 9 / ^ ^ ? EPA/STATE WASTE TYPE EPA/STATE HAZARD CODE. tPeSay 2 h r ^ / . / ; ^ = ^ H. SHIPPING INFORMATION D BULK LIQUID DBULKSOLID )g^RUMS G OTHER SHIPPING FREOUENCY: QUANTITY _ _ _ Z _ _ PER _£21«£- E. a D D D D D D D D OTHER COMPONENTS PCB'S* A t ^ PESTICIDES/HERBICIDES* yV/' CYANIDE OR CYANIDE PRODUCING yV/! SULFIDE OR SULFIDE PRODUCING AJA PHENOLICS y / A RADIOACTIVE. INFECTIOUS _ yyy7_ yzz^ ELEMENTAL METALS*_ OTHER. y A •ATTACHED DISCLAIMERS MUST BE SIGMED yZA_ I. SPECIALHANDUNG INFORMATION/COMMENTS: I HEREBY CERTIFY THAT ALL INFORMATION SUBMITTED ABOVE ANO ALL ATTACHMENTS ARE COMPLETE ANO ACCURATE. ANO THAT ALL SAMPLES SUBMITTED ARE REPRESENTATIVE OF THE WASTE. DATE TITLE GENERATOR'S SIGNATURE 301412 Poiychiorinated Biplienyi (PCB) Warranty "^his disclaimer is to all persons who generate and dispose of chemical waste. The terms PCB and r'CB's are used in this disclaimerto referto any chemical substances and combinations of substan- ces that contain 50 ppm orgreaterof PCB's as defined in 40 CFR 761.3 (s), including any byproduct in a process which contains less than 50 ppm PCB because of any dilution; again, these latter shall be included as PCB and PCB's. Substances that are regulated by this rule include, but are not limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and other chemical substances or combination of substances, including impurities and byproducts. It is unlawful for S&W Waste, Inc to receive PCB's. Any generator and/or transporter who knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal prosecution. hereby warrants that materials transferred by it to S&W Waste, Inc. for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl (PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby agrees to idemnify and hold S&W Waste, Inc. harmless from any costs, damages or other liability resulting from the breach of this warranty. DATED: : BY: WITNESS: Herbicide/Pesticide Warranty J^'yU'ZZi CrXa^.i/fryr:^ .Z^j^&rehy warrants that material transferred by it to S&W Waste, Inc. fortransportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level greaterthan 0.001% when measured in each container or vessel transferred to S&W Waste, Inc., and hereby agrees to indemnify and hold S&W Waste, Inc. harmless from any costs, damages or other liability resulting from the breach of this warranty. XSij^iMT^ C t r t ^ l C / " ^ CO ~<uC. DATED:. 3-3i-n ,.-.^sk±lkA: • ^ r . \ g W ^ y^.yyyAC WITNESS:. '' yj^y/T^^- y \ y ( , y ^ - ^ y Aiuminum and Reactive IVIetal Warranty '^ZAyyFZ^ C^pA\f{Z\^ ^ . T / I ^ k hereby warrants that material offered to S&W Waste, Inc. for transportation, treatment and/or disposal does not contain elemental aluminum or reactive metal paste, powderorpigment and hereby agrees to idemnify and hold S&W Waste, Inc. harmless from any costs, damages, or other liability resulting from breach of this warranty. XSLAMIi CH©n[C/^ co.^rf^c 3-^'-^^ , BY:J^eki-Ly^ DATED WITNESS: . y^A^^AAZy 301413 INDUSTRIAL CORROSION MANAGEMENT INCORPORATED NJDEP Cercified Drinking Wacer/Vasteuace: Laboracory IDif 14116 . __* REPORT DAIE: April U , 1986 LAB H 52956 1152 ROUTE 10. RANOOLPH. NEW JERSEY 07863 201-584-0330 CLlENT: ENVIRO SCIENCES - Island Cheaical Projecc SAMPLE SOURCE: Sample #3 S.\MPLE DATE: Februarv «£8, 1986 T.^CZN BY: A. Kvles AT LAB DATE: March 7, 19 = 6 LABORATORY ANALYSIS RZPORT PARA-^TER Flashpoinc Specific Gravicy pH(unics) RESULT GT 95'C boiled @ 95°C 0.9319 7.i4 If you should have any quescions, please do noc hesicace Co call. INDUSTRIAL CORROSION MANAGEMENT, INC. RSL:dlh GT=Greacer Than Richard S. Ee'v^ne Presidenc 301414 yfy-y<s- 6 i y 7 a TABLE 1.3 30870-0705 ENVHtOSCIBNCBS SaaiJle Identification: ALAE 64869 PCB Isomer R e sill t. mff.^ll? PCB 1016 PCB 1221 PCB 1232 PCB 1242 PCB 1248 PCB 1254 PCB 1260 3.0 3.0 3.0 3.0 3.0 3.0 3.0 301415 YWC INC. • 200 Monroe Turnpike • Monroe. Connecticut 06^8 • (203) 261-A^S INDUSTRIAL CORROSION MANAGEMENT INCORPORATED J 1152 ROUTE 10, RANDOLPH. NEW JERSEY 07869 201 •584-0330 Augusc 13, 1986 Mr. Al Kyles ENVIRO SCIENCES INC. 610 Wesc Main Screec ...... . Rockaway, NJ 07866 RE: Island Chemical Project - Flashpoincs Dear Mr. Kyles: Upon your requesc chree sa:=?les from Island ChemicaK Sample dace: 2/28/86) have been reanalyzed for Flashpoint using a Pensky-Martens Closed Tester. Sanpls ?5 (Labi? 52958) and Sample a'7(Lab-? 52960) were composited and analyzed on August 7, 1986. The composite boiled at SZ'C. The original results reported(Report date: March 7, 1986) were Sample #5 - 40°C duplicace ^ T C and Sample H 7 - Zs'C. Sa-iple #5 and v7 were originally analyzed separacely. There was insufficienc sample remaining Co reanalyze sample S5 and S7 individually.• Sample jf4(labi? 52957) was also reanalyzed on August 7, 1986. The original Flash- poinc reported for this sasple was 50''C. The reanalysis resulced in a flashpoinc of 54''C. We do not feel that the resulcs of these reanalyses are as reliable as possible since the samples-have been held for over five monchs from che dace of collection. As stated in the mechod erroneously high flashpoincs may be obtained due Co loss of volacile material. These samples were:n-Dr stored in volatile organic bottles and therefore volatiles may have been lost. We are also unsure as to the correctness of compositing hazardous waste for analysis. Enclosed please find a page from the NJDE? Field Procedures Manual, November 1985, caucioning against this practice. I have also enclosed a copy of the procedure for decermining flashpoint by Pensky- Martens Closed Tester. If you have any further-questions, please do not hesitate to call. Sincerely, INDUSTRIAL CORROSION MANAGEMENT, INC. Susan Richardson Quality Assurance Coordinator SR:dls enclosures 301416 .y}4y^6¥tf67 STATE CERTIFIED DRINKING WATER/V/ASTEWATER LABORATORY I.D. #14116 INDUSTRIAL CORROSION MANAGEMENT INCORPORATED NJDEP Certified Drinking Water/ Wastewater Laboracory ID/ U116 RZPORT DATE; April 14. 1936 LAB 3 5 29=' 1152 ROUIE 10. RANOOLPH, NEW j£j?SEY 07869 201-584-0330 CLIENT: ENVIRO SCIFJiCES - Island Chemical Proiect SAMPLE SOURCE; Sample .U-• SAMPLE DATE: Februarv 28. 1986 SAMPLED BY: A. Kvles _AT LAB DATE: y.ar:h 7. 10R6 LABORATORY ANALYSIS REPORT Paramete: **Pecroleum Hydrocarbon Result 176.000 mg/l(ppm) We thank you for this opportunicy to serve you.- If you have any quescions, please do not hesitate to call. Sincerely, INDUSTRIAL CORROSION MANAGEMENT, INC. ^/:^^!^^^uc^ lichard S./Levi;<e Presidenc RSL:dlh LT-less than . A m i **This test employs analytical mechodology which can give false posicive readings. Simply stated, this test is measuring che Carbon-Hydrogen linkage in organic molecules. While Petroleum Hydrocarbons most certainly possess chis link, a number of organic molecules (Humus, Lignin ecc.) not considered petroleum based, also possess it as well. Therefore, in order to aore correctly confirm a high reading, ic is suggested that a GC ran be additionally performed. ^The above Total Petroleum Hydrocarbon concentration may noc represenc crue pecrol hydrocarbon value as indicated by an incerference at 1745 ca-1. 301417 yftiyi ^e<tf6'L. INDUSTRIAL _ CORROSION MANAGEMENT INCORPORATED NJDEP Certified Drinking Wacer/Vastewace: Laboratory ID# 14116 REPORT DATE': April 14. 1986 LAB # 52957 1152 ROUTE 10. RANOOLPH. NHW JERSEY 07869 201-584^0330 CLIENT: ENVIRO SCIENCES - Island Chemical Project SAMPLE SOURCE: Sample #4 SA.MPLE DATE: Februarv 28, 1986 TAKEN BY: A. kvles AT LAB DATE: March 7, I9S6 LABORATORY ANALYSIS REPORT PARAMETER Flashpoint Specific Gravity pH(units) RESULT 50°C 1.0565 6.81 If you should have any quescions, please do not hesicace Co call. INDUSTRIAL CORROSION M.'^AGEMINT, INC. Xichard S./lV-fine Presidenc' RSL:dlh 301418 ,i<./)£<iii*''i , S & W WASTE, INC. 115 JACOBUS AVE. . SOUTH KEARNY. N.J. 07032. (201)344-4004 GENERATORS WASTE MATERIAL PROFILE SHEET APPROVAL CODE TECHNICIAL REP. INITIALS I. GENERAL INFORMATION GENERATOR MAI^F y S C / h ^ klYy^/Cec/Jy^ ( j ADDRESS ^ : : e ^ g 7 ? S (Zyy/?/jrr:>afj7ZD , J r ZUr*^ . GENERATOR EPA LD. NO. A/£_£.£^L^uZyC?T TECHNICIAL CONTACT WASTE NAME. y^Lz*f yZ. /AZyzu^ Cky/iy/yjc JiayyueA TITLE //fyTygyuti.^ Z^MifZ^ >c/g^.ie y y c ^ ^ - V/> PROCESS GENERATING WASTE A y < Z 7 y ^ PHONE ,^£AZ^£zLk^^^^ B. PHYSICAL CHARACTERISTICS OF WASTE PHYSICAL STATE @ 70°F • SOLID ^LIQUID n SEMI-SOLID C POWDER % LIQUID %H20 ODOR 'yrfycy> I'V'ORGANIC i J :: INORGANIC COLOR C/<i^y~.//Sy^<v^<^t^ D CHLORINATED ORGANIC BTU VALUE PER GAL G U^/t/^a*<- ««> CL_ BS4W_ %ASH. ;X •fcS . LAYERS 0 MULTI LAYERED D BI-LAYERED JSlSINGLE PHASED TOC. COD. '>*! SOLIDS yiZ^Ty^ pH: co-2 D 7.1-10 C 2.1-4 •10.1-12.5 • 4.1-6.9 • > 1 2 J • 7 • EXACT • N/A <'7 SPECIFIC GRAVITY • -ca D .a-.g • .9-.95 • .95-1.0 • 1.0-1.1 • 1.1-1.24 • 1.25-1.4 a 1.5-1.7 n FXArT ^ • FLASH • POINT DCF) • CC • • OC • EXACT_ • <90 • <100 • 100-140 • 140-200 • <200 9/'<: \ ^ p O S m r (Centipois*) ^ 1 - 1 0 0 C 100-1000 • 1000-10000 • >iaooo • EXACT CHEMICAL COMPOSITION (MUSTTOTAL IOO%) % 'y-t^:&iruyiy^ /yyc/^u:=^ < r o . o t T O / D. Ag. As. Ba. Cd. Cr_ Cu. METALS D TOTAL W/Z 'TJTT y/A ~yJAZ OTHER. y/y. D EP TOX Hg Nl Pb Se Zn Te yJA y y A y j y ; yyyr yUA AZK. E. D a D Q D D D D G OTHER COMPONENTS PCB'S* PESTICIDES/HERBICIDES* CYANIDE OR CYANIDE PRODUCING. SULFIDE OR SULFIDE PRODUCING _ PHENOLICS . RADIOACTIVE INFECTIOUS _ yZAT ~^Z Z^HL .AyA ELEMENTAL METALS'_ OTHER. Z^/1 yyA •ATTACHED DISCLAJMEHS MUST BE SIGNED F. HAZARDOUS CHARACTERISTICS: TOXICITY RATINGS INHALATION DERMAL ORAL D EXPLOSIVE D WATER REACTIVE D MSDS ATTACHED y/// NFPA RATING D PYROPHORIC a SHOCK SENSITIVE G. MANIFEST INFORMATION - J y. PROPER DOT SHIPPING NAME ^ r y u A ^ ^ ^ (Z/yyT^ y Z y S i y r o / i / u ^ DOT HAZARD CLASS _ UN/NA NO. y^AA o y y f / ' € ' ^y,r? EPA/STATE WASTE TYPE . Z c ^ V ^ EPA/STATE HAZARD nODF ^ W v yL. H. SHIPPING INFORMATION D BULK LIQUID DBULKSOLID " ^ DRUMS G OTHER SHIPPING FREQUENCY: QUANTITY - ^ ^ P=R C-fc^ I. SPECIALHANDUNG INFORMATION/COMMENTS: I HEREBY CERTinr TMAT AtL INFOI ARE REPflESENTATlVE OF THE WAS' •3~-|D''^7 DATE 3RI|0»T10N SUBMlfTEBlABOVE ANA AU. ATTACHMENTS ABE COMPLETE ^^^^fci y^ ' T I T L E I GENERATOR'S SIGNA' AND ACCURATE. AND THAT ALL SAMP_ES SUBMITTED 301419 Polychlorinated Biphenyl (PCB) Warranty is disclaimer is to all persons who generate and dispose of chemical waste. The terms PCB and JB's are used in this disclaimerto referto any chemical substances and combinations of substan- ces that contain 50 ppm orgreater of PCB's as defined in 40 CFR 761.3 (s), including any byproduct, in a process which contains less than 50 ppm PCB because of any dilution; again, these latter shall be includec as PCB and PCB's. Substances that are regulated by this rule include, but are not limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and other chemical substances or combination of substances, including impurities and byproducts. It is unlawful for S&W Waste, Inc. to receive PCB's. Any generator and/or transporter who knowingly or willfully ships-PCB's to our facility will be subject to civil penalties or criminal prosecution. hereby warrants that materials transferred by it to S&W Waste, Inc. for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl (PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby agrees to idemnify and hold S&W Waste, Inc. harmless from any costs, damages or other liability resulting from the breach of this warranty. DATED: BY:. WITNESS: Herbicide/Pesticide Warranty T S L I ^ V J ^ C^^^'^'lCf^^CQilXZherehy warrants that material transferred by it to S&W Waste, Inc. for transportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level greater than 0.001% when measured in each container or vessel transferred to S&W Waste, Inc., and hereby agrees to indemnify and hold S&W Waste, Inc. harmless from any costs, damages or other liability resulting from the breach of this warranty. 3:su/VOi>CCiO^.(C'^t\_ 0D<. X•^Xl. DATED: I ' ^ J - ^ BY: i 4 4 v . A f k ai'Tr WITNESS: Aluminum and Reactive Metal Warranty " T ^ \ . N ^ r.m^Ai/^ftV- (^. X A ^ . hereby warrants that material offered to S&W Waste, Inc. for transportation, treatment and/or disposal does not contain elemental aluminum or reactive metal paste, powder or pigment and hereby agrees to idemnify and hold S&W Waste, Inc. harmless ^^om any costs, damages, or other liability resulting from breach of this warranty. — y DATED:_llill^3 . BY: J ^ c W K ^ ^ ^ f c ; ! WITNESS: 301420 TABLE 1.0 30870-0705 ENVIROSCIENCES SajnT3le Identification: MARE 64980 PC3 Isomer PCB 1016 PCB 1221 PCB 1232 PCB 1242 PCB 1248 PCB 1254 PCB 1260 Result. ug./L <0.20 <0.20 <0.20 <0.20 . <0.20 <0.20 <0.20 301421 YWC. INC. • 200 Monroe Turnpike • Monroe. Connecticut 06^66 • (203) 261-4.458 G' INDUSTRIAL CORROSION MANAGEMENT INCORPORATED 1152 ROUTE 10. RANOOLPH. NEW JERSEY 07869 :01-5S4.0330 Augusc 13, 1986 Mr. Al Kyles ENVIRO SCIENCES INC. 610 Wesc Main Screec ...... Rockaway, NJ 07866 RE: , Isiand CheTsical Pro j ecc - Flashpoincs Dear Mr. Kyles: Upon your requesc chree samples from Island ChemicaK Sample dace: 2/28/86) have been reanalyzed for Flashpoinc using a Pensky-Marcens Closed Tescer. Sanple r5 (Lab// 52958) and Sample #7(Lab# 52960) vere composiced and analyzed on Augusc 7, 1986. The composice boiled ac 98°C. The original resulcs re?orced(Reporc dace: March 7, 1986) were Sample #5 - AO'C duplicace UVC and Sample il 7 - A5'C. Sample i;5 and #7 were originally analyzed separacely.' There was insufficienc sample remaining Co reanalyze, sample #5 and #7 individually. j (. : Sample i^4(labi? 52957) was also reanalyzed on Augusc 7, 1986. The original Flash- poinc reporced for chis sairole was 50*C. The reanalysis resulced in a flashsainc of 54'C. - ' We do noc feel chac che resulcs of chese reanalyses are as reliable as possible since Che samples have been held for over five monchs from che date of colleccion. As seated in che mechod erroneously high flashpoincs may be obtained due to loss of volacile material. These samples were:ntj£ stored in volatile organic bottles and therefore volatiles may have been lost. We are also unsure as to the correctness of compositing hazardous wasce for analysis. Enclosed please find a page from the NJDEP Field Procedures Manual, November 1985, caucioning against this practice. I have also enclosed a copy of the procedure for decermining flashpoinc by Pensky- Marcens Closed Tester. If you have any further questions, please do not hesitate to call. Sincerely, INDUSTRIAL CORROSION MANAGEMENT, INC. Susan Richardson Quality Assurance Coordinacor SR:dls ( • ! enclosures STATE CERTIFIED DRINKING WATER/WASTEV/ATER LABORATORY I.D. #14116 y*f/l/ZCCHf9S^ 301422 INDUSTRIAL CORROSION MANAGEMENT INCORPORATED NJDEP Certified Drinking Wacer/Vascewace: Laboracory ID# 14116 RZPORT DATE; April 14,, 1986 LAB S 5296G 1152 ROUTE 10. RANDOLPH. NEW JERSEY 07869 201-584-0330 CLIENT: ENVIRO SCIENCES - Island Chemical Projecc SAMPLE SOURCE: Samnle #7 SAMPLE DATE: February.28. 1986 TAKEN BY: A. Kvles AT LAB DATE: March 7. 1985 LABORATORY ANALYSIS REPORT PARAliETER RESULT Flashpoinc Specific Gravicy pH(units) 45°C 1.0836 5.05 If you should have any questions, please do not hesitate to call. INDUSTRIAL CORROSION MANAGEMENT, INC. RSL:dlh Tchard S. Lk^ resident ^ i / j A * : ^ vTAe 301423 yafyty rt> 4 . ^ i ^ INDUSTRIAL CORROSION MANAGEMENT INCORPORATED NJDEP Certified Drinking Wacer/Vascevace- Laboratory ID? 14116 REPORT DATE: April 14, 1986 LAB? 52958 1152 ROUTE 10. RANOOLPH. NEW JERSEY 07869 201-584.0330 CLIENT: ENVIRO SCIENCES - Island Chemical Proiecc SAMPLE SOURCE: Sample #5 SA.MPLE DATE: Februarv JJ8, 1986 TAKEN BY: A. Kvles AT LAB DATE: March 7, 15S6 LABORATORY ANALYSIS REPORT PARAMETER RESULT •CS Flashpoint 40°C 41*0(dup) Specific Gravicy 1.0206 pH(units) — 4.51 If you should have any quescions, please do not hesitate to call. INDUSTRIAL CORROSION MANAGEMENT, INC. RSL:dlh Richard S President A 301424 ^ A C C 6<-'Jt'' INDUSTRIAL --- CORROSION - MANAGEMENT INCORPORATED 1152 ROUTE iO. RANOOLPH. NE"W JERSEY 07869 201-584-O330 NJDEP Cercified Drinking Wacer/ Wastewater Laboracory LD# 14116 REPORT DATE: April 14. 1035 LAB i 52958 CLIENT: ENVIRO SCIENCES - Island Chemical Proiect SAMPLE SOURCE: Sample J?5 SAMPLE DATE: February 28. 1986 SAMPLED BY: A. Kvles _AT LAB DATE: Msr:h 7. 1986 LABORATORY ANALYSIS REPORT Paramecer **Pecroleum Hydrocarbon Resulc LT 5 mg/l(ppm) We thank you for this opportunicy to serve youl If you have any quescions, please do not hesicace to call. Sincerely, INDUSTRIAL CORROSION MANAGEMENT, INC. lichard S./leviXe Presidenc RSL:dlh LT"less than **This test employs analytical methodology which can give false positive readings. Simply scaced, this test is measuring the Carbon-Hydrogen linkage in organic molecules. While Pecrcleum Hydrocarbons mosc cercainly possess chis link, a number of organic molecules (Humus, Lignin etc.) not considered petroleum based, also possess it as well. Therefore, in order to more correctly confirm a high reading, it is suggested that a GC run be additionally performed. ^The above Total Petroleim Hydrocarbon concentration may not represent crue pecrol hydrocarbon value as indicaced by an interference at 1745 cm-l. 301425 ^ y t / c e " G^flfO INDUSTRIAL CORROSION MANAGEMENT INCORPORATED NJDEP Cercified Drinking Water/ Wascewacer Laboracory IDt 14116 REPORT DATE: Anrll 14. 1986 LAB S 52960 1152 ROUTE 10. RANOOLPH. NEW JERSEY 07869 201-584-0330 CLIENT: ENVIRO SCIENCES - Island Chemical Proiect SAMPLE SOURCE: Sample 47 SAMPLE DATE: February^ 28. 1986 SAMPLED BY: A. Kvles AT LAB DATE: Mar:h 7. I9{ LABORATORY ANALYSIS REPORT Parameter **Pecroleum Hydrocarbon Resulc 100 mg/l(ppm) We thank you for this opportunity to serve you'. If you have any questions, please do not hesitate to call. Sincerely, INDUSP.IAL CORROSION MANAGEMENT, INC. Aichard S./ievi;(e Presidenc J RSL: dlh LT-less than **This test employs analytical mechodology which can give false positive readings. Simpl: stated, this test is measuring the Carbon-Hydrogen linkage in organic molecules. While Petroleum Hydrocarbons most certainly possess this link, a number of organic nolecules (Humus, Lignin etc.) not considered pecroleum based, al.«?o possess ic as well- Therefore, in order to more correctly confirm a high reading, it is suggested that a GC run be additionally performed. The above Total Petroleum Hydrocarbon concentration may not represenc true pecro hydrocarbon value as indicated by an interference at 1745 cm-1. 301426 / n y i j i t y 6 < ' J f ° S & W WASTE, INC. 115 JACOBUSAVE. . SOUTH KEARNY, N.J. 07032. (201)344-4004 GENERATORS WASTE MATERIAL PROFILE SHEET APPROVAL CODE TECHNICIAL REP. INITIALS .. GENERAL INFORMATION ^4^^^ "/O'^'^y/ GENERATOR NAME. -2^^^^^^ y^fyTfyCS,, d>, ADDRESS. ^ ^ GENERATOR EPA LD. NO. \ZZ^_2if^Syo^r~ yis!:*i' (s-A?S k k y l y j / f ^ T ^ ^ S r <Z/Zyr.Ay / / S V / g t e ^ ^ o TECHNICIAL rnNiT^rT y ^ ' > ^ / • / ^ ^ » g ^ / ' C f y r r - e J O U ^ U C A ) WASTE NAME />^.e<<Zy<^ <:yyyy:7ZZ J ^ / y ^ < ^ ^ TITLE. vy P H O N F - ^ g / A ^ ^ - g - Z J - Z . PROCESS GENERATING WASTE. /yyryy^ADu/yy B. PHYSICAL CHARACTERISTICS OF WASTE PHYSICAL STATE © 7 0 T ^ S O U I D C; LIQUID D SEMI-SOLID O POWDER to LIOUID '><.H20 ODOR y j f ^ C t O . / ^ . ^ C y c '^ORGANIC C INORGANIC COLOR 2 < i , S U ^ • CHLORINATED ORGANIC BTU VALUE PER GAI ( / y . f K / / C U ^ «*> C L _ BS«W_ % A S H . % S . LAYERS / ( / / C MULTI LAYERED G BI-LAYERED • SINGLE PHASED TOC. COD, y/y? <K) SOLIDS. pH: DO-2 D 7.1-10 D 2.1-4 D 10.1-12.5 D 4.1-6.9 0 1 2 . 5 D 7 O EXACT _ D N/A SPECIFIC GRAVITY ~ J-.9 D .9-.95 2.95-1.0 O 1.0-1.1 D 1.1-1.24 a 1.25-1.4 D l i - 1 . 7 • >1.7 < . - t t ' y O EXACT _ £ £ : L i _ D FLASH n POINT DTF) D C C D O C DEXACT. D < 9 C D < 1 0 0 D 100-140 D 140-200 X y t 2 0 0 VISCOSnY (CentiooiM) C 1-100 C lOC^lOOO • 1000-10000 o i a o o o j r , y C S X A C T ^ y Z Z L C H E M I C A L C O M P O S I T I O N (MUSTTOTAL ioo%) % j ^ * * Zcy'Af£/^<^tL, \ <JtO yZ/^^v^yr ZL^ •:y/y^A:<^£ey ^ / 2 - 7 ^ ^ „ A \ D . M E T A L S nTOTAL Ag y A A A^ yy/: Ba Cd Cr Cu OTHER. yy/i yyy: y / A a E P T O X Hg. A M Ni. Pb 'Zn ^ A T P / t A yi/A OTHER COMPONENTS PCB'S* A / / . PESTICIDES/HERBICIDES*. E, D D D D a D a D ELEMENTAL METALS*_ D OTHER. .^J/L y / A y l ^ CYANIDE OR CYANIDE PRODUCING . SULFIDE OR SULFIDE PRODUCING . PHENOLICS ^ y/A... RADIOACTIVE INFECTIOUS A/A y Z / ^ .yi^iSL y / A •ATTACHEO DISCUUMERS MUST BE SIGNED F. HAZARDOUS CHARACTERISTICS: TOXICITY RATINGS INHALATION DERMAL ORAL n EXPLOSIVE a WATER REACTIVE G MSDS ATTACHED y A NFPA RATING D PYROPHORIC D S H O C K SENSITIVE G. MANIFEST INFORMATION PROPER DOT SHIPPING NAME y-/,7MCe.fii, c U y i Z r A . / y y ^ DOT HAZARD CLASS ^ S ^ ^ UN/NA NO / i A / f ~ 9ycP7 EPA/STATE WASTE TYPE EPA/STATE HAZARD CODE. ^-^Sf y H. SHIPPING INFORMATION D BULK LIQUID CBULKSOLID X^DRUMS C OTHER. SHIPPING FREOUENCY: QUANTITY__Z___ PER. OT..£y. I. SPECIALHANDLING INFORMATION/COMMENTS: /^^^^^gy^jyofTcz. ^cytcAJy^yjiy^ yuyZ'.j^Ayft^f^tfcy.y Jay>s^ gty*^ y;^y*<'^ yJAJJy^ ^yyATyf 1 HEREBY CEHTIFY TMAT A1.L INFORMATION^ ARE REPRESENTATIVE OF THE WASTE. [JBMITTED ABOVE ANO ALL ATTACHMENTS ARE COMPLETE AND ACCURA' . 1 - / ^ - ^ ^ TITLE ^Sm^Me^U. SAMPLES SUBMITTED 301427 GENERATORS SIGNATURE Polychlorinated Biphenyl (PCB) Warranty "• 's disclaimer is to all persons who generate and dispose of chemical waste. The terms PCB and ^B's are used in this disclaimer to referto anychemical substances and combinations of substan- ces that contain 50 ppm orgreaterof PCB's as defined in 40 CFR 761.3 (s), including any byproduct, in a process which contains less than 50 ppm PCB because of any dilution; again, these latter shall be included as PCB and PCB's. Substances that are regulated by this rule include, but are not limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and other chemical substances or combination of substances, including impurities and byproducts. It is unlawful for S&W Waste, Inc. to receive PCB's. Any generator and/or transporter who knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal prosecution. hereby warrants that materials transferred by it to S&W Waste, Inc. for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl (PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby agrees to idemnify and hold S&W Waste, Inc harmless from any costs, damages or other liability resulting from the breach of this warranty. DATED: BY:. WITNESS:. Herbicide/Pesticide Warranty ySW^-ZQ C'rtQH(C(H^^^X^^:C• hereby warrants that material transferred by it to S&W Waste, Inc. for transportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level greaterthan 0.001% when measured in each containerorvessel transferred to S&W Waste, Inc., and hereby agrees to indemnify and hold S&W Waste, Inc. harmless from any costs, damages or other liability resulting from the breach of this warranty. J ^ L / W V > CHQ^AVC/^ CO ~«CC. o...o:yyn ,.. ^^L.irUrrl wiTNF«;s / y ^ . i < y ^ y k y / j ^ ^ Aluminum and Reactive Metal Warranty I L ^ L N J O rt^GtVj^f? Q2i.1Z\AX hereby warrants that material offered to S&W Waste, Inc. for transportation, treatment and/or disposal does not contain elemental aluminum or reactive metal paste, powder or pigment and hereby agrees to idemnify and hold S&W Waste, Inc. harmless ^rom any costs, damages, or other liability resulting from breach of this warranty. _ ,^ ^ / a :c:^LAjo-^ (;^^g^^(;^ <J5 rKiC DATED: ; BY:. WITNESS: / y ^ / ^ ^ - A k y k Z ^ y y ^ t y 301428 TABLE 1.2 30870-0705 E2TVIR0 SCIENCES Sample Identification: ALAS 64867 PCB Isomer . Result • rif.'S? FC3 1016 PCB 1221 PCB 1232 PCB 1242 PCB 124S PCB 1254 PCB 1260 1.0 1.0 1.0 1.0 1.0 1.0 1.0 301429 YWC. INC. • 200 Monroe Turnpike • Monroe, Connecticut 06468 • (203) 261-4458 INDUSTRIAL CORROSION MANAGEMENT INCORPORATED NJDEP Cercified Drinking Wacer.'Vascevace: Laboracory IDi* 141L6 REPORT DATE: April 14, 1986 LAB il 52954 1152 .lOUTt 10. R;>NOOLPH. NCtV llRSey Q78£: :Ql-5a4.0330 CLIENT: ENVIRO SCIENCES - Island Chenical Proiecc SA^[?LE SOURCE: SamDle in SA>f?LE D.-i.TE: Februarv.28, 19 = 5 T.-.KEN 3Y: .-i.. KvLes .J.T L.^3 DATE: March LA30R.iT0RY ANALYSIS REPORT P.A-RA-METER Ignicabilliy - Specific Grav: pH(uniC3) RESULT ISS wichouc persis; 21.97 8f06 If you should have any quescions, please do noc hesicace co call. INDUSTRIAL CORROSION MANAGE^IE:rr, INC. lichard S. /Le^J^ne Presidenc/ RSL:dlh 301430 / l y t i i ' f / ' i ' ••.•••• PRIORITY POLLUTANT VOLATILE ORGANIC ANALYSIS '— f.'^ J I LABORATORY ID /14116 ••"•' ••••'- ' • • LAB # 52955 " - " " ' " M CLIENT: E N V I R O '^rT-vrES - I^I.T^H r>.o,. SAMPLE SOURCE Sa~ple ^2 - •-' GC/MS Method 624* Tier II Deliverables PARAMETER Chloromethane Bromomethane Vinyl Chloride --"-"- '• — Chloroethane Methylene Chloride 1,1-Dichloroethene 1 ,1-Dichloroethane Trans-1,2-Dichloroethene Chloroform 1 ,2-Dichloroethane 1 ,1 ,1-Trichloroethane Carbon Tetrachloride Bromodichloromethane 1 ,2-Oichloropropane - - Trans-1,3-Dichloropropene Trichloroethene : ; — — Dibromochloromethane 1,1,2-Trichloroethane Benzene cis-V,3-Dichloropropene 2-Chloroethylvinyl ether Bromoform Tetrachl oroethene 1,1,2 ,2-Tetrachloroethane Toluene Chlorobenzene Ethyl benzene Total Xylenes *Dichlorobenzenes noc analyzed under this method. Analyzed by GC/MS Method 625, RESULT ug/kg u u u u 7.SB U U U U u u u U u U U u 3. OB U U U U U U U u 1.295 HETriOD BLANK ug/kg IT u u 7.5 J U u u 7. 8J U U U U u u u u u 2.0J u u u u ' u t.9J U U U MDL 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 301431 /ic^<^ 6t/-^7 • INDUSTRIAL CORROSION MANAGEMENT INCORPORATED NJDEP Certified Drinking Vacer/Vastevace: Laboracory ID^ 14116 REPORT DATE: April 16. 1966 LAS S 52955 1152 ROUTE 10. RANOOLPH. NEW JERSEY 07863 201-584.0330 CLIENT: ENVIRO SCIENCES - Island Cheaical Proiect SAiMPLE SOURCE: Samole HI SAMPLE DATE: Februarv 28, 1986 TAKEN BY: A. Kvles AT LAB DATE: March 7, 155: LABORATORY ANALYSIS REPORT P.ARAMETER Z Paraphenetidene RESULT None Found FINDINGS: Seac benzophenone If you should have any questions, please do not hesicace to call. INDUSTRIAL CORROSION MANAGEMENT, INC. Rfchard S President RSL:dlh /qcy ^^f^-(''7 301432 INDUSTRIAL CORROSION MANAGEMENT INCORPORATED NJDE? Certified Drinking Vater/Vasteva-a- Laboracory ID# 14116 REPORT DATE: April 14, 1986 LAB i 52955 1152 ROUTE 10. RANOOLPH. NEW JERSEY 07563 201-584.0330 CLIENT: ENVIRO SCIENCES - Island Cheaical Proiect SAMPLE SOURCE: Sample 02 SA.MPLE DATE: Februarv 28.--1986 TA-KEN BY: A. Kvles AT LAB DATE: March 7, 19S5 LABORATORY ANALYSIS REPORT PARA.METER Ignitability Specific Gravity pH(units) RESULT Ignites without persistent burning - ' 32.47 7.38 If you should have any quescions, please do noc hesitate to call. INDUSTRIAL CORROSION MANAGEMENT, INC. RSL:dlh Presidenc y ^ C A ^ i i - f f i y -. 301433 S&W WASTE, INC. 115 JACOBUS AVE. . SOUTH KEARNY. N.J. 07032. (201)344-4004 GENERATORS WASTE MATERIAL PROFILE SHEET APO^OVAL CODS TECHNICIAL REP. INITIALS \. GENERAL INFOmwiATION C^"?])^^'! GENERATOR M A U C - Z - ^ ? ^ ^ C r T . y n ' K A / , d ) k j y . \ l " " •-) GENERATOR EPA I.D. N n k / Z 9 / ^ T r c ? ' . . p n c r Q . ; 2 s c Z ' < ^ ^ - ^ ^ ( T U y ^ r / T S x ^ J / ^ J r " C y ^ ^ : , C / J V / u^ACTPNiAMP AZka<>u/fuy..~ AyysJTZ:, /y&cy^c ' A I A ^ t:^or2.o TITLE __ / P PHONF ^C//:£6-GZZ PROCESS GENERATING WASTE. yye*-*^£-^ B. PHYSICAL CHARACTERISTICS OF WASTE PHYSICAL STATE @ 70'Fj 3 SOLID ^ L I Q U I D | C SEMI-SOLID G POWDER % LIOUID <><JH20 ODOR / c i y i a * . m j t ^ COLOR y < j i pg'ORGANlC ] 3 INORGANIC n CHLORINATED ORGANIC BTU VALUE PER G A L . c y ^ y : y t f * ^ r * i «b CL _ BS«W_ " B A S H . 9i>S. LAYERS Q MULTI LAYERED G BI-LAYERED " ^ S I N G L E PHASED TOC, COD. ifc SOLIDS y y r y y - c pH: CO-2 D 7.1-10 C 2.1-4 D 10.1-12.5 0 4.1-6.9 0 1 2 . 5 C 7 D EXACT _ D N/A ^z2Z. SPECIFIC GRAVITY D < J C.8-.9 C .9-.95 D.95-1.0 D 1.0-1.1 O 1.1-1.24 D 1^5-1.4 D li-1.7 0 > 1 . 7 D EXACT_ y-ce' • FLASH D < 9 0 C POINT • <100 G f F ) C 100-140 G CC D 140-200 D O C G EXACT: . • g . < 2 0 Q p T v r yiSCOSmr (Ceniicxjise) ^ 1 - 1 0 0 C 10O-100O C 1000-10000 . Oiaooo c EXACT CHEMICAL COMPOSITION (MUSTTOTAL 100%) % / S c ^ y ^ u ^ I y ^ e 7 ? y ^ ^ e y y y v c , ^ J ^ t7 y / , i y / D y y * f f ; 7 r / < L . / c z y / j y f - c ^ ^ O - v e ^ / D. METALS C TOTAL yyA As Ba r.fl Cr r.u y / f i yyA y y A y / A y / A DEPTOX Hg y y A Nil y y / : Ph ^ ^ SP Ayy; 7n y y A Te. y / / ^ - / - r - F. HAZARDOUS CHARACTERISTICS: TOXICITY RATINGS INHALATION DERMAL ORAL • O EXPLOSIVE D WATER REACTIVE D MSDS ATTACHED NFPA RATING y ^ c y y ^ • PYROPHORIC D SHOCK SENSITIVE G. MANIFEST INFORMATION . PROPER D O T S H I P P I N G NAMP A A i i y u , / e t x / / ' y y - J T ^ / C y f T e y / ' i y y ^ f DOT HAZARD C L A S S . UN/NA NO. y / y ^ O/Cy^e 9yf? EPA/STATE WASTE TYPE EPA/STATE HAZARD CODE. AA2.Za y H. SHIPPING INFORMATION D BULK LIQUID DBULKSOLID ' ^ D R U M S D OTHER. SHIPPING FREQUENCY: QUANTITY / _ PER jr>«ct— OTHFR Ai/A E. OTHER COMPONENTS n PCB'S* n PP=;Tir.inF';/HPPRirinF.'?» a CYANIDE OR CYANIDE PRODUCING. D SULFIDE OR SULFIDE PRODUCING n PHFNni in.<? n RAniOArrivF n iNFPCTir)u.<i n Fl FMFNTAI MFTAl 5?* n OTHFR . yJA y j A y y / : y/A y / A yyA y / A y/A y A •ATTACHED DISCLAIMERS MUST BE SIGNED I. SPECIALHANDUNG INFORMATION/COMMENTS: I HEHEBV CERTIFY THAT ALL INFORMATION SUBMITTED ABOVE AND AU. A ARE REPRESENTATIVE OF THE WASTE. 3-/0_<i-7 DATE ARE COMPLETE AND ACCURATE. AND cy€.y TITLE GENERATORS SIGNATURE SUBMITTED 301434 # Polychlorinated Biphenyl (PCB) Warranty "^his disclaimer is to all persons who generate and dispose of chemical waste. The terms PCB and JB's are used in this disclaimer to referto anychemical substances and combinations of substan- ces that contah 50 ppm orgreaterof PCB's as defined in 40 CFR 761.3 (s), including any byproduct, in a process which contains less than 50 ppm PCB because of any dilution; again, these latter shall be included as PCB and PCB's. Substances that are regulated by this rule include, but are not limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and other chemical substances or combination of substances, including impurities and byproducts. It is unlawful for S&W Waste, Inc to receive PCB's, Any generator and/or transporter who knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal prosecution. hereby warrants that materials transferred by it to S&W Waste, Inc. for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl (PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby agrees to idemnify and hold S&W Waste, Inc harmless from any costs, damages or other liability resulting from the breach of this warranty. DATED: BY: WITNESS: Herbicide/Pesticide Warranty XSvPn^'^ cw^f^^c^r^ CC\ ITi^hprehy warrants that material transferred by it to S&W Waste, Inc. for transportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level greater than 0.001 % when measured in each container or vessel transferred to S&W Waste, Inc., and hereby agrees to indemnify and hold S&W Waste, Inc harmless from any costs, damages or other liability resulting from the breach of this warranty. Zil^\^f\tZi'i> C HH$I"Ai r/?rL ce). ITkOc. HATPn- 3 - ^ l - F f RY- \ ^ ( / y , . ,~k CUgVv^' • y y y y WITNESS: ,zZ%-^.^yzZjy A Aluminum and Reactive Metal Warranty TSl^^tvv^ LAAy^\^J\\ c^ ; X K I C I hereby warrants that material offered to S&W Waste, Inc. for transportation, treatment and/or disposal does not contain elemental aluminum or reactive metal paste, powder or pigment and hereby agrees to idemnify and hold S&W Waste, Inc. harmless from any costs, damages, or other liability resulting from breach of this warranty. 3-31-H ,, yzAxCkv^ WITNESS: 301435 ^ - • w TASLE 1.1 30870-0705 EJTTISOSCIENCSS Sample I d e n t i f i c a t i o n : MARS 64981 PC3 I s o m e r R e s u l t . -^i^/L PCB 1016 <0.20 ?C3 1221 <0.20 PCB 1232 . <0.2Q PCB 1242. . «0.20 PCB 1248 <0.20 PCB 1254 <0.20 PCB 1260 <0.20 301436 YWC INC • 200 Monroe Turnpike • Monroe. Connecticut 06468 • (203) 261-^^3 INDUSTRIAL ^ ^ ^ ^ certified Drinking Wacer/Vascevace- ^ ^ ^ _ , ^ Laboracory JUtf K116 CORROSION MANAGEMENT "^'^^^ DATE: Aoni K . 1986 INCORPORATED LAS ^ 52959 1152 ROUTE 10. RANDOLPH. NEW JERSEY 07S53 201-53*^330 CLIENT: ENVIRO SCIENCES - Island Cheaical Proiect SAMPLE SOURCE: Samole #6 SA.^?LE DATE: Februarv ^S. 1986 TAKEN 3Y: A. Kvles AT LAB DATE: March 7, 19£6 LABORATORY ANALYSIS REPORT PARA-^IIR RESULT Paraphenetidene ~ Not Present Findings: chloroaethyl benzene benzene nechananuime, n,n-dimethyl If you should have any quescions, please do noc hesicace co call. DTDUSTRIAL CORROSION M.\NAGZXENT, I^'C. Richards. Livr^e Presidenc / ^/ik^"-^ RSL:dlh .-/^^n 3 01437 INDUSTRIAL CORROSION MANAGEMENT INCORPORATED 1152 ROUTE 10. RANDOLPH. NEW JERSEY 07SS3 201-58i-0230 NJDE? Certified Drinking Water/Wastevat. Laboracory ID? 14116 REPORT DATE: April U . 1986 LAB S 52959 CLIENT: ENVIRO SCIENCES - Island Chenical Proiect SAMPLE SOURCE: Samnle US SA.MPLE DATE: Februarv iS,..1986 TAKEN BY: A. KvLes AT LAB DATE: March 7, I9E6 LABORATORY ANALYSIS REPORT PARAMETER RESULT m . Flashpoint gT'C boiled 3 97'C Specific Gravicy 1.0809 pH (units) — 6:71 If you should have any quescions, please do not hesicace Co call. INDUSIXIAL CORROSION MANAGEMENT. INC. y^ RSL:dlh 301438 y ^ y y t T ^ t Z y T / S & W WASTE, IN CODE 1 5 JACOBUS AVE. . SOUTH KEARNY. N.J. 07032. (201) 344-4004| TECHMCIAL GENERATORS WASTE MATERIAL PROFILE SHEET "^^'^'^'^^^ GENERAL INFORMATION / l ^ ^ ^ - 7 4 ^ 7 GENERATOR NAMP yAh--?^/) Cy/^y?f/c:^ Cy k : ^ y . / . , / , ( ] GENERATOR EPA LD. NO. / y ^ ^foes'yo^r- ^^^, ^ . . y . /I yzz. zkkzz. ^ ADDRESS. <A^Z^.^./Zy/ys/yzy^jrc/:. Jr- Ckk'^ 0(Z\T ^ o / ^ TECHNICIAL rnvTArT / ^ ^ / Z y c U t - / ^ ^ r / y / t y i J : ^ ^ ] TITLE. y / PHONE j ^ £ v ^ £ £ - i Z . r ; ^ .'ASTE NAME. PROCESS GENERATING WASTE . y / c '(T^/C- B. PHYSICAL CHARACTERISTICS QF WASTE LAYERS y A ^ C MULTI LAYERED Q BI-LAYERED D SINGLE PHASED =HYSICAL STATE @ 70'F sfSOLIO C LIQUID Z SEMI-SOLID G POWDER ^ LIOUID 5«H20 ODOR y y o y i y t ^ " Z ORGANIC JClNORGANIC COLOR y y A : CHLORINATED ORGANIC BTU VALUE PER GAL V Cl y y A ^ % R?J.VJ <feASH yZAZ TOC. COD. % SOLIDS. DH: 0 0-2 C 7.1-10 C i 1 - 4 C 10.1-12.5 C 4.1-6.9 0 1 2 . 5 D 7 a EXACT _ > N/A SPECIFIC GRAvmr c.a-.9 C .9-.9S C.95-1.0 D 1.>1.1 C 1.1-1.24 S . 1.25-1.4 C l i - 1 . 7 C>1.7 • EXACT. a FLASH O POINT DCF) DCC C O C CEXACT. n<90 o <100 Q 100-140 C 140-200 VlSCOSiTY (CenliDOise) C 1-100 D 100-1000 G 1000-10000 D > 10.000 y y A - C EXACT _ r Z ^ % CHEMICALCOMPOSmON (MUSTTOTAL 100%) % A ^ r r L . mheyiyyf yZ/A/cer y<<Ltni^AA 7 o y^^:^^<.ga^fr^<L^ S O o.cyxy F. HAZARDOUS CHARACTERISTICS: TOXICITY RATINGS INHALATION DERMAL ORAL C EXPLOSIVE a WATER REACTIVE D MSDS ATTACHED NFPA RATING y/(>u^ D PYROPHORIC a SHOCK SENSITIVE D, Ag As Ba Cd Cr Cu O T H E R . METALj^ C TOTAL vW y A XML y y ^ y/A DEPTOX Hg Ni Pb Se Zn Te y . « ZZA^ yC*±_ y/y: y/A y y G. MANIFEST INFORMATION y _t / • PROPCRDnT.«;HippiNiRNAMFyi^^>i.iyA> /yAy^/i- J ^ ' A y / c L DOT HA2ARD CLASS € A A ' - ^ UN/NA NO. y ^ A f 9 y J ' 9 EPA/STATE WASTE TYPE EPA/'STATE HAZARD C O D E . . ^ 2 2 ^ H. SHIPPING INFORMATION C BULK LIOUID C B U L K S O L I D ^ DRUMS SHIPPING FREQUENCY: QUANTITY y7A'ZyZL €>// / COTHER. PER. g r ^ - g ^ E. D C • a n c D n D OTHER COMPONENTS PCB'S* y / / PESTICIDES/HERBICIDES' y ^ ^ cyANioe OR CYANIDE PRODUCING y / A SULFIDE OR SULFIDE PRonnCiNn yJiC PHENOLICS y-'A RADIOACTIVE. INFECTIOUS _ y/A y.'A ELEMENTAL M E T A L S * . O T H E R . y/A •*TTACHED DISCLAIMERS MUST BE SIGNED yZA_ y I. SPECIALHANDUNG INFORMATION/COMMENTS: yj/^'fCc,: /Z^c/SZZ, /k^ccaeZ, 2)^M^y^y<cy ^ ^ ^ • f ^ ^ ^ - ^ yCiyiC^y<L y2y.y;A.,y:r^y y Z Z y Z ^ l 7 ^ 'y^y.^Xy^<Z ZZ^Z/^'AI^T^, ^ yitii I HEBESY CERTIFY THAT ALL INFORMATION SUBMITTED ABOVE AN^ ARE REPRESEhTTATIVE OF THE WASTE. DATE TTACMMENTS ARE COMPLETE ANO ACCURATE, A N D T H A V A L L SAMPLES SUBMITTED kZ^t ,Z ^^<t 301439 TITLE GENERATOR'S SIGNATURE Polychlorinated Biphenyl (PCB) Warranty •^'-'is disclaimer is to ail persons who generate and dispose of chemical waste. The terms PCB and >B's are used in this disclaimer to refer to any chemical substances and combinations of substan- ces that contain 50 ppm orgreaterof PCB's as defined in 40 CFR 761.3 (s), including any byproduct, in a process which contains less than 50 ppm PCB because of any dilution; again, these latter shali be included as PCB and PCB's. Substances that are regulated by this rule include, but are not limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and other chemical substances or combination of substances, including impurities and byproducts. It is unlawful for S&W Waste, Inc. to receive PCB's. Any generator and/or transporter who knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal prosecution. I_S>LfVJT^ r VrQNA(.(l^ CohPrPhy warrants that materials transferred by it to S&W Waste, Inc. for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl (PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby agrees to idemnify and hold S&W Waste, Inc harmless from any costs, damages or^ther liability resulting from the breach of this warranty. ' X ^ L ^ ' Z O Ctt^f^^rTL. C o -HNC^ DATED: ^-(i-y . ^.^.Ckak WITNESS Herbicide/Pesticide Warranty X S L \ ^ 0 i i k ^ ' M d ' ^ (L^l^^ffirPhy warrants that material transferred by it to S&W Waste, Inc. for transportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level greater than 0.001 % when measured in each container or vessel transferred to S&W Waste, Inc., and hereby agrees to indemnify and hold S&W Waste, Inc. harmlessfrom any costs, damages or other liability resulting from the breach of this warranty. JTS t f-rAJZ) C f p ^ C l ^ L CO. ZZ.^^ DATED: _ . 5 l l h l 3 _ _ _ — RY- ^ I.LpJ^^- , 1 e ^ ^ S ^ ^ ^ i r c / . . y WITNESS: yZy^^iiy^A^ X T 'Z^yC Aluminum and Reactive Metal Warranty T S l f l \ ] r ) r , H t M / C f a _ C J ^ TVVJC. hereby warrants that material offered to S&W Waste, Inc. for transportation, treatment and/or disposal does not contain elemental aluminum or reactive metal paste, powder or pigment and hereby agrees to idemnify and hold S&W Waste, Inc. harmless *-om any costs, damages, ot other liability resulting from breach of this warranty, r.^ ^_ 1-^^ • • BY: "S . ClllLrw-1 \e.f.Ml--V DATED: --^ _ WITNESS: 301440 1 15 JACOBUS AVE. . SOUTH KEARNY, N.J. 0 7 0 3 2 . (201) 344-4004 GENERATORS WASTE MATERIAL PROFILE SHEET CODE TECHNICIAL REP. INITIALS \ . GENERAL INFORMATION k^lA} ^"^0-^7 GENERATOR NAME -ASCC^c C ^ ^ ^ ^ t ^ c Z ^ o . ( \ f U ,i . i ^ - r J GENERATOR EPA LD. NO./^i:^ 'PA^S'yp^ ADDRESS ^ ° A : '^<^y^S, ZZyyy^yyrySfy.f/ZD . J r . CygZy.^, C/SiZZ OcfJLts TITLE / y ^ PHONF ^y<Ty.^C-<^zS7k TECHNICIAL rnNTAr.T y Z ^ y y '^Z. A Z U S J J z ' ^ y y f i x } - k / i ^ e t k l WASTE NAME y ^ ^ ^ y j ^ y ^ ^ y ^ y:yy^^^ZZ yZyaeyy/p PROCESS GENERATING WASTE . • ^ A^Ttzy^A ZZAy,^....rojA.., ^ > ^ € i . yZgy^ A^trc3^..m^Zi~ J ^ ^ y^rTc B. PHYSICAL C H A R A C T E R I S T I C S OF W A S T E y7c>cyyy.o ZZ. • y ^ c i i r ^ y ^ y k PHYSICAL STATE @ 70"F D SOLID C LIOUID C SEMI-SOLID C POWDER % LIQUID % H20 ODOR COLOR • ORGANIC • INORGANIC C CHLORINATED ORGANIC BTU VALUE PER GA1_. % CL_ BS«W_ %ASH. % S . LAYERS • MULTI LAYERED • BI-LAYERED Q SINGLE PHASED I »«i SCLICS . TOC. COD. pH: DO-2 G 7.1-10 C N/A C 2.1-4 m 0 . 1 - 1 Z 5 C 4.1-6.9 0 1 2 . 5 C 7 D EXACT SPECIFIC GRAVITY G < J . G .8-.9 G .9-.95 C.95-1.0 C 1.0-1.1 D 1.1-1.24 a 1.25-1.4 a 1.5-1.7 a > i . 7 D EXACT. G FLASH D POINT GCF) GCC GOO OEXACT. Q <90 C <100 0 100-140 D 140-200 G < 2 0 0 VISCOSITY (CentiDoise G 1-100 G 100-1000 G 1000-10000 O 1 0 . 0 0 0 C EXACT C. C H E M I C A L C O M P O ^ I O N ( M U S T T O T A L 100%) % D. Ag. As. Ba. Cd. Cr. Cu. METALS yyy n TOTAL yyA y y y ; ~yz;y yyy; y y y GEPTOX H g . y < ^ ^ Ni_ Pt>, sg y^yy 7n y < / / r • Te y , ' A y A T OTHER. Al/L E. OTHER COMPONENTS y / / P a PCB'S* D D D D D a a D OTHER y^'A PESTICIDES/HERBICIDES* . CYANIDE OR CYANIDE PRODUCING. SULFIDE OR SULFIDE PRODUCING, PHENOLICS RADIOACTIVE INFECTIOUS y/. ~yZ7S ELEMENTAL METALS*_ OTHER. y ^ •ATTACHED DISCLAIMERS MUST BE SIGNED F. HAZARDOUS C H A R A C T E R I S T I C S : TOXICITY RATINGS — y , NFPA RATING INHALATION «i<iC y^'TT^aetetC DERMAL 2 > ^ y ^ y y h f r . ORAL ! D EXPLOSIVE D PYROPHORIC D WATER REACTIVE .. O SHOCK SENSITIVE D MSDS ATTACHED G. M A N I F E S T I N F O R M A T I O N . PROPER DOT SHIPPING NAME Ayf;-z::yU,^^e^ y/yZrATt yZ-cc: DOT HAZARD CLASS. UN/NA NO y > ^ y ? y y ^ y € / J r y . y > j r A Ay:yyy:A-C' rSr:^ y/yjA EPA/STATE WASTE TYPE jAy^JypyiC J ^ yZy's. EPA/STATO-I lAZARD CODE iyy<y<^<ft£j:/'Js^^ y/^rlZ] 1 H. SHIPPING INFORMATION A-7AAtZrccc a.A/. C BULK LIQUID DBULKSOLID X DRUMS MOTHER SHIPPING FREQUENCY: QUANTITY ^ 9 P F P f*>*c, I. S P E C I A L H A N D L I N G I N F O R M A T I O N / C O M M E N T S : ^ ^ / O g / ' g c y y ^ , y , ' ^ 6<yy77y y^/sayzA**/^ C' ^ J . I HEREBY CERTirr THAT ALL INFORMATION SUBMITTED ABOVE AND ALL ATTACHMENTS ARE COMPLETE ANO ACCURATE. ANO THAT ALL SAMPLES SUBMITTED ARE REPflESENTATlVE OF THE WASTE. DATE TITLE' " GENERATOR'S SIGNATUR 301441 Poiychiorinated Biphenyl (PCB) Warranty ""^is disclaimer is to all persons who generate and dispose df chemical waste. The terms PCB and JB's are used in this disclaimerto referto any chemical substances and combinations of substan- ces that contain 50 ppm orgreaterof PCB's as defined in 40 CFR 761.3 (s), including any byproduct in a process which contains less than 50 ppm PCB because of any dilution; again, these lattershall be included as PCB and PCB's. Substances that are regulated by this rule include, but are not limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and other chemical substances or combination of substances, including impurities and byproducts. It is unlawful for S&W Waste, Inc to receive PCB's. Any generator and/or transporter who knowingly or wiiirully ships PCB's to our facility will be subject to civil penalties or criminal prosecution. J , 5 L f i r A j ^ Ctf^CcfT^C-c^^Vphy warrants that materials transferred by it to S&W Waste. Inc. for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl (PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby agrees to idemnify and hold S&W Waste, Inc harmless_from any costs, damages or other liability resulting from the breach of this warranty. 4 ^ ^ L r r < ^ ^ Cfr=#Tvi(c^r\ (Lo . X J c DATED:. ^-"-^7 Br-.^^Rykd^y^ WITNESS:. / ^ ^ J y ^ y ^ ^ T Warranty [TStt^rr^o^ C t t P ^ C ^ ^ Cl^TiPrfihy wan-ants that material transferred by it to S&W Waste, Inc for transportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level greater than 0.001% when measured in each containerorvessel transferred to S&W Waste, Inc., and hereby agrees to indemnify and hold S&W Waste, Inc harmless fromjgny costs, damages or other liability resulting from the breach of this warranty. X ^ C A ^ ^ C t t V ^ ^ ^ ^ H - ^ -'^^ < DATED: _ 3 _ : i b £ I RY- l ^ / W l o ^ V - ^ , " ^ . ^ y ^ j - ^ ^ y ^ y WITNESS: - • Aluminurn and Reactive Metal Warranty T^StfVKjT^ f f - H ^ a r / ^ 0 5 h J^K^rehv warrants that material offered to S&W Waste, Inc for transportation, treatment and/or disposal does not contain elemental aluminum or reactive metal paste, powder or pigment and hereby agrees to idemnify and hold S&W Waste, Inc. harmless '•"om any costs, damages, or other liability resulting from breach of this warranty. _ ^ , ^ A DATED: WITNESS:. '^ ^ ty 301442 AZ^^^z^y^ S & W WASTE, INC. 115 JACOBUS AVE. . SOUTH KEARNY. N.J. 07032. (201)344-4004 GENERATORS WASTE MATERIAL PROFILE SHEET - • TV- A P o q o v A L C O D E TECHNICIAL REP. INITIALS . GENERAL INFORMATION i j A ^ ' ^ - / Q ^ ^ f j GENERATOR NAMC . Z s z ^ ' y ^ kl/</ynyCS<, d s k ^ ' ^ " A .' •y:> v. ADDRE?;.'^ ysiyi' ( Z A / S (kky?y.^^-^^:/ZC J r . <Z!yZe'..,j a<SVy €ky(^2.a GENERATOR EPA I.D. NO. ^^<^ ?A-^ryeCr~ TPrHNiriAi r.nNTArT /•^r>? A - A^Zyg^ AkZfyfy-a J c u t ^ o i j ) VASTE NAME ^ o < g ^ < ^ j y / y y T e Z J p y / / yZAc'^ T I T L E . y y 9H0U^'iZZ//l^JLZ^^^ PROCESS GENERATING WASTE AAr-yryyi!>u/yy B. PHYSICAL CHARACTERISTICS OF WASTE PHYSICAL STATE @ TOTj ° ° ° " y?/yCy:i . XSOLIO C LIQUID I / Z ^ C y C ~ SEMI-SOLID a POWDER "A^ ORGANIC I J ~ INORGANIC % LIQUID «b H20 COLOR 2<:2c 'cyku Z CHLORINATED ORGANIC STU VALUE PER GAI =« CL _ BSAW_ »<.ASH. «b S TOC . LAYERS / ( / / C MULTI LAYESEO C ai-LAYERED i ^ • - ^ G SINGLE PHASED ! >b SOLIDS . y / A p H : 2 0-2 C 2.1-<» C 4.1-6.9 G 7 G 7.1-10 C 10.1-12.5 0 1 2 . 5 G EXACT _ G N/A <r.Sf SPECIFIC GRAVITY G ca G .8-.9 C .9-.95 G.95-1.0 G 1.0-1.1 G 1.1-1.24 G 1.25-1.4 a l i - 1 . 7 C >1.7 G EXACT. ^^.^7 G FLASH G POINT GCn GCC G O C G EXACT. D <90 O <100 G 100-140 C 14O-20O S > 2 0 0 VISCOSITY (Centiooise G 1-100 G 100-1000 G 1000-10000 G > 10.000 G EXACT_ / V A CHEMICAL COMPOSITION (MUSTTOTAL 100%) % y Z / ^ ^ ^ y r zZy -y:y:yA^iey J A S-Zry,^/) F. HAZARDOUS CHARACTERISTICS: TOXICITY RATINGS INHALATION D E R M A L ORAL C EXPLOSIVE G WATER REACTIVE G MSDS ATTACHED y A NFPA RATING D PYROPHORIC C S H O C K SENSITIVE D. M E T A L S C TOTAL Ag y.'A A.. y / / : Ra yy/t Cd /ZZAL Cr y/A Cu y/zZL. O T H E R . A Z ^ D EP TOX Hg A/A Nii y y A Ph y</AZ .<;«. yJ/'A 7n y / A Te yZAZ G. MANIFEST INFORMATION PROPER DOT SHIPPING NAME y^Tt^ty:*^. C^A'r<Ai. f y . A yV^-, DOT HAZARD CLASS y P A y f - ^ " UN/NA NO. y J A ^ 9 y ( Z ^ ^ EPA/STATE WASTE TYPE cy.^S'^ EPA/STATE HAZARD CODE ^ » ^ ~ - ~ ^ / H. SHIPPING INFORMATION G B U L K L I Q U I D C B U L K S O L I D X ^ D R U M S " O T H E R . SHIPPING FREQUENCY: QUANTITY / P E R . tzyr-y,. E. OTHER COMPONENTS n PCR-s* n PF.<;TiciOES/HFnRi'~iOP'^ G CYANIDE OR CYANIDE PRODUCING a SULFIDE OR SULFIDE PRODUCING n PHFNOLICS a RADIOACTIVF n INPFCTIOUS n ELPMFNTAI WFTAI ??• G O T H P H •ATTACHED OISCLAJMEBS MUST BE SIGNED y y y y y y y y y y / y ; y y y y/A y y y yyy; y/yj I. SPECIAL HANDLING INFORMATION/COMMENTS: y ^ ? . ^ /2y*y^ /:AZtyy^ ykyiA/y*/^ ^yyAAyf I MEBEBY CESTIFY THAT ALL INFORMATION ABE SEPRESENTATIVE OP THE WASTE. BMITTED ABOVE ANO ALC ATTACHMENTS APE COMPLETE ANO ACCURAT DXTE fntE /ye. M : NO THAT Ajfl. SAMPLES SUBMITTED 301443 GENERATOR'S SIGNATURE TABLE 1.2 30870-0705 ENVIROSCIENCSS Sainple Identification: ALAE 64867 PCB Isomer P.es'clt. rsv-^Kg PCS 1016 <1.0 PCB 1221 <1.0 PCB 1232 <1.0 PCB 1242 - ci.O PCB 1248 <1.0 PCB 1254 <1.0 PCS 1260 <i.O 301444 YWC. INC. • 200 Monroe Turr.pike • Monroe. Connecticut 06468 • (203) 261-4^53 PRIORITY POLLUTANT VOLATILE ORGANIC ANALYSIS T^-- LABORATORY ID #14116 ~ ' —• ' " LAB # 52955 ' """"" ""' CLIENT: ENVTRO SCT^MP^C - 1,1^.^^ r:-. SAMPLE SOURCE Sami^l^ •?? ' • 2 ~ -. • GC/MS Method 624* Tier I I Deliverables PARAMETER Chloromethane Bromomethane Vinyl Chloride 1 - . . - — Chloroethane Methylene Chloride 1 .l-Oichloroethene 1 ,1-Dichloroethane Trans-1 ,2-Dichloroethene Chloroform 1 ,2-Dichloroethane 1 ,1 ,1-Trichloroethane Carbon Tetrachloride Bromodichloromethane 1 ,2-Oichloropropane ' Trans-l,3-Dichloropropene Trichloroethene Di bromochloromethane 1,1 ,2-Trichloroethane Benzene cis-T,3-Dichloropropene 2-Chloroethylvinyl ether Bromoform Tetrachloroethene 1,1 ,2 ,2-Tetrachloroethane Toluene Chlorobenzene Ethyl benzene Total Xylenes *Dichlorobenzenes noc analyzed under chis mechod. RESULT ug/kg u u tJ u 7.83 U U U U U u u u u u u u . 3. OB U U U U U U U U 1.295 METHOD BLANK ug/kg u u u u " . 5 J u u u 7 . 3 J U u ;j !j IJ. U u u u 2.0 J U U u U " u 4.9 J U U U MDL 10 ; n : r\ . -.1 LO 10 LO 10 10 10 10 10 10 10 10 10 10 10 ..- iO 10 10 10 10 10 10 10 10 10 10 Analyzed by GC/MS Mechod 625. 301445 / I C M l f t S f S ^ ' / Polychlorinated Biphenyl (PCB) Warranty r^^is disclaimer is to all persons who generate and dispose of chemical waste. The terms PCS and % 3's are used in this disclaimerto referto any chemica! substances and combinations of substan- ces that contain 50 ppm orgreaterof PCB's as defined in 40 CFR 761.3 (s), including any byproduct .n a process which contains less than 50 ppm PCB because of any dilution; again, these lattershali be included as PCB and PCB's. Substances that are regulated by this rule include, but are not limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and other chemical substances or combination of substances, including impurities and byproducts. It is unlawful for S&W Waste, Inc. to receive PCB's. Any generator and/or transporter who knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal prosecution. hereby warrants that materials transferred by it to S&W Waste, Inc. for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl (PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby agrees to idemnify and hold S&W Waste, Inc. harmless from any costs, damages or other liability resulting from the breach of this warranty. DATED: BY:. WITNESS:-. Herbicide/Pesticide Warranty i^3Li^\C> C^C^.{C{Z^f:^i<jZ • hereby warrants that material transferred by it to S&W Waste, Inc for transportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level greater than 0.001 % when measured in each container or vessel transferred to S&W Waste, I nc, and hereby agrees to indemnify and hold S&W Waste, Inc. harmless from any costs, damages or other liability resulting from the breach of this warranty. XTSLAIMII^ C ^ ^ M U ; / ^ QQ ~ K C . DATED:. WITNESS Aluminum and Reactive Metal Warranty lXLh^Z^r\ravj(^Z? C'2).lyJZ hereby warrants that material offered to S&W Waste, Inc for transportation, treatment and/or disposal does not contain elemental aiuminum or reactive metal paste, powderorpigment and hereby agrees to idemnify and hold S&W Waste, Inc. harmless *rom any costs, damages, or other liability resulting from breach of this warranty. _ , _ X 5 . L ^ ^ ^ C V ^ Q ^ I C ^ C J O . , ^ ^ ^ ^ DATED: •- BY; \<~r^;r>A-A \ ^ \ \ J A X J 7 \ — , WITNESS: / ^ ^ y k y j ^ ^ / A L / . . . y- y c/ 301446 INDUSTRIAL CORROSION MANAGEMENT INCORPORATED N J H E ? Cercified Drinking Wacar/Wascevace- Laboracory ID// 14116 REPORT DATE: April 16, 1986 LA3.-? 52955 .1152 ROUTE 10. RANOOLPH. NEW JERSEY 078S9 201-534.03;0 CLIENT: ENVIRO SCIENCES - Island Chenical P r o i e c c SAMPLE SOURCE: Samole ill SANIPLE DATE: Febr'jarv 28, 19S5 T.AKEN BY: A. Kvles AT LAB DATE: March 7, 1? = = LABORATORY .ANALYSIS REPORT P.AR.iMETER RESULT 7. Paraohenacidene None Found FINDINGS: Neac benzophenone If you should have any q u e s c i o n s , p l e a s e do noc h e s i c a c e Co c a l l . INDUSTRIAL CORROSION MANAGEMENT, INC. Ri^chard S. 1 / e A ^ P r e s i d e i S. I/e inc ^ RSL:dlh # 301447 y^cy A-6ffC7 INDUSTRIAL CORROSION MANAGEMENT INCORPORATED NJDEP Carcified Drinking Wacer/Wascavaca- Laboracory IDi* 14116 RZPORT DATE: April 14, 19S6 LAB # 52955 1152 ROUTE 10. RANOOLPH, NEW JERSEY 07865 201-3a4-03;o CLIENT: ENVIRO SCIENCES - I s l a n d Cheaical P r o i e c c SAMPLE SOURCE: Samnle if2 SA2-IPLE DATE: Februarv I S . 1935 T.iJCEN BV: A. KvLes .-^T L.AB DATE: March 7, I = :£ LABORATORY .ANALYSIS .REPORT PASAMETEPv Ignicabilicy - Specific Gravi pH(unics) Ig^i; RESULT as wichouc persisce •?2.4: nc Durr.^ng 7.38 If. you should have any quescions, please do noc hesicace co call. INDUSTRIAL CORROSION MANAGEMENT, INC. ''Richard S./LeV{ne Presidenc/ RSL:dlh 301448 y9/y£'<£^'f67 S & W WASTE, INC. ; 15 JACOBUS AVE. . SOUTH KEARNY, N.J. 07032. (201)344-4004 GENERATORS WASTE MATERIAL PROFILE SHEET APPROVAL C O D E TECHNICIAL REP. INITIALS . GENERAL INFORMATION C t^'5'll'^i^'^ GENERATOR S.AK.P - 2 ^ ? ^ ^ k!^yf/ycay. (ZZ> k / y A - t ^ = = i ^ - ^ /Sc£Z'(^^'^, C^ytTyy!>rjrZ£ J f Zy.y<-t^ C/JV/ OaT2.0 GENERATOR EPA LD. NO. YiC^^^2^r7C?:r A D D R E S S T E C H N I C I A L CONTACT y ^ ^ A A Z y c y ^ / t k r ^ y y u i t J d J ' * ^ ^ ) /ASTE N A M E Ay^yiyKy/tyy..' A ^ y ^ ' Z e ^ Aye>t:yfc - y / c ^ TITLE. / P P R O C E S S GENERATING WASTE . _yZA P H O N E ^ C ' ' / Z 6 B. PHYSICAL CHARACTERISTICS OF WASTE PHYSICAL STATE ® 70'F Z SOLID ^ L I Q U I D Z ScMI-SGLID - POwOc.=^ % LlOUlO \ H20 ODOR / c ^ y i O i r Z ^ T ' { " ^ ' O R G A N I C 3 r j VALUE PER G A L . £ j y i f / l ^ y * < - ^ COLOR 'S/* y. £.0 - INORGANIC Z CHLORINATED CRGANIC ^ CL _ B S i W . »: ASH . ">>> S LAYERS C MULTI LAYERED a BI-LAYERED ^ ^ SINGLE PHASED >= SOLIDS y y t T C t L - PH: CO-2 C 7.1-10 C Z.l-i - 10.1-12.5 C 4.1-6.9 3>12.5 G 7 Z EXACT _ C N/A ^.7/ SPECIrIC GRAVITY Z <.8 z .a-.9 ~ .3-.95 r .95-1.0 Z 1.0-1.1 C 1.1-1.24 Z 1.25-1.4 Z 1.5-1.7 z EXACT _ _ i l i r i _ a FLASH G POINT GCF) CCC GOC G EXACT Vsco; ^ 1 - 1 G 10< G 10< - G.<20q-5 _ _ G>10.' D <90 G <100 C 10O140 G 140-200 OSITYfCentiooisei 00 G 100-1000 G 1000-lOOCO 000 XACT J >' C. CHEMICAL COMPOSITION (MUSTTOTAL 100«r:) % y, yco/l^yrfiTTrWc. /^ti^^^V'x.g. ^?^ /^c*tftj-^.^ , yrre /?y^y^iy^yv<=. Ly ' . ^ ^ y t y , y / - 2 > y y * f ' ^ y i — y e z z y - y j y f t * ^ 0 . i-^^i^/ F. HAZARDOUS CHARACTERISTICS: rOXICITY RATINGS INHALATION DERMAL ORAL N r r A RATING yi/<r7y<t C EXPLOSIVE G WATER REACTIVE G MSDS ATTACHED G PYROPHORIC G S H O C K SENSITIVE G. MANIFEST INFORMATION PROPER DOT SHIPPING NAME AAi^^yty./my / y y ^ y C y T c ' f ' i . D. METALS C TOTAL Ag A^A A . A / / : Ba ''yA Cd A'A Cr yyA c Z ^AZZ G EP TOX HQ A J A Ni y / A Ph y t / A Se. A/A Zn. Te. DOT HAZARD C L A S S . UN/NA NO. y A y - q y y ^ ' e 9yA? EPA/STATE WASTE T Y P E . EPA/STATE HAZARD C O D E . Ay^ziZa y/A y y y ; H. SHIPPING INFORMATION G BULK LIQUID C B U L K S O L I D ' ^ D R U M S G OTHER SHIPPING FREQUENCY: QUANTITY / PER J T ^ i i u nTHFP A / A E. OTHER COMPONENTS n PCR'S* r pc=;Tir.inp=;/HPPRirinp.s;« G CYANIDE OR CYANIDE PRODUCING _ a SULFIDE OR SULFIDE PRODUCING n PHFNni ir.9 n RAninACTivF p iNFPrTinn.<:; n Fl FMFNTAI MFTAI f^* n OTHFR . yJA y J A y / / : y / A y A yyA y/y; y/A y y •ATTACHED OlSCLAlWESS MUST BE SIGNED I. SPECIALHANDLING INFORMATION/COMMENTS: I HEREBY CEBTirr THAT ALL INFORMATION SUSWITTEO ABOVE ANO ALL A H A C H M ^ T S ARE COMPLETE ANO ACCURATE. AND ARE REPRESENTATIVE OF THE WASTE. y - \ SUBMIT 3-/0 -'^1 u -yJLyl ULiclL DATE TITLE GENERATOR'S SIGNATURE 301449 Polychlorinated Biphenyl (PCB) Warranty This disclaimer is to all persons who generate and dispose of chemical waste. The terms PCB and \ 3B's are used in this disclaimer to refer to any chemical substances and combinations of substan- 'jes that contain 50 ppm orgreaterof PCB's as defined in 40 CFR 761.3 (s), including any byproduct, in a process which contains less than 50 ppm PCB because of any dilution; again, these latter shali be included as PCB and PCB's. Substances that are regulated by this rule include, but are not limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and other chemical substances or combination of substances, including impurities and byproducts. It is unlawful for S&W Waste, Inc. to receive PCB's. Any generator and/or transporter who knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal prosecution. : hereby warrants that materials transferred by it to S&W Waste, Inc. for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl (PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby agrees to idemnify and hold S&W Waste, Inc. harmless from any costs, damages or other liability resulting from the breach of this warranty. DATED; BY: WITNESS:- Herbicide/Pesticide Warranty Cb'v.Pnv'^ C K ^ A i c A ^ CC- j : i ' < hereby warrants that material transferred by it to S&W Waste, Inc. for transportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level greater than 0.001 % when measured in each container or vessel transferred to S&W Waste, Inc., and hereby agrees to indemnify and hold S&W Waste, Inc. harmless from any costs, damages or other liability resulting from the breach of this warranty. X S t P V ^ I ^ C'i^-'$r/\icnrt. ce). ^vOc. DATED: T^-^i-r^ R v ^ ( ^ . .:iCUi:^Ow- WITNESS Aluminum and Reactive iVietal Warranty TSt^^'v^ cHv^vtrr^ r^ , X K \ C , hereby warrants that material offered to S&W-Waste, Inc. for transportation, treatment and/or disposal does not contain elemental aluminum or reactive metal paste, powder or pigment and hereby agrees to idemnify and hold S&W Waste, Inc. harmless from any costs, damages, or other liability resulting from breach of this warranty. 3 - B ' - " .• ... ^rk\ CK DATED: BY: __ WITNESS:. 301450 INDUSTRIAL CORROSION MANAGEMENT INCORPORATED NJDE? Certified Drinking Vacar/Wastevaca- Laboratory IDi? 14115 RZPORT DATE: April 14. 1986 LAS il 52959 1152 ROUTE 10. .RANDOLPH. NfW JERSEY 07Se9 2Ql:a4-0:30 CIIZNT: ZNVIROSCIENCES - Island Chenical Proiect SA>SLE SOURCE: Saiapie =?6 S.^-LPLZ D.-^TZ: Februarv ^ S . 1936 T-AiCZN 3Y: A. Kvles AT L.\3 DATZ: March :. . r z - LABORATORY ANALYSIS REPORT P.AR.iJ>!ZTZ; RZSUIT ParaDcenetidena ' Xoc Present Findings: chloronethyl benzene benzene cethananuiae, n,n-dinethyl If you should have any questions, please do not hesitate to call. INDUSTR.IAL CORROSION Mi^AGEMINT, INC. Rfchard S. Livi^^e President / h/f/yj/^^-^ RSL:dlh 301451 y y A r^cHlSl ?C3 Isomer PCB 1254 PC3 1260 TABLB 1.1 30870-0705 MYIHgSCIENCES Samnle Identification: HARE 64981 PCB 1016 <0.2G PCB 1221 <0.20 PCB 1232 PCB 1242 PCB 1248 <0. <0. <0, <0 <0 20 ,20 .20 .20 .20 301452 YWC, INC. • 200 Monroe Turnpike • Monroe. Connecticut 06468 • (203) 261-4458 '"ill it i'i INDUSTRIAL - CORROSION MANAGEMENT INCORPORATED NJDE? Cartified Drinking Water/Wastevate: Laboratory IDi/ 14116 RZPORT DATE: April 14. 1986 LAB if 52959 1152 ROUTE 10. RANOOLPH. NEW JERSEY 07863 201-534.0330 CLIZNT: ENTIRO SCIZNCZS - I s l a n d Chenical P r o i e c t SA.MPLE SOURCE: Samole f?6 S.A>:PLZ D . \ I Z : Februarv I S , .19 = 6 T.AKZ^; 5Y: A. Kvles .AT L.A3 DATZ: LABORATORY ANALYSIS RZPORT P.ASAMZTZP. Flashpoint Specific Gravity pH(units) RESULT 97°C boiled (3 97'C 1.0809 6.71 If you should have any questions, please do not hesitate to call. INDU^TRLAL CORROSION M.ANAGZMINT, INC. Richard S. Lerrt. President / RSL:dlh 301453 y t ^ y y y ^ - z y T / S & W W A b T t , I N O , CODS 5 JACOBUS AVE. . SOUTH KEARNY. N.J. 07032. (201)344-4004; TECHNICIAL GENERATORS WASTE MATERIAL PROFILE SHEET i "^"^ '^'^'^^s w l GENERAL INFORMATION • M g B A x n R KJAtuig y A k . - > f / ) C y / t ^ f f / Z T : / . ADDRESS ^ ^ ^ ^ ^ y y A y a r T ^ / n c a . J?- Z:^^''^ . Z/Z^'T C o Z ' ^ ^ ^ z y ^ 7 ^^••'ZZ GENERATOR EPA I.D. NO. / / / : ^ A o 6 S y C ? r - TECHNICIAL CONTACT X ? ^ ^ / Z Z c C ^ / A £ r 7 / y y : y > J i i ^ c y STE NAME //s^'Sy-yifiiU.' Ak/furt, J r i Z o y^ye/S^ z y T I T L E , y y PHONE J 2 £ Z / I ^ £ Z ^ ^ ^ - ^ P R O C E S S GENERATING WASTE , y ^ r '<r>^<. B. PHYSICAL CHARACTERISTICS OF WASTE " H Y S I C A L S T A T E © 70=F! ' S O L I D , C UOUIO _ SEMl-SOLIO C POWOSa =o LlOUlO H20 COOR y < y ( j y y ' ^ COLOR y y y \ Z Oi=iGANlC J ^ I N O R G A N I C J Z CHLORlNATcD I CRGANIC BTUVALUSPERGAL % CL y y y ««> .=; HS*W %ASH LAYERS ^ ^ k k . ~AZA n MULTI LAYERED ; '"~ C Bl-LAYEREO . " - - " Z SINGLE PHASED I =>: SOLIDS i pH: a 0-2 G 7.1-10 C 2.1-4 C 10.1-12.5 G 4.1-6.9 0 1 2 . 5 G 7 O EXACT _ ^ N / A SPECiFlC GRAVITY Z <Z& G.S-.9 G .3-.95 •-.95-1.0 G 1.>l.l G 1.1-1.24 iS.1.2S-1.4 G 1.5-1.7 G>1.7 G EXACT_ G P U S H D POINT G m G CC GOC Z EXACT. D <90 C <100 G 100-140 G 140-200 ^i/^°^ y y / i r VISCOSrrY (Centiqoise) G 1-100 G 1CO-1000 G 1000-10000 G>io.ooo y y A C. C H E M I C A L C O M P O S . i T I O N (MUSTTOTAL 100"?=) % /^cy/ra^ y^yyy^ /yyfMZ^y<ctniy^ ^c ' yZkft^^yaa^fr'Zy _" s o y^'ZZZ, /^y(^/ZZ'-^yjk C c / x y F. HAZARDOUS CHARACTERISTICS; TOXICITY RATINGS INHALATION D E R M A L ORAL G EXPLOSIVE C WATER REACTIVE n MSDS ATTACHED NFPA RATING y / d A i ^ - C P Y R O P H O R I C • S H O C K SENSITIVE G. MANIFEST INFORMATION ^ / ' PROPER DOT SHIPPING NAME A i 4 r y y y y ( ^ y / ^ l ^ - r ^ y y / c Z ^ L, DOT HAZARD CLASS Q A A / - i f [__ UN/NA NO. ' ^ A i <pyj>9 ] _ _ D. M E T A L S C TOTAL Ag A y y j A' A/A Cd d/AL Cr y / A Cu y / A i C EP TOX Hg Ni Pb Se Zn Te A/A ~zv:^ y < K y/AL y/A y y EPA/STATE WASTE TYPE _ EPA/ST7>r?= HAZARD C O D E . _ ^ S 2 ^ /7/f ^%^ ^ / / H. SHIPPING INFORMATION C BULK LIQUID C B U L K S O L I D ^ D R U M S C O T H E R . SHIPPING FREQUENCY: QUANTITY / P E R . i f ^ y y . . OTHFP y / A E. OTHER COMPONENTS n pcc^TicinFS/HPPRicinPR* Q CYANIDE OR CYANIDE PRODUCING G SULFIDE OR SULFIDE PRODUCING n PHPNOi irs n RAniriAr.TivF n iNPPrTinu?; . n Fl FMFNTAI MFTAI .9* k O. OTHFR y/A/ y A y / A y / 1 ^/y: y / y j y.'A y/y; y / y •ATTACHED OISCUAIMERS MUST BE SIGNED / I. SPECIALHANDLING INFORMATION/COMMENTS: yA'T^y,.' /ZZAuZ^Iyl. /ZZzyy^ ykyy^yAyZ^yc•yyz y / y . A ^ y^Ay-.A:ya^C_ /^^^^^Aj^/^y I 3 1 HEREBY CERTIFY THAT ALL INFORMATION SUBMITTED ABOVE ANi ARE REPRESENTATIVE OF THE WASTE. / ^ 3-/^-^7 DATE \^M. dLM TTACMMENTS ARE COMPLETE ANO ACCURATE. ANO T H A ^ A U . SAMPLES SUBMI TTED c uA u^<Z TITLE GENERATOR'S SIGNATURE 301454 I Polychlorinated Biphenyl (PCB) Warranty ^ ^ ^ ' ~ ' s disclaimer is to all persons who generate and dispose of chemical waste. The terms PCB and ' • • yB's are used in this disclaimerto referto any chemical substances and combinations of substan- - jes that contain 50 ppm orgreaterof PCB's as defined in 40 CFR 761.3 (s), including any byproduct, in a process which contains less than 50 ppm PCB because of any dilution; again, these latter shali * be included as PCB and PCB's. Substances that are regulated by this rule include, but are not - limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and other chemical substances or combination of substances, including impurities and byproducts. It is unlawful for S&W Waste, Inc. to receive PCB's. Any generator and/or transporter who -* knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal prosecution. I S L H T P ' O C k i ^ y ^CfV^ COfiereby warrants that materials transferred by it to S&W Waste. Inc. for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl (PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby agrees to idemnify and hold S&W Waste, Inc harmless from any costs, damages or other liability resulting from the breach of this warranty. IX5>uAJ^•vp C r r O ^ ^ r p - (Z/Z -^^v'C DATED: -^ WITNESS:. Herbicide/Pesticide Warranty -LSL \ V J C ) ('y^Al(iZ^ d^ir\ih'k'rphy warrants that material transferred by it to S&W Waste, Inc. fortransportation, treatment and/or disposal is not contaminated by herbicide/pesticide ata level greater than 0.001 % when measured in each container or vessel transferred to S&W Waste, Inc., and hereby agrees to indemnify and hold S&W Waste, Inc. harmless from any costs, damages or other liability resulting from the breach of this warranty. X S t f ^ r V / D Crh^VNA.^/^ ^ CO.ZZ'J^ DATED: _ _ ^ 1 [ / Z i 1 _ _ PY- ^ /,(/i_r7 I T V — r i ^ ^ V . - J - ^ ^ r ^ ^ ^ y WITNESS: y^^^y^y^yy^^ztyA. Aluminum and Reactive Metal Warranty r ^ l f V O n r h t O M ^ C i ^ U C J ^ TVVJC. hereby warrants that material offered to S&W Waste, inc. for transportation, treatment and/or disposal does not contain elemental aluminum or reactive metal paste, powderorpigmentandherebyagreestoidemnifyandholdS&WWaste, Inc. harmless • ' -im any costs, damages, or other liability resulting from breach of this warranty. ^^ _ ._^ -'- HATPn. Z - ) \ - k y : py. ' ^ . (\m.rsry-,^.//Jz^--/ y ^ / ^ - ^ y ^ y ^ "' wiTNpg;?; Ayc-^ytAy. y^fyCcyy^ ^ a 30I455 O C5t VV V V M O I C J I I M \ ^ . 115 JACOBUS AVE. . SOUTH KEARNY, N.J. 07032. (201)344-4004 GENERATORS WASTE MATERIAL PROFILE SHEET TECHNICIAL REP. INITIALS A, GENERAL INFORMATION ,Cy^ '3'-/0-'By ENERATOR NAME -AS^--^^ ZZiryy^.^^^ <Za. A^S-.V k t K ^Z^..\^) GENERATOR EPA I.D. N O . K ^ ^ ^ J - / , ADDRESS 2 ^ ^ T ' y s Z Z k y y y r y ^ ^ y j r ^ , J ^ . (Z'y^aZy . ( y r ) / Z y g f y L o TgrHNiriAi rnNTAr.T y ^ L s y y y^- AZyc^f J'ZZyiyyyy} Acy:ynciyj TITLE / / ^ /VASTE NAME A / k ^ a y S y i z y ^ < ^ . ^ i ^ yj^yptyyc PHONF ' Z y c y / T i : £ y i . PROCESS GENERATING WAS 7P y ^ A;^7/Zy<i^ (ZZlyyfy^itJL > ^ y ^ yC:iy^. A€yayiy.yzZ B. PHYSICAL CHARACTERISTICS OF WASTE J ^ ^ ykATc 'rTo'Cy/yA yyy?<^iy:^ A/,. PHYSICAL STATS © 70^F: ° ° ° " G SOLID Z LIQUID I G SEMLSOLID C POWDEa j coLOR »» L I Q U I D : »* H20 I ! G ORGANIC G INORGANIC G C H L O R I N A T E D O R G A N I C 3TU VALUE PER G A L . 9b C L _ 3 S A W _ = » A S H . "fcS. LAYERS I _ ^ ^ C MULTI LAYERED i ' G BI-LAYERED ! ^ ^ ° G SINGLE PHASED i =^ SOLIDS . pH: G 0-2 G 7.1-10 C N/A G 2.1-4 G 10.1-12.5 G-S-l-e.g 0 1 2 . 5 G 7 G EXACT SrECIFiC G.nAVITY G <8 G ,8-.9 G .9-.95 G.95-1.0 G 1.0-1.1 G 1.1-1.24 G 1.25-1.4 G 1.5-1.7 G > 1 . 7 G EXACT. G PLASH C POINT GCF) G CC GOC CEXACT. Q <90 C <100 C 100-140 C 140-200 C < 2 0 0 VlSCCSrTY (CentiDoisei G 1-100 G 100-1000 G 10OO-10O00 G > 10.000 G EXACT C H E M I C A L C O M P O S I T I O N (MUSTTOTAL lOCri) J e z . y/r^Cyy/:/} y^^ri^j.-^ y Z - j y F. HAZARDOUS CHARACTERISTICS: TOXICITY RATINGS — y , NFPA RATING INHALATION >SdC yArT^CM<:.C DERMAL 2 y u t y ^ y y h Z z . . ORAL D EXPLOSIVE D PYROPHORIC C WATER REACTIVE Q SHOCK SENSITIVE a MSDS ATTACH ED G. MANIFEST INFORMATION PROPER DOT SHIPPING NAME A/6-::7yU:^cU y j / k / T t AZ^ cc'y£. DOT HAZARD CLASS. UN/NA NO yyCypyyy/dC A s . , . yZj r-) M E T A L S y y y D, Ag As Ba Cd Cr Cu OTHER. C TOTAL y y A z/yy ~yZZ^ y y i x y C EP TOX Hg Ni Pb Se Zn Te y(AA ~y7Zr EPA/STATE WASTE TYPE >^<^/^'<f<:C> Skz. AyZ/~) EPA/CTATgi lAZARD CODF AAy^yc'/CC A J c ^ y/rzk) ZyyZ^ y y y y y y y.'A H. SHIPPING INFORMATION A'AAA J r c c i . O - A / C BULK LIQUID Q BULK SOLID "5? DRUMS C OTHER SHIPPING FREQUENCY: QUANTITY ^ ' P PFR <y>'CJ^ E. C D G a • a a D a a OTHER COMPONENTS A\A'/? PCB'S* y/A_ PESTICIDES/HERBICIDES* CYANIDE OR CYANIDE PRODUCING . SULFIDE OR SULFIDE PRODUCING . PHENOLICS RADIOACTIVE INFECTIOUS AK. y// w ZA/AZ y/A ELEMENTAL METALS*_ OTHER. ZMZ y y UTTACHED DISCLAIMERS MUST BE SIGNED I. SPECIALHANDUNG INFORMATION/COMMENTS: J ^ ^ yvryfcy/iit:} A)y:^y4yrf yZyjtf' • yA^ i £ ^ y^^y^yZs>c^ y ^ . ^ ^ £ > <:>cyy77y y ^ ^ ' ^ y y i : A C ^ J . I HEREBY CERTIFY THAT ALL INFORMATION SUBMITTED ABOVE ANO ALL ATTACHMENTS ARE COMPLETE AND ACCURATE. ANO TVlAT ALL SAMPLES SUBMITTED ARE REPRESENTATIVE OF THE WASTE. DATE f..Mj(it[l yzy.i.x) TITLE GENERATOR'S SIGNATURE 301456 Polychlorinated Biphenyl (PCB) Warranty T<- is disclaimer is to all persons who generate and dispose of chemical waste. The terms PCS and .B's are used in this disclaimerto refer to any chemical substances and combinations of substan- jes that contain 50 ppm orgreaterof PCB's as defined in 40 CFR 761.3 (s), including any byproduct in a process which contains less than 50 ppm PCB because of any dilution; again, these lattershali be included as PCB and PCB's. Substances that are regulated by this rule include, but are not limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and other chemical substances or combination of substances, including impurities and byproducts. It is unlawful for S&W Waste, Inc. to receive PCB's. Any generator and/or transporter who knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal prosecution. J,5LrTAJV) Ctt'Qi'^CcnrvCx4TF>Veby v/arrants that materials transferred by it to S&W Waste, Inc. for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl (PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby agrees to idemnify and hold S&W Waste, Inc. harmless_from any costs, damages or other liability resulting from the breach of this warranty. f ^ i f\fA ^ Crt^TM-fC/^TV Co X-u'v DATED:. ^ - ^^-^7 RV. ^ . rki^irw—- ,<Uz^sjJr^ V/ITNESS .' y^^^y^jy T Herbicide/Pesticide Warranty T S L I V N A : ) C-iitl^fxC ( ^ ^ e ^ i i p r f i h y warrants that material transferred by it to S&W Waste, Inc. fortransportation, treatment and/or disposal is not contaminatec j y herbicide/pesticide at a level greaterthan 0.001% when measured in each containerorvessel transferred to S&W Waste, Inc., and hereby agrees to indemnify and hold S&W Waste, Inc harmless fromjgny costs, damages or other liability resulting from the breach of this warranty. j T ^ C / V ^ ^ L ' t f \ / v \ f f ^ 0 ^ S ^ < ^ DATED: 3-11-^7 ,..^X[\k V/ITNESS: Aluminum and Reactive Metal Warranty J S ^ f W T ) rH-T-V^Kf/^ O J ^ T^Hi^reby warrants that material offered to S&W Waste, Inc. for transportation, treatment and/or disposal does not contain elemental aluminum or reactive metal paste, powder or pigment and hereby agrees to idemnify and hold S&W Waste, Inc. harmless m any costs, damages, or other liability resulting from breach of this warranty. ^ ^ , )ATED: V/ITNESS 301457 D R U M INVENTORY race / cf •9 -. Crunn Type j m Nu'mber Generator Hazard Cess y r - "-'rTik. / 7 / A y y z y / //€/>/:: y sc fyyjzi kA'iir^if/eC/- ka. A~cCy>/y>^yy/Z /yci^'y/z VJPS a Date y A / y y /•/. y y 'y^/zpz/s d<;/>e z j - y % CUANTiTY HAZ.ARDCUS SUESTANCc 2Ay7?' 1 Vv'ASTH A/Cs yr:y.,rAy/.r U D O T . , ? l . D . O CC.MME.NTS A/A/(y/<^ \yyrf:= 1 r^y=o£ /^^y-.y^ /P-.!. WAS" i \ y / y Z i r ~ . y/'-y^ y-Z^.-^. WASTE yA..-x:.tyk~ / - - / - y y ^ . 1 WASTE - / ' WASTE WASTE V;ASTE 1 - 1 WASTE ! :••"• 1 WASTE - i 1 i WASTE 1 1 WASTE i l l 1 WASTE 1 WASTE ! 1 WASTE 1 1 WASTE 1 1 i WASTE I I 1 WASTE 1 • WASTE 1 I WASTE " • ! 1 1 WASTE - 1 .1 WASTE \ \ \ WASTE I ' l \ WASTE •i WASTE - 1 WASTE 1 WASTE 1 1 1 1 WASTE I ' l l WASTE 1 WASTE 301458 •_ Drum Type j m NuTnber Generator Hsrard Class DRUM INVENTORY y y - <:,d^. J'zkiZ^, A 7/A /Jhyy /4:v/^ • yzL Zyksd.';'yyA yz.^yyy^t Cy/r'^yr/'.eti., ^AOZ / • y ^ y ^ : / zZ. WPS » Data Pace _ ^ rf / s y y / y /y;-fy "y^z^yzy} caae T j - y - m CUANTiTY HAZ.ARDCUS SUESTANCc . DOT..? z?.^ I . D . ? /y7z^Az:\ WASTE /kyzyZ^yy/7ZyA_^ ^<^/^<ri? \y/CC3= /yys:^:-^ y=^,c';-y/z^yyj: '" J, -= --l WAb . c 1 1 y/t-Zt^ / • / ^ _ / . ^ ^ ^. ''•'' WASTE yrAi:-:yy cyT-.yZ-zyZ^-- yyy^-^.:-y:\ W A S T E x f e ^ . v ^ A \A.'yyrj</:g yyc7£ \^y;:/:C y A y y ^ y-z- • Vv/ASTE I x-Z-'-^r'-• ^y/T/r^-j.- W A S i c 1 1 ry-^A^^:-^y Vt'ASTE 1- 1 1 WASTE ' '-'• WASTE • l i l WASTE i WASTE 1 WASTE WASTE WASTE WASTE 1 WASTE 1 1 1 WASTE 1 WASTE WASTE - WASTE WASTE 1 WASTE 1 WASTE 1 WASTE 1 WASTE 1 WASTE 1 1 1 WASTE - I 1 " WASTE - 301459 ^ Drum Type j m Nu'mber Ha-ard Class D R U M INVENTORY yyay. Generator — — " kfyy::yr7^yf/<_ AZ^. / = ^ . •ys^y>f'^-z.^i:yi •c ykp^y^c Page "^ r« cf / WPS J* Data . y / Z y ; ; / yZ-yjZ, ^ / y p ^ S / U ! CyrZi-^: T / ~ # QUANTITY y / ^TA . 1/ HAZ.ARCCUS SUESTANCE WASTE ykrisTAZf,/^-/y.. WAS". 1 . DOT..? y y , / . ^ : ^ I . D . ? 6/A/:£ WASTE i f- ' - \ l . . C M ~ C ^ ^ ...•».C;M I o J?/^^r: y^/7cyy y':>r.c/-'y yy/.r-r"•• j T / y y . t^y^.^: ! y y y z / y ^ ^' " 1 V/ASTE 1 i 1 -^ <y.'y /.• A ^ r ^ 1 / y-rr 1 Vv'ASTE yy-zy/y, /-^y/^-l^yy.. 1 WASTE WASTE yAc-Zy/Ar y.'y; / / v y \ i/y.'/zo7 WASTE 1 WASTE ZPt-riVytyt^ 1 WASTE y ^ y / / ^ c i SC.-/ //Z=''f ' e r r <.>c__L ^nrv7=<" (. y \ yZy^ .:>yy/yy A c y y y ^ t . \ '• ^ <Wi:>s/ L 1 r y k ' t7yy.'.-y /^-yy/ALi^ \k ^ VRASTE 1 ! W A S T E 1 WASTE ' I I t WASTE 1 1 1 1 WASTE 1 W A S T E 1 1 WASTE 1 W A S T E WASTE WASTE • 1 W A S T E WASTE WASTE WASTE \ 1 1 WASTE 1 *\ WASTE WASTE 1 WASTE WASTE 301460 - . D r u m Type j m Nu'mter Generator Harard Class D R U M INVENTORY - y I JkZZyk /7A/AZ^yyy.j y'/k,. /A-'y/y ^ .zLSy.lyyj) /ky^:yy^,rr./. ^ /y^rzfT/y7yi^.^ yZZyJ-y/jC P a s e _ £ _ c f ^ WFS # Data .Z^ y^zyy y<^r-y ' /i^zsyyi l i a a ^ : 2Z CUANTiTY HAZARDOUS SUESTANCE DOT..? i J* -"V T D rt cc.M^;E:^JTS ^ ^ • / ? ~ \ ' • / . WASTE V.'AS" E ^L'TZ.y kAAcyy^. y \ Ayy/yA^7 \ \ -\ \ WASTE 1 WASTE 1 1 Vv'ASTE 1 1 WASTE A. -\ V/ASTE . ^ c c / \ <^vr '^A ryZy,.^. yr-' y y y y - ' y y . y y > 1 ! i 1 I WASTE 1 1 WASTE • WASTE i 1 1 \ WASTE I I I 1 WASTE i 1 WASTE 1 1 WASTE 1 1 WASTE 1 1 WASTE WASTE 1 1 WASTE WASTE WASTE . . 1 1 V/ASTE \ WASTE WASTE WASTE WASTE 1 WASTE \ WA«;-r- 1 • WASTE t WASTE 1 301461 ^ -.Drum Type , j m NuTriber Generator Hazard Class DRUM INVENTORY z r y - 9 o A L ky<yjk A7//AZ^.yy^y //yi^y.^ . y . S^v-A zkyty^/rnzk, ZZk • > f ^ - ' . yZ^'Z^^yyy: P a C 9 _ ^ r f 9 cf V.'PS ^ Date t X y r y y / y ^ y y ^ f 3 y 2 / } d^A)<£': / / ( y ^ r ^ / j y , .J. C^y^.*yyt>y QUANTITY HAZARDOUS SUESTANCE - DOT..? I . D . ? //,-Tr 1 Vv'ASTE y^yy^y/^yy^e Az^-Gyc yZZyy/y,^ y/y/y^^z. P c 7 r C C M : / . = N T S A/..-/. / . y -• y y / T y ^' WAS-.i y^i^t.i.^..iZC) \ . 1 • ^ '^ <// yiyZ. WASTE WASTE yAy.:,y...y A-Af.y^c. /-/.w//.. //v^/^o^ \ / ^ ' 7 s ' i-r. y.:..y y/yyP:^ V/ASTE ' X','.v'<r,....7' 1 1 ' "^ WASTE A^'.A 1 WASTE tZ-/Z'.T>::y/i-<//e,yz,y- /yy,v/fZ Z^co/ /i7c?C /,:•.-./- ' I ,/ WASTE I I ' '•• 1 WASTE '- 1 1 WASTE 1 WASTE ' WASTE 1 1 WASTE WASTE 1 1 WASTE 1 1 1 WASTE - 1 1 ! WASTE WASTE 1 1 WASTE 1 1 1 WASTE - ' i WASTE 1 1 WASTE 1 1 1 WASTE i 1 ' WASTE ! . 1 1 • 1 WASTE 1 WASTE 1 WASTE I ' l l WASTE 1 1 WASTE 301462 D R U M INVENTORY Ps^e - '=^ cf _f_ ^ /—:.. Drum Type -••^^ j m Nu'mber ^•^ Generator ,~ Hazard Class ^=^ss-ccc j'A/ /7A/ ck:y //LA• ^ ZZZr<.^'^/A Cyy'^'yzyyy^y.. (ZZy>- k^y/i'A'/y/i'' /./c/f/Zz: WPS # Date y A f A / / ^ / - ^ , A<?Z3/10 C c ^ i ^ ' Z " QUANTITY HAZARDOUS SUESTANCE / t .^.-ryZ A • ^ y ^ DOT,.? E?.\ I . D . ? COMMENTS W. ^STE y / r z T ^ y / y / y / y y - y y . . / / y / y - y C ^-ccZt^S / Z - / " . . . y -CA^CCJ /-^ WASTE TE yky,.-y.<Z' / k y y / y k : . / A y / y Z / ' WASTE IA '^ Vv'ASTE WASTE WASTE WASTE / WASTE- • WASTE WASTE- . WASTE WASTE WASTE 1 WASTE WASTE WASTE WASTE V/ASTE WASTE 1 WASTE 1 WASTE 1 WASTE WASTE WASTE WASTE WASTE WASTE WASTE 301463 DRUM INVENTORY -. Drum Type ^ jm Nu~mber Generator Hazard Class S'^-^y/Z. Z%yi /7yA Zj^.^y/k,</ Z2?cr.:'-^ r /Jy^.'.tn/y'rk y : C y . i , : f ; y ^ y y C /y yZ/Cc/y/i V/PS » . Date . Pace 7 ^^ 9 / J y ^ / y ' / y^j-yc uZ r k^tu/yv.^ QUANTITY HAZARDOUS SUESTANCE • r - y ' - W A S T E yAy.':-rMvcr7,r,,y.<^ w . DOT .? yyryyy<r<:Z Z I K T n /.' i}cc/ y y z . \ W A S T E - yy.s,-7yi.yi7j/nyy.jt£- COMMENTS >^- xr-1::^ .-^-r-i c.^- ^v. ^/-' '' y yyy/y$-</. \ 2 r c / 1 <-/c>-..-/r:'v /^l-^T^ ' 1 WASTE ^ A / ' z / k WAS 1E /yy-2^'/y.'y,;yy>r' y/yyyy'P/: y - c c / y - A y r J . y y / y A^./r^.^^ ' ' WASTE '•• ' / y ^ y VMSTE 7^y>yyy^y.^ \ A/yAy:2Z<k\ y/ZA'p A - A a y / f.yZ.t.^'yky'yy^- WASTE 1 ^ ' -^ ' •'• W A S T E '• 1 WASTE WASTE 1 WASTE WASTE WASTE WASTE WASTE WASTE 1 WASTE 1 WASTE WASTE 1 WASTE 1 ^ 1 WASTE WASTE WASTE WASTE WASTE WASTE WASTE WASTE 1 301464 D R U M INVENTORY Pac Z ..9 e ^ r- Drum Type j m Nulnber Generator Hazard Class SzZ'-'-T^A, / / / / ^ y f y j ^^yir) V JZ^iZWy> ZAr^6^//t:C/- Ca. AlZ.Z^y»/yT/!c'y£ /yCc'y/D WPS » Data y A A / ^ y y ? : . f y Aypppy:^ ^ ^ ^ ^ CUANTiTY HAZ.i.RDCUS SUESTANCE DOT..? E?-\ I . D . ? COMMENTS . A^ffyrl^ 1 WASTE '7Z^r/?<iy/'y£/?c-/rcy£y/ 6Zy(/eoz:& \ Z / Z / S 1 / Z c r T p C O o C 0 1 V/AS-E 1 • ' I • • WASTE 1 - WASTE i I WASTE 1 1 WASTE 1 t V;ASTE i - 1 1 1 WASTE ' 1 ;••• 1 WASTE - I I ' I WASTE- 1 WASTE I I ! WASTE 1 WASTE 1 1 • WASTE 1 1 ! WASTE WASTE 1 WASTE WASTE WASTE 1 WASTE WASTE 1 WASTE WASTE WASTE 1 WASTE WASTE WASTE ' 1 • WASTE WASTE 301465 . Drum Type j m Nu'm.ber Generator Hazard Class D R U M INVENTORY SzZZ'-trcji:^, y 7 / A Ay/Ay/ y/Z!fS) y k y y t y s . ZZyr-trrif/cCc ka. AlZLZ^yvyyfyl/ZtZZ •^'^cu/. Ccyy/Z Pccs ^ cf 9 WPS S Date .yAr/V/AZjZ //S^<D i£c^ r ^ QUANTITY HAZARDOUS SUESTANCE DOT..? . D . ? AZ ^'R I WASTE 7ir/?clyy^Aiyr-->/^-e/y£yy yyy/3czz^ \ y / t / S /ZZZA CjyzZ— C WAS-,c 1 l - l 1 WASTE 1 " " • WASTE 1 I Vv'ASTE 1 1 WASTE V/ASTE WASTE ;••• WASTE WASTE- WASTE WASTE WASTE 1 ' WASTE WASTE 1 WASTE 1 1 WASTE 1 1 WASTE 1 WASTE WASTE 1 V/ASTS WASTE WASTE 1 WASTE WASTE WASTE WASTE WASTE WASTE 301466 DRUM INVENTORY Page /__ cf -. Drum Type j m Nulnber Generator Hazard Class SzT-r-jk, /7/A Zy/fy/ yZrJs: 1 y s^ f. 7yt/Si ZArr'iZnf/CiU. C^, Ai^Z^y/ATycZt^x Z/Ci/yy; WPS ^ Data ZPAZy//7Z^ 'y^^S>/^ d <;y>€- z ^ y CUA NTIT Ay?^ L- \ •Yl HAZARDOUS SUESTANCE 1 i WASTE /ycdr:y,,riy^r 1 V.'AS", i DOT ,? A/yl/<zyA^ \ WASTE I i WASTE 1 1 WASTE 1 WASTE t I Vv'ASTE WASTE WASTE - WASTE 1 WASTE WASTE Z I K Z.D . i y / r r : ^ 1 0 C.M ME NTS Syy^-CC /=^y::y^ /t'^i'.. y/i-Z Z / '. yy-^^ y~y.'? -. yZ —— 'A y y 1 . ^ - ' ^ - ' ^ T ^ £ ^ ^ ^ ' - d ^ y ^ \ \ -^ c 1 1 i 1 1 1 i 1 1 WASTE i l l 1 WASTE 1 WASTE 1 WASTE 1 W A S T E 1 WASTE WASTE WASTE WASTE i WASTE WASTE WASTE 1 W A S T E WASTE WASTE WASTE 1 1 WASTE 3 0 1 4 6 7 Cr'jm Type __ j m Nulnber Generator Hazard Class CRUM INVENTORY yZr- <;<'.//. J'zkiZ^, A 7/A /kkyy /Aly/^ y L .zZ. ZZiL'TyyA ^ . 'tc.., cy; / y yk^. •yyy^^if/A ^ c ^^yyy: i-3ce cf 9 WPS S Data -^^^^^y A^y. '^y^zS/ey] caae'.- -r -y— •^y ^ 1 CUANTlTr'j HAZ.AF.DCUS SUESTANCE DOT..? /AZz^Az: '• WASTE /k-.T^yy/TZZyZ^, 1^''>/«;ci? ••=^ ' V.'ASli I ''' I WASTE 1 ±Z'y;.-'.:.7Z': WAS~E ^ i ^ T ^ . - / / ^ / - - : XA.'Ay/yz: '•' \ WAS-E 1 ! WASTE 1 i Vv'ASTE i WASTE 1 1 •• ! WASTE - 1 1 WASTE 1 WASTE I WAS 1 = ! WASTE 1 W A S i E 1 WAS.=: I WAS . c WAS , E 1 W A S i c I . D . i- C C M M E : . - 3 Z-^CVJ^ \y/ys=--l y A - . ^ .fzz^-^^r 1 / / - " o T " - y y l _ / y t . . . " / \ yrAfZ/yy CyT-.^ry;,,.^..-^ \<Acy7£ \ l^/4irc yiyyyy y c r 1 1 y / z . ^ r ' = yy..-^..r^.^^- \ 1 ^ - ^ - • \ \ \ 1 1 1 1 • 1 1 1 - 1 1 I I 1 1 1 1 I WASTE ' 1 1 WASTE - 1 WASTE 1 WASTE WASTE WASTE 1 WASTE 1 1 WASTE 1 1 WASTE t WASTE WASTE 1 301468 — Drum Type j m Numoer Hazard Class D R U M INVE.NTQRY /yy-yy^... Jzzzzk.. /7y /^-v? K/A'f^L Generator ..——" ". kfy^-Cy^^<:ni.^ Ak>, A^gyyy;yr7-Z^£y^ yZZ^. •fyyl f " 3 C S « • <:* — ^ - _ AAp^'S/i/i cc^-e-; JZ r - CUANTITYI H . — . ^ f ^ / - \ , . ^ ^ t , ^ . ^ . . . . . . . . . . . . r\.i -^ l~, l_ v_ ^ i l i 'w 3 .S 1 '-M^ >w C 0C.-.'r.*.E?-iT3 . S / ^ T Z 1 WASTE yky2.yTyy/', AZ^Ay y y / y - y t ' ^ I ^ / ^ j r r^/r.^y yr^t^yy y,zcyr-,' - 'I ^ • li ' 4 . / ' -^ 'A (, AT- ,y i ''•' W- ' • 1 -v.. i 1 ! y" 1 1 ^ ! 1 •y 1 1 V.'AS". -i WASTE WASTE WASTE V/ASTE V/ASTE W A S T E W A S T E /Trr-yy, /•::>r ^ -.^/'> y y y Z y / - ^ /yc,'77Ay</'y.. I 1 1 ! I 1 y/y y / ' / y \ \ 1 1 z/yJ/Z^7 \ \ . 1 A-'^'^/yZc 1 W A S T E 1 V/ASTE W A S T E 1 W A S T E 1 W A S T E W A S T E W A S T E 1 /Scz/ \ ^y 1 a C 3 / y^'r.^-f •' . : r : y y ^ tyA^^y.-< y, r r ./zy-— c c '.ZcC....- yZt:/r<' c y y y ^ -.>^-.'-i/ <^ <.•//<:> y . y y ,y/y.-.-y / k y / k ^ \ k 1 W A S T E W A S T E WASTE W A S T E W A S T E W A S T E W A S T E V/ASTE 1 W A S T E W A S T E W A S T E W A S T E W A S T E , 1 •i 1 . 301469 ;. Drum Type j m Nu'mber Generator Hazard Class CRUM INVENTORY zky-<z<f^i JZ^yJ Ay//Ap^yyj//k,y/: • y / yZSclyy/) /k.c<^ dy> yZkyrz^yyZy/^ yZ/y^-^y^y: Pace <- r.^ 9 WFS ^ Data yzzzzky^z, * //^zsy^/} ^ ^ ^ .. J- CUAN~iTYl A-.z..^>-,•_. v>US S'_ r e 1 .-^i^oc !0T ,? T -> ^ - — I . ' . _.'* . c WAS" WASTE WAS' I c WASTE WASTE WASTE y ^ - y / . 1 • • c WASTE V/AS". E y^ 'Zz:/ kAAr.zzy J \ A/yy/AZ 7 £>cc^ i 1 • 1 \ WASTE i 1 WAS-E 1 1 1 V/ASTE 1 i </.=•.,A- -yyy.^yyy.y^^^ /•^ y / y y y - i WAS'E 1 t i \ V/ASTE V/ASTE W A S T E • \ - i 1 1 i ' 1 WASTE 1 1 •• 1 V/ASTE 1 1 1 1 WASTE 1 1 WASTE 1 1 1 WASTE I I 1 WASTE 1 1 WASTE 1 1 1 WASTE V/ASTE 1 1 WASTE WASTE WASTE 1 WASTE - 1 V/ASTE 301470 :, Drum Type j m Nulnber Hazard Class D R U M I N V E N T O R Y yy-Cy^y. J k Z j L A7A/A7^^^y / / k i . ^ ^ • enerator — £.~^-^ Zkyy'yyizyr^y, /Zko /=k:^.>^:yrzz yk'y •S'^y.'y: P a g e _ _ ^ c f 9 WPS ^ Date yy^A/y/-^, y y ^ z ^ / ) dsyxE-' y/(/5yy^^y,u£_ mC CCY^yyayjy^j \ QUANTITY HAZARDOUS SUESTANOE D O T ? z?.\ yf^.-ir \ WASTE y<yyzy£)yy^e Az.^Z-yc /-yy/zy^L \ / A y / y ^ S ^ P < : 7 r r - ^ ^ t ' ' ^ \ i AP<zy. ry, --. y ^ yyy- . ^' \ V/AS", i y^i^t.i.it:.cC) 1 • ^ >/ 1 V.'ASTE tf//:7r:. 1 V/ASTE /o-..,/^...' /c/^^.-.c /-x,'//^/_ y / y / / y r y / " f ^ S ' \ A7'. ^ . y . . - y f ^ / T ^ -' 1 V/ASTE y : y ^ . . . - r \ . 1 j " ! V/ASTE 1 / < • - / WASTE A - /Z.-y:^A<,'>c.yz.,y- \ y / y i Y y f Z Z>y:o/ \ Xrct-C ^ , j . . . . ' - , _ ' 1 WASTE ' • . " i ^ "' WASTE " • ^ WASTE V/ASTE WASTE 1 WASTE 1 WASTE I 1 WASTE WASTE WASTE 1 WASTE V/ASTE WASTE WASTE WASTE WASTE WASTE 1 WASTE ^ ^ WASTE ^ ^ WASTE • 1 WASTE 1 WASTE 1 301471 ^—:. Drum Type l ^ k j m Nulnber Generator Hazard Class DRUM INVENTORY ys-<,.cZJ'7^y.. /7A/ c k , y //y^y • ^ yzrc.^yy.zZ CyyAy;:.yy/'y k y . J". 1>yA.:'*//f/' /yAZy / y / : Pase-_£_cf ^ WFS # Date y y ^ y / y ^ ; - ^ . /^z3/z/z cc/zy- QUANTITY HAZ.ARDCUS SUESTANOE DOT .? Z l K I . D . ? CCMME:NTS /Z.-J.yyZ \ WASTE /A-ziTTZZ / ^ T A r y / k i / k y . / y / y - y y r \:^-ryzZ^\ / Z Z - / - - ^ / . ^ y . . ^ / . WAS", i 1 • " ^ A y ^ V/ASTE Aky.ZZy, y k y y A y y^ y A y / y 7 y ^ i - C c ^ , | A - y : y ^ ^ y ^ ^ ^ y y ' ^ — \ V/ASTE ' ^^ '^' 1 V/ASTE 1 1 ! WASTE 1 1 1 V/ASTE - K \ WASTE WASTE • V/ASTE .' WASTE 1 WASTE WASTE WASTE WASTE WASTE 1 WASTE WASTE 1 WASTE WASTE • 1 WASTE WASTE 1 WASTE 1 WASTE WASTE WASTE 1 WASTE WASTE - 1 1 1 WASTE 1 301472 -.Drum Type _ j m Nu'mber Generator Hazard Class CRUM INVENTORY S y - ^ y /^.^y, A AAA yy^f-^AAki.ck 7" /rcry.-s Ak.^.,-,/y'^k / y /Zii:y:'r,:yyyyyC A y e yyzcyy^ Page ^ cf / V/FS ii Data • y y / z t ' / y t y r r y A/ffZ9£€ <LC/)^' r \ Q U A N T i r r HAZ.ARDCUS SUESTANCE . DOT .? E?.-. I . D . ? COMMENTS • r ^ y . - 1 WAS 1 = yA.'^^y^'-e.r,y,.^^<£' yy/yy£'<y. A > C ^ / \ p . y - . . ^ -iy-: tyy y<. .y- 1 V/AS", E 1 ' \ "^ •"' . y < : i . i - \ v / A S i c .^/-•-.-^cr^/A-'^/'./c' y y y / y ^ ^ \ 2 r c / 1 y - A < y ' - - J t - ' y ^ y y 1 WASTE 1 ^ Z • / ' z y k \ V/ASTE /.^T--_-.-.'•/'< ry^z^y,^ / / y / y yOy.\ j . ,^ r. / \ / - / y . P . y Z , / y y . r y r ' V / A S - E 1 ! ^' ' /'.'y-y \ V/ASTE TZAyyyy^y.., AAyAy2Z<L.\ y/ZZ-'7 \ A - Ayj.y-.pyZ.'.j:/ykAZ WASTE '^'•' ^' WASTE • 1 1 V/ASTE WASTE 1 WASTE 1 WASTE WASTE WASTE 1 V/ASTE WASTE I WASTE WASTE 1 WASTE WASTE WASTE WASTE 1 WASTE WASTE WASTE 1 • WASTE WASTE 1 301473 DRUM INVENTORY Fac; Z ..^ ^rum type j m Nulnber Generator Hazard Class yy-r--^. /7y y/zyy y/zrz. V y Z Z y i y / y Crt'^^/ycC:.. Ca. A~Cvy»/y7/l/:Ze:Z J-ZCcy/ZZ WPS ^ Date ZP Azyy/?:: O ' yyp<?PyjP ^ ^ ^ ^ . w .-M N . . I 7 t—' ' T * •:C.i '•> c ; ' = • t /-^ j \ V-^ w DOT ^ S " ^ ! ^ ' V/AS I E 7cr/?pyyv/j/r'Z,!:rc-A£y., k zAA/2o^^ \A/z/^ 1 /<:'"crrr^ ^:^ps^ VA'A.C- 1 V/AS' >«':i C—— 1 i V/ ASTE Vr .-^ C 1 w 1 WASTE ' 1 WASTE WASTE• 1 V/ASTE WASTE WASTE 1 1 ! . 1 1 • i 1 WASTE WASTE V/ASTE WASTE 1 1 WASTE WASTE WASTE WASTE WASTE WASTE WASTE WASTE WASTE - 1 WASTE WASTE WASTE 1 1 301474 -. Drum Type j m Nu"mber Generator Hazard Class DRUM INVENTORY y y - ' " Z k . /7/A ZZPZyy yZ'z.0 ZAz-'i^y/cC:. Ca. A~<z:Z:yfyyyA/^<^£ /.yccyyy: n Pace Z ^. .y ct V/PS ^ Date yA^y^/A} • r.y /45sa<^ da/^^ - TZ QUANTITY! H/-\i..^ r". L- ^ U i SUES I AN 0 E AZ k V/ASTE 7cr/!^yy<y<o/?r:^z.yy:yy V/AS'E I \.', / • c — ~ I yyy/ec^^ \.yz/s I /t^V.^ (Z:yc<-^ \ , _ 1 Wk '' ^ - 1 - ! WASTE 1 - ! V/ASTE ! • 1 WASTE - 1 V/ASTE 1 1 V/ASTE 1 i WASTE 1 I 1 WASTE 1 WASTE 1 1 WASTE 1 1 - - V/ASTS 1 WASTE 1 WASTE V/ASTE WASTE WASTE 1 1 1 1 1 1 1 I • 1 WASTE ; • • WASTE I WASTE WASTE 1 ^ ' • , -&. y WASTE 1 1 WASTE WASTE WASTE 1 1 301475 S & W WASTE, INC. 15 J A C C B U S AVE. . SOUTH KEARNY. N.J. 0 7 0 3 2 . ( 2 0 1 ) 3 4 4 - 4 0 0 4 GENERATORS WASTE MATERIAL PROFILE SHEET APPROVAL COOE TECHNICIAL REP. INITIALS GENERAL INFORMATION kykk]~^-/DSl GENERATOR NAME - Z r < : g ' ^ ZZyyfyr^yCt'y, y ^ , / ^ - ^ ^ . i . . y . . k y . ^ J GENERATOR EPA I.D. NQ. Ay<Dp(fiyi^r-yCr% ADDRESS - y r r . <c773'. Cyyyyrr'r^ftjyta J k C Z u - y cyytyy c>c^3r3 TPri-iNJiriai rr^MTArT y / e l p y y y A<Zycc^QcZZZyy/zg j S l ^ ^ d : ^ / TITI F A A > VASTE NAME A > ^ i £ ? y y k f t ^ C ^ / y Z t jZr-Ar: ^ y C A p f ^ PROCESS GENERATING WASTE . PHONE .^V^gl-c-^— B. P H Y S I C A L C H A R A C T E R I S T I C S OF W A S T E PHYSICAL STATE @ TO'T GOGH XsOLID Z LIOUID j C SEMI-SOLlD C POWDES ; % LIQUID I %H20 I x V ^ i i . COLOR y A y f I Z CPGANIC : )$ INORGANIC i Z CHLORINATED i ORGANIC =TU VALUE PER GAL »a CL _ as4w. % ASH. zzzzkycz^s^ % s LAYERS y y y D MULTI LAYERED C BI-LAYERED D SINGLE PHASED TCC. CCD. AA/ «*> SOLIDS. DH: CO-2 C 7.1-10 ^ N / A C 2.1-4 G 10.1-12.5 G 4.1-6.9 GM2.5 G 7 G EXACT SrECIFiC GRAVITY G <za G3-.9 G .9-.35 G.95-1.0 G 1.IM.1 C 1.1-1.24 G 1.25-1,4 G 1.5-1,7 GEXACT_ C FLASH G POINT OCPI GCC COC D <90 C <100 C 100-140 G 140-200 • <200 G EXACT ^ " ^ g y ^ T y y VISCOSrrY (Centiooisei G 1-100 G 10O-10O0 G 1000-10000 G >10.000 ^ ^ G EXACT yy*^*r£.. C H E M I C A L C O M P O S I T I O N (MUSTTOTAL 100%) % yk/t/^yZy-T-T^ ( L . ' / • O Aoy^yjyLr^ (^yAeciciki <:^e>. y>ce-cy F. H A Z A R D O U S C H A R A C T E R I S T I C S : TOXICITY RATINGS INHALATION DERMAL ORAL G EXPLOSIVE D WATER REACnVE G MSDS ATTACHED NFPA RATING y V c i y y t S ' C PYROPHORIC a SHOCK SENSITIVE G. M A N I F E S T I N F O R M A T I O N / j . r • PROPER DOT SHIPPING NAME Ar^^irT^yu^a^ A ' / r i ] y . kZ,.y^? ~y, DOT HAZARD CLASS CPyyTZ—rS^ UN/NA NO. y i y y P - 9 y < f 7 D. M E T A L S ^ C TOTAL Aa y y y A.<; Ba Cd Cr C'J yyyf y y y y / y ; y y y y y y OTHER. y y y ; C EP TOX H g . N i . Pb. Se. Zn. Te. yzA EPA/STATE WASTE TYPE <y^20 EPA/9f*?e HAZARD CODE tfr'^i.^-.^ T y y y ' y y J - y ^ / / y y y H. S H I P P I N G I N F O R M A T I O N Ay yA k c C C ( D / / C BULK LIQUID G BULK SOLID ,Xt)RUMS "OTHER SHIPPING FREQUENCY: QUANTITY A O PER e^fiJ. yz^ E. G G G G G G G G G O T H E R C O M P O N E N T S PCB'S* PESTICIDES/HERBICIDES* CYANIDE OR CYANIDE PRODUCING . SULFIDE OR SULFIDE PRODUCING . PHENOLICS RADIOACTIVE INFECTIOUS /ZZ^ A/A. y / A _ y/A ELEMENTAL METALS* OTHER. A/A_ •ATTACHED DISCLAlMEflS MUST BE SIGNED :yL I. S P E C I A L H A N D U N G I N F O R M A T I O N / C O M M E N T S : y / t r r - A t (ZAyryyy y^yCec^ y,yr y ^ y X ^ A:>y^,^-n^ y<yyyryyr' Cy^f/^yy/e^) T-Cd.eyyirf.y r>.^,~,'rn-m'yyyi^ , - ^ ^ y ^ y < i . t ^ ^ ^ r " t i < y ^ < y fTTyy^.r. /€y.yj-e.y>. A ^ . y t H i J tyyy y y / y y ^ r r y i ^ r- C . ( y . f : t ^ ^ i A r Z ^ ' ^ J . I HEREBY CEHTIPC THAT ALL INFGBMATION SUBMITTED ABOVE ANO ALL ATTACHMENTS ARE COMPLETE ANO ACCURATE. A^O THAT ALL.&AMPLE3 SUBMITTED ARE REPRESENTATIVE OF THE WASTE, y ^ y i / } • ' / I 3'-/^^g 7 L^i^.i ' py.iA DATE TITLE GENERATOR'S SIGNATURE "^"7 301476 Polychlorinated Biphenyl (PCB) Warranty This disclaimer is to all persons who generate and dispose of chemical waste. The terms PCB and PCB's are used in this disclaimerto referto any chemical substances and combinations of substan- ces that contain 50 ppm orgreaterof PCB's as defined in 40 CFR 761.3 (s), including any byproduct, in a process which contains less than 50 ppm PCB because of any dilution; again, these lattershall be included as PCB and PCB's. Substances that are regulated by this rule include, but are not limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and other chemical substances or combination of substances, including impurities and byproducts. It is unlawful for S&W Waste, Inc. to receive PCB's. Any generator and/or transporter who knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal prosecution. Vr-yy / ^ , _ , 1 ^ ^ ^ • .' '^ • "^^-J hereby warrants that materials transferred by it to S&W Waste, Inc. for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl (PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby agrees to idemnify and hold S&W Waste, Inc harmless from any costs, damages or other liability resulting from the breach of this warranty. 'JZZ^K.i\!\^{Z) QfrAA^^^^^/'^ZZAA 3"/^'=^ DATED: WITNESS; Herbicide/Pesticide Warranty ^ ^ A ]yzye>-^c\k^'^^itk^ c^"^^^ f kjAI hereby warrants that materic rial transferred by it to S&W Waste, Inc. for transportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level greater than 0.001 % when measured in each container or vessel transferred to S&W Waste, Inc., and hereby agrees to indemnify and hold S&W Waste, Inc. harmless from any costs, damages or other liability resulting from the breach of this warranty. X ^ l L f V t ^ ^ C t ^ c ^ ^ r l T \ ^H2) ^ ^ DATED: ^ - (f-<^^ RV- fe^> CLr7,.Wv\^ S e c ^ J z i > y - ^ WITNESS:. k2k^^^y^z/C7 Aluminum and Reactive Metal Warranty ^ ' ^^^^^ '' ~ , ^ M hereby warrants that material offered to S&W Waste, Inc for transportation, treatment and/or disposal does not contain elemental aluminum or reactiv metal paste, powderorpigment and hereby agrees to idemnify and hold S&W Waste, Inc. harmles from any costs, damages, or other liability resulting from breach of this warranty. ^ , _ DATED: WITNESS 301477 S & W WASTE, INC. 15 JACOBUS AVE. . SOUTH KEARNY, N.J. 07032. (201)344-4004 GENERATORS WASTE MATERIAL PROFILE SHEET APPROVAL COOE TECHNICIAL REP. INITIALS GENERAL INFORMATION '.ENERATOR NAUC / k s ^ ^ y i kk'£y*'^CS^ < ^ . / ^ C m / ' ^ ) ADDRESS, ^^TH ^ 7 7 S yy-yyAi-yrttm^sy-y f r . Cyyry: / y j i ' ^ y>cfZc GENERATOR EPA I.D. NO. AZ/l££0^yZyC9s - y TECHNICIAL CONTACT • ^ ^ ^ / • P ^ C ^ i ^ k k * f y ^ y - ^ J ( Q ^ t : ^ ^ ) ASTE NAME /y^^^yyyJtJAi A ^ / ^ 7 t S < c y n y A c Z ^ TITLE. A/=> PHONE • y < : y - i ^ - i z . r c PROCESS GENE.RATING WASTE ^•"'^^^g- k < ^ s ^ ^ ^ ^ / ^ J B. PHYSICAL CHARACTERISTICS OF WASTE PHYSICAL STAl 70T CDOF tSOLlD C LIQUID I y < f J o Z SE.MI-SOLID Z POVVOE.n Ofc LIQUID , •>H20 :COLOR y / y Z ORGANIC r INORGANIC ~ CHLORINATED ORGANIC STJ VALUE PER G A L . y y y =0 CL _ asiw. «» ASH. % S TCC. y ^ yr LAYERS y<y'A Z MULTI LAYERED ; Z BI-LAYERED j " " ^ ^ G SINGLE PHASED I «* SCUDS 1 I pH: GO-2 G 7.1-1 C 2.1-A G 10.1- G 4.1-6.9 G>12.5 G 7 C EXACT 0 y 12.5 ^ N/A SPECIFIC GRAVITY G <L8 G .S-.9 G .3-.95 G.95-1.0 G 1.0-1.1 G 1.1-1.24 G 1.25-1.4 G l.S-1.7 G EXACT_ a FLASH G POINT GCF) GCC a <90 G <100 G 100-140 C 140-200 G EXAC ^Z. <?00 VlSCOSiTY (Centiooise) G 1-100 G lOC-1000 G 1000-10000 ^ ^ ; i ^ AAA! CHEMICAL COMPOSITION (MUSTTOTAL I00<r!) % yJc/^JZ. 'Jk/^js^p^ - (ZO Aytg^/ys^^r- C , <?.o yZ/cyZZZ:^ /kyPL A ^ / y - ^ ^ y . c n t y , / F. HAZARDOUS CHARACTERISTICS: TOXICITY RATINGS INHALATION DERMAL ORAL G EXPLOSIVE C WATER REACTIVE C MSDS ATTACHED NFPA RATING /y'CyiA€' C PYROPHORIC G SHOCK SENSITIVE D. M E T A L ^ ^ G TOTAL Ag As Ba Cd Cr Cu OTHER. y/A '7777 ~Z77r ~y7y ^ i ^ A y77> G E? TOX Hg Ni Pb Se 7n y/y^ TP y / A y/Ai 'y/TT G. MANIFEST INFORMATION PROPER DOT SHIPPING NAME AAnTryy^y.: / y y / Z Jri..zjyi,i:;L DOT HAZARD CLASS y ^ A A - f - d " UN/NA NO. y / y <7yf? EPA/STATE WASTE TYPE 2Z^X;>2.. E.=A/S»*f5 HAZARD CODE. ~y/7r H. SHIPPING INFORMATION G BULK LIQUID CBULKSOLID " S T D R U M S G OTHER. SHIPPING FREQUENCY: Q U A N T I T Y ^ _ 5 _ _ ?••=•?.. E. G G a G c n C G OTHER COMPONENTS PCB'S' PESTICIDES/HERBICIDES' CYANIDE OR CYANIDE PRODUCING . SULFIDE OR SULFIDE PRODUCING . PHENOLICS RADIOACTIVE ^ INFECTIOUS //A: y/A "PATr /vy AZTA y<yA_ ~Z<7Ar ELEMENTAL METALS*_ OTHER. AAJk y / y vrTACHED DISCL*IMERS MUST BE SIGNED I. SPECIALHANDUNG INFORMATION/COMMENTS: y y ^ t ^ ' . k y A y ^ A /v.^.Ht- i>y^ / ^ r i ^ //tiyy? AAry(yf<y.. gk^-^-t, yyi^t/.y. TTZy^cL yZryyt'dai cyr/f/tJ ^?.f-.ge/cc?/sg> i p 7- /yicycuo £yyyrry yZ/Ux^A —y — J . I MESEBY CERTiri' THAT ALL INFORMATION SUBMITTED ABOVE ANO ALL ATTACHMENTS ARE COMPLETE ANO ACCyRATE. AND Tl^AT ALL SAMPLES SUBMITTED ARE REPRESENTATIVE OF THE WASTE DATE TITLE GENERATOR'S SIGNATURE 301478 Polychlorinated Biphenyl (PCB) Warranty • disclaimer is to all persons who generate and dispose of chemical waste. The terms PCB and d's are used in this disclaimer to referto any chemical substances and combinations of substan- ^.JS that contain 50 ppm orgreaterof PCB's as defined in 40 CFR 761.3 (s), including any byproduct, ..1 a process which contains less than 50 ppm PCB because of any dilution; again, these latter shali be included as PCB and PCB's. Substances that are regulated by this rule include, but are not mited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic ..uids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and other chemical substances or combination of substances, including impurities and byproducts. t is unlawful for S&W Waste, Inc. to receive PCB's. Any generator and/or transporter who knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal !:°^^^H!^^^LAvO CrP^yn ^ Co - hereby warrants that materials transferred by it to S&W Waste. Inc, 'or transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby agrees to idemnify and hold S&W Waste, Inc harmless from any costs, damages or other liability -esulting from the breach of this warranty. XSL/VAJHi CtKA^^C}^^ CO -^Vw DATED: _ 2 J 1 [ 1 I 1 ? RY- l < . r [ \ ^ l ? W - "S^fi WITNESS: A /kyk^y py^yZi::j. ^ J (/ ^ Herbicide/Pesticide Warranty hereby warrants that material transferred by it to S&W Waste, Inc. for transportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level greater than 0.001 % when measured in each container or vessel transferred to S&W Waste, Inc., and hereby agrees to indemnify and hold S&W Waste, Inc. harmless from any costs, damages or other liability resulting from the breach of this warranty. _j> -^/^yy} r ^i^C^M. ^CPrx. C^"" I^NJ ^ DATED: y WITNESS: y^yyi^^y^ykry / \ y / y . Aluminum and Reactive Metal Warranty hereby warrants that material offered to S&W Waste, Inc. for transportation, treatment and/or disposal does not contain elemental aluminum or reactive metalpaste, powder or pigment and hereby agrees to idemnify and hold S&W Waste, Inc. harmless >m any costs, damages, or other liability resulting fr©ffl±)reacly3f t h i s w | ^ O ' " ' o WITNESS:. 301479 S & W WASTE, INC. 115 JACOBUS AVE. . SOUTH KEARNY, N.J. 07032. (201)344-4004 GENERATORS WASTE MATERIAL PROFILE SHEET APPROVAL CODE TECHNICIAL REP. INITIALS GENERAL INFORMATION O^-^^/o - ^ 7 'y&iy.. <Zc k-/^ GENERATOR NAME _ , _ ^ A D D R E S S x ^ t - ^ i ^ 7 7 S y y y y / s y 7 - ; ) ^ j / Z D . k r / y y ^ - ^ ^ f y y O c ^ f Z t S GENERATOR FPA I n NO ^ ' ' 0 y Z ' - € 7 y c 9 \ TECHNICIAL CONTACT . //£. ^zy Z^ \ T I T L E . yp WASTE N A M E . A ' / y y ^ tZAz. yx> y<A(Si^ PROCESS GENERATING WASTE y ? y y y y e x y - n P H O N E ^ / / J & 6 - 6 L ^ B. PHYSICAL CHARACTERISTICS OF WASTE PHYSICAL STATE s> 70°F • ODOR y SOLID Z LIQUID I sz^yk/^^ Z SEMI-SOLID % LIQUID •SH20 .=owDea ,- ''^ORGANIC _ Z INORGANIC C O ^ R y - ) : CHLORlNATcD ORGANIC STU VALUE PSH GAL. _ c/yr CyyeiyTrr «b C L _ SSAW. »t>ASH. % s, LAYERS y i / P • MULTI LAYERED C BI-LAYEBED D SINGLE PHASED TCC. CCD. y / y : »s SOLIDS. pH: C 0-2 C 2.1-4 0 4.1-6.9 C 7 C 7.1-10 C N/A Z 10.1-1 2.S SPECIFIC GRAVITY : <a :3-.9 : .9-95 : .95-1.0 : 1.0-1.1 Z 1.1-1.24 Z 1.25-1.4 Z 1.5-1.7 CE^'cT_aif£- Z FLASH G POINT GCF) zee C O C CEXACT. D <90 C <100 C 100-140 C 140-200 S>«200 VISCOSITY (CentiDocaei " 1 - 1 0 0 Z 100-1000 Z 1000-10000 G>io.ooo y / y Z EXACT 1 _ C H E M I C A L C O M P O S I T I O N (MUSTTOTAL lOO'r:) »o "^JyT^yzyyyiyn:^ yk/^yky'zi y d ^ y y ^ y - t - ^^^^^y^X _y^_ <'C-CSZi/ F. HAZARDOUS CHARACTERISTICS: TOXICITY RATINGS - . INHALATION D E R M A L ORAL C EXPLOSIVE O WATER REACTIVE G M S D S ATTACHED y/k? NFPA RATING C PYROPHORIC D S H O C K SENSITIVE y/TT ~y/z D . M E T A L S C TOTAL Ag A / A ^ As Ba Cd Cr Cu OTHER Aiy y/A Z/Z/A ZUTT C EP TOX Hg Ni Pb Se Zn Te y / A Zy/A y / y j y / y y y y G. MANIFEST INFORMATION PROPER DOT SHIPPING N A M E A/P^r. r y c C i / t J / y r ^ y r r , J y ^ / y ^ . OOT HAZARD CLASS < Z 7 y y ' f - < S UN/NA NO. A A y 9 ( ? 9 ' EPA/STATE WASTE TYPE EPAySTATE HAZARD C O D E . CASZO H. SHIPPING INFORMATION G BULK LIQUID C B U L K S O L I D ' ^ D R U M S C OTHER SHIPPING FREQUENCY: QUANTITY ^ PER J ! : ! l £ £ r y/y: E. o a a a c D a OTHER COMPONENTS PCB'S* y / ^ PESTICIDES/HERBICIDES* CYANIDE OR CYANIDE P R O D U C I N G , SULFIDE OR SULFIDE P R O D U C I N G . PHENOLICS RADIOACTIVE INFECTIOUS . y//^ yAi y/> y y y y . ELEMENTAL METALS*_ O T H E R . Z ^ A P y •ATTACHED DISCLAIMERS MUST BE SIGNED I. SPECIALHANDLING INFORMATION/COMMENTS: y-^aZZZutyyy:i^y:y^iy^ y * - u ^ £ . y y A i Z y y y y U < y / y.i-<y {^/(^{tcay c < y : ^ yz/Cca-yC/yr^ dy J . I HEBEBY CERTIFY THAT ALL INFORMATION SUBMITTED ABOVE ANO ALL ATTACHMENTS ABE COMPLETE ANO ACCURATE AN^O THAT ALL ^ M P L E S SUBMITTED ABE HEPSESENTATIVE OF THE WASTE / ) / , z ' l / ^ . / / / ? ^ DATE C-y. I AA TITLE GENERATOR'S SIGNATURE -f- 301480 Polychlorinated Biphenyl (PCB) Warranty 's disclaimer is to all persons who generate and dispose of chemical waste. The terms PCB and ^B's are used in this disclaimer to refer to any chemical substances and combinations of substan- "Les that contain 50 ppm orgreaterof PCB's as defined in 40 CFR 761.3 (s), including any byproduct, in a process which contains less than 50 ppm PCB because of any dilution; again, these latter shali be included as PCB and PCB's. Substances that are regulated by this rule include, but are not limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and other chemical substances or combination of substances, including impurities and byproducts. It is unlawful for S&W Waste. Inc. to receive PCB's. Any generator and/or transporter who knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal prasecution. trrr-r^ hereby warrants that materials transferred by it to S&W Waste. Inc. for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl (PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby agrees to idemnify and hold S&W Waste, Inc harmlessjrom any costs, damages or other liability resulting from the breach of this warranty. Jr-5LlV^'0 C ^ Q A K U 1 \ ^ CO nr(^<. DATED: 3-)l-SV =Y. fii^CU'/>v^.S^^;k^^^ WITNESS:. ^^1*/ EHJerbicide/PesticBde Warranty - p ^ • ^ ' y . ^ y, - A fy=^-. -"^^ ^ z - '^-^^ hereby warrants that material transferred by it to S&W Waste. Inc. for transportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level greaterthan 0.001% when measured in each containerorvessel transferred to S&WWaste, Inc., and hereby agrees to indemnify and hold S&W Waste, Inc. harmless from any costs, damages or other liability resulting from the breach of this warranty. ^ S i^fYtZ'O C t-pe^ C C n-\-C (J DATED: ^- j y ^ ^ „v. ^ V r ^ d ^ ^ l ^ y — /CecAjJs- WITNESS: / ^ < < k y y ^ ^ ^ y ^ € y Aluminum and Reactive Metal Warranty ^ ^ II r ' * ^ ^~~ l \ \ k - ~ y ^ ,^^^=-nc_tJ^ hereby warrants that material offered to S&W Waste, Inc. for transportation, treatment and/or disposal does not contain elemental aluminum or reactive metal paste, powderorpigment and hereby agrees to idemnify and hold S&W Waste, Inc. harmless -im any costs, damages, or other liability resulting frornJoreach of tbis warranty ^ ^ ,T^^ J-^^: DATED: _ ^ : l L ! l l i ^ BY: ^ ^ U^CM, WITNESS: y Z ^ ^ ^ p ^ y c ^ ^ i z k L y / (/....... 301481 PRIORITY POLLUTANT VOLATILE ORGANIC ANALYSIS LABORATORY ID I U U 6 LAB # 5295^ • - - • CLIENT: ENVIRO SCTgNCES-Islar.d Cherj^'cal P r s i e t SAMPLE S O U R C E s a r i D l e l l -• ---.-:. GC/MS Method 6 2 4 * Tier II Deliverables PARAMETER Chloromethane Bromomethane . Vinyl Chloride -- — Chloroethane Methylene Chloride 1,1-Oichloroethene 1 ,1-Dichloroethane Trans-1 ,2-Dichloroethene •— Chloroform ; 1 ,2-Oichloroethane 1 ,1 ,1-Trichloroethane Carbon Tetrachloride Bromodichloromethane : 1 ,2-Oichloropropane Trans-1,3-Oichloropropene Trichloroethene Dibromochloromethane 1 ,1 ,2-Trichloroethane • Benzene — • cis-T,3-Dichloropropene 2-Chloroethyl vinyl ether Bromoform Tetrachloroethene 1,1 ,2 ,2-Tetrachloroethane — Toluene Chlorobenzene : Ethyl benzene Total Xylenes *Dichloroben2enes noc analy2ed under chis mechod. RESULT ug/l u IJ u u u u u u 8 . 2 3 u u u L' U u u u u u u u u u 3 . 9 0 0 B U 6 . 7 J U METHOD BLANK u g / l u IT u u u u 7 . S J IT u u u r: U U U U 2.0J u u u u u i . 9 J U u u MDL I n ! n i n 10 10 10 LO LO LO 10 10 LO 10 10 10 10 10 - 1 0 10 10 10 10 10 10 • 10 10 10 10 Analyzed by GC/MS Mechod 625, 301482 X^CV-JVJ:'^ INDUSTRIAL - CORROSION MANAGEMENT INCORPORATED NJDE? Certified Drinking Vacer/Vascevate- Laboracory ID-:/ 14116 RZPORT DATE: April 16. 1986 LAB H 52954 .1152 ROUTE 10. .RANDOLPH. NfW JERSEY O/HSi ZCl-SSi^ljO CLIZNT: ENVIRO SCIENCES - Island Chenical Proiecc SAMPLE SOURCE: Samole 5*1 SA>C?LE DATE: Februarv 2S,.19S6 TAKEN BY: A. Kvles AT LAS DATE: March 7. L9=: LA30RAT0RY ANALYSIS REPORT PARAMETER. RESULT Ben2c::h£r.cr.a Neac Benrochancr.e If you should have any quescions, please do not hesicace t o call. INDUSTRIAL CORROSION M.^AGEMZNT, INC. Richard S. L Presidenc RSL:dlh y/<^.C6'/S^,f 301483 INDUSTRIAL CORROSION MANAGEMENT INCORPORATED 1152 ROUIE 10. RANOOLPH. NEW JERSEY 07865 2Q1-S84<1320 NJDEP Cercified Drinking Vacar.'Vastavace- Laboracory IDrf 14116 REPORT DATE: April 14, 1986 LAB il 52954 CLIENT: ENVIRO SCIENCES - Island Chemical Proiecc SAMPLE SOURCE: Sample ill SA-^dE D.klZ: Februarv.28, 15H5 TAKEN 3Y: A. Kvles .Kl L.\3 DATE: y.a: LABORATORY ANALYSIS REPORT P.ARAMETER Ignicabilicy Specific Gravicy pHCunics) RESULT ,Igr.iC5s wichouc persisc=r.c burni: 21.97 8; 06 If you should have any quescions, please do noc hesicace co call. INDUSTRIAL CORROSION MANAGZMEin, INC. RSL:dlh lichard S. /Lev^tne P r e s i d e n c / 301484 ycyt'C'j/iS' Appendix J Disposal Manifests \WORK\24231\02 \WORKPLAN.REP HARDING LAWSON ASSOCIATES 301485 nAZ.A,iuuub WASTL MANlPtb" 1 ^ y ^ (As Recuired By The Alabama Department of Environmental Wanagement) •••Jfc« bnnt or TVO*. I f o r m aesigned for usm on e/it» ^J2-0itcnj tyo9>Mf,ttf ; •: U M I F O R M H A Z A R D O U S W A S T E M A N I F E S T / ' / - ^ i f - g . g . ^ ^ r ^ / • tf^^ • i H T ^ ^ y i ^ ' ^ i vjffnoraior & t%atT\a ana .N^anin; Acores& S'oto y/^/yy^*y^ /€o&a G«oeraiors Pnnne i Z < ' Z ) ^ 9 < i . ^ - < y 0 3 foem Aooroit9< ^ res 7-31 -SS 2. Pa«* I ATiACHMI}.. K ,7-7777 01 X F a c a r al T r a i l e r Nu=ber .=::M.- 251880 > ^ S u i * M a n t a A Document Numcw •:-CW!V1A.:--2^30 3 i B. S u i a d m n m r a i o t a 10 "' • ^: • v ' . ' t. . - Z • -.''-.' TtTnsoonaf . i-omoanv \ d m « O'yy^^yiC's TyZocxyiyG. « r.€3yccyz, T y i B * t f / > o y r - , y ' y r C 6. US EPA 10 Numoar C S u i « . . T i s 10 "orTfi ••» .PT«n« iransoonar i vomoanv >^am« yyiey</yt., yr.i'yyttyy r.*9yi£yKX.7~yy/e. u s £?A 10 Numoaf £. Stat* T r a n a o o n v » IO uasignaiaa racmry HMtrta anc Siia Aocras^ C H E M I C A L W A S T E . M A . N A G E M E N T . I N C . E.Tieile Faciiiry A l a o a m a HiyivAay 17 at M i l e M a r k e r 163 Emelle. A l a o a m a 2 5 - i 5 9 \ ^ i ^ ' D '. 9 ' - f f l a l A i r f l « I J ^ 7 -C I F. Trarv«oon*ri PTxx»« 107 US EPA 10 Numo«r I A, L| 0. 0, Ol 0 , 6 I 2 I 2i 4 , 6 I 4 C S u t a f a o i t r y t lO M. FaciuTY 1 ^ i o r m 205/652-9721 11. US OOT Oascriotior\ llneiutiin^ Prepar Sliioomg Nan-im. Maja/a CUia. anc ID ftv/ncarl 12. Containars I No. I TvOB ' 13. Total QuantiTv Unit i ! w i / V c l W a I ^*o. ....-! y y ^ z y y ^ c o ^ -^<i^.'/c-. yyC'^yy:' ryzy/'yTc/.^yt/yytZ. ^ , A y j c / y y ^ ' ^ c y e / y - y y y y 9yf^ C.V.M Profile N u m o e r y C A Z ^ i ' 7 . Z C ^ C ^ I ! 1 !) . / 'A 'AS ! yrs-iyyt'^r-.y.. c / y e y y p ^ y y y y ? 9 y & 7 c c y / A Z y^yy^y^y^ y y c ^ / A c K ^ t / y y c f cy^-'ycyz-yiy,')! C'.V.M P r o d l e N u m o e r yAy^/ZZA 9 ^ ^ ^ 3 /<yPByCA/:a/yj /yySJ/z.- sa/ua yy:Jk7Zc<y»f<, <S'(Zf^cayeai^,fysyJJ\ &,CA7-y yyy f y / ^ C . ' A , 1 Profde N u m a e r y < ^ 6 ' f ^ ^ l / ^ C i / ^ 6Sd'AA\ I I I I I / l ^ ^ I I I o. C'.VM Profile N u m o e r I I .. AooriKxiat Lkeacricuons lor M s i s n a i x u s i a a Aaova y /Ayf^AtUJ T^y^Af y./,'yi 7o<^-*»c y ^ * ' S ^ S ^ < - 'P. - / / £ . yyy-^yieyynAfZO/ jz^ 'A a>yt4:Stty£.j/=yzyy^y>y^yi-y ^ ' / ' ^ y c y^cc/ftt... 'kziApt. / / c s x i^Psxu / ' ^ ' / ^ T ' ^ c ^ j M * ^ ^^y*y> jSta^ liws. CAAeyt^y^tmty I I ! I r 15. Soociai nanoiing insiructions ana Aaojiionai irTo/mation K.. Hanoling Cooes tor Wasias u s e e Aoovo /z^i 3. doociai nanoiing insiructions ana Aaoitionai irTo/mation / >. ^ / / c . J ^ y > c M ^ y ^ ^ i c ^ 2 i y y < m / . yfAuy^y^ ^ ^ - ^ - ^ 5 ^ ^ /yy^,y>yoyi ^ ^ ^ ^ 1 6. G c . N E R A T O R ' S C c A T l F I C A T t O N : i nereoy caciara tr^ai tna'caniants oi mis ccnsignmeni are tully and accurately aescrioec aoove sv prooar snioomg n a m * ana ara cla»i<i»a. oacxec. m a r i a d . ano laeeiaa. ana ara m ail r a u e c u in prooar conoition lor iransoon Sv n i f rrway accordir>g to aoplicaoie iniarnational and national govemmant refutations. Unless I am a small auanriTy generator w n o Kas deen examotea Sy statute or regulation Irom ine Suty to make i waste m m i m i ^ j n o n cenification unasr Saciion 30C2(&) of RCHA. I also cenify tnai I nav« a program in place to raouca tne volume and IOXICMY ol waste genarateo *.o ine oegraa I ttata determined to ba economically practieaol* and I nave selected tne mctnoo of treatment, storage, or oisoosal currently avaiiasie to me w m c n m:nTmiras tne oresent and futura threat to h u m a n neartn and tne environment Print»a/7yt3ed N a m * 1/ 1 yced f<am« ^ ^ A:. pZy/M Signaiufj ^ ^ c A ^ < : ^ i ^ M o m n Oar ''«« / t O i / a \ f f i . T 17.Transoon«r 1 Acxnowi»agem«ni ot R*caiof of Matariais O^Neale s xransporc Inc. Signaiura (1- m . /CU;, *^ u t^ ? ^ ' Mont/1 Oar yat 1 II nlir? te t O IS.Transoonar 2 Acx/^owiaagamant ot Recaiot ot .Materials (^r>»tad/Typed Nama / / S i g n ^ u r * kykkyZc/fyy. Mortr/1 Omt Y»» y y y , Aky)y^k: TsiOiscraoancy indication Soaca i y yy^/z T 20.Facility Owner or Ooaraior: Canilication ol recaict ol na^ardous materials covered Oy this mavTiast V^ceot as noiec m nam 19. Pr:m«Q/Typ«i N a m a ^ • A h y A ^ / A r > y ^ P c - ^ Signal -pPczcAuAyy/zl.^ M a m n Oar Ta \/\z.s>3y EPAFt«ng7oo-22(R«.*.8B)Pr.vH.ui«iitK)n.1 oDMiaia. STATE OF A L A B A M A (Mus/Acccmpanv Shipment) y///' - ) , . ' ^ • ' . 301486 u UNIFORM HAZARDOUS i » ; . v j e n e r j i o r j '.,5 £.-A iC . \ o . M a n i i a s i O o c u m a m No f o r m A o o " - e a C M S MO : C X > lyto-i E i o . ' n 7 i i A y /) 9 S o 6 s ' / o 9 s - WASTEMANIF^-^T- (ContinuaTioc/SheeT) 2 3 . G e n e r a t o r s Njmv.- , " ' - a i l e ' " N - i r i h p ^•^"'•t? '^zz'"yy'y.- Azy^tz . ^ y y y y y y/tle^ -:yjyj/.y C * * « J ^ C?oy/^ fvr - ^ / i » 1 4 . T r a n s p o n a r V.omoany N a m a • . . . r a g e Za/Z, i n i o r m a i i o n .n m e s.-.acea aress IS n o l r s Q u i r e d Oy P o c a r j i l a w iZc'cyyc-Cye. yy^^yy^uyyzy: ; C . ' f o n t p n I ' l m n a n v N a m a "is. u s EPA 10 N u m o e r y e a <? g o ff O S 9 7 7 L. S l a i e M a n i l e s i D o c u m e n t N u m o a r CWMA ^ 4 - ^ ^ ^ / :-:-. M . ^ t t i s G a n a r a i o r s lO "" !— U S EPA 10 N u m o e r N. S l a i o T r a n t o o n a r s i U 0 . T r a n t o o n a r s. P n o n a P. Scaia T i o n s o o a e r s 10 . . - • U . T r a n i D o n a r s ^ " o n a ~ T p _ i, 7 Q r o / t Q 28. U S D O T D e s c r i p t i o n ( I n d u l g i n g P r o p e r S h i c p i n ^ N a m e . H a z a r d Class, a n d ID Humberl^ . i S . i - o n t a i n a r s '...'fia'is y'yiyjy/3uy,^C>S^^^^^^^sy-Z r r r . i rre:..e Numoer / k j ^ y ^ T Z C Z z k — ' - No. ' "vpe T o i a l Unit [ uant!Tv ».M.*vo! W s i i e No.- •- LU °- ~Zv^2Z^/^ylcy/:S c i / ^ y Z y^<?cy/c yy<-fAy-scc/,iyyt^,fcy^cfirey/7^ ]^Z1L\ a p y y f - t f >y/f 9r&9;zz:z C.V.M " r o f i l * N u m o e r -.k y<yA3 <fF^a^ I .A<k^AAi y/s^euyyf**^ AiAtxyT^ ^ A k y i ^ AA^/ y:z:c<y^MC^ /(Zy/cyi^f^Xjat/ < ^ y y y ^ y y C y y J ' / / J ' V ^ . C-.VM P^ome N u m o e r ^ ^ ^ ^ t p ^ ^ f f ^ i I CV.'M Profile N u m o e r C W M Profile N u m o e r C.'f4tyi Profile N u m o e r ••^zzz:y^'->. YkAkkkkAkk g. C'.VM Profile N u m o e r zyzkyzAPz C'.VM Profile N u m o e r C'.VM Profile N u m o e r , , . ,,i;~r,:.-.- S. A a d i t i o n a l O e s c i o x i o n i for M a t e r i a l s Listea A b o w \4* . i ^ ^ * Ay( 77"^ Jea^ti^ A2<:i!^:^ T . Hanc.lmg C c c e j i o r VVajtn l_ii:ec A b o v e a. a . . - 9 . •--;'•• b. e. r i : •. 32. S o a t r e i - r f a n a l i n o I n s t r u c t i o n s a n d A c n i y t i f t ' ' ~ i . r — .T.t". yy • _ * _ , y > • / - > , y i . g g / r ^ • _ y . c/pZ ^ i y < ^ . y^k/cyriZ^.* 33. T r a n a o o n a r A c X n o w t e o g e m e n t o« Raceiot o l M a t e r i a l s 34. T r a n i o o n a f " ^ A c x n o w i a o g a m e m or H a c a i o t of M a t a n a l i D a t e T/Stl/^T /T) klcz/^oAjy^lATk^Tr^^. 1/0-1 C^ 1^ 3 5 . OiacrapanCY i n d i c a t i o n S p « c a 3 0 1 4 8 7 n/MA. tUUU^WAb 1L MANiFEST (As Required By The Alabama Depanment of Environmental Management) • a sa onnt or rvDa. t f c r m emsiqnati for usa on alira f t 2-oitcftl tYoe.mrner.1 f a r m Aoortitietl Q M B Na. 20<X-C.iCJ Eioitfs 7 . J ; UINJIFORM H A Z A R D O U S W A S T E M A N I F E S T i. vjtfherator s Same ano .Vtamnc Aooress SscSMP Cy^y/CSc day>ryffy/ty 3'ffo yrt^y/irysu) ^oSa oyyz-ia aiyyj'yyt^, ^.Ciiy--A,Ljej/ty c**» *u 4. Generators Phona ( • Z - ^ / ) £ 9 < i - t X / O O I. uanarator s uS cPA 10 No. Manilas! ^^^^^/>'7.g; o i£ I r- /: oy^i^f^i^^o*^ 2. Page I ol Z , Intormation .n ir.a $.-iac«c i r e i s '» n o t r a q u i r a o Sy f e o o r a i (aw. Trailer Number I^ZLZ 680365 A . State Mamlftsi Ooeumant fnimcar cvvnviA_24303 2 Q. Stata Ganaraior $ 10 3^ transooner 1 Company Name QZA/£^<-ff ryyycjiyyye- .--t-«3 rf.sycj:y.. r/iS-uU y>oxr~ - ^ y / c . uS EPA ID Numoer C S u t a Trantoonar s lO \ / ^ ^ . / S . ' . £ > \ 9 ' . S \ a \ ^ \ P ' t ^ \ £ ' \ 7 ' 9 i 0. Transooner » Pnona .ransoonar 4. company Name r/iV/cc/i. y^yayAyif y^z^jj-rya^rjj'yyi. 6. uS cPA lO Numoer l-^'/^'^)! ? i ^ l <:>.6^<3.\ <£.:£'\ 7 ' 9 E. S U i a Traruooner s 10 P. Trartsconer s Phone < - / y : f f . , , ' i r — \ i / i > - •- • " * ^r-_L-^ / t~. I.J ^. uasignaied racmry Name ano ^ i i e Address C H E . M I C A L W A S T E M A N A G E . M E N T . I N C . Emelle Faciiiry A l a o a m a Hi9nvvav 17 at Mile M a r k e r 1 6 3 Emelle. Alacjama 35-^59 10. US EPA 10 Numoer Al L. D. Ol Ol Ol 6 I 2 I 2i 4 I 6 I 4 G. State Facility s lO K. Faciirtv s Phone 205/652-S721 1 1 . u s OOT Description (Including Propar Sfiipping Name. Hazard Class, and ID Humoar) /y^-By/yz/yffcyj /yy^'^/z A/^cyy/y yycs(7-oca,f»i: p/S^^zu/e) 12. Containers No. I Tvpa 13. Total Ouaniirv Unit 1 W i / V c i Wasts No. oyty^-e' yyy9A,/7 C^•^/^.l Profile N u m o e r ^ . ^ ^ t p g ^ C 2 . ! ••^1^./? ! I ! I A/^£y/C/?ciys c<y3tj/c Ayg///^ -^y'c/'(y^</.ur^ ^(Zyt'ccyecyo'ijA) C7/<y7/&£' y 0 j y <P/P(p c.-.TVl P-=file N u m o e r , , < ; ^ _ ^ ^ 6 0 . s \'C/)\AA I AyPcAyLaays c a ^ r S Acyy^o yycf {/r/c;s<L i>/Cayif/Jj C } ^ y 9 / ' y y/yf f'AiPP C:-M?ToneHt,mbtryC6y^^(ffi7^ [kmiA. C".\'M Profile N u m b e r I X AdcitKxiai Descriptions tor Matenais Usied AOcva . VAs..- / a ^ y /9^a¥ty A o y i -f^ht^iCfxe.. OftoiC &>^tyce.^ k / / 6 ' y ^ ' ^ c y - ' ^ ^ ^ r ^ T i ^ ^ O y i ' C y ^ ^ 0 ^ t P . y / / 3 y j y P a < Z / f ' ^ ; ^ ^ ' U ^ ^ •'-'•" r " --' -' yi>f/pZyZ ' . ^ ^ ' V / g . • ^g<w»*»*? c r P ^ ^ jOtiyyUA/ t^yZ y » ^ * ^ y Z ,^yt^y»^ e v / yby '<A/ K. Handling Cooes tor Wastes u s e s Asova 15. Spvoat nananng instruciions ana Aocitionai irformation /Ac,. ^^^^jKPi* U P U J .yyiy^<^ ^yi<.^j^y^usCy ^•*'iA^^^Pj^iy^m t u ^ ^ Ceyjy>fy? i . y 16. GE.NERATOR'S C E R T I F I C A T I O N : 1 nereov declare mat tne cements ot tnis consignment are tuily ano accurately oescrioeo aoove oy prooar snipping name and are classified, packed, marred, and laoeied. and are in all resoaas in proper condttion for i r a n s o o n oy hignway according to aoolicaole intemational and national govemmertt regulations. Unless I am a small quantity generator w n o has been exempted by statute or regulation Irom the dury to make a waste m i n i m i i j t i c n cenification under Section 30021b) ol RCRA. I also cenihy that 1 have a program in piaee to reduce the volume and toxicity of waste generated to tne degree I hava determined to Ba economically pracricaole and I have seieaed the method of treatment, storage, or disposal currently availasie :o me wnicn m m i m i i e s tna oresent and future threat to h u m a n health and the environment. V Printed/Typed Nama yk^'S/y y / ^ 9 c & Signaiur ^^/^^c^z^pdy v M o m n Day Year \ A a \ y y \ P J T 1 ".Transooner 1 Acxnowiadgement df Reeaim of Materials •i^ud" / L . Printea/TypsP Name Oneale s iransoorr Inc Norton C. M. Burt Signature • Montn Day Year IS.Transoortar 2 Acxnowieagamen^ of Recaiot OT Materials Prirjtea>^yp«d Name / / kzy/PykJyy yzkLy yzz aignaturv / / / ^ - , M o n t n Oar rear .yp-Yya. Z y / y - ZAy y-^:^,?^ 7r~y3 IS.OiscreoancY tnaicatton SoacA / EPA F o m . 6 7 0 0 - 2 2 ( R « . 4-aB) Pravtoua edition IS otaoiata. f T T A T P O P A I A R A U A / M I . « r t - < f l > r m m r . n n v S h i p W ^ T ^ ^ a o . t 5 ? ^ l / Z s O 301488 ' ^*<taft« o/'H! Of rvp« (Porm designed for use on eltte fl2-0tTcri) tvegwfTer ) V UNIFORM HAZARDOUS -* WASTE MANIFEST (ConTinuation Sheet) 21.vjcnerator i uS c?* No. /tannest Document No A / j> 9 / C £ S'y a 9 - ^ y C o o s fai^.f. A eo'o»»a QMS So :ooo OJ.-.4 E.c..-^ 7 : • 13.Generator J Name IscPttA^ Z'y^/yc^^ < - - * " ^ ' y T r a i l e r Nunber Soo y^yi^^yryc/js y^eru, ^-^a-^o ""TMIZ 680365 Ci/yk/A/Jif, yy£a) tJ^A/€y (9ai-siao rTc ^ o y - ^ ' p i ^ . ^/.oo 14. Transooner O C o m o a n y Nama f s ! uS EPA ID Numoar 7?5y/&CA. yyATTtfy/Mi^ti. yy <^ y) 9 9 o 8 0 2 9 7 7 ...rage ;^yy. inioi.-anon m ire snacec afeas IS not reouirec 6v Federal law L. Stata Manitast Oocurn^ni Numoer CWMA yz^^^z.^ 26. ^'enacai^e' Go^gany '^•'"in pvn—:—r, ^ " r ' L 27. US EPA iD Numoer M.State Generators ID N. Slate Transooner s i3~ 6. Transooriar s Pnone P. Slata Transooner s 10 r s . US DOT Dascnotion (Including Proper Shipping Name. Hazard Class, and ID Numoer, 29. Containers No. I Type U. TransDonor s Phone'^ "j p ^"^^Q f:"} I' Q ZO. ^ ^ ^ - . . / - Total Quantity Unit I R. gV(^^Vqi Waste No. '• JA^^y^yk^a^ jt/yzr/x Aypc///} yiyyjLr^7ocL/af^^.^w^) C-.VM Prolile Numoer y ^ / j U ) j J / J S ^ ^ - L Z ^ \/^Ai ' A/rnyiyiyjoaa 'c/As4^ /^yp<yyy) /yesATTicujttit. f ' 77]^ dAy\ ^ - r.n.,yiyypry.Zya<il / W d/-' C'.VM Pro file Number • ky/k/ /t=Z^, CWM Profile Number I f. C'.VM Profile Numoer C.VM Profile Number h. C'/VM Profile Numoer C.VM Profile Numoer S. AdOitionai Descriononsyor Materials Lisrea Abme • ^ ^ / i . : A i ' ^ ^ j » ^ ^ A o ' y ' ^ y u M K ^ t g ' y^^UtTZiy^ e Z u ^ ^ f i ^ y / i i i/ayii,/ T. Hanoling Coces for Wastes Urtea Above a. ti. g. b. e. h. . c. f. . i. 32. Soeciai Hiae*rr[5Tr\itr' C2Ac/yC/. Y T 33. Tranaoonar Acxnovwioogemani of Rocaiot of Materials Date Rrvw»d/T;yp«<J Nama Drrrr—me r- i.t - Q , . ^ . 34. Tranaoonar "^ AcXnowi>ogament or Recaioi ot Materials ZZZ Signature yy Mantn Day Ye. Pript««l/Typ«a Nama y - \ ' ~Z fianaiure t l \ ^—-* / ] I Date Momn Oav Ye. \/Z2L 2J V 35. Oiacraoancy Inojcaiion Spaca N :PA Form 8700-22A (3-84) STATE OF ALABAMA (Must Accomoanv Shioment) 301489 UrvJIFOBIV. HAZARDOUS hAZAr^!JUUS"WASTL i/iAf^iPEST (As Required By The Alabama Department of Environmental Management) form AoBrommtl. Q M B Na. 2000-0^-^ i r e n t s 7.2; v u a i a onnt or type.. (ferrri easign^c hsr usa on alita (12-oitcni iroamrnttr I WASTE MANIFEST Mailing 1. Ganaraior s uS EPA iC No. ^ • n a r a i o r s .Same and Mainrig >«doress .Zst-S-iya /Z/JCyfCSt^ (Z^arrya/yy ^ o o < y y y fy£yy> / Z a : ^ 4 Generators Phona I S ! o / | ^ - ? « - ^ / O S Vx//>P S-0'^-s.y'0^9^^:P°r^'''P^/ 1. Page 1 of ^ inlormaiion m iha SPacec areis n n o t r a q u i r a o Sy F a o a r a i i r a : Ler Nu=:ber RTMZ;27^676 A. Slat* Maniiaci Oocumam Numoar CWMA 2 4 3 0 " a. State Ganaraior s lO v J U v 3 Z .ransDonar 1 Comoany A^ame a 'yyiS'iXsyr r^iyey^yyc yi /TZ^/uAt r t i i £ y y s y ^ y —. r y y l . ^ 6. US £PA 10 Numoar C Stata Trantoonar I lO O. Tranaoonar a P h o r j transooner *. .-ompany ttArnn y ^ - ^ y c s / i . yr7Aijcyyy^ y/fayytSr^S^r-^ X y / C ^ uasignatad raciiiiy Nama ano Site Address C H E . M I C A L W A S T E M A N A G E M E N T . I N C . Emelle Faciiiry A l a o a m a H i g n w a y 17 at M i l e M a r k e r 163 Emelle. A l a o a m a 3 5 ^ 5 3 uS c f A 10 Numo«i \/':/!:,/}\ 9 y : C ' ^ ' ' i \ ^ ' S 7 \ 9 £. State Transodnar s 10 P. Transooner I Phona I I ! I 10. u s C P A 10 Numoar A, L, 3. 0. Ol 0 . 6 . 2 I 2i 4 1 5 1 C S t a t * raciiiry a lO H. Facility s Phona 205/652-9721 I t . u s OOT Oaacription (Inelucing Propar Shiooing N i m : rrmjard Class, and ID Numoarl 12. Containers No. : Tvoa 13. Total Quantity j Unit i Wt/Vol • - r . • - • Waste No. G l a T £ | Nl . /yyzy/eAi<J</j a'/}sr£ tTac/yi yyyos CAc<-u'€'iye fy/cer^rrrej \ C/CAt-CZ C-.VM Profile N u m o e r / f ^ / ^ ' < r . ^ g g ' < a J I l / i ^ ^ i / T t I I I A l 0. ^y^zyijcacus o/StJTZ Sci/yi yyi:>s(~<su/£y^ (£Cy//yp^o/='a^y>t) c/yiyr>'i^ y y y 9/(f9 cw.\9^ou\tfi^mott/pc/7/)<^f^yy^\ ^zy£>Af\ ! I y^Ayyy AAy ^ / f y C.%-MProfi.e N u m o e r ^ d ^ ^ < $ y g ^ ^ | t ^ / ' ^ l / > ^ | | a. C'^VM Profile Numcjer AooitiorMii OoacriptiQfa ior Ma APiu I I ! I 1 y t a t a n a i s u s t e d AOovv _ ^ //Oty. Aess yPctj A.o 'A 7<'<yy-*>*» <»^*</^t^«^c^ Z / / 6 a A - * ^ ^ T ^ a y f / . O ' / 7oU/-i»tc i l r u < (!y/tifiy^i3/i/*t //t* /e-LS f^a^ P ^ y i 7^/Mme^ a^,ai£^^t^K^ K. Handling Cooes tor Wastes u s e d ASiove ^ . ^ - . d. • t a . Special nandimg Instryctions and Additional iricrmation y l / a ^ € ' / y / 7 k i ; yye^" 0yA6. Joyc,. yf.:y^r-/?<., yy/r-/r,z^ ySy cyi/'Cy-y^yp yyy'cyL /~o 2yr-r=^y.yt/z€/:- yy^-:.:! JT. cy^yiz. y'f/€y^.'y/-'^yyj<:cy£^ ' i 6 . G c N E H A T O H ' S C E A T t P i C A T l O N : I nareov o e c u r t mat :n« contents ot tnis consignment are tuiiv ana accucaieiy aescnoao aoove Dy prooer sniooing n a m * and mr^ classifi«0. oacxati. rrarxac. »r\C taDaiad. and are m all resoecrs in prooor condtiion (or iransoon Dy n i g n w i y according to applicaole international and national gov«fnmcnt ragulations. Unlasa I am a small a u a m i i y ganaraior w h o has &««n exemoieo by statuia or regulation from tne duty (o maka a waste minimization cenification under Saction 300Z[b) of RCAA. I also canity tnat I have a program m place to reduca the volume and toxicity of waste generated to tne degree I have determined to be economically practicaPle a r ^ t f\m>f% selected tne metnod of treatment, storage, or disposal currently avaitasie to me w m c n minimiies tne oresent and future tnreat to h u m a n neatirx and trie tnvtronmeni. Printed/ Typed Name /^CffA/ P . PZi/tZS Signature »ignature ^ J ^ M o m n Oar Year \Atr\/7^Z>yz 17.Tran*ooner I A c x n o w i e d g a m e n i of Receipt ot .Materials Prinied/Typwd Name O'Neale"^s T r a n s o o r t I n c Norron C.M. Burt Signature m. /d-o^tt yH. Montn Day Year 11 ! 0 11 I 7 18 ' = 18.TransDonar Z Acxno>wiedgement of flecetoi of Materials n a t u O ' - ' ' / * ' '"" / / Montn Oav Tear J/yAyy/kL yfA/y// c^ A T ' A ' /k^k)y\ y PTimsj3/Typ«o Nama . / pyyyypA //yye/z/ I Signaiu IS.Oiscreoancy Indication Space (T^^y L lO.Paciliry QMmer or Oparaior: Canilication ol receipt ol naxarcous materials c o v a ^ by this manilesi eig4ot as noted in Item 13. P f t m a o ^ y p i d N a m e ^ 4 £ ^ _ j ^ > ^ ^ ^^r ircf~~ . ' " J l y . ^ K. t y / o , — . . ^ ^ y J y . . . . . . . i I . t i . / . " M o n t n D t r r e t i i / ' ' 2 r < ^ 3 i r ^ IPA Fo<m 8 7 0 0 - 2 2 (Re«. 4 - 8 6 ) Prevwus adilion is o m o i a i a . S T A T E OF A L A B A M A (A\ust A c o D m w j w ^ShiRfSrW^^ / f d l A J ' O 301490 .11 Of rvoe I f o r m c t f u a n e d ' o r use o n gtite (1 2 o * t c n ) t v o e w n t e r I UNIFORM HAZARDOUS WASTE MANIFEST (ContinuaTJon Sheet) A . . u o n f r a ; o r i .^5 £ r A i J .No. M a n i l e s i " O o c u m e n i N o t o t f *oo'Ov«e QKiQ No roOC 0*0* C.o"v^ 7 31 n6 3 . G e n e r a t o r $ N a m e . y s c S ' i M } d y y y y ^ ' < ^ < - C ^ i f ^ y ^ y y / '^yxyy/^^ y / d ^ yyCf-iy • WO«;urn«ni (NO. y / y> 9 8 o ^ s / o 7 s\ yzZoo / ^ ^ ^ ./-ag« i n l o r m a i i o n .n : r e s . - j o e o areas IS n o i ' e q u i r e c Oy F o o e r a i l a w Trailer Number RTMZ; 274676 rtC .a0/-6 P'i. €.yoo L. S l a t e M a n n e s t D o c u m e n t . t u m o e r CWMA Z^S^Zsy M . S l a t a u a n a r a t o r s lO i f a n » o o n a r » ^ C o m p a n y N a m a y y - ^ ^ / z / . . y A . 4 T-zt.t^tijfjxi- ' ^ n ^ ' * " * t n n - a ' -• " " • ^ - - " y N a m e . ; 5 . u s c P A lO N u m o a r JN. State T r a n s p o n a r s -G ^ r j y < ^ - 0 7 g a 9 t o 3 . 9 7.7l^7rt y r I - d . 1 . U S EPA 10 N u m o a r r a n s o o n a r 4 P h o n e P. S t a t e T r a n s p o n e r 3 . 0 U . T r a n a o o n a r s P f i o n e ^ i n 2 8 . U S O O T D e s c r i p t i o n ( I n c l u d i n g P r o p a r S h i p p i n g N a m a . H a z a r d C l a s i . a n d I D N u m b e r , '• /pS^AA/ezzpiyr-a/u//^. zi)Ly/.y -7=6^<T- -^^^ Py^^iy^S^k^ y e / y - ^ y , y ^ 9 ^ f ? . . y^!4y^^A&2^ 2 9 . C o n t a i n e r s No I Type Total I Unit I G u a n l i t v ' A V . / g l :i?G,;;9/io R. • '-• W a s t e N o . Azy/>A^ AyzS<^eA9U^ ti^y^^/z Ao/jy.^ Ayc.r^^4.<^^ f i^<'<ii.yj/Zf.iitifk^ I I " y^.y2><?/u;^ -^.a,?Uu/i < 7 y y V - y y y y _ ^ y f i O _ _ -Oil.'.! ".'.ll" e .*wmo«r XTSu/Z^c -fyU^yAy^J —-" crvM Prolile Numoer y c y ; i i y ^ ' ^ C'.VM Profile N u m o e r L y ^ y C ^ / r / / \ . . y - Z ' - - - • • ' : I ':-Z--Zz:-~-:'y~.i \ :-.--zyz-----'-1 C W M Profile N u m o a r C'.VM Profile N u m o e r C W M Profile N u m b e r C W M Profile N u m o e r C W M Profile N u m o e r -TS. A d d i t i o n a l O e s c r i p t i o n s ' o r Materials L i s i e a A b o v e I - _,^^»»52^—V»*.BCi/&»^Zeey TScia^ ^^*y^ dyj'J-^"^^ ^ • T . H a n o l i n g Coces l o r '.Vastes U$:ea A b o v e b . 22. Sutti-TTi uiiUTi.ig i n s t r u c i i o n i a n c A a d i t i o n a i Inforrrvation sZrP P^yyT^-f-yrtyr X7$^rr<j AAa. i( yy<<. yyc/jr" /?^: y-yy/ypfcrco y^yyfsiy^rAyp yyycy:y 7c J/iA'Pye^^/jetL yryoTT' yiCyecy/: yt^y^yr-y^ccy/ter^ y/Z^AZyyy' Acy^p/fj— 33. Tranaoonar A c x n o w i a o g e m a m of Receipt o< M8t%ciais - ^ 0 ? ? « 3 1 - ^ r n ^ t i - J ! ; - , _ ^ ^ ^ T . . I Signature , , ^ ^ j 1 « r. M n..—• 1 /iyyiucr\ C. 777. IZZy-^u: /*-. 1 34. i r a n a o o n a r y Acxnowi*og«mant or Receipt ot MatMials • ' Pf*m»d/Tyo«id Nama ^ . y , , . k j y ^ j / y / K. /L/DUC^-h '"O/rv,.//^ r/^.^#^ a Oiacrarxncy Indication Spaca ' ( Oaie Monrn Oay \ V nl r -, \ - Date Mtfnrn Oay 1 /.LI .^ 301491 1 /ear i R =^1 1 Year 1 \<y\ A Form a700-22A (3-84) C;TATP D P A» A R A M A f M i . ^ A^ cu:...— • Appendix K ESI February 7, 1986 Letter to USEPA Regarding Waste Disposal \W0RK\2 4231\02\WORKPLAN.REP HARDING LAWSON ASSOCIATES 301492 '^^'ij 5CI&KE5 inc. 19 COPELAND RD., DENVILLE. NEW JE.RSEY 07834 (201)365-5256 February 7, 19 8 6 Mr. Conrad Simon USEPA Region II 26 Federal Plaza New York, N.Y. 10007 Dear Mr. Simon: Enviro-Sciences, Inc. (ESI) has completed the proposed scope of work for on site cleanup of the Island Chemical Company (Berlex) facility in St. Croix, U.S: Virgin Islands. The cleanup program and methodology were presented to Mr; Robert Harris of your office in December, 1984 and ammended in a subsequent report dated April 4,1985. Briefly, the cleanup involved decontamination at several locations. These are: i 1) soil around above ground storage tanks - Toluene; ':Z 2) soil around a concrete pad - Toluene; 3) soil along a collapsed drain line - Toluene, Heavy Metals; 4) water and sludge in a process pit - Toluene, Heavy Metals, Benzyl Acetate; and 5) soil in a laboratory waste pit - Pyridine. All materials from the first four (4) locations listed above were containerized in proper 55-gallon steel drums, manifested and shipped as hazardous wastes to Chemical Waste Management, Inc. (CWM) Emelle, Alabama. CWM acknowledged receipt of these materials for disposal. The laboratory waste pit soil was treated on site to decrease pyridine contamination level from above 1000 ppm to less than 2 ppm. ESI considers this level of contamination to be.below levels which would require any additional cleanup efforts. 301493 February 7, 1986 Page -2- The collapse of the drain line and subsequent analysis of soil has initiated the need to conduct additional sampling off-site in the "cut" or dry creekbed. ESI will undertake this sampling program immediately to ascertain the presence of contamination and, if present, concentration levels. We would appreciate any comments relating to our cleanup program at the Island Chemical Company site. You may contact me cr Mr. Irving Cohen at (201) 366.-6256, Very truly yours, ENVIRO-SCIENCES, INC. Alan L. Kyles, Ph.D, Vice President ALK/ak cc: Robert Milos Frank Curtis 301494 Appendix L USEPA Pollution Reports \WORK\24231\02\WORKPLAN.REP HARDING LAWSON ASSOCIATES 301495 4 / I # U.S. EKVIRONKENTAL PROTECTION AGENCY POLLUTION REPORT . y Region II Response and Prevention Branch Edison, New Jersey 08837 (201) 548-8730 - Comnercial.and FTS 24 Hour Emergency DATE: February 8, 1989 TO: W. Muszynski, EPA S. Luftig, EPA R. Salkie, EPA M. Randol, EPA G. Pavlou, EPA ERD, WH-548B (E-Mail) B. Sprague, EPA G. Zachos, EPA P. Gelabert, EPA A. Smith, DPNR LEPC TAT POLREP NO: INCIDENT/SITE NO, POLLUTANT: CLASSIFICATION: SOURCE: LOCATION: AMOUNT: WATER BODY: One (1) N/A Lab Chemicals, Alcohols, Solvents, Acids Major Virgin Island Chemical Company (VI CHEM) St. Croix, US Virgin Islands 800 Lab Chemicals, 400 Drums, 22 Tamks Groundwater, Caribbean Sea 1. SITUATION; A. The Virgin Island Chemical Company (VICHEM) site is located on the Island's south side. The site is situated on Route 66, approximately 0.5 miles due north of the Alexander Hamilton Airport. The site covers approximately 3.5 acres and is bordered to the north by an intermittent stream that originates on the north side of the Island and discharges into the Caribbean Sea. A nmnber of residences and industries are located as close as one-tenth of a mile from the site. In addition, several well fields are located in the vicinity of the site. The St. Croix prison is located 1/4 mile downwind froa the site. DPNR stated it would be very difficult to evacuate prisoners in the event of a chemical fire at the site. B. The site consists of a main warehouse building including offices, the reactor, centrifuge and maintenance buildings and fourteen above ground tanks. Living on-site adjacent to the main warehouse building are anywhere from 15 to 25 guard dogs housed in individual kennels. Also living on-site is the kennel operator, Kate Wesp. A house trailer is located on the concrete surface near the 301496 loading dock. It is also apparent that Wesp uses the restroom facilities and kitchen area in the main building as living quarters. .*- C. Presently occupying the site is the company VIAG Fuels, Inc. VIAG utilizes some office space in the main building and also has ethanol stored in four of the aboveground tanks. The principals of the firm plan to begin an alcohol dehydration project on-site in the near future. D. The 3.5 acre site is owned by Charles H. Steffey, Inc. On May 1, 1969 Steffey leased the property to Houston Chemical Industries, Inc. Houston Chemical assigned the lease to Caribe Chemical Company, Inc., (subsequently )cnown as Pierrel America, Inc.) on March 20, 1972. On June, 1978, Pierrel America assigned the ground lease to Cooper Laboratories, Inc. (Cooper). On October 30, 1979 Cooper Laboratories assigned the lease to its subsidiary, Island Chemical Company (ICC). On November 1, 1979, Cooper Laboratories sold all of the stock of ICC to the predecessor of Berlex Laboratories, Inc. (Berlex) . .. On September 14, 1984, ICC sold its assets to Virgin Island" :- Chemical Company (VICHEM). This background information has been supplied by the Virgin Islands Department of Planning and Natural Resources (DPNR). E. Limited PRP (Berlex) site clean-up and soil excavation has taken place in the recent past under a RCRA enforcement action. Berlex is currently finalizing a scope of work for a remedial investigation/feasibility study addressing soil and groundwater contamination. 2. ACTION TAKEN: A. On Tuesday, January 31, 1989, the U.S. EPA Response and Prevention Branch conducted a Preliminary Assessment and Removal Evaluation at the VICHEM site. This action is in reply to a request from George Pavlou, Associate Director Enforcement Programs dated 1/23/89. B. This preliminary assessment vas coordinated with and observed by DPNR personnel. DPNR's primary concerns with this site are the threat of fire/explosion, and the threat (or actual) migration of spilled materials to the surrounding coil and groundwater. C. The initial entry into the main warehouse building vas made at 0930 hrs. on January 31, 1989. All safety procedures were followed for a level "B" entry in a hot climate. Air monitoring was conducted with OVA, HNU, CGI, Radiation Detector, HCN Monitox, H2S Monitox and pyridine 301497 Draeg.er tubes. All air monitoring readings were equivalent to background (taken off-site), except for in room 5 of the drum warehouse which showed ambient conditions 1 unit above background on the OVA. All further entries were made in level " C . D. Three areas were delineated based upon the type of material located in each of these areas are: A. The laboratory (main building). B. The drum storage warehouse (main isuilding). C. The grounds outside the building including the reactor and centrifuge. Each of these areas will be described below. 1. Laboratory 813 containers of laboratory reagents and unJcnown liquid and solid material are located in^this area. Some of the more dangerous items of note'are as follows: 'vr: ^^^' 'kkr-- » ,• ^-, - a. Sodium metal (2 _boxes). Water reactive. b. Ethyl Ether (6 cans). Potential explosive. c. Diisobutyl aluminum hydride (4 lecture bottles). Spontaneously combusts in air. d. Potassium cyanide (2 bottles).. Poisonous. Stored.near acids, potential for release of hydrogen cyanide gas. -f^ ,,^, e. Phosphorous pentoxide (1 bottle). Reactive. f. Sodium hydride (1 bottle). Water reactive. g. Two flammable storage cabinets containing various materials and un)cno%ms. • h. Two office type storage cabinets. One cabinet has spilled material on the top shelf which has dripped downward to mix with other chemicals. Many other chemicals exist in the laboratory; as veil as many containers vith unlcnovn materials. All the chemicals vhich had dates are at least five years old. 2. Drum Storage Warehouse In-the main varehouse are located approximately 400 drvims, of these, 211 are green painted dmms vhich have the vords ETHYL ALCOHOL stenciled on the lid. The condition of the ethyl alcohol drums vary from fairly sound to extremely deteriorated. Some of the drums consist of only a rusted shell with gaping corroded holes. A rough estimate shovs that 100 are empty and 100 contain material. This material may be some type of sludge. Other materials found are as follows: 301498 a. Laboratory unknowns (75 c o n t a i n e r s l e s s than 1 M gal.) b. Methanol (5 x 55 g a l . ) c. Glacial acetic acid (13 x 55 gal.) d. Benzyl acetate (21 x 55 gal.) e. Toluene (8 x 55 gal.) f. Antifreeze/glycol (20 x 55 gal.) g. Benzyl chloride (28 x 55 gal.) h. Salicilic acid (27 fiber drums) i. Methyl isobutyl carbinol (12 x 55 gal.) j. Sodium hydroxide (12 x 55 gal.) k. iJulging drum, unmarked (1) 1. Drums in which some type of reaction has taken place, lid popped off (2) m. Drums of known and unknown material, n. Paint (97 x 5 gal. - 21 x 1 gal.) o. Cylinder chlorine (1 poor condition). p. Cylinder hydrogen chloride (Ideteriorated condition). g. One dnim of sulfonic acid, broken and leaking its contents, r. A cistern with PVC pipe leading to a pumping system outside the building. 3. Outside Grounds An inspection of the reactor and centrifuge and maintenance buildings revealed various production materials including lubridating oils; propane; oxygen and acetylene cylinders; filter media; ethanol; assorted paints and some sodium hexa-meta phosphate.. Some of the oil drums are leaking. Scattered aro\2nd the facility are eight stainless steel tanks with quantities of unJcnown liquid varying from empty to three quarters full. A large storage tank is on site along with numerous pressure and reaction vessels. Fourteen large green storage taxoks are also on-site." Ten are planned to be used in the alcohol dehydration project. Four of the ten are full of ethanol. The other six are empty. The remaining four not being used are empty and unsound. E. The Governors office Department of Fire Services was contacted to assess local chemical fire control capabilities. Three fire companies are located on the island with the nearest to the site being Grove Place. All firefighting personnel are equipped with SCBA, however, only some have had formalized chemical hazard training. A limited amount of foam capability is available. 301499 3. FUTURE PLANS AND RECQMKENDATIONS: A. The USEPA CERCLA Enforcement Program is actively pursuing PRP involvement in a site clean-up and drum removal. B. An action memo and disposal plan will be drafted by this branch in the event the PRP's fail to act promptly. FURTHER POLRZPS FINAL POLREP. FORTHCOMING X SUBMITTED BY. DbuglaS R. Kodama, OSC ' ' Response and Prevention Branch DATE RELEASED ^ ^ gjl'^g'l. 301500 > I U.S. ENVIRONMENTAL PROTECTION AGENCY POLLUTION REPORT DATE: June 7, 1989 Region II TO: Response and Prevention Branch Edison, New Jersey 08837 (201) 548-8730 - Commercial and FTS 24 Hour Emergency w. s. R. M. G. Muszyns Luftig, Salkie, Randol, Pavlou, ki, EPA EPA EPA . EPA EPA ERD,- WH-548B - • B. 8. P. A. (E-Ma Sprague Zachos, Gelaber Smith, LEPC TAT il) , EPA EPA t, EPA DPNR':. POLREP NO.: Two (2) INCIDENT/SITE NO.: N/A POLLUTANT: Lab chemicals, Alcohols, Solvents, Acids CLASSIFICATION: Major SOURCE: Virgin Island Chemical Company (VIChem) LOCATION: St. Croix, U.S. Virgin Islands AMOUNT: 800 Lab Chemicals, 400 Drums, 22 Tanks WATER BODY: Groundwater, Caribbean Sea 1. SITUATION: A. Same as previous polrep. Site conditions have not significantly changed. 2. ACTION TAKEN; A. OSC discusses contents of Notice Letters with ORC and Enforcement Programs. On March 13, 1989 Notice Letters were issued to the following Potentially Responsible Parties (PRPs): Berlex Laboratories, Island Chemical Company, CHS Holding Company (land owner). Virgin Island Chemical Company, and VIAG Fuels. B. March 30, OSC receives copies of Notice Letter replies from Berlex, VIChem and VIAG Fuels. None of the PRP's are willing to conduct or finance a CERCLA response. OSC informed verbally that Region II will conduct a removal action at this site and that an Administrative Order may not be issued to the PRPs. 301501 C. April 5, OSC contacts D. Weston of VIAG Fuels and requests him to inform Enforcement Programs of VIAG's intended use of ethanol, paints and water treatment chemicals, thus averting the need for EPA to dispose of these materials. D. OSC drafts memo to Enforcement Programs concerning enforcement issues which must be addressed prior to an EPA removal action. Issues include material owned or planned for purchase by VIAG and temporarily evacuating VIAG and St. Croix Security Kennels (SCSK). Memo issued April 20, 1989. E. Draft Action Memorandum prepared and distributed for comment on May 17, 1989. Comments due June 2. F. OSC contacts Fred Schubert, .President..of. VIChem and receives verbal permission for access to the site during the week of May 22, 1989. Mr. Schubert was not aware that there were hydrogen chloride and chlorine cyliners on-site and knew nothing about the cans of ether stored in the labs. Mr. Schubert informed the OSC that he is making plans to repair the warehouse. G. OSC discusses proprosed removal action with representatives from" DPNR on May 22. Discuss possibility of having DPNR order VIAG and SCSK to leave the site during on-site removal activities and monitoring the site prior to EPA's mobilization to the site. OSC will write a formal' request for DPNR to carry out these tasks. H. May 23, 1989, OSC discusses with Lt. Steve Hanewich, the possibility of using the US Coast Guard HazMat unit in San Juan for technical and contractor oversight assistance during the removal. USCG will need a Memorandum of Understanding (MOU) for reimbursemewnt of lodging/per diem and disposable personnel protective gear, I. OSC briefs the Caribbean Regional Response Team on EPA's proposed removal action at VIChem. FEMA recommends that during on-site treatment activities or a fire at the facility that the nearby prison not be evacuated. J. OSC visits VIChem with OH Materials Project Manager on May 25, 1989 to review site conditions and discuss proposed clean up activities for the site. Conditions within the labs remains the same. Drums within the warehouse have been restaged in an orderly fashion however they are not staged by compatibility groups. The warehouse floor has been swept clean and the leaking drum of sulfamic acid has been overpacked, according to VIChem's President, however this drum was not located. One drum labeled "skin cleaner" was leaking. According to D. Weston of VIAG, the company remains inactive and is having trouble getting ethanol from Europe. Within the tank farm., the first four tanks contain ethanol and the fifth tank contains diesel fuel. The red tank truck contains water • •" ...A 301502 VIAG has had water from the on-site well analyzed and determined that it was free of contamination and suitable for their treatment process. OSC inquired if chloroform was included in these analyses, Mr. Weston was not sure. K. May 26, 1989, OSC meets with Winston Turnbull, Director for VI Fire Services and Kirk Grybowski, Director for VI Emergency Management Services and briefed them on EPA's proposed removal action. Grybowski recommended meeting with the St. Croix hospital administrator and EMS's Deputy Director on St. Croix to discuss EPA's on-site decontamination procedures since neither the hospital or EMS is prepared to receive contaminated personnel. L. May 30, OSC receives copies of letters from VIChem (thru Enforcement Programs) stating that " VIChem is prepared to make its best effort to undertake the clean-up at the site" and "As you know, I feel the clean up needed at the site is quite manageable...". This contradicts VIChem's reply to the Notice Letter in which VIChem stated "...I have to indicate for the record that Virgin Island Chemical Company has no funds with which to have any required work carried out and has no staff to perform such work," ' M. OSC coordinates with Enforcement Programs and is informed that ORC and NY/CC will meet on June 1 to develop an enforcement strategy. N. June 2, 1989, OSC has received comments on draft action memo from AD-REPP and at his suggestion will include^resampling of wells contaminated with chloroform in the scope of work for this removal. • 3. FUTURE PLANS AND RECOMMENDATIONS: A. OSC will investigate the possibility of developing a MOU with USCG for MSO-San Juan HazMat assistance during the removal action. B. OSC will request ATSDR to notify and inform the St. Croix hospital and EMS of EPA's proposed activities and decontamination procedures which will be available. C. OSC will prepare notification procedures and a contingency plan for the prison at Golden Grove. D. OSC will develop CAMEO plume models for various weather conditions and air release scenarios. 301503 E. OSC will formally request DPNR to monitor the site prior to EPA's mobilization, investigate the possibility of DPNR ordering SCSK and VIAG off-site during EPA's removal action, and request a list of appropriate agencies and politicians to notify concerning the proposed removal action. FINAL POLREP FURTHER POLREPS FORTHCOMI N G " ^ SUBM ITTED BY Douglass R. Kodama OSC Response and Prevention Branch DATE RELEASED -X^7\q^ # 301504 U . S . ENVIRONMENTAL PROTECTION AGENCY POLLUTION REPORT Region 11 Response and Prevention Branch Edison, New Jersey 08837 (20i) 548-8730 - Commercial and FTS 24 Hour Emergency DATE: August 8, 1989 TO: W. Muszynski, EPA 5. Luftig, EPA R. Salkie, EPA M. Randol, EPA 6. Pavlou, EPA ERD, WH-548B (E-Mail) B. Sprague, EPA 6. Zachos, EPA P. Gelabert, EPA A. Smith, VIDPNR LEPC TAT Three (3) N/A Lab Chemicals, Alcohols, Solvents, Acids Major Virgin Island Chemical Company (VIChem) St. Croix, USVI 800 Lab Chemicals, 400 Drums, 22 Tanks Groundwater, Caribbean Sea POLREP NO.: INCIDENT/SITE NO. POLLUTANT: CLASSIFICATION: SOURCE: LOCATION: AMOUNT: WATER BODY: 1. SITUATION A. Same as p r e v i o u s P O L R E P S . S i t e c o n d i t i o n s have n o t s i g n i f i c a n t l y changed. 2. ACTION TAKEN A. June 14, 1989, conference cal1 conducted between ORC, NYCCB, OSC and F. Schubert (owner of VIChem). Mr. Schubert explained that he will not be able to finance a clean-up at the facility. EPA informed him that due to the significant hazards presented by the site. Region II is prepared to conduct a removal action and remove the chemicals from .the facility. EPA informed Mr. Schubert that he will have approximately one month to contact facilities which may be interested in buying some of the materials on-site. EPA will send him a Letter OT Intent form to be used during these recycling efforts. Mr. Schubert had no objection to EPA removing all chemicals from the site and further stated that he would not be obstructive to EPA • s, cleanup. • B. 301505 July IB, 1989, Action Memorandum finalized and sent to NY office for concurrence and approval. DSC received a copy of a letter from Mr. Schubert to NYCCB, stating that he has a potential buyer for the site and requesting EPA to hold off on the removal action. OSC coordinated with NYCCB on this matter. C. July 25, 1989, Chief RPB coordinated with ORC on potential sale of VIChem. D. August 1, 1989, receive fax from NYCCB concerning VIAG's request to start operation shortly and install a water treatment unit for their ethanol dehydration operation. E. August 4, 1989, conference call conducted with OSC, ORC, NYCCB and F. Schubert. The potential sale of VIChem has fallen through and it appears doubtful that a sale with other potential buyers will occur. Mr. Schubert assured EPA that all prospective buyers of VIChem Are aware of EPA's interest in having the site cleaned-up. ORC informed Mr. Schubert that EPA will proceed with our plans for a Superfund clean up, EPA will send him an access agreement form for his signature and wanted to be sure that all prospective buyers have received copies of the March 13, 1989 Notice Letter to VIChem. F. August 8, 1989, Consent for Access to Property form sent by ORC to F. Schubert. Acting Regional Administrator approves Action Memorandum. FUTURE PLANS AND RECOMMENDATIONS: A. OSC will initiate a Delivery Order for O.H. Materials to conduct the site clean up. B. OSC will inform USVI DPNR about the Action Memorandum approval. C. OSC will coordinate contingency planning meeting for appropriate U.S.V.l. public agencies. FINAL POLREP FURTHER POLREPS . FORTHCOMING X SUBMITTED BY Douglas R. Kooama On-Scene Coordinator Response and Prevention Branch DATE RELEASED 301506 S.yl.7Hg=l. ../, 3 . U.S. ENVIRONMENTAL PROTECTION AGENCY POLLUTION REPORT Region II Response and Prevention Branch Edison, New Jersey 08837 (201) 548-8730 - Commercial and FTS 24 Hour Emergency DATE: September 8, 1989 TO: W. Muszynski, EPA S. Luftig, EPA R. Salkie, EPA M. Randol, EPA G. Pavlou, EPA ERD, WH-54BB (E-Mail) B. Sprague, EPA G. Zachos, EPA P. Gelabert, EPA A. Smith, VIDPNR LEPC TAT POLREP NO.: SITE NO.: POLLUTANT: CLASSIFICATION: SOURCE: LOCATION: AMOUNT: WATER BODY: (4) Four 4V Lab Chemicals, Alcohols, Solvents, Acids Major I Virgin Island Chemical Company (VIChem) St. Croix, US Virgin Islands BOO Lab Chemicals, 400 Drums, 22 Tanks Ground water, Caribbean Sea 1. SITUATION; A. The Action Memorandum was approved by the Acting Regional Administrator on August B, 1989. Site conditions have not significantly changed. 2. ACTION TAKEN; A. August 8, 1989, DSC coordinated Mith ORC concerning language in Consent for Access to Property for« to be sent to F. Schubert, owner of VIChem and discuss possibility of placing a lien on VIChem's property. B. August 9, 1989, OSC informed of Action Memo approval. Receive Site ID No. from PSB, 4V. Delivery Order Number 7445-02- 064. Initiate Procurement Request for •250,000. Upon reveiwing and approving the Action Memo, the Acting RA revealed several concerns about this removal including 1) possible RCRA violations by Berlex, 2) a schedule for tbe removal of the 40,000 gallons of ethanol stored on the site, 3) additional PRPs and 4) can the site be designated. OSC instructed to contact VIAG and determine the schedule for removing the ethanol from the site. Other concerns will be addressed by other, program offices. 301507 ' A , C. August 10, 1989, receive DCN, KE3042 for $250,000. D. August 25, 1989, OSC contacts VIAG, D. Weston and was informed that VIAG intends to buy the 40,000 gallons of ethanol from Ethanol Corp. by the third week in September. It will take VIAG one day to dehydrate this alcohol and less than one week to sell and ship the material off—site to the buyer. By October, VIAG expects to be able to purchase ethanol froa Europe and start full operation. OSC expressed his concern for the safety of VIAG and St. Croix Security Kennels personnel (and dogs) while EPA is conducting the clean—up at the site and the hazards posed by the materials on-site. Mr. Weston shared the same concerns and seemed agreeable to vacating the site while EPA is working at the site. OSC drafts reply addressing Acting RA's concerns regarding a schpdul^ l a r the removal of ethanol froa the site and sends it to ERRD for a coordinated response to the Acting RA- E. August 29, 1989, John Higgins assigned as alternate OSC for the VIChem removal -and D. Kodama to act as his mentor under the new Mentoring Program per OSWER Directive h9285.9-6l. A. Bosques of the CFO may also assist with this removal. Initiate two Procurement Requests for •250,000 and »500,000. F. August 30, 1989, OSC coordinates with DPNR (B. Rhymer) concerning contingency planning Aeeting for VIChem removal. DPNR will send out letters to appropriate public agencies and schedule the meeting. DSC reviews Delivery Order scope of work with Prograa Management for the ERCS contractor, O.H. Materials (0<-H1) . OHM will be the ERCS contractor for this removal since they are the only ERCS contractor to serve the Caribbean. G. September 5, 1989, Jeff Bodi assigned as Response Manager for OHM. OSC coordinates with DPNR and informed contingency planning meeting scheduled for September 13, at 10 am. St. Croix Fire Department, Police Department, Emergency Management Agency, Emergency Medical Team, and Department of Justice (Corrections) will attend. OSC coordinates with ORC concerning access agreement. The signed access agreement has not been received from VIChem yet. However, ORC contacted Mr. Schubert on August 31 and was informed that he will send it to EPA soon. 3 01508 H. September 6, 1989, OSC receives two additional DCNs. 4 KE3069 for •500,000 (9/1/89) and KE3073 for $250,000 (9/6/89). This brings the total obligated funds for mitigation contracts to $1,000,000. OSC develops removal briefing and contingency plan for September 13 meeting. OSC writes letter to VIAG informing them to proceed with removal of paints and that their alcohol dehydration operation may proceed as long as it does not interfere with the removal action. As for their request to discharge water from thveir operation to the adjacent ditch, NYCCB will make this decision. I. September 7, 1989, OSC initiates a Procurement Request for •262,000. This will bring the total obligated funds to •1,262,000 which is the mitigation contracting ceiling. Discuss Delivery Order with OHM Response Manager. The Response Manager and a Chemist will attend the contingency planning meeting and visit the site with the OSC. J. September 8, 1989, OSC distribute's POLREP 3 and sends Preliminary Assessment form (EPA Form 2070) to PSB for processing. .; Concerning future plans listed in Polrep 2, time and administrative constraints will not allow for development of an Inter Agency Agreement with the US C:oast Guard. OSC will coordinate with EMT, and if appropriate, the St. Croix hospital next week. TAT continues to work on CAMEO plume model for possible chlorine and hydrogen chloride release. 3. FUTURE PLANS AND RECOMMENDATIONS: A. Discuss local response agency concerns at contingency planning meeting on September 13. B. Visit site and develop plan for mobilization with OHM on September 13 and 14. C. Site mobilization tentatively scheduled for September 25 or October 2. 4. FINANCIAL ACCOUNTING: A. Total Project Ceiling Authorized •1,840,000 B. Total Funds Authorized for Mitigation Contracts as of 8/8/89 1,262,000 C. Expenditures for Mitigation Contracts I.a. Amount Obligated to DCN KE3042 250,000 301509 l.b. Estimated Expenditures as of 9/8/89 -0- l.c. Balance Remaining 250,000 2.a. Amount Obligated to DCN KE3069 500,000 2.b. Estimated Expenditures as of 9/8/89 -O- 2.C. Remaining Balance 500,000 3.a. Amount Obligated to DCN ICE3073 250,000 3.b. Estimated Expenditures as of 9/8/89 -0- 3.C. Remaining Balance 250,000 D. Unobligated Balance Remaining -O— E. Estimate of Total Expenditures to Date for All Mitigation Contracts F. Other Extramural Costs I.a. TAT salary/travel as of 8/8/89 H. Total Expenditures X of S2 Million —O- OX I. Percentage of Total Project Ceiling OX FUTURE POLREPS yy F I N A L POLREP ^FORTHCOM I NG_^i_SUBM I TTED BY D o u g l a s O R . Kodama, O n - S c e n e C o o r d i n a t o r R e s p o n s e a n d P r e v e n t i o n B r a n c h DATE RELEASED ,Z>eD C^/ O l \ ( y K 301510 U.S. ENVIPOI^MENTAL PROTECTION AGENCY POLLUTION REPORT Region II Response and Prevention Branch Edison, New Jersey 08837 (201) 548-8730 - Commercial and FTS 24 Hour Emergency DATE: Sept. 29, 1989 TO: K. Muszynski, EPA S. Luftig, EPA R. Salkie, EPA M. Randol, EPA G. Pavlou, EPA ERD, WH-548B (E-Mail) B. Sprague, EPA G. Zachos, EPA P. Gelabert, EPA A. Smith, VIDPNR LEPC TAT POLREP NO.: SITE NO.: POLLUTANT: CLASSIFICATION: SOURCE: LOCATION: AMOUNT: WATER BODY: Five(5) 4V Lab Chemicals, Alcohols, Solvents, Acids Major Virgin Island Chemical Company (VIChem) St. Croix, US Virgin Islands 800 Lab Chemicals, 400 Dmms, 22'Tanks Ground water, Caribbean Sea 1. SITUATION: A. Site was impacted by hurricane "Hugo" from September 17 through September 19, 1989. 2. ACTION TAKEN: A. September 12, 1989, OSC and Assistant OSC fly to St. Croix. Meet with VIAG, D. Weston. OSC reiterated his concerns for the safety of VIAG and St. Croix Security Kennels during site clean- up. D. Weston affirmed VIAG's agreement to vacate the site while EPA is working at the site. VIAG also reassured EPA of their plans to process the ethanol that is now on-site and ship this material off-site by the end of September 1989. This ethanol will remain the property of Ethanol Corp. VIAG has an agreement with Ethanol Corp.in which VIAG dehydrates ethanol for them. Their plans to commence full operation of their alcohol dehydration process were also on schedule to occur in October 1989. OSC noted the addition of a trailer to the site and VIAG responded that it was for removing their paint materials. 301511 I 9 : # B. September 13, 1989, the Contingency Planning meetiTig is held at the St. Croix VIDPNR offices. The meeting went well with all concerned government agencies, except the National Guard, in attendance and actively participating. Agreement was reached to schedule a subsequent meeting for the following day for the purpose of developing a Local Responders site specific contingency plan using the Virgin Islands Local Contingency Plan as a model. C. September 13, 1989, the OSC conducts a tour of the site for Jeff Bodi (Response Manager) and Jack Herzig (Chemist) of OHM, and Jeff Bechtel (TAT). Several items were discussed at subsequent meeting. OHH agreed to develop waste treataent plan, QA/QC Plan, by September 22, 1989. The OSC agreed to coordinate with VIDPNR in requesting a waiver of the excise tax which would otherwise be levied on the materials OHM is to transport to the site. OSC directed OHM to provide daily Progress Reports while on-site, and informed OHM that financial data would have to be inputted to ROMS. OSC stated his preference for overpacking all drxims to be transported for disposal because of the -potential for reactions to occur during sea transport of bulked materials. The OSC directed OHM to mobilize crew when equipment is received on St. Croix. OSC wrote up work orders for OHM activities for past two days. D. September 14, 1989, met with VI Govt, officials at VIDPNR offices. Greg Rhymer of VIDPNR distributed a draft site-specific Contingency Plan. The Plan was reviewed,•revised for phone number corrections, and the final version distributed during the meeting. E. September 14, 1989, OSC met Alan Chardon of St. Croix Security Kennels and informed him of risks, prior to and during the clean-up, to humans and dogs that would be on-site. Alan agreed to drop off dogs prior to daily start-ups and pick up dogs after 6 p.m. OSC will write letter acknowledging this agreement and requesting contact numbers in the event of problems with the dogs. F. September 14, 1989, VIAG expressed confusion with gaining government approval for their intended discharge of 10,000 gallons/day of wastewater from the reverse osmosis desalinization of saline well water, which is part of the alcohol dehydration process, to a drainage ditch. After conferring with Marcia Taylor of VIDPNR, the Assistant OSC and VIDPNR informed VIAG that a NPDES permit issued by VIDPNR would be necessary. VIDPNR further advised VIAG that it does not permit discharges to drainage ditches and advised VIAG to contact VIDPW for connection to the public sewerage system. 301512 G. September 15, 1989, Assistant OSC drafted excise tax exemption letter to be signed by the VIDPNR Commissioner and sent to the VI Bureau of Internal Revenue. Greg Rhymer revised draft and said he would see to it being typed and signed. H. OSC letter to U.S. Coast Guard, dated September 12, 1989, inforining them that time and administrative constraints would not allow the development of an Inter-Agency Agreement for EPA to fund USCG involvement but that they will be welcome to observe site under USCG funding. I. September 18, 1989, OSC receives additional DCN, KE3085 for $262,00. This brings the total obligated funds for mitigation contracts to $1,262,000. J. Site Safety Plan developed by TAT is insufficient. OSC and assistant OSC will develop final plan. K. September 26, 1989, EPIC aerial photos taken; photos showed very little structural damage to VIChem. The roof to the dnim warehouse and labs appeared intact. All tanks appeared to be unaffected. L. September 27, 1989 overflight of site was unsuccessful because site air space was closed for air traffic control reasons. September 28, 1989, Carlos O'Neill and Greg Rhymer visited site and the site conditions were assessed ais stable and secure. The dogs were alive but some fence damage was noticed. VIDPNR agreed with EPA that site is not an emergency and clean-up can be postponed until support services are available. M. October 2, 1989, Assistant OSC spoke with ORC conceming status of the Consent for Access to Property for*. F. Schubert, owner of VIChem, stated to ORC on August 31, 1989 that he had received the form and that he would soon be returning the completed form. ORC has not yet received the completed form and will again contact Mr. Schubert. Also, Assistant OSC discussed possibility of placing liens on Vichem property, and any legal or financial ramifications of disaster relief, as a result of "Hugo", accruing to VIChem. 3. FUTURE PLANS AND RECOMMENDATIONS: A. Continue to discuss hurricane impact on site with CFO, VIDPNR, OHM, and TAT. B. Coordinate clean-up operations with VIDPNR and prepare to mobilize when basic necessities (i.e., power, vater, and lodging) are restored. 301513 4. FINANCIAL ACCOUNTING: A. CEILINGS TOTAL PROJECT MITIGATION EPA $1,840,000 $1,262,000 $200,000 B. UNOBLIGATED MITIGATION FUNDS REMAINING C. COSTS t BALANCES as of 9/29/89 DCN KE3042 KZ3069 KE3073 KE3085 Subtotal OBLIGATED A.MOUNT $250,000 500,000 250,000 262,000 $1,262,000 Other Costs TAT Salary\Travel as of 8/31/89 EPA Salary\Travel as of 9/22/89 Estimate of Total Expenditures to Date D. CEILING PERCENTAGES TOTAL PROJECT 1* PERCENTAGE OF $2 MILLION 1* MITIGATION 1% EXPENDED AMOUNT $7,116 0 0 0 TAT $105,000 $0 BALANCE $242,884 500,000 250,000 262,000 $7,116 $1,254,884 0 9,306 $16,422 EPA 5% TAT 0% FINAL POLREP. FUTURE POLREPS FORTHCOMING. X SUBMITTED BY ^uglas R. Kl % $ - - ^^oT Douglis R. Kodama, On-Scene Coordinator Response and Prevention Branch DATE RELEASED Z>P c Z V ^ m ^ r 2> 1 H O 7 3 0 1 5 1 4 U.S. LNVJRQNMENTAL PKOTECTION AGENCY POLLU r ION fgtIPORT DATE : i>j\^\-^^ V\%\ Region 11 Respon-jc? ^nti Prevention Branch Edison, New Jersey 08837 (201) b4b-8y30 - Commercial and FTS 24 Hour Emergency TO: W. Muszynski, EPA 5. Luftig, EPA R. Salkie, EPA M. Randol, EPA 6. Pavlou, EPA E. Schaaf, EPA ERD, WH-548B (E-Mail) B. Sprague, EPA G. Zachos, EPA P. Gelabert, EPA A. Smith, VIDPNR LEPC TAT POLREP NO.: SITE NU.: POLLUTANT: CLASSIFICATION: SOURCE: LOCATI UN: AMOUNT: WATLR DUDY: Six (6) 4V Lab Chemicals, Alcohols, Solvents, Acids Major Virgin Island Chemical Company (VIChem) St. Croix, US Virgin Islands 800 Lab Chemicals, 400 Drums,'22 Tanks Ground water, Caribbean Sea 1. H1 IUAI 1 ON; A. Site was impacted by hurricane "Hugo" frora September 17 through September 19, 1989. Sc-ijlember 28, 1989, EPA and DPNR visited site and the siti condition'^ were assessed as stable and secure. 2. ACnUN TAKEN: A. October 17, 1989, OSC contacted by Scott Silverlight, attorney for potential purchaser of VIChem facility. Potential purchaser interested in getting the plant operating in three to four months- OSC informed Mr. Silverlight that the EPA removal action may take nine months or longer and may be postponed even further due to island disruption caused by hurricane Hugo. USC al^ao informed Mr. Silverlight of the anticipated costs to conduct the clean up, types of materials present at the site, and wr)y VJAU and SCSK have been allowed to continue operating at the silt*. OSC referrt?d him to Lnforcement Programs concerning jnl ur ni.3l J tjii on any subsurlace remi'diation at the site. UiJlJ in lormed Enforcement Pro«jrams and Office of Regional 301515 ':i]i Count.el jtjcjut his phone conversation with Mr. Silverlight. B. U(. tuber 24, 1989, OSC informed that Chief, RPB instructed the EHi:s contractor to prepare to mobilize to the site to repair the site's, perimeter fence and stabilize the site. Under the circumstances of St. Croix's devastated infrastructure, OSC has revised the scope of work for this first phase to securing the site (fence repair), and if possible, sampling, segregating and overpacking drums. Due to concerns for worker safety, on-site treatment of reactiwe materials may not be corjducted at this time. C. one coordinated with ERCS contractor, OH Materials, October 24-27 deciding what equipment and supplies should be mobilized. A gaily trailer (food), decon trailer, office trailer (command post), equipment t r a i l e r j three generators, bobcat, passenger van, pick-u|) truck, microwave communications system, foam fire fighting unit and other appropriate response gear Are scheduled to be shipped from Elizabeth, NJ on Friday, October 27 and arrive in St. Croix on Thursday, November 2. All attempts to air lift the above equipment and supplies proved unsuccessful. The cost for this mobilization may range from •lOC^OOO to •200,000. A'j ot October 27, lodging for the ERCS contractor remains an unresoved issued i Due to the fact that the St. Croix hospital is not fully operational and outbreaks of typhoid and cholera may occur in the near future, OSC has requested an EMT certified Health and Safety Officer to monitor and treat the clean up crew as needed. D. Hei»pcMise Manager Arrives, on St. Croix October 26 with an electrician and structural engineer to assess electrical generator hook-up needs and structural integrity of the buildings. Initial entry by ERCS revealed water damage to the office Area, liowever no spills were noted in the lab or drum storage area. E. OLtober 26, 1989, OSC receives a copy of a letter sent from DPNR Commissioner Smith to the Director of the Virgin Islands Interna J Revenue Services dated October 11, 1989 requesting waiver- of the Virgin Islands Excise Tax for equipment and supplies shipped to St. Croix for EPA's removal action. CJSC will inquire as to the status o i IRS's decision. 3. miUHi: PLANS AND RECOMMENDATIONS; A. OSC will arrive on St. Croix, November 1, 1989 and coordinate removal activities. OSC will instruct ERCS to mubili2e irew once equipment has A r r i v e d on-island. 301516 4• FINANCIAL ACCOUNTING: A. CEILINGS TOTAL PROJECT MITIGATION EPA $1,840,000 $1,262,000 $200,000 B. UNOBLIGATED MITIGATION FUNDS REMAINING C. COSTS & BALANCES as of 9/29/89 DCN K23042 KI3069 KE3073 KE3085 Subtotal OBLIGATED AMOUNT $250,000 500,000 250,000 262,000 EXPENDED >_MOUKT $7,116 0 0 0 TAT $105,000 SO BALANCE $242,884 500,000 250,000 262,000 $1,262,000 Other Costs TAT Salary\Travel as of 8/31/89 EPA Salary\Travel as of 9/22/89 Estimate of Total Expenditures to Date $7,11'> $1,2 54,88 4 0 9,30C> D. CEILING PERCENTAGES TOTAL PROJECT U PERCENTAGE OF $2 MILLION MITIGATION 1% $16,42? EPA 5t TAT 0% FINAL POLREP FUTURE POLREPS FORTHCOMING / SUBMITTED BY k fiT^ [/sgAjWsrv Kodama, On-Scene C o o r d i n a t o r Response and P r e v e n t i o n Branch 301517 U.S. liriV]hOli«£HTil. DhOTHCTlOH iOHrtCif t'UliJilUQtL-iLtlfDiil K . . . I' -. ( 'z'. l u l l i l DATB: I Hovcfcibar 8, 1989 TO: C !•..(.' UII.I Prev»5nLio/i bl u>i(.-ii 1.. How J e r s e y Ooti'jil '..•1H-U730 - CtLiiorcihl aiij Vl'^ 24 Hour Eiior^tana-y SivitA.un-Bri«toff, BPA hw»..yiiuki, SPA L u f t i g . KPA S a l k i e , BPA H a r s h a l l , EPA P a v l o u , BPA NH-S48B B K a i l ) , S p r a ^ t , BPA G. ZaohoB, BPA P . O t l a b t r t , BPA A.' S B i t h , ?IDPIR L^PC TAT ¥ . S. R- a] B B 0 i'i.l h-ci hi'). : !•'.:! i.i--TA«'i' • (M A.'".:-IFJCATION : :",UiilirK. J.'.!-"AiTTO.i . .••.KMUhT W/.TLh luiuY: A l c o h o l s , S(.l vtiita, Acids SoVBl. ( V ) 4V l.ab Cj.t-ljiciil; Mao or Virgin IjJuJifl C h e n i c a l Coii,'»i;iV (VIChem) S t . Crojjf. UO V i r g i n Itsle^nde 600 Lub C l m c i c a l a . 400 Druua, 22 Tank* Grojrifl water, Caribbean SJea i i^liUcJLLnH: I . : •iateugB frvi. hurricaiic liLifo wbd uinaV. I ' o r t i o n s of A :; 1.1. 1 --i icoi.Br feju,B wert> kiiockwd du«f;. Ho sp'illfc of a a t t r i a l s Hill ,l...l.t.-d t o s t o r e , deiiiilto Juoit^-c t o roof of one l a b . BRCS c-.:;-. rr <u lur (OK Kateciiils) d i r t c t e d Lo B o b i l i z b t o K i t e t o r e p a i r y.i . It. .:•'z.y fojiue, tui.l if fu-.s^ il i e , f;ntiple, s t a b i l J ' B (ovefp»ck>, (ii..i {..11^ I'cilutu kjnLoiJ^lb. MiQrt TAKKH: f. t .. (ii.i.'btr 3 1 , lOctf. OSC Cuiitinuea r e n o v a l ' u ^ b i 1 i z a t i o n .11.f.l lull and C'rr.i-fcrt»l i<yi< fron Bdibon 6fflb*r. OSC a u t h o r i z « B :..:iiir lo&dt uf uvoTt'ock druLb, trauxia k i t for • e d i c (EMT ; i{.!ulUi hi.d S a r r l y O f f i c e r ) , c y l i n d e r w ^ a i r a c k s , and . i ..li uf [tbri'.al (.»oH f; >. i- L'HCS: R8Bi>ur._-. Ku.iager, F i e l d ...i ;.iloriiB t.hux, ,.. . ./wriii" OCC i I.. • . . VTCliCk. Prej.. . .c tPA ( v e r b a l I. 1.1'/. *i a c t i o n . I l i e s t a t u a '. I "Y B t i l l have . but t h a t • Hi he Mould 3 0 1 5 1 8 ^ ~ " . - i • ' . ' • V I - •i>".v'; iuforuor^ thfct h i ] fw>Ji- tl ui Itjra (dtinoi., c d i l 7 » o f f i c e .....I .-,-1 ii-ijuiit t.rttilorb), luiboQt, p i c k - u p trv ck unri two 100 KM j<;ii,-i .'.K>j & w i l l ar.'ive on Gt Cri.ix Novenbor 1 or 2 . ,.^.••. Leo kjBij b© . a . - i I t b l e a t priuon itliin ona uontjh OSC t r i l l i n s t r u c t •rd l i n e a s veXl ua Eicrowave .••:.<.' xiifi.."uud .l.b I v >•.*>... .1.. .li.iTtex u i l n t'lOk. •.>itr.. i'i.ri I »• I'l-cp f'honts 'iine;> f o r i" » ' l . ^ ) j '. 1 o i l . !'• hi.vjkiber 1. 35)60. 0:3C fj.-io t o S t . C r o i x . lihCS B o b i l i r e o jM.iLi'il crew (ReGponae Hnnt^ur, F i e l d C l e r k , ajid two i; 1 Uv. 1. X i o j aiicj) i . 1 - I !- / : • J Mw.ciabor 2, 1W88, OSC teu^oi or i l y Horkfl out of FBMA D i a a s t e r .; (Jffice Ar.nex, and cuoriJ iii&tos with DPNR on s t a t u s of e x c i a e -.'.vi-.r. OSC i n f o r t o J t.luil. VI I n t b r n a l Revenue S a r v i c e . .M.; t.lmt ihes wnivftr cf tlit; e x c i s e tax i'« r.pproprimte '. !.i.ui:li a tirivute i;t.ntro. l o / i s s h i p p i n g bnd utting » a t © r i B l s . ^•.^etJJ ut QjJi.roiJr i i» Lo r.-vtu eJid procedui'cs t o c l e a r i .1 .1 hfid c-vju Ji'i^oii I tJiruLiuli Cu^tOBS. ; . ^ . ; i y , . \ _ .; r ». f. l l '.nforuoJ K K O S i.ubi.-.>..i . octor (Lynan JBri.-li&rs) on-island l o g on thb inuLul luL ).>«. of sicrovavW cocAunicationii . 1. . I i • . k / i > r i K-iuU hourn, O^C xir>et.£> wiih Jios-ponae Har\a£«r and on9 i i j i i h u . Three OHH pt-rscnnel a r e stayinji; on S t . Thosaa and .i: i..^ Lu S t . Croix. T))oy vuria a b l e t o f|ind l o d f i n f f o r ona t.rjvian on S t . C r o i x , ho>«'.;ver, h o t e l doep n o t hAT9 ti i.:iLy, p)ioijbt> ur w b t e r . Ali four OHM p e r s o n n v l v i l l s t a y ( TliuBHis tonigliL ajid c h ^ r t b r p l a n e t o opiuDute bet««*n I,-ill OSC will ucet DilM bl a i r p o r t a t 1800 h o u r s t o g a t 1. '.I OHM'e s e a r c h for on i s l a n d lodging', r e n t a l Oft7f (thajr nrttiiitly uhiiii toxj atiTM i c e ) and if t r a i l a r B a r r i r e d in nuuberb l o r t r e i l e r a and s u p p l l a a t t p p l i u s tirrivud in S t . Croix t o d a f a t uSC aota waybill h'.i :.••'(. nrit'i inforued su Ittj^iTii via Navieras de P u e r t o Kiuo. IbJO iiuLirs, DSC ttofetb Cihh a t a i r p o r t pr I.., :..t TlKieaa. OHM wat not sl.Je t o f i n d ' o n - r....iul > arti and wafa i n f o r c e J thai /lone of t h :.w,i 1 ;'-... have a r r i v e d in the t ^ r t . OHM depa OB 0700 lor t o t b t i r f l i g h t i s l a n d l o d g i n g or i r e i l a r s or r t s f o r S t . T h o s a s . . w.-ril i nut ca v« J I (. £nji.^.. ^ ' f i o t i and ^UCS Progri '..i bi>() i^; iiii'urt.1.J tl.i.t i.M.jlers and; s u p p l i e s a r e due in . t.Mturvuv, Hvjvetbcr ^ .-. i O'OO h o u r s . lEdiaon o f f l o e has I littL it. i./iy bu t..i..;.:i .:... t . £ e t hard jlinH phone hook ups re-jjcJt K i t e / « VI V iw i Lb b i l l . a J i J »,r».J by Ms Woej' {tjpJione CoBPar.y (VITJJtCO). 1 3 0 1 5 1 9 a.t>. i_ with Eate Mest}, t^ite r a a i d s n t . i h u t Iw,. <<ther hurrlchi.f h o s a l e a a I . r pnorln fsre l i v i n g tn r.'.l.' vi*.)i h*>r Ofir B " ! ^ '. • ' ' *• <• i.-r..;irj \^Q p o n r l b l c t o h i r e .*^Cr>F. f-i':'>c!'. '.]nftn iv gwn-d l}-''''^rr- »,r,,> , . . , , . . i j , . _ wliilo P.PA/OHM i s o f f - y j t ' ? . H?. ^''•vv hnr. hmtZ v ^••'i'lrg o)l."with her f>srLner, b u t F t i l l ''-i*: ^.hnrt,,,., Jp thn b<jr {''..-••'-, S^** ^.-R? roljM-lunt t o havft ETA v.v.o ilm n t t s r k dngn, I'Ut oxp"! "R i rir-d t h a t ehn hpn never had n trrsprtns/vsndp.l i s n / r o b b o f y prp»-ler, ^i. tho B i t e nnd nould voliml.Brrly look a f t r our ftquir^"*^* '"""^ rjurrlieg ovnr-nijjht. .She f o l t < IIM p i t - vni'ld hn rnfr!.*^'"' -^'oure. D. Noveaber 3 , 1999, 0100 h o u r s , OSC iJoes j : ' ^ Mrvinr^r n f r i o p a t p o r t and was inforr^H thnt. four t r n i l o r r a.-rlv^H ->f. TnuBdp.y, October 3 1 . OSC proceedn t c uStn ^nH rn**?:- T.yrnn DiC'l'"«Tn nn-J TITFJ.CO. VITEf.CO i s a b l e to p r o v i d e two " h i r d l i n e " conn n d i r.-«n «nd T.yjcnn B r o t h e r s w i l l l a y l i n e Ihrnuj^h pprT>'^' »'u< e>"ly '''"• '"'"^ ff "oungle" in order t o r e a c h s i t e . OSC Boets with 0H><, r]e>r«? *.hrnri tre.il'-r!- ' ' • • - • T ! - ^nr^'.t^ns. Docon »rid e q u i p n e n t t r o i l e r R ar «< ^.'-nnapcr <-.«*rJ "r "•»•. r- -r * i.i. pjt.o. Thf< th«rd t r a i l o r ( g a i l y ) w i l l nrrW»» rn-r5'«* ' -.r-- • v.-. J]i» o t f i o r t r a i l e r i s cinpiMji pnd unBPConnl.ed f c r . "Hard l i n e " phcnpi* i n n t s l l e d i n ' ' working ^vr '.'.• l.hr trrr-"*T »ry n a t u r e of t h e " ' "hard l i n e " hooV up'- ., ''"'^ •;,.--;-'»^-.. <n p r o i - ' ^ e ^ w i t h B i C r o w - v - - y r ' n r fjin'-'! -^n;. th^'T \.- •';""' -• ] i'- 1.« UHH d e p a r t s for fi Thorn-: »i 3 9^n h o u r s . '^"" ^^ • • ' " : < ' lodj!'""^ on S t . Croix fo- 1'-imrrtjw. Since o f f i - ' ' T - . ' ? - - - " . I ^ oth^r f»'juipBent and FDpt'lics nrn du*- i n t o p c ' '' •' ^''•'•" , -T-'.' dnridoi* to B O b i l i r e »<dH''. inni"! RRCr. p"'-7onn''1 ' • - • ' - •»• ? '!.''"«.n up T'":hB, 1 l a b o r e r , aixl 1 c a r p e n t e r ) . n:'>C a e e t s with D. v-)"ton of VIAG a t a i t q . E. Hoveaber 4 , IfiPn. o T T^orkr v - t h CEP rn '•••••n-^r' '.,r: VTCSPTI p r e s s r e l e a s e . OHH e l e c t r i c i a n e . t ' T p t B t o r^na'-r VJChw*-''- r n - ' e r w t c r . Klp»^ir«r power i c in'rr»^ ''.'.^nt fr>' '.'^^icr" nrnr. - ' '• • < Ir*!nr;. f"'^' coordln««.er> ^•- " *-MTPI<"'I •-.«J ... ...i^,-i.. , ....-i._„p f{ir f.-.r.r l i n o B f o r r ^ r • • - v f , p y r t r r ^'-.'ly trailer r*bc'.' ^^ cite. Or.r infoTBed by 0. V^Rfnn cf VT^G thwt r'T«-':*-!r- pcle on- giiM br-. elctricity m ^ "nly needr n hnok-up. V. HoveBber 5. JPP9. 0«00 hcurr OHM on-r.. -u" I'nloadinS of dbn-.n and equipront trnSlers inti» cffirn arr" r^'" builrtitig. Field Clerk and Cook depur*. t.n look for additicnn] .T<;r.t«l cars and ptock up on food for lunch and liquidr. Lyren Prothi^rB on- BCoii' end at Bicrowpvp r'n»ion (off-Fit.e) vorVfia nr ricrowfivB 301520 sysl''«i p r e p a r a t i o n . Tl ^ «n «••'-,>wn v- -'..fit.Vnn «;! Btojtr ovnod by ?,nT)\'• n.n-- r^uir. P I M ' '.'>'?, i-iT--- fvjl'- ^i«rit«llnti(M^ - r < ''^ i r p v j i ' e M y . M r t n p s b u i l t for nqi'ipi.-n* t r - ' l " - . Wotrr »-r.^ V-.-* • • c- .''rcn on- R i t e h y d r a n t t o de.eon. "IT*!- u n j l ond f J T hC'-»- " " ' ur -•:• 'J-UB wprrhnuoe. B l e c t r 3r im' i.'r»P t. iPU"»p in a t t e r i p t r T - r i • p*" cm-hite goii-tfitor. The vDl<ef»r. r»'f»iilntor '"or th? r.H.r K"-- ~»^'•'" Jr -"<- f u n c t i o n i n g p r o p e r l y , vnltoRo o.f ci Intifi)? by K'M v u J l ? . "'.^•.'•^ hourn OSC c o n d u c t s (JV^rfliiiM. of viCbHC Bit*-, !.y.-r'. n,.,.tb--v Brruiir'f.- for a i r froiphl o.<* r.'t:r«^wnve iJinbon e.-' •••]•• = r' • r - f I (i:^C drafts Been fcr rPKP C O O . - T 1 ntf c'«"M" •-",-. p-''»n:--;rr Dnd inforiJHtional BoetJMg o-> VTChen pi'-e. R-t.j.ir-r'- ...,,.•"»--:e by PulJnp, Fire, KMT, DPHP., VITKHA nn-" CM-rccMn:. '••'': THqi"?-=*.e BBotinG to be Rohodnlt-d HovorH^^r '', «. or "^, i-!'- '-i --^T 3'--^K and Mtcbiliration jirtivitiBK. 'C. G. Hoveaber B, 19Pfi, 9000 b">)r'.i 'JH" np 3-rnr -••!» •^--f--,- BHfot.y B e a t i n g . Mirrownve r y n t e u «rriv©E. C r r p e r ' ropijirjnff binl'JJng roof and d r H i r i n n B»?t»»r fm^j rrflirifl *-tr,: ( - - - - t i - . o c u n t r n i ) . OSC inforrr^^^ •vo l.'-nil*':-; cf rjr-^rr--' •' I - • .rl or Hovnr.bor 2. nil** to lack of gen'!r»i'"T'« and nn-i'• t r i r !.y o r i ' - - - - --.-•i-':' t i r r . 0.<'«C c o n a i d e r a »5 r Tr-i/^ht. n^" • 1 "0 kf :u»- -- """.* l?rr- rhonc working r:|..)-mii CB P y . '^'^''. d e l i v e r e d r ^ f t '••>••' i r f . c r - •«••-^c-f "ir" -i"- Crow u s i n g wee.d oH^^erK t o «^1«»«i- V9g'>1 B t i'•• neodiii}' r e p a i r . Posponr" Mftnegor v i l l nhock - ' [-^r'. t r ^io jf overi.?»<'k druBS havo nrr'^'ftJ. Cook r - p c r t r I.'i »''n-.<'..- »-f.5«. t.'.- >fet i n t o Pu«»blo groce.ry K I O ' " , Grpnd "I'ion s t i l l r !-'-«•? r-in-p "o prnr """•» for g a i l y , r'"r>v ' iiv? f h o r r ^ ^ i gri"*! r.-- 1 HI'Towave d i s h ref -t: on ^ i t c nnrl J» t. of ^ •-= < ,- . f „ i i , . . _ Nor lb vide of fftnoo lin' - I c o r ^ d -<*' vn^..!.*.! lo:- ' v . • • ' • - - • ' '."-Wr ContiniT'.ns a i r B o n i t " r i - ^ vM>^ cxr ^ ">• " r - t r r t?"' ''•'•: -'-••••••' -.- e3".v-'<d readingB Hu-^i'-r ' ^-o. fir.^.--;r r r ^ - ' - . ' ^ - ' •• ' " -.:' r.l •••». •!., drop off b ' ••-•_' ' .' n^' r ^ ' .r'o.-: r-„.;....• _. . • ,,. tr ' ' ' ' ' T ceiJin/? ' ".'' "-i ! r p« i • bn ^ II ii7>; / •'/^pair of northrr-^ ••"•^ticn of p r T i u i ' ' ' ' r f - - ' y c-hH-ft tetik- - v i t i a t e d . Kler.f.r 5 ci "ni p l a r v t ) : e j c ? t r i r r . . ' •s'j'.'i for t r u i K r c o n n e c t i o n s . OFT apprnvcp " w froigM '•<• T^? kv geiT-;: r l o r . OSC infnreerl by Edjpon t h a t P'^A pr>r • ir.--! v c r k i n g on hiirri (•''.>'e daBage sav an »dd t.b.ni Hr'-ifr-^r hnr •• vf'-.r^r-ni'ir nnd bobchi for r e n t . 0.*iC jrtids e l r c t r i c i m to pnrr tn •••vvire ebout thn;.-e ) 1 OBS and check s r r i n l niirbpr'- <o Ban :T • ho"'- err. Y P A ' H . K l t t i t r i n i a n r e p o r t s *hfl< w.Mvirres v.,p.w notinnjy "?-'•'•;« l^r edM, g e n e r a t o r or b o b c a t . 3 0 1 5 2 1 nPC infoTBed t h e t i «-> ifen«*r»it-'- . •pir'k up '•u'-l e-vH hnbcnt . j - . i l y b«^iiio li.t..l.;d Oil jJiii' in Gan Jyaii today and due to .. i:c. Ctoi-j. un WcdiicJ.iu) . OSC cancepe a i r l i f t of 100 kw I. Crfiitc t r a i l e r and ovtrpacka Bay'be a v a i l a b l e today i ..iw thrciJijb TM? ( s h i p p e r ) . ' .<,....*.bci 7, l&o3. 0:>i; hcc-uiipuuies H. Chpn^f of RPB to WAPA .1. wAPA l i u r tt.uiM!iviuur VlChfii e l e o t r i c p o l e and r e q u e s t s ..t J h..f>u-\jii. Thir. i-ower will bo good For b u i l d i n g a i r 1.1.1.It: Ouly. If »!Al'A pu».cr i s o b t a i n e d e l e c t r i c i a n w i l l : i <!..;.t'v..rtLr :ii 1..JL ioii« LK p r e v e n t fp.re h a z a r d . Thia -<.- tr.nncil I f i.5.jd to t l 6 p down WAPAl power (480) for uae ; r.s \^:'.y.O). nM'h vc.<Ui.i.ts .'rloaring pbtli t o pole BO they .. !.i...:k i;. wi.vl ciK;ck t r aiis, f ;> r o t r B . |*APA w i l l r e t u r n at :. . . .'s.. u b i ;3 I. 1 iju'i c d . •i..:ivi.tti .'>:jt. rur b / 1 2 - y / l 5 and 1 0 / 2 4 - 1 1 / 3 . Review b.'j'ti. Proi-iiiirt a r r i v t s , however jfally propane tank* 11 <n,| f u l l Carpcitit«rt> o o n t i n u e b u i l i i n g r e p a i r s ^ ii.i rouf. K l e o t r i n i h i i t-untinues t r a i l e r hook-ups. .1... c ](-«.. I ic:i .i;i (phrir.c) d«jsob«atd f roe e i t e . TAT haa b.-^u .i'jL.ii ie.-i t.u work with EPA/TA" on h u r r i o a n t jriiii2 TAT";. i i r ; , t f u l l day on-Bcen» thoy inventory BRCS i..J fiji.pl ii;:i cii Ditt;. Medio (BMT C e r t i f i e d h e a l t h and i. .-.J ) u r r i . o i i o n e i t t r . ERCS t r y i n g t o d e t e r a i n e how hi.;* fa Ili p.'od t o S t . C r o i x . I ' .••1 IvbJi'wiiwo Ht>^>ri«{er ^-..1 to p o r t t o check on two t r a i l e r s i-,v<.rp8:k3 and office- t r a i l e r . Overpack t r e i l e r a have }, .jffit:t, L r a i l o r cltiared t h r o u g h Custosa and scheduled v»ir,(J 1-v :;ite tusiorruw. Mo g e n e r a t o r s , bobo»t or p i o k - ..-. J v,oiiV.iiii.r.-» i.o ». Icwr puth to u t i l i t y p o l e . P o r t a John . . i - u i L e . "iiurd l i n e " ^^hon^s w o r k i n g ' a p o r a d i o a l l y , VAPA ... it k i l l Li.kt^ I.WO L(< tliree weeks t p g e t e l e c t r i c i t y t o i.tiCJ titrtrLa x:Jebrin^ vi.£utBLion a l o n g , w e s t e r n p o r t i o n of i r.,- fuitce neuJiiiiJ r e p a i r . . i i u i \Taot.ti k i t hirivfro : . n - 9 i t e . Lab roof r e p a i r e d . . . <AiiU<->r bei.L w h i l e dikft^i'^E f e n c e poBt holu, s p a r e auger -l.l I'l-oi.:^;. :>uil id e x t r c L o l y h a r d . B x t r e s e l y low i.k..>U|^ «•'r e w . h H . i V. ; t 1 . • ,>. . . . A i b v - r d , . .. i J ia t h e r ,. W.ZiL i s St : ,.. .1V ? \ :^ . . . . 1 : be . . i J * r I L f c - . . f i t . 1 i i . I < • K : b u iubvr d, JbOQ, htiniu ^^..^ale anong oraw i s e x t r e B a l y lov. i:s t h e r e no u i r c o n d i t i o n i n g a t t h e I s i t e , but t h e h o t e l i i s steyiini bnu no a i r c o n d i t i o n i n a and t u r n s off i t s .iV ?\:^C\ b .iirs tii.d t h r BosquitOBS a r e bad. Thia ri.-.i. i-f u t i i m d t a l a r i a haa acrjfu.ly daBponed 301522 I wit.. J^L-4,.»-.».-.o n li.i li ti t.z. s h i p a i t j . t^vusrators, .ii> ivuck >%ill M-jt be dockod u n t i l 1300 houra and \ 1. I »• k C; • • i. u^tjiprent u n t i l toaorrow III . u f ••> 1.1 urdwr tCi t r y to buoyt crtiw B o r a l e , w i l l i n s t r u c t Roaponso ^ -...t.,,!.-. i b n t u f t e r tlie fence iw r e p a i r e d otof may have t h e r e s t ...;• 1 i... (liiy off, if tlitsy want. " u r i i o t r t i l r - r urrivoB on a i t e . Power luger blows engine .>-. i. •:'afc;^"tl Ifitt .-u3t Jiole. OSC c o o r d i n a t o a with C o n t r a c t s in I-.: r * v . i . ( i i . j to cbuii^u pur dicu i.u a c t u a l s i b e i s t b n c a for ERCS. /•.... :'.ii:.iMi offict: iz.r E.~.j^;i rit aji.u iri t h i a s a t p e r . Lysan B r o t h e r s i. ••i--ii.j, .:' phc.i;r fty_tok. LiJ t r;. i 1 o r . 1 .it.u.. up t . . i . w\.i.i-j, iioii while r e p i i i r i n j f e n c e . .••1 Xitu.. k,v..uJiJ, I bo no".. <.iitored forward of the s t e a l shank :. • r...ih b!/oLa. ttoJic ttdui..jutfjra f i r s t ^id i n j u r e d haa had :.ji;;i. wltliiii tJiu lt.3t yitiT. Clean upjtecJj v o l u n t a r i l y . 1 . 11.1 HLi/k Pnuues workir>^ s i p o r a d i c a l l j . . . i/.iit.u.' foncw Jt> rcptiiii:.] and two s t r a n d s of barbed wire I . ;•• t . t i l d d . Oiil/ tww clfeaai up t e c h s ( i n c l u d i n g i n j u r e d ) .:. . . u 1.1. tukw afttjri.ijon off. .:,•' ,-ii:k:> up voltage- re^iuliitor for a i t o jgen&rhtor. 1500 iu jij:<t i^ci.tiini ill t c I ' o r t . B l e q t r i c i a i i f i n d s i i i..;t rcCult»'_-..r i:. broko.i a j sJiipped, ino power. ...:.'iU tjmL£\'ZJ.hv i<.-:\.'i;hftHnii,-.Tl(iKa.; i ,,, t 11. <:ujiJ>ti t u safo rcAiuvul a c t i o n . I ...-. UBLiuii rt-juoiiiE de:iptrfatc and no g e n e r a t o r s Arv I w. 1 1 dejuob crew. • J .1 /iiiii.liil^Ai;CLa^allflii: A •. .i...il P r o j e c t C o i l i n g AuDiorized [•> '...llii Ku!id3 Authorized for Mil.iyaliuji Conti a r t s at> of b / 8 / b 9 0 i,. . nui r.urci for Mitigaliuii C o n t r a c t e : I. £»,ount UbiijiaVcJ t o 1>C« LB3042 . b KBtiBbled BApcnditurco as of 1 1 / 5 / ^ 8 : ttaJanoe hekinininii 1 Amount O b l i ^ a t n J to D'H EE30BB '; h.-il juatnd E^i'tind 1 tuj'B& aa of 3 0 1 5 2 3 nofc.h'• li ing itnlaucu .-...i.^ji.t ObUtutesil tu bOh ttSO'/S • 1,640,000 1,262,000 250,000 148,686 100,114 500,000 -0- 600,000 250,000 . J U.S. ENVIROHMENTXL PROTECTION AGENCY POLLUTION REPORT M Region II Response and Prevention Branch Edison, Nev Jersey 08837 (201) 548-8730- Commercial and TTS 24 Hour Esergenc; DATE: November 17, 19 89 T0{ C. Sidamon-Eristoff, EPA W. Xuszynski, EPA 8. Luftig, EPA R. SalXie, BPA J. Xarshall, BPA O. Pavlou, EPA ERD, WE-548B (E-Xail) B. Sprague, EPA 0. Zachos, BPA P. Gelabert, EPA A. Smith, VIDPNR LEPC TAT Eight (8) 4V Lab Chemicals, Alcohols, Solvents, Acids Kajor Virgin Island Chemical Company (VIChem) St. Croiz, US Virgin Islands 800 Lab Chemicals, 400 Drums, 22 Tanks Ground vater, Caribbean Sea POLREP NO.: SITE NO.: POLLUTANT: CLASSIFICATION: SOURCE: LOCATION: AMOUNT: WATER BODY: 1. SITUATION; A. Site damage from hurricane Hugo vas minor. Portions of the perimeter fence vere Icnoclced dovn. Ko spills of materials attributed to storm, despite damage to roof of cne lab. ERCS contractor (OE Materials) directed to mobilise to site to repair perimeter fence, and if possible, sample, stabilise (overpack), and segregate materials. 2. ACTION TAKEN: A. November 9, 1989, OSC receives vaybill.s for tvo generators and bobcat, shipper informed Response Manager that pick-up truck is still in San Juan. OSC and Response Manager go to port to clear Customs and arrange for transport of generators and bobcat from the port to the site. After clearing Customs, OSC and Response Manager accompany transporter to dock and see that the pick-up truck is also at the port. OSC contacts shipper and is given vaybill for pick-up truck, and eventually clears Customs vith some difficulty. Generators are 10 kv and not 100 kv generators. Apparently, the retailer shipped the vrong size generators, OEM had purchased tvo 100 kv generators. May be able to supply enough pover for the 301524 O i i - " ' * i - / F £.10 ST r. : '.. I >. I i i. K i i t J u t v t e d L A I - O I U I i t u x ' e ^ a u o f J I KoBaiiilng Dalajjce \j li.M.bl iguted Balance RoBiij.ning !•: h.-.i it-ulc of Totul Expendi turefi li DuLc- f o r A l l M i t i g a t i o n C o n t r a c t s I . •.;,;.-.; K x L r u i i U r o i C O i i t B . VhT bnlary/LiftVcl aa of 11/03/89 KPA u a l u r ^ / t r a v e l a& ui' 13/6/68 ;i iiiu.1 l-ixi-enditiJicb X of $2 M i l l i o n ; - . :-...{txHii of Ti.'tol P r o j e c t C e i l i n g •i J . M ' _ . KUTUhB POLRKPS , / FDKTJjCOMlMG K.. liUbMJTTKD BY - 0 - 250,000 -0- 149,888 16,234 15,300 9.11 9.9Z Dduglas7K. l o d A s t , On-Soene C o o r d i n a t o r Response and P r e v e n t i o n Branofa DATB RKLBASBD. fi\.o.l6K:^ 301525 office trailer lighting and air conditioning, but these generators vill not supply adequate lighting for inside the varehouse and labs. OSC considers demobing crev. OEM can airlift a 100 kv generator through American Airlines, however EPA vill have to f&z American a recjuest since the airline can only airlift emergency relief supplies for private companies. OSC coordinates vith EQ-Contracts attempting to get actual subsistence for ERCS contractor. Contracting Officer and RPB Chief call back OSC and inform him that CO haa authorised actual subsistence for ERCS and vill send OSC a memo confirming this matter. Ths cloan-up tech vho stepped on a nail yesterday vas informed by the local police last night that his vife is in the hospital (no phones available at hotel). This clean-up tech demobed today. B. November 10, 1989, OSC completes POLREP 7 and gives to TAT for distribution. OEM having difficulty finding a 100 kv generator vhich vill fit on air craft. Generator vhich does fit inside jet vill have to be purchased in Columbus, Ohio and driven to JPX Airport by 0700 hours tomorrov in order reach St. Croiz Airport by tomorrov afternoon. Pev transporters vork over the veekend, so ve vill have difficulty^ getting the generator delivered from the airport to the site. Due to the xineertainty that a generator vill be airlifted to the site, OSC requests EPA to ask rsMA if EPA can rent, buy or borrov a generator, this appears doubtful since VIChem is a superfund action and not hurricane relief related. OSC goes to Eess and requests a generator from Eess. P. Rube* of Bess vill look into it and ask that the OSC return tomorrov since Eess does not have vorking phones. OSC also asks Mr. Rubee if he thought that Eess may consider recycling some of the materials from the VIChem site. Ee replied that Eess vas not interested. Stairs built for office trailer. ERCS begins staging of lab reagents and drums. Generators are hooked up for lighting in varehouse (minimal lighting) and office trailer air conditioning. Demand from office trailer is too great and generator vorks for no more than ten minutes. OSC informed that tvo people at the PEMA Disaster Pisld Office Annex have come dovn vith Dengue Pever. OSC informs medic. Response Manager and TAT. Crev morale drastically affected by this news. Ask ERCS and TAT to research Dengue Pever. While staging thirty of the drums in the varehouse, tvo of the drums developed leaks. These drums appeared to be in good condition, but use of a drum cart as opposed to a remote handling drum grappler, vas apparently too much rough handling. ERCS experienced break-through in respiratory protection (Level C). TAT conducted Eot Zone perimeter air monitoring and found seven units on the hnu. All Eot Zone operations cease. 301526 OSC receives the folloving information on Dengue Pever from TAT: Description-acute, febrile epidemic disease, mosquito transmitted virus. Incubation 3-15 days, usually 5-6 days. Symptoms-seldom fatal, tvo fever periods vith intermission, skin eruptions similar to measles, severe pain in muscles and joints, high temperature, lazy, loss of appetite, diminished urine, irritability. Treatment-no specific treatment, analgesic sedative treatment. A safe removal action cannot be conducted at this time. Additional equipment and supplies are necessary. Island conditions vill have to improve or stabilise. OSC demobs crsv except for Response Manager, Poreman and Pield Clerk. TAT informs OSC that air monitoring shov no readings above one unit along the Eot Zone perimeter. C. November 11, 1989, ERCS secures eq^uipment on-site and posts varning signs on building entrances. OSC goes to Eess and is inforsdd that overnight Eess had tvo generators stop vorking. Eess has no extra generators to loan to EPA. OSC informed that 125 kv generator is on American air freight and vill arrive at airport . this afternoon at 1500 hours. ERCS looks for security firm to 1 guard site vhile EPA/ERCS are off-site. Ko security services available on St. Croiz. ERCS vill look for security guards on St. Thomas, hovever either no phones or not ansvering. ERCS and OSC receive 125 kv generator at airport. Pev transporters are available over veekend, so car carry-all is hired. This process takes tvo hours even though site is less than one mile from airport. Carry-all is also used to transport bobcat from port to site. OSC must clear generator through Customs on Monday. D. November 12, 1989, OSC picks up Chief, RPB at airport and tours the site vith him. E. November 13, 1989, vaybill for generator has not arrived at American air freight office yet. OSC leaves mote for other EPA OSCs on island to clear generator through Customs vhen vaybill is available. OSC flies to Kevark, NJ. 7. November 14, 1989, J. Rotola clears generator through Customs. OSC had previously decided to leave the trailers containing drum overpacks at the port until ERCS is remobilised to the site. The monthly rental charge for these trailers is minor, the port may be more secure than the site, and ve may use trailers to store drums vhen they arrive on-site. ERCS informs OSC that they have found a security service on Puerto Rico. This service vill cost $4000-$5000 per veek for a 24 301527 .: i hour guard service. It is the OSC's opinion that this guard service is too costly, vill have minimal impact on security (may make the site less secure) and is not necessary. Chief, RPB concurs vith this rational. Security measures vill involve regular visits to the site by EPA, TAT and possibly DPNR. TAT distributes Polrep 7. 3. FUTURE PLANS AND RECOMMENDATIONS: A. Deliver all remaining medical supplies, electrical supplies drum over packs and sorbents to the site. B. Remobilization for sampling, segregation and stabilisation activities tentatively scheduled for January, 1990. 301528 4. PINANCIAL ACCOUNTING: A. CEILINGS TOTAL PROJECT MITIGATION EPA $1,840,000 $1,262,000 $200,000 B. UNOBLIGATED MITIGATION PUNDS REMAINING C. COSTS A BALANCES as of 11/12/89 DCN KE3042 KE3069 KE3073 KE3085 Subtotal Other Costs Estimate of Total Expenditures to Date D. CEILING PERCENTAGES TOTAL PROJECT 17% PERCENTAGE OP $2 MILLION 16\ TAT $105,000 $0 OBLIGATED AMOUNT $250,000 500,000 250,000 262,000 $1,262,000 S Of 11/03/89 s Of 11/17/89 MITIGATION 22% EXPENDED AMOUNT $250,000 28,178 0 0 $278,178 16,234 22,576 $316,98$ SPA 11% BALANCE 471, 250. 262, $983, $0 ,822 rOOO ,000 ,822 TAT 15% PINAL POLREP. PUTURE POLREPS PORTECOKING, k SUBMITTED BY Douglas R. Xodama, Cn-Scene Coordinator Response and Prevention Branch DATE RELEASED ^O^. O.l'^gl 301529 U.S. ENVIRONMENTAL PROTECTION AGENCY POLLUTION REPORT Region II Response and Prevention Branch Edison, New Jersey 08837 (201) 548-8730 - Commercial and FTS 24 Hour Emergency DATE: January 10, 19 90 TO: C. Sidamon-Eristoff, EPA W. Muszynski, EPA S. Luftig, EPA R. Salkie, EPA J. Marshall, EPA G. Pavlou, EPA E. Schaaf, EPA ERD, Washington, (E-Mail) B. Sprague, EPA G. Zachos, EPA P. Geiabert, EPA A. Smith, VIDPNR LEPC, VIDPNR TAT POLREP NO.: SITE NO.: POLLUTANT: CLASSIFICATION: SOURCE: LOCATION: AMOUNT: WATER BODY: Nine (9) 4V Lab Chemicals, Alcohols, Solvents, Acids Major Virgin Island Chemical Company (VIChem) St. Croix, US Virgin Islands 800 Lab Chemicals, 400 Drums, 22 Tanks Ground water, Caribbean Sea 1. SITUATION; Site conditions remain the same. 2. ACTION TAKEN: A. December 5, 1989, OSC certifies Invoice 001. B. January 8, 1990, EPA, TAT and OH Materials travel to St. Croix. C. January 9, 1990, OH Materials, EPA, TAT mobilized on site for the first phase of the VI Chem removal. Two trailers containing overpack drums cleared through customs. D. Phone service was returned to the site along with electrical service via the use of an on-site generator. E. A contingency planning meeting was held on January 10, 1990, with the local government agencies to inform them of the removal action being taken at VI Chem. Site visit by local responders scheduled for January 11, 1990. 301530 m ?. A public notice will be placed in the Daily New newspaper as soon as possible informing the public of the VI Chem renoval action. The administrative record was placed in the DPNR office on St. Croix for public access. G. Additional OH Materials personnel were mobilized to the site on January 10, 1990. FUTURE PLANS AND RECOMMENDATIONS; A. The overpacked drums will be delivered to the site from the port authority on January 11, 1990. B. TAT will sample public wells in .area to determine if there is a change in the level of chloroform contamination. C. Sampling and stabilization will commence as soon as mobilization is complete. Anticipate starting on Friday, January 12, 1990. FINANCIAL ACCOUNTING A. CEILINGS TOTAL PROJECT MITIGATION EPA TAT $1,840,000 $1,262,000 $200,000 $105,000 B. UNOBLIGATED MITIGATION FUNDS REMAINING C. COSTS & BALANCES as of 1/10/90 DCN OBLIGATED EXPENDED BALANCE AMOUNT AMOUNT KE3042 $250,000 $250,000 $0 KE3069 500,000 53,304 446,696 KE3073 250,000 0 250,000 KE3085 262.000 0 262.000 SUBTOTAL $1,262,000 $303,304 $958,696 OTHER COSTS TAT Salary\Travel as of 1/5/90 26,786 EPA Salary\Travel as of 1/10/90 24.576 Estimate of Total Expenditures to Date $354,666 301531 D. CEILING PERCENTAGES TOTAL PROJECT. MITIGi 19% PERCENTAGE OF $2 MILLION 18% ^TION • 24% EPA 12% TAT 26% FURTHER POLREPS FINAL POLREP FORTHCOMINGXSUBMITTED BY / ^ . . ^ t . ^y^-^-iXaj^ [-AN \ ' "Douqlas <k. «6dama Dougli On-Scene Coordinator Response and Prevention Branch DATE RELEASED ///i/^o 301532 •JsS m U.S. ENVIRONMENTAL PROTECTION AGENCY POLLUTION REPORT DATEt January 13, 1990 Region II Response and Prevention Branch Edison, New Jersey 08837 (201) 548-8730- Commercial and FTS 24 Hour Emergency TO: C. Sidamon-Eristoff, EPA W. Muszynski, EPA S. Luftig, EPA R. Salkie, EPA J. Marshall, EPA G. Pavlou, EPA E. Schaaf, EPA ERD, WH-548B (E-Mail) B. Sprague, EPA G. Zachos, EPA P. Gelabert, EPA A. Smith, VIDPNR LEPC TAT POLREP NO.X SITE NO.: POLLUTANT: CLASSIFICATION: SOURCE: LOCATION: AMOUNT: WATER BODY: Ten (10) 4V Lab Chemicals, Alcohols, Solvents, Acids Major Virgin Island Chemical Company (VIChem) St. Croix, US Virgin Islands 600 Lab Chemicals, 400 Drums, 22 Tanks Ground water, Caribbean Sea 1. SITUATION: A. St. Croix Security Kennels have removed their dogs from the site. There is currently only one on-site resident, hired by VIAG for site security. Site conditions remain the same. 2. ACTION TAKEN; A. January 11, 1990, two additional phone lines were installed, received and unloaded two trailers containing overpack drums, cook trailer brought on-line, additional crew mobilized to site bringing total crew to twelve. The microwave phone system was demobed due to lack of a functioning phone line at the relay station. Approximately 200 feet of phone line was stolen at this location affecting not only the relay station, but at least 30 residences upstream from the break in the phone line. 301533 A bull wandered onto the site and was chased off by the owner. DPNR, Fire Marshall, and EMS visited the site. OSC and Health and Safety Officer visited the St. Croix Hospital. Hospital will not be rebuilt until July, 1991 at the earliest. EMS encouraged OSC to make own arrangements for airlifting injured personnel to San Juan. OSC contacted USCG-MSO San Juan and requested USCG Search and Rescue to be on standby for airlifting site personnel to San Juan Medical Central. OSC was informed that the response time to St. Croix was at least one hour. OSC offered the opportunity for USCG to visit the site and observe clean-up operations. B. January 12, 1990: information was gathered from labels of lab reagents and drums, drums were numbered, initiated, packaging and overpacking of bagged and drummed material, two additional unknown cylinders were discovered near dog kennels. OSC coordinated with VIAG. One electrician demobed bringing total crew to eleven. C. January 13, 1990: 69 drums were overpacked, inventory of lab reagents continued, drum grappler repaired with on-site welding equipment, caps of unknown cylinders were removed and photographed. Photos will be mailed to cylinder specialists for possible identification. Air monitoring in labs and warehouse showed some elevated readings during clean-up activities. EPA coordinated with the Deputy Chief of Public Safety, to notify the Golden Grove Correctional Facility when site activities are concluded for the day; this will be done daily. D. A public notice will be placed in the Daily News newspaper on January 16, 1990 informing the public of the VI Chem removal action. The administrative record was placed in the DPNR office on St. Croix. If necessary a copy of the Administrative Record will be placed in the DPNR office on St. Thomas. 3. FUTURE PLANS AND RECOMMENDATIONS A. TAT will sample public wells in area to determine if there is a change in the level of chloroform contamination. B. Sampling and stabilization may be completed by January 26, 1990. 301534 / r FINANCIAL ACCOUNTING! A. CEILINGS TOTAL PROJECT MITIGATION EPA TAT «1,640,000 *1,262,000 S200,000 $105,000 r B. UNOBLIGATED MITIGATION FUNDS REMAINING «0 C. COSTS & BALANCES as of 1/12/90 ' DCN KE3042 KE3069 K:E3073 KE3085 Subtotal Other Costs TAT SalaryNTravel as EPA SalaryNTravel as Estimate of Total Expenditures to Date D. CEILING PERCENTAGES TOTAL PROJECT 22*/. PERCENTAGE OF »2 MILLION 217. OBLIGATED AMOUNT $250,000 500,000 250,000 262,000 $1,262,000 of 1/12/90 of 1/13/90 MITIGATION 277. EXPENDED AMOUNT $250,000 91,482 0 0 $341,482 43,932 25,776 $411,190 EPA 137. BALANCE 408, 250, 262, $920, $0 ,518 ,000 ,000 ,518 TAT 427. FUTURE ^ FINAL POLREP FORTHCOMING X SUBMITTED BY_^2i^AAi^aJl_S^/^:^!^ilIY^C^v,^ DouglasO R. Kodama, On-Scene Coordinator Response and Prevention Branch DATE RELEASED | U ^ M Q U.S. ENVIRONMENTAL PROTECTION AGENCY POLLUTION REPORT 301535 U.S. ENVIRONMENTAL PROTECTION AGENCY POLLUTION REPORT DATEt January 16, 1990 Region II Response and Prevention Branch Edison, New Jersey 08837 (201) 548-8730- Commercial and FTS 24 Hour Emergency TO: c. u. s. R. J. G. E. Sidamon- Muszynsk Luftig, Salkie, Marshall Pavlou, Schaaf, •Eristoff, EPA : i , EPA EPA EPA ,, EPA EPA EPA ERD, WH-54BB B. G. P. A. (E-Mai Sprague, Zachos, Gelabert .1) EPA EPA :, EPA Smith, VIDPNR LEPC TAT POLREP NO.: SITE NO.: POLLUTANT: CLASSIFICATION: SOURCE: LOCATION: AMOUNT: WATER BODY: Eleven (11) 4V Lab Chemicals, Alcohols, Solvents, Acids Major Virgin Island Chemical Company (VIChem) St. Croix, US Virgin Islands 800 Lab Chemicals, 400 Drums, 22 Tanks Ground water, Caribbean Sea 1. SITUATION; A. Site conditions remain the same. 2. ACTION TAKEN: A. January 14, 1990, 96 drums overpacked to date, samples collected from 21 drums, unknown lab reagents temporarily secured on-site, known lab reagents secured in drums with sorbent, options explored for sampling of drum containing potentially shock-sensitive tetrahydrofuran, one additional cylinder found on-site. B. January 15, 1990, label information gathered from all cylinders. Inspection of reactor tower revealed a minor amount of residual product in these vessels. This material will be removed. Gathering of outdoor drums/containers was initiated, 52 drums sampled (73 to date), securing of known lab reagents 301536 m completed, and inventory of unknown lab reagents completed. Sample techs experienced skin irritation (protective clothing breakthrough) while sampling benzy1 chloride drums and flammable vapors present from sampling triethylamine. Hot Zone was evacuated until ventilation reduced to safe levels. A public notice was published in the Virgin Islands Daily News newspaper informing the public of the VI Chem removal action. OSC coordinated with VIAG. C. January 16, 1990, gathering, documentation and overpacking of outdoor drums completed, 10 drums sampled (83 to date). OHM had a car stolen the night of January 15/16. TAT previously had a car stolen the night of January 7/S. OSC reviewed options for sampling of unknown lab reagents, on-site treatment of shock- sensitive materials, and known and unknown cylinders. Breathing air in short supply and it may be difficult obtaining additional A i r . TAT sampled WAPA public wells in Area to determine if there is a change in the level of chloroform contamination. The on- site well was sampled for priority pollutant and bacteriological analyses. Two wells owned by the Virgin Island Port Authority could not be sampled because power had not been restored to the pump. 3. FUTURE PLANS AND RECOMMENDATIONS A. One chemist will be demobed on January 18, 1990'bringing total crew to ten. B. Unknown lab reagents are scheduled to be remotely opened on January 22, 1990. C. Drum sampling, sample shipment, and analytical arrangements will be completed. D. TAT will conduct asbestos sampling of material on the reactor and bulk material. 301537 4. FINANCIAL ACCOUNTING; TOTAL PROJECT MiriGATION EPA $1,840,000 $1,262,000 $200,000 B. UNOBLIGATED MITIGATION FUNDS REMAINING C. COSTS & BALANCES as of 1/16/90 DCN KE3042 KE3069 KE3073 KE3085 OBLIGATED AMOUNT $250,000 500,000 250,000 262,000 EXPENDED AMOUNT $250,000 123,800 0 0 $1,262,000 Subtotal Other Costs TAT SalaryNTravel as of 1/12/90 EPA SalaryNTravel as of 1/16/90 Estimate of Total Expenditures to Date D. CEILING PERCENTAGES TOTAL PROJECT 247. PERCENTAGE OF $2 MILLION 227. MITIGATION 307. $373,800 43,932 26,976 $444,708 EPA 137. TAT $105,000 $0 BALANCE $0 376,200 250,000 262,000 $688,200 TAT 427. FINAL POLREP FUTURE POLREPS FORTHCOMING .SUBMITTED BY 3*^ DATE RELEASED Doug l a p R. Kodama>-./ On-Scene C o o r d i n a t o r Response and P r e v e n t i o n B r a n c h 301538 U.S. ENVIRONMENTAL PROTECTION AGENCY POLLUTION REPORT DATE; January 19, 1990 Region II Response and Prevention Branch Edison, New Jersey 0B337 (201) 548-8730- Commercial and FTS 24 Hour Emergency TO: C. Sidamon-Eristoff, EPA W. Muszynski, EPA 5. Luftig, EPA R. Salkie, EPA J. Marshall, EPA 6. Pavlou, EPA E. Schaaf, EPA ERD, WH-548B (E-Mail) B. Sprague, EPA G. Zachos, EPA P. Gelabert, EPA A. Smith, VIDPNR LEPC TAT POLREP NO.: SITE NO.: POLLUTANT: CLASSIFICATION: SOURCE: LOCATION: AMOUNT: WATER BODY: Twelve (12) 4V Lab Chemicals, Alcohols, Solvents, Acids Major Virgin Island Chemical Company (VIChem) St. Croix, US Virgin Islands Approximately 566 Known Lab Chemicals, 590 Unknown Lab Reagents, 210 Drums, 22 Tanks Ground water, Caribbean Sea 1. SITUATION; 2. Site conditions remain the same. ACTION TAKEN; A. January 17, 1990, arrangements were made with the Department of Public Safety and the Virgin Islands Police Department to utilize police issued .22 caliber r i f l e s i a r remote opening of unknown lab reagents on site. A police represenative will notify the prison officals and remain on site during the activity. Continued overpacking drums; 37 drums were sampled and 120 drums have been sampled to date. EPA coordinated with VITEMA and USCG. Cylinder specialist, believes that the two unknown 301539 cylinders are probably inert gases. The Department of Public Safety will also provide information on the procedures and permits necessary to obtain explosives on the island for detonating the unknown cylinders and shock-sensitive materials on site. B. January 18, 1990, two represenatives from the U.S. Coast Guard Marine Safety Office in San Juan, Puerto Rico mobilized on site for observing a hazardous waste site and clean-up. The two were given a tour of the hot zone and removal actions utilizing level "B" personal protective equip.oent. One chemist was demobed, total crew now stands at ten; EPA coordinated with USCG, VITEMA and Public Safety. 17 drums sampled (137 to date). C. January 19, 1990, results from the bacteria sample analysis of the on-site 250,000 gallon water storage tank indicated severe coliform infestation of the water poses a significant health risk. All personnel on-site were warned not to use the water. Containerization of lab reagents has been completed. A total of 10 drums were filled. Two c,abinets are being used for storage of reactive and shock-sensitive materials until such time as they can be detonated. Unknown lab reagents are stored on shelves until they can be remotely opened. Drum sampling and overpacking has been completed. A total of 174 drums have been sampled. Device fabricated for collection of liquid and solid unknown lab reagents, during the remote opening of these containers utilizes a .22 caliber rifle. Remote opening of these containers scheduled for 1/22/90, TAT informed neighboring businesses of this activity, EPA coordinated with on- site resident, VITEMA and Public Safety. 3. FUTURE PLANS AND RECOMMENDATIONS A. Unknown lab reagents are scheduled to be remotely opened on January 22, 1990 B. Sample shipments and analytical arrangements will be completed. C. On site storage tanks will be sampled. D. TAT will conduct asbestos sampling of material on the reactor and bulk material. Virgin Island Port Authority wells will be sampled once power to them has been restored. E. ERCS contractor will be demobed from the site until analytical results are obtained, disposal options are addressed and phase two is initiated. 301540 -a 'm 4 . FINANCIAL ACCOUNTING A. CEILINGS TOTAL PROJECT MITIGATION EPA $1,840,000 $1,262,000 $200,000 B. UNOBLIGATED MITIGATION FUNDS REMAINING C. COSTS & BALANCES as of 1/19/90 DCN KE3042 KE3069 KE3073 KE3085 Subtotal Other Costs Estimate of Total Expenditures to Date D. CEILING PERCENTAGES TOTAL PROJECT 267. PERCENTAGE OF $2 MILLION 247. MITIGATION 327. EPA 147. TAT $105,000 $0 OBLIGATED AMOUNT $250,000 500,000 250,000 262,000 $1,262,000 of 1/19/90 . of 1/19/90 EXPENDED AMOUNT $250,000 147,838 0 0 $397,838 51,305 28,476 $477,619 BALANCE $0 352,162 250,000 262,000 $864,162 TAT 497. FINAL POLREP FUTURE POLREPS FORTHCOMING k SUBMITTED BY -iS^ Dougld^^ R. Kodama, On-Scene Coordinator Response and Prevention Branch 3 01541 DATE RELEASED T,^. "Z'^, \ <^ ^ Q U.S. ENVIRONMENTAL PROTECTION AGENCY POLLUTION REPORT Region II Response and Prevention Branch Edison, New Jersey 08837 (201) 548-8730- Commercial and FTS 24 Hour Emergency DATE: January 23, 1990 TO: C. Sidamon-Eristoff, EPA W. Muszynski, EPA S. Luftig, EPA R. Salkie, EPA J. Marshall, EPA G. Pavlou, EPA POLREP NO.: SITE NO.: POLLUTANT: CLASSIFICATION: SOURCE: LOCATION: AMOUNT: WATER BODY: 1. SITUATION; ERD, WH-54BB (E-Mail) B. Sprague, EPA 6. Zachos, EPA P. Gelabert, EPA A. Smith, VIDPNR LEPC TAT Thirteen (13) 4V Lab Chemicals, Alcohols, Solvents, Acids Major Virgin Island Chemical Company (VIChem) St. Croix, US Virgin Islands Approximately S66 Known Lab Chemicals, 590 Unknown Lab Chemicals, 210 Drums, 240 Empty Drums, and 22 Tanks. Possibly Asbestos and Dioxin Containing Materials Ground water, Caribbean Sea A. Drum sampling and stabilization have been completed. 2. ACTION TAKEN; A. January 20, 1990, sampling of all tanks and reactor vessels completed, QANQC of samples and drum logs, general clean up of warehouse area completed, list of chemicals needing dioxin analyses provided by OHM. Three five gallon containers of. potentially dioxin contaminated material sampled. Three bids for analytical work provided by OHM, low bid, ETC labs will be used. Decon trailer's water tank chlorinated. Equipment serviced. B. January 21, 1990, device for collection of unknown lab reagents completed, all drums in warehouse restaged and placed on pallets, warehouse floor cleaned, completed sampling of spent personnel protective clothing and paints, initiated documentation 301542 for shipment of samples. C. January 22, 1990, OSC coordinated with VI Police Department and informed of proper procedures for shipment of explosives to St. Croix. VI Police Department also provided two .22 caliber rifles for the remote opening of unknown lab reagents. Remote opening of unknown containers successfully completed. Paints secured in drums on—site. Most samples packaged and prepared for shipment. General site clean up conducted. D. January 23, 1990, bulked, unknown lab reagents solidified, sampled and secured in three drums in warehouse. Shipment of samples initiated. Initiate final clean up activities and securing of site. 3. FUTURE PLANS AND RECOMMENDATIONS: A. Finalize shipment of all samples. B. TAT will conduct asbestos sampling of material oo the reactor tower and bulk material. Virgin Island Port Authority wells will be sampled once power to them has been restored. C. OSC through DPNR will inform applicable local agencies of the completion of this phase of the removal action. List of chemicals, their location on-site and a video tape of this phase will be distrbuted to these agencies in the near future. D. Analytical, transportation and disposal coordination. E. Demob for this phase. F. In approximately two months, on—site detonation of shock- sensitive, explosive materials, off—site (on-island) detonation of known and unknown cylinders, crushing of empty drums, and if appropriate treatment of dioxin-containing materials. 4. FINANCIAL ACCOUNTING A. CEILINGS TOTAL PROJECT MITIGATION EPA TAT $1,840,000 $1,262,000 $200,000 $105,000 B. Ifl^OBLIGATED HITIGATION FUNDS REMAINING $0 301543 C. COSTS & BALANCES as of 1/21/90 # DCN KE3042 KE3069 KE3073 KE3085 Subtotal Other Costs TAT SalaryNTravel as EPA SalaryNTravel as Estimate of Total Expenditures to Date D. CEILING PERCENTAGES TOTAL PROJECT 27X PERCENTAGE OF •2 MILLION 257. FUTURE POLREPS . FINAL POLREP FORTHCOMING, 7 OBLIGATED AMOUNT $250,000 500,000 250,000 262,000 $1,262,000 of 1/19/90 of 1/23/90 MITJGATION 33Z )(. .SUBMITTED EXPENDED AMOUNT •250,000 166,019 0 0 $416,019 51,305 29,113 $496,437 EPA 15X 1 BY fisu-^^rtNsi^ ^ ' BALANCE $0 333,981 250,000 262,000 $845,981 TAT 497. JWfvV«^3. Dougla^ R. Kodama, On-Scene Coordinator Response and Prevention Bi 'anch DATE RELEASED ijx^ao 301544 X . \- — y MAY2ii.oQg U.S. ENVIRONMENTAL PROTECTION AGENCY POLLUTION REPORT ff^y r Region II Response and Prevention Branch Edison, Nev Jersey 08837 (201) 548-8730 - Commercial and FTS 24 Hour Emergency DATE: May 18, 199 0 TO: C. Sidamon-Eristoff, EPA W. Muszynslci, EPA S. Luftig, EPA R. Sallcie, EPA J. Marshall, EPA G. Pavlou, EPA E. Schaaf, EPA ERD, WH-548B, (E-Mail) B. Sprague, EPA G. Zachos, EPA P. Gelabert, EPA A. Smith, VIDPNR LEPC, VIDPNR TAT POLREP NO.: SITE NO.: POLLUTANT: CLASSIFICATION! SOURCE: LOCATION: AMOUNT: WATER BODY: Fourteen (14) 4V Lab Chemicals, Alcohols, Solvents, Acids Major Virgin Island Chemical Company (VIChem) St. Croix, US Virgin Islands Approximately 566 Known Lab Chemicals, 590 Unlcnown Lab Chemicals, 210 Drums, 240 Empty .Drums, and 22 Tanlcs. Ground vater, Caribbean Sea 1. SITUATION: Emergency Response to a report of a fuming drum. 2. ACTION TAKEN; A. May 9, 1990, 4 TAT personnel and Adalberto Bosque of the EPA Caribbean Field Office arrived on-site in Emergency Response to a report of a fuming drum. TAT suited up in Level B with SCBA's to assess the situation. The fuming drum, Drvim No. 29, was found in the rear of the warehouse. After Edison EPA was informed that the drum vas still fuming and that drum was in a bulging condition, EPA decided to mobilize the ERCS contractor. B. May 10, 1990, tvo ERCS contractors arrived on site and one TAT vas demobilized. ERCS made an entry along with TAT and EPA in Level B. The ERCS contractor loosened the lid of the overpaclc in order to dissipate the pressure build-up, exited Hot Zone, conducted literature search for benzyl chloride, initiated plans to transfer chemical, made a request for shipment of necessary 301545 equipment (i.e., poly overpack drums. Level A PPE, teflon pump). Benzyl chloride is a corrosive liquid and a severe slcih irritant. An incident involving sampling of benzyl chloride drums during Phase I at VIChem occurred on January 15, 1990 and is documented in POLREP #11. In the previous incident, sample techs experienced s)cin irritation vhile sampling benzyl chloride drums, the Hot Zone vas evacuated -until-safe .^ir levels were .reached, and the OSC decided that it was not necessary to continue sampling of benzyl chloride drums. C. May 11, 1990, tvo additional ERCS contractors arrived for a total of four ERCS on site. Equipment was piclced up at the airport. ERCS contractor is delayed due to condensation build-up inside the drums during shipment. Tvo ERCS in Level A suits on an air line entered the Hot Zone. Two TAT and the EPA representative entered in Level B with SCEA's. Three men were on baclcup. Level B personnel didn't handle the drums. The fuming drvim was found to have a bung not in the bung hole but off to one side sitting on the top of the inner-drum. Apparently, benzyl chloride reacted vith moisture in the air to form hydrochloric acid fimes. Except for the un-secured bung, the inner-drum was assessed to be in good condition. ERCS secured the bung and used lime based cement as an absorbent/neutralizer. D. May 12, 1990, ERCS contractor performed a site clean-up before demobilizing. The site electric generator was in operation during the day. E. Other site activities durinq emergency response While on-site during the emergency response, ERCS contractor had their ordinance specialist assess site for the on-site detonation of shoclc-sensitive materials that is planned for June 1990. A suitable on-site area was located. Also, ERCS noted that the EPA phones, which are in the office trailer, were not in service and that an ERCS 12,000 gallon waste treatment pool was missing. F. Other activities - February 2, 1990, OSC received a call from Dave Weston of VIAG. He said that a stranger was on the site during the past three days claiming that he was providing security for EPA. Dave told him to leave site yesterday but noticed today that hand tools, lawn mower, etc. are missing. Dave got the license plate number of the stranger's white Chevrolet pic)cup and he will follow up on this. - March 2, 1990, OSC updated Paul Simon of ORC on status of Removal Action and on March 5, 1990 the OSC mailed him a complete set of Polreps (nos. 1-13). - March 5, 1990, OSC reviewed analytical results collected from materials potentially containing asbestos. None of the insulation on the reactor tover or bul)c material with hand- 301546 .3 t written asbestos labels had any detectable levels of asbestos. They all were comprised of a cellulose-type material. April 11, 1990, due to the significantly increased SPCC activities associated with recent oil spills, OSC duties vere transferred, vith branch chief approval, to the former AOSC, John Higgins, and the former OSC, Doug Kodama, assumed the AOSC position. • April 24, 1990, separate letters were sent to Commissioner Smith, members of the VI Local Emergency Planing Committee, and VITEMA updating them on the Removal Action status and plan for Phase II. List of chemicals, their location on-site and a video tape of Phase I were distributed to these agencies. April 26, 1990, OSC letter was transmitted to Commissioner Smith requesting VIDPNR approval for use of the Anguilla landfill, or an alternate site, for detonation of cylinders containing both Icncvn and un)cnown hazardous substances. May 1, 1990, the AOSC received a call from Jim Sutherland of VIAG. He complained that EPA conducted a very shoddy job, cut electric lines, blev up phone junction box, interfered vith their business, is storing additional hazardous waste on site. AOSC disagreed with his statements. He stated that VIAG will seelc compensation. He also sated that he wants the equipment trailer to be .moved next to the decon trailer. The AOSC agreed that this could be done during Phase II. May 15 & 16, 1990, OSC met with TAT in Edison and discussed the chemical analytical data on water samples collected from the on-site water tanX and Fairfield Wells Nos i t 2. TAT was instructed to provide summary tables and a narrative summary on the cjuality of the data to the OSC by May 25, 1990. Based on these discussions, the data is of good quality and indicates no exceedances of Drinlcing Water Maximum Contaminant Levels. However, since sample collection was both incomplete (WAPA wells were not sampled because they vere not operating) and perhaps not representative (Fairfield well pumps had been inactive, as a result of Hurricane "Hugo", and were just turned on the morning of sampling), additional well sampling will be conducted during Phase II. May 16, 1990, OSC discussed Phase II plans with Jeff Bodi of ERCS and instructed that a worlcplan be submitted for this worlc by May 25, 1990. Also, we discussed whether ERCS had any responsibility for the fuming drum and whether ERCS should absorb some of these costs. The OSC will discuss matter with AOSC, TAT, and the contract DPO prior to concluding the matter. May 15. & 18, 1990, OSC discussed the status of the Removal Action with ORC Attorney Carol Burns, who was recently assigned VIChem. She informed OSC that ORC is proceeding with placing a lien on the VIChem property. I faxed her a copy of this POLREP on May 18. 301547 f - • ' 3. FUTURE PLANS AND RECOMMENDATIONS: A. ERCS completes lab pac)c, paint waste, and empty drum disposal arrangements as soon as possible. B. ERCS develops Phase II worlcplan by May 25, 1990. C. TAT completes Phase I drinlcing water data summary by May 25, 1990. D. TAT completes Phase II field sampling plan by May 25, 1990. E. ERCS must have all supplies and equipment necessary for Phase II shipped to St. Croix via Tropical Inc. in Miami by May 29, 1990. F. Mobilization for Phase II is scheduled for June 11, 1990. Phase II will consist the off-site detonation of cylinders, the on- site detonation of shoclc-sensitive lab reagents, crushing of empty drtims, and the disposal of lab pacXs, paint waste materials and empty drums at a mainland hazardous waste incinerator. G. The OSC will prepare an Action Memo requesting additional monies and a twelve month time limit extension for the completion of VIChem. H. Drum compositing scheme for waste incineration .analysis must be finalized by ERCS, approved by EPA, waste analysis conducted, and drum disposal arrangements finalized for actual drum disposal in Phase III, which is planned for the autumn of 1990. I. The OSC will review the results of the dioxin data analyzed from the three five (5) gallon containers. 301548 '% 4. FINANCIAL ACCOUNTING A. CEILINGS TOTAL PROJECT MITIGATION EPA — - . $ 1 , 8 4 0 , 0 0 0 $ 1 , 2 6 2 , 0 0 0 - . $ 2 0 0 , 0 0 0 - B. ' UNOBLIGATED MITIGATION FUNDS REMAINING C. COSTS & BALANCES a s Of 4/24/90 TAT $105,000 $0 DCN KE3042 KE3069 KE3073 KE3085 Subtotal Other Costs TAT Salary\Travel as EPA Salary\Travel as Estimate of Total Expenditures to Date D. CEILING PERCENTAGES TOTAL PROJECT 33* PERCENTAGE OF $2 MILLION 30t FURTHER POLREPS X POLREP FORTHCOMING_> OBLIGATED AMOUNT $250,000 500,000 250,000 262,000 $1,262,000 Of 1/12/90 Of 5/18/90 MITIGATION 41% L SUBMITPED BY EXPENDED AMOUNT $250,000 268,049 0 0 $518,049 43,932 40,630 $602,611 ' EPA 20% ZZJLI BALANCE $0 231,951 250,000 262,000 $743,951 TAT 42% •t^,9c-^ DATE RELEASED John H i g g i n s On-Scene C o o r d i n a t o r Response and P r e v e n t i o n Branch 3 0 1 5 4 9 • ^ f • /bty'^Xy) m :S U . S . ENVIRONMENTAL PROTECTION AGENCY POLLUTION REPORT Region II Response and Prevention Branch Edison, New Jersey 08937 (201) 548-8730- Commercial and FTS 24 Hour Eioergency DATE: June 13, 1990 TO: C. Sidamon-Eristoff, EPA W. Muszynski, EPA S. Luftig, EPA R. SaUia, EPA J. Marshall, EPA G. Pavlou, EPA ERD, WH-548B (E-Mail) Sprague, EPA Zacho«, EPA Gelabert, EPA Smith, VIDPNR B. 6. P. A. LEPC TAT POLREP NO.I SITE NO.: POLLUTANT t CLASS1HiCATI ONJ SOURCE! LOCATION: AMOUNT: NATER BODY! 1. SITUATION: Fifteen (15) 4V Lab ChemicalSi Alcohols, Solvents, Acids Majnr Virgin Island Chemical Conp^ny (VlChaa) St. Croix, US Virgin Islands Approximately 366 Known Lab Chemicals, 590 UnknOMn Lab Chemicals* 210 Drums, 240 Ejtpty Drums, and 22 Tanks. Possibly Asbestos and Dioxin Containing Materials Ground wateri Caribbean Sea Initiation of Phase II Be«ov«l I details. See previous polreps for Phase 2. ACTION TAKEN: A, June 5, 1990, OSC discussed bids for waste analysis of composite drum samples with ERCS and Rick Haworth, Region 1 DSC. Based on the discussions the' OSC directed ERCS to contract with the second low bidder, " Analab**! for disposal analysis. 301550 ^ I B. June 7, 1990, as requested, AOSC transmitted memo to Regional Administrator Sidamon-Eristoff that furnished detail on the May 1, 1990 phone conversation between the AOSC and Jim Southerland of VIAG. C. June 11, 1990, all personnel arrived on Bt. Croix. OSC and TAT visited site and spoke to Andy with Infinity Services, who is a sub-lea*ee of a portion of the warehouse. Infinty Services was inforfped that they could not access the hot zone during clean—up activities. D. June 12, 1990, OSC discussed clean-up status and plans with Jim South»erlwnd of VIAG. He reiterated his complaints, which are docureentsd in P0LREP«I14 and in the June 7, 1990, memo fro* the AOSC to the Regional Administrator. However, he was calm and agreed that EPA and E.RCS could utilize space for storage of equipment and supplies in the warehouse. He also agreed that EPA could use his phone to aake credit card calls. EPA, TAT and ERCS (7) mobilized on site. ERCS started site CBt-up and reported a set of aluminum «iteps stolen "from the galley trailer. In addition, phone lines to the command post were cut. VITELCO was notified and indicated that phone service may be restored at the end of the weak. EPA *nd TAT met witli D«tv» Canegata, Assistant Commiccioner of DPNR to discuss cylinder detonation. In addition, EPA and TAT flket with Delroy Richards, Chief of the Department of Public Safety to request police assistance with the detonation. Police agreed to accompany detonation convoy from site with two police cars and to seal off landfill from public during operations. TAT also met with Fire Marshall Cyprian King tn rpquest A tirt truck and EMS service for the detonation. E. June 13, 1990, site set-up continues. ERCS mobilized five (5) personnel on site and demobilized one (i) personnel. A chemist from Ch«m Waste arrived on site to supervise the lab pack operation. Breathing-air and a port-a-john were delivered to the site. EPA and TAT held a Contingency Meeting with the following agencies: DPNR, VI Fire, Bureau of Corrections, Department of Health, ERCS. In addition EPA, TAT, ERCS and two represenatives from DPNR visited the detonation site (Anguilla landfill). WAPA and VIPA were notified by TAT that the Fairplain wells »6 and *9} and VIPA wells fl and «2 will be sampled i o r halogenated hydrocarbons. A press release will be placed in the Daily News newspaper on Friday June 10, l990 informing the publii. of the temporary road and landfill closing during the detonation activity. 301551 : • ERCS began re-staging the overpacked drums according to their compatabjlity classes delineated by the analytical results. ERCS restored phone service to the command post. 3. FUTURE PLANS AND RECOMMENDATIONS: A. TAT will prepare minutes of June 13, 1990 Contingency Planning Meeting. B. Detonation of shock sensitives and of cylinders off-site at landfill on Saturday »orning June 16, 1990 in accordance with the Ordinance Plan. C. TAT will provide all necessary notifications regarding the detonation, including St. Croix Prison, Police, Fire, EMS, DPW St. Croix STP, Alexander Hamilton Airport, FAA, and businesses near the airport and landfill. Also, TAT will notify the NRC of the environmental ralease within one hour after final detonation. TAT will also conduct air monitoring. D. ERCS and Chem Waste will initiate labpacking on June 14, 1990J ERCS equipment and supplies will be delivered on June 14, 1990. E. Drum crushing will be initiated the week of June 16, 1990. The sixteen drums containing Benzyl chloride will be transferred to poly 55 gallon closed-top drums and overpacked inside 65 gallon drums. F. The OSC will review the results of the dioxin data analyzed from the three five (5) gallon containers. G. TAT will perform sampling of the WAPA and VIPA wells. 301552 « ' . •* 4 . FINANCIAL ACCOUNTING A. CEILINGS TOTAL PROJECT MITIGATION EPA TAT •1,040,000 il,262,000 «200,000 S105,000 B. UNQBLIBATED MITIGATION FUNDS REMAINING SO C. COSTS & BALANCES as of 6/13/90 DCN OBLIGATED EXPENDED BALANCE AMOUNT AMOUNT KE3042 »250,0OO ^250,OOO >0 KE3069 500,000 327,999 172,001 ICE3073 250,000 0 250,000 KE30a5 262,000 O 262,000 Subtotal »1,262,000 «577,999 »684,001 Other Costs TAT SalaryNTravel as of 6/13/90 58,326 EPA SalaryNTravel as of 6/13/90 46,097 Estimate of Total Expenditures to Date •682,422 D. CEILING PERCENTAGES TOTAL PROJECT MITIBATION EPA TAT 37X 46X 23X 56X PERCENTAGE OF »2 MILLION 34X FUTURE POLREPS V CT ") D /I FINAL POLREP FORTHCOMING /\ SUBMITTED BY ^"--^i e*-''^--^- f-f-wAO>(,..^o John Wiggins vjC On-Scene Coordinator Response and Prevention Branch DATE RELEASED ^^/.^^-^^^g^ ^ ^ / ^ 9 0 301553 .4 CCT I i 1990 U . B . ENVIRONMENTAL P1?nTFr.TinN AGENCY POLLU1 ION REPORT R e g i o n I I R e s p o n s e and P r e v e n t io.n B r a n c h E d i s o n , Wew J e r s e y 08B37 <2013 t>4G-8730- Cotr.mercial ^nd FTS 24 Hour Emergsrncy DATE: J u n e 16, 1990 TO: C. S i d a m o n - E r i s t o f f , EPA W. M u s z y n s k i , EPA S. L u f t i g , EPA R. S a l k i e , EPA J . M a r s h a l l , EPA G, P a v l o u , EPA ERD, WH-548B ( E - M a i l ) Rnragiio. FPA Z a c h o s , EPA G e l a b e r t , EPA S m i t h , VIDPNR 8 . G. P. A. LCPC- TAT POLREP NO. I S I T E NO.I POLLUTANT: CLASSIFICATION: SOURCE: LOCATION: AMOUN1 I WATER BODY: S i x t e e n (16) . 4V Lab Chemicals, A l c o h o l s , Solvent*, Acids Major Virgin Icland Chemical Company (ViChcm) St. Croix, US Virqin Islands Appruximatcly 5CG Known Lab Chmmicals, S90 Unknown Lab Chemicals, 210 Drums, 240 Empty Drums, and 22 Tanks. Possibly Asbestos and Dioxin Containing Materials' Ground water, Caribbean Sea 1. SITUATION; Phase II Removal Action continues. 2. ACTION TAKEN; A. June 14, lyyo, ERCS continues labpacking and drum cogregation. Box trailer with ERCS supplies uoH delivered to the site frnn the ship container port. Also, airport containers with ERCS equipment were delivered to the site ana were unloaded. TAT speaks to Dave Caney^La (DPNR) about a press release informing the public of the detonation and obtain"^ Mr. Canegata's Approval to release the notification. TAT investigates a well drilling operaliun on the east side of the 301554 til C^mm cito no>r fh« usiPCi F.iirnlrtlnt Wall t6i «I.S. Geologic burvey was installing wiylil (0) cbservaiion wel 1 c as part nf A series of ground water flow-monitoring wells in the brackish aqui fer. Todd Shank of DPNR stops by the site to inform EPA that thi» Dept. of Public Works (DPW) is hesitant about the detonation taking place at the landfill. ERCS explosive expert arrives o»i *ite. CPA, TAT and explosive expert visit detonation site. CRCH iMtcsr-« ePA n* prftStpnc; trancwurtino Cylinders and "-.hock sensitives from VI Chem to landfill. EKCS requests a waiver of RC1RA tr Ancportat ion rpgulations and not to hold ERCS harmlesa if somethiftq Qoea wrcnj during transpwft. CPA infefMcd Pf^Cfi that th* NAtinnrtl Contingency Plan (NCP) allows EPA to transport hazardous materials in emergenty situations. It challenged, EPA would exhibit credentials, however, it is unlikely for EPA to be challenged since the Police Dept. and DPNR are a part OT tne exercise. EPA infwrjutrJ CRCC •iha* OCC did not have authnrlty to write the requested hold-harmless waiver. Subsequent consultations with ERCS and tPA contract offiti.»ls revealed that EPCS is covered by liability insurance. EPA faxed January well ixsrftpl ing data summary to Susan Shaw nf EPA's Region 2 Water Management Division (WMD), At UMT7 request, EPA directed TAT to investigate the Texaco gasoline station on Centerline Rd. east of FrederikStpd to observe at wei I digging w«»* yulnW on. TAT reported no activity At that station and no artivity At the other two Texaco stations nearby rrederikstfcfU. EPA, TAT and ERCS have a meeting to discuss detonation operations. B. June 15, 19VO, press r*»l ease noiifying the public of detonation was not in the Virgin Island Daily News newspaper. En.yil'.fml"'* exprr* and TAT vicit with H r ^ CJnlpf CyBrJiij Kif^d to give details about detonation for June 16, 1990. ERCS continues to lab pack and segregate drums. TAT, EPA and DPNR meet with several DPW officials and receive approvals from Mr. Slater, landfill supervisor, and Mr. Hanson, sewerage treatment plant supervisur, contingent upon the approval of the acting DPW Commissioner, who is on travel in St. Thomas. Mr. Canegata of DPNR subsequently informs EPA thai DPW approval for dotonatinn at the landfill was received. TAT called Del r uy Ri^-hords, Chief of Public Safety »nd gavi- ({K>L.4i1s of the detonation. 301555 Cyf^rian King, of the Vl Fire DepI-. dRlivcred the cxplosivoc permit to ERCS on the VI Ch^m site. FRr.fi inforras EPA of problems with transporting explosives to the island. Detonators and ptrf forstor charges are still In Tex«». They will not arrive* until Monday. When questioned, ERCS stated that the transporter verbally confirmed o«i Tuesday, June 12, 1990, that the shipmeni h.id bean transported. Another shipment of explosives JS on tne island ^lur^rj «t the quarry locked up anfj the owner is on Puerto Rico until next week. Numerous attempts to expedite matters failed. EPA and TAT contact all necassary agencies to inform then of the postpoMfr/nent of tho detonation and to schedule a Cor»Lingeney Planning Meeting at DPNR offices for 10:00 AM Tuesday, June 19, 1990. EPA informed tKUls" tnat tnsrtr will Lc .,,., ve>\*U an Sunday. EPA questioned ERtE -bw«l the »*a%uc of tha drum rrii'Sh opBritO'' and equipment. ERCS did not knov when equipment would arrive, ERCG informed EPA that their (ERCG) lab (ETC) mad« a mistake *nd used all of the samples from the acid liquid compatibility grouping snri thai additional sampling was needf»rt. ^iso, samples from drum numbers 132 and 136 generated reactions (ie. elevated temperature* and gas evolution). From drum markings, it is suspected that these drums contain Muriatic acid And Hydrochloric acid and should be included in a sep/irate waste stream. ERCS wanted to know if it was okay to composite samples oo site. EPA informed ERCS that n.-»rk,Toino *nd rA«pnniting of sample from the acid liquid group would be at ERCS expense and that on site compositing of nAapI«r v«» inappropiate due to lack of adpnuate laboratory facilities. Explosive expert will work as a laborer and be billed accordingly until detoi)«tion is back on track. C. June 16, 1990, the Daily News newspaper released an article informing the public of the postponed detonation. In addition, the Daily N P W S mentioned that there was no nvw% release notifying the public of tho proposed detonation. However, the article did not mention that this omission was due to their failure to print the public notice furnished to xhem by TAT oi, June 14, 1990. ERCS fiiii*nes l«bpacking ww» k and contJnuec overgtckinq. A drum (#81) of Benzyl acetate mixed with Acetic acid (glacial) which is • fl^mmiblo o»^9*nic ;arirl And is the nnly drum in a single waste stream. If the drum cannot be neutralized or diluted to a non- flashpoint condition, disposal analysis and transportation cost will approximate »8500, as it nay require its own SeaLand container. A bench scsle experimenl was performed. A small portion of the Benzyl acetate and Acetic acid mix w<a> diluted with water to see if the two would separate (Benzyl acetate insoluble in water and Acetic acid soluble in water). Results were inconclusive. It is decided to ship the «^tor.k quart sample to ETC for bench scale 301556 , I testing lo requii-ed dilution. Final rlrt er niinat Ion ef how to handle rlriim number 81 will be made priur Lu Phane 1X1. ERCS starts and completes packaging of additional sample stock iiifc-ultrJ for d i ^ ^ u ' - ^ l AHAlycic And disposal. 3. FUTURE HLANS AND RFnOMMENDATIONCi A. On June 19, 1990, there will be m Contingency Planning Meeting. B. Remainder of explosives are to arrive on St. Croix, June IB, 1990. C. Detonation of shock sensitives and cylinders off-cite at landfill will be resth&duled during the Continqency Planning Meet ing n. TAT will crovide all nu't^ksary not i f i rat ions regarding the detonation, including St- Croix Prison, Police, U r e , CM3, DPW St. Croix STP, Alexander Hamilton Airport, FAA, and businesses ne^r the airport and landfill. Also, TAT will notify the NRC of the environmental release within one hour after final detonation. TAT will also conduct air monitoring. E. Drum crushing will be initiated the week of June 10, 1990. The sixteen drums containing Benzyl chloride will be transferred to poly 55 gallon closed-top drums and overpacked inside BS gallon drums. r. Tho DSC will review thr results of tho dioxin dat;% AnalyrttJ from the three five (5) gallon containers. ,v 6. TAT will perform sampling of the WAPA and VIPA wells nearest the site. 301557 •1 1 . FINANCIAL ACCOUNTTNQf A. CEILINGS THTAi PROJECT MITIGATION EPA •1,640,000 $1,262,000 S200,000 B. UNOBLIGATED MITIGATION FUNDS REMAINING C. COSTS fc BALANCES as of 6/X6/90 DGN KE3042 KE3069 KE3073 KCOOOS OBLIGATED AMOUNT S250,000 500,000 2:30,000 2fi?.0O0 EXPENDED AMOUNT •250,000 375,081 0 O $1,262,000 Subtotal Other Costs TAT SalaryNTravel as of 6/16/90 EPA S.ilaryNTravel ac of 6/16/90 Estimate of Total Expenditures to Date D. CEILING PERCENTAGES TnTAJ PROJELT MIT I OAT ION 40X SOX PERCENTAGE OF *2 MILLION 37Z «625,081 63,366 48,097 »736,544 EPA 24X TAT •105,000 SO BALANCE •0 124,919 2bO,000 262,000 •636,919 TAT 607. FINAL POLREP FUTURE POLREPS _FORTHCOMING SUBMITTED BY John h i g g i n s ^ ^ C gy^ns >-'(^ On-Scene C o o r d i n a t o r Response and t-revention BrMui.ii DATE RELEAStU '''^. '"??A 301558 I • i U . S . ENVIRONMENTAL PROTECTION AGENCY P O L U m O N REPORT Region II Response and Prevention Branch Edison, Nev Jersey 08837 (201) 548-8730- Concnercial and FTS 24 Hour Emergency DATE: June 20, 1990 TO: C. Sidamon-Eristoff, EPA W. Muszynski, EPA R. Caspi, EPA R. Sallcie, EPA J. Marshall, EPA G. Pavlou, EPA ERD, WH-548B (E-Mail) ' B. Sprague, EPA G. Zachos, EPA P. Gelabert, EPA A. Smith, VIDPNR liEPC TAT POLREP NO.: SITE NO.: POLLUTANT: CLASSIFICATION: SOURCE: LOCATION: AMOUNT: WATER BODY: 1. SITUATION; (17) Seventeen 4V Lab (^lemicals. Alcohols, Solvents, Acids Major Virgin Island Chemical Company (VIChem) St. Croix, DS Virgin Islands Approximately 566 Known Lab Chemicals, 590 Unlcnown Lab Chemicals, 210 Dirums, 240 Empty Drums, 2uid 22 Tanlcs. Possibly Asbestos and Dioxin Containing Materials Ground water, Caribbeem Sea Phase II Removal Action continues. 2. ACTION TAKEN: A. June 18, 1990, ERCS mobilized a subcontractor (drum crush operator) on site and continued overpacking . Initiated and completed labpacking, waste paint inventory and drum segregation. An air freight container was delivered to the site. ERCS resampled drum numbers 81, 163 and 164 for disposal analysis and waste streaun. This was the only additional drum sampling 301559 I . ' conducted in Phase II. ERCS will nanifest, with material safety data sheets (MSDS), the drums containing Benzyl chloride as a seperate waste stream. ERCS indicated that the Benzyl chloride may have to be put in one gallon charges. It was then decided that the Benzyl chloride will not be repacked vintil it is known how Chem Waste and other disposal facilities will acx:ept the Benzyl chloride. This may not be Icnovn until completion of Phase II. In addition, EPA directed ERCS to contacrt "Velsicol", the manufacturer, as to returning the drums of Benzyl chloride, which have manufacturer seals. Cyprian King, Fire Cliief re-certified the explosive permit. EPA contacted the following : Jet Research in Dallas, Arrow zind Four Star, both in San Juan, several times and successfully arranged for explosives to be delivered to St. Croix at 1330 hours. Explosives arrived at 1400 hours and were cleared through Customs by EPA and ERCS. ERCS informed EPA that drum crushing equipment is in Port Elizeibeth, NJ. EPA was informed that equipment would be in St. Croix at 14 00 hours on June 19, 1990. EPA apprised ERCS that they (ERC:S) and their subcontractors have managed equipment and supply delivery inadequately. It took zm extended effort by EPA to get the explosives in St. Croix. EPA faxed and received back a fax of release form for transmittal of Uranyl acetate and Merciiry (metallic) compounds to Poly Sciences, Inc. a recycling/reusing facility. B. June 19, 1990, EPA, TAT, DPNR and ERCS attended a Contingency Planning Meeting to set a new date for the detonation. EPA, TAT and ERCS meet with the Deputy Commisioner of DPW to schedule a new date for the detonation. ERCS sampled drum numbers 81, 163 and 164. ERCS also overpacked t h e spent wet cell batteries on site. In addition, ERC:S completed labeling of l2±>packs. ERCS informed EPA that there is a problem with a five (5) gallon can of asbestos and mineral spirits (flashing cement). This roofing material (mineral spirits) caruiot be landfilled and cannot be incinerated. Dave Martin, of Chem Waste attempted to see if Chem Waste would accept the material. A material profile was sent. ERCS informed EPA that they are "uncomfortable* shipping a glass container of Mercury (metallic) to Poly Sciences, Inc. ERCS stated that they would prefer shipping the material in a welded steel conical container,which is the single package specification for air shipment of Mercury for DOT and Intemational Air Transport 301560 # Association (LATA) regulations. EPA indicated that this would entail the following: package shipment, receipt, clearing customs and VI excise tax and transferring Mercury from glass container to steel container. EPA then recommended that ERCS proceed with alternate packaging (overpacking) in accordance with DOT and lATA shipping regulations. ERCS questioned whether EPA was compelling them to do something that they (ERCS) was "uncomfortable" with. OSC responded that he would sign the shipping papers. Drum crushing equipnient was shipped from JFK airport, but did not arrive in St. Croix as it vas taken off the plane in St. Thomas. C. June 20, 1990, TAT provided all necessary notific:ations regarding the detonation, including St. Croix Prison, Police, Fire, EMS, DPW , St. Croix STP, Alexander Hamilton Airport, FAA, and businesses near the airport and landfill. ERCS completed restaging of drums. EPA discussed packaging of Mercury with ERCS. ERCS chemist informed EPA that he has contacted All-PAK 2md that they informed him that their container is acceptable for overpacking the glass container of Mercury. EPA indicated to ERCS that they should further safeguard shipment by placing materialin overpacked metal can with vermiculite . ERCS agreed to overpack materials, but is still uncomfortable. OSC signed shipping papers. Drum crushing equipment ai-rived on St. Croix emd will be delivered tomorrow. 3. FUTURE PLANS AND RECOMMENDATIONS: A. Detonation of shock sensitives and cylinders off-site at landfill will take place on June 21, 1990. B. TAT will notify the NRC of the environmental release within one hour after final detonation. C. Drum crushing will be initiated upon arrival of the drum crushing equipment. D. TAT will perform sampling of the WAPA and VIPA wells nearest the site on June 22, 1990, contigent upon CLP Lab selection. E. Transportation of labpacked materials and paint waste will be coordinated with mini-removals at DVI on June 25, 1990, and June 26, 1990. F. Phase II Site Demobilization. G. The OSC will review the results of the dioxin data analyzed froa the three five (5) gallon containers. 301561 • ^ f " # 4 . FINANCIAL ACCOUNTING A. CEILINGS TOTAL PROJECT MITIGATION EPA $1,840,000 $1,262,000 $200,000 B. UNOBLIGATED MITIGATION FUNDS REMAINING C. COSTS & BALANCES as of 6/20/90 DCN KE3042 KE3069 KE3073 KE3085 Subtotal Other Costs Estimate of Total Expenditures to Date D. CEILING PERCENTAGES TOTAL PROJECT 421 PERCENTAGE OF $2 MILLION 38% FUTURE POLREPS FORTHCOMING TAT $105,000 $0 OBLIGATED AMOUNT $250,000 500,000 250,000 262,000 $1,262,000 of 6/20/90 of 6/20/90 MITIGATION 51* EXPENDED AMOUNT $250,000 398,823 0 0 $648,823 68,706 49,867 1 $767,396 EPA 25* BALANCE $0 101,177 250,000 262,000 $613,177 TAT 65 FINAL POLREP SUBMITTED BY John Higgins On-Scene Coordinator Response and Prevention Branch li DATE RELEASED 301562 /\:yV^O zy U.S. ENVIRONMENTAL PROTECTION AGENCY POLLUTION REPORT Region 11 Response and Prevention Branch Edison, New Jersey 0883/ (201) 548-8730- Commercial and FTS 24 Hour Emergency POLREP NO.: SITE NO.: POLLUTANT: CLASSIFICATION! SOURCE: LOCATION: AMOUNT: WATER BODY: DATE: June 23, 1990 TO: C. Sidamon-Eristoff, EPA W. Muszynski, EPA R. Caspe, EPA R. Salkie, EPA J. Marshall, EPA G. Pavlou, EPA ERD, WH-54BB (E-Mail) B. Sprague, EPA G. Zachos, EPA P. Gelabert, EPA A. Smith, VIDPNR LEPC TAT Eighteen (18) 4V Lab Chemicals, Alcohols, Solvents, Acids Major Virgin Island Chemical Company (VIChem) St. Croix, US Virgin Islands Approximately 566 Known Lab Chemicals, 590 Unknown Lab Chemicals, 210 Drums, 240 Empty Drums, and 22 Tanks. Possibly Dioxin Containing Materials. Ground water, Caribbean Sea 1. SITUAjriDN: Phase 11 Removal Action continues. 2. ACTION _ T^KEN: A . J u n e 2 1 , 1 9 9 0 , d e t o n a t i o n o f s h o c k s e n s i t i v e s o r r e a c t i v e m a t e r i a l s and c y l i n d e r s c o n d u c t e d b e t w e e n 0 6 0 0 - 0 8 0 0 h o u r s a t A n g u i l l a l a n d f i l l . EPA n o t i f i e d NRC o f t h e e n v i r o n m e n t a l r e l e a s e w i t h i n a h a l f - h o u r 301563 bIRCS initiated and completed drum crushing. ERCS prepared galley trailer for demobe. ERCS demobed explosive expert. B. June 22, 1990, EPA (Higgins) and TAT (Bechtel) demobed from site. ERCS demobed foreman and drum crush operator (subcontractor). ERCS continued general site clean-up and preparation for demobi1i zation. Box trailer for labpacked materials and paint waste arrived on si te. C. June 23, 1990, Dave Martin from Chem Waste informed EPA that the box t r a i l e r delivered to site is owned by "Tropical" and they a r e not allowed to transport hazardous waste. Loading of labpacks onto appropiate boxtrailer postponed until arrangements can be made with hazardous waste transporter. ERCS demobed three personnel from site. 3. FUTURE PLANS AND RECUMMENDATIONS; A. TAT will perform samplinq of the WAPA and VIPA wells nearest the site on June 25, 1990. B. Transportation of labpacked materials and paint waste will be coordinated with mini-removals at UVI. Scheduling of hazardous waste transportation is unknown at the present time; and may be determined on June 25, 1990. C. Phase II Site Demobilization. D. The OSC will review the results of the dioxin data analyzed from the three five (5) gallon containers. 301564 -. 1 ^ • PJ.NANCJ AL ACCOUNTING A. CEILINGS TOTAL PROJECT MITIGATION EPA SI,840,000 SI,262,OOO S20O,00O B. UNOBLIGATED MITIGATION FUNDS REMAINING C. COSTS & BALANCES as of 6/20/90 DCN KE3042 KE3069 KE30/3 KE3085 Subtotal Other Costs Estimate of Total Expenditures to Date TAT S105,0O0 so OBLIGATED AMOUNT S250,000 500,000 250,000 262,000 SI,262,ooo of 6/20/90 of 6/20/90 EXPENDED AMOUNT S250 398 S648 68 ^9, S767 ,000 ,823 O 0 ,823 ,706 ,867 ,396 BALANCE 101, 250, 262, •613, SO 177 ooo 000 .177 D. CEILING PERCENTAGES TOTAL PROJECT 427. PERCENTAGE OF S2 MILLION 387. FUTURE POLREPS L POLREP F0RTHC0M1NG_X MITIGATION 517. &\ n- SUBMITTED BYJV, EPA 257. \\ rx i - V) ^ r 3-o<W\52rV\r TAT 657. \ \ v<>5\Avi*iSl John Hoggins On-Scene Coordinator Response and Prevention Branch -W DATE RELEASED 301565 U . S . ENVIROhiMENTAL PROTECTION AGENCY POLLUTION REPORT Region I I Response and P r e v e n t i o n Branch E d i s o n , New J e r s e y 08837 (201) 548-8730- Commercial and FTS 24 Hour Emergency POLREP NO.: SITE NO.: POLLUTANT: CLASSIFICATION: SOURCE: LOCATION: AMOUNT: WATER BODY: DATE: J u l y 12, 1990 TO: C. S i d a m o n - E r i s t o f f , EPA W. Muszynski, EPA R. Caspe, EPA R. S a l k i e , EPA J . M a r s h a l l , EPA G. Pavlou, EPA ERD, WH-548B (E-Mail) B. Sprague, EPA G. Zachos, EPA P. G e l a b e r t , EPA A. Smith, VIDPNR LEPC TAT Nineteen (19) 4V Lab Chemicals, Alcohols, Solvents, Acids Major Virgin Island Chemical Company (VIChem) St. Croix, US Virgin Islands Approximately 566 Known Lab Chemicals, 590 Unknown Lab Chemicals, 210 Drums, 240 Empty Drums, and 22 Tanks. Possibly, Dioxin Containing Materials Ground water, Caribbean Sea 1. SITUATION: Phase II of Removal Action completed. 2. ACTION TAKEN: A. June 25, 1990, VITELCO restores phone service. TAT samples VIPA and WAPA wells, packages samples, and ships samples via FedEx. This completes all TAT work on-site. Dave Martin of ChemWaste informs EPA that Trailer Marine Transport (TMT) is a certified hazardous waste transporter. TMT spots box trailer on-site for labpack loading. B. June 26, 1990, EPA reviews ERCS memo regarding theft of treatment pool and aluminum stairs between Phase I demob (1/24/90) and Phase II mob (6/11/90). ERCS demobilizes the galley trailer and air compressor. The bomb box is picked up at the site for .transport to EPA, Edison. ERCS contacts John Bergman of Velsicol regarding the possible 301566 reclaim of the eight, 55 gallon benzyl chloride drums. Velsicol vill consider and contact EPA. ETC informs OHM who informs EPA that additional compatibility testing revealed unacceptable reactions for drum nos. 159 and 75 within the acid liquid group and dnim no. 133 within the base neutral group. Additional four quart samples are taken from each of these drums. ERCS also informs EPA that the bench scale testing for d m m no. 81 indicated that neutralization of the acetic acid would generate 3-4 additional drums of waste. AOSC informs ERCS of his approval to reimburse ERCS for replacenent of aluminum stairs and treatment pool. The basis for this decision is EPA's prior determination, as documented in a November 27, 19S9 EPA letter to ERCS, to not provide security while off-site. EPA informs ERCS to provide landfill/incineration analysis for the crushed drum sample. C. June 27, 1990, ERCS packages samples for drum nos 81,75, 159, and 133 and arranges transport via Four Star Transport to San Juan Airport where the samples will be shepherded by TAT, who will retain the services of a custom clearance broker, and will be transferred to FedEx for delivery to ETC, Findlay. Dave Martin of ChemWaste packages the 1 quart glass container of mercury waste and ships material to Bethlehem Apparatus, Hellertown, PA. (EPA IDI PAD002390961). Box trailers, loaded with labpacks, are transported to the container port and clear U.S. Customs. Phase II demobilization completed. ERCS and EPA leave site. D. June 29, 1990, AOSC discusses compliance status of Trade Waste Incinerator (TWI) with Region V and there is no problem with sending CERCLA wastes. Also, the status of Bethlehem Apparatus is discussed vith Region 3 and they are in compliance. TAT delivers Detonation Report Summary. OSC mails letter to Mr. Cherra Hyliger, Deputy Commissioner of Operations for the Public Works Department, detailing the June 21, 1990 detonation of VIChem hazardous waste materials at the Anguilla Landfill and addressing his concerns regarding pubic health. E. July 2, 1990, AOSC arranges to meet Dave Martin of ChemWaste at Port Everglades to clear hazardous waste through. U.S. Customs. FedEx informs ERCS who informs EPA that Analab is not an approved lab for the receipt of "soil from a foreign land", which was the shipping paper description for the crushed drum samples. ERCS arranges for the sample to be transported to the NYTEST lab, which is a US Dept. of Agriculture and US (^istoms approved lab, for analysis. 301567 TAT informs EPA that the driim sanples are still in San Juan at the Four Star Company and that TAT cannot provide the transfer services requested by EPA because such work would constitute "personal services". EPA holds several heated discussions with the TAT leader and the TAT Zone Management before TAT agrees to provide the requested transfer sezrvices. The VIChem drum samples clear customs and leave San Juan via FedEx. Off-Site Facility Selection checklists completed for TWI and Bethlehem Apparatus are approved by Bruce Sprague. F. July 3, 1990, ERCS informs EPA that the mercury product and Uranyl acetate arrived at Polysciences intact. OSC discusses the matter of the stolen aluminum stairs and treatment pool with the Contract Officer, Tim Grier. He agrees that, since EPA decided not to demobilize equipment and to not provide security vhile off-site (as documented in the November 27, 1989 letter), replacement of this equipment is an eligible cost and he approves of the expenditure. G. July 5, 1990, AOSC arrives in Florida and meets with U.S. (Customs officials and Crcwley Maritime Corp. at Port Everglade. Customs inspector is confused as to the appropriate "PL No." to be entered on Customs Form 7523 and requests EPA to return tomorrow. H. July 6, 1990, VIChem and St. Croix "mini-removal* hazardous waste clears Customs (PL No. is 3209.90*00004). Crowley trailers are inspected by AOSC and all dmms are intact, no leaking or damaged drums. Drums are transferred from Crowley trailer to ChemWaste Truck by ChemWaste. ChemWaste Truck, which is placarded "Dangerous", "Poison", and "Flammable", departs Port Everglade. I. July 9, 1990, OSC reviews status and plans for disposal analyses. ERCS agrees to furnish revised bulking scheme and informs EPA that drum samples are scheduled to arrive at Analab today for 21 day turnaround analysis. J. July 10, 1990, OSC discusses possible reclaim of the benzyl chloride drums with Mr. Bergman of Velsicol. He informs OSC that he had passed the matter on to Velsicol, Memphis and that someone from that office should have contacted EPA. OSC informs Mr. Bergman that he would again contact him if no word is heard from other Velsicol representatives. At this point, reclaim of this 20 year old product does not appear to be promising. OSC directs ERCS to furnish drum location map and inventory of unused supplies at VIChem. 301568 3. FUTURE PL^NS AND RECOhtMENDATIONS: A. The OSC vill prepare an Action Memo requesting a twelve month time limit extension. B. The OSC will review expended and expected costs and determine whether a request for additional monies is necessary. C. The OSC will review the results of the dioxin data analyzed from the three five (5) gallon containers. D. TAT vill complete Phase II photodocumentation. E. TAT vill complete Phase II well sample analysis summary. F. Analab vill complete disposal analyses. G. ERCS will transmit analytical data to EPA and procure drum disposal facility. H. Phase III will be planned and mobilized. 301569 4 . FINANCIAL ACC0UN7TNG A. CEILINGS TOTAL PROJECT MITIGATION EPA $ 1 , 8 4 0 , 0 0 0 $ 1 , 2 6 2 , 0 0 0 $ 2 0 0 , 0 0 0 B. UNOBLIGATED MITIGATION FUNDS REMAINING C. COSTS & BALANCES a s o f 6 / 2 3 / 9 0 TAT $ 1 0 5 , 0 0 0 $0 DCN KE3042 KE3069 KE3073 KE3085 Subtotal Other Costs TAT Salary\Travel as EPA Salary\Travel as Estimate of Total Expenditures to Date D. CEILING PERCENTAGES TOTAL PROJECT j 45% PERCENTAGE OF $2 MILLION 41% FURTHER POLREPS AL POLREP FORTHCOMING_X \ . OBLIGATED V AMOUNT $250,000 500,000 250,000 262,000 $1,262,000 Of 7/6/90 - of 7/12/90 MITIGATION 54% ._ SUBMITTED BY. DATE RELEASED^^ EXPENDED BALANCE AMOUNT $250,000 $0 434,673 65,327 0 250,000 0 262,000 $684,673 $577,327 80,880 62,387 $827,940 EPA TAT 31% 77% ^ ^ > y John Higgins On-Scene Coordinator Response and Prevention Branch ZVUii^^-i. A-K^O 3 0 1 5 7 0 u U.S. ENVIRONMENTAL PROTECTION AGENCY POLLUTION REPORT /^^GumQA ^n. Region II Response and Prevention Branch Edison, Nev Jersey 08837 (201) 548-8730- Commercial and FTS 24 Hour Emergency POLREP NO.: SITE NO.: POLLUTANT: CLASSIFICATION: SOURCE: LOCATION: AMOUNT: WATER BODY; 1. SITUATION; DATE: August 3, 1990 TO: C. Sidamon-Eristoff, EPA W. Muszynski, EPA R. Caspe, EPA R. Salkie, EPA J. Marshall, EPA ;E.Schaff, EPA» G. Pavlou, EPA ERD, WH-548B (E-Mail) B. Sprague, EPA G. Zachos, EPA P. Gelabert, EPA A. Smith, VIDPNR LEPC TAT Twenty (20) 4V Lab Chemicals, Alcohols, Solvents, Acids Major Virgin Island Chemical Company (VIChem) St. Croix, US Virgin Islands Approximately 566 Known Lab Chemicals, 590 Unknown Lab Chemicals, 210 Dmms, 24 0 Empty Drums, and 22 Tanks. Possibly, Dioxin Containing Materials Ground water, Caribbean Sea Emergency response to a report of a fuming drum. 2. ACTION TAKEN: A. July 24, 1990, Jim Southerland of VIAG informs EPA that a dnim housed in the warehouse at VIChem is fuming. The OSC contacted TAT and ERCS and instructed them to prepare for site mobilization. B. July 25, 1990, the OSC and 1 TAT personnel arrive on-site and determined the fuming drum to be drum no. 22. A review of the drum logs indicated that this vas one of sixteen drums containing benzyl chloride. Benzyl chloride is a corrosive liquid, a severe skin irritant, and will volatilize to form hydrochloric acid. A previous response to a fuming drum emergency was conducted in May 1990 and is the main subject of POLREP #14. The OSC confirmed ERCS mobilization for the next day. A single site telephone line (#809- 778-2199) was operational. TAT vas instructed to furnish a 301571 -.-.s # m Material Safety Data Sheet (MSDS) for benzyl chloride in the event that it became imperative to ship this material off St. Croix. C. July 26, 1990, the OSC visited the Virgin Island Department of Planning and Katxiral Resources office in Christiansted and informed Mr. Leonard Reed of the emergency situation at VIChem. 3 ERCS mobilize to site in the late afternoon. The plan to stabilize the fuming drum, to inspect all other benzyl chloride drums, to obtain additional sample from drum #81, and to ship the benzyl chloride samples stored on-site is discussed. OSC informs ERCS that material transfer of benzyl chloride to poly drums will only be conducted if the drum is fuming because of drum deterioration. Generator vas started and all electric equipment functioned. However, only the single site telephone line was operational. Only 2-150# air cylinders, vhich will be needed to supply the ERCS airline, are full. C. July 27, 1990, no site telephone line is operational. Based on previous arrangements, OSC utilizes VIAG phone line with his EPA AT&T card. TAT purchases 2 floor fans, which will be used to ventilate the warehouse, and obtains a fax of benzyl chloride MSDS. ERCS enters Hot Zone in Level B Acid Splash Suits. ERCS loosens overpack lid of fuming drum #22, obtains additional 3 quarts of sample from drum #81, and informs OSC that drum #26, another benzyl chloride drum, is fuming lightly. ERCS packages samples for drum no. 81 and 3 quart samples of benzyl chloride. ERCS drops off 5- 150# air cylinders for recharge. After warehouse is, ventilated, ERCS reenters Hot Zone, removes overpack lids for all sixteen benzyl chloride, reinstalls missing bungs on drum nos. 22, 26 and 21, stabilizes these drums with lime, replaces overpack lids, and returns drums to pallets. OSC warehouse inspection indicates that the drums have been successfully stabilized. TAT arranges transport of samples via Four Star Transport to San Juan Airport (SJA) where the samples will be transferred to FedEx for shipment to the mainland. TATL Henne, who had conferred with TAT Zone management, instructs TAT member Bechtel that TAT cannot procure the customs broker services necessary at SJA, as this would constitute "personal services". Without success, OSC discusses matter with TATL Henne and reminds him of the two previous occasions in January and June, 1990 when TAT provided the same services being requested. OSC confers with Jennifer Johnson, who was standing in for the EPA TAT project officer, Karen Tomimatsu. After conferring with Sue Anderson, Ms. Johnson advised OSC to contact Ms. Tomimatsu on Monday. OSC responded that there was a need to settle this issue but that the problem at hand had to be resolved this afternoon. OSC instructed ERCS that they would have to provide for clearing sample packages through U.S. Customs in San Juan. D. July 28, 1990, ERCS picks up a7x3 delivers the 5 fully charged air cylinders to VIChem. OSC again inspects warehouse; inspection indicates that the drums have been successfully stabilized. EPA, TAT, and ERCS demob site. 301572 # E. July 31, 1990, OSC reviews and approves VIChem Invoice #6. F. August 1, 1990, OSC drafts request to the Regional Administrator for. exemption from the 12 month time limit and an increase to the total project ceiling. If approved this increase would establish a new total project ceiling of $1,950,000. G. August 2, 199 0, OSC and jJp€__R.otola, the OSC for the Virgin Island mini-removals, review the costs being charged by ChemWaste for the joint labpack disposal. Manpower costs are distributed based on the site entry logs whereas transportation and disposal costs are apportioned by the weight of labpacks at each site. Total costs to be charged to VIChem for ChemWaste services is $53,066.10. 3. FUTURE PLAJJS AND RECOMMENDATIONS; A. The OSC vill review the results of the dioxin data analyzed from the three five (5) gallon containers. B. TAT vill complete Phase II photodocumentation. C. TAT vill complete Phase II well sample analysis summary. D. Analab vill complete disposal analyses.' E. ERCS vill transmit analytical data to EPA and pirocure drum disposal services. F. Phase III will be planned and mobilized. 301573 4 . FINANCIAL ACCOUNTING A. CEILINGS TOTAL PROJECT MITIGATION EPA $1,840,000 $1,262,000 $200,000 B. UNOBLIGATED MITIGATION FUNDS REMAINING C. COSTS & BALANCES as of 6/23/90 DCN KE3042 KE3069 KE3073 KE3085 OBLIGATED AMOUNT- $250,000 500,000 250,000 262,000 EXPENDED AMOUNT $250,000 434,673 0 0 $1,262,000 Subtotal Other Costs TAT Sa1ary\Travel as of 7/6/9 0 EPA Salary\Travel as of 7/12/90 Estimate of Total: Expenditures to Date D. CEILING PERCENTAGES TOTAL PROJECT 45% PERCENTAGE OF $2 MILLION 41% MITIGATION 54% $684,673 80,880 62,387 $827,940, EPA 31% TAT $105,000 $0 BALANCE $0 65,327 250,000 262,000 $577,327 TAT> 77% FINAL POLREP FURTHER POLREPS F0RTHC0MING_2(_ SUBMITTED B DATE RELEASED John Higgins On-Scene Coordinator Response and Prevention Branch 301574 c cc r 2 4 I9-; m U . S . EN-VIRONMENTAL PROTECTION AGENCY POLLUTION REPORT Region II Response and Prevention Branch Edison, New Jersey 08837 (201) 548-8730- Commercial and FTS 2 4 Hour Emergency DATE: September 7, 1990 TO: C. Sidamon-Eristoff, EPA W. Muszynski, EPA R. Caspe, EPA R. Salkie, EPA J. Marshall, EPA E. Schaff, EPA G. Pavlou, EPA ERD, WH-548B (E-Mail) B. Sprague, EPA G. Zachos, EPA P. Gelabert, EPA A. Smith, VIDPNR LEPC TAT POLREP NO.: SITE NO.: POLLUTANT: CLASSIFICATION: SOURCE: LOCATION: AMOUNT: WATER BODY: 1. SITUATION; Twenty One (21) 4V Lab Chemicals, Alcohols, Solvents, Acids Major Virgin Island Chemical Company (VIChem) St. Croix, US Virgin Islands Approximately 566 Known Lab Chemicals, 590 Unknown Lab Chemicals, 210 Drums, -24 0 Empty Drums, and 22 Tanks. Including, Dioxin Containing. Materials Ground water, Caribbean Sea # Disposal arrangements underway for Phase III. 2. ACTION TAKEN; A. August 6, 1990, OSC reviews total waste analysis data for suspected dioxin-containing material. This material consists of two (2) five gallon containers of "Weedox". Total waste analysis data for this material indicate that 2,3,7,8 Tetrachlorodibenzo- dioxin (TCDD) was not detected but significant levels of Octo- chlorodibenzodioxin (OCDD) and Heptachlorodibenzodioxin (HpCDD) and furans were measured. OSC contacts Paul des Rosiers, Chair- man of the EPA Dioxin Disposal Advisory Group, regarding disposal options for the "Weedox" herbicide and OSC faxes Paul a copy of the Analytical Data Summary. 301575 -ej B ^ B. August 7, 1990, OSC revievs TAT costs with TATM Bechtel. TATM Bechtel informed OSC that certain TAT preliminary assessment- type costs vere planned to be be transferred from TAT's Removal Account for VIChem to TAT's Preliminary Assessment Account for VIChem. Accordingly, TAT has been furnishing cost figures vhich vere adjusted downward for POLREP purposes. Hovever, since the Technical Direction Document (TDD) for the VIChem Preliminary Assessment is closed out, there is no possibility of proceeding vith the planned transferral. Therefore, all future POLREPs, including this POLREP, will shov all current TAT costs charged to the VIChem Removal Action. C. August 10, 1990, Paul des Rosiers contacts OSC and informs OSC that because of the small quantity of the "Weedox" material and the absence of TCDD, he recozimends that the "Weedox" be applied on-site vith respiratory protection in accordance with manufacturer instructions. According to Paul's 8/13/90 memo to the OSC, such application "will result in the promotion of UV photolytic destruction of not only the active ingredients but the CDD's (dioxins) and CDF's (furans) as well." Furthermore, the alternative of removing and disposing of this material requires pretreatment to reduce the CDDs and the GDFs and there are no permitted facilities in the U.S. to accomplish this requirement. D. August 31, 1990, Regional Administrator approves Action Memo granting a time limit extension and increasing the total project ceiling to $1,950,000. E. September 4, 1990, ERCS informs OSC that all disposal analyses have been completed. OSC directs ERCS to solicit for drum disposal. F. September 7, 1990, OSC revievs ERCS draft, disposal solicitation letter. VIChem drum disposal will be coordinated with drum disposal for St. Croix mini-removals. Upon selection of disposal company, ERCS will prepare waste profiles for OSC review and approval. 3. FUTURE PLANS AND RECOMMENDATIONS; A. TAT will complete Phase II photodocumentation. B. TAT will complete Phase II well sample analysis summary. C. ERCS will procure disposal facilities for VIChem drummed waste. D. Phase III will be planned and mobilized. Project exigencies and EPA budget constraints indicate that Phase III mobilization will occur sometime after the latter half of October 1990. 301576 FINANCIAL ACCOUNTING A. CEILINGS TOTAL PROJECT MITIGATION EPA $1,950,000 $1,516,000 $200,000 B. UNOBLIGATED MITIGATION FUNDS REMAINING C. COSTS i BALANCES as of 7/25/90 DCN KE3042 KE3069 KE3073 KE3085 OBLIGATED AMOUNT $250,000 500,000 250,000 262,000 EXPENDED AMOUNT $250,000 500,000 10,489 0 $1,262,00,0 Subtotal Other Costs TAT Salary\Travel as of 8/31/90 EPA Salary\Travel as of 9/7/90 Estimate of Total Expenditures to Date D. CEILING PERCENTAGES TOTAL PROJECT 50% PERCENTAGE OF $2 MILLION 49% MITIGATION 50% $760,489 152,261 71,649 $984,399 EPA 36% TAT $195,000 $254,000 BALANCE $0 0 239,511 262,000 $501,511 TAT 78% FINAL POLREP FURTHER POLREPS FORTHCOMING_X SUBMITTED BY DATE RELEASED John Higgins On-Scene Coordinator Response and Prevention Branch 301577 U.S. ENVIRON-MENTAL PROTECTION AGENCY POLLUTION REPORT DATE: November 8, 199 0 Region II Response and Prevention Branch Edison, New Jersey 08837 (201) 548-8730 - Commercial and 24 Hour Emergency TO: FTS Sidamon-Eristoff, Muszynski, EPA Caspe, EPA Salkie, EPA Marshall, EPA Pavlou, EPA Schaaf, YiVhTyy ERD, WH-548B, (E-Mail) Sprague, EPA Zachos, EPA Gelabert, EPA Smith, VIDPNR VIDPNR C. W. R. R. J. G. I? B. G. P. A. EPA LEPC, TAT POLREP NO.: Site NO.; POLLUTANT: CLASSIFICATION; SOURCE: LOCATION: AMOUNT; WATER BODY; 1. SITUATION; (22) Twenty Two 4V . Lab Chemicals, Alcohols, Solvents, Acids Ma j or Virgin Island Chemical Company (VIChem) St. Croix, US Virgin Islands Approximately 566 Known Lab Chemicals, 590 Unknown Lab Chemicals, 24 0 Drums, 24 0 Empty Drums, and 22 Tanks. Ground vater, Caribbean Sea Disposal arrangements underway for Phase III. 2. ACTION TAKEN: A. September 21, 1990, OSC received copy of ERCS disposal solicitation letter with list of bidders. Since one of the bidders is an ERCS subsidiary company, OSC directed ERCS to instruct bidders to mail all bids to OSC to avoid the potential for ERCS conflict of interest. B. October 3, 1990, The videotape of the June 1990 detonations was distributed to: all local officials who participated in coordinating the detonation; the US Coast Guard in San Juan, vho observed the detonations; and Sherrel Henry, the RPM. 301578 C. October 5, 1990, OSC evaluation of disposal bids indicates that incineration of the 17 drums of benzyl chloride to be prohibitively expensive. Only one disposal company bid on the Benzyl chloride wastestream. ChemWaste Management bid $170,000. for transferal of material from drums to 1 gallon charges, and transportation and disposal of material; an alternate bid of $130,000. vas submitted by CWM for on-site treatment. OSC decides to explore recycling this material. D. October 9, 1990, Based on their overall low bid for transportation and disposal and their prior experience disposing of labpacked material in June 1990, OSC selects ChemWaste ManagejTient, Inc. (CWM) for disposal of drummed material. Hovever, OSC writes letter to CWH requesting a clarification of their bid, especially CWM proposed transportation costs ($426/drum). E. October 18, 1990, OSC completed a "Compendium of Well Water Data Collected at VIChem by EPA from 1986 to 1990." Over this period, there vere five separate sampling events at seven different locations. The data consistently indicated Chloroform contamination. The Compendium, complete vith a three dimensional color graphic plot, vas distributed to the RPM and VIDPNR and it vill be appended to the OSC Report. F. October 23, 1990, CWM letter reduced transportation costs to $3 3 0/drum vhich is acceptable to OSC. G. October 24, 1990, OSC met vith D & O Chemical company representatives and discussed their interest in accepting 17 drums of Benzyl chloride product. The meeting went well. The OSC examined company files, including DEA import forms and invoices for Benzyl chloride, and determined that the company is a legitimate concern actively engaged in importing and wholesaling Benzyl chloride. Transportation arrangements vere discussed and vill be finalized prior to Phase III mobilization. H. November 1, 1990, OSC presented a slide show of the detonations at the OSC National Conference held in Washington, D.C. The presentation was well received with avid interest displayed by OSC's in attendance. I. November 8, 1990, OSC hand delivers signed waste profiles for twenty-one wastestreams of drummed material at VIChem for submittal to CWM for approval. 3. FUTURE PLANS AND RECOMMENDATIONS OSC vill complete plans for removal and disposal of drummed material at VIChem. 301579 • i FINANCIAL ACCOUNTING A. CEILINGS TOTAL PROJECT MITIGATION EPA TAT $1,950,000 $1,516,000 $200,000 $195,000 B. UNOBLIGATED MITIGATION FUNDS REMAINING $254,000 C. COSTS & BALANCES as of 10/27/90 DCN OBLIGATED EXPENDED BALANCE AMOUNT AMOUNT KE3042 $250,000 $250,000 $0 KE3069 500,000 500,000 0 KE3073 250,000 69,000 181,000 KE3085 262,000 0 262,000 Subtotal $1,262,000 $819,000 $443,000 Other Costs TAT Salary\Travel as of 8/31/90 - 152,261 EPA Salary\Travel as of 11/3/90 77,650 Estimate of Total Expenditures to Date $1,048,-911 D. CEILING PERCENTAGES TOTAL PROJECT MITIGATION EPA TAT 54% 54% 39% 78% PERCENTAGE OF $2 MILLION 52% FURTHER POLREPS FINAL POLREP FORTHCOMING_J(_ SUBMITTED BY DATE John Higgins On-Scene Coordinator Response and Prevention Branch RELEASED /V J^^^-^^WyJ^^^-TS^/?^Q 3 0 1 5 8 0 - 4 \ U . S . ENVIRON-MENTAL PROTECTION AGENCY i j POLLUTION REPORT DATE: November 15, 19SO Region II TO: Response and Prevention Branch Edison, New Jersey 08837 (201) 548-8730 - Commercial and FTS 24 Hour EmBergency C. Sidamon-Eristoff, W. Muszynski, EPA R. Caspe, EPA R. Salkie, EPA J. Marshall, EPA G._ Pavlou, EPA tiE. schz^Bif yzpky ERD, WH-548B, (E-Mail) B. Sprague, EPA G. Zachos, EPA P. Gelabert, EPA A. Smith, VIDPNR LEPC, VIDPNR TAT EPA POLREP NO. ; Site NO.: POLLUTANT: CLASSIFICATION: SOURCE: LOCATION: AMOUNT: WATER BODY; Twenty Three (23) 4V Lab Chemicals, Alcohols, Solvents, Acids Major Virgin Island Chemical Company (VIChem) St. Croix, US Virgin Islands Approximately 566 Known Lab Chemicals, 590 Unknown Lab Chemicals, 240 Drums, 240 Empty Drums, and 22 Tanks. Ground vater, Caribbean Sea 1. SUMMARY OF VANDALISM INCIDENT: A. The VIChem Site demobilized on July 27, 1990. During the past three veeks, thieves made several break-ins at the Site. Equipment left on-site vas stolen and the trailers vere ransacked. The intruders broke into the drum storage room and tampered vith approximately 40 drums. The yellow poly-overpacks previously holding the drvims were stolen and removed from the Site. On Saturday November 10, 1990, Mr. Adalberto Bosque of the EPA Caribbean Field Office (CFO) and TATM's Bechtel and Mentzel arrived on the Site and assessed the extent of the situation. ERCS mobilized to the Site on Sunday November 11, 1990. A crew of ERCS and TAT righted the drums, placed fiber pack drums on pallets and spread lime inside the warehouse to neutralize spilled acid. The U.S. Attorney on St. Croix and local enforcement agencies are conducting a criminal investigation. 3 01581 2. SITUATION/BACKGROUND A. See Previous POLREP. B. The VIChem Site demobilized in July 1990 vhile EPA awaited approval to dispose of the approximately 240 drums remaining in the varehouse. During this demobilization ERCS and TAT left equipment and gear on-site to be used in the final phase of the removal. The decision to leave gear on-site vas made due to the high cost of shipment off and back on to the island. At the time the Site vas demobilized VIAG was preparing to operate an alcohol dewatering facility on the property. VIAG's owner maintained offices in the building on-site. 3. ACTIONS TAKEN A. On Friday, November 9, 1990, the VI Department of Planning and Natural Resources (DPNR) inspectors notified EPA a break-in had occurred at the VIChem Site. EPA/TAT immediately responded to the Site to conduct a preliminary investigation in order to ascertain the extent of damage. B. On Saturday, November 10, 1990, EPA/TAT arrived at the Site at 0800 hrs. Mr. Bosque informed OSC of the following observations made and recorded by EPA and TAT: 1. A new "Gateway" was cut into the fence surrounding the property. A well-worn pathway had been created in the vegetation. This path was obviously made by vehicular traffic over a period of time. 2. The EPA/TAT office trailer had been broken into and ransacked. Thieves stole any items which may have had any commercial value including chairs, coolers, fax machine, five telephones and other items. Expendable personal protective equipment was not removed. The intruders apparently entered through a broken window. 3. The ERCS equipment storage trailer and the decontamination trailer were broken into and ransacked. Some items stolen included tools, power tools, a washer and dryer, shovels, non- sparking drum tools, radios and other response gear. In addition, the four tires on the decon trailer were stolen. The ERCS pick-up truck vas stripped of tvo tires, the battery, mirrors, radiator, one door and the vindshield vas broken. 4. VIAG offices vere also ransacked. 301582 5. The drum storage area vas also broken into. The intruders removed the lids from approximately 42 yellov poly overpacks and tipped the contents onto the floor. Several drums were broken in this process. Twenty-seven fiber drums containing powders, including salicylic acid, were removed from overpacks in the front storage room. Fifteen poly drums containing liquids, including glacial acetic acid, sodium hydroxide and other corrosive material, were removed from overpacks in the back room. Liquid corrosive material vas observed on the backroom floor. Apparently, this spillage was the former contents from Drum # 159 that had contained a corrosive liquid but is now empty. This spillage was entirely contained within the varehouse. 6. Items vhich vere not stolen and are apparently in good condition are the 125 KW generator, the bobcat, the trailers themselves, four SCBA's and other gear. A full inventory is available. 7. On the top level of the distillation tower evidence was found that a vagrant had been sleeping on-site. A bed and food were found by EPA/TAT. After consulting with Mr. Angel Rodriguez', who is the EPA OSC on- scene at the Muriatti Site in Puerto Rico, OSC activates ERCS to respond to the Site and directs ERCS to utilize the Response Manager (RM) and two Response Technicians from the Muriatti Site. The local police were notified of the incident and dispatched an officer to the scene. The VI Police will drive by Site but are unable to provide full time security. C. On Sunday, November 11, 1990, DPNR visited the Site, agreed to coordinate efforts with EPA, assisted in the provision of security, and provided EPA with hand-held radios. DPNR informs EPA that yellow overpacks vere spotted at a St. Croix housing development, which is within one mile from the Site. Also, DPNR took the initiative on the subsequent criminal investigation. DPNR efforts in assisting EPA are exemplary. ERCS crew arrives on Site. At TAT directive, TATM Devine mobilized to site. D. On Monday, November 12, 1990, ERCS and TAT make a Level "B" Site entry and uprighted the overturned drxims. The trailers were cleaned and reorganized. At TAT directive, TATM Bergmueller mobilized to Site. E. On Tuesday, November 13, 1990, ERCS placed all fiber drums on pallets and spread six bags of lime around the drums to neutralize and stabilize the spilled material. A full inventory of all equipment remaining on site was made. Also, ERCS was directed to develop a list of stolen equipment and a list of equipment necessary to conduct future removal activities at the Site. 301583 VIDPNR Enforcement vent before the St. Croix Magistrate to obtain a seach warrant for the planned raid. When the Magistrate was infonr.ed of the nature of the vandalism he instructed VIDPNR to coordinate vith Federal Criminal Enforcement Agencies. VIDPNR contacted the U.S. Attorney on St. Croix and a meeting vas arranged. As discussed vith the OSC, Mr. Bosque contacted Mr. Jay Harrison of the FBI. Mr. Harrison explained that the FBI had only 2 agents in the USVI and they vere stationed in St. Thomas. He vould contact FBI Offices in Puerto Rico to see vhether they could participate in the investigation. Mr. Bosque met with the U.S. Attorney's Office on St. Croix, DPNR Enforcement, and the local police to discuss the criminal investigation and plans. A Strike Force raid is planned for Thursday, November 15, 1990. Besides vandalism at VIChem, the Strike Force is also concerned with illegal drug activity at the housing development. TATM's Mentzel and Bergmueller demobilized from Site. The fence surrounding the property was repaired. OSC and Mr. Bosque discussed situation with Mr. Gary Nurkin of ORC. ORC will contact Mr. Jim Peters of the U.S. Attorneys Office in St. Croix and is willing to advise OSC in the event OSC is requested to testify before a Grand Jury. OSC leaves messages at OEP, OCI and for Mr. Andy Prachak of the CFO. OSC contacted Mr. Southerland of VIAG at his home in St. Croix. Mr. Southerland informs OSC that vandalism has been ongoing for the past three weeks. OSC asked why he did not contact EPA directly, or through VIDPNR. • He replied that his files, including his personal telephone directory was ransacked and that he did not think to go through VIDPNR. He further stated that he encountered vandals at Site but he alleged that he did not receive strong police support. Police apprehended but released a vandal for no apparent good reason. He indicated to OSC that he was abandoning VIAG operations at VIChem. OSC contacted ChemWaste Management (CWM), the selected disposal company, for the purpose of expediting planned disposal activities by temporarily storing VIChem drummed material prior to approval from disposal facilities. He felt that this could be done, as early as the first week in December 1990, but that he would have to check with CWM Memphis facility. E. On Wednesday, November 14, 1990, TAT assisted the U.S. Attorney with preparation of the search warrant affidavit. Mr. Bosque, TATM's Bechtel and Devine, and 3 ERCS demobilize Site. 301584 Mr. Chris Miller of OCI contacted OSC. OCI will not get involved in the criminal investigation of vandalism at VIChem because OCI is responsible for pursuing "environmental" crimes. For example, if the warehouse spillage reached outside the building to the soil, OCI would then be involved. Mr. Andy Prachak, ORC Attorney at the CFO, contacted OSC and OSC updated him on status of criminal investigation. ERCS subcontracts for twenty-four hour security at the Site. F. On Thursday morning, November 15, 1990, a Strike Force raid lead by the VI Police was conducted and 8-10 yellow overpacks were recovered and the names of the thieves were learned. ERCS foreman assisted the raid, established 24 hour security at the Site, and demobilized. 4. FUTURE PLANS AND RECOMMENDATIONS; A. EPA will cooperate with the ongoing VI Police criminal investigation and any subsequent criminal prosecution. B. Drum removal is tentatively scheduled for December 1990. 301585 FINANCIAL ACCOUNTING A. CEILINGS TOTAL PROJECT MITIGATION EPA TAT $1,950,000 $1,516,000 $200,000 $195,000 B. UNOBLIGATED MITIGATION FUNDS REMAINING $254,000 C. COSTS & BALANCES as of 10/27/90 DCN OBLIGATED EXPENDED BALANCE AMOUNT AMOUNT KE3042 $250,000 $250,000 $0 KE3069 500,000 500,000 0 KE3073 250,000 69,000 181,000 KE3085 262,000 0 262,000 Subtotal $1,262,000 $819,000 $443,000 Other Costs TAT Salary\Travel as of 8/31/90 152,261 EPA Salary\Travel as of 11/3/90 ' 77,650 Estimate of Total Expenditures to Date $1,048,911 D. CEILING PERCENTAGES TOTAL PROJECT MITIGATION . EPA TAT 54% 54% 39% 78% PERCENTAGE OF $2 MILLION 52% FURTHER ^ — ^ POLREPS K \ D / I- FINAL POLREP FORTHCOMING_X_ SUBMITTED BY ^^^ [ o-KLw^ M ^ ^^''"'^-^ John Higgins On-Scene Coordinator Response and Prevention Branch DATE RELEASED K ^ Cr-Cr-c^-'tM^iS'k^/^^Q 301586 >\kyO U.S. ENVIRONMENTAL PROTECTION AGENCY FINAL POLUmON REPOR-y DATE: October 25, 1991 Region II Response and Prevention Branch Edison, New Jersey 08837 (201) 548-8730 - Commercial and FTS 2 4 Hour Emergency TO: c. Sidamon-Eristoff, EPA W. Muszynski, EPA K. Callahan, EPA R. Salkie, EPA J. Marshall, EPA G. Pavlou, EPA • E. Schaaf, EPA y^ C. Berns, EPA ERD, WH-548B, (E-Mail) - B. Sprague, EPA G. Zachos, EPA P. Gelabert, EPA A. Smith, VIDPNR Y. Canegata, VIDPNR TAT POLREP NO.: Site NO.: POLLUTANT: CLASSIFICATION; SOURCE: LOCATION: AMOUNT: WATER BODY: Thirty (30) 4V 'Lab Chemicals, Alcohols, Solvents, Acids Major Virgin Island Chemical Company (VIChem) St. Croix, US Virgin Islands Approximately 566 Known Lab Chemicals, 59 0 Unknown Lab Chemicals, 240 Drtuns, 24 0 Empty Drums, and 22 Tanks. Ground water, Caribbean Sea 1. SITUATION The final phase of site cleanup operations was completed in April 1991. This removal action, which was been pending the final disposal of all hazardous material, was completed on October 24, 1991. 2. ACTIONS TAKEN A. On April 26, 1991, Chem Waste Management (CWM) informed OSC that a tractor-trailer containing 21 drums from Wastestream / 5 (base neutral liquids) was involved in an accident while en route to CWM's Lake Charles facility. The accident occurred at 2 AM this morning when the truck jack-knifed and collided with an automobile. A pregnant female passenger in the automobile was taken to the hospital for observation and released the next day with no reported problems. No drum material was spilled, the drums were transferred to another trailer, and transported to the disposal facility later this morning. 301587 J i , y ^ -* y r ' /,. 4. FUTURE PLANS AND RECOMMENDATIONS; A. Complete review of upcoming 1900-55 forms and invoices. B. Completion of OSC Report in FY '92. C. Coordinate with ORC on enforcement case. D. The OSC will continue working on closing this project out. ERCS has requested reimbursement for-approximately $57,000. vorth of supplies and equipment that vere stolen or damaged during the November 1990 vandalism incident. A complete reviev of costs by the OSC, as requested by the Contract Officer, vill require that ERCS submit additional documentation. 5. KEY ISSUES In accordance vith the Action Memo and -the CERCLA Off-Site Compliance Policy, the following materials were disposed of at off- site facilities during clean-up activities: over 8,000 pounds of laboratory chemicals; 189 - 55 gallon drums of hazardous waste chemicals; 40 - 85 gallon drums of miscellaneous hazardous waste (i.e., drained batteries, contaminated PPE, and contaminated floor sweepings); and 240 crushed empty drums. Approximately 590 unknown laboratory containers were opened remotely on-site by rifle and the contents solidified into 3 - 5 5 gallon drums that were included in drvun disposal operations. The following materials were disposed of through ori-site/off-site treatment or recycle: 11 compressed gas cylinders and 70 pounds of shock-sensitive chemicals were detonated; 43 - 55 gallon drums of virgin product were recycled; and 2 five gallon containers of herbicide were sprayed on site. -^-^•;- The final draft of the .Site ::.Inspection report was submitted by FIT to EPA (ESD) on September *s4r^s=i^l9 91. The in-house FIT data validation for organic and inorganic data was completed but only the inorganic data^has received EPA final approval. Groundwater^, data r indicated-^chlorof orm Jcontjimination in ' thel^^^ ug/L) :and thie two downgradient public jwaterrrsupp^ Fairplains /9 (12ug/L) and Fairplains / 8" (12ug/L) ": The "onTsite. soil^andiisediment'? sample - data also "indicated, contaninatjion. The Pre-Remedial and Data Support Section will review the SI"i^report and determine whether a Hazard Racking Score package is warranted. « There are no hazardous laboratory or drummed materials remaining at the site. The possible remediation of suspected contamination of groundwater, soil, and sediment originating from VIChem will be considered under the National Priority List system for priortizing site remediation as required by S300.425 of the National Contingency Plan. 301588 «. DISPOSITION OF WASTES Wastestream* labpactt of Chen1cil« Kediua Solid t H o u t d Quantity 7990 pound* Treataent Tncfnentlon Disposal O * Tradg Wind Incliy.-atof Hgigrdous CylIndent Cai n evllrxfert Detonation AnqulUi l a n d f i l l . St. Crelx Shock-Serai tlve Otet*. SoUd I l i q u i d 7D pocnd* Detonation Anguilla I a n d f f U , St. Croix Uranyl Acetate Solid 100 grann »ecycl> Polysclence*, tne. Mercury Solid 1 pouid tecygU Polysciences, Ine. •Veedox* Herbicide Liquid 2/5 q. drum On-site Spraying VlCTea. St. Croix 1 - Organic liquid* l i q u i d U/55 g. drjM Tnclrieratlon Holllna, Deer Part, Tx. 2 - Organic liquids l i q u i d 13/55 g. drvjns Incineration t o l l l n s . Deer Park. Tx. Flan. Organic l l q . l i q u i d 19/35 g. druns Incineration Solllrta. Deer Park, Tx. t - Flaffl. Organic U q . liquid 11/55 9. druns Incineration B e l l l r a . Deer Park, Tx. ; - Base N e u t r i r U q . liquid 21/55 9. drtra Wastevtr treat. CUM lake Qiarles. l l . 6 - Base Keutral U q . l i q u i d 17/55 a. dnjns Incineration Kollins, Deer Park, Tx. 7 - Bate neutral Sol. Solid 21/55 fl. drum l a n d f i l l VM Ewelle. Ala. 7A- Base Meutral Sol. Solid 15/55 g. drvjns l a n d f i l l CiM Enelle. Ala. 8 - Acid l i q u i d * l l q j i d 15/55 fl.dnjra trclrSeratlon > o l t i n * i Deer Parkj Tx. 9 - Organic Solid* Solid 6/55 g. dram Incineration H o l l i r a , Deer Park, Tx. 9A- $*Hcyllc Acid Solid 27/55 S' drLiaa lecyclt: PtO Oienlcal/Pfltter O.eia. gnolewood.nj/ltidqefield.llj 10- Chlor. Org. U q . Uquid 1/55 g. drum Incl.-teratfon t o l t i n * . Deer Park, Tx. 11- f l a n . Org. U q . IIquid• 1/55 g;'dnjm Tnclneratlbn XolHraj Deer Part. Tx. 12- Base Meutral U q . l i q u i d 1/55 fl. drum Inclneritlen Rollln*, Deer Park, Tx. 13- Acid l i q u i d l i q u i d 1/55 flJ druM Iheirteriitioo 8oUtn«. Deer Park. Tx. 15- Tartaric Acid Solid 6/55 g. drum landfiU OM Eielle^ Ala. 17- HCHA Effoty Druig Solid 2tO dnim landfiU CW Epelie; Al*: 20- Benzyl Chlortd* Uquid 16/55 8- drum tecyclt DiO Oienic*l/Jame Fine Che«. Englewocd.WJ/Bound Brook.MJ OraIned Batterie* Solid 3/as flf.-drum l a n d f i l l CJM Eaeller Ala^ Battery Add Uquid 3/5 fl. drum Wastevtr. treat. CW ttodel City, WT line/Floor Sweeping* ''' Vol id'^ 7/85 fl. drum l a n d f i U OM E ^ t U . Ala. Protective Clothing Solid 29/85 fl. drum Incineration TVl. Sauqet. t l Protev-tive Clothing Solid l/tS g. drug* Incineration EM5C0. l i t t l e Bock, Ki Sanple Glasswar* Solid (/5 fl. drum Incineration EWSCO, little Bock, A» * Murfaert preceding certain MstettrcaMS identify those uattettrcaiw accordinQ to tK« bulking tchene. WS MM, wat a one drua wastettreaa the content* of which were spilled during v*r>dalt«a. WS i 16, 18, and 19 were Uastettream* for th* St. Croix 'Minl-Reneval** project that were bid and disposed of with VIChem waste but charged under the St. Creix •>tinl-»effovals* pre)ect. 301589 FINANCIAL ACCOUNTING A. CEILINGS TOTAL PROJECT MITIGATION EPA TAT $ 1 , 9 5 0 , 0 0 0 $ 1 , 5 1 6 , 0 0 0 $ 1 5 0 , 0 0 0 $ 2 4 5 , 0 0 0 B. CONTINGENCY COSTS $39,000 C. UNOBLIGATED MITIGATION FUNDS REMAINING $154,000 D. COSTS & BALANCES as of 7/30/91 DCN OBLIGATED EXPENDED BALANCE AMOUNT AMOUNT KE3042 $250,000 $250,000 $0 KE3069 500,000 500,000 0 KE3073 250,000 250,000 0 KE3085 262,000 262,000 0 KE0036 100,000 7,658 92,342 Subtotal $1,362,000 $1,269,658 $92,342 Other Costs TAT Salary\Travel as of 3/29/91 219,361 EPA Salary\Travel as of 10/25/91 147,250 Estimate of Total Expenditures to Date $1,63 6,269 E. CEILING PERCENTAGES TOTAL PROJECT MITIGATION EPA TAT 84% 84% 98% 90% PERCENTAGE OF $2 MILLION 82% 301590 The above accounting of expenditures is an estimate based on figures known to the OSC at the time this report was written. The OSC does not necessarily receive specific figures on final payments made to any contractor(s) . Other financial data which the OSC must rely upon may not be entirely up-to-date. The cost accounting provided in this report does not necessarily represent an exact monetary figure which the government may include in any claim for recovery. FINAL POLREP X FURTHER POLREPS FORTHCOMING SUBMITTED B A , ^ - > - ^ DATE RELEASED John Higgins, P.E. On-Scene Coordinator Response and Prevention Branch • 301591 virgin Island Chemical Cocpany Removal Investigation, St. Croix, U.S.V.l, * Site inspection conducted January 31, 1989 * AOO drums inventoried * ^00 lab reagents inventoried * 8 steel tanks vlth liquids ^ * 4 full tanks of ethanol * Sodium metal; Ethyl ether; Phosphorous pentoxide; Diisobutyl aluminum hydride pose serious threat * Dog kennel operating on site, ovner living on site * PRP actively using site * St. Croix prison } mile downwind * Air monitoring results on site equivalent to background 301592 From: Kichael Mentzel TAT-2 ^ A t Jeif Bechtel TAT-2 To: Doug Kodama OSC U.S. EPA Response and Prevention Branch Subject: Virgin Islands chemical Company (VI CHEM) Removal Evaluation and Site Investigation preliminary report. Data: 2/2/89 INTRODUCTION On Tuesday January 31, 1989 the U.S. EPA Response and Prevention Branch conducted a Removal Evaluation and Site Investigation at the Virgin "island Chemical Company (VI CHEM) site in St. Croix U.S. VI. This action is in reply to a request from George Pavlou, associate director Enforcement programs dated 1/23/89. PERSONNEL Doug Kodama ' (201) 906-6905 U.S.EPA RiP Branch " Edison N.J. Adalberto Bosque (809) 729-6915 U.S.EPA CFO Santurce PR Michael Mentzel (201) 225-6116 Jeff Bechtel Edison N.J. TAT-2 Arnaldo Martinez (809) 723-8A66 TAT-21 Santurce PR Francine Lang (809) 773-0565 Leonard Reed St. Croix VI Henry Thomas Greg Rhymer V.I. Department of Planning and Natural Resources (DPNR) 301593 A. LABORATORY Over ^ 0 containers of laboratory reagents and unknown liquid and solid Ejaterlal are located in this area. Room 22 is the main lab area. Room 18 is the lab storage area, Room 15 contains unmarked glassware and Room 11 contains only a few items. Some of the more nefarious items of note are as follows: 1. Sodium metal (2 boxes). Water reactive. 2. Ethyl Ether (6 cans). Potential explosive. 3. Diisobutyl aluminum hydride (4 lecture bottles). Spontaneously combusts in air. A. Potassium cyanide (2 bottles). Poisonous. Stored near acids, potential for release of hydrogen cyanide gas. 5. Phosphorous pentoxide (1 bottle). Reactive. 6. Two Flanmable storage cabinets containing various materials and unknowns. 7. Two office type storage cabinets. One cabinet has spilled toaterlal on the top shelf which has dripped downward to mix vith other chemicals. Many other chemicals exist in the laboratory,as well as many containers vith unknown materials. Refer to table I for a listing of the known chemicals. All the chemicals which had dates are at least five years old. B. DRUM STORAGE VAREHOUSE In the main warehouse (Room 3,A,5 and 6) are located approximately AOO drums, of these, 200 are green painted drums which have the words ETHYL ALCOHOL stenciled on the lid. The condition of the ethyl alcohol drums vary from fairly sound to extremely deteriorated. Some cf the drums consist of only a rusted shell vith gaping corroded holes. A rough estimate shovs that 100 are empty and 100 contain some type of material. This material may be some type of sludge. Other materials found are as follovs: 1. Laboratory unknowns (75 containers less than i gal.) 2. Methanol (5x 55 gal.) 3. Glacial acetic acid (I3x 55 gal) 4. Benzyl acetate (22x 55 gal.) 5. Toluene (lOx 55 gal.) 6. Antifreeze/glycol (19x 55 gal.) 7. Benzyl chloride (28x 55 gal.) 8. Salicilic acid (27 fiber drums) 9. Methyl isobutyl carbinol (12x 55 gal) 10. Sodium hydroxide (12x 55 gal.) 11. Bulging drum, unmarked (1) 12. Drums in vhich some type of reaction has taken place, lid popped off (2) 13. Many other drums vith contents as shown in table 2 IA. Drums of unknown material. 15. Paint (97x 5gal. 21x Igal.) 16. Cylinder chlorine (1 bad condition). Cylinder hydrogen chloride (1) A cistern is located in room 2. PVC pipe leads to a pumping system outside the building. One drum of sulfonic acid is broken and leaking it'contents. 301594 OUTSIDE CROUyBS An inspection of the reactor and centrifuge buildings revealed various production materials including lubricating oils; propane, oxygen and acetylene cylinders; filter media; ethanol; assorted paints and some sodium hexa-oeta phosphate. Some of the oil drums are leaking. Scattered around the facility are eight stainless steel tanks with quantities of unknown liquid varying from empty to three quarters full. A large storage tank is on site along with numerous pressure and reaction vessels. Fourteen large green storage tanks are also on-site. Ten are planned to be used in the alcohol dehydration project. Four of the ten are full of ethanol. The other six are empty. The remaining four not being used are empty and unsound. Mr. Southerland stated that- -sludge was removed from these tanks when his company began operation.. Mr Southerland is a partner in the alcohol dehydration project being undertaken by VIAG Fuels Inc.on the site. Mr Southerland was interviewed in order to gain information about present activities on site. VIAG uses some of the office space in the main building. 301595 i^ACHKEfJT A iland CbAfflioal SltO T^cationt gt Croix, U,8, y.I.. The Island cheaical eite is located on the Isl&nd's South side n*ar tha west end (Figure 1). The site is situated on route 66, approxiaately 0.5 miles due north of the Alexander Hamilton Airport. The site covers approximately 3 acres and is bordered to the north by an intermittent stream that originates on the- north side of the Island and discharge into the Caribbean eea. A number of r*«idenc«s are located as close as one-tenth of a mile from the site. In addition, several well fields are located in the vicinity of th* «ite. --- _ In connection with sale of assets of Island Chemical Cospany(ICC) to Virgin Island Chemical (VICC), in October, 1984, Enviro- Science^ Inc. (ESI) was retained to investigate the ICC site. The inve$tigat^onj:onducted-by^,ESI,,revealed that both'^ofithelpits^ andvth"e;rarea5:iroui*i3thl^ were contaminated with ' ToltJene' and Pyt'i<3iS« (^i-Snire 2). Following the discovery of the contaaination, ESI removed and/or treated soma of the contaminated material at the Site. Additional investigations are necessary, however, to evaluate the nature and extent of any remaining contamination" at the site and the threat, if any, posed by such contamination. ESI haa submitted a RI/PS work Plan to address the additional investigations that are necessary and EPA has coamented, ESI is now revising the Work Plan. Tha Votk.PlAn, however, does not address & possible renoval of cheaicals stored in a portion of the main building owned by vice. The Virgin Island Company is in the process of finalizing the sale of this &ain buildincf. On Koveaber $th EPA and DPKR conducted a sita inspection of the aain buildin^r* The aite inspection revealed that & portion of the building contains large amounts of stored cheaicals in bags and druaa. Some of the cheaicals includedi sodiua hydroxide, toluene, eulfaaic acid(granular), potassium sulphate and benzyl chloride. Many of the bags and druas have ruptured and have spilled all ever the floor. There are pools of liquids, and powders over various parts of the floor. There are druns with portions of their sides rusted; others ehowed danger signs, such aa bulging, pitting, and visible accuaulation on soae druns. w 301596 ISIA}JD CKtHTC^L S I T ^ gite History The 3.5-acre site is owned by Charles_JL_-^t-a£^ey^_.Iac. On Hay i, 1969 Steffey leased tha property to Houston Cheaical Industries, Ino. Houston Cheaical assigned the lease to-CSTlbe cEenica! Coapany Inc., (subsequently known as Pierrel Aaerica, Inc.) on March 20,1972. . " ^ — on June 30, 1978—Pierrel Aaerica assigned the ground lease to CoopexiiAboratoriefiTijiIne,^ On October 30, 1979'-'Cooper LaBoratories assigned^the-iease to its subsidary. Island Cheaical conpany(ICC). On Kovesber-1, 1979 Cooper Laboratories told^ll"" of the -Stock "Of ICC to the pr^deccessor of Berlex Laboratories, Inc. (Berlex). on Septeaber 14,1984, ICC sold its assets to virgin Island Cheaical Coapany (VICC). (See figure 1 for break down b"Jf~o^7neTiShlpy'i site Operations - ^ — o f t ^ : |Berl<exS«icquired:§th^^ At "^Ke^tiae of purchase "tHe facility was in a non-siperational aode. Prior to the acqfuisition of the leasehold by Cooper, it is believed that the prior owners were in the pharaaceutical area of the cheaical industry and used the site to manufacture phenacetin and ethoxyquin. Cooper produced quinidine; operations vas halted in the aid-1979. Be^ex •revaapMs'^''the facility and operate"d for about t^o of its four' years of ownership. The facility produced prinarily quinidine from quinine. Production vas discontinued vhen the aethologies used produced a aore expensive product than never aethods used elsewhere in the industry. Tho plant did not operate for aore than a year prior to purchase by VICC. gtt» lnY»=>tigat.lon Enviro-Sciences, Inc. (ESI) vas contracted by Berlex to conduct an enviromnental study of the ICC sitel Under the contractural agreeaent between Berlex and VICC, ESI was responsible for certifying that the site vas environaentally clean and free of cheaical contamination; if not, the site had to be reaediated. ESI initiated a sit* evaluation in Septeaber, 1984 and continued the investigation into October. Contaaination vas found at several locations and a prelininary cleanup plan was subaitted to EPA. 301597 -2- - - ISLAND CHKHICAL SITE • fq^ijqu-XlP AND PECO?-ygKDATTOy;<;: It is recoaaended that the TAT teaa evaluated the site to deterained if the site warrants a renoval action under CERCLA. In the interia, the following corrective actions should be iEpleaented: .Cheaicals in container that are leaking, rust&d etc., should be repackaged. Cheaicals should also be staged on a platfora so that water can not get to thea, E?A vill aail notice letters to PRP's to offer thea a chance to perfora a reaovai action, if the TAT teaa aaJces the detemination that one is necessary. In the interia, the site will be evaluated for possible inclusion on the NPL. All existing available data will be used for the HRS ocoring. 301598 CHEiMICAL NAME TABLE 1 Laboratory Reagent Inventory COMPANY QTY STATE 1,3-dinitroben2ene 1-butanol 1-chlorobutane 1-propanol 18-Crown-6 99% 2,2-oxydiethanol 2,6-dimethoxyben2oic acid99% 2,6-ditertiarybutyl p-cresol 2-hydroxyben2yl alcohol 99% 2-hydroxyethyl ether 2-methyl-1-butanol 99% 2-methylbutyl ajnine 3,3-diaethoxy benzidene 3-hydroxybenzoin acid 4-chlorobenzene sulfonamide 4-hydroxy 4methyl 2pentanone 4-hydroxyben2oic acid 4-methylbenzo phenone 97% 9-hydroxyflourene Acetic acid Acetone Acetonitrile Alkalinity C,D,E,G Aluminum Chloride Aluainum chloride Amaonium acetate Ammonium acetate Ammonium acetate purified Ammonium hydroxide Ammonium persulfate Ammonium persulfate Ammonium thiocyanate Amyl alcohol Arsenic trioxide Barium chloride Barium chloride Barium chloride Barium hydroxide Benzaldehyde Benzene Aldrich Chemical J.T.Baker Chemical MCB J.T.Baker Chemical Aldrich Chemical Kodak Aldrich Chemical Biesterfeld Aldrich Cheaical Aldrich Chemical Aldrich Chemical American Laboratorie Kodak Aldrich Cheaical Aldrich Cheaical Aldrich Chemical Aldrich Cheaical Aldrich Cheaical Aldrich Cheaical MCB Fisher Scientific Supelco Mogul Corporation Mallinckrodt Witco Chemical Fluka Aldrich Chemical Jarchem Industries Sargent Welch Scient J.T.Baker Cheaical J.T.Baker Chemical Fisher Scientific Mallinckrodt Fisher Scientific Drew Chemical Mallinckrodt Fisher Scientific • Fisher Scientific J'.T.Baker Chemical Tenneco Oil 100 500 4 500 25 1 25 500 25 1 10 15 100 100 100 500 50 50 g ml L al g xg g g g 3cg g g g g g g g g 2x25 g 2x5 4 lb L 1 box 4x2 1 500 1 2 250 500 2.5 •500 500 1 oz lb g kg Jcg g al kg g g pt 2xll3g 1 • 500 1 1 500 qt g lb lb al 2xlgal solid liquid liqaid liquid solid liquid solid solid liquid liquid liquid liquid solid solid solid liquid solid solid solid liquid liquid liquid liquid solid solid solid solid solid liquid solid solid liquid liquid solid liquid solid solid solid liquid liquid 301599 Benzhydrol Benzoic acid Benzoin Benzoin 98% Benzophenone Benzophenone Benzophenone Benzophenone 99+% Benzoyl chloride Benzyl acetate 99% Benzyl alcohol Benzyl benzoate Benzyl chloride Ben2yl chloride Benzyl cinnamate 98% Benzyl ether Benzy ltrietJiylammoniu=chl ori Bismuth subnitrate Bromine Bromophenol blue Brucine sulfate Buffer solution pH 10.00 Buffer solution pH 4.00 Buffer solution pH 7.00 CAO-3 BHT Calcium sulfate anhydrous Cello-Seal Chloride F Chlorodiphenyl aethane 98% Chloroform Chromotropic acid >Ta salt Cinnamaldehyde Citric acid anhydrous Citricacidtrisodiumdihydrate Cobalt chloride Color standard 4 Congo red Copper metal Cupric sulfate Cupric sulfate DPD #1,2,3 Reagents Dibenzo 18-Crown-6 98% Dibenzoyl tartaric acid Dichloroethane 99% Dichlorophenyl aethane 99% Dichlorotoluene 99% Diethylene glycol Diisobutyl aluminum hydride Diphenylmethane 99% Diphenylthiocarbazone Eosin Y Ether anhydrous Ethoxyguin Ethyl acetate Ethyl acetate Ethyl benzene Ethyl ether 99% Ferric ammonium sulfate Kodak Mobay Chemical Fluka Aldrich Chemical Aldrich Chemical K&S Chemical Upjohn Aldrich Chemical Mobay Chemical Aldrich Chemical Mallinckrodt Aldrich Chemical unknown Velsicol Aldrich Chemical Aldrich Chemical Aldrich Chemical MCB Fisher Scientific Fisher Scientific Fisher Scientific Fisher Chemical Fisher Scientific Fisher Chemical Sherwin Williams W.A.Hammond Drierite Fisher Scientific Mogul Corporation Aldrich Chemical Fisher Scientific Fisher Scientific un>:nown J.T.Baker Chemical Aldrich Cheaical Fisher Scientific unknown Fisher Scientific Fisher Scientific Fisher Scientific Mallinckrodt Taylor Chemical Aldrich Cheaical Knoll Fine Cheaicals Aldrich Chemical Aldrich Chemical Aldrich Chemical Fisher Scientific Texas Acres Aldrich Cheaical Fisher Scientific Aldrich Chemical Fisher Scientific unknown Aldrich Chemical MCB Dupont Fisher Scientific Fisher Scientific 100 1 2x1 g lb ka 4x50Gg 500 q 1 bag 500 50 1 100 1 100 4 500 100 1 25 1 113 5 1 500 500 500 . g g lb g pt g oz g g kg g lb g g oz ml Bl ml 1 bag 4x5 25 3 100 4 25 2x1 500 1 2x1 1 25 500 500 500 3x1 50 1 1 25 100 1 4 ( 500 25 25 4 4 5 < lb g oz g L g kg g 3cg lb oz g g g g oz g kg ^9 g g qt =yl g g g qt oz gal Sxlgal 1 qt 6x500g 500 g solid solid solid solid solid solid solid solid solid liquid liquid liqjid liqjid liquid solid liquid solid solid liquid solid solid liquid liquid liquid solid solid liquid liquid solid liquid ,. solid liquid solid solid solid liqaid solid solid solid solid liquid solid solid liquid solid solid liquid gas liquid solid solid liquid liquid liquid liquid liquid liqiud solid 301600 Ferric chloride Ferric chloride Ferric chloride anhydrous Ferric chloride anhydrous Ferrous ammoniua sulfate Formic acid Glacial acetic acid Hydrazine sulfate Hydrazine sulfate Hydrochloric acid Hydrochloric acid Hydroxylamine hydrochloride Hydroxylamine hydrochloride Iodine Iron chloride anhydrous Isoamyl alcohol Isobutyl alcohol Lead acetate Lead nitrate Lithium perchlorate Magnesium sulfate Medical oxygen Mercuric chloride Mercuric oxide Mesityl oxide Methanol Methenamine Methyl alcohol Methyl orange Methyl red Monochlorobenzene N-methylaniline Na salt of ME salicylate Niacin N.F. Nitric acid concentrated Nitrobenzene Non aqueous buffer soln. Nutrizyme Oil #3 Paraffin oil Paraformaldehyde Paraformaldehyde prills 91% Perchloric acid Phenol red Phenopthalein Phenylhydrazine. .. Phenylhydrazinehydrochloride Phosphorous pentoxide Piperazine Potassium bromide Potassium butoxide . Potassium chloride Potassium cyanate Potassium cyanide Potassium dichromate Potassium ferrocyanide Potassium hydroxide Potassium hydroxide unknown Fisher Chemical Pennwalt Corporation Kodak Fisher Chemical unknown Fisher Chemical Fisher Scientific Fisher Scientific MCB Fisher Chemical Fisher Scientific MCB Fisher Scientific BASF Fisher Scientific J.T.Baker Chemical MCB Fisher Scientific Aldrich Chemical Fisher Scientific MSA Fisher Scientific Fisher Scientific Aldrich Chemical Fisher Scientific Fisher Scientific Mallinckrodt Fisher Scientific Fisher Scientific- PPG Industries Kodak • Sattra Chemical Nepera Chemical J.T.Baker Chemical Fisher Scientific Beckman Instmments Merck Frich Oil Fisher Scientific MCB Celanese Cheaical MCB Fisher Scientific Fisher Scientific Fisher Scientific Fisher Scientific Fisher Scientific MCB Fisher Scientific Callexry Chemical Beckman Instruments Fisher Scientific Fisher Scientific Fisher Scientific Fisher Scientific Mallinckrodt Fisher Scientific 100 1 al lb 5x50Cg 500 1 200 5 4 100 2X6 3x1 1 4 500 500 500 500 1 100 500 500 g lb g lb 02 g lb L kg oz g g ml ml lb g g g 1 cyl 2xl00g 500 100 4 500 g g L g 1 gai 113 g 2x10 g 10 1 oz kg 1 bag 250 2X8 1 1 2 g lb qt pt oz 5 gal 1 1 1 2X8 5 1 4x4 2 1 100 qt qt lb lb g oz oz lb lb g 5x500g 50 2X6 1 500 500 3 2x1 500 g oz lb g g kg lb -^g_ 301601 liquid solid solid solid solid liquid liquid solid solid liquid liquid solid solid solid solid liquid liquid solid solid solid solid gas solid solid solid liquid solid liquid -solid liquid liquid solid solid - liquid liquid liquid solid liquid liquid liquid solid liquid solid solid liquid solid solid solid solid solid solid solid solid solid solid solid solid • potassium iodide Potassium iodide Potassium periodate Potassium platinate Potassium sulfate Potassium sulfate Potassium sulfate Potassium thiocyanate Resorcinol Salicylaldehyde 99-^% Salicylic acid Salicylic acid Salicylic acid sodium salt Sicapent Silica gel dessicant nitrate nitrate Chloride acetate acetate anhydrous acetate anhydrous amide benzoate benzoate benzoate benzoate Sodium borohydride Sodium carbonate carbonate anhydrous chlorate dichromate formate Sodium hydride Sodium hydroxide Sodium metal Sodium nitrite Sodium nitro ferricyanide Sodium sulfate Sodi\am tartrate Sodium tartrate Sodium thiosulfate Succinic anhydride Succinic anhydride Sulfamic acid Sulfanilic acid Sulfite 0,P,Q Sulfuric acid Tetraphenolboron sodium 99% Thiopene Total alkylinity indicator Tributyl borate Trichloroethylene Triethyl borate 97% Triethylenediamine Weedox C/R 250 herbicide Xylene Zinc chloride Zinc chloride anhydrous Silver Silver Sodium Sodium Sodium Sodium Sodium Sodium Sodium Sodium Sodium Sodium Sodium Sodium Sodium Drew Chemical Fisher Scientific Fisher Scientific Varlacold Chemical Indiana Army Ammo Plant Aldrich Chemical un3cnown Fisher Scientific Koppers Aldrich Chemical Aldrich Chemical Aceto Chemical Aldrich Chemical MCB Davison Chemical J.T.Baker Chemical Sargent Welch Scientific Fisher Scientific Sattra Chemical Niacet Corporation CDF Chimie Noth America Farchan Research T-ab Sattra Cheaical Dastech International Ishihara Corporation Pfizer Fisher Scientific Fisher Scientific Mallinckrodt Hooker Cheaical Fisher Scientific unknown Thiokol/Ventron Division Mallinckrodt RMI Fisher Scientific MCB Fisher Scientific J.T.Baker Cheaical Fisher Scientific Fisher Scientific MCB Aldrich Cheaical Fisher Scientific H&S Cheaical Mogul Corporation J.T.Baker Chemical Aldrich Cheaical Kodak Drew Cheaical Aldrich Cheaical Mallinckrodt Aldrich Chemical Air Products Southern Mill Creek Prod, Fisher Scientific Fisher Scientific Mineral Research i qt 2x500g 100 g 5 g 250 g 500 g 50 g 500 g 3 bags 100 g 100 g 500 g 100 g 2.8 L 2x1 qt 1 oz 30 g 500 g 3 bags 250 'g 2x500g 500 g 1 bag 1 bag 250 g 100 lb 4x25 g 1 kg 1 lb 1 box 10 kg - 5 lb 1 lb 500 g 2 boxs 2x500g 4 oz 500 g 2 oz 6xll3g 2x1 lb 6x250g 2x1 kg 500 g 1 bag 3x2 oz 10 lb 25 g 100 g 1 qt 750 g 1 pt 100 g 250 g . 2x5gal 5x1 L 500 g 1 lb 301602 liquid solid solid solid solid solid solid solid solid liquid solid solid solid solid solid solid solid solid solid solid solid solid solid solid solid solid solid solid solid solid solid solid solid solid solid solid solid solid solid solid "solid solid solid solid solid liquid liquid solid liquid liquid liquid liquid liquid solid liquid liquid solid solid p-chlorobenzene sulfonamide HiS Chemical 2 bacs <^oi -^ p-naptholbenzein Fisher Scientific 25 g l o U - p-toluenesulfonicmonohydrate Aldrich Chemical 500 q kkk pH indicator A Mogul Corporation 2 oz H L T - z Miscellaneous unknowns on site lab glassware 280bot miTk^ z Miscellaneous unknowns on site one oz bottles 238bot liq-ji-^- 301603 TABLE 2 Drum Inventory Chemical Name Company Qty State Acetone Acetylene Activated carbon All-veather patch material Amersite 2 Ashland MeOH -^Benzyl acetate Benzyl chloride Chlorine Chloroform Crofox Crystal Clear floor finish Degreaser Drewtrol 8500 Ethyl alcohol Filteraid Glacial acetic acid '^Glycol Humisorb Hydrochloric acid Hydrogen chloride Insulation (asbestos??) Insulation fiberglass Lubricating oil Lubricating oil Magnesium sulfate trihydrate Methanol Methanol Methyl isobutyl carbinol Methyl isobutyl ketone Micro aedia filter sheets Oxygen Oxygen Paints Paints Paints Paints Para-phenetidin Pentosin Potassium acetate Potassium sulfate Powdered filter media Propane Purafil II Quinine sulfate Rinseline injector fluid Ashland Chemical VI Gas Calgon Corporation Revere Chemical Valley Freight Syst. Ashland Chemical Island Chemical Velsicol Corporation VI Gas unknown Cerfact T-=^boratories Cerfact Laboratories unknown Valley Freight Syst. unknown un>cnown Celanese Chemical Island Cheaical Culligan Certified Laboratory VI Gas unknown unknown Texaco Texaco Tomita Pharmaceutica Ashland Chemical unknown Van Waters & Rogers Ashland Cheaical Ertel Engineering VI Gas Santa Maria Gases unknown unknown International Paint International Paint unknown Deutsche Pentosin Jarchea Industries un3cnown Ionics unknown unknown Kiaafarma Bob Chamber Ltd. 55 G 2 cyl 30 baa 55 G 55 G 5 G 21x550 28X55G 1 cyl 55 G 55 G 2x20 G 55 G 55 G 115x55 10X30G 13X55G 20X55G 30 G 55 G 1 cyl 13 box 7 box 2X10 G 5x55 G 6x25kg 5x55 G 3X55 G 12X55G 55 G 18 box 3 cyl 1 cyl 44x5 G 53x1 G 97x5 G 21x1 G 55 G 20 L 8xl00# 50 bag 2 boxs 4 cyl 15X10G 20 G 55 G liquid gas solid solid liquid liquid liquid gas liquid liquid liquid liquid liquid liquid solid liquid liquid solid liquid gas solid solid liquid liquid solid liquid liquid liquid liquid solid gas gas liquid liquid liquid liquid liquid liquid solid solid solid gas solid liquid liquid 301604 Rout Salicylic acid Salt Soda ash Sodium acetate anhydrous Sodium acetate anhydrous Sodium bicarbonate Sodium hexa-meta phosphate Sodium hydroxide Sodium hydroxide Spent toluene/acetone Sterling salt crystals Sulfamic acid Tartaric acid Thinner Thinner Toluene Toluene Triethylamine Waste oil z Empty drums 2 Miscellaneous unknowns Cerfact Laboratories Rhone-Poulenc unknown Allied Chemical unknown Jarchem Industries Stauffer Chemical FMC Mantek Manuel del Valle Inc unknown unknown Dupont Pfizer Chemical unknown Advance Ashland Chemical unknown Air Products unknown unknown on site containers 20 G 27drum 2x30 G 15x100 50 lb 200 lb 8x1001 200 lb 55 G 12X55G 2x55 G 50 lb 400 lb 15x100 6x1 55 3x55 5x55 55 2x55 130 25 G G G G G G solid solid solid solid solid solid solid solid liquid liquid liquid solid solid solid liquid 1 i qu i d liquid liquid liquid liquid n/a misc. 301605 S T . C R O I X ^=r:Z-. ,.''^--'-' - " • • • . : • . ' . • • : • • • . ' • • - . y ^ .liit-[,\\V^ )•• -/-.^hotjCrcS-i \ ^ ' y j \ u p f P t o t a y L J > - ^ ' y)\}pZy''-T-y^ v^ ^ AZ • -:.--••• ' z k - r, •'% ri>- -x-zz^^^r-; •^'"'' " • ^ ll • • ^ - . . i - '•" 'y .PZrK • \ \ y y - ' ' } ^ y . ^ k^. ^k-^'f^-iy A...-. - -z -- \y \A^Ayi"-\ \ m& \--:..zy^yy V yyk::?-z-yp A- 7j-'Ai^^'T'y''''.:MA\yfr. i--Z\^$ ''yzyyryA A'^-A ^vii-K {YV:^A^ZZA"' ' '>- • \ v IU-—<-•' • J r 1—r—^<-r ' — V : r—.—=——v \v-Oi ..•L^-- T'. ^ ' • • . ^ - u - g ^ ^ ^ ^ •l.v- \ l--< \'-'^^:r:z>-z-kZ zi=<y • ' . \ y k \ \ ' kk^^,:yj^h^' • - k z y y y kz^^ ' Izyz^^^'- ykhy- . —•jTsI v m^.>p^yy'^y<z •^kyirrsrifc;. y y y ^ : • rz ', \ - 1 : 'l-i-l t - ^ ^ ^ - \ y t:\.: •.•z:.\::-e; S ^ ^ . i -^^ .-\|\-./ ...•-• .!^y//yyk'k'^y'^y ! 'AAz¥/tPS fV*^-'i9:^i. V- 5- i . y' J ^ \ S ^ • ^pyz='k^ MkZA p;r^-'^}> A ) \ iV *]225——- ^;!1V \ «' I y-Ji y :".«• .•• V l T f— Al«un<3rr H i w * y.Kyi ^ i"^- SPIU. PRE^yENTION & EMERGENCY RESPONSE OMSlON rn.VNVociaum wiih ICTTcchnolo^ In<L.CCJonn»oo A.-ksvaciates. Inc_ Koourcr Applicsiions. |nc_ Coo/Rnouire Cunvulvints. Inc.. a n j tn^Tronrr^-nuJ Toxjcolo^ tnicmaiiooaJ. Inc. EPAPM KODAJi^A TAT PM MENTZEL FIGURE 1 SITE LOCATION VI CHEM SITE ST. CROIX US VI 301606 Pt.AllT tNTXANCt SPIU PRr/E>moN & EMEHGcNCY RESPONSE DIVISION EPAPM KODAMA F l G i n ^ 2 SITE DLACRA.M la Auociauon «>nLh ICF Tcchaotog}' lac_ C C Johnson tt Auociaio. l o c R o o u m Applk3tiona. I n c Cco/Koource Consulunu. Inc_ ind EnvironmcnLiJ Toxicolo^ (nterTuiionai. t n c TATPM KENT2EL VI CHEM SITE ST. CROIX DS VI 301607 .<: L o a d i n g D o t k :. A V . : . , COfvCRETE SURFACE ':' W s ; « h Q u ^ ^ : - > - . -5 26 25 23 Wt 20 Errr^ri'. -17 IS I Jt.,-:iy •I ^1 -"r 4 .r. ^i^kk i^.izz • 1 •DRUMS (MT) t7??77T(MT) ^ 3 ( M T ) ^ 3 ( 3 / 4 ) .'-fa% ^ ^ ^ -TANXS • =DRUMS •DRUM AREA LAB AREA =W0RX ARZA/NO CHEMICALS =0FFICE AREA (1/4) u L -'. l-+_.]_4-.J. •_^. — I - L_4-_L_i_i._. ...^_L 301608 # APPENDIX I PHOTOGRAPHS 301609 Photo #1. Virgin Island Cheaical Company Alcohol dehydration apparatus Photo #2. Dog kennel operating on site 301610 Photo #3. Maintenance building Photo til. View of tanks, nain building, and alcohol dehydration unit 301611 Photo /5. Main building office area 23 Photo /6. Area 22 lab in the main building 301612 Photo f l . Virgin Island Cheaical Company Sodiua metal in area 18 Photo #8. Area 18 chemical and glassvare storage 301613 Photo *9. Incompatable storage of lab reagents Pho to *10. Incompatable and leaking storage of lab reagents ,01614 Photo *11. Incompatable and leaking storage of•lab reagent- Photo ^i:. IncompacabU storage of lab reagents 301615 Photo #13. Paint cans in area 1 Photo till. Cylinder of chlorine :,;jo*HAtfj::ni 301616 « —<u»fcwO»r^.**^..i,-.o.^ —*i Photo #15. Drums in area i ; note water on the floor Photo #16. Drum contents undergoing a reactlc 301617 Photo #17. Virgin Island Chemical Coapany Drums and debris in area 5 Photo i l 8 . Drums in area 5 301618 Photo ='19. Deteriorating drums in area 6 Photo ^20. Drums and floor contamination in area 5 301619 Photo ?21. Deteriorating bags in area 6 Photo #22. Drums in area 6 301620 Appendix M Laboratory Results \WORKU4231\02\\VORKPLA.N.REP HAHDING LAWSON ASSOCIATES 301621 Laboratories Inc. Memorandum To From Date Subject J. Beck 2.V. McKennon Occober 15, 19Si ISL.-!uND OiEMICAI. iNVtKCNXEMT.^L SAMPLES Cn 9/17/8i, we received several samples frc= Ir-/ Coher. of ir.virc Scisr.cas Ir.: for analysis fcr various organic components. VTe agreed to exa=ir.e the samples for volacile organics via GC cech-irues , ar.d Chen for ncr.volscile organics like cuinidine using H?I.C I2chr.i:--ss . Cur invescigacicn is conplece, and data is attached. 3I5C'JS3I0N :. GC ANALYSIS Quantitable amounts of toluene were found in sanples T8-1 and ~ank-c. Also, quantitable aaouncs of pyridine were found in satrples D-1, D-2, and D-5. Qualitatively, the chromacograns were exaained for additional peaks. Samples S4-2, D-5, T8-1, and T8-2 contain an unknown peak eluting between the pyridine and toluene peak. Tank-8 had an unidentifiable peak which eluted shortly after toluene. II. HPLC Quantitable amounts of quinidine and/or quinine were found in 3-1, D-2, D-5, TS-1, Tank-8, Tank-4, and Tank-9. Qualitatively, the HPLC chromatograms in many cases have some unidentifi: early eluting peaks which are not related to quinidine, quinine, or any of the other cinchona alkaloids. DEPOSITION or SAMPLES On October 10, 1984, all samples were given to Al Kyles who is a representative of Enviro Sciences Inc. Note: Due to the extreme rush to analyze these samples, limited precautions were taken to protect either CC or LC columns. Total replacement cost for columns is approximately $960. M kr>^Yp D.W. McKennon DUM/hms Attachment Pyy.^.yyy^ R. Willis R. Wohl R. Milos I ^.Cohen/Enviro Sciences I 301622 c c . A.V.^YS-S* L.C. A-N-.V^YSIS-" S.O<?LE I2£:!T:?IC.^TICM 5i.-l S.i-2 S--2 S i - - S i - 5 u r f a c e D-1 D - : D-3 D-- D-3 TS-I T 8 - : Tank-S Tar.k-4 Tank-9 Tank-7 "Ji Sample r i - H i g h Cone. TOLLT-E N/D N/D N/D N/D N/D N/D N/D N/D N/D N/D 694 pcm N/D 13,880 ppm - - - - - PY-RIDINE N/D N/D N/D N/D N/D 920 ppn 507 ppn N/D N/D 3014 ppm N/D N/D N/D - - - - - QU-N-D::;E C1VC-N.J>— N/D N/D N/D N/D N/D 452 ppm 55 ppm N/D N/D 170 ppm 274 ppm 47 ppm 4050 ppm 8227 ppn N/D N/D N/D N/D QU:N:;;I N/D N/D N/D N/D N/D 82 ppr. N/D N/D N/D N/D 101 ppn N/D ' 1 5 2 1 ppn 2594 ppn 354 ppn N/D N/D N/D N/D • None Detected •G.C. Reference Bk. 83-9, pp. 75-79, EGO **L.C, Reference Bk. 83-11, pp. 22-30, MSM 301623 Pi.sr-/ J :v / Laboratories Inc. Me.mcrsncL: To: Cr. '•?. B. Caldwell cc: w. :,^- ?.. Vic: Frc.-n: G. ?.UC^ Ca:e; Cc-cber 19, 1534 Sutiec:: .---.alysis cf Scil Sajr.ples frcm Isl = .-.d Ch.a.T.ic3.1 by Headscacs-Gas .Cr_rcn:a-ccracr.v Three scil sa.T.plas received 10/15/84 frcn the Islar.d Charr.ical si^e v>'sra e.xami.-.ad by haadscaca gas chrcr-azc fcr the presence of toluer.s and =yridi.-.e. Tha rasulc ara listad in tha table belcw. Chrcrr.a-ccrar-.s cf tha three sa.Ticlas are attached. Ths larca caaks cbsarved ac tha becin.-.inc cf eac.n c.-.rc.tatccrachic run ar he heacscacs excer:.-.ent. Sa-=] Xoluana, :n K-22 I'A H-21 2-3 .1 <0.2 none cstactad- none datactsd "CO.2 lone del 1.2 CD Limit of dataction ca. 0.1 cpm Quantitation was performed by standard addition (Ippr.) tc the sair.ple and comparison to the unspi.ked saiiiple. Chromatocrachv Conditions A. Toluene Column: 6' x 2nra glass packed with 80/100 Carbocach C/ 0.1% SP-1000 Ta.T.ceraturss: Injector - 250°C Detactcr - 27S°C Oven - 1 min (§ 100"=C; 200°C 9 iS^C/rr.in Carrier: Nitrogen, 22 mi/min Detector: FID 3. Pvridine • Column: 4' x 2ra, glass packed with. 60/80 Carbopack 3 / 4% Csriowax 20M/0.8% XCH .-.•.-j:i,?^.r:CVi3i^'-" 301624 'srr.z s JTi CJJTSS ; C a r r i a r Oven :r - 250-C De: 120Cc i s c t h a r r r)7--^ 3--^C 5.0 grarr.s o f sa.rr.pla v e r a p l a c e d in a £0 ~ 1 serur. b c t - 1 ; was Healed with a Taflcn lined secf.:n".. Tha sealed ssr". beetle ccntaininc the sa—.pla was equilibrated, at 90^C : 1-1.E hours. With a previously heated gas tig cf the headspaca vcl'ur^a frcm tha serum bcttle a.-.d cuicklv i.-.-ect=d into tha cas chrcmatcrrac t syrtn was with : a , 0. •'.cMeal, T. a.-.d Hradar, C.V., J.i.OAC. 65, 1 = 4-137 (1982! Mctabcck Rafara.nc GI?,-1-143-145 '£j.M/^, ^i^:S G. I . Rude 301625 . c r i ; • t t u .ir.>,\ I' CO o cr\ to til I f j ^ I j INDUSTRIAL CORROSION MANAGEMENT INCORPORATED IIS? ROUli 10 RtNpOirH m*i KRSII 0)I69 701 M< OilO uji^i-ivaeteixic.,,. lat.oi-atoru IIE.HOSPACE U t ' l ' o i t O n i c : Ociol.i.-r 9, IDfi'i I.a I). < 3'if>2'i C o m p o u n d s d e t e c t e d i n p a r t e p e r m i l l i o n ( m i l i g r a m a / k i l o g r a m s )Ory Wgt.Bas S.VMPLE SOURCE; S.AMPLE n.ATE: ENVIRO SCIEMCES SAMPLE ID: | . n Hole #20 Sept. 18-19, 19811 T.AKE.X nV: A|,-,n_!..KY.!.£I AT I.AR DATE: 9/2 7./fill i'( ( ClILOROMEni.A.K'E BUOMOMETIIASE ^ niCIILOROniFLUORO.METIlANE. " • y Vl.WL CHLORIDE . / ^., . <r CHLOROETIIA.SIE y • METHVLE.XE CHLORIDE j Z> ^ACETONE. TKlCHLOROFLUOROMETH.A.Vi;. . 1,1-DICML0R0ETHYLE.\E 1,1-D1CHL0R0ETHA.\E ' • t-],2-DlCHL0R0ETHVLE\n.. LHLOROFOR.M T " ' FKEO.V 115 1 ,:-DJCllLOROETIIANE , l-BUTYL METHYL ETHER 1 . 1 .1-TRlCHLOROETIIA.VE. . . CARBO.V TETRACHLORIDE BROMODICHLOROMETHANE 1 ,2-DICIII.0HOI>R0PA.\E C-1 ,3-niCIII.OROPRnPENE t-l,5-niCIH.OROPK0PHSE TCE (TRICIILOROETIIYLENE). . niBRDMOCIILOIiOMETIlA.VE Hr.VIfNF Ill ISOPtiOPVL ETHER :-cin.oi(OETini\iNVL ETHER. HEX WE BROMOFORM 1.1,2,2-irir(AciH.ORnFTin\E pri: (11 ri(ACiii.ni(ot;TiiviL.\L) HEPT.VVE TOMIL.VE CIILOKOnn.XZE.VE •. iETIIVLBENlENE n. I 6^ F o r t h e a b o v e l i s t e d v o l a t i l e p o l l u t a n t s , n o t h i n g i l e t e c t e i l a t n.oi|i|.m5ens i i i v i t y l e v e l . X O t h e r p e a k s d e l e c t e . l . F l u o r e t h y n e '^ 0 . ' . 5 ; 2-me t h y I | , r o , . a . u . I 0 . 2 0 ; p o . u a n e O . O I ; ^ LT " Less t h a n , CT-fire;t(er tlian, \'I)»Noi d e t e c t e d , •'•NOrr: I'd-.. •, i l> I y from plastic; li.ii). INDUSTRIAL CORROSION MANAGEMENT INCORPORATED HEADSPACE I'L'port U n t e : Orioher 9, l9B'i l..il>. i 3'i62!, IIW ROUll 10 RttjDOlM NiM <(RSI(OrU) 701 M< 01)0 VOLATILE ORf.AMCS BY PIHUir A V Q I U P r.r/H.S Compounda d e t e c t e d i n p a r t e p e r m i l l i o n ( m i l i g r a m a / k i l o i j r a m s j O r y Ugt.Bas S.AMPLE SOURCE: ENVIRO SCIEMtES SAMPLE I D : j , i (, | | „ | e //h SAMPLE DATE: S e p t . 1 8 - 1 9 . 198'i TAk'E.V BY: AJan_L^Ky!e_r AT LAB OATE: 9 / 2 7 / 0 ' i U> o l-» a\ to -J CHLOROMETHANE BROMOMETHANE DICIILORODI FLUOROMETHANE, VINYL CHLORIDE CHLOROETHANE .. METHYLENE CHLORIDE ACETONE TRICHLOROFLUOROMETHANE.. 1,1-DICHLOROETHYLENE 1.1-DICHLOROETHANE I-1,2-DICHLOROETHYLENE.. CHLOROFOR.\| FREON 115 1,2-DICHLOROETHANE I-BUTYL METHYL ETHER 1,1,1-TRICHLOROETHANE... CARBON TETRACHLORIDE BROMODICHLOROMETHA.NE 1 ,2-l)ICIH.OIl6IM(ni'\\i; C- 1 ,5-DICIII.nROPROPENE t - l ,5-niClllOROPROPENE TCE (TRICIIKMIOETIIYLENE). . 0IBR0.M0CIIL0l;O^IETIIANE BENZENE. niISOPROPYL ETHER 2-CIII.OROEIIIVLVlNVL ETHER. HE VANE BROMOFOR.M , 1 , l , 2 , 2 - T r T R \ r i l l O R O E T I U V E . PCE (TETR.\flHOI!OElllYII;NE). HEPTANE TOLUENE CHI OROBENZENE ETHYLBENZENE X For t h e a b o v e l i s t e d v o l a t i l e p o l l u t a n t s , n o t l i i n g d e t e c t e d a t o . o i p p n e e n s i t i v i t y l e v e l . X O t h e r p e a k s d e t e c t e d . f l u o r e t h y n e - 0 . 3 8 ; 2 - m c l h y l p r o p . u . . . l 0 . 1 6 „ , . . „ . . . , iVMOTF- I ' o b b i l i l v f I o m p l a b i l e liiii). LT - L e s s t h a n , G T ' C i c i i i c r t h a n , ND'Not d e t e c t e d , ' " " ' t . Y I c . c r i . j t u ...;•.i,M'_: u . i t j r / u j a t z w o H o\ to 00 INDUSTRIAL CORROSION • MANAGEMENT INCORPORATED M7 ROUll 10 RtXPOirH NIM l(RS(< O'H) 701 ;>t>0)10 •'>^'t':r Uloi-atortj HEADSPACE R e p o r t D a t e : October 9, 190't I.ill), i 3(,6?,6 VOLATILE ORGANICS BY PHRGE ANIJiJjUP QC/MS Compounda d e t e c t e d i n p a r t a p e r m i l l i o n ( m i l i g r a m o / k i l o g r a m s ) O r y WQi.Baii S.AMPLE SOURCE: ENVIRO SCIENCES S A M P L E ID: 31 (i-|lole # 1 3 SAMPLE DATE: Sept. I8-I9. igBlt TAKEN BY. A)an_L;KyJej: AT LAB DATE: 9/2 7/0'! CHLOROMETHA.VE BROMOMETHANE DICHLORODlFLUOROMETHANE. VINVL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE TRICHLOROFLUOROMETHANE. . 1.1-DICHLOROETHYLENE 1 ,1-DICHLOROETIIANE l-l,2-DICHLOROETHYLENE.. CHLOROFOPv-M. FREON 115 1 . 2 - D I C I I l O R O E T I I A N E t-BUTVL METHYL ETHER 1 , 1 .1-TRICHLOROETHANE.. . CARBON TETRACHLORIDE BROMODICHLOROMETHANE 1 .2-niCIII.0R:iPRnP\VE c- 1 .S-DlCIHv'ROPIiOPENE t - l .5-DICIIIOROPROPLNE TCE (TRICIH.OROETHVIENE). . niBROMOCIILOP.OMETIIANE BENZENE DlISOPROPYL ETHER 2-CHLOROETHY IA INYL ETHER. IIEWNE BROMOFORM , 1 , 1 , 2 . 2 - I L I R \ r i H . O R O r : l l l \ N E , Pr.r (TLIKACIIIOROEIHVILNE), HEPTANE T O I D E N E CHLOROBENZENE ; , ETIIVLBENZENE _X For t h e above l i s t e d v o l a t i l e p o l l u t a n t s , n o t h i n g d e t e c t e d .n o . o i p p m s e n s i i i v i t y l e v e l . J O t h e r p e a k s d e t e c t e d , f i i . » r p i hynp ^ 0 , 3 1 ; 2 - i i i e t t i y l p r o p . i i i n l " - K ' LT » Less t h a n , r i T ' C i r c a i e r t h a n , NI)=Not d e t e c t e d . ••.NOTE: ('<)s:.ilily friiiii p I 0 s I I c Iwni INDUSTRIAL CORROSION MANAGEMENT INCORPORATED k Z k k ' ^ " •"•:--"-^ ^'"-^'Vt-istdUH^,. LtiLoratoi-tj HEADSPACE R<'|"><t H a t e : Octol.ur 9, l98'i Lal). t 3/,f,2-/ VOLATILE ORl'.ANICS BY PIIRrii; AND TIKP^ GG/.'llS Compounda d e t e c t e d in p a r t s per m i l l i o n (miligvtimo/kiloQrams)(*ry U.jt.Dd S.AMPLE SOURCE: ENVIRO SCIENCES SAMPLE ID: i, , Q „ „ | e 21 lis? ROUll 10 RtNDOtrit NIM KRSII D»&9 701 Sil 0)10 SAMPLE DATE: S e p t . 1 8 - 1 9 . 198'i TAKEN HY: A!c-.i>_L,u!<y.!£_r AT LAB HATE: 9 / 2 7 / B ' i ; 1 1 ! 1 1 I. !. 1 ••• 1 ! ! o ; H i (X\ I IO ! VO CHLOROMETHAN'E BROMO.\|ETHA.NE DICIILORODI FLUORO\IETIIANE, VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE TRICHLOROFLUOROMETHANE. . 1 ,1-DICHLOROETHYLENE 1,1-DICHLOROETILANE l l ,2-DICHLOROETIIYLE-;E. . CHLOROFORM FKEON 115 1.2-DICHLOROETHANE t-BUTVL METHVL ETHER 1 .1 ,1-TRlCHLOROETILANE. . . CARBO.N TETRACHLORIDE BRO.MOD I CHLOROMETHANE 1.2-i)iriii.oRopi(np\vE c-1 ,5-I)K:III.OROPI(OPI;NE t - 1 ,5-|l|CIII.OR0Plt0IM:KL TCE (TRlCHI.OROrillYl ENH). . DlRROMOrillOMO.MnTHANE BENZENE Ill ISOPROPYL ETHER 2-rillOROLIIIVI.V INVI. ETHER. HEXANE BRt^MOFOR.M 1 , 1 ,2,2-TEIR.\CIII.OROETllVNE p("L (Trik.vciii.oRnrriiviLNi.) IHPIVNE 101 DENE CIHOIKMU NZL\C •. ElllVI BENZENE . . 1 X For t h e above l i s t e d v o l a t i l e p o l l u t a n t s , n o t h i n g d e t e c l c ; ! a t n.olppni sens i t i vi i y l e v e l X O t h e r p e a k s i l e t e c i e d . fJ.iJ2L^L'*Yi}.?"_?:_"§J_?llI'l''l.yL_!'!;".'J'2"" ' " • ' ' ^ • /^-"i'-' hyl - ' ' ' " - l " ^ " ^ " • ^ ' ; Dyi:Lt!.lnu-_i?:-Q?-- - - - - IT • Less t h a n , r,T=C.i c i i i e r t h a n , Nl) = N(ii d c U L i c d . NOTE : ' r i . i . - j i ll I y f i d m p I .i s l i i; l>.i<). ^ c- ^/, /^V Ervs» « i xtaxsi srx. CHAIU OP CUSTODY .^ICORD 1» CC»»EU>J»0 RO.. CENVllXE. »6W JtJlSET 07SM I n s t a l l a t i o n : ZAt.cy Asj>s .Z^yc. S u r v e y No .'7<' Cfyiiafje^ yyyfayyy y7c»m,as Saaplera: (Signature) a. e ' rs CI CO 3 S t a t i o n L c c a c i o n I D a t e T l a e S a n p l e Type! a Leap . vjrao •..,.. Z. / S 2^ y r - y f Z y y r - X I y ' j / I y s /s y / ¥ ' J 2 / R e l i n q u i s h e d b y : ( S i g n . ) R e i m q u i s a e a b y : ( S i g n . ) R e c e i v e d b y : ( S i g n . ) Date l1\.-3.^ ( R e c e i v e d b y : ( S i g n . ) Date/Tiae Reiinquisned by: Ciiga.) .ved b y : ( S i g n . ) I D a t e / T i a « R e l l n q u l a h e d b y : ( S i g n . ) R e c ' d by L a b o r a c o r y f o r f i e l d a n a l y s i s ( S i g n . ) yz. D a t e / T i a e Dispatched by: (Sign.) Dace/Time lec^ f y i Laioracory yAvJAz^ D a t a / T l a e Method of S h i p m e n t : 301630 ^?M% YORX LABORATORIES DIVISION CERTIFIED REPORT TRANSMIHAL REPORT NUMBER . 30850-145 DATE ... Xcve.T.ber 12, 19 3 4 CL;SNT £.-.viro-3ciences , inc. 19 Cccela.".d ?.c3.d. Denville, New Jersey 0 7 8 3 4 ATTcNTlON Mr. Ijrr Cohen The above refefencec report is enclosed. Copies of this report and supporting cc:c will be relcinec in cu tiles in tne event ihey cre requir©a (cf future refecenca If there are any quesrions conceming tftis report, please do not hesitate to contact us. Any samples submitted to our Laboratory will be retained for a maximum of sixty (60) days from receipt ct tnis report, unless other oirangements are aesired. Naturally, as inthe pest, CLrslultwill be pleased to quote on any future recuirem.enrs you may hcve In ccditlon fo the service provicec we also offer the following: HazcnSous Waste Analyses Prccuc: Evaluoiion/R&O Wcrer and Wastewcrer Analyses Air end Process Gas Analyses • Incustnal Hygiene Surveys • Metallurgical Analyses • MIcrablological Analyses • Mess Spectrometry Services Robert Q. Bradley CA Vice President -.-iC. • tL'.c s:.->-v:e •r.,-r.c:''e • Mc.-coa Ccnracric^" 'Zt>.U,& • |2Qi) ;ii-.ii£a 301631 si ••loveniber 12 , 19S4 30350-145 E>rviRO-SCIENCES, INC. 19 Copeland Road Oer.ville , Ne^f Jersev 0733' Atte.':tion: Mr. Irv Cohen PU?.?OSS Nine (9) soil saaples were submitted to Yori Laboratories for deterrtinatlon of toluene and pyridine on a quantitative basis. Other compounds found in the samples were also Indentified and are reported on a seai-quantitative basis. The sait^ples •sere also analyzed for oil and grease. METHODOLOGIES The samples were analyzed for toluene using the dyna-mic headspace Gas Chromatograph/Mass Spectrometry method in accordance with Cher.ical Analysis of Sediments and Elutriate Testing, EP.\ 1979. A Tekmar Model LSC-3 Purge and Trap interfaced with an HP 5995C GC/MS/DS were used for the analysis. The samples were analyzed for pyridine and oil and grease in accordance with EPA/CZ-81-1 Procedures for Handling and Cheai- cal Analysis of Sediments and Water Samples, May 1981. An ii? 5995C GC/MS/DS was used for the pyridine analysis. RESULTS The results are listed in the following tables. Prepared by: Gail 0. Sprio Senior, Chemist snior. ^,nerais^; y Approved by: \ Z r L/.,-,I (J • \Au.u!i'<^~^ GDS/JCC/mz J.eiff|rey C. Curran ChiisfrX^Uetnist YWC. IMC • 2CQ Mojvcf Ti«npi>"r • iM-.-.oi.:.<- CO'-<-.t?ciicu O.V».'>a • • C m i^l-cai-i 301632 w TABLE 1 ENVIRO-SCIENCES, IVC. TOLOENB AND PYRIDINE RSSnr.T^ IdenlS^Lior, i.kkkkiy . P y : - i d i . e u g / k g r o s b l <1 ,000 <1 ,000 < 1 , 0 0 0 <1,000 13 ,000 2 6 , 0 0 0 4 3 , 0 0 0 < 1 , 0 0 0 < 1 , 0 0 0 20 Septic 20 A-2' 21 .\-2' 2 1 .^-4 ' 25 - 2' 2 7 - 2 ' 32 - 2' 35 - 4' 36 - 2' CAuger) 540 690 15 43 210 16 15 8 7 V^'C.-NC •2C:M:ii,t^-,>rz-..i:.!A..--r.t. r:.-r-..-..-::-..,:,^.. . , - „ , , ,,. ^..., 301633 ...^—... ^^ ^-, 1-7 TABLE 2 E^fVIRO-SCISNCSS. INC. Samole Identification Comoounds -ound ' ' ^ " " u ^ ' ^ e f 20 A - 2' methylene chloride chloroform benzene ethyl benze.".e Y'MC. INC • 2nO M.-«-»-r.^ T(yo,-;,i... >.;-.,.,-, .--y-f-ir "r.-.i-::e-^i'i •':-:-^t 2r-- iJ^ a ,400 20 S e p t i c (Auger) 1,1-methylene b i s - b e n z e n e a ,t^'j diphenyl methanone 64,000 methylene c h l o r i d e <5 chloroform 12 benzene <3 <5 <5 6S total xylenes 500 21 A - 2' methylene chloride <3 chloroform <5 trichloroethylece • <5 benzene <5 tetrachloroethylene <5 ethyl benzene 7 21 A - 4' methylene chloride <5 chloroform' <5 benzene <3 2 5 - 2 ' methylene choride <5 chloroform 5 benzene <5 27 - 2' methylene chloride <3 chloroform 19 benzene <5 3 2 - 2 ' methylene chloride <5 chloroform <5 1,1,1-trichloroethane <5 benzene <; 3 5 - 4 ' methylene chloride <5 chloroform 13 1,1,1-trlchloroethane 11 benzene <3 3 6 - 2 ' ..methylene chloride <5 chloroform <5 benzene <5 •Results are reported on a semi-<iuantitative basis. 0.3 2 .3 0 .9 2.4 3 .3 O.S 0.5 0.9' 2.2 2.S 0.4 1 .7 0.4 2.2 0.6 4.4 4.2 0 .8 0.3, 2.4 0.4: 1.6 1.4 0.2 301634 TASLH 3 E-WIRO-SCISNCES. INC. OIL A2TD GREASE RF<?rTT.T<; .->' Sa.T.ple Identification 20 Septic (Auger) 20 A - 2 ' 21 A - 2 ' 21 .4. - 4 ' 25 - 2 ' 27 - 2 ' 3 2 - 2 ' 3 5 - 4 ' 3S - 2 ' 0: 1.1 _mg And Grease /ks Cacm^ 241 555 1 ,500 27.3 89.S 137 50.6 39.5 ,: 965 301635 Si'i INDUSTRIAL CORROSION UANAGEMENT INCORPORATED |lilM)>i\i It &uaOllH.ll(lllJltUItlUI IOIW««IM CLIEHT: ICNVtHO SClKNfiK - ICC (HerlcM) NJDiP I c i l l l i e u uiiiiKiiitj LaLoraiury 10 l U l 16 s o n . SAMPLE REPORT DATE; .Inly T l , 19H5 LAB i _ i m } l SAMPLE ID: llrnjo j l n u 112 SAMPLE DATE: 6/7/85 SAMPLED BY; A. Kyluu VOLATILE ORGANICS BV PURGE AHO TRAP By CC •BTy/"tADSPACE AT LAB DATE: fi/m/flS CIILOROHETIIANE • BROMOMETHANE • VINVL CHLORIDE • CHLOROETHANE • METHYLENE CHLORIDE - - - ACETONE I.I-OICHLOROETHVLENE -- I,I-DICHLOROETHANE **-- t-l,2-DICHLOROETHYLENE CHLOROfORH 1,2-DICHLOROETHANE I-BUTYL METHYL ETHER -- I.I,1-TRICHLOROETHANE - CARBON TETRACHLORIDE -- BROMODICHLOROMETHANE -- 1.2-DICHLOROPfiOPAN£ --- Compounds detected In parts per tnllllon (ml 11 Igrams/k I lograms) dry weight basis. K ^,c-l,3-DICIIL0R0P«0PENE — X 'l-l,3-0ICIIL0R0PH0P£H£ ! X TCE (TRICIIIOROtTHVLENE) ) ],2l,n M l,l.2-TRICIILnK0£TIIAHE 6B 10 ^Compounds co-elute (could be either material). LT-Left Than, CT-Creater Than dwb-Dry Weight Basis. X-Not Detected 'DIBROHOCHLOROHETIIAHE BEN2ENE DIISOPROPYL ETHER 2-CHLOROETIIVLVINYL ETHER BROMOFORM 1,1,2,2-TETftACHLOROETHAHE PCE (TETRACIILOROETHYLEHE — TOLUENE - CHL0R0BEH7ENE _ ETHYLBENZENE - _ H-XYLENE _ « I O-XYLENE P-XYLENE — **Teiraliydrofuran ( Phosgene also elute at this point. Numerical results are calculated for I,l-Olchloroethane only. s.6nn For the above listed Volatile Pollutants, nothing detected at a sensitivity level o f : y Unknown peaks detected (retention t Imr,est Imated amount): Xyltinc-a IH; 11) iiiikiinwn liyilrociirlion pcwika raii[^£i;t; fron) 2 to 10 oK/klt- _ _ _ ____ . NOTE:Compound Identification Is based upon retention time matches with specific known standards. Confirmation of analysis using CC/MS Is required to positively Identify any materldl and/or amount detected. IKOUSTRI ApCOJJROS I mtiiCMT, YJ w:. yy ^ — - ^ — . _ _ \f<^ • y ! Z J I i INDUSTRIAL CCRHCSiCN MANAGE'/ZNT INCORFGF^TED •.i:: ^ouTi -.0. .^incc'.-i'v. .-icw :y:rf a7aa5 ::•. ;-i-:2;c CLiz:;t: ;:r.":?.o scrz^tcts. ';tc c_i_wp^r SCL'?.£Z: ICC CEEP-iZIC^ ??.C_'iCT y V.'ascava;ar Ljboritsr-/ 12 i-'l-:.li ilCPC'C SACZ; .^uiusr If. 19 = : LA3 ••/ ii2SS2 SAM?!.; I.;: Dr21.-. S.C<3L3: C A " : 6 / ' / 3 5 SA^Jir: 3Y: A. Kvlas soil. SA:-C?LE i.A3a?ACC5.v A:;AI.";:SZ£ .\r ' - ^ CACZ; -i/lS/ :5 :lcn Tf 3lacx S o i l : p ^ ' ^ - ^ a ; a ^ Ser.= 5.-.a Coluer.e :-vl:ar.::er.e £:hyl: .«-;-:vlar.e 0,?-Xvl=r.e 0. IC Q.ZS 0.22 0.2? Simple has "Toiue.ie l i k e " or soLvenc odor. 3..t. e.S'S ac 4Q !ns?/'<3 R . r . 3 0 . 2 1 _c 2 Sij/kg All rasulrs rapocrad ir. a5/'<.g. Ve cr.cr.k. /cu foe chis opporcunl;-/ co s-r.fe you. I: you have any quasctcr. p'.za.ss do r.oc hesicica co call. -\ l:^USZ^l.\L CC-L'.GSICN yjLNACiC-li:: L~/jng •cl. _.'"L.*ss Than Eduia. Tlcr.er.or Vice Presidenc 301637 . LAB NO. 42885 Pit duplicata (liquid) Priority Pollutants +40 (Process Pit) Saaples not analvzed because sample volume too stiai; 301638 • • • r i r m a i ' i a ^ ' ^ m INDUSTRIAL ^^^^ CORROSiON SA.MPLZ MANAGEMENT INCORPORATED [IJ2 RCUIE 10. RANOCCfH. NEW jERStT 073S9 r01-S34-0330 NJOE.' C e r t i f i e d Drinking Wac-r/ Wastewater Laboracory to ./litllo REPORT DATE: Julv 3 1 . n s s LAB H 42936 & 42887-rn>?ng- AA CLIENT:. iN-1 ?0 SCISNCIS SAMPLE SCURCE: SAMPLE DATE: 6/14/85 ICC (3erlax) SAMPLED BY: A.Xylea AT LAS DATE: PRIORITY POLLUTANT VOLATILE ORGANICS + ^0 by GC/MS + I 5 PEAKS 6/18/85 Paramecer Result Paramecer Resul : acrolein" acrylonitrile* benzene bromoform carbon tetrachloride chiorobenzene ch i orod ibrwTicmethane chlorethane - - - . 2-chloroethylvlnyl ether chloroforn dlchlorobrcmcmethane : 1 ,1-d!chlorcethane 1,2-dichlorcethane 1 ,1-dichloroethylene 220 1 ,2-dichloropropane 1 , 3-dichloropropy1ene ethylbenzene methyl bromide methyl chloride methylene chloride 1 ,1,2,2-tecrachloroethane - tetrachloroethylene toluene •. 1,2-trans-dichloroethylene 1,1,1-trichloroethane I,1,2-trichloroethane trichloroethylene vinyl chloride —•• Resulcs reported in mg/Vg (ppa), dry weight basis. LIS X 1,560 X •Detection Liait LT-Le5s than X=Not detected 100 Dom OTHER COMPOUNDS DETECTED APPROXIMATE CONCENTRATIONS 22 1430 l - c h l o r o - Z - s e t h y l benzene 40 benzyl a c e t a t e c h l o r o n e t h y l benzene INDUSTRIAL CORROSION MANAGEMENT, INC. ET/Jag Edwia^Tlchenss- Vice President V- A Pz> 301639 INDUSTRIAL CORROSION MANAGEMENT INCORPORATED 1152 MUTE 10. HlKOQl?^. NEW IIKTI 07U3 20Mi*Ji220 CL 1 EMT: E^n^ISO SCIENCE NJOE? C e r t , . e d O r i n k i n c W a t i r / UasLe-rtoter L a b o r a t o r y 10 . ? 1 H 1 1 S = .\^. REPORT DATE: July 3j. LAB I SOIL SAXPLZ L9S5 ^2386 & 42387 CCy.50SI~ SAMPLE SOURCE: ICC (Berlex) SAMPLE DATE:_iZiil2i___SAMPLED BY: A. Kvles .AT LAB DATF-- <./-'g/a- PESTICIDE S PCB EXTRACTABLES PRIORITY POLLUTANTS + 1*0 by GC/MS Pa rameter Result Aldrin LT 2- a-3HC - L7 2 b-BHC - — LT 2 d-3HC LT 2 g-SHC - - - — — LT 2 Chlordane LT 12 l»,U'-DOO — LT 3 '»,'*'-00E - LT 3 A,U'-ODT ----- - - LT 3 Dieldrin -' LT 3 Endosulfan I LT 3 Endosulfan II : LT 3 Endosulfan Sulfate ; LT 3 Endrin ; •• LT 3 Endrin Aldehyde LT 3 Heptachlor LT 3 Heptachlor Epoxide LT 3 Toxaphene LT 12 PC3-10'16 IT 45 PC3-1221 - LT 45 PC3-U32 - LT 45 PC3-12i*2 LT 45 PC3-12l4a — L-r (.tt, PC3-125^ - — LT 45 PC3-126Q - - t-T 45 All r e s u l t s a r e reported In sig/kg (ppm), dry veighc b a s i s . INDUSTRIAL CORROSION MGMT., INC, r H > » ^ ^ ^ ^ v r U fi.-Tvr:T / Edw i>^^ T i ch'TWior ^— It ET/jmg V i c e P r e s i d e n t /QZ^ L T - L e s s T h a n X=»Noc D e t e c t e d 301640 rp % I N D U S ' ^ . , A L Wastewater L CORROSION ^ 2 1 ^ ^ ^ „^^„,^ „^^^._ M A N A G E M E N T ^ ^ / 42386 & 42aa7-rn'.ioo<;TTT INCORPORATED r a i o r y iQ ^ 11,1 1 6 11S2 ROUIE 10. RANIXIPH. NEW JERSEY 07853 ai-5*l.03:0 C L I E H T ; r S V I R O SCIENCES ICC (Berlex) SAMPLE 50URC- SAMPLE DATE: 6/14/85 SAMPLED BY: A.Kyles .AT LAB DATE:. 6/13/3; BASE/NEUTRAL EXTRACTABLES PRIORITY POLLUTANTS + kQ by GC/MS + 15 PEAKS X Parameter Result acenephthene —•- acenaphthylene anthracene benzidine benzo(a)anthrac8nc benzo(a)pyrene 3,'f-benzof luoranthene benzo(ghi)pery1ene benzo(k)fluoranthene bls(2-chlQroethoxy)methane b i s ( 2 - c h I o r o e t h y l ) e t h e r ' b I s ( 2 - c h l o r o I s o p r o p y l ) e t h e r - b l s ( 2 - e t h y l h e x y t ) p h t h a l a t e '»-brotiwpheny1 phenyl ether butylbenzyl p h t h a l a t e 2-chloronaphthalene - - — - - - — - - *i-chlorophenyl phenyl ether chrysene. dlbenzo{a,h)anthracene 1 ,2-dIehlorobenzene 1,3-dlchlorobenzene 1 ,'»-d Ichlorobenzene — — - - - - - - '3 i3-dlchlorobenzidlne . Parameter diethyl phthalate dimethyl p h t h a l a t e di-n-butyl phthalate 2,'*-dlnl trotoluene • 2 , 6 - d i n i trotoluene d l - n - o c t y l p h t h a l a t e I,2-dlphenylhydrazine(as azobenzene)- fluoranthene fluorene — hexachlorobcnzf.ne hexachIorobuladiene hexachl orocycl open tad iene — --- hexachloroethane lndeno(l ,2,3-cd)pyrene i sophorone naphthalene nitrobenzene — N-n11rosodI methy I amine N-nltrosod i-n-propylamine N-nItrosod Iphenylamine ---- phenanthrene pyrene -- I ,2,'»-trlchlorobenzene - — --—. Resu' Y X •7 X r T X X X X _x_ None of the above listed Priority Pollutants detected at a sensitivity level of 450 mg/kg (ppa) dry weight basia. ** . IT-Less Than X=Not Detected **Large dilution necessary due gp high concentration of benzyl ace: APPROXIMATE CONCENTRATION OTHER COMPOUNDS DETECTED benzyl acetate - - / / • rg/Ci benzene methanol l , l ' - [ o x y b i s (taethylene) bis]benzene 170,000 15,000 4,000 Chloromethyl benzene diphenyl methanone — 9H-fluorene-9-one — - 4,400 -30,000 - 3,000 All results reported in mg/lcg (ppm), dry weight basis. ET/iT INDOSTSIAL CORROSION MGMT.,". 301641 iiWxr?K.-<=?' %f^- w o cr. to INDUSTRIAL pORROSION MANAGEMENT L'J N I INCORPORATEO iiii»aniii.itAMioi>H.|<Yiiuitnaiu4 UI-U^IIM NJDEP Certified Drinking Udlcr/Uautcwd. Laboratory 10 Il<tll6 son. SAMPLE REPORT DATF: -'"ly 31. ISQj LAB Jl A2afl6 & 42887 COHPOSTTE CLIEHT: -£HUliQ-SCltUCEa. SAMPLE SOURCE :__icc_XiluiiliixL SAMPLE DATE; fi/14/flS SAMPLED BY: k , Vy}.,^ AT LAB DATE: Jdl&JM. AGIO EXTRACTABLES PRIORITY POLLUTANTS + tiO bv CC/HS4 IQ PEAKS ACID EXTRACTABLES PRIORITY POLLUTANTS » 10 Peaks 2-chlorophenoi y 2-nltrophenol X phenol X 2,4,-dimethylphenol X 2,<«,-dlchlorophenol -- ' X pentachlorophenol X 2,Ji-dlnl trophenol X 'i.S-dlnltro-o-cresol x ^-nltrophenol X 2,'(,6-irlchlorophenol jj 'i-chloro-J methyl phenol X None of Che obove liaced Priority PoIlucanCa dececced a t a senlstlvlcy level of 450 mg/kg (ppni) dry weight baalu OTHER COMPOUNDS DETECTED APPROXIMATE CONCENTRATIONS No other I'lienollc compounda detected ac a senalclvlt] of 500 mg/ku (ppm) dry welghc baula. ** INDUSTRIAL CORROSION M A N A G E M E N T , INC. ** Large dilution neceBBary due Co high concencruclon of benzyl acecace. ET/Jmg LT-Lc$i Than X-Not Detected Edwl rt- T i cli<Jiior Edwl rt- T i cli<Jiior V i c e P r e s i d e n t iiixzni A% INDUSTRIAL CORROSION SOIL SA.MPLE HJDE? Certified Drinking Water Wastewater Laboratory 10 ^1^116 MANAGEMENT INCORPORATED Ii'i; ROUll m. RiNooiPH. NtW j{RsiTo;itfi9 M I U4UIT(I n IFNT; ENVTRO SCIENCES REPORT DATE: -LL^ LAB / 42886 & 42387 Co=oosits SAMPLE SCURCE: ICC (Berlex) SAMPLE OATE: 6/14/85 SAMPLED BY: A. Kvles AT LAB DATE:6/18/85 PRIORITY POLLUTANTS + 40 TOXIC POLLUTANTS: Metals, Cyanide and Total Phenols PARAMETER T o t a l Anti.TXiny Total Arsenic Total Beryl 1ium — Total Cadmium Total Chromium --- Total Copper Total Lead ------- Total Mercury Total Nickel Total Selenium Total Silver Tota I Tha I 1 ium -••- Total Zinc RESULT T T Iiq 40.0 LT 2^87 22.8 592 327 688 2.73 134 LT L.08 iT 7^48 LT 66.2 3.594 Total Cyanide Total Phenol - _L.44 _1,Q1 All results are reported in ag/Vg (ppm)', dry weight basis. We thank you for this opportunity to serve you. If you have any questions, pleose do not hesitate to call. Very truly yours, INDUSTRIAL CORROSION HGMT..INC. ^ A^^j<r<rry~\ i Zzy Edwin TicheivQr -T^-e^ / ET/jmq LT»Less Than X=Not Detected Vice President /0£) 301643 (A) O M INDUSTRIAL CORROSION MANAGEMENT INCORPORATED son. SAMPLE NJDEP Certified Drinking Udter/Udstcwdte Laburdtory ID / U l U iiwtouii It uiicaini.Ma.«U4f(iui MIU4«IM CLIENT: ENyiRO SOIKNCK ICC (Iterlcx) REPORT DATE:_ LAB / ^111112. SAMPLE ID: •Inly 31.19(15 J)ry(;r_ SAMPLE DATE; 6/14/05 SAMPLED BY: A. Kyleu VOLATILE ORGANICS BY PURGE AND TRAP By CC BTX/HEADSPACE AT LAB DATE: 6/m/H5 CHLOROMETHANE • BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE - — ACETONE 1,1-DICHLOROETHYLENE - 1,1-DICHLOROETHANE **— t-l,2-DICHLOROETHYIENE CHLOROFORM 1,2-DICHLOROETHANE t-BUTYL METHYL ETHER -- I.I,I-TRICHLOROETHANE - CARBON TETRACHLORIDE -- BROMODICHLOROMETHANE -- 1.2-DICHLOROPROPANE --- Compounds detected In parts per million (ml 11Igrams/kllograms) dry weight basis X 4.0 340 4.2 i^Compounds co-flut« (could ba cither material), LT-Less Than, CT-Creater Than dwb-Dry Weight Basis. X-Not Detected ^[C-I,3-DICIIL0R0PR0PENE 't-l,3-DICIIL0H0PR0PENE ^ TCE (TRICIIIOHOETHYLENE) ^,1,1,2-TRICIILOROETIIANE 'DIBROMOCHLOROMETHANE BENZENE DIISOPROPYL ETHER 2-CHLOROETIIYLVINYL ETHER BROMOFORM 1,1,2,2-TETRACHLOROETIIANE PCE (TETRACHLOROETHYLENE TOLUENE CHLOROBENZENE ETHYLBENZENE M-XYLENE - wO-XYLENE P-XYLENE **Tetrahydrofuran ( Phosgene also elute at this point. Numerical results are calculated for I,I-Dichloroethane only. X X 6.6 X X X X X 4,000 X 16.1 17.7 I S . I For tha above listed Volatile Pollutants, nothing detected at • sensitivity level of: 1 mn/Vn dml>. _Unknown peaks detected (retention timr,estimated amount): NOTE:Compound Identification It based upon retention time matches with sf>eclflc known stanJdrds. Confirmation of analysis using GC/HS Is. required to positively Identify any materldl and/or amount detected. illDIISTHIA!^ORflOSiON.»CMT,^|MC. t ! CHAIN 0? CUSTODY .RECORD It COPLAND TO.. DENVIUX WW JEPSTY 07834 I n s t a l l a t i o n : ICC (Eeriex) Survey No.: o. a nj C in. Station Location Saaplers: (Signature) Date Analysis Tine Sampl - J - e i y p e< u <-o3o . ij r a 0 G f^ i.1 • s o o 2 -J Drain Line y^?zi Toluene 6/5/85 Identify the contents cr t.ne black soil sanple.] / - La'ooratory Pit ' P 5 - ? ^ "b Pyridine 6/14/85 Laboracory Pit-duplicate ^ ^ VGA j / ; ^ li4 6/14/85 [* Tise liait may have expired, if so do not run.] ly-^tia-^ i Pic-duplicats (liquid) Priority Pollutantb 6/14/85 -kkJl V(5 iTi-;.^ combine and Pit-Int erf ace (liquid/sl'jdgejX j-^j, 6/14/85 Pit-sludge t4.s.9&~/ j priority dis-;s tsollutants 6/14/85 /P^A-c V v!/ Ona container has a vhite lump, segregate it and an lyze for ilne quinidine.] Dn •••er l y C y Mi- />^'-^f Toluene 6/14/85 Relinquished by: (Sign.) RecSlyed by: (Sign.) Relinquished by: (Sign.) yyy Received by: (Sign.) Date/Tiae Date/Time is.eiinquLsnea by : ( Sign. ) jRecaived by: (Sign.) Date/Ti Reiinqjiiatied by:/^Sign.) Rec'd by Laboratory for field analysis Dispatched by: (Sl/in.) r (Sign.) Date/Tiae y / Date/Tlm^[Rec'd for Laboratory by: D a t e / T i m ' M A l ^ Method of Shipaent: Express Air Freight kl/uyyA/- 301645 mm YCRX LABORATORIES DP/ISICN tg/r CERTIFIED REPORT TRANSMITTAL R=.=CRT NUMEg= : c g ; o - i i ? ; DAT •) = ' z - : - . CUENT Er.vircsciar.css^ Ir.c. 19 C = celar.c P.c^^ D e = v i i l e , NJ 07334 ATTcNTlCN Dr. A. Kyles Th.e cocve refe<-encsc raccn is enciosec. Ccpies cf T\'is reccn end succcrtng cere will t e rercinec: in cur !H*s in the even: ffiey cre recuireC fcr furure refefenca If there cre cny cuesricrti ccnceming this repcrt. piecse dc net hesitcre TO conrcc: us. Any scmoles suPmiKeQ tc Cur LcPcrcrcry will be rercined fcr c mcxin-.um cf sixr/ [iO] dcys from receipt of tni^r^iscrr, unless omer crrcngemenis cre cesirec. Ncojrcily, cs in the pcsT; o u ' srcff will t e piecsec to cucte cn cny fuu'e rec.uiremer:Ts ycu mcy neve. In ccciticfi ro the service provided, we else crfer ihe 'cilcwing: • Hc2c.-C3\:sWcsfeAnctyses . Prccuc: ?vciucticn/R&D • WcTerijrcv/csTewcTerAnclyses • Air one Ptccess Gcs Anclyses • indusrrct Hygiene Surveys • Mefcilur^jccl Analyses . Mlc-ocic^c9iccl Anciyses • Mess Sp^ctrcmeiTY Services w f y Tnjiy Y< Robert G-Brccley Vice President 301646 vrfT^=^--- ?s. S e o t e n b e r 25, 1985 30850-1195 E^^VIKOSCIiNCSS , rac. 19 Copeland Road D e n v i l l e , New J e r s e v 07834 Atte-'i-icn: Dr. A. K y l e s ?'r~.:=CSS .:^D RESULTS E i g h t (8) s o i l sa.T.ples were s u b m i t t a c t:c York L a b c r a t c r i e s f c r a n a l y s i s . The sarr.ples were c r e c a r s c £.~c. a.nalyzed i.-. acccrda.nca w i t h P r o c e d u r e s f c r Hancli.-.c and Cha.^.ical A n a l v s i s cf S a c i - = n t and >:ater Sa.T.clas, £ ? A / C r - 3 1 - 1 . ~ T.^.a r e s u l t s a r e recoct:ed in t h e follcwi.nc T a b l e s . P r s c a r e d by: Z J > x < k C ' P - C ^ D a n i e l r , otiz L a b o r a t o r y Manaeer Aoeroved bv: .y ^ u^^ •a^£.t-&v f C C u r r a n /cHZeP Che-itist DFO/JCC/md r.vC. INC. • 2C:Q •Mor.'Cft Tvrr.cike • Monroe. Connecrcut C^Aio • [IZZ) 261-^i-i53 • 301647 3 - • 5 T c l u CS» ^*—-nC!!<e.;Mca-ce.C; ^""^ncu:C^44a.(:„,,2,, 301648 ^&o P i t i - a o -Dii. i ^-VC. ;MC. . 20Z .«. ''ic.-.-ce > >*'.=--^e-.V,onroe.Ccn.ne^.„..,^^. 301649 CO o M a\ tn o U INDUSTRIAL CORROSiON MANAGEMEhTT INCORPORATED ti-.i HUM u kuica. lit al a M till n u t i«iui«iM HJOEP C c r i i / i t i i Drink ing Wdlur/Wdilcwdier Ldbordlory 10 ,?l'il 16 CLIENT: EKVIHO SCIENCES. I HP.. SAMPLE DATE: 7 / l / f l 5 ICC (IIEKI.EX) PliOlECT SAMPLED BY: E n v i r o S c i e n c e s REPORT DATE:_ IAD g iiriZtl SAMPLE I D ; \}£t^r_ .Aiiljii.sr IS,19H5 AT LAB DATE: 7 / l l / f l 5 VOLATILE ORGANICS BY PURGE AND TRAP GAS CtlROHATOGBAPllY/HEADSPACE Compounds detected in parts per m i l l i o n (ml IIIgrams/klloQrams) dry weight basis I .2-DICIILOROPROPAHE - CHLOROHETIIANE UnOMOMfTllANE VINYL CIILOHJDE - CHLOROETIIAHE - METHYLENE CHLORIDE r — ACETONE - »,I-DICHLOROETHYLENE . l.l-DICHLOROETHANE ** I-I,2-DICHLOROETHYLENE CHLOROFORM 1,2-DICHLOROETHANE t-BUTYL METHYL ETHER - I,I,1-TRICHLOROETHANE CARBON TETRACHLORIDE • BROHODICHLOROMETHANE '"'Compounds co-elute (could be either material). LT-Lest Than dwb-Dry Weight Basis. GT"Creater Than X-Hot Detected ^|C-l,3-0ICIII0K0PfinpfNE '|-I,3-0ICIIL0R0P«0PEN£ TCE (TRICIILOROETIIVLEME) ^,I,I,2-TRICHL0R0£TIIANE___ 'OIBROHOCHLOROHETIIAHE BEN2EHE 01ISOPROPYL ETHER -- 2-CIILOROETIiyLVINYL ETHER - BROMOFORH - 1,1,2,2-TETRACHLOROETIIANE - PCE ( TETRACHLOROETIIYLEHE)- TOLUENE - - -- CHLOROBENZENE ETHYLBENZENE -- . . . . K X X i . . . X ! X : X Jf i X ; X Q^J X **Tetraliydrofuran t, Phosgene also elute at this point. Numerical results are caluclated for 1,1-Dichloroethane only. For the above listed Volatile Pollutants, nothing detected at a sensitivity level of mg/kg dwb. Jf Unknown peaks detected ( r e t e n t i o n time, estimated amount) niiinuroiiii otlier liyilrociirlioii pcukii, 0.02 to Q.l iii|;/k); ^ v NOTE: Compound identification is based upon retention time matclies with specific known' standards. Confirmation of analysis using CC/MS is required to poslllvely INODSTHIAI. COHHOSIOH HGHT.. INC. Pflwiii TIclicnor, Vice PreiiileiK •- \ , '•• 1 ! 1 1 U) o H a\ tn H '•n INDUSTRIAL CORROSION MANAGEMEf/T INCORPORATED IDIKUII K lAaMkni M o i i U K I I I t i IOI 1114110 I NJDEP C e r i i f i e d Drinking Uuicr/Wuitcwuicr Laboratory ID n h \ 1 6 REPORT DATE: LAB I /.WS? Ain;ii.st l5.19flS CLIENT; ENVIRO SCIENCES, INC. - ICC (HEKI.EX) PIIO.IECT SAMPLE DATE: 7/1/85 SAMPLED BY: Enviro Sciences SAMPLE 10: Dryer VOLATILE ORGANICS BY PURGE ANO TRAP CAS CHROMATOGRAPHY / HEADSPACE AT LAB DATE; 7/11/fl^ Compounds detected In parts per million (milligrams/kilograms) dry weight basis CHLOROMETHANE j, BROMOMETHANE * VINYL CHLORIDE x CHLOROETHANE x METHYLENE CHLORIDE 7 X ACETONE - 2.0 l.l-DICHLOROETHYLENE - X 1,1-OICHLOROETHANE ** - X t-l,2-01CHLOfiOETHYLENE X CHLOROFORM X 1,2-OICIILOROPROPAHE ^,c-l,3-DICIIL0R0PnnPENE__. 't-l,3-DICIILOR0PR0PEH£"" TCE (TRICHLOROETHYLENE) ^, 1,1,2-TR I CIILORO£TilAHE_ 'DIBROHOCHLOROMETHANE 1,2-OICHLOROETHANE t-BUTYL METHYL ETHER ^ 1 .1,1-TRICHLOROETHANE CARBON TETRACHLORIDE BROMODICHLOROMETHANE • iiCompoundi c o - e l u t e (could be e i t h e r m a t e r i a l ) . LT-Less Than dwb-Dry Weight Basis. GT-Greater Than X-Not Detected BENZENE --- DIISOPROPYL ETHER 2-CHLOROETHYLVINYL ETHER -• BROMOFORM • 1,1,2,2-TETfiACIILOROETHANE • PCE ( TETRACHLOROETHYLENE)- TOLUENE - CHLOHOUENZENE -- ETHYLBENZENE " - L ^ **Tetrahydrofuran i Phosgene also elute at this point. Numerical results a r c caluclated for 1,1-Oichloroethane only. For the above listed Volatile Pollutants, nothing detected at a sensllivity level of Unknown peaks detected (retention time, estimated amount )_j/L.j)L£_i5_|]n;/liii mg/kg dwb. NOTE: Compound Identification Is based upon, retention time matches with specific known standards. Confirmation of analysis using CC/MS is required to poslllvely f j f identify any material t n d / o r amount detected. niDIISlHIAl. COHHOSIOH MGMT.. INC. fdwiii Tichenor, Vice President ^ iT;,-^"^ trfmomkic:a^X2STiC. 1 • COf^UkHO P O , DtKVTUl. NCW jePSFT OTSU CHAIN OF CUSTODY RECORD tM'l. yH- z^y^ ys-b •PS\ yy - I n s t a l l a t i o n : Vdcl J / P ^ / y k S u r v e y N o . : u •—* °- a • ra c VJ a S t a t i o n L o c a t i o n , —J L^^y'^-.-S, /<^^<'/---v- • * ^ "V* ' ^ 4 ^ V4 P t ^ e k r r r^ / 'PZyyy^t.yy, " y Z y ^ ' • - ^ ' y y . y y ^ • A'-U<z-r:y^ R e l i n q u i s h e d b y : ( S i g n . ) ^A.yyyf-y R e l i n q u i s n e d j ^ y : ( S i g n . ) R e i i n q u i a n e d b y : ( i j i g n . ) R e l l n q u l a h e d b y : ( S i g n . ) D i a p a t c h e d b y : ( S i g n . ) D a t e / T i m * S a a p l e r s : ( S i g n a t u r e ) C a t e T i a e i yyA^y y . - e c ^ ^ A/Z^ic<y /X^y '^Ju/y Ajkc-y 'r <• * 'r y r , -J- y , t*/t.y y Sample Type! wOBp . 1 k j c a o — T t - ; u « c O n LJ • c o o ^ / X Y V yt > R e c e i v e d b y : ( S i g n . ) R e c e i v e d / b y : ( S i g n . ) R e c e i v e d b y : ( S i g n . ) R e c ' d by L a b o r a t o r y f o r f i e l d a n a l y s i s | ( S i g n . ) 1 R e c ' d f o r L a b o r a t o r y | b y : / / / / / D a t e / T i a e '!>i!y r.-^ D a t e / T i a e r D a t e / T i a e D a t e / T i a e | D a t e / T i m e Method of S h l p ; n e n t : : y , / / 1 , ^ k S r ^ : / P ^ ^ ^ ^ ' ' ^ ^ 301652 YORK LABORATORJI5 DIVISION CERTIFIED REPORT TRANSMIHAL R£.=CRT NUMBEf^ ;C5:0-12S3 DATS Sa-- . a - •?= I o s : CLIENT AHSNTiCN ir.vir=scianc=s, l:ic. 19 Copelar.d Xcad Denville, JTJ 0783i. Dr. A. Kvlas, Th.e ccove referencec r%ccrT is enclosed. Ccpies ci tnis reccrr end succcrcng CCTC will be rercjnec in ourSlftS in ine event ttiey cre rec'jirec fcrfurure reference. If there cre cny quesT;of« ccnceming this repcn, pf'ecse Co nor hesitate to conTCcrus. Any samples submirteci ?c our Lcbcrctcr/ will be retcined fcr c rr.cximum cf sixr/ .;*Q) ccys from receipt of thu reccrr, unless other cn-cngerrienrs cre Pesirec. Ncturctly. cs in fhe pcst our srcff will be pleased tc cucte cn cny futu-e recuirerr.er.ts ycu may hcve. In ccc.licn to the service provicec we else offer the following: . Hc:c.-ccus Wcste Analyses • Product SvcluctiorvR&D • Water cr.d Wastewater Ana ly ses • Air cnQ Process Gas Anciyses • Industry! Hygiene Surveys -• Merclhjrgtcal Analyses • Mic-obiclcgiccI Analyses • Mess Screctrcmetry Services Vec^y Truly Youri RoceffQ.Brcaley / Vice President ' r.vc. :.NC. • : : : ;.ic.-.rc2 r<,^^:.;3 • ••vic.--=8. ccrr.ec-z-^: • ^ i ^ i • •;::;•; z=-\ 301653 Secteraber 25, 1985 30850-1233 ENVIROSCrSNCES, INC. 19 Ccceland Road De.nvllle, New Jersev 07334 At:te.-.ricn: Dr.-A. Kyi*s PUH2CSE AND R ; S " L T S Si.-c (o) scil sa.Ticlss were submitt^ed tc York Labcra-cries fcr analysis. Tbe sampi^S were cracared ar.d analvzed in acccrda.-.ce T.he results ara repQ^-l^c i.-i the follcvi.-c Tables. Pracared by: -,...li- ^ ^ L - ^ Daniel ?\ o t t Laboratory Mar.aaer 3^£rcey C, Curran DFC/JCC/md •mc. :.Mc. • : : ' Mc.-a*i« ru.T.=::^e-;vicnrca.conrect:=utC6'i45 -vz:;; :;t- 301654 TABLE 1 ^ ^ 30850-1283 ^ ^ ^ ^ S l ^ - I l e n t a i c ^ t i c T ^ 5434 - . , , , , , , ^ , ^ ^ ^ l 2 i H e n e . . _ u c ^ 5435 - c r y e r , 7 / 1 / 8 5 920 V^.VC.'.VC.ZCaMc.-ro^^-^ , CUtO<i^S.(3n,;-.,.^l^, 301655 TABLE 2 30850-1233 E^VIROSCIENCHS, T^C^ Sa-nriple I c e r . t l ' i c a t i c n 5436 - Lab ? i t , * 1 , 7 / 1 / 8 5 5437 - Lab P i t , # 2 , 7 / 1 / 8 5 5433 - Lab P i t , * 3 , 7 / 1 / 8 5 5439 - Lab P i t , # 4 , 7 / 1 / 8 5 ?yrici.-.e> ue/:<c 1 ,100 3,400 <150 <150 "Ave, INC. • 2CC .Mcrs<» niT-.piKS- Mcnrce. Cannecttcur06^*3 ••;2:21 :*-!~ii£5 301656 t. : I' i ? -J INDUSTRIAL CORROSION MANAGEMENT INCORPORATED iiilMuii lo.iUMoarH.wwjiiiSiroiii xnsimiKi IIJIlLI' C u l t i l i c i l U i i n k i i i y W d l L i V W j b l c W a l Ul L < i l i U i a l u i y ID l l \ ' i \ 16 REPORT OATE: l-AO * Vifi/Q Aiiniisr I 5 , j 9 n 5 CLIEHT; KNVIHO SClKNCi:.';, INC. SAMPLE DATE; 7/I7/»S \cc (iii:i<i.i:x) piio.ii'CT SAMPLED BY: Liiv/ro Scicncco SAMPLE ID: Orynr. AT LAB DATE: 7/25/(15 VOLATILE ORGANICS BY PURGE AMD TRAP GAS CHROMATOGRAPHY / HEADSPACE Compounds detected In parts per mill Ion (milligrams/kilograms) dry weight basis CIILOROHETIIANE BROMOMETHANE VINYL CHLORIDE - - CIILOROETIIAHE METHYLENE CHLORIDE - ACETONE I,1-DICHLOROETHYLENE I,I-DICHLOROETHANE ** - t-I,2-OICHLOROETHYLENE JL X AA.. Z& 1,2-OICIILOROPROPAHE X_ ^,c-l,3-DICIIL0R0PR0PEHE ' t - l ,3-DICIILOROPROPEME " — TCE (TRICIMOROETIIYLEHE) X_ ^,1,1,2-TRICHLOROETHANE 'OIBROMOCIILOROHETIIAHE — CHLOROFORM 1,2-DICIILOROETHANE t-BUTYL METHYL ETHER - 1,1,1-TBICHLOROETIIANE CARBON TETRACHLORIDE - • BROMODICHLOROMETHANE • '''Compounds co-elute (could be either material). LT-Less Than dwb-Dry Weight Basis. GT-Greater Than X-Not Detected BENZENE -- DIISOPROPYL ETHER 2-CIILOROETHYLVINYL ETHER - BROMOFORM • 1,1,2,2-TETRACIILOROETIIAHE • PCE ( TETRACHLOROETHYLENE)- TOLUENE CHLORODENZEHE - ETHYLBENZENE 0.07 0.36 **Tetraliydrofuran & Phosgene also elute at this point. Numerical results are caluclated for 1,1-Oichloroelhane only. For the above listed Volatile Pollutants, nothing detected at a sensitivity level of mg/l<g dwb. J^ Unknown peaks detected (retention time, estimated amount) niiinerniifi olilmr liytlrocarlion peaks 0.01 to 1 mp/k^ NOTE: Compound Identification Is based upon retention time matches with specific known standards. Confirmation of analysis using GC/MS Is required to positively CT/ identify any material ind/or amount detected. INDUSTRIAL CORROS|ONi HGHT., INC. yky o> ,w^ XJHtJOSTX. CaAI3 OF CUSIODY a2CQ2D ittssmyx aa.ooaamsi.tKm jBimrr Qtxtn I n a c a l l a t : -°°*- 2rk(L : ^ ^ Surv«7 H o . : Samplara: ( 3 i j n a t u r « ) a U3 Station Location / Data Tiaa j 2" Saapla Typa « (.osp. v>rao o « • e a o ^(i<6?f y !/S<yCyZ k Ag pyyy. y'S^^ / y P .^^f>Ka/.c J A^p^yyyy^) /<£>/»rf y ^ z< / y/ /., / yCyyrP^fii,) o ^ / -r /ZPy//e/ry Aal^cy/S^/S •7^p<Z} // y/ ><. ^ y^ycyyi 'y^ Aikaodz. Syy^ycy:^ yLoti,^ .^y y./y^ /ry.^/rs.y^/— yyar" /=r,f£yy*jo ^y^ryc yf/^-r^/i... rvyvyejy yy^.a <g^yy/et£ji. Z^tej^y^py^^ y9y7icuys~ RFiiaqui3h.e<i by: ( S i j a . ) Rayiicquished by: (Sign^/) R a x i n q u i a n a a by: ( 2 1 g 3 . ) Racalvad by: ( S i g n . ) Aecaivad by: (jSlgn. ) D a t a / X i a * D a c a / T i a a jlecalvaa by: ( S i g n . ) O a t a / I i s a Raiiaqulshad by: (Sign.) Rac'd by Laboratory for fiald analyaia (Sign.) D a t a / T i a a Dispacciiad b y : ( S i g n . ) Data/Tiaa Rac'd for Laboratory by: Data/Tia« Method of Shipaent: ckkyL/yA!!/ p2Py /k^/^Azk' 301658 INDUS,rllAL CORROSiON MANAGEMENT INCORPORATED NJC£.= C = . Cifisd Orinkl.ig -.Vare.-V" Wastewater Laboratory ID .^lljlo .: 6 - REPORT 0A7E:_ LA a .^ ^"^18 ••August: 15,1985 1152 aOUIE 10. .PANCCLrH. NC.V JE.^Srf 07863 :Q1-5E4-:320 CLIENT: Z:rr?.0 SCIHNCZS. IVC, SA.MPLE SOURCE: ICC r B E ? X r n ^-'-'-•'-Cl SA.V?LI ID: St.C.rni-r. SAMPLE DATE: - « H « I O W » - SAMPLED BY: Al K v l e s .AT LAB DA-r: 7/22/85 WA: PRIORITY POLLUTANT VOLATILE ORGANICS bv GC/HS Pa rane!:er acrolein* a c r y l o n i t r i l e ^ benzene brcrr.oform carbon t e t r s c h l o r i d e chlorobenzene ch 1 orod ibrcr.cmechane chlorethane • 2-chloroethy1Vinyl e t h e r - chloroform di ch lorcbrcp.cr^ethane 1 , 1-dichloroethane 1 , 2 - d i c h l o r o e t h a n e I , 1-d Ichloroethylene Result X O.Oi Parameter I,2-dichiorcpropane I,3-dichloropropy1ene ethylbenzene methyl brcrr.ide methyl chloride methylene chloride 1,1 ,2 , 2-tetrachloroethane - tetrachlcrcechyIene toluene 1 , 2 - t r a n s - d i c h l o r o e t h y l e n e I , 1 , 1 - t r i c h l o r o e t h a n e 1 , I , 2 - t r i c h l o r o e t h a n e tricTiloroethy lene — vinyl chloride Resulcs reporced in mg/l (ppm). Dececcion liaic 0.001 ag/1 (ppm), *Dececcion Llnit: 0.1 ag/l Rssult E T / j m g INDUSTRIAL CORROSION MGMT.,INC, Edwin T i c h e n o r V i c e P r e s i d e n t LT=Less Than • •X'^m: Dececced 301659 m . iiNuuoi...iAL CORROSiON MANAGEMENT INCORPORATED Laooratory 10 ,116 REPORT OATE: Augusc Ij.igS tv" LAB i . 4i41S 1152 SOUTH 10. S>NCOL?H. HtH JERSO 07863 201 534.0330 CLIEHT: -^r-r-'n ^r'^^vr^';. ivc. SAMPLE -SSL'SC;: ICCf 3E?J.-:t') St. Croi-t SAMPLE DATE: ••rV-"-- SAMPLED BY: Al Kvles AT LAB OATEu yyy^t^ty.^r'yy WATER PESTICIDE S PCS EXTRACTABLES PRIORITY POLLUTANTS bv GC/MS Parameter Result Aldrin LT 0.01 a-3HC - — — LT 0.01 b-3HC LT 0.01 d-3HC t l 0.01 g-3HC LT 0.01 Chlordane LT 0.02 !•,«•'-000 — LT 0.01 i4,t»' -DDE LT 0.01 '«,'«'-DOT - - LT 0.01 Dieldrin . LT 0.01 Endosulfan I LT 0.01 Endosulfan II . LT 0.01 Endosulfan Sulfate LT 0.01 Endrin LT 0.01 Endrin Aldehyde '• LT 0.01 Heptachlor • LT 0.01 Heptachlor Epoxide LT 0.01 Toxaphene ; LT 0.02 PC3-I016 — — - LT 0.01 PC3-1221 LT 0.01 PC3-1 232 LT 0.01 PC3-12'»2 LT 0.01 PC3-1248 LT 0.01 PCS-US'* — LT 0.01 PC3-1 260 r - LT 0.01 All r e s u l t s reported In mg/l (ppm). INDUSjaiAL CJliiOSI, Edv< in T i c h e n o r ET/jmg V i c e P r e s i d e n t LT=Le s s t h a n X=»Not d e t e c t e d 7/22/85 , INC, 301660 u> o INDUSTRIAL CORROSION UANAGEMENT INCORPORATEO ii>2*0Kifit.kutcoini.MmMuiinui M I M I O M HJULI' C c r t l l l c d Ul iiikliiij Wuicr/Ud^tcwjtcr Laboratory ID I l ' i l l 6 fiEPDRT OATE: Aii)!iiiit 15,1905 LAB H A A } 3 CLIENT: KNVIRO .SCIKNni'.S, I N C . , SAMPLE SOURCE^ SAMPLE DATE; Jinluuiuiv» ICO (ui:iii.i:x) |'KO.II;CT SAHI'I.K II): ST. <:ro(K SAMPLED BV; y^JZ'cyy^Jlr^ Al Kylea AT LAB DATE: l l l l l ^ ^ BASE/NEUTRAL Parameter • Result acenaphthene X acenaphthylene X anthracene X benzidine X benzo(a)anthracene X benzo(a)pyrene X J . ' i - b e n z o n u o r a n t h e n e X benzo(ghl)perylene ; X benzo(k)fluoranthene X b I s (2-chloroethoxy)methane X bls(2-chloroethyl)ether - X b l s ( 2 - c h l o r o l s o p r o p y l )etlier X bis(2-eihylhexyl)phthalate X ^-broniophenyl phenyl ether X butylbenzyl phthalate X 2-chloronaphthalene X 'i-chlorophenyl phenyl ether X chrysene X dlbenzo(a,h)anthracene X 1,2-dlchlorobenzene X 1,3-dlchlorobenzene X I ,'i-dlchlorobenzene X 3 , 3 - d l c h l o r o b e n z l d l n e X None nf tliu uliovu I ' r l o r l l y I'ol liiliiiit u ilutuctuil **Otlier compound!! see Aiiiieiuliini I LT"Less Than EXTRACTABLES PRIORITY POLLUTANTS bv GC/MS Parameter diethyl phthalate - i l l m d i i y l pill II.I I •Itu - dl-n-butyl phthalate — : 2,'i-dlni trotoluene - -- 2,6-dIni trotoluene di-n-octyl phthalate I,2-diphenylhydrazine (as azobenzene) fluoranthene fluorene hexachlorobenzene hexachlorobutadiene hexachlorocyclopentadiene hcxachloroeiliane indeno(1,2,3-cd)pyrcne Isophorone naphthalene n i trobenzene N-nltrosodlmethy I amine N-nlt rosodI-n-propylamine --• N-nltrosodiphenyI amIne phenanthrene pyrene "- I ,2,11-1 rich lorobenzene lit 11 ijuiiul C IV I ly level of 0.(11 inf,/I (|i|iiii) INDUSTRIAL CORROSION MANAGEMENT, INC. Result X F/)i.i in T i r hcnr^r :^i'i ^fJDE? Carcified Drlzxing Vacar/ Wascewacer Laboracory ID v l i l l a REPORT DATZ: August 15.1985 LAS 'i i'iiia a.i£>rr: ET.IRO SCIINCZS, I:^C. SAMPLE SOLUCE: SAJ^LE DATE: ICC (Berlex) SAXPLZ ID: Sc. Croi-x SA^CLZD 3Y: Al. Kvles .AT L.A3 DATZ: 7/22/S5 y 9 j Z * y y f / j — BASZ/NELTRAL ZXTRACTA3LZS PRIORirf PGLL'uTA-NTS ADDE>roL^. I 0~-:Z7. COMPOUNDS DETZCTZD by GC/MS ?3ra=ecer becxaldehyde chlcronechyl benzene benzene mechanol phenyl acecace diphenyl mechane Resulc 3. 0 24 26 0 0 0 3 0 0 u. .4 l-l'-ioxybis(mechylene]bts benzene All resulcs are reporced ia mg/l (ppm). We chank you for chis opporcunicy co serve you. If you have any quescions, please do noc hesicace co call. INDUSTRIAL CORROSION M.ANAGZMZNT, INC. ZT/jmg end. LT=Lass Than Edwin TicSenor Vice Presidenc 301662 r g . ic INDUSTRIAL CORROSION MANAGEMENT INCORPORATED NJOE? Certified Drinking Water/ Wastewater Laborator/ ID j i U l l o REPORT 0ATE:__Aji23i^ 1152 ROUIE 10. SAXOOU'M. .Sfi* IIRSVI 07869 201Si4-0130 LAB .¥ 4Adl8_ CLIE.NT: ENVIRO SCIZNCZS. INC. SAMPLE SCURCE ICC (3ZRLZZ) PROJZCT ST. Crol.T SAMPLE DATE: <-..'>...--TT SAMPLED BY: Al Kvles yPJ^ycyrpy/ ACID EXTRACTABLES PRIORITY POLLUTANTS bv GC/MS AT U B DATE :__:_JLillli5_ WATER Parameter 2-chlorcphenol 2-n i t rcche-iol • Resulc pnenol 2,'»-dir>ethyl phenol 2,4-dichlorophenol 2, l* ,6-tr ichlorophenol 7-- pentachlorophenol 2,'•-dini trophenol i*,6-dini t r o - o - c r e s o l i(-n i trophenol A-chloro-3 methy! phenol None of che above Prioricy Pollucancs dececced ac a sensicivicy level of 0.01 mg/l (>• OTHER PEJLKS DETECTED: benzoic acid (? 3 ag/l ET:jmg lT=»Less Than "X=»Not Detected NOUSTRIAL CORROSION M G M T . , INC Edwin Tichenor Vice President 301663 L-e INDUSTRIAL CORROSION MANAGEMENT INCORPORATED lis; ROUIt 10. BANCClPM. Nt)» JtflStr OJiifiJ ?01iJ4QlVI CLIEKT: Z:r'7IR0 SCIZNCZS INC. NJO£? C - j r t i f i e d Oriniiing Water U j s i e w a t e r L a b o r a t o r y 10 j ' l A l I S REPORT OATE: i , . „ . « - T •= l o a c ' " • • 11 'w . .. 1 ^ y - -r LAB / 44418 SAMPLE S C U R C E L SAMPLE DATE: ICC (3ZRLZX) PROJECT SAMgt-Z ID: Se. Croix riffsss:;:^ SAMPLED B Y : ^J- ^v^gg ypy^^y^rr ,Pt'X LAB DATE.- 7/22/35 PRIORITY POLLUTANTS WATER SAMPLE TOXIC POLLUTANTS: Metals, Cyanide and Total Phenols PARAMETER Tocal Anci.Ticny - Total Arsenic -- Tota1 Bery11ium Total Cadmium -- Total Chromium • Total Copper Total Lead :-• Total Mercury -- Total Nicitel — Total Selenium Tota1 SIIver -- Total Thai Iium Total Zinc Total Cyanide Total Phenol - RESULT r T LT LT TT 0, ft. ^ • 0 0 0 q n n n n n 4 0 0 v.i 005 013 003 027 n s on nm 0*^0 OITi nos O^q fi'i .053 •1$! All results are reported in ag/i (ppm). Ue thank you for this opportunity to serve you. If you have any questions, please do not hesitate to call. Very truly yours, INDUSTRIAL CORROSION MGMT.,INC. £T/jmq LT'Less Than X=Not Detected J.^ Edwin Tichenor Vice President 301664 C f trv»oMxaex3srKm CHAia OF CUSTODY RSCOID 11 coti-fcxa ao. oonnxL K » j w i cm* I n a t a l l a t i o n : 7~y*y Surv«7 Ho,: S*«pl«r«: (3ljn«tur«) k^^yk'yp^y^ l-l Scatlon Locatioa Data Tla« S a a p l * T7p« ^ o a p . -Ajca o o « o o I I I I <A/^ ypyyyyyy y^-yyyyrr^yj -r 9^0 Xyp/ekcy/kyyo k. \y yiy^^^ yZy^ A^k^ A R e l i n q u i s h e d b y : ( S i g n , ) Received by: ( S l j a . ) I D a t « / T i a « . l e i l n q u i s n e a b y : ( S i « n . ) T" R e l l n q u i a n e a by: ( S i g n . ) XZZI^.L.^J, 7./? i" _•>•(<- RecBlvea by: J S i g n , ) D a c e / T i a e Relinquiahad by: (Sign,) Recelvea by: (Sign.) Date/Tiae Rec'd by Laboratory for field analysis (Sign.) D a t e / T i a e D i a p a t c h e d b y : ( S i g n , ) D a t e / T i a e Rec'd for L a b o r a t o r y i D a t e / T i a e by: r -Method of S h i p m e n t : ^ . . yP<y • ckyci^.^^ '/^^y 301665 ..ii:2^:i^-jiy:.Z^?i'^-r'a^'Ti.-%i to o bil LU INDUSTRIAL CORROSION MANAGEMENT INCORPORATED llimOUK 10. KlNOCiPllHfWJEIISK 0)111 lOIMIOlM II.)DI:P C o r i i f i u i l DiiiiKJiKj l/al er/V/ds lewaier Laboriiiory ID ; I 'il 16 REPORT DATE: ^i;i!LL'!!!L'!;l_L2JOQl. I-AI) ; /.VlfiZ CLIENT: l-NVTKO SOTF.NCI- - ICC lll'HI.KX I'liaiKCT SAMPLE DATE: August 7, 1985 SAMPLED BY: K i w i r o SCUMICH SAMI'I r ID: i.,ii, I'll ri'lf.S AT IAD DATE: Aii);ii.sr 9. I'IflS CHLOROMETHANE BROMOMETHANE VINYLCHI.ORIDE i CHLOROETHANE --- HETHYLENE CHLORIDE --- ACETONE I, I-DICHLOROETHYLENE - 1,1-DICHLOROETHANE ** t-l,2-DICIIL0R0ETHYLENE CHLOROFORM 1,2-DICIILOROETIIANE t-BUTYL METHYL ETHER - I,1,1-TRICHLOROETHANE • CARBON TETRACHLORIDE -• BROMODICHLOROMETHANE -• VOLATILE ORGANICS BY PURGE AND TRAP GAS CHROMATOGKAPHY/ HEADSPACE Compounds detected In parts per million (mi I 11 grams/k i logrdiiis) dry weight basis ^ - - - X 0.32 1,2-DICIU-OROPROPANE c-1 ,3-DICIIIOROPROPFIIE t - l ,3-DICIIIOHOI'KOI'rHi;'"' TCE (TRICIILOROETIIYLCIIE) 1,1 ,2-TRICIILOROETIIAIIE 0.02 0.02 'DIBROMOCHLOROMETHANE BENZENE DIISOPROPYL ETHER -- 2-CIILOROETIIYLVINYL ETHER - BROMOFORM 1,1 ,2.2-TETRACIILOROETIIANE - f>CE ( TETRACIILOROETIIYI.ENE)- TOLUENE - - - CIILOROIIENZrilE ETIIYLDENZEIJt - X X X X X JA X X X n. X 0. M ni "Compounds c o - e l u t e ( c o u l d be e i t h e r m a t e r i a l ) . LT=Less Than dwb=Dry Weight Basis. GT=Greater Than X=Not Detected ••'••^Tel rahydrofiiran C Phosgene also e l u t e at t h i s p o i n t . Numerical r e s u l t s are c a l u c l a t e d for 1,1-Dichloroethane o n l y . For the above l i s t e d V o l a t i l e P o l l u t a n t s , nothing detected at a s e n s i t i v i t y level of 0,01 mg/kg dwb. j { Unknown peaks detected ( r e t e n t i o n time, estimated amount) Xylem.'s .iiipriix.O^Ofj nm/kiidwb NOTE: Compound I d e n t i f i c a t i o n Is based upon r e t e n t i o n lime matches w i t h s p e c i f i c known standards. Confi unaiion of a n a l y s i s u s i n g GC/MS is required to ( l o s i l i v e l y i d e n t i f y any m a t e r i a l anil/cir ainnunt detected. INI)|I;;TI!I/\I. COKKOSION HANAOI-MKNT, INC. izi^j/(fpL-^.c 'l. i c l l . l 1 .1 . / I.U'V i'liI: /I'l'l.'S i I I L M I £ U) o M ;fe'i'i INDUSTRIAL CORROSION MANAGEMENT JNCORPORATED I I S K I k l K i j M'CHOIKPIi.linkJIIISEt 01161 20ISK41JU CLIENT: NJDEP Cell i i i n l Diiiil.iiiy V/aier/V/as I ev;u l e r l.abcir.iioiy ID ; 1 'il 16 REPORT DATE: Si'pfiMnlu-r I2.19fl5 LAB .f ''i')l(il FN'yiRo scrnNCK - ^r.c. m-m.Kx I'ltn.ir.cr SAMPLE DATE: Aiipust 7. ]9fl5 SAMPLED BY: F.nviro Science SAMPLE ID: l.,i|, l>(l: //V.)fi6 AT I.AII OATE: August 9. 10R5 CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE - CHLOROETHANE HETHYLENE CHLORIDE --- ACETONE --- 1,1-DICHLOROETHYLENE - I ,1-DICHLOROETHANE ** t-l,2-0ICIIL0R0ETHYLENE CHLOROFORH I,2-DICHLOROETHANE --- t-BUTYL METHYL ETHER - I ,1,1-TRICIILOROETIIANE CARBON TETRACHLORIDE -• BROHOD ICIILOROMETHAIIE -• VOLATILE ORGANICS BY PURGE AND TRAP GAS CHROMATOGRAPHY/ HEADSPACE Compounds detected In parts per million (milligrams/kilograms) dry weight basis X 0,27 I ,.2-Oirill.OROPROPANE --- ...c-i ,3-niciii.nROPRnPENE ' • ' l - l ,3-DICIII.0U0n(0l'CIIE'" TCE (TRICIILOROETIIYLENE) ,,I,I.2-TRICHLOROETHANE ••'DIBROMOCHLOROMETHANE 0,02 0.01 BENZENE DIISOPROPYL ETHER 2-CIILOROETIIYLVINYL ETHER - BROMOFORM l.l,2,2-TETRACIIL0R0ETIIANE • PCE ( TETRACIILOROETIIYI.ENE)- TOLUENE CHLOROIlENZriin - - ETIIYI.DENZENE J.t2L X "Compounds co-elute (could be either material), LT=Less Than dwb=Dry Weight Basis. GT-Greater Than X=Not Detected •"•"Tet rahyilrofuran t Phosgene also elute at this point. Numerical results are caluclated for 1,1-Dichloroethane only. For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 0.02 Unknown peaks detected (retention time, estimated amount) nig/kg dwb. NOTE: Compound Identification is based upon retention time matches with specific known standards. Confirniation of analysis using CC/MS is required to positively identify any material and/or ainnunt deiecied. iN'DiisriiiAi. f:oi(i(n.';TON HANAGLMLNT, kdy. INC. : i \ l i . : • ' • / •'' l . i V i l u : / I ' l L';; i I I L M I A O H 00 M INDUSTRIAL CORROSION MANAGEMENT IKlbdRPORATED ii&iiuxnt io.*>iipo^hi.iri<tJifisi(bfit9 201 ii4<i])a NJDEP C e n i f lull niiiil.iiiy \/aier/Was tewaier Lahoralory ID / I ' l l 16 REPORT nATE:__Soi.re!!!!.er_Lia9fli. LAB H /iVIfi/, C L I E N T : Kt^yiRO .SCTI'NCE - TCC HFKI.KX I'HO.II'CT SAMPLE DATE: Aupiist 7. 1985 SAMPLED BY: Elnvlro Science SAMPI r ID: l.iili I'It //S')67 AT LAB DATE: Aiii'iuit 9. 10(15 VOLATILE ORGANICS BY PURGE AND TRAP GAS CHROMATOGRAPHY/ HEADSPACE Compounds detected In parts per million (milligrams/kilograms) dry weight basis CHLOROMETHANE X EROMOHETHANE 7 VINYL CHLORIDE -r CHLOROETHANE ---- • METHYLENE CHLORIDE ACETONE 1,1-DICHLOROETHYLENE -- 1,1-DICHLOROETHANE * * - t-l.2-0ICIILOfi0ETIIYLENE CHLOROFORH 1,2-DICIILOROETHANE t-BUTVL METHYL ETHER - - I,1,1-TRICHLOROETHANE - CARBON TETRACHLORIDE - - BROMODICHLOROMETHANE - - 0.23 0,03 O . l l I ,2-DICIILOROPROPAIJE - ,.,c-l ,3-DICIII.ORnPROPfllE " ' t - l ,3-DICIILtW<OPROI'CIIE TCE (TRICIILOROETIIYLENE) - - , , 1,1,2-TRICHLOROETHANE •'oiBROMOCHLOfiOMETIIANE BENZENE DIISOPROPYL ETHER 2-CIILOROETIIYLVINYL ETHER -• BROMOFORM I ,1 ,2,2-TETRACIILOROETIIANE - P'CE ( TETRACHLOROETHYLENE)- TOLUENE CIILORODENZCNE ETHYLBENZENE 0.01 0^05 "x" 0.0/| ^Compounds co-elute (could be either material). LT=Less Than dwb=Dry Weight Basis. GT=Greater Than X=Not Detected -•"Tetrahydrofuran C Phosgene also elute at this point. Numerical results are caluclated for 1,1-Dichloroethane only. For the above listed Volatile Pollutants, nothing detected at a sensitivity level of o.OI X Unknown peaks detected (retention time, estimaled amount) Xylene —O.IIL' m^/ki; (Iwlj mg/kg dwb. NOTE: Compound I d e n t i f i c a t i o n is based upon r e t e n t i o n time matches w i t h s p e c i f i c known standards. Confirmation of a n a l y s i s u s i n g GC/MS is required to ( l o s i i i v e l y i d e n t i f y any m a t e r i a l anil/or amtiiint d e l e c t e d . INDIISTIilAI. COkllOSIOH MANAGKHKNT, i NC. ziz.y^/./tX^ 'A.\7^-r-.r^. 'i: i Vli,' I .1 ! i . / I.ev' iiii. / I ' r i . ! ; i i l u i i l • y .V 9tfJ9omxsexssnc CaAI3 0? CUSTODY RSCORD J^V <.'~4 H 5 11 c=m»« MO-oeMvxL >«• xnerr r m I n . t a l l a t i o n : y ^ ^ k ^ . y ^ y Survey H o . : * m ^ i • ' <• C S t a t i o n L o c a t i o n Samplers: ( S i g n a t u r e ) i y^yyyy \ Data u 1 1 Tiae Saaple TypJ - o a p . -vjcao ^m f . O « _o _o Zz^y^d^ kyP^^^^) \ -Ay^^k^ya.-^ \ 1 V 1 / 1 -.^3i Ps.y'S/ZklA^^ZZZZ^ikLitiy^ • \ -t.o--i S-i 1 • yy^ryy/Z kZTZyyiyyZey^ -. z "<l y A i n q u i s h e d by: ( S i « a . ) \ k \\. 0 -ix..y^J^. i^yy.^^.^ // z7:^^J\ \ y ^ ^v^^l 1 \ \y- • .Received by: ( S i g n . ) i D a t e / T i a « ]C^. r . l , ^ ^ ^ r ^ ] ^-/a^tfi i n q u i s h e a by: ( S i g n , ) I / K e l i n q u i a n a a Uy: ( S i g n . ) R e l i n q u i s h e d b y : ( S i g n . ) D i a p a t c h e d b y : ( S i g n , ) Recelvea b y : y ( S i g n , ) i D a t e / X i a e j RecBiveo by: ( S i g n , ) jRec'd by L a b o r a t o r y f o r f i e l d a n a l y s i s ( S i g n . ) D a t e / T i a e Rec'd for L a b o r a t o r y by: D a t e / T i a e i D a t e / T i a e 1 P a t e / T l a e i 1 1 • 1 iMethod of S h i p a e n t : ^ -^ 301669 YCRX LAJ30RATORIE5 DlVISiON y.',7/. CE.^TlFiED REPORT TRANSMITTAL RE=CRT NUMBER. •G85C-l3i3 DATr Se::5=ber 2 5 . 1955 CLIE.NT Hr.vircscissiias, Inc. 19 Copeland. 5.Qad Denville, >t-,J 07834 ATTiNuCN J:yle3 The ccove referencaC 'reccrr is enc!ose<3. Copies cf ttnis reccrr cne succcrrtng cc:c will be rercinec in cuxfiles in me event iriey cre recuirec ter rurure reference. If mere cre cny quesicns ccnceming fhis reccn, p.e<zzQ Co ncf hesifcrs fo ccnrco: La. Any scmples submirttC to cur Lcccrcrcry will Ce retcineo fcr c rr.cxin',um cf sixr/ [60] ccys frcm receipt cf TUS rfepcrr, unless ottier crrcngemenis cre Cesirec. Ncujrclly, cs in trie pes;, oxj stcfl will be piecsec tc cucte cn cny tutue recuirerr.er.ts ycu mcy hcve In cccittcn TO itie service provicec we ciso offer tne Icllcwinc: • Hczcrccus Wcste Anciyses • PrccL!tttEvcluction/Rai.D • VVcr^ crK2 Wcstewcter Anciyses • Air QftC.^rccess Gcs Anciyses • • incvaSTict Hygiene Sun/eys • MeicjturgiccI Analyses • Micratioicgiccl Anciyses • MG5$ ScecrcmeiTV Services Very Toily Yc PUi{ i?cbertcarcCley Vice PresiCenr f TUC. IMC. • 2CC .Mc.-,-^^ KiT.c:xe• .Vic.-.rce. Ccrnec-curCii^o • ; - ; 3 ; Z~'.—^l 301670 Septie.T.cer 25, 1985 30850-1342 E^^/rHcscIEMcrs, INC. 19 Ccceland Head Cenvllig, Nev Jersev 07334 At:ta.':{:i.on: Dr. A. Kylsa r'.-~..r C b c .-l^•^ i<£^joU.^J Four (4) soil samples were suc.-^iicted tc York Lai:cr2cori£3 fcr analvsis. T.'-.e sa.TicI^g were crsparsd a.-.d analyzed in acccrda.-.ce ""•if- PrccecLjrss fcr -Ha.ndli.-.c a.^'d Che.-jcal .Analvsis cf S^di.r.s-.- and AJTar Sa.-.cles . i: j.X/'cS-5 i - i . ' T.'ie r = SL:Ics ara rspc?^%d i.': t.ne follcwi.-.c Tables. bv: y^yt^i Acoroved bv DFO/JCC/rr.d Daniel F. o^t Labcrat.qry Manaeer O / / r i^y !yAy ^ y y y/^.. T'/C, INC. • 2Ca Mc.-rc% Ti^rp-xe• -Monrca Ccnnecrcwt Ci^3 • r:C3) 26l-.:.:53 301671 TABLE 7 ^C.I,NC..::G,MC,-.', •ce "urcike • Mcs-^e. Cc.-„-.9crcu7 C<i^a.;2Ca) 241^1453 301672 TABLE 2 ^ 20850-1343 ^52220SClENCZsllNC ^ ^ - l e _ ^ d e n ^ ^ ^ i ^ 3 ^ ^ J^, 5751 - La'=: p i ^ ^^ 5752 - Lab p i . .^ <150 <150 V-VC. :NC. . irr, '^='^r^n„e.Mon.eCcnnec.=.o...a.(203,2.l.a.:S 301673 m YORK LABORATORIES DIVISION CERTIFIED REPCRT TRANSMITTAL ^ ^ REPORT NUMBER 30850-1^^^ DATE Sepcasber 25, 1955 CUENT E:iviroscisncas» l a c . 19 Cooeiand ?.Qad Denville, NJ 0783^ AHENTICN Dr. .\. Xyles The cCove reference reccrr is enclosed. Copies of this report end supccrring ccrc will be reicined in ou? files in the even: they cre required fcr furure reference. If there are cny quesTions ccnceming ihis repcrx, piecse do net hesitcre to ccnrcc: us. Any samples sufcmittecj to cur Lcccrctcry v/iil be retained fcr c mcximurn of six?/ [60] days from receipr of tt^5report, unless other crrcngements cre cesirec. NcTurclly, cs in the pest cur stcft will be pleased to cuote on cny future recuiremenrs you mcy hc/e. in cdctticn tc the service provided, we ciso offer the following: • Hczcrccus Wcste Analyses • Product £vclucticrvR&D • Wcter end Wcstewcter Analyses • Air crvi Prccsss Gos Anciyses . • IndLWKtcl Hygiene Surveys ' MeTQihrgiccI Analyses • Mlcrcfciotogiccl Anciyses • Moss Specrrcmetry Services Toily RccertGLBrc Vice President •r.'iC. ;.NC. • ICC Mc.-rpsa :.JT.Z:-<B • :'vlcnrc9. Ccrnscrcut '2z'ici--.ZZ: 301674 September 25, 1985 30850-1444 ElMVIROSCIENCES, INC. 19 Ccceland Road Denville. New Jersev 07834 Atte.ntion: Dr. A. Kyies PURPOSE -AND RESULTS Five (5) soil sa.T.ples were submitted to York Laboratories anaiysis. The sar.pl.es were prepared and analyzed in acc; ancs with Rrccedurea fcr =a.".dlinc and Che-tiical .^.nalvsi; Sedi.~enr a.nc >7a-er Sa;?.cles, E?A/CE-a 1 -1 . " The results are repor^fed in the fcllcwina Tables Precarec bv: y k y ^ ' \ J ADorovec Daniel ?» -Qtr Labcracorv. Manager a .-^-.yk. (A. /A,,.,.... ^ s f r e y Q» Curran DFO/JCC/md r.VC. ;NC. • zee Wcr«:e ruT.c:i<e • Mcrrca Ccnnectcut Zti/il • f.203', 2a•l-u.,iiSa^ Jt^ «- rs a 301675 ?5. --' ^ TABLE 1 -5 30850-1444 E>ryiR0SCI2NC2S, rNC. Sample I d e n t i f i c a t i o n T o l u e n e , uc/:<c O^Z-^V ICC B e r l e x , 8 / 7 / 8 5 1:00 360 r.VC. :NC. • ICC .Mcnrce^onpike • Mcp--ca Ccnnecrcu: C6443 • {20311^,-:^^^ 301676 TABLE 2 3 0 8 5 0 - 1 4 4 4 ENVTROSCIENCES, INC. S a m o l e I d e n t i f i c a t i o n p v r i d i n ICC B e r l e x - Lab P i t , 8 / 7 / 8 5 12:00 2 , 7 0 0 ICC B e r l e x - Lab P i t , 8 / 7 / 8 5 12:00 <150 VVVC. INC. • I-C Mcrrcs Tirr;c:Ke • Mcnrce, Ccr.necr.cu: Cd-icS • ^IZZ] Zi'.-^-^h A -c '-- '^ 301677 cs. TABLE 3 30850-1444 ENVTROSCIENCES, INC. VOLATILE PRIORITY PCLLOTANTS All results reported in ug/l. # Ccmrcund chloromethane brcmomechane vinyl chloride chloroethane me-hyla.ne chloride trichlorofluorcmethanfe acrolein acrylonitrile 1 ,1-dichloroethene 1 , l-dichloroechane trans-1 ,2-dichloroeth«.ne chloroform 1 ,2-dichloroethane, 1,1,1-trichlcroe-han^ carbon tetrachloride bromodichloromethane • 2-chloroethylvinyl ether 1 ,2-dichloropropane trans-l,3-dichloroprQcene trichloroethyle.ne benzene cis-1 ,3-dichlorcprop^n.e dibromochlorcme-nane 1 ,1 ,2-trichlorcethan.^ bromoform tetrachloroethyle.ne 1 ,1 ,2-2-teT:rachloroe*thane toluene chlorobenze.ne ethvl benzene Samcle Identificaticn ICC Berlex ICC Berlex ICC Berlex Lab P i t Lab P i t Lab •=-- 8/7/85 3:00 8/7/85 3:00 3/7/3= "-nn <1Q <10 <10 <1Q <1Q <10 <100 <1Q0 <10 <1Q <10 <'io <10 <10 <10 <10 <10 <10 <10 <1Q <10 <10 <10 <10 <10 <10 <10 22 <1Q <10 <10 <10 <1Q <10 <10 <10 <100 <100 <10 <10 <10 <10 <10 < ] 0 . < i o '• , <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 21 <10 <10 <1C <'iO <-. Q <':Q <'. c <10 ^ 1 r n <1G0 <1Q <10 <10 <10 <10 <10 <:c <ia-. <10 <10 <!0 <10 <'0 <1Q <":o <10 <'0 <10 <10 350 <10 < i O r.vc. iNC. • 2CC .Mcr-ta \:r-.pixe • MorrcaCcnnectcu:O.t-i^i • iZZZ\ 261-4^= 301678 i — Berlex Labs, Inc. St. Croix, VI VID80651095 Table I Results of Organics Analysis on Samples j 1 Mm """" • Organic Compounds Toluene Flourene Bis(2-ethylhexyl)Phtha- -late Benzophenone Di-n-octyl Phthalate Chloroform Benzene Di-n-butyl Phthalate Sample^ 087001 ug/kg 460 9200 13000 15^000000 Sample// 087002 ug/kg 560 1300 4700 2600000 500J Sampled 087003 ug/kg 420 16000 SampleQ 087004 ug/kg 440 1900 4200 200K 200K i I 1 Sampled 087005 ug/kg 360 51000 600J Sample// 087006 ug/kg 400 36000 2000 , 75000 Sample #087001 - Aerated Soil Composite from Storage Room (left side) - '' Sample #087002 - Aerated Soil Composite from Storage Room (right side) Sample #087003. - Surface Soil Composite from North Side of Lab Waste Drainage Area Sample #087004 - Subsurface Soil Conposite from North Side of Lab Waste Drainage Area Sample #087005 - Surface Soil Composite from South Side of Lab Waste Drainage Area Sample #087006 - Subsurface Soil Conposite from South Side of Lab Waste Drainage Area K " Actual value known to be less than value given J • Estimated value Blank Space - Material Analyzed but not detected 301679 1 •j£- n<V1IOM«INTAl r t o T i m o N A O I M C T - I I O I O N K Environmental Services Division I01J0N, MfW J H U T M t l 7 N « a k « f • t C«iit«i*«ri SV7Cc3 1 I I \ D*scrip«i«ii af | a a » U » f a n t m A t M s i k f l a t » « « t i k l l i t T («c S«Byl«: «,/^/i J5 \ama\t N « * k a r tali»««ltW«^ l y : t«Ufl4wUli«W l y : ft*cai*a4 l y : I c u i y t ^ l y : t « l M ^ v i f W « ^ l y r » r ft«taiv«rf l y : l a i t ' i T t ^ l y : Tia* T i - t TiB. 0«t« 0«« D M * » • ! • t»««wi i«f a « « t * •> tmnaiy lama— i— U««|» al Ci<i*4y t a o M (•< CW<a|> •< C«i)*^T l « « ( M i t * f C k « > t > • ' Calla^T 301680 f r — M*. CHAIN O? .P^t" :^V :;iiCORD ii*¥i»ON«miAi pioTtcnoK AOINCT - itoiON H Environmental Services Division EDIION, MIW JttSIT o i t i r Maaa al Uaii ami A i i t t t t : . , ^ VXD^otSlcSS U s » U M«Bka' Maakar al Caaf»iaar« I I Ottvlplitm •( i a a ^ l * * 5;^/n>*- ...x^ f«ft«m ••%««>»! t««y»lWU>tT> f*r S«spl«: H a t D«u S«B»U M ^ fwi^ lau^Ta^ I r riaa ^Z/^T^ Bal* ta««*i> far C l i o i a al Cnta^y >aa»l, Haakal •to or?cA)(, %aXtmmm^%A If: Mi/rr^ FT/ZU:^ »r r.aa B « a ^ ^ . 7. (»«>•« fai C k o f a al Canary S«a»l. *Uo t l«lmni»igl>»^ ty: ,Jkk^ ft«t«»*«4 I T fi/yu^y^ Tiaa /3. Oa4* Mr Ia«*«a tat Cl>«afa a< CaMa'r 7 ^ ^ i u < ^ ' 301681 /aaa>a Haakai ^f7a/ lali. 7 4 ' ) ^ < ; ? ^ P a a a ^ 0««a # • a«f«* <•' Cli««(a at Canary i ' l i i. INDUSTRIAL CORROSION MANAGE.MENT INCORPORATED iisj »oui£ IU. IIAMOOL!^. ^en tihstr O^JSK :UI.SI4.«JJO NJDE? C e r c i f i e d Dririk.i.-:g Wacer/U'as:: Laboracory ID :/lAil6 RZPORT DATZ: March 5. L935 LAB II 5 2^63 PRIORITY POLL'JT.A.NT LA30R.\T0RY A.NALYSIS CLIZ.NT: E:.'VIR0 SCIZNCZS IMC. S.-^MPLZ SAMPLE UNITS: SOURCE: ID: C-l -.2/k?^ T c ^ - i - t i .^r,,.,\ r — r T • . = . - . - - , 1 .•3 •.• ^ V . r r.^ *-v 2 C - 5 SAMPLZ DATE: -»s-.,,-.,. To SAMPLED BY; il 3T, V'.l AT LAS DATZ: r^; M-A.TRIX: qo-:^ (This raporr for-m contains boch cha original sample resulc and che duplicace resulc.) iPararr.ecer :: a-p _ e Resulc ia-p-e Duoiicace ;.\nci-onv RPD X C 0 r. c r 0 i Lirr.ics X Min:L.T.u- Dececcicn Linii c .-.cc .--r£.:.vsis Arsenic Bervilium Cadniiua Chromium Coooer Lead .Mercurv Nickel Selenium Silver Thallium Zinc : X ! ! X i ! LT 0.2i ! ! 14.5 ^! ! 37.3 • i \ 21.0 ' 1 LT 0.092 1 X i X ! X ! X • 1 63.1 X X LT 0.2= 17.9 43.5 25.7 LT 0.093 X X X X 67.8 X X NC 20% 15" • 20% NC i X i X ! X 1 X 1 77. i X 1 i X ! 1 NC f20- • - I Q Z t20Z i NC ! X 1 ! X X 1 x 1 t207. LT T_T LT LT LT j LT x X 0,24 0.22 0.52 1.3 0.092 X X X X 2.23 1 1 1 ,_ t LT i LT 1 LT i LT j ! 1 I X ' X 0.24 '• 0.22 "i 0.62 ' - 1 . 3 i 0.092 •' X • X X '. X •' 1.03 ' Phenol Cvanid; X X ! X X 1 X 1 X X X X : . X X V i i i 1 NC - Non-caicuabie .RPD due co value(s) less chan dececcion limic. dub - D r y Weig.hc Basis X = Hoc Analyzed LT - Less Than INDUSTRIAL CORROSION MAxNAGZMZNT, INC. RPD » Relative percenc difference. RSL/dlh R ^ P ////Jy ik. cnard S. L*^vf^ jfcnard S. 1.4. r e s i d e n t ' ' / i / } v ^ • 301682 l^ m INDUSTRIAL CORROSION MANAGE.MENT INCORPORATED 1152 ROUTE '0. MuiOCLPH. .ItW .EJUET 37S69 :0I-5J4-J33a NJDE? Cercified Drinking Wacer/yascevacer Laboracory ID //14116 RZPO.RT DATE: March 5 LAB If 52464 1996 PRIORITY POLLUTANT LA30.R.\T0.RY ANALYSIS CLIZNT: ENVIRO SCIZNCZS. INC. SAMPLZ SA.MPLZ UNITS: SOURCE ID: C- 2 -- Is: ,- \ .and drv Chemica veishc 1 Co. b s. '^" s SAMjiLZ DATE: SAMJ'LZD BY: AT LAB DATE: M_\TRIX: Soil -oX^-,=>--. 1 Q' Alan Xvlss Februarv 21. 1 cc i 1 C I A iParam.e car S amp 1e Resulc dvb =• Dry Weighc Basis X » Noc Analyzed LT » Less Than Xinimum Dececcion Mecncc Blank .•i.nalvsis .-SLncimonv Arsenic X X 1 i X ! X V i Bervllium i X 1 X i X Cadmium Chromium 1 CoDoer Lead Mercurv LT 0.23 1 LT 0.23 LT 0.23 15.4 3S.3 22.0 LT 0.103 Nickel ! X Selenium 1 X Silver Thallium Zinc Phenol X X 57.S X Cvanide J X LT 0.21 LT 0.21 LT 0.5 9 LT L.3 LT 0.103 X LT Q.r? i LT L.3 ••" ! T — n ' p, *: X 1 X 1 X i X t X j X 1 X LT 2.1 1 0.97 i X X ! X 1 X 1 I 1 I RSL/dlh INDUSTRIAL CORROSION MANAGEMJINT. INC. gr±£hard S. lev<£ne P r e s i d e n c / 301683 INDUSTRIAL CORROSION MANAGE.MENT INCORPORATED .IU KOUfE 10. WKOCUM. Hly».;VtSlt 07SS9 ZOt-iU-OZZO NJDE? Cercified Drinking War.-/Vasc=v, Laboracory ID •/14116 R£?ORT DATZ: .March 5. 1986 LAB it 52465 , PRIORITY POLLUTANT LABORATORY ANALYSIS CLIZNT: ENVIRO SCIZNCZS, INC. SA.MPLZ SAMJ'LE UNITS: SOURCE: Island Chemical Co. ID: G-3 r.s,''kE(-3on) drv veishc basis SAMJ'LE DATZ: S.i_M?LED 3Y: AT LAB DATZ: Tebruarv 1?. Alan Kvles Zabrua^'.* '^' i_ c c ; 19Ef M-ATRIX: Scil dwb •• Dry Weighc Basis X - Noc Analyzed LT =- Less Than RSL/dlh Paramecer Ancimonv Arsenic ' Bervllium Cadmium Chromium CoDoer Lead .Mercurv Nickel Selenium Silver Thallium Zinc ' Phenol Cvanide Sampla Resulc V V X T - p T? I c - 33.3 ' 4. =; T-T" n, '01 X X X X 129 X ! X 1 1 Minimum | Dececcion j Limic 1 1 Y 1 i V 1 -T^ 0.22 ! TT 0.21 1 1 TT 0.58 ' i T T 1 . -, - • 1 TT n . ' 0 ' ! X i X 1 X 1 X 1 LT 2. ' X X Mac.-.cc Blank Analvsis .,. -,- Y T T n -!-> T - n -11 T - n :: - — 1 I 1 i ! i i • \ i r - : - i T T n -• •".I V V X X 0.95 1 t i 1 1 i 1 1 ~. INDUSTRIAL CORROSION MANAGEMZNT.INC. Pochard S. lieviiie P r e s i d e n c ^ 301684 r Ml INDUSTRIAL CORROSION MANAGEME.NT INCORPORATED NJDE? Cercified Drinking Vacer/Wasce-- Laboracory ID r^l4115 M .i Murt 10. WJ«OOL«I. .itw jtRSEY i i u i M\-iu-iiza RZPO.RT D.A,T£: M?.rch 5, 1986 LAB It 32466 PRIORITY POLLUT.^.MT LA30PA.T0.RY ANALYSIS CLIENT: ENVIRO SCIZNCZS INC. SAMPLZ S.A^-PLZ UNITS: SOURCZ: Island Chemical Co. ID: G-4 me''ks''t;rm'* drv veishc basis • S.-iiMPLZ DATE: SAM-PLZD BY: AT LAB DATE: e Druar-' 1 Q _ 1 OS, M-ATRIX: Spji Paramecer .-.ncimonv Sample Resulc .Minimum Dececcion Limi! M e c.-. c c Blank .^nalvs: .Arsenic Bervllium X Cadmium LT 0. LT 0.22 0.2: Chromium 12.0 LT 0.20 LT 0. Coooei 7<; .T 0.5 7 Lead I 7 7 L.3 T T ! Mercurv LT 0.102 LT 0.102 LT 0.1C 2 Nickel Selenium Silver Thallium Zinc 37.1 LT 2.1 0.9^ Phenol Cvanide dwb » Dry Weighc Basis X - Noc Analyzed LT - Less Than RSL/dlh INDUSTRIAL CORROSION MANAGEMJiNT, INC. Ri£hard S. L^ilifi P r e s i d e n c f 'w(yiy>*'^ 301685 # INDUSTRIAL CORROSION MANAGEMENT INCORPORATED a NXiiE 10. HAAOOLP^. NEW jEfistr o/isa :oi-ii*.ujjo NJDZP Cercified Drinking Wacer/'-'ascev Laboracory ID i/14ll6 ^ RZPORT DATZ; M^rch 5 . 1°.= - LAB it 5 2 4 6 7 PRIORITY POLLUT.\NT LABORATORY ANALYSIS CLIZNT: ZNVIRO SCIZNCZS INC. SAM-PLZ SOURCZ: Isla SAMPLE ID: G-5 Cha-ical Co. UNITS: ms./ke'^-om') drv ;asis ' SAMPLZ DATZ: Februarv 19. 19S6 SAMJ'LZD BY: AT^..^ yy-'^c AT LAB DATZ: MJ>ITRIX: <;. .1 ' 1 Q C ; ;c'-- Paramecer 1 1 1 Sample i Resulc Minimum Dececcion L imi c '—1 Mechcc 1 31anl< I Analvsis 1 1Ancimonv jArsenic dwb - Dry Weighc Basis X - Noc Analyzed LT - Less Than RSL/dlh Bervllium Cadmium Chromium Coooer ! iLead Mercurv Nickel Selenium Silver Thallium Zinc Phenol Cvanide X LT 0.23 17.1 36. 1 20. 2 LT 0.105 X X X X 57.2 X 1 X X ! LT 0.23 ! LT 0.21. ! LT 0.50 ^i LT 1.3 1 LT 0.105 ! X X ! X X 1 LT 2.2 X X X LT 0.23 LT 0.21 LT 0.5C LT 1.3 LT 0.105 '. 1 1 1 1 X X X X 0.95 X X i i 1 1 1 1 1 INDUSTRIAL CORROSION MANAGZHZNT,INC. 1/Ty^i, (.ichard S./LeVdne Presidenc 301686 c I? i'l INDUSTRIAL CORROSION MANAGEMENT INCORPORATED t\%l ROUIE IQ. fUMXlLPH. t e n JEASET a7I«9 201014.0^^11 NJDEP Cercified Drinking Wacer/ Laboracory ID ^14116 REPORT DATZ: March 5. iQg6 LAB it 52468 "<i3 -s-ace r PRIORITY POLLUTANT LABORATORY .^ALYSIS CLIZNT: ZNVIRO SCIZNCZS INC, SAM-PLZ SOURCZ: Island Chemical Cc. S.AM-PLZ ID: G-6 UNITS: -.T.^^^r 1 -» - c - c SAM-fLi: DAT:L: Februarv 19". 195 5 SAMPLED BY: .:^lan Kvles .kT LAB DATZ: ^»-„,.,,_.. -i ' C C A M-\TRIX: c„,-i iParamecar 1 Sample I Resulc Minimum Dececcion Limic Mechcc j Blank Analvsis 1 dwb - Dry Weighc Basis X - Noc Analyzed LT - Less Than Ancimonv Arsenic Bervllium Cadmium 1 1 t 1 i i Chromium ' Coooer Lead Mercurv Nickel. Selenium ! 1 Silver Thallium Zinc Phenol Cvanide X X X ^.0 46.5 40.0 32. a LT 0.122 X X X X 349 X X 1 T T T T LT LT LT LT X i X i X i 0,23 ' 0,25 : 1 0.71 ! 1.6 1 0.122 X 1 X 1 X X 2.6 X X LT T f LT T_7 LT X 1 X 1 X 1 0.2= i 0.25 1 0.71 i 1.5 '- ! 0.122 1 X i 1 X 1 X i X 1 1.2 ! 1 X : 1 1 1 1 RSL/ dlh INDUSTRIAL CORROSION MANAGEMENT,INC. 7 / M Z ^ /(//7yyy^ Ridhard S. Lfvi.1^ Preside! I S. Leva mc [/ 301687 n •i I i i i 1 I > ; i. INDUSTRIAL CORROSION MANAGE.MENT INCORPORATED •ij •<ourt :o. SXCCL.IN. itwjt.iiCf 0/1(69 :oi-5j<-oa:;u .NJDZP Cercified Drinking Wacer/Wasceva-; Laboracory ID .'/'14115 .RZPORT DATZ: March 5. 1985 LAB /; ^lifia PRIORITY POLLUTANT LABORATORY A.NALYSIS CLIZNT: ENVIRC SCIZNCZS INC. SAMPLZ S.^MPLZ UNITS: SOURCZ: Island Chemical Co. ID: G-- — c ' '.' c •' — '^—1 ^ .'•* •^•T 'v'2 ' '7'^ r n 3 c -' c SAMPLZ DATE:Februarv 19! 19=6 SAMPLED BY: Alan Xvles -AT LAB DATE: Februarv 21. ICC — M-ATRIX: So--"' (This resor: :orm concains boch che original sample resulc and che spike recover-.'.) 1 1 Parame cer' Samole Resul: So ike Added 1 Soikec ! i Sample j ' Resulc ! . 7R Concrol Limics for JR ^'.inimum Dececcion Limic M 5 : r. 0 c Blank .Analvsis lAnc ir.cn V 75-125 I Arsenic '• Bervllium ! Cadmium 1 Chromium. 1 Coooer • 1 Lead Mercurv ' Nickel ! Selenium 1 Silver ' Thallium Zinc Phenol Cvanide X X 1 1 2.4 ! 71.1 ! SI. 4 i 45.4 1 LT 0.121 1 X X 1 X i X i 851 X X X X 1 1 \ 1 0.004 X X X X 1 X - X X i X i 1 1.13 i i 4.0i 1 i 2.39 i 2.92 ': 0.0035! 1 X 1 ! X 1 i X ! ! X ! i 1.72 ! X i 1 X 1 i 1 1 1 1 1 1 X 175-125 X 1-7 5-125 103% 75-125- 119% 175-125 83% 175-125 106% 75-125 • 88% I75-I25 X 75-125 X 175-125 X 175-125 X 75-125 103% 'r75-125 X I7 5-125 X ^75-125 % ! %r % 1 LT % ! LT % 1 LT mt % LT LT - 1 /. 1 % 1 •f i 7. 7. ILT 7. 1 7. i i • X X 0. 0; 0. 1. 0. X X X X i 1 28 1 LT 25 LT 72 T_T 5 i LT 121 -^- 1 . 1 20. 1 i X X 1 I — V Y 0.2s 0.25 0.72,. 1.5 n : "; 1 T T T T • " 7 Y Y 1 i I 1 1 t i 1 i 1 ] %R =» Percenc Spike Recovery NR = Noc required. Scandard addicion performed- dwb =» Dry Weighc Basis X » Noc Analyzed LT =• Less Than The spiked sample resulc is based on che soil in solucion. Ic does noc direccly reflecc che final mg/kg dry weighc basis resulc of Che sample. RSL/dlh INDUSTRIAL CORROSION MANAGEMENT.INC. c UL//lAyf./Alyy- 301688 Ricl^^rd S. L&v/znkl/ fe L'J INDUSTRIAL CORROSION MANAGEMENT INCORPORATED IISJ WUIE 10. .^xOCU'^'. MtW .WSET J/S69 : a i - i 4 l - J J ^ NJDE? Cercified Drinking Laboracory ID •/141i5 5 rtacer;^a; cevacer RZPORT DATZ: M^ L.\3 // 5 24 70 1 Q 5 A PRIORITY POLLUTANT LABORATORY .ANALYSIS CLIZNT: ZNVIRO SCIZNCZS INC. S-AM-PLZ SAM-PLZ UNITS: SOURCZ ID: G- _~,"^-- . 3 ., Isl -rZ = nc .;_. c- . • - a r . -•a: .ical an - Co. ba=- _' SAMPLZ DATZ: Februarv SAM-PLZD BY: AT LAB DATZ: il = - Con..-. •<v-= = . 3 • » - • - "^ ^ : C C X .MATRIX: Cn-'i 1 Paramecer Ancimonv ! 1 Arsenic Bervllium Cadmium Chromium Coooer Lead Mercurv Nickel Selenium Silver Thallium Sample Resulc Y X V LT 0.2 3 2C . 4 32-3 19.4 LT 0.093 X 1 X X X Minimum ' Dececcion Limic X i Y ! X ! LT 0.23 1 LT 0.21 ' LT 0.60 ' i LT 1.3 LT 0.093 X X X X Mechcc .Analvsis .,- •r Y T — r) "^" T —- ,-v -. ^ T - -^ ; ,1 . T — 1 ": LT 0.09 3 •Jl X 1 1 i i . ! i 1 ! i 1 1 Y X Zinc Phenol Cvanide 76.2 X X LT 0.44 X X 0.99 ' X • Y dwb - Dry Weighc Basis X - Noc Analyzed LT » Less Than RSL/dlh INDUSTRIAL CORROSION MANAGZMZNT,INC. RL6h P idhard S. L^vl residenc / AiAyAA. 301689 3 ! f , 1 i INDUSTRIAL CORROSION MANAGEMENT INCORPORATED -Ml HOuIt 10. SAJiCCUM. >£W ;EMtT a;!59 :<il-5a4<jJM -NJDZP Cercified Drinking Wacer/Wascevacer Laboracory ID :/14il6 RZPO.RT D.\TZ:- M_2rch 5, 19S6 LAB li' 3 24 7 L PRIORITY POLLUTANT LABORATORY ANALYSIS CLIZNT: ZNVIRO SCIZNCZS INC. S-AM-PLZ SA.MPLZ UNITS: SOURCZ: Island Chemical Co. ID: G-o _ ^ .••..-. ^ _ . , _ - , ^ _ . , ._.o , • _ • _ _ • _ . _ - • - • SAM-PLZ DATZ: Februarv 19; 19S6 SAMPLED BY: Alan Kvles AT L.AB DATZ: -Q•-.-., = -.. 71 , a z - MATRIX: c^,-i r'aramece; Ancimonv S amp1e Resulc X Minimum Dececcion Limic X aian.-; Analvs: Arsenic Bervllium Cadmium LT 0.23 LT 0.23 LT 0. dwb » Dry Weighc Basis X =» Noc Analyzed LT » Less Than RSL/dlh Chromium Coooer Lead Mercury Nickel Selenium Silver Thallium Zinc Phenol Cvanide 19.3 34. 9 2' . 4 LT 0.113 X X X X 75.7 X X LT 0.21 ! LT 0.61 1 LT 1.1 LT 0.113 X X 1 X X LT 0.44 X X LT 0.21 ! LT 0.51 1 LT 1.1 i LT 0. 113 1 X 1 X X • i 0.9? 1 X X i 1 INDUSTRIAL CORROSION MANAGZM-ZNT.INC. Ri^ard S. Laving Presidenc C 301690 INDUSTRIAL CORROSION MANAGEME.NT INCORPORATED .12 flourE 10. (UNOCLPM. Ntiii JE.HSET oithi joi-s«4.oj;a NJDEP Carcified Drinking Wacer/Wascavace: Laboracory ID ^14116 RZPORT D.ATE: Mjzr: LAB it 52472 5. 193; ?-RIORITY POLLUTANT I-ABORATORY ANALYSIS CLIZNT: ^vVTRO SCIZNCF-. rvc. S.JMPLZ SA-MPLE UNITS: SOURCZ: ID: G- rT,c-/'<^''^ Is • ' ^ n-n^ .and r-'-.r Chemi ve"' ""^ ca r 1 •n Co. 3 e - c SAM-PLZ DATZ: SAM-PLZD BY: AT L-AB DATE: M J ^ T R I X : <;n- Februarv 19. Alan Kvles r=,-.,_,,-_,, ->• 1 1_ cc- ! c c - j Paramecer Ancimonv Arsenic Bervllium Cadmium Chromium Coooer Lead -Mercurv Nickel Selenium Silver Thallium Zinc Phenol Cvanide Sampla Resulc Y X X LT 0.30 30.6 62.7 16.5 LT 0.106 X V .V X X 66. 5 X X 1 1 Minimum | Dececcion 1 Limic 1 X ' X i X i LT 0.30 ! LT 0.27 LT 0.77 i LT 1. 4 LT 0.106 X X X X LT 0.56 X x Mechcc .Analvsis x X X i 1 LT 0.30 LT 0.-7 1 LT 0-77 i LT 1.4 '- 1 LT 0.106 X Y ! X X 1.3 1 I X Y 1 ! i 1 t i dwb - Dry Weighc Basis X " Noc Analyzed LT » Less Than RSL/dlh INDUSTRIAL CORROSION MANAGEMENT,INC. A / y y ^ R^c'hard S.'yLaKC^dhe Preside: 1 S. i- snc / 301691 l\ r.ii i I ' l .k : : ! INDUSTRIAL CORROSION MANAGEMENT INCORPORATED l U J - U U l l IU KAlrUUl.l'n I t W J l H i L T 0/3»M lUI )•< UJJU NJDE? Cercified Drinking Wacer/Wascevac: Laboracory ID (/i4116 .REPORT DATE: March 5. JOfift L.\2 it 52473 PRIORITY POLLUT.A-NT L.A30R.AT0RY A-\ALYSIS CLIZ.NT: ENVI.RO SCIENCES INC. SAMPLE S.-^-MPLE UNITS: SOURCE: Isiand Chemical Co. ID: G-11 ma/ke i':3-3m) drv veishc basis ' SAMPLE DATZ: February 19. 19S6 SAMPLED BY: Alan Kvles AT L.A3 DATE: Februarv 21. 195 6 MATRIX: Soil 1 i • 1 1 params cer '.Ancimonv iArsenic i s ! R 1 1 1 ampl esul X X e c 1 M De i i inimum ceccion Limic X X M=..-cc Blank .Analvsis Y X Bervllium Cadmium Chromium. X LT 0.34 41.1 X LT 0.54 LT 0.49 X LT 0.54 LT 0.49 ICoooer 1 .4 LT Lead 12.8 LT 2.5 T "" 7 ^ Mercurv ' Nickel ' Selenium 1 Silver Thallium Zinc Phenol Cvanide LT 8 0.194 X X X X 71 X X LT LT 0.194 1 X 1 X X 1 X 1 5.1 1 X 1 X LT 0.1 X X X X 2. 3 Y X ?4 i i 1 1 dwb = Dry Weighc Basis X = Noc Analyzed LT =• Less Than RSL/dlh INDUSTRIAL CORROSION MANAGZM-Z.NT, INC. '/VhitJL Lchard S. Presidenc 301692 I il k CO o M to U> . , - INDUSTRIAL I ' I . CORROSION r . y l MANAGEMENT UI i INCORPORATED IISI ItOUK 10. (UHOOIPII. NEW JfASt V 0?a6J ;0I S>< ()]]0 HJDEP r.eri i f ied D r i n k i n g Waier/V/ui.leviater l . a h o r a i o i y ID i l ' i l l 6 REPORT HATE: H;,rnl. ID, 19R6 A:l -' CLIEHT:_ENyTRO_saiKNCES^Na._:^Ifi].an!LJ]lieifilcaLJ:.(Wfliiy_ni:Qjcct_ SAMPI E lf):_G-i -z ' SAMPLE n A T E : F e b r i i n r v 1 9 . 1986 SAMPLED BY:_ ALnn_KyIea ^^T LAR DATE: i.-ciiniary 2 1 , 10»6_ VOLATILE ORf.ANICS DY PURGE ADD TRAP ; . By fiC/HS - HEADSPACE Compounds d e t e c t e d In p a r t s p e r m i l l i o n (mi 11 igranis/k i lofjroins) dry weight b a s i s , CIILOROHETIIAHE BROHOHETIIANE VINYL CHLORIDE - CHLOROETHANE HETHYLENE CHLORIDE ACETONE 1,1-DICHLOROETHYLENE - 1,1-DICHLOROETllANE t-l,2-DICHL0R0ETHyLENE CHLOROfORH 1,2-DICHLOROETHANE t-BUTYL METHYL ETHER -- I,1,1-TRICHLOROETHANE - CARBON TETRACHLORIDE -- BROHODICIILOROHETIIANE -- - N l ) _ J J I ) _ - N l ) _ . N i ) _ -Nl)_ JJ I I - NI) _.N!L _N!L _N!L -NIL J ! L ..NIL ND 1,2-DICIII OROPROPANE c-i,3-niciiinRoi'Rnpi:NE - - - l-l,3-niCIIL0R0PR0l'ENE - - - TCE (TRICIIIORnLTHYLENE)-- 1,1,2-TRICIII.OROETIIANE DIDROHOCIILOROHETIIAHE - - - - BENZENE DlISOPROPYL ETHER -- 2-CHLOROETIIYLVlNYL ETHER • BROMOFORH 1,1,2,2-TETRACHI.OROETHANE PCE (TETRACHLOROETHYLENE) TOLUENE CHLOROOENZENE ETHYLBENZENE • Nil, • N!)_ N!l_ NIL NIL _ H ! L NIL _ H ! L NIL __N!)_ NIL N|)_ _ N ! L .Nn_ — N I L LT=Less T h a n , G T = G r e a t e r T h a n , Nn=Nou D e t e c t e i l dwb-Dry Weight B a s i s SIMtUOOATI' KI'CnVKKll'S: d^ motbylene c b l n v l . l e - 60% ' ' H ' II I'll d.. t o l u e n e - 12 5% - 131% X For t h e above l i s t e d V n l n t l l e P o l h i l a n t s , n n l h l n g d e l e c t e d a l a s e n s l l i v i l y level of 0 . 0 2 m|;/l<|',(ppin) ilwb. I • * ' •* Other compounds delected:^ i^ , Li- •••I...I • TNI)ll#iaAI, C,a\AtWl()U HANAGI'MI^NT, TNC^ .. /ck.{AU A/{/-/.•( r^i \'{yyyZzz. _ • • ' • ' •• < A / i / l l . . . . I I , , , , , . ^ o M VO I , I INDUSTRIAL ' j . CORROSION • ' I MANAGEMENT J I J INCORPORATED nil ROUl 10. MNOOini. M(wjifts(yo;i(i JDI sitoi^o NJOEP Ceriified Drinking Water/Wastewater Lahoralory If) //I'd 16 REPORT PATE: _M,,rch_|n._]9ft6_ L A D // v^/,r,/, CLIENT: ENVIRO .SnTjENOE.S TNO. - T.slnnd Chcmlcnl rnwpnnv Prolect SAMPLE DATE; FebrMarv 19. 1986 SAMPLED BY: Alan_Kyle3 SAMPLE ID: f;-2 •:|/.'>i.-, _AT IAR DATE: Pcl.nii-iry 2 1 . 19116 VOLATILE ORGANICS BY PURGE AND TRAP By GC/MS r HEADSPACE ^yi Compounds detected In parts per million (mi 11igrams/kilograms) dry weight basis. CIILOROHETIIANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE HETHYLENE CHLORIDE ACETONE 1,1-DICHLOROETHYLENE -• 1,1-DICIILOROrTIIANE t-l,2-DICHL0R0ETIIYLENE CHLOROFORM 1,2-DICHLOROETHANE t-BUTYL METHYL ETHER -- 1,1,1-TRICIILOROETHANE - CARBON TETRACHLORIDE -- BROMODICHLOROMETHANE -- — N I L _ N I L NIL NIL NIL Nl) Nl) Nl) N l ) _ _ Nl) un Nl) Nl) NU 1,2-DICHLORnpROPANE — - - - c-l,3-DICIII0RnpR0ITNE - - - t-l,3-0ICHIOROI'R0l'tNE - - - TCE (TRICIII.OROETIIYIENE)-- 1 ,1 ,2-TRICIIl OROETHANE - - - PIBROHOCIILOROMETIIANE BENZENE - - - 01 ISOPROPYL ETHER 2-CIII.OROETIIYLVINYI. ETHER • DROMOEORH - 1,1,2,2-TETRACIILOROETHANE PCE (TETRACIILOROETMYLENE) TOLUENE CHIORODENZENE ETHYLBENZENE • _ N ! 1 :„nn • _ H I } ' — N l ! . _ N I ) _ n i ) _ N I ) _ N l l _ i i n __NI> _ N I 1 Ml) Nil Nl) N|) LT=Less Than, GT=Greater Than, ND-Not Detected dwb=Dry Weight BasIs 5L'!!!?Q^.'^TLl!!!?f:f}^!:!'.!!:5' ''2 merliylene'chloride - 6/(% (I. toluene 11 I'll - 126% (I . toluene - 1 1 't% X For tho above listed Volatile Pollutants, nothing detected at a sensitivity level of 0.02 ni|;/ke(n()m) duh. Other compounds delected: i ''' '• ' : / (NDiWTiaAi. c.omuyjjm iiANAotHKNT, rue. / U k / u ( y / { ( / y A . n ^ 1L •• • -"••"• I i 'M INDUSTRIAL CORROSION MANAGEMENT INCORPORATED )IS)fUXn( 10. R<NOO(ni.MWJ(RSEV 07169 201 i l 4 « } ] a # o o^ vo cn NJDEP Certified Drinking Water/Wastewater Laboratory ID yCl'il 16 REPORT DATE:_M,-,rc!iJ|),_19ft6_ LAR // «/,6S CLIENT; ENVTRO SCTENCE.S. TNO. - T.slnnd Chcmlcnl Coinpany P r o l e c t SAMPLE I D : _ ( ; - ] • • ' ' ' :'!••••• SAMPLE DATE; February 19. 19R6 SAMPLED BY: Al2!LKyIS5 ^^^ " ^ " '^'^TE: Fe!,r,,nry_21^J9n6_ VOLATILE ORGANICS BY PURGE AND TRAP By GC/MS -. HEADSPACE ...' I - • ' • ^ . Compounds detected In parts per million (milligrams/kilograms) dry weight basis. CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE --- ACETONE 1,1-DICHLOROETHYLENE - 1,1-DlCIILOROETHANE t-l,2-D|CIIL0R0ETIIYLENE CHLOROFORM 1,2-DICllLOROETilANE - - - - t-BUTYL METHYL ETHER - - l.l,l-TRICHLOROETIIANE - CARBON TETRACHLORIDE - - BROMODICHLOROMETHANE - - N|)_ NIL NIL NIL N[L Nn_ NIL Nlll NU_ NIL N n _ NP NP N P . _ Nl) 1,2-DIClll OROPROPANE c-l,3-DlClliOROPROPrNE - - - l-l,3-DICIII0K0PI(0PEIIE - - - TCE (TRICHI.OROETIIYLENE)-- I ,1,2-TRICIIL0R0ETI1AI(E - - - DIBROHOCIII.OROHETIIANE BENZENE DIISOPROPYL ETHER 2-CHI.OROETHYLVINYL ETHER • BROMOFORM 1,1,2,2-TETRACIII.OROETHANE PCE (TETRACHLOROETIIYLENE) TOLUENE CHLOROBENZENE ETHYLBENZENE • N n _ Nl) Nl) Nl) ND , Nl) Nl) ND . Nl) N D _ _ Nl) Nl) NU Nl) Nl) LT=Less Than, GT=Greater Than, ND=^Not Detected dwb=Dry Weight Basis ^L'llHOL'.ATLHl'frL'V''•'!!''•-'= ''^ methylene' chloride - 9fi% liient 57% li. t o l u e n e - 61% lU'lt For the above l i s t e d V o l a t i l e P o l l u t a n t s , n o t h i n g d e t e c t e d at a s e n s i t i v i t y l e v e l o f 0.02 mp,/k|;(p|)iii) iK/h. Other compounds d e l e c t e d : > INDUJ y ,1'iiiAi. (:Qrtj;«,';ini) HAMAnriitiNT, inc. • / f / / y<.//A%/ /^^f-i^ 1. w o l - » vo INDUSTRIAL CORROSION MANAGEMENT INCORPORATED IISI ROUIE 10. RANDOtni. IKW JlHsrv 071(9 201 i l l Olio J ••• NJDEP C e r t i f i e d D r i n k i n g W a l e r / W a s l e w a i e r l a b o r a t o r y ID ij'I'il 16 . 1 . I • • • l A l i . - ^ ] REPORT DATE:__H.n-cb 10,- 19fl6i'-.'ri I An § 52466 ykA I.-' CLIENT; ENVTRO SCTENOES. INC. - T.slnnd niiemlcal Ooinpnnv P r o l e c t SAMPLE ID:_(:_/i SAMPLE DATE; F e b r u a r y 19. 1 9fl6 SAMPLED BY: :AJn!i_KyJe!i AT IAR DATE :_p,.ijrunL-y_2L_lQD6- VOLATILE ORGANICS DY PURGE AND TRAP By GC/MS ,- HEADSPACE i. -'A'- . • I . .,.'••; I • ' • Z ' Z ' I Compounds d e t e c t e d In p a r t s p e r m i l l i o n ( m i l l i g r a m s / k i l o g r a m s ) dry w e i g h t b a s i s . CIILOROHETIIANE BROMOMETHANE --- VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE I.I-DICHLOROETHYLENE - 1,1-DICIILOROETHANE t - l . 2 - D I C I I L 0 R 0 E T I I Y L E N E CHLOROFORM 1,2-DlCHLOROETHANE t-BUTYL METHYL ETHER -- 1,1,1-TRICHLOROETHANE - CARBON TETRACHLORIDE -- BROMODICHLOROMETHANE -- .Nil - N l ) _ J J U _ JIU -1ID_ JJQ- -NIL_ J l l i _ J^l)__ _NI)__ _N}) j j ) _N|) Nl) I,2-DICHIOROPROPANE c - l , 3 - D l C I I I 0 R 0 P R 0 P E t l E - - - t - l , 3 - D I C I I I 0 R 0 P R 0 P E N E - - - TCE (TRICIIIOROETHYLENE)-- 1 ,1 ,2-TRICIILORflETIIANE - - - DI BROHOCUI.OROHt THANE BENZENE Dl ISOPROPYL ETHER 2i-CIIL0R0ETIIYLVINYL ETHER • BROMOFORM I ,1 ,2,2-TETRACIil.OROETHANE PCE (TETRACHLOROETHYLENE) TOLUENE CHLOROBENZENE ETHYLBENZENE „.N!L „ N ! L _!!!L __.N!L __N!L _ H ! L _I!!L _l!!)_ —liiL _.N!L H!)_ _ N n _ __.NP._ _ N ! L ND .5!J!!!!!?flAT!:J?!'l'f^y!r!!ll-'i= ''^ "'etbylcne cblnrl.le - 100% <l toluene - 70% LT-'Less Than, GT=Greater Than, ND-Not Detocte.l '"'" ~ ^'^^ dwb'=Dry Weight Oasis X For the above listed Vol al 11 e Pol lut ant s , nothing delected at a st.-ii'.. il I v i Iy level of (].(]2 m(;/k|'(ppm) duii Ot her compotinds de I ec I ed: '). )\\?/n/\ ]mu?/Y\<u\, oniTifn^nN HANACKMRNT, INC. ///A/2yJ%J/AAtt\. •: .... CO o vo INDUSTRIAL CORROSION MANAGEMENT INCORPORATED IIS2 ROUIE 10. RANOOini. NIW JERSEY 07et9 201 Sa4 01)0 I ••* NJDEP Certified Drinking W a t e r / W a s t e w a t e f Laboratory ID yfi'il 16 , :,. : -i^i.' ,'.: . .1 t . ' i . ' f • . * •* 1 • I * • • • • 'Z^iZA' ^ ' ' .•' REPORT DATE: Marcl. 10. 19n6'i.''li:U ' •.•' : LAD // 52/,67 •t'r. CLIENT; ENVTRO S C T E N C E S , T N C . - Tsland Chemical Compnny Project SAMPLE in:_C-5 SAMPLE DATE; February 19. 1906 SAMPLED BY; Alan Kyles y\y AT LAR DATE: I'ebruary 21. I9fl6 VOLATILE ORGANICS BY PURGE AND TRAP §L_£lZi1 S - IIEAD S PAC E CHLOROMETHANE - BROMOMETHANE - -- VINYL CHLORIDE CHLOROETHANE HETHYLENE CHLORIDE ACETONE 1,1-DlCHLOROETIlYLENE -• 1,1-DICHLOROETHANE t-l,2-DICHL0R0ETIIYLENE CHLOROFORM 1,2-DICliLOROETHANE t-BUTYL METHYL ETHER -- I,1,1-TRICHLOROETHANE - CARBON TETRACHLORIDE -- BROMODICHLOROMETHANE — •: '\\Zi-i.A^ i. zy C o m p o u n d s detected In parts per million (mi 1 1 igrams/k i lograms) (Iry welgitt b a s i s . _ N ! 1 _ _ N ! > _ _m _ N U _ _ N I ) _ _ N I ) _ _ N ! I _ _NIL_ _NP._ _ N P _ _ N ! } _ . N Q — _N!)_ -NP— . U P _ 1,2-DICIil OROPROPANE c-l,3-DICIII.OHOI'ROI'rNE - - - t-l,3-DICIM0R0PR0PENE - - - TCE (TRiCIII OltOETIIYLENE)-- 1 ,1 ,2-TRICIILOROETIIANC DIBROMOCIILOROMCTNANE BENZENE DIISOPROPYL ETHER 2-CIII.OROETIIYLVINYI. ETHER • BROMOFORM I ,1.2,2-TETRACIILOROETIiANE PCE (TETRACHLOROETHYLENE) TOLUENE CHLOROBENZENE ETHYLBENZENE ND _N|) JJl) _.Nn _NP Jin _N|) JI!L_ -NIL_ _NI)_ JI!I_ JI!L_ _N|) _N|1 J M SIlItltOCATI' ltl'CnVI'ltlli:.S: LT=Less Than, GT=Greater Than, ND=Not Detected dwb-Dry We I gilt BasI s (1-2 mntbylene chloride - 97% (I, toluene - 67% IIKIl - 66% X For the above l i s t e d V o l a t i l e P o l l u t a n t s , nothing detected at a sen;, i I i v I i y liivel of 0.02 mc/kcCppiii) ilul). Other compounds delected: ^ ' '' ' • INnilknitlAl, COIi/oyON IIANACI'MENT, IIJC, CJ o M <Ti VO 00 INDUSTRIAL CORROSION MANAGEMENT INCORPORATED IS2 ROUIE 10. RANOOini. NEWJERSIr07169 201 i t 4 0310 N.IDEP C e r t i f i e d D r i n k i n g V/ater/V/aslev-^ater Laboratory ID /?I'll 16 • ^ ; ; '/[ REPORT n A T E : _ M a ! : c ! . J O , _ i 9 n 6 _ l L l LAB II v2/i6H '•••. . CLIENT; ENVTRO .SCTENCES. TNC. - T.slnnd Cbemical Compnny Project SAMPLE \0:j]-.f^ SAMPLE DATE; February 19. 1986 SAMPLED BY: .AJan^KyJen AT LAD DATE: [.yuniary 21. 19n6 VOLATILE ORGANICS BY PURGE AND TRAP By GC/MS - HEADSPACE Compounds detected In parts per million (milligrams/kilograms) dry weight basis, CHLOROMETHANE BROMOMETHANE -- VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE • ACETONE -- - • 1,1-DICHLOROETHYLENE -• 1,1-DICIILOROETIIANE t-l,2-D|CHL0R0ETIIYLENE CHLOROFORM 1,2-DICIILOROETHANE t-BUTYL METHYL ETHER - - I,I,1-TRICHLOROETHANE - CARBON TETRACHLORIDE - - BROMODICHLOROMETHANE - - _ND _ N n _ _NI)_ _NIL_ _NIL_ _NI)_ _N|)__ JJIL_ _NI)__ _NIL_ -Nl)_ JIII— _Nn_ -NIL_ _NII_ 1,2-DiCIILOROPROPAIIE c-1 ,3-DirillOROPROI'LNE - - - t - 1 , 3 - 0 1 CIII OROI'ROPfNE - - - TCE (TRICIII OROLrilYI.ENE)-- I ,1,2-TRICIII OROETHANE - - - DIBROHOCHIOROMETHANE BENZENE DIISOPROPYL ETHER 2-Clil.OROETIIYLVIIIYL ETHER • DR'OMOFORM 1 .1 , 2, 2-TETRACIII OROETHANE PCE (TETRACHLOROETHYLENE) TOLUENE CHLOROBENZENE ETHYI.DENZENE NP N P _ Nil Nl) l l l ) _ __N|) _ _ N P Nl) l-JU N U _ Nl 111 NU_ NU_ NU_ SIIRUOCATI': RKCOVI'.ltlKS tl-^ motliylene c h l o r i d e 66% n/i% LT=Less Than, GT=Greater Than, ND=Not Detected dwb=Dry Weight Basis d.. t ( i l i i e i \ e II I ' l l 59% For the above listed Volatile Pollutants, nothing delected at a sensitivity level of 0.02 m(;/k|>,(ppm) iluli. Other compounds deled ud: . I . INDIl^fia^/l. jltil^KJION^I.ANACLUKNT, INC. //k^y/ yyn't-<- • ~J li' i t>j o H <T» VO VO L I INDUSTRIAL CORROSION MANAGEMENT INCORPORATED 1152 ROUIE 10. HANOOlhl. NEW JERSEY 07669 201 i a i 0110 t 1 I. r •;;. t it i, NJDEP C e r t i f i e d D r i n k i n g W a t e r / W a s t e w a t e r L a b o r a t o r y ID / y i ' i l 16 REPORT DATE: M.ircli 1 0 . 1 9 ( 1 6 ^ LAD .// r?./,()<} ) i ' l n v CLIEHT;_EHV.iRO_SGIENCES-JNn.^_Ialaiid_Ghei!ilGflLCQn)nnny_PcQj£ct SAMPLE in:_j;_7 SAMPLE DATE: pciiruai:x_l5-^lQf]6_SAMPIfD BY: Alan.Kyles AT IAD OATE: l / . i | . n i n r v 2 1 . 19R6 VOLATILE ORGANICS BY PURGE AND TRAP By G C / M S - H E A D S P A C E Compounds d e t e c t e d I n p a r t s p e r m i l l i o n ( m i l l i g r a m s / k i l o g r a m s ) d r y w e i g h t b a s i s i CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE 1,1-DICHLOROETIIYLENE -• 1,1-DICIILOROETIIANE t - l , 2 - D | C I I L O R 0 E T H Y L E N E CHLOROFORM 1,2-DlCHLOROETIIANE t-BUTYL METHYL ETHER - - 1,1,1-TRICIILOROETIIANE - CARBON TETRACHLORIDE - - BROMODICHLOROMETHANE - - _ _ N I ) NU NU ND NU NU NU NU NU ND ND ND J I L ..NIL ND 1,2-DICIII.OROPROPANE c - 1 ,3-DICIIIOROI'ROIMNE - - - t - l ,3-DICIIIOROPROPLNE - - - TCE (TRICIII OROLTHYIENE)-- 1 ,1 , 2 - T R I C I I I OROETHANE - - - DIBROMOCIIIOROMETIIAIIE BENZENE DlISOPROPYL ETHER 2-CIII.OROETIIYI.VINYI. ETHER • BROMOFORM 1 ,1 ,2,2-TETRACIII.OROETHANE PCE (TETRACHLOROETHYLENE) TOLUENE - - CHLOROBENZENE ETHYLBENZENE _ND_ _NP_ _N!L J!!L J U L _N!L _m_ J!!}_ -NIL -NIL -till, -.NIL -!IP_ .NIL ND LT-Less Than, GT=Greater Than, ND=Not Detected dwb=Dry Weight Basis SURROGATE JIKCOVI'lt I MS: .Ij metbylene chloride - 111% •'ll ^ " ' RKll - ( I . t o l u e n e - 126% X F o r t h e a b o v e l i s t e d V o l a t i l e P o l l i i l a n l s , n o t h i n g d e l e c t e d at a s e n s i t i v i t y l e v e l o f 0 . 0 2 mB/l<i;(ppm) d u b , X O t h e r compounds <'elec l e ( l : | | y d i - o c / j i |io|!_llT._^^LI!l|ll,_!J|!IU!}!<.._Oi !> .!!!li/!^i:(ll'.'!;..' I ! . ' I Y . ! ! ' J l ! ! ! ! u ) _ J '1 im\\'.i7i<\Zf.A.i]nny\(fii 'MANACEMENT, INC. iii;i/Ruf: cimuYimi MAI ////(Uy y J/,At. / . i . I CO o H • J o o ;^;i'i INDUSTRIAL CORROSION MANAGEMENT INCORPORATED IIS2 ROUIE 10. RANOOini. NEW JERSEr 07)69 201 i64 OUO NJOEP Cert ified Drinking Water/Was Iewater Laboratory ID Al'il 16 ,.y/z REPORT D A T E : _ j j a r c b m . 1906 ' " LAO i --,2/.70 :••• -• CLIENT; ENVTRO SCTENCES. TNC. - Tslnnd Cbemical Compnny P r o l e c t SAMPLE ID: C-D SAMPLE DATE;Kebninrv 19. 19n6 SAMPLED DY; ^Xnn__KyJ[es AT LAR DATE: F e b r u a r y 2 1 , 1906 VOLATILE ORGANICS BY PURGE AND TRAP By GC/MS - HEADSPACE Compounds d e t e c t e d In p a r t s p e r m i l l i o n ( m i l l i g r a m s / k i l o g r a m s ) dry weiglit b a s i s , CIILOROHETIIANE - BROMOMETHANE VINYL CHLORIDE CHLOROETHANE HETHYLENE CHLORIDE ACETONE --r--- 1,1-DlCIILOROETHYLENE - 1,1-DICHLOROETIIANE t-l,2-DICHLOROETHYLENE CHLOROFORM - - 1,2-DICHLOROETHANE t-BUTYL METHYL ETHER - - 1,1,1-TRICIILOROETIIANE - CARBON TETRACHLORIDE - - BROHODICIILOROHETIIANE - - NP N!) _ _ N P _ i l P NP NP _:_NP N P _ _ NP NP NP Nl) . NP N!) I,2-DICHIOROPROPANE c - 1 ,3-DICIIIOROI'ROI'ENE - - - t - l , 3 - P I C I I I 0 R 0 P R 0 P E N E - - - TCE (TRICIII OROETHYI E N E ) - - 1 ,1 ,2-TRICin.OROETIIANE - - - DI OROHOCIILOROMETHANE DEN2ENE - - - DIISOPROPYL ETHER 2-CliLOROETiiYLVINYL ETHER • BROMOFORM 1,1,2,2-TETRACHLOROETIIANE PCE (TETRACHLOROETIIYLENE) TOLUENE CHLORODENZENE -- ETHYLBENZENE _Np_ _L'P_ _.N|L -NIL _N|L _N!L -L'lL -MIL -NP_ -NIL -NP_ -NP_ -NP_ -NIL Nl) LT=Less Than, GT=Greater Than, ND=Not Detected dwb=Dry Weight Basis SIIUHmWiTE KI'COVKUIKS: dj methylene chloride d. toluene - 72% HI'11 - 5y/. 10/,% X For the above listed Volatile Pollutants, nothing detected at a sens i t i v i I y ii:vi;l of O.DZ mi;/k(;(p|im) dub Other compounds detected: \ •_ ^ ^ 1II0II.;^IIIAK ('-(Wm:.il)U IJANACKMKNT, INC. I, J fc.:.,. ili i . ^ INDUSTRIAL CORROSION MANAGEMENT INCORPORATED 1162 ROUIE lO.RAMOOU^I. HEW JERSEY 07669 201 661 0330 L 15 I'l w o i-» ~ j o NJDEP Certified Drinking Water/Wastewater Laboratory ID ,^l'il 16 REPORT nATE:_^|;,^.ci,_in._10Q6. IAD f__s:j/,/| CLIEHT: ENVTRO SCTFNCIl.S TNC. - Tiilnnd Cbemical Conipnny P r o j e c t SAMPLE 10: j j - i j • SAMPLE DATE:_Fei>iugE^_[9^i9fi6_SAMPLED DY: .Alfln_KyIfi2 ^AT IAD DATE: February 2 1 . 19R6 VOLATILE ORGANICS BY PURGE AND TRAP By GC/MS - HEADSPACE Compounds d e t e c t e d In p a r t s per m i l l i o n ( m i l l i g r a m s / k i l o g r a m s ) dry weight b a s i s , CIILOROHETIIANE BROMOMETHANE VINYL CHLORIDE - CHLOROETHANE METHYLENE CHLORIDE ACETONE --• 1,1-DICHLOROETHYLENE -• 1,1-DICIILOROETHANE t-l,2-DICHLOROETHYLENE CHLOROFORH --- 1,2-DICHLOROETHANE t-BUTYL METHYL ETHER -- 1,1,I-TRICHLOROETHANE - CARBON TETRACHLORIDE -- BROMODICHLOROMETHANE -- _N!L_ _N!L_ „NP_ INP_ _NP_ _NIL_ -NIL- -Nil- M ) - .Nl)_ M\— - N n _ .ND_ .NU_ 1,2-Dirill OROPROPANE c-l,3-DICHI0R0PR0PENE - - - t - l ,3-niCIII.OROPROPENE - - - TCE (TRICIII OROETHYI EHE)-- 1,1 ,2-TRICIII OROETHANE DIBROMOClll OROMETHANE BENZENE DlISOPROPYL ETHER --- 2-CIIIOROETIIYI.VINYI. ETHER • BROMOFORM 1 ,1 ,2,2-TETRACIII OROETHANE PCE (TETRACIIIOROETIIYLENE) TOLUENE - - - - - -- CHIORODENZENE ETHYLBENZENE NIL ' N I L -NIL ..NIL ND _Nn AllL _-NP_ -NIL -NIL -NIL -NP_ -NIL -NIL ND LT=Less Than, GT=Greater Than, ND=Not Detected dwb=Dry Weight Basis SIIKimCATE HECnyr.ltlES: (bi m e t b y l e n e c b l o r l . l e I iieiu 611% 102% d . t o l u e n e - 76% IIFII For the above l i s t e d V o l a t i l e P o l l u t a n t s , n o t h i n g d e t e c t e d al a s e n s i t i v i t y level o f 0.02 m|;/kt',(ppm) di;b. Ol her compounds de I ec I e d : \ ; IMnnc'Ti/. /TT-iv;;:: INDUSTRIAL CORROSION MANAGEMENT INCORPORATED ll32ROUIf 10. RANDOini. NEW JERSEr 07669 201 Sai 0}30 NJDEP Ceriified Drinking Water/Wastewater Laboratory ID /'I'll 16 REPORT DATE LHarcb J0._19L1(L IAD II r,?/,7T CL I ENT; ENVTRO SCTBHCE.S. T^C. - Tslnnd CheiHlcnl Company Pro | cct SAMPLE I P:._j;-I I SAMPLE DATE: February 19. I9ft6 SAMPLED BY: Al nn Kyles AT IAR DATE: Februnry 21, I9R6 VOLATILE ORGANICS BY PURGE AND TRAP • By G C / M S - H E A D S P A C E Compounds detected In parts per million (milligrams/kilograms) dry weight basis. U) o M o lO CIILOROHETIIANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE HETHYLENE CHLORIDE ACETONE - 1,1-DICHLOROETHYLENE -• 1,1-DICIILOROETIIANE t-l,2-DICHLOROETHYLENE CHLOROFORM - 1,2-DICHLOROETIIANE t-BUTYL METHYL ETHER - - 1,1,1-TRICHLOROETIIANE - CARBON TETRACHLORIDE - - BROMODICHLOROMETHANE - - . N P _ . N l > _ . . N l l _ J ^ l l _ _NL _ N U _ _ N U _ _ N U _ . - N U _ -Na__ JJU__ J i n _ _ND_ _NI)_ ND LT=Less Than, GT=Greater Than, ND=Not Detected dwh-'Dry Weight Basis 1,2-DICIILOROPROPANE c-l,3-DICIIIOROPROI'ENE - - - t-l,3-DIClliOROPROPENE - - - TCE (TRICIII OROETHYI ENE)-- 1,1,2-TRICIU OROETHANE - - - DIDROMOCIII.OROMETIIANE DEN2ENE DIISOPROPYL ETHER -- 2-CIIIOROETIIYLVINYI. ETHER • BROMOFORM 1,1,2,2-TETRACIIlOROETHANE PCE (TETRACHLORflETHYLENE) TOLUENE CHLOROBENZENE ETHYLDENZENE __NI1 _ N | ) __LJ|) __NP Nl) __N1) NO _ N U _ N U — N i l Nil Np iip Nl) un -WATER SIIUUOCATE RECOVER I K.S: i\-^ m e t b y l e n e c l i l o r i d e - T l ) [ % " 173% d.. t o l u e n e It I'll 16T% X For the above l i s t e d V o l a t i l e P o l l i i l a n l s , n o t h i n g d e l e c t e d at a s e n s i t i v i t y I r v d o f s iij-./l (ppli)-wiii ei (1. I mc/l^;(|'|"") " "n I I Oilier compoiiiuls del ec I ed: _^ UYi iNi)ii.';;yi( /i iLyin/vi. cnHHO?;iijN HANACF.MFNT. mc. ////k f. /y{ k 1-^ k - • • • & • » . ..b »1 * , :|l • # b I Jl. INDUSTRIAL CORROSION MANAGEMENT INCORPORATED IIS2 ROUIE IO.IUlHDO(rtl.UIWJERSElD7l69 201 3I««]30 n L'J SAMPLE SOURCE: ENVTRO SCIENCES SAMPLE DATE: February 19. 19R6 State C e r t i f i e d Drinking Water/Wastewater L a b o r a t o r y ID # l ' i l l 6 REPORT 0 A T E : _ A i . r l L ^ L _ 1 9 ( i 6 LAB y}'__5/LS0i SAMPLE ID ••_Cn!!!|!0!iJ te_nC C-6 .'md (;-7 TAKEN D Y : _ A U < y i < l « . AT LAB DATE : Fel.runry 2 1 . I9D6 KEACriVATEl) DATE: A p r i l 10. 1906 EP T O X I C I T Y TEST l e a 9 b ? . l S _ A n a l v 5 ] s J C F R _ y o l _ . J i 5 , _ N o . 3(1) PARAMETERS TESTED I n o r g a n i c Chemicals by AA A r s e n i c Barium Cadmium Chromium Lead Mercury Selenium S i l v e r - TEST as I.T 0 RESULT mg/l .005 1.2 I.T 0 I.T fl 0 I.T 0 I.T 0, I.T 0. .02 02 2/. 010 OOS 01 MDI, I.T (I.DO'i I.TJ).;| 1:0:.!?L l.'rj).D2_ l,TJ).D6 j . l M ) . ()I () 1,'r 0,1)02 I.T 0,0) METHOD MAXIMUM PERMISSIBLE !!!:^i^!^ Concerit r a t jon as mo/1 I.T 0,005 5.0 I.T 0.5^_ 100.0 l.r 0.02 1.0 l.r 0.02 . 5.0 br_().oi6_ 5.0 l.r 0.010 0.2 i.rj)j^05 ' - 0 l.r 0.03 5.0 //////////////////////////ii/////i//////////////////////////////////////////////^^/^/^/^^^/^^^^^/y//^////^//yyy^y All r e s u l t s a r e r e p o r t e d In m g / l ( p p m ) , u n l e s s o t h e r w i s e s t a l e d . o •J o to W e t h a n k y o u f o r t h i s o p p o r t u n i t y to s e r v e y o u q u e s t i o n s , p l e a s e d o n o l h e s i t a t e to c a l l . RSL'dlh e n c I . If y o u h a v e a n y V e r y t r u l y y o u r :• , I N D U S T R I A L C O R R O S I O N H(;HT.,INC kycA:^J>y k>- kiZi^c-,.,&./ Rlclinnf S. I.evliie • k / / , Preaident ^•^ \ V.-- oc- ^I|J OP CUSiODY RECORD ^ p, _^ ^„ I n s c a i l a t i o n : _/.'•<r.^y/; (Zi-yyr.-o't. <^r7r/?.rrv' S u r v e y N o . : C S t a C i o n L o c r j c l o n .. •/ .'.z^-.iy y ^ r . z y-^ 1 ' y V ^ i\ i m p l e r s : '.yo't \.: y / z y T— • / ; S a m p l e r s : ( S i g n a t i u r e ) y D a c e Time ! U 0 3 p . i u r a o l.j_ Zl /A/y/Z-^yk 'A-y-^y- z - / I.'. 'y--:'-'..' y- ..• .'^/Z' < . • • - i y . y i t f 1 y y y ^ z y - y y y ^ y ; • ' , ' ' ,.-'.C' y . ' y y'^y^-i y . - i R e l i n q u i s h e d b y : ( S i g n . ) z/^^.y y^.kkykyy 1 • • T l c i i n q u j . . s l i e a b y : ( . i l ^ n . ) R e c e i v e d b y : ( S i g n . ) Iba e e / T i m e R e c e i v e d b y : ( S i g n . ) O a c e / l ' l n i r : Rec e i v e t i by : K S i g n . ) Da ce / T i m e R c i i n q u i s h e a by : (. S i g n . ) R e l i n q u i s h e d b y : . ( S i g n . ) R e c ' d by L a b o r a c o r y j D a c s / T i . ' n e f o r f i e l d a n a l y s i s ( S i g n . ) D i s p a c c h e d b y : ( S i g n . ) D a c e / T i m e R e c ' d f o r L a b o r a c o r y par. e / T i m e b y : n. {j. f u<—- W ' - r Mechod o f S h i p r a e n c /; / . / • ^ • . ' ' • / • ' 301704 'V^^fl?(^ <k^o6 Pry C y - I 18 CC*^LANO TO.. D€MVIU-E. NEW JtSSEY 07JJ4 CHAIN OP CUSTODY RECORD Installacion:^^^^ ^ ^ k ^ r ^ ^ y k ^ ^ / i ^ Survey No . : c £ tn Station Location Saaplers: (Signature) zy iZAi^^ A D a t e .ne S a = p l e T y p e i - o : : p . i i j r a 0 j ^ zz^ r^ar-v y z .'^cZ A^'k^-f^A^^yZy. yh-f > ^^te» ya > Z ^ Ak^y-y yZZZtk V ,<S^ yo N; k-f\ yyt^y^TkAj V y A ka (Z-y y/y^-^y/k^ \ y y /o o \ k-^'^ //Zk^yy^ y y t ^ ^ - ^ y ^ y Relinquished by: (Sign.) Rei.inquis2ie^d. by: C Sign . ) Received by: (Sign.) Date/i Reiinquisned by: (Sign.) Received by: (Sign.) Dace /- Relinquished by: (Sign.) Received by:(Sign.)Dace/ Rec'd by Laboracory (Dace/ for field analysis (Sign.) Dace/Time R e c ' d f o r L a b o r a c a r y Method of S h i p m e n t : 77 D a c e / 301705 (^. .iir ,' rcT'i-ii rz^Les pk CHAIN OP CUSTODY RECORD z'. • ^ J\ 19 CCPSLANO HO.. D€XV1UL£. NEW je.=!Srr 07S14 Installation: y ^ . y ^ • y Survey No . : OJ .—1 a. e K3 a CO x: Station Location Samplers: (Signature) Date Tiae S a .-2 p i s T V p e! Losp.r u r a o C rL /yZ^^..yyAZAkyj G^ ^ ^ 1 y^ A9yy^At • y y y yy/,^ y 1 y Relinquished by: (Sign.) RexinquiS'hea by: (Sign. ) Rexinquisnea by: (Sign.) Relinquished by: (Sign.) •yy y y . - ^ y ^ y y Dispatched by: (Sign.) Received by: (Sign.) Date/Tiae Received by: (Sign.) iDate/Tiae Received by: (Sign.) Dace/Tiae Rec'd by Laboracory Date/Tiae for field analysis (Sign.) Date/Tine Rec'd for Laboratory by' Mechod of Shipment: D a t e / T i c e <v ^ y . 301706 . I / - M LU CO. ..-iOSION MANAGEMENT INCORPORATED NJDE? C^.r:. .ed Drir.kir.s V£r = r/:;£s:2--a: Laboracory ID;/ 14116 REPORT DATE: Mav 2. 1986 LA3 f?. 5 3581 1152 SCUTE 10. RANOOlPH. NEW JESSEV 07369 201-53--0230 CLIENT: E^TVIRO SCIENCES INC - I s l a n d Cher.ical P r o j e c t SA:-1?LE SOURCE: Tank U SAINPLE DATE: March 12, 1986 TAKEN 3Y: A. Kvles AT LAB DATE: y.arch 20, 19:6 LABORATORY ANALYSIS REPORT =ARA:-!E-ER RESULT Eenzoauinone 30' siuorenone 70% If you should have any quescions, please do not hesicace co call. INDUSTRIAL CORROSION MANAGEMENT, INC. (ichard S./Lev^fie Presidenc RSL:dlh 301'70'7 INDI TRIAL CORROSION MANAGEMENT INCORPORATED 1152 ROUTE 10. RANDOLPH. NEW JERSEY 07869 201-3J4-O230 iVJDE? Cercified Drinking Vacar/^Cascavata; Laboracory IDi-' 14116 REPORT DATE: M.av 2. 1986 LAB it 53582 CLIENT: ENVIRO SCIENCES INC. - Island Cheaical Proiect SAMPLE SOURCE: Tank 7 SAMPLE DATE: March 12, 1986 TAKE:'; 3Y: A. Kyles AT LAB DATE: :-terch 20. .A-BORATORY .ANALYSIS REPORT ?.i^A:-!ETER RESLT-T Benzophenone — Fluorenone Unknown Alkane 39.6" 43.8" 16.62 If you should have any quescions, please do not hesitate to call. •'; INDUSTRIAL CORROSION M.ANAGEMENT, INC. Richard S. President .eve;ne RSL:dlh . - •-*! - .r- 301708 INDU^.RIAL CORROSION MANAGEMENT INCORPORATED NJDE? Certified Drinking Vaca: Laboracory ID;/ 14116 REPORT D.ATE: Mav 2, 1986 LAB it 53533 •>aj cava car 1152 ROUTE 10. RANOOLPH. NfiV JERSEY Q73S9 201-52<S-O320 CLlENT: Ey.'IP.O SCIENCES INC. - Island Cheaical Proiect SAMPLE SOURCE:- Tank SA_MPLE DATE: March 12. 1986 TAKEN BY: A. Kvles AT LAB DATE: M=rch 20. 1^=6 -ABORATORY .ANALYSIS REPORT P.AR.AMETE?. RESL'L'; Benzophenone Fluoenone -r— iD . / /. 14.3% If you should have any quescions, please do noc hesicace co call. INDUSTRIAL CORROSION MANAGEMENT, INC. Presidenr RSL:dlh 301709 y. J .UK; 11 r-ULLUirtiNi V U L A T i L t UKbnN. ANALYSIS LABORATORY ID #14116 LAB i? 53583 PARAMETER Chloromethane Bromomethane Vinyl Chloride Chloroethane , Methylene Chloride 1,1-Dichloroethene 1,1-Oichloroethane Trans-1 ,2-Dichloroethene Chloroform 1,2-Dichloroethane 1,1,1-Trichloroethane Carbon Tetrachloride Bromodichloromethane 1,2-Dichloropropane Trans-1,3-Oichloropropene --• Trichloroethene Dibromochloromethane 1,1,2-Trichloroethane Benzene cis-V,3-Dichloropropene 2-Chloroethylvinyl ether Bromoform Tetrachloroethene 1,1,2,2-Tetrachloroethane --• Toluene Chlorobenzene Ethylbenzene Total Xylenes *Dichlorobenzenes noc analyzed under chis mechod ' CLIENT: ENVIRO SAMPLE SOURCE GC/MS Method 624* Tier II Deliverables _ SCIENCES INC. - Isla-r: Tank 8 RESULT ug/ kg U U u U u u u U U u u TI n u TT u - u U u u u U u u 8000 u u u METHOD BLANK ug/kg U u u . T7 rr TT T- U IT U r' IT U tT u u u u u u u u u u 2. 7J U U U Che-icai MDL ug..'kg 100 100 1 nr\ ino 1 on 100 • '"r i ' 100 1 on lOQ 1 on • ^ 1 no 100 100 100 100 100 100 - 100 .100 100 100 100 . 100 100 100 100 100 Analyzed by GC/MS Mechod 625. INDUSTRIAL CORROSION MANAGEMENT, INC. 301710 INDUSTRIAL CORROSION MANAGEMENT INCORPORATED U52 ROUTE 10. RANDOLPH, NEW JERSEY 07869 201-58-:-0230 NJDE? C a r c i f i e d Drinking Wacar/Vascavace: Laboracory ID;/ 14116 REPORT DATE: Mav 2, 1986 LAB •? 53584 CLIENT: EN'VIRO SCIENCES INC. - I s l a n d Cheniical Proiect SA:-IPLE SOL-RCE: Tank 9 SAI-:PLE DATE: March 12, 1986 TAKZN BY: A. Kvles AT LAB DATE: March 20. 19S6 LABORATORY ANALYSIS REPORT '.IRAI-IETER RESLT.T p-Pheneridine 89. 1% Unknown arcsacic M'.v'=217 10.9% If you should have any quescions, please do noc hesicace co call. INDUSTRIAL CORROSION MANAGEMENT, INC Richard S .^Lavine President RSL:dlh 301711 # lh l'j INDUSTRIAL CORROSION MANAGEMENT INCORPORATED REPORT DATE: Mav 2, 1986 LAB it 53589 1152 ROUTE 10. RANCOLrH. HVN JERSEY 07859 201-:a4-02;0 CLIENT: E^TVIRO SCIENCES INC. - I s l a n d CheTnical P r o i e c t SANIPLE SOURCE: Tank U LABORATORY .ANALYSIS REPORT P.ASAM-ETER RESULT Benzophenone 64.8% . Fluorenone 35 . 2% If you should have any q u e s c i o n s , p l e a s e do noc h e s i c a c e to c a l l . INDUSTRIAL CORROSION M-ANAGEMENT, INC Rf chard S. LflZiii& P r e s i d e n t RSL:dlh (3 NJDE? Carcified Drinking Wacer/Vascevaca: Laboracory IDi/ 14116 SAMPLE DATE: March 12, 1985 T.AKZ:'; BY: A. Kvles AT LAB DATE: March 20, L = = - 301712 ts^ / ^ ,• y / r - t C H A I N OF C U S T O D Y 'j:r>c : ^ sczTtCZS inc. > • • - ' • • " • 3 6 6 - 6 2 5 5 Sena fleoprt To: y ^ y y ^ ^ J c y j y ^ C t ^ y y y y c r x . u i l a t i tion: ySCiP^y/y y/yyyyryen,^ <^c-yjr<S<Zy) ..Tiolinq Series: (ZAiy.'-t.J yct-r/tr,.-^ Samoieris) Nane: y<<:r:^y y . yr^yy.- I b i g r a :ij.-s: X:.. y yz-^. y y ^ t ^ y f f y ^ mole Identification Samoli ng Location Point Samel ing Gate Samoling Time Samole Tyoe Analysis Come. Graa Recuirec No. C I v-cr. ; a i n e r s <' ."/<- 9 ^ /yy^AA f'Z /<p-/2. y>^ y /<i- / y.d~ I '' p 1 1 ry ' / \ j ^ y ' AO 1 1 '/ 1 t ! - 1 X y y \c<?~ .J,(X— 1 / \ A ^ .z<y ^ \. £ i / ! '^ / / / / /<? A^ y. 'i'/- ^/ /<y • < i oy.Tiy eiinauisnea 3y: CSign.3 ;eiincuisnec 3y: CSign.] Receivea 9y: CSign.] Gate/Time 1 1 Receivea By: CSign.] Date/Time leiincuisnec- To L a o o r a t o r y ay: (Sign.3 Receivea For Laboratory Sy: (Sign.) C ate/Time 4 e i n o a Of Relincuisr.ment: Name Of Laooratory: ANALYSIS Rg.QUIPgD out cooe m prooer column] Priority ooilutant^--lO: Petroleum hyarocaroons: Volatile organics CGC]: Volatile organics CGC/MSh ,Cyanides: CODE I ANAL'^'SIS CCCS i A N A L ' ^ S I S COOE I ANAL'^SiS CCCE 01 02 03 ( ^ 05 Nickel: Chromium: Arsanicr Coooer: Laad: Mercury: Antimony: 06 07 08 09 10 1 1 12 Zinc: Cadmium: Selenium: Silver: Barium: COO: BOO: 13 14- IS IS 17 18 19 301713 ^01 PRK FY POLLUTANT VOLATILE ORGANIC / LABORATORY ID il4116 LAB it 53362 . .YSIS r CLIENT: E^rviRO SCIENCES - I s l a n d Che- SAHPLE SOURCE 0 8 5 - 2 5 1 - E S I '" ac GC/MS Method 624 * T i e r I I D e l i v e r a b l e s METHOD PARAMETER RESULT BLAMK MDL SPIKE DUP SPIKE RPD ug/kg ug/kg ug/kg Chloromethane u u lo 200 ; Aj, 33 oromomethane L^ U 10 2-0 19; ?: Vinyl Chloride u u 10 156 127 . "tt~ Chloroethane u U 10 44 LL: CQ Methylene Chloride u 7 .:J 10 122 lOL T ^ 1 ,1-Oichl oroethene '• - u U 10 90 9; T " ; 1,1-Oichloroethane u u IQ 90 L-:6 Tg^ Trans-l ,2-Dichlcroethene U U 10 105 11: y _ Chloroform • U 7.3 J 10 IQ6 119 1,2 1,2-Oichloroethane U U 10 106 132 22 1,1,1-Trichloroethane U U 10 112 121 7.7 Carbon Tetrachloride U U 10 104 131 39 Bromodichloromethane U U 10 98 153 44 1,2-Oichloropropane U U 10 104 116 g Trans-1 ,3-DTChloropropene U. U 10 104 12G L4 Trichloroethene U U 10 125 132 4.7 Dibromochloromethane U U 10 118 137 15 ,1 ,2-Trichloroethane U U 10 96 125 26 Benzene - U 2.0 J 10 ' 100 105 ^ _4_^ cis-1 ,3-0ich1oropropene U " U 10 10^ 11= 13 2-Chloroethylvinylether U U LQ 102 119 15 Bromoform U U LQ 98 U4 38 Tetrachloroethene U U 10 114 72 45 1,1 ,2,2-Tetrachloroethane U U 10 76 58 15 Toluene U 4.9J 10 102 65 44 Chlorobenzene U U 10 104 116 11 Ethylbenzene - U U 10 114 110 • _3_J Total Xylenes - — U U 10 130 115 12 *Dichlorobenzenes noc analyzed under chis mechod. Analyzed by GC/MS Mechod 625. 3 01714 1 • f. i'l PP'ORITY POLLUTANT VOLATILE ORGANIC ANALYSIS LABORATORY ID #1 41 U LAB # 53363 CLIENT: ENVIRO SCIENCES Island Cha-ic2! ?: SAMPLE SOURCE 085-252-ESI GC/MS Method 624* Tier I I Deliverables PARAMETER Chl oromethane Bromomethane Vinyl Chloride Chloroethane Methylene Chloride • 1 ,1 -Dichloroethene. 1 ,1-Oichloroethane Trans-1,2-Dichloroethene Chloroform 1 ,2-Dichloroethane 1 ,1 ,1-Trichloroethane Carbon T e t r a c h l o r i d e Bromodichloromethane 1 ,2-Oichloropropane Trans-1 ,3-Oichloropropene . Trichloroethene Dibromochloromethane '• . 1,1 ,2-Trichloroethane Benzene , cis-V,3-Dicnloropropene 2 - C h l o r o e t h y l v i n y l ether = Bromoform Tetrachloroethene 1 ,1 ,2 ,2-Tetrachloroethane ^ Toluene Chlorobenzene Ethylbenzene Total Xylenes *Dichlorabenzenes noc analvzed under chis mechod. RESULT ug/kg u u 153 HETriOD BLANK ug/kg u f * U y 7 07 4.9- MDL ; g ; Q To" 10 10 • c To' IQ 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 Analyzed by GC/MS Method 625. 301715 -^ PP^ORITY POLLUTANT VOLATILE ORGANIC ANALYSIS LABORATORY ID 11411. LAB i 53364 CLIENT: zyviRO SCIENCES - Icland C-^-ical ?- SAMPLE SOURCE 85-252-E5I k__ GC/MS Method 624* Tier II DelIverabl es PARAMETER Chloromethane Bromomethane Vinyl Chloride — Chloroethane Methylene Chloride 1 ,1-Oichloroethene 1 ,1-Dichloroethane Trans-l ,2-Dichloroethene Chloroform 1,2-Dichloroethane 1 ,1 ,1-Trichloroethane Carbon Tetrachloride Bromodichloromethane 1 ,2-Dichloropropane Trans-l,3-Dichloropropene - Trichloroethene Dibromochloromethane 1 ,1 ,2-Trichloroethane Benzene cis-V,3-Dichloropropene 2-Chl o r o e t h y l v i n y l e t h e r Bromoform Tetrachloroethene 1 ,1 ,2 ,2-Tetrachloroethane Toluene Chlorobenzene — Ethyl benzene — Total Xylenes *Dichlorobenzenes not analyzed under chis mechod. RESULT ug/kg S.-3 U 4.4B U 2.SJ U HETriOD BLANK ug/kg T: "JHT 4.9J MDL 10 10 10 10 10 •0 JJL JJL l.Q 10 10 10 10 - 10 10 10 10 10 10 10 10 10 Analyzed by GC/MS Method 525. 301716 . 1 . \ j r : . ' i i PULL'J I rtit I VQLATiLE ORGAN" LABORATORY ID #1 41 ,, LAB i 53365 ANALYSIS CLIENT: ENVIRO SCIENCES - Island Che=ical Pro- SAMPLE SOURCE 08?-2' •-3i- e.c: GC/MS Method 624* Tier II Deliverables , PARAMETER Chloromethane Bromomethane Vinyl C h l o r i d e • Chloroethane Methylene Chloride • 1 ,1-Dichloroethene 1 ,1-Dichloroethane Trans-1 ,2-Dichloroethene ; Chloroform 1 ,2-Dichloroethane 1 ,1 ,1-Trichloroethane Carbon Tetrachloride Bromodichloromethane 1,2-Dichloropropane Trans-l,3-Dichloropropene ; , Trichloroethene Di bromochloromethane 1,1 ,2-Trichloroethane Benzene • ci s-l",3-0ichl oropropene 2-Chl oroethyl vinyl ether —'• Bromoform Tetrachloroethene 1 ,1 ,2 ,2-Tetrachloroethane Toluene Chlorobenzene Ethyl benzene • Total Xylenes *Dichlorobenzenes noc analvzed under this method. RESULT ug/kg U a Q T5 METHOD BLANK ug/kg U 2.0J 4 Q T MDL 10 1 n To" 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 Analyzed by GC/MS Method 625. 301717 r-k Tk\ ''RITY POLLUTANT VOLATILE ORGANI-- LABORATORY ID #14116 LAB # 53366 NALYSIS PARAMETER Chloromethane Bromomethane Vinyl Chloride Chloroethane Methylene Chloride 1,1-Oichloroethene 1,1-Dichloroethane Trans-l ,2-Dichloroethene Chloroform 1,2-Dichloroethane 1,1,1-Trichloroethane Carbon Tetrachloride Bromodichloromethane 1,2-Oichloropropane Trans-l ,3-Oichloropropene --• Trichloroethene Dibromochloromethane 1,1,2-Trichloroethane -• Benzene cis-V,3-0ichloropropene 2-Chloroethylvinylether Bromoform Tetrachloroethene 1,1,2,2-Tetrachloroethane — Toluene Chlorobenzene Ethylbenzene Total Xylenes *Dichlorobenzenes noc analyzed under chis method CLIENT: ENVIRO SCIENCES - I s l a n d Che---; , 1 o - . . .; SAMPLE SOURCE 0 8 5 - 2 5 5 - E S I GC/MS Method 6 2 4 * T i e r I I D e l i v e r a b l e s RESULT ugAs U JJ _ _ . « . M « . ^ . . _ _ _ ^ . . TT . . — — — .— ».» — — * . * . . _ TT „ ,.,3 '.„• ., ^ L — / —. 3 . a a , "~~ " " u . u L ~ " ~ ]j u - - - - - - - - - - - - - - - - ^ u . - - - - - - . _ . _ - - . . - u . _ - y - - — - - - - _ _ - - - - _ _ - jj - - - - - - - - - - - - - - - - y — — — — — — — — — — — — — — — — TT - - - - - - - - - - - - - - - - \J — — — — — — — — — — — — — — — — TT — — — — — — — — — — — — — — — — TT — — — — — — — — — — — — — — — — TT - - - - - - - - - - - - - - - - u . — — — — — — — — — — — — — — — — 7T . - - - - - - - . - - - - - - - - n METHOD BLANK ug/kg IJ U 'A : . 2.., w z i j 7 . 3 J U ;• TT :: :T U TJ U 2 . 0 J u U U U u 4 . 9 J U U U MDL " n • 0 ^ ' j • ~ • 10 IG . ,-v 10 10 10 10 10 10 10 10 •-' 10 10 10 10 10 10 10 10 10 Analyzed by GC/MS Mechod 62; 301718 C H A I N OF C L ' S T C D Y lAO-^Ozz-' ' • i i ^ i ^ w ^ 3 6 6 - 5 2 5 5 m0amm>m^m Send Reo.ort T o : '• y ^ ^ y y./Ay y<Ay ' i l l a t i o n : m o l i n g S e r i e s : y ^ y - y / / C y y f SamolerCs) N a m e : 2 1 5.-;a ture: / ^ £ V / y<k/yc^ ^ . . / m o l e iGenti f ica tion S a m o l i n g L o c a t i o n P o i n t S a m o l i n g Gate S a m o l i n g T i m e S a m o l e Type C o m ; Grao A n a l y s i s R eouirec - y - y . y / - ^ - ^ . (Aiy. y z /^y/k/jz I ^ y ^ > <r^ ' - - ^ ^ C 2 A^yr- Z^-y yy y-zS'- cS / .y- y y cc X cy. N o . C ! C c . - : a i n e r s y y A^ -y-^s^-yzr 'y-s-r-yr y.yiyk/^ y y - y y y ^y y y<: ^ y c 1 ^' c ^ 1 ^ V$. z^ e i i n o u i s n e o 3 y : ( S i g n . ] A N A L V S I S PEOUIRED out c o o e in p r o o e r c o l u m n ] P r i o r i t y pollutant+-"iO: P a t r o i e u m h y d r o c a r o o n s : V o l a t i l e o r g a n i c s CGC]: V o l a t i l e o r g a n i c s CGC/MS]: C y a n i d e s : 1 F COOE 0 1 °Sr ^ j ^ (o>^ QS _ _ A N A L Y S I S N i c k e l : C . l r o m i u m : A r s a n i c r CoDDsr: L a a d : M e r c u r y : A n t i m o n y : CODE 06 07 08 09 10 11 12 A N A L Y S I S Z i n c : C a d m i u m : S a l a n i u m : S i l v e r : B a r i u m : 1 COO: B O D : COQ£ 13 14- IS 16 17 18 19 ANALYSIS TSS: TCS: pH: P C 3 : Otner: CSoacify) c-z^ j 1 20 2.1 22 1 23 24. ,01719 C H A I N OF C U S T O D Y yk.^ - k y 7 •jir« ^ -csi-vc^ \ nc. • 6 2 5 5 . s t a l l a t i o n : / T ^ r : ; ^ ^ y/A''-<Zyy/Cy/.^ A Z / A y ^ y ) (- — - _ y i m o l i n g S e r i e s : C / V 7 / y C y y i m o i e I d e n t i f i c a t i o n - : 7 - ^ r y y A r ^.r-.yr2-yfZy r..''z:>r3-y^.T •:---'-r-2r<-<sy y.r- yrr-r^sr ) S a m o l i n g L o c a t i o n P o i n t yyyy 1 ^ ; ^ , y y S a m o l i n g Gate y ^ yyyy.f/A / y y y - y ^ c yr^ y - y r ^ y y - ' / ^ e l i n q u i s n e o 3 y : ( S i g n . ] Send R e o j r t T o : y / ^ y yy y " • SamolerCs) '<.a-w y... /•...yc,y...y^ N a m e : i S . g r a f j r e : /z^^z^ y y^ycci^ S a m p l i n g T i m e /•'AZC^.^:.y / y y / j y A:yy...-. ... y-sc.:....., / S-C<Z.-.-r, ' / - - -— k^:-<zy< S a m o l e Tyoe C o m p . Grao > / y 7^ < A n a l y s i s R s c u i r e c i^y z:</' y y y * y t y y / y ^ ^ N o . Cf C o n t a i n e r s — 1 — ' • — ) ! / \ / \ f \ / ! / 1 I 1 _ _ _ R e c e i v e d By: CSign.] C a t e / T i m e T e linQui s n e o ' 3y:^>iS,ign.] | R e c a i v e d By: ( S i g n . ] i C a • e / ' T i m e ^;7/;c./-^ R e i i n a u i s n e c To L a o o r a t o r y Sy: ( S i g n . ) R e c e i v e d For L a o o r a t o r y 3 y : ( S i g n . ] l a t e / T i m e M e i n o o Ot R e l i n c u i s n m e n t : N a m e Ot L a o o r a t o r y : A N A L Y S I S REOUIREO CODE ( c u t c o o e in p r o o e r c o l u m n ] P r i o r i t y p o l l u t a n t 4-40: 0 1 P e t r o l e u m h y d r o c a r o o n s : 02 V o l a t i l e o r g a n i c s (GC]: 03 V o l a t i l e o r g a n i c s ( G C / M S ] : 04 C y a n i d e s : QS A N A L Y S I S COCE I A N A L ' ^ S I S N i c k e l : C J i r o m i u m : A r s e n i c r C o o o e r L e a d : M e r c u r y : A n t i m o n y : 06 07 08 09 IQ 1 1 12 Zinc: Cadmium: S a l a n i u m : S i l v e r : B a r i u m : C O O : B O O ; CCCE 13 14 I S 16 17 18 19 A N A L ' TSS: T C S : p H : P C S : O t n a r : ( S o a c i f y l y^<r^- y^p.rrcL. Oy.f^ 20 2 1 22 2 Z _ " 2 4 " ; 301720 o -J to :ei'i INDUSTRIAL CORROSION MANAGEMEhrr INCORPORATED K'JOCP C e r t i f i e d Drir.king Wa I er/WcS I ewal er Laboratory 10 /('I'll 16 RtPCjRT DATE :_.. Hay 2, . l'Jli6 _^ LAB i' _ 5r)62 '^1^'E''"'": ENVIRO _SGIENCES_INC^=J:ilimci.Chcoilcal.l'rn.1er.t_ — SAKPLE SOURCE: 085-251::ESI SAMPLE DATE:„ 3/1.3/86 SAhPLED OY: Al_!<yleH AT LAB DATE: :i/17/06 ACID EXTRACTABLES PRIORITY POLLUTANTS + hO _b y.-G C./.M S -LI Q. P £ £ K S ACID EXTRACTABLES PRIORITY POLLUTANTS + 10 Peaks 2-chlorophfcnoI '2-ni t j-ophenol - - - - phenol 2,'i,-dimethyIphenol 2 , * » , - d i c h l o r o p h e n o ! pentachlorophenol 2,'l-dinl t rophenol '(.S-dinl 1 r c - o - c r e s o l — 'l-nl t rophenol - - - 2 , ' t , 6 - t r l c h l o r o p h e n o l - - k-ch)oro-'i melhyl phenol _33ni)_ 33011 _ 3 3 0 i r _33QfL _330!L .165niJ_ i^SOiL _330ll_ _33QIL. S'.IKItOCATE UI'.(:OVI-.l<rES 2 - l ' l iii)r|)liciui I P h e n o L-(I5 2, /(, 6-Tr Ihroiiioplicnr)] Ali^'^ S O . b X 5 0 . U All r e s u l c s are r e p o r t e d In ug/l<g(ppl)) dry weight b a s i s . INDUSTRIAL CORROSION hAKAGCHENT, INC .''''yl yW.'^. . / l . f V i IIU RSL: dlh • L T - l e s s T h a n ND'h'ot Pet ec ted Pri'i Idcnt rC LO O H to to • I I INDUSTRIAL CORROSION MANAGEMENT INCORPORATED ni; »D.'n If. UNDD.Prt. wrw j|RSf» a m ?c- sutuo l.'JDLP C c i t i f i t - d D r i n k i n g Wa t er/Wa s t ewa I er Laboratory ID /f Mi 1 16 REPORT DATE:. Miiy 2,._|'J(!f). LAB (i'__531(>J . CL I ENT:_|^Hyj|{n_SCIENCES_INC..-r-Ialand.Chem lr.il l-Prn.|er.L_... SAKPLE SOURCE: n85-252-EST SAKPLE DATE:_3Zl2/56 SAhPLED BY: _ . .A.,_ Kyles. AT LAB DATE: .3/1 7/1! fi. ACID EXTRACTABLES PRIORITY POLLUTANTS + 'i 0 _b.Y._GC7.H5,-LlO_PEAKS _AClD_E>(TRACTABLES_PR!ORITY_POLl,yTANTS 2 - c h l o r o p h e n o l - _330U 2-ni t rophenol - - _33QU . phenol - _33QIJ_ 2 , ' l , - d i m e t h y l p h e n o l - - _330ll 2 , ' i , - d l c h l o r o p h e n o l _330IJ__ p e n t a c h l o r o p h e n o l - J650n 2 , J j - d i n l t r o p h e n o l - .16501J i t i f i - d i n l i r c - o - c r e s o l - - J^SOU ^i-nl t r o p h e n o l - - .1650IJ_ 2 , ' « , 6 - t r i c h l o r o p h e n o l - _ 3 3 n u _ ^i-chloro-j methyl phenol _ 3 3 Q U _ All results are reported In iig/kg(ppb) dry weight bnsls. KSL: L T = L e s s T h a n ND=Not D e t e c t e d S'.lKKnnATEJUjCnVEUT E.S 2-l''lii(iroph(!n()l 9fl. 5% I'lien()l-d5 7R.8Z 2,'!i , 6 - T r Ibromoiilicnol 90.6% INDUSTRIAL CORROSION MANAGEMENT, INC R l c » i a t d S . P r e s i d e n t n INDUSTRIAL CORROSION MANAGEMEfJT INCORPORATED o l-« to NJDLP C f c f t i f i t d O i i n k i i u j Wa t er/Was t ewa I er I a b o r a i o r y ID /M'i I 16 REPORT DATE:.M.iy. 2, !0)i6 LAB H yVUi'i •^l-IENT: EHVIRQ.SGIENCES_INC.-.-_Ibland.Chemica I-Prnject.. SAKPLE SOURCE :_85rl52-ESI ; SAMPLE DATE: 3/J3/86 SAMPLED BY: A^,..I<ylea AT LAB DATE :._.;_ 3/!.7/fj6. ACID EXTRACTABIES PRIORITY POLLUTANTS + kO _bY._CC7M5.t:l.Q_P.[£KS ACID EXTRACTABLES PRIORITY POLLUTANTS + 10 Peaks 2-chlorophenol - -- 2-nitrophenol phenol 2,'*,-dimethylphenol 2,'i,-dichlorophenol pentachlorophenol - 2,'l-dini t rophenol V 6 - d i n l t r o - c - c r e s o l — ^-nitrophenol 2,'<,6-tr Ichlorophenol -- •t-chloro-B melhyl phenol 33011 330U 33011 330IJ 330U _ 16.5 nil- J65n!J_ J65Ql!_ 165QU_ _J3QU_ __33QIL_ All results are reported in ng/kg(ppb) dry weight basis. R?L:dlh • LT = Le SS T h a n KD^Uot Detected .SIlHIiOCATl-: RECOVERIES 2-I''l iioi'opheni) I Phenol (15 All. 52% 2,/i, 6-Tr IbromoplienoL 38^ OTIjER COMPOUNDS DI'TECTEI) APPROXTMATE CONnENTR_ATTONS Unknown liydroc.irlion peaks t o t a l l i n g 26 7,700 INDUSTRIAL CORROSION MANAGEMENT, INC Ul^Ci^^'^/[y/l/^^^i. H / r h i i f d S. I^LVJiic Presitltnt u INDUSTRIAL CORROSION MANAGEMENT INCORPORATED l i ; ; I.D.1I IC RtKHJ.IV. xfVi JlRSfl b U H ?0- i l K i ' . U to o M to 1 ^ NJDEP Certified Drinking Water/Wastewater Laboratory ID /f I'll 16 REPORT DATE:... M')y ' I L A ^ M . LAB ff 53365 CL I ENT:_ENyiRO_SCIENCES_INC._r-Is land. Cliemical.Project SAMPLE SOURCE :__085-254-ESI SAMPLE DATE:_3/.13Z86 S A K P I ED BY:, A._Kylea. . _ A T LAB D A T l : •)/!V/(!6_ ACID EXTRACTABIES P R I O R I T Y P O L L U T A N T S + ^i 0 _ b y _ _ G C y M S t ; I Q_PE£KS _ __ ACID EXTRACTABLES PRIORITY POLLUTANTS t 10 Peaks 2-chlorophenol 2-nitrophenol phenol - ' 2,'(.-dimethylphenol 2,'4,-dichlorophenol pentachlorophenol 2,'j-dini t rophenol 'f.S-dinl t ro-o-cresol 'j-nl I rophenol 2 , ' i , 6 ' ' ' ' i c h l o r o p h e n o l - - It-chloro-B methyl phenol 33011 l30ir 33011 _33Q!L _330U_ .1650LL .i65QU_ i6501L .I65QU_ ! J } 3 Q I L S'.IRIIOCATE KECOVEKTES J3Q1L All results are reported in ug/kg(ppb) dry weight basis, 2-El imroplioiii) I Pheiiol-(l5 2 , /|, 6-Tr lbr(iiiiii|>lii:no1 _^1 51 52 8% 5% INDUSTRIAL C O R R O S I O N M A N A G E M E N T , INC Richard S. / i v/ffe RSL: (ill, • L T = L e s s Than ND=Not Detected I'res Idem, \ '\ ih INDUSTRIAL CORROSION MANAGEMENT INCORPORATED l.'JDLP Certified Drinking Water/Wastewater laboratory ID /Tl'il 16 RIPORT DATE:.. May. 2,_I'Jfi6_ LAB l/_^r\M CLIENT:_ENVIRQ_SQlENGEa_JNG.-_--l3land.Clieralcal..l'i-o.)ect, SAMPLE SOURCE : 085^255:iEST SAMPLE DATE:_3,n3/86 SAMPLED BY: .A.;_Kyles._ .AT LAO DATE : _ J / ! 7 / f ] 6 _ ACID EXTRACTABLES PRIORITY POLLUTANTS + 'i 0 _byi._GcyMSi_|.Q..P.EAKS ACID EXTRACTABLES PRIORITY POLLUTANTS + 10 Peaks 2-chlorophenoI 2-nitrophenol phenol 2,'i,-dimethyl phenol 2 , ' ) , - d l c h l o r o p h c n o l pentachlorophenol 2,'t-dini I rophenol A , 6 - d i n l t r o - o - c r e s o l it-nl t rophenol 2,*(,6-tr Ichlorophenol -- l|-chloro-3 methyl phenol _330!!_ 33011 _33Ql!_ -_33QLL _33QU_ _1650li_ _[650ll_ J 6 5 0 t J _ _i65Qli_ 330ll_ 33011 All results are reported in ug/kg(ppb) dry weight basis .SUR KOC ATE RECOVERIES 2-El iiropluMio 1 IMieiH)l-(l5 2, ' i , 6-Tr I Uniniophennl 98.2Z 96.57. INDUSTRIAL CORROSION M A N A G E M E N T , INC u> o M to ( J l I RSL: (llll • . L T = L e s s T h a n h'D=Not D e t e c t e d _ £^'^.y'^A/iAy'.- Rlch^rd S. \ k \ \ k President A^ r INDUSTRIAL CORROSION MANAGEMENT INCORPORATED 1152 ROUt£ 10, SANOOLPH. .NEW JE.=?S£Y 07859 20l-5a4-033Q CL1£NT: ENVIRO SCIINCES INC. - I s l a r . d CheT-.icaL P r o - J e r t NJD£.= C e r t i f i e d D r i n k i n g W a t e r / Wascewacer Laboracop/ 10 ^ U l l S REPORT DAT^: Mav 2. 1986 LAB I 53363 SAMPLE SOURCE: OS5-2f2-ESI SAMPLE DATE: 3/L3/36 SAMPLED 3Y: Kvles .AT LAB DATE:. BASE/NEUT-RAL E.XTRACTA8LES PRIORITY POLLUTANTS •*- kQ bv GC/MS + 15 PEAKS Pa ra.T.ecer aceneohc^iene acer.acncny 1 e.'^.e anchracene . benzidine benzo (a)an cr.racene benzo{a) py rep.e 3 , i4-ben2of lucran chene benzo (gi^ I ) pery 1 ene benra(!<.) f l u o r a n t h e n e bis(2-chlorQechoxy)mechane b i s ( 2 - c h I o r o e t h y i ) e t h e r bi s ( 2 - c h 1 o r o i s o p r o p y l ) e t h e i b ! s ( 2 - e t h y i h e x y l ) p h t n a l a c e i4-bromopheny I phenyl e t h e r butyibenzy! p h t h a l a t e 2 - c h l o r o n a p h t h a l e n e ii-chl oropheny I phenyl e t h e r chrysene d ibenzo(a ,h)anthrace.ne 1 , 2 - d i c h l o r o b e n z e n e 1 ,3-cii chl orooenzene 1 , i^-d ichl orobenzene 3,3-d ichlorobenz i d i n e . Resul r --r\\t '^^!(1r• ',01! .Resul t Pa rameter -:;0U diethyl phthalate Z'ZZ'Z dimetnyl phthalate ;.;.QU di-n-butyl phthalate '-.LlZ'l 2,'4-d i n i t rotol uene '-QU 2,6-dinitrotoluene J J O U di-n-octyl phthalate j.^ou 1 ,2-di pheny I hydraz ine(as azobenzene)- ; A^n; 330L' fluoranthene, -^-ni 3~Grj fluore.n'e 330U hexachlorobenzene 330L' hexachlorobutadiene 320;.' hexachlorocyclopentadiene 330L' hexachloroethane r • 33QL' _ indeno(l ,2,3"Cd)pyrene 330U isophorone • 33Q(j naphthalene • 330U nitrobenzene 330U N-nitrosodimethyiamine 33QU N-nitrosodi-n-propylamine 330U N-ni trosodi phenylami ne 330U phenanthrene 330U pyrene 660L' I ,2,^-trichlorobenzene Of -;TOr- ni- TTHi' nt' 33C'J 330U 330U 33 OU 330U 3 30U SURROGATES LT=Less Than ND=Not Detected d5-Nitrobenzene - 84.0% 2-Fluorob:i.phenyl -L13.0% it-Terohenyi-dU -123.IZ APPROXIMATE CONCENTRATION OTHER COMPOUNDS DETECTED All resulcs are reporced in ug/kg(ppb)dry weighc basis. INDUSTRIAL CORXOSION MANAGEMENT, INC. y y u ^ Stichard S. ;^v4rna Presidnec. RST.:H1h 301726 INDUSTRIAL CORROSION MANAGEMENT INCORPORATED 1152 ROUfi IQ. RANOQL.''H. .N£W llRSlI 073S3 201 534.03;a CLIENT: ENVIRO SCIENCES INC. - I s l a n d Chenical Prr'-'ec- NJOEP C e r t i f i t o D r i n k i n g ' J a z t r / Wastewater L a b o r a t o r y ID ;?U116 REPORT DATE: Mav 2. 1986 LAS i 53564 SAMPLE SOURCE: 85-252-ESI SAMPLE GATE: 3 / 1 3 / 8 5 SAMPLED 3Y: A. Kvles .AT LAB DATE:. -: /' ZO BASE/NEUTRAL EXTRACTABLES PRIORITY POLLUTANTS ^ kC by GC/.'-,S + 15 PEAKS Pa rameter aceneohthene ace-ac".:.-5y 1 ena anznrccene b e n z i d i n e • b e n z o ( a ) a n t h r a c e n e b e n z o ( a ) p y r e n e 3 , ^ - b e n z o f l u o r a n t h e n e benzo(ghi)pery1ene benzo(k.) f l u o r a n t h e n e b i s (2-ch 1 oroethc.xy )methane - — - b i s ( 2 - c h l o r o e t h y 1 ) e t h e r bi s ( 2 - c h l o r o i s o p r o p y l ) e t h e r b i s ( 2 - e t h y l h e x y 1 ) p h t h a 1 a t e 4-bromopheny1 phenyl e t h e r b u t y l b e n z y l p h t h a l a t e 2 - c h l o r o n a p h t h a l e n e 4-chIoropheny1 phenyl e t h e r chrysene d ibenzo(a,h)anthracene 1,2-dichlorobenzene I ,3-dichlorobenzene 1 ,4-dichlorobenzene 3 ,3-dichlorobenz idine Result Pa rameter ;30V diethyl phthalate ] '-.'j'Z dimethyl phtnalate 3 3 0U di-n-butyl pnthaiate 1c;2U 2,4-dinitrotoluene ;30U 2,6-dinitrotoluene 3 J OL' di-n-octyl phthalate 330U 1,2-dipheny1hyarazine(as azobenzene)' 33QL' fluoranthene 3 30r fluorene 330U hexachlorobenzene 330U hexachlorobutadiene 3 30L' hexachlorocyclopentadiene 330U hexachloroethane 330L' indeno(l ,2,3-cd)pyi'ene 330L' isophorone 3 30U naphthalene • 330U nitrobenzene 330U N-nitrosodimethyiamine 330U N-nitrosodi-n-propylamine 3301' N-ni crosodiphenylamine 33QU phenanthrene 330U pyrene 6 6 ou 1,2,^-trichlorobenzene Resu! : LT=Less Than N D = N G C Dececced SURROGATES nzene - 37Z phenyl- 70% dl4 - 58% d5-N i trobe 2-r 1 uorob.i 4-Terpheny nc ^ n I • APPROXIMATE CONCENTRATION OTHER COMPOUNDS DETECTED All resulcs are reporced in ug/k.g(?pb)dry weighc basis ^.nv T!(VI --.rw •>. tor- Tin" -l-!0" rjoi 330U 330U 330U 330L' 230U # INDUSTRIAL C0R;510SI0N MJ^LNAGEMENT, INC. ifi chard S . Le Presidnec y RSL:dlh 301727 INDUSTRIAL CORROSION MANAGEMENT INCORPORATED 1152 SOUlc 10. SANOOlPH. N£W )£,SS£Y 07369 201-534-02;D CLIENT: EN^.'IRO SCIENCES INC. - Island Che'n-ical Pro^ecr NJDE? Certifiea Drinking Water/ Wastewater Laboratory ID ,^14116 REPORT DATP: M.qv 2. '.9g6 LAB a 53365 . SAMPLE SOURCE: -035-254-E5I SAMPLE DATE: 5/15/86 SAMPLED BY: A^ Kvles .AT LAS DATE:. le cer ocenesntnene ace.^.asn-ny 1 ene anc.Tracene ben2 id ine . b e n z o ( a ) a n t h r a c e n e benzo (a) py re.ne 3 , 4 - b e n z o f l u o r a n t h e n e b e n z o ( g h i ) p e r y i e n e b e n z o ( k ) f l u o r a n t h e n e b i s ( 2 - c h l o r o e t h o x y ) n e t h a n e b i s ( 2 - c h l o r o e t h y 1 ) e t h e r —. b i s ( 2 - c h l o r o i s o p r o p y l ) e t h e r b i s ( 2 - e c h y l h e x y 1 ) p h c h a l a c e 4-brcmophenyI phenyl echer butylbenzyl p h t h a l a t e : 2 - c h l o r o n a p h t n a 1 e n e 4-chlorophenY1 phenyl e t h e r chrysene dibenzo(a,h)anthracene • 1,2-dichlorobenzene 1,3-aichlorooenzene 1 ,4-dichlorobenzene 3,3-dichlorobenzidine BASE/NE'JTRAL EXTRACTABLES PRIORITY POLLUTANTS -r 40 by GC/MS f 15 PEAKS Resulc Parameter 3'C'L' diethyl phthalate .-3Of dimethyl phtnalate 3 30L' di-n-butyl phthalate 1-52U 2,4-dinicrocoluene 3 3GU 2,6-ainitrotoluene 3 30L' di-n-occyl phtnaiace 330'j I ,2-di pheny I hydraz i ne(as azooenzene)' 3 3G'j fluoranthene 33QU fluorene 330U hexachlorobenzene 330U hexachlorobutadiene • 330U hexachlorocyclopentadiene 3 30U hexachloroethane 330U indeno(l,2,3-cd)pyrene 330U "isophorone 330U naphthalene 330U nitrobenzene 330U N-nitrosodimethylamine 330U N-nitrosodi-n-propylamine 330U N-nitrosodiphenylamine 3 30U phenanthrene 330U pyrene iboOU 1 , 2 , 4 - t r i c h l o r o b e n z e n e • o r - nnr- - O i : ' 0 " 10" : - > 0 r - •:o,'- T - n i ' '.Of 33QU 330U :0U 330U 3 30U SURROGATES LT=Less Than ND=Noc Dececced d5-Nitrobenzene - 37% 2-Fluorobiiiphenyl - 69.7% 4-TerDhenyl-dl4 - 72.1% APPROXIMATE CONCENTRATION OTHER COMPOUNDS DETECTED A l l r e s u l c s a r e r e p o r c e d in ug/itgCppb) -dry weighc b a s i s . INDUSTS.IAL CORROSION MJ^NAGEMENT, I.NC Ri<fhard S. L/ev%e P r e s i d n e c RSL:dlh 301728 INDUSTHIAL CORROSION MANAGEMENT INCORPORATED 1152 .'?OUr£ 10. RANOCL.=H. ,V£W JERSEY Q7S69 201-:3-t-0230 CLIENT: EN'/IRO SCIEI^rCES INC. - I s l a n d Che:?.ical Pr?-!- NJOEP C e r t i f . D r i n k i n g Wacer/ Wascewace.'- L a b o r a c o r / I0 f'I 4 1 1 £ K REPORT DATE: Mav 2. [ORn LAB # 53366 SAMPLE SOURCE: 085-255-ESI SAMPLE DATE: 5/15/56 SAMPLED BY: A. Kvles .AT LAB DATE:. BASE/NEUTRAL EXTRACTABLES PRIORITY POLLUTANTS -r 40 bv GC/MS + 15 PEAKS :3GL 3 50L" O Z - Parameter Resul t aceneohthene 3 30L' ac e.'^ a cn cny 1 e.".e _ anthracene _ benzidine _j b e n z o ( a ) a n t h r a c e n e •- _ b e n z o ( a ) p y r e n e _ 3 , 4-benzof1uoranthene _ b e n z o ( g h i ) p e r y 1 e n e _ b e n z o ( k ) f l u o r a n t h e n e _ b i s (2-chloroethoxY)methane _ b i s ( 2 - c h l o r o e t h y 1 ) e c h e r _ bi 5 ( 2 - c h l o r o i s o p r o p y l ) e c h e i _ b i s ( 2 - e t h y l h e x y l ) p h t h a l a t e ~ 4-bromopheny1 phenyl e t h e r butylbenzyl p h c h a l a c e _ • 2 - c h l o r o n a p h t h a l e n e _ 4-ch1oropheny1 phenyl e t h e r c h r y s e n e _ d i b e n z o ( a , h ) a n t h r a c e n e 1 , 2 - d i c h i o r o b e n z e n e 1 , 3 - d i c h l o r o b e n z e n e 1 , 4 - d i c h l o r o b e n z e n e 3 , 3 - d i c h l o r o b e n z i d i n e Paramete.- R e s u l c y y 330U 5 50U 33QL' 330U 350U 330U _120U_ ?50u 330U 330U 330U 330U 330U 350U 330U 330U 660U diethyl phthalate -- dimethyl phthalate di-n-butyl phthalate 2,4-dini trotoluene 2,6-dini trotoluene di-n-octyl phthalate 1,2-diphenyihydrazine(as azobenzene)' fluoranthene fluorene hexachlorobenzene hexachlorobutad iene hexachlorocyclopentadiene hexachloroethane -' • indeno(l,2,3-cd)pyrene i sophorone naphtha 1ene ni trobenzene N-ni trosodimethyiamine N-n i trosod i-n-propylami ne N-ni trosod iphenylamine phenanthrene pyrene ' 1 ,2,4-trichlorobenzene -.r:- .-,-\r _2-lQiL J2Q1 T;ni; 3~,nr- "'Or.- ~-.0r: 3 5QU 5JOU 33QU 5 30U 3 3QU 350U LT=Less Than ND=Noc Dececced SURROGATES d5-Ni trobenzene 2-r ] uorob^ipheny I ] no surrogaces added 4-Terpheny1-dl 4 APPROXIMATE CONCENTRATION OTHER COMPOUNDS DETECTED All resulcs are reporced in ug/kg(ppb"*dry weighc basis. RSL:dlh INDUSTRIAL CORROSION MJI^NAGEMENT, INC. ^ . ^ ^ ^ % r ^ Ridhard S Presidnec / 301729 CHAIN OF CUSTODY yz'k .1 %^ •••«••• 3 6 6 - 6 2 5 5 S e n c Reoflrt To: Z^z^^7%^J . ^ i l a i i m o l i n g S e r i e s : y ^ y y > - / / ^ ^ X r SamolerCs) Name: I i. 1 g.-; a [ u r = ; •tfty. Z-Ty^-y <ZMJ.. i m a l e icenti f ica rion i S a m c l i n g Location Point S a m o l i n g C a ; e S a m o l i n g T i m e S a m o l e T y p e j A n a l y s i s R e c u i r e c Com: Grao No. Cf Containers ^ -y./r/-yrzrr yyr-,(ZZ-/ /3AfAy.AC A-Zro y . t '•r-zz-y.- yriziz y y y (^-3 A-sC yzz yr-y-c e i i n a u i s n e a Sy: CSign.] R e c e i v e a 3y: CSign.] !a t e / T i m e ' < y - ^ r ^ ~ y y •-.^-.yzry- y ^ . ' S ' y A y y ^ y y r y : y r - \ 'y r y S- cc \ S-^c - •K V • — • • " • y z 1 zy i / 1 / . 1 1 ! 1 _ - . , _ . , l e u ncuisnt (fSigo^ R e c e i v e d - By: CSign.) (}yL ^•rOt^uTcG y "2 a te/Tifna / y. i ••// J^i: /^. y l e i i n c u i s n e c To Laoaraflory By: CSign.} Received For L a o o r a t o r y 3y: CSign.] ; a I e / T i m e .Aetnoa Of Relincuisnment: Name 01 L a o o r a t o r y : A N A L Y S I S R £ O U I ? = 0 put c o c a in p r o o e r c a i u m n ] Priority pollutant+'<iO: Petroleum hyarocaroons: Volatile organics CGC]: Volatile organics CGC/MS]: , C y a n i a e s : CCCE I ANALYSIS COCg I ANALYSIS . CCCE 01 02 03 04 OS Nickel: C f i r o m i u m : A r s e n i c r C o o o e r : L e a d : M e r c u r y : A n t i m o n y : 06 07 08 09 10 1 1 12 Zinc: Cadmium: Selenium: S i l v e r : Barium: COO: B O O ; 13 14- 15 16 17 18 19 ANAL'^SiS TSS: TDS: p H : PCS: Otnar: CSoecify} C C C S 20 2 1 24 301730 INDUSTRIAL CORROSION MANAGEMENT INCORPORATED U52 SCur£ iO. SANCCL=M. NEW ;£.RS£'f 07359 2 Q I ; S . ; - G ; 3 0 NJDE? Carcified Dri.-iking Wacar/Vastavaca; Laboracory ID;/ L4LI6 REPORT D.^TE: in—'i i6 loa- LAB i* 53562 CLIZNT: EN\"RO SCIENCES - Island Checiical Proiecc SAMPLZ SOURCZ: 085-25I-ESI SAMPLE DATE: March 13. 1986 TAKZN BY: A. Kvlgs AT LA3 DATZ: y.^r:h MATRIX: Soil ' G9;; ?C3 ANALYSIS '.2choc 605 bv G2.S Chronaco^raohv vich Zlaccron Ca-ci ?.\RAMZTZR RESULT SPIKE DUP SPIKE RPD DETZCTICN' LIMITS Arochlor L016 Arochlor 1221 Arochlor 1232 Arochlor 12^*2 Arochlor 1243 Arochlor 1254 Arochlor 1260 ND ND ND ND ND ND ND X X X X X X X X X All resulcs are raporced in csg/kg(ppm) dry weighc basis. If you should have any quescions, please do noc hesicace co call. DBC SURROGATZ RZCOVERIZS; Blank: *^Tt Saciole: 39% Spike: *** Spike Dup:*** 0. 1 0. 0. 1 0. • 0.1 RSL: dlh ND=Noc Dececcion RPD-Relacive Percenc Difference INDUSTRIAL CORROSION MANAGEMENT. INC. Richard S. iievi-£e Presidenc A PCBEC0125 PCBECW/S150 SOITBI # INDUSTRIAL CORROSION MANAGEMENT INCORPORATED U52 ROUTE 10. SANOQLOH. NEW JE.'SEY 07869 20l-5a4-03:0 NJDE? Carcified Drinking Wacer/Vascevac Laboracory IBit 14116 RZPORT DATE: .-Voril 16. 19g'^_ LAB it 53363 CLIZNT: ENVIRO SCIZNCZS - Island Cheaical Proiecc SAMPLZ SOURCZ: 0S3-252-ZSI SAMPLZ DATZ: March L3. 1986 TAKZN BY: A. Kvles AT LAB DATE: March I~. I?S- MATRIX: Soil ' , ?C3 .VN.ALYSIS Mechcd 608 bv Gas Chromacoaraahv wich Zleccron Caocire P.--RAMZTZR Arochlor 1016 Arochlor 1221 Arochlor 1232 Arochlor 1242 Arochlor 1243 Arochlor 1254 Arochlor 1260 RZSULT ND DUP SPIKZ ND ND ND ND RPD J L . DZTZCriCN LIMITS ND _s_ ND JL _S_ 0. • 1 n n 0 0 Q , . • . -, All resulcs are reporced in ng/kg(ppni) dry weighc basis. If you should have any quescions, please do noc hesicace co call. DBC SURROGATZ RZCOVERIZS: Blank.: *** Sample: 61!: Splka: *** Spike Dup: *** INDUSTRIAL CORROSION MANAGEMZNT, INC. Richard S. Liv2^ne Presidenc / RSL: dlh ND=»Noc Dececcion RPD-Relacive Percenc Difference PC3EC0125 PC3ECW/S150 301732 # INDUSTRIAL CORROSION MANAGEMENT INCORPORATED NJDE? Cercified Drinking Wacdr/Vascavacer Laboracory IDii* 14116 REPORT DATE: April 16. 1985 L A B ;/ "^-s-sfii • 1152 SCUTE 10. RANCCL'H, NEW JE.RSEY 07369 201-!S4-03;0 CLIENT: E^TVIRG SCIZNCZS - Island Cheir.ical Proiecc SAM-PLZ SOURCZ: 85-255-;SI S.\M?LZ DATZ: March 13. 1986 MAT RIX: Soil T.^<ZN 3Y: A. Kvlas AT LAB DATZ: March 17. 1986 PCB ANALYSIS Me'ihod 608 bv Gas Chrocacozraohv wich Zleccron Cascura P.ARAMZTZR Arochlor 1016 Arochlor 1221 Arochlor 1232 Arochlor 1242 Arochlor 1248 Arochlor 1254 Arochlor 1260 RZSULT ND SPIK DUP SPIKZ JSL ND Jffi. ND ND ND RPD X X X X X X X DETZCTICN LIMITS ; n 1 _ Q i.O 1 :-\ : :-. •i n 1 n All resulcs are reporced in mg/kgCppm) dry weighc basis. If you should have any quescions, please do noc hesicace co call. DBC SURROGATE RECOVERIES: Blank: *** Saaple: L08" Spike: *** Spike Dup:*** INDUSTRIAL CO N MANAGZMJINT, INC. Rf chard S. I^viiie Presid ard S. Le\ idenc C RSL:dlh ND=»Noc Dececcion RPD=Relacive Percenc Difference PCBEC0125 PC3ECW/S150 301733 7 1 INDUSTRIAL CORROSION MANAGEMENT INCORPORATED 115; ROUTE 10, ,RA,NCGL.=H. ,N£W JERSEY Q7859 : 0 1 : 3 4 - 0 2 ; Q NJDE? Carcified Drinking Wacer/Wasc-vac; Laboracory IDi/ 14116 REPORT DATE: Aoril 16. 193^ LAB it 53365 CLIZNT: ZNVIRO SCIZ:-;CZS - Island Chemical Proiecc S.AMPLZ SOURCZ: 085-254-ESI SAMPLZ DATE: March 13. 1985 TAKZN SY: A. Kvles AT LAB DATZ: March '•'. :9z~ MJ^TRIX: Sell PCB .ANALYSIS Mechod 60S bv Gas Chromacozraahv wich Electron Caocura PAR.AMZTZR Arochlor 1016 Arochlor 1221 Arochlor 1232 Arochlor 1242 Arochlor 1248 Arochlor 1254 Arochlor 1260 RZSULl ND SPIKZ DUP SPIKZ ND ND X ND ND X ND ND X RPD X X X X X X X DEI EC" " O N : - • U T TS A ; 0.5 0.5 0.5 0.5 0.5 0.5 All resulcs are reporced in ng/kg(pptn) dry weighc basis. If you should have any quescions, please do noc hesicace co call. DBC SURROGATE RECOVERIES: Blank: *** Sample: 60% Spike: *** Spike Dup: *** INDUSTRIAL CORROSION MANAGEMENT, INC i R^fchard S. L§r/±tf^ P r e s i d e n S . LarV] RSL: dlh ND=»Noc Dececcion RPD»Reiacive Percenc D i f f e r e n c e PCBEC0125 PCBECW/S150 301734 INDUSTRIAL CORROSION MANAGEMENT INCORPORATED 1152 ROUTE 10. RANDOLPH. NEW ,'E.RSEY 07363 201-534.03;o NJDE? Carcified Drinki.Tg Wacsr/Vasce-. Laboracory ID!/ 14116 REPORT DATE: ..•^oril 15. 1986 LAB it 53366 •a Car CLIZNT: ENVIRO SCIENCES - Island Chenical Project SAMJ'LE SOURCE: 085-255-ESI S.AMPLE DATE:v=--- i "! iQS6 MJilRIX: Sell " TAKZN BY: A. KVI QC AT LAB DATE: \<, ?C3 ANALYSIS Mechod 608 bv Gas Chroaacoeraohv wich Electron Caocurs PA.RAMETZR Arochlor 1016 Arochlor 1221 Arochlor 1232 Arochlor 1242 Arochlor 1243 Arochlor 1254 Arochlor 1260 RZ3UL" ND ND SPIKZ X DUP SPIKE ND ND ND ND ND X RPD X X X X X X X DETEC: ^ICN 0. 0. 0. 0. 0. 0. 0 i . _ : -* • \ ; ; ; - V T TS All resulcs are reporced in nig/kg(ppa) dry weighc basis. If you should have any quescions, please do noc hesicace co call. DBC SURROGATE RECOVERIES: Blank: *** Sample: 70% Spike: *** Spike Dup: *** RSL: d l h ND=Noc Dececcion RPD"Relacive Percenc D i f f e r e n c e INDUSTRIAL CORROSION MANAGEMJINT, INC. y - chard S. leoqi^ne Richard S. I Presidenc / PCBEC0125 PCBECW/S150 301735 INDUSTRIAL CORROSION MANAGEMENT INCORPORATED NJDE? Carcified Drinking Wacec'Vascevace: Laboracory ID;/ 14116 REPORT DATE: Aoril 16. 19S6 LAB if --,-!ST 1152 ROUTE 10. RAN001..=H. NEW JERSEY 07869 201-53-J-03;o CL I.::NT: E^rv'IRO SCIZNCZS - Isl.a.r.r' Cher.ical Proiecc __^ SAMJ'LE SOURCE: 085-256-ZSI . SAMJ'LE DATZ:M.^.---.. I-. :OS6 TAKZN 5Y: A. Kvles ^ AT LAB DATZ: March 1~. l-~f- M_AIRIX: varar PZSTICIDE & PCB ANALYSIS-PRIORITY POLLUTANTS Suicabia for Compliance Tescing by Mechod 608 Gas_Chrcn:acosrat3hv wich Electron Caocure P.ARA^-IZTZR RZSULT SPIKZ DUP SPIKZ RPD DZTZCTION LIM: Aldrin yp x x x O.Q2 a-3K.C \T) X X X 0.02 b-BHC NTP X X X 0 Q2 d-3KC N^ X X _i_ 0.02 g-BHC (Lindane) vrp x x x 0.Q2 Chlordane ^ x X X Q. 5 p,p'-TDE(DDD) ND X X ^ X 0.2 p,p'-DDE ND X X X Q.04 p,p'-DDT ND X X • _X_ 0.2 Di^drin ND X X X 0.04 Endosulfan 1 >n3 X X X 0.04 Endosulfan 2 ^ X X X 0.04 Endosulfan sulfaca NP X x X 0. 1 . Endrin NP X X X 0.04 Endrin aldehyde NTD X X X 0.2 Hepcachlor ND X X X 0.02 Heptachlor epoxide ND X X X 0..1 Toxaphene. ND X X X 0.5 Arochlor 1016 ND X X X 1.0 Arochlor 1221 ND X X X 1.0 Arochlor 1232 : ND X X X 1.0 Arochlor 1242 ND X X X I. Q .A^rochlor 1248 — ND X X X 1.0 Arochlor 1254 . ND X X X I.O Arochlor 1260 ND X X X 1-0 All resulcs are reporced in ug/l(ppb). If you should have any quescions, please do noc hesicace Co call. DBC SURROGATE RECOVERIES: Blank:*** Sample: 145% Spike:*** INDUSTRIAL CORROSION MANAGEMENT, INC. Spike Dup: *** 1/ J f JjA pMnsT^jA^i RSL:dlh Ric?nard S. LaViGe('/Presidenc ND-Noc Dececced / RPD-Relacive Percenc Difference ~ ^ - „ _ ^ INDUS MIAL CORROSION MANAGEMENT INCORPORATED 1152 ROUTE 10. RANOOLPH. NEW JERSEY 07869 201-534-0330 NJOE? Cerci; j Drinking Water/ Wascewacer Laboracory 10 .^l^^llS -L) REPORT DATE: .Aorll 74, l o a ^ LAS a 53367 CLIENT: ^^TX7T?.0 SCIZNCZS INC. - Island Che-.ic.^l P-n^°cr SAMPLE SOURCE: 085-256-ESI SAMPLE DATE: -3/15/36 SA^.PLED BY; A. Kvlas AT LAB DATE:. - / ' - / c S Paramecer acrolein* aery 1 cn i c r i 1 e" benzene bromoform carbon cecrachI oride chlorobenzene chlorodibrcmomechane chlorechane 2-chloroechylVinyl ether chloroform dichlorobromomethane 1 , 1-dichloroethane 1 ,2-dichloroechane 1 ,1-dichloroechylene PRIORITY POLLUTANT VOLATILE ORGANICS + i*0 by G C / M S + 15 P E A K S Dececcion limic 10 ug/l(ppb) Resul t jnL :SL ZZL JiL- ND_ :nL _2L ND ND ND ND ND ND ND Paramecer 1 , 2-dichloropropane 1,3-dichloropropy1ene ethylbenzene methyl bromide methyl chloride methylene chloride 1,1,2,2-tetrachloroethane - tetrachloroethylene toluene 1 , 2-'trans-d ichl oroethy 1 ene 1 ,1,1-trichloroethane 1 ,1,2-trichloroethane crichloroechyiene vinyl chloride Resu i :iiL ND Jffi_ ND ND .ND JS- •ND *Dececcion Limic LT=Less than ND»Noc Dececced IOOO ug/lCoob). OTHER COMPOUNDS DETECTED APPROXIMATE CONCENTRATIONS SURROGATZ RECOVERIES 1,2-dichloroechane d4 - 104% dS toluene - 99% BFB - 96Z 95%(spike) 99%(spike) 103%(soike) 98%(spike duplicace) 98%(spika duplicace) 93%(spike duplicace) INDUSTRIAL CO RSL:dlh Richard S Presidenc 301737 :--A i I i 1 1. . I., i. to o r-» - J U> 00 :^:i'i INDUSTRIAL CORROSION MANAGEMENT INCORPORATED IISIROUTl 10. RAMDOim NCWJfRSEr OMit lOISeiOllO NJOEP Ceriified Drinking Water/Waslewaler Laboidtory ID #l'il 16 REPORT 0ATE:.Ai>rLl_24,_L9ft6_ LAB // .53!(.7_._ CLIENT; ENVTRO SCTENCES TNC. - Island Chemical Project SAMPLE SOURCE: Ofl5-256-EST SAMPLE DATE: March »3. i9fl6SAMPLED BY: A. Kyles AT LAD OATE: Marcli 17, 1986 ACID EXTRACTABLES P R I O R I T Y POLLUTANTS + 'lO _biL_G C7Jii±_l.Q_P. E A K S ACID EXTRACTABIES PRIORITY POLLUTANTS + 10 Peaks 2-chlorophenol 2-nitrophenol phenol 2,'),-dimethylphenol 2,'(,-dlchlorophenol pentachlorophenol Z.'j-dinI t rophenol - 't,6-dinl t ro-o-cresol — ^-nitrophenol 2 , ' t , 6 - t r l c h l o r o p h e n o l - - 'i-chloro-B methyl phenol _loy_ 1011 IQIL I oil JDU_ M\L JQiL JQIL _LQIL I oil JillRKOCATI' KKCOVF.Uir.S 2-FI iioroplieni) I Phenol-(l5 2 , 4 , 6 - ' r r i l)roiii()|iliun(>l 5 2 . 1 % 21 .OZ 67.9% OTIII'lt COMPOIIND.S DETI'm'ED APPROXTMATE CnNr.F.NTUATTONS Unknown llydroc/irhon Peak 5. ft INDUSTRIAL C O R R O S I O N M A N A G E M E N T , INC RSL:dlli R i c h a r d S./I.uv ini; I'res iilfciu INDUSTRIAL CORROSION MANAGEMENT INCORPORATED 11S2 aouI£ 10. RANDOLPH. .'i£W lEaStf 07863 2i:i-5i4..o;;o CLIE.MT: ZNVIRO SCIEMCES IMC. - I s l a n d Cher.ical Pro-iect NJOE? C e r t i f . - 0 Drinking Uacer/ Wastewater Laboratory 10 ;?! 1*116 REPORT OATE: Aoril 24. iggr, LAB < / _ _ l l ] i I <;AMP[F SOURCE: 08;-25n-rsT <;AHPI F DATE: j/l 3/S6 SAhP LED 3Y: A. Kvioc AT lAa OATE: 3/17/ BASE/NEUTRAL EXTRACTABLES PRIORITY POLLUTANTS + ^40 bv GC/.'-.S + 15 PEAKS Pararr^eter aceneoht.~.ene ::Ce.naG."ic."y i e.ne -in-nracene . ' \ benzova)pyrene • ^ 1 " 1 j,-f-oen2or[ucrancriene / I • \ . \ _ _ b i s (2-c.hloroethoxy)methane - bis(2-chloroethyl)ether bi s(2-cnloroi sopropyl)ether- bls(2-ethylhexyl)phchalate - i4-bromoDheny 1 phenyl echer - outyiDencyi pntnaijte z-c.-1 oronapncna 1 ene it-chl oropheny 1 phenyl ether , cnrysene • 0 1 den20 la , n ^ an t.-raCe-ne , . , . , , , 1,2-d1ch1orobenzene -------- • . _ . , . 1,3-d Icniorobenzene 1 1 J . - 1 L- 1.H-d1cnlorobenzene 3 ,3"d 1 cn 1 orobe.nz 1 a 1 ne LT=Less Than .ND=Noc Decaccad Result _., '. CL lOU - -T — — ^j , _ ;0U IGU lOU I OU LOU lOU iOU - - - -1 n r IOU _ IOU _ '.ou IOU lOU lOU lOL - IOU _ 10b 20U SURROGAT d5-Nitrobe 2-r 1 uorob.i. '^-Terpheny Parameter di-n-butyl phthalate di-n-occyi phthalate 1 ,2-diphenylhydrazine(as azobenzene) fluorene - - - - — hexachIorocyclopentadiene inaenoii,z,j-ca^pyrene 1sopnorone -------------—---— napn t.na i ene N-n 1 trosod ifr.etny 1 ami ne N-n1trosoo i -n-propyiamine - - - — - - — N-n i t rosod i phenyl ami ne ------------- phenanthrene pyrene 1,^,H-tr1ch1orobenzene —----- ES nzene - 6.3Z phenyl - 59.7% l-dU - 91.8% APPROXIMATE CONCENTRATION OTHER COMPOUNDS DETECTED 36 Resu! : ! .irr :0U 50L- I ni- - 2 . i J 5 on '01' IOU 1 nu ^ IOU • ou - ,. 1 n r' I n n - 1 nif - 1 Of 1 ^ ) ^ ' . IQU LOU IOU IOU IOU • ~ IUU RSL:dlh INDUSTRIAL CORROSION MANAGEMENT, UC. Richard S. Kevi^'e President / .01-739 Zn CORROSION MANAGEMENT INCORPORATED 1I5J KOurE '.O. RAHOCUM. .IEW :iJI&ct 37183 2ai.5j4.0JM NJDE? Carcif: • Dri.ikir.g Vatar. Laboracory ID .14116 REPORT DAIE: Mav 2. 19S6 "•io ..evacar LA3 It 53367 PRIORITY POLLUT.ANT L.\30.RAT0RY AMALYSIS CLIENT: --rZ^.^O SCIEMCES SAxHPLE SOURCE: Island Chsr-.lcal SAxMPLE ID: OS5-25o-;SI UNITS; -g/l^oo-' SAMPLE DATE: March 13. •. ; c ; SAMPLED BY: A 1 Kvlas AT LAB DATE: March 17. -,« — .- MATRIX: vatar (This report Lav~ concains boch che original sample resulc and che duplicate result.) j Arsenic ' aervlli-n ! Cadmiun ' Chromium ! Coooer ' Laad ) Mercurv Nickel • Selenium Silver Thallium Zinc Phenol Cvanide 1 ';.007 ! LT O.OOL LT 0.001 i 0.002 0.007 0.005 0.0005 LT 0.006 0.019 0.004 LT 0.014 0.022 LT 0.005 0.007 r- nn^ ' 0. OQ 1 0.001 0.002 0.007 0.005 LT 0.0007 0.006 0.029 LT O.OOi O.OU 0.027 X 0.008 17^: i NC i NC i NC NC ! NC 17% 1 • NC 42% NC NC 20% X 13% :75!: NC NC NC NC NC i55% NC ;33% NC NC t20% X = 20% -^-- ; T LT LT :LT LT LT LT LT LT LT LT LT LT 0.0C2 '- O.QCl ! 0.OC 1 ! 0.001 i 0.001 1 0.002 ! 0.0005 i 0.006 0.005 i 0.001 i 0.014 i 0.001 i 0.005 ! 0.007 i -- 'T T^-- T -> :.. — i ^ I •_-2 -_- -_- «i. r_- LT -_- 0.002 I 0.001 i 0.001 0.001 0.001 i 0.002 1 0.0005 0.006 0.005 0.001 0.014 1 0.001 0.005 0.007 1 1 1 1 1 NC = Non-calcuabie RPD due co vaiueCs) less chan dececcion limic. dwb =» Dry Weighc Basis X » Noc Analyzed LT =• Lass Than INDUSTRIAL CORROSION MANAGEME.NT, INC. RPD =» Relacive percenc difference. RSL/dlh itichard S./tev'f'ne Presidenc Ai^'^*-^ 301740 ^ ) C H A I N OF C L / S T O D Y jiTic :m xi^tOii ;nc. %^^ w — 3 6 6 - 6 2 5 5 Sena Reopr; To: y'.^ y ^ yyc'Tty y.yZyi-z. yzcy I l l a t i o n : ^ S c r ^ a ^vsV./^.-«c^ C^. ( Z T i / i L ) . m a l i n g S a r i e s : y ^ / y J V i i ^ x r i i n a i e I c e n t i ( i c a tion S a m s l i ng- L o c a t i o n P o i n t S a m c I i n q Cate - -ir^ - ^ r S -yr/J" coyctz. yzfy^yy- I'c y Z ; : K • C Z • ~ " I I I I . I - -I I n a i i n a u i s . i e a By: CSign.] R e c e i v e a 8 y : CSign.] 'w a t e / T i m e R e c e i v e d 8 y ; ( S i g n . ) C a t e / I I .Tl e lAJilJA'^ I '•:/•'. I < y nei'incuisneo To Laooratory 3y: (Sign.3 Receivea Far Laooratory ay: CSign.} Cate/Time iMetnod Qt Relinauisnment: Nama 01 Laooratory: I A N A L Y S I S R g Q U I P g P iCout c a a e in p r o o e r c o l u m n } P r i o r i t y pollutant+-<iO: Petroleum h y a r o c a r o o n s : I V o l a t i l e o r g a n i c s CGC}: V o l a t i l e o r g a n i c s CGC/MS}: , C y a n i d e s : COC£ 1 <^P 02 1 03 1 / ! & 05 1 A.^4ALYSIS N i c k e l : C h r o m i u m : A r s a n i c r C o o o e r : L e a d : M e r c u r y : A n t i m o n y : C C O E 1 06 07 OS 09 10 n 12 A N A L Y S I S Zinc: C a d m i u m : S e l e n i u m : S i l v e r : 1 B a r i u m : 1 COO: B O O : CCC = 13 14- I S 16 17 18 19 A N A L •' s ; S T S S ; T D S : p H : PCS: Otner: CSoecify} C C C ^ 20 2 1 2 * 301741 tMtkl' Berlox . ^ ^ r a t o r l e a St. Croix, Virgin lalanda ik tiaitJi ••^4-4.3 > . ^ i L__i.l C.::J l^t^uixl 1 ^ ^ : : -.3 VID980651095 Table 2 - Results of Organic Analyais- Organic Compounda Detected Compound name Sample location/Sample > VGA Xylene Chloroform Gut Back- ground* 1085251 Lab waste pit seep #085252 Drainage pit disch. 1085253 470 Lab waste pit il 1 •085254 huh waste pit # 2 #085255 On-site well (ug/l) #085256 130 NVOA Butyl benzyl phthalate Dl-n-octyl phthalate 1,4 dichlorobenzene 1/2 dichlorobenzene Napthalene Flourene Phenanthrene Bis(2-ethylhexyl)phthalate Aliphatic 6 aromatic hydrocarbons 1000 17000 9000 7700 870 2900 2100 2000 2400 M 4900 3200 2K 3.9 280 PCB PCB-1016 PCB-1221 PCB-1232 PCB-1242 PCB-1248 PCB-1254 PCB-1260 to O -J to 1000K 1000K 1000K 1000K 1000K 1000K 1000K 1000K lOOOK 1000K 1000K lOOOK 1000K 1000K 1000K 100 OK 1000K 1000K 1000K 1000K 1000K 1000K 1000K 1000K 1000K 1000K 1000K 1000K 1000K 1000K 1000K 1000K 1000K 1000K lOOOK IK IK IK IK IK IK IK •All values in ug/kg except where otherwise stated. K " Actual value known to be less than value given. M =• Presence of material verified but not quantified. Blank space means compound was not detected in samr»l <» x"»"»--» I t. Berl^'^^ boratorles St. CroiX, Virgin Islands I: , t ,i I A •;, I t Table 3 - Results, of Metals Scan Analysis Compound name Sample location/Bample I *A11 values in mg/kg except where otherwise stated. J - Estimated value. H •• Presence of material verified but not quantified. Blank space means compound waa not detected in sample analysis. to o 'iN VID980651095 Silver Arsenic Beryllium Cadmium Chromium Copper Mercury Lead Nickel Antimony Selenium Thallium Zinc Gut Back- ground* •085251 2J 10 40 19 IJ 100 Lab waste pit seep 1085252 U 7J 22 45 20 J 10 63 Drainage pit disch. #085253 0.8J 8J 52 52 30J • 32 IJ - 360 - Lab waste pit 1 1 #085254 0.8J 7J 27 55 25 8.4 O.BJ 80 Lab waste pit # 2 #085255 2J 7J 26 58 27 O.BJ 79 On-site well (ug/l) •085256 2J 5J 3 J 7J 8J 0.6J 3J • 20J • \ . •J i{:k to \ ! b.'-.z'"! :m t(fl(: vt crdiir l|>lll: «}-tiei-oi •;«i(Pll« OAtf: 11711 im cm no.: is'ij m VOIAIIUS Simie 10 no. Irillic Report No. i l J l f i i •mils : ilulion rjclor, PetcenI Koiiture . * SITE INSPECTION SA ^-RESULTS «8/0j/')| 1 I I 1 1 I Mil 4 flnfwmn :irM,w),n!V|.i ow: Vl.-i CW1IPUV1?5CII< VI250«5 VI25CW6 VI2S-SC0I VlJS-StOJ V125-StOJ VI2S-StO«(OVIJ5-S£OS VI25-SID4 VI25-S1IIIS/ VI25-S2 VI25-5i VI25-Si VI25-|I|I(I Bf.lOI UAUt 1 1 u.. o: w-llll O ' l 1 1 BUOl ii;)iiR ICIO< UAHI) lltjli 1 1 ICIOS VUII) ug/l t 1 IGlOi UAKR ug/l 1 (ClO» s ( i ) i « r n i ug/kg 1 V ICllO SCDIntHI ug/kg 1 1 JJ BGlll :(Dtn(Ht ug/kg t 1 (J ICU2 SCDIACKI ug/kg 1 1 J< IGlll StOIMHI ug/kg t X 11 I U U SCOIKCMI ug/kg 1 1 IUU soil ug/kg t 1 l i ICIH SOU ug/kg 1 1 U K l I S SOU ug/kg 1 1 11 IC12J SOU ug/kg 1 1 9 1(118 VAUR ug/l ., '.hloroielbane Iroioiethint vinri Chloride Lhloroelhine itthirlenc (hloriije icdont iirboii Disulfide .l-Dichloroelhene ,I-Oi(li|oroelhi(\e iiflt-l.?-Dichloroellient i<ll hloroloii / .2-Dich|oroeliiin( lirlinoAi .I.MrlcMoroelhint irbon leltichloride inyl (celile oiodifhloroietlijne 7-OicMoiooropine fl,J-Dichloropropen< ichleioelhene broiochloroielhine 1,2-lriclilorectlijne niene iM-I.J-Oichloropiooer.t iioloii lelhifl-2-Pe(iliiio/ie leiincne richloroelhene uene ,2,;-letricliloroethir.e orobtnrene flbemene rem met (totill (J: <k ipicc • ceipound inily.ti) U i twi M l delected (oepound found in lib i\in> ,'. ai|| tiipje, indjcilei potiitle tiotiiii blinl conliilnillon eitiiiled vtlue eiliiiled vilue, coepound presiM keloi CROl but ibe>c lOi I inilriil did nol pisi ( M OA/OC 'reiMPliti evidence ol the pitttncc ll li>e iileriil inilfSis nol required tion lieili elevited il Dilution r >l ind/oi parceni eoisluri .01 12 i IS t liO It t 210 I t J to o \ •, TO (D < XT O o o ro 1 UO t—• o H - • o .p» 1/1 " i ' l \ ' [ \ i I I ^IK U M : VI CHlnlCAl IOU: O2-9I01-0* CUNPIIW DAIt: J/28/91 (PA CASf NO.: I595J U B . i . II n •ri n 1 -^ n '1 fTn n SITE INSPECTION SAMPLING RBBUbTS (cont'd) .:onPucHfn to o \^ ~J * > • cn VOIAIIKS iiiplt ID Ro. Irjltic Repoit Ho. Hatrix Unili Dilution fjclor I'trcent Noislure CMotoietliine lioioitlhine Vin/I Chloride thloroethine nelhylent CMoride "Tfcelone Cirbon bitullide l,l-Dich)oroilbifle 1,1-OicMoroelbine lrini-l,2-DicMoiotlhent i .UII Chlorolori 1.2-DlcMofoel)iinc 2-lulinont l.l.l-lricMoroelhine C.rbon lelrichloride '~ifinrl Aceljle IroiodicMoroeelhjne l,2-Diih)oropropine cis-l,]-DicMotopr3pene _l;ichloroelbene MbroiocbloroieU.jne l,l,2-lricliloro(lbint lenrene Irent-I.J'Ditliloroproper.t iroiolore ""l-llelhirl-J-Penljnone J-Neiinjne letricMoiottbene toluene ^1,1,2,2-tetrjcMoroelhjnt (Morostniene (Ibylbeniene Slyrene ryler.es I I O I J I ) VI2b-RII(2 VI2S-I8HI ICI 19 IGi:2 WAUR WAHR ug/l u g / l I I l>i"l|'. ilini spirt • (lapovino «nil|.(0 k : u : nol »teclid I • toepouna lounc ',i n t t l i ' i »• . i . : , H i t . t , .noKJiti point.t t ' : ; j [ . i blank coAliiinition f • cslliilid vilue J • estitiled «)lut. coepot.ni: pteicM belo. CROl bill ibovc IDl I • intlysil did nol piii (PI 0«/0f « • Pitsunplive evidence ol Die pretintt ol Ihe laleiiil >l - tnilyiii Ml reouired Nitcllon l i i i l i eleviled il Dilution ticior >\ tat/at H'teni Miiiuie >C\ pa c n> ^ < I I tilt l... IDPI: t: i n CASt KO ^ ^ i : t • \ i I ^ y \"\ y I59:J U '.C«:'•>[•< SITE INSPECTIO..^riPLING RESULTS (cont'd) n n#^> I I 5tH|-V0IAI|l(5 Saiple ID Ro. Iridic Report Ho nilrii Units Dilution faclot/tPt i . \ i i u t i , i • Percent Hoisture Phenol bisl2-ChloroeIhynelb;i I-Chlciophenol I.J-Oichlo'obenitne . l.l-Dichlorobeniene Itniyl alcohol l.2-0icMorobtni(nr 2-Helhylphenol bisl2-Chloroi50trooy!l?ltff l-Helhylphencl R-Rilroso-di-n-dijtooyliiiie lle>achloro(than( Kiliobenient Isophorone J-mirophenol J.l-Diielhylohenol Itntoic acid bis(2-Chloroetho«i lie Ihji.i 2,1-Dichlorophenol l,2.(-lrichloroben;(ne Kiphtbiline t-Chloroinillne Heiachlorobutidiene 4-Chlcro-J-lltthy|phfnol 2-llethylnaphlhalfne Keiachlorocycloi'cnljdiene I.l.i-lrichlorophenel 2,4,5-lricMoiophenol 2-Chloronaphlhalene __7-llitrojniIine Diitthylphlhalale Aceniphthylenf 7,i-Dinitrolo|jene J-Hitroaniline _jlcenipMhent 2,<-Dinltrooh(nol Mlilrophenol Dibtnioluran J,l-Dlnltrplolu«ne Jiethylphlhilite l-Chlorophenylphenyl elh/i fluorene 4-Kilioinllint l.4-0lnllro-2-»elhyl;hfril jt-niliosodiphenylaeine «-lroiothenylphtnyl t\»f Heaachlorobeniene to o H-* -J i r i C J i n s (tlOl HdtP u;/l 1 irscu; fcio: UAKD iig. I 1 J vL'V'.Kiiouvirs-wi m O J BC104 VAHR VAUfl ug/l ug/l 1 1 V125-;ilS IGIOS MAKR ug/l 1 KR KR KR KR NR KR KR MR HR HR NR HR HR HR HI NR KR KR NR HR KR NR KR HR NR NR HR NR NR HD HR NR IIR KR IIR HR Hf) IIR NR NR HR HR IIR •IR KR Nl HP V I 2 5 - ( ; W tUOi mn . ug/l . . . . y . . . . . VI25-5t01 8(lQf SIDUIINI ug/kg 1 1 27 R ;-. VI25-5fD2 ICI 10 SlDinCNI ug/Vg t 1 JJ R - VI25S(DJ BClll SCDIKIKI ug/kg 1 1 <J VI25-StOI(tVI2S-SfOS BGII2 SlflMtm ug/kg 1 J« R 6«n SIDinCNI ug/kg 1 1 19 UO ( Vi:5-5JD4 BCIK SEDimNI ug/kg 4 42 V I ? S - 5 l ( « / VI2S-52 BCIIJ SOU ug/kg 1 1 R CCII4 SOU ug/kg 1 1 l i R VI25-SJ ICI IS SOU ug/kg 1 1 It VI25-C4 icirj sou ug/kg 1 1 9 VI2SaiKI BCtIt VAHR ug/l 1 . 1 If: », I'A $ r t »A1f: » IDDI: 0:-«ICIO< SAnriiKC M i t : i ; : ( fPA CASf NO.: n i J : H i : i.y L ..] L..J L J L_J LiAB^«i:.../ i' j' SITE INSPECTION .^^LINGi.RESULTS (cont'd) :fii'.' i!:ii I 1 I t I t I ] I I stni-toiAiiirs Saiol! ID No. I r a l f i c Pepoil No. Ilatrii Units Dilution faclor/crc ''\i >.-. Percent Moisture : n : s - i . v i . i K ; BciC'; • WflIP ! ug.'t ; 1 I:5-CM: BC102 NAUR ug/l 1 7i:scu;iouvir5-CK4 ICIOJ UAUR ug/t 1 BG104 UAUR ug/l 1 V125CK5 8C10S NAUR ug/l 1 VI25-CK6 80106 NAUR ug/l 1 VI2;-SfDI ICI 09 StOIKfKI ug/kg 1 21 VI25-5[D2 BCIIO StDlhlHI ug/kj ) JJ V1?S-SI0J I G l l l SlDlntNI ug/kg 1 4J VI25-S(D4IDVI2SS(D5 IGII2 SlDlniKI ug/kg 1 Jl ecin StOlnCHI ug/kg 1 1 19 VI25-S(D6 BGII6 SIDIPfHI ug/kg 4 42 V i r S S I I h S / VI25-52 8CIIJ SOU ug/kg 1 1 16 B C l l l SOU ug'kg 1 1 16 VI2S-S: 8GUS SOU ug/kg 1 1 It vi;s-S6 8C12I sou ug/kg 1 1 9 VI2S-RIHI I G l l l NAUR u g / l 1 1 Penlachlorochenol Phenanthrene Anthracene Di-n-bulybhthalilc fluoranthsne Pyrene lutylbeniylphlhiUle J,J'-Dichloroben(iJir> leniolalanlhracene Chrysene blsl2-Elhylhe>yllphli.al<lf DI-n-oclylphlhalate lentolblMuoranlhene lentolUlluMinlhi-ne leniolaloyrene l n d e n o l l . ? . J - c d l p i f n f D i b e n r l a . h l a n t h r a c c n e leniolg.h.iloerylent KOUS: Hank space - conpount i n j | y ; e l h i b'll not detected I • coipound found In la:< tiUnV i ; veil js staple, indicale; oc i s l M e / i rr-sjlle blank contaainallon [ - eslinaled v i l u ; J • cstitaled v a l u i . (oroi.-il F V E I I belov (ROl but abo.f : M R - analysis did nol pi-f t ' - i ' t - H • Presuirli>e f/id:i''.» .1 ihf : i i n . : ! of the a i l e i i a l KR • j n a l y i s njt I»T.' i ; ! Deletlion l i o i l s e l f . i l I i ! IT. ' i n Fatloi I »nd.oi p c ' . ' i ' I.- 'U.t. '.-' NR HR KR KR HR HR KR HR KR HR KR KR NR KR NR KR KR KR 10 ( R J R J J J J R R R 22C0 [ R R R R R R R 0 0 o M •J m Krt|': iza SIfl lAI UU: { rAHPllft OAII: 2.'.V'-| fPA CASf NO : tS«!; 1 L.ij • LlJ izZs y As! m , m ' y j LJ SITE INSPECTION^IPLING RESULTS (cont'd) n_n.._an_n«i _ i ^ . i _ . i"-)rri' if-c sfHi-vmAiiic Saeole ID No. Iralfic Report Ho. Nalrii Units Dilution racloi/i'.Pf rir.'..j,-i ' i l Percent noislure fhenol bis(2-Chloroelhyl!tlh'i }-Chloioph(noi I.J-Oichlcrobtnieie l.<-Dichloioben;rnF leniyl alcohol l.I-Dichlriohentene J-helhylphenol bisl2-CMorDisopiopy|telh( 4-Helhylphinol N - K i l r o s o d i - n - d i M W i l i m i f Heaachloroelhane Kllrobentene Isophorone 2-KilropSenol 2,4-Diielhylphenol lenjoic acid bts(i-Chlo'ottho<ylirll.i'e 2,4-Dichloripnenol l,2,4-lricMo(Obenirii. Kaphthilene 4-Chloraaniline llMachlorobutaJien. 4-CMoro-J-Nelhylohfiol I-ltelhylnaphlhalen' HeiachlorocyclopentaJitn; t . l . i ' l r i t h l o r o p h e n o l ?,4.5-fiicMorothe>ol l-Chloronaphlba'.enr 2-Nilroaniline Di>ethylthlhalal( Acenaphthvlene 2.6-Oinitioliluene J-Nitroaniline Aceniphthtnr 2,4-Pinilroph'nol 4-Hitropheno: Dibenroturan 2.4-Dinilrotoluff." Diethylphthalate 4-Chloro(hen/|-|<h'n, I M'.i' lluoiene 4'Hilioaniline 4.t-Dinilr6-7-inlh»tihf'ol K-niliosodiphenylaai i; a-lroaoohtnylphenvl | i u > Heiathlrrobfi.'t'e K!;S -•[M: B t l . ' KA°(; ug'l OJ o H -J 00 V U ' . U l ' . l Bct:.- KillR jg'l K.A 1/A HR KF | : R IR KR NR KR NR KR KF NR NR NR NR NR tm NR NR N l KR NR KR NR VR HP NR KR NR NR KR IIR Nf HR KF HR Kr K l tn HP IIR HR »R K l 'IR VB IP i... uu IDDI: SAKPIINI )H CNIMICAl l-OI 2/28/91 tP» CASI NO.: I59JJ lAI: CCNPUCHtN 1 i I L..^, I i i i I i I ] [• i: r \ m \ r 1 SITE INSPECTION „^^.^LIN6 RESULTS (cont'd) pfsriciDfs Silpit ID Ho. traltic Report No. Nilrli Units Dilution Faclor/CPC Cleanup IT) Percent Hoisture lIphi-tHC bela-IHC deUa-IHC gaiaa-IHC (lindane) Keptichlor Aldrin Heptachlor epoaida (ndosullin 1 Dieldrin 4,4'-00( Codrin (ndosulfan 11 4,4"-DDD (ndoiullaA sulfate «.l'-ODI tiethoiychlor (ndrin ketone ilphi-Chloidine gaiia-Chlordant loiaphe'ne AtocUi-1016 ltr6clor-l221 *roclor-l2J2 «roclor-IJ4J ; Arocloi-nil ; «roclor-l2SI ', «roclor-12iQ ', ;*I25-RIN; : 8GII9 1 NAUR : ug/l 1 [ virsimi tCl22 UMIR ug/l N/A N/A NR NR HR KR NR KR HR NR NR NR KR NR NR HR NR KR RR HR NR KR HR NR H) HR NR HR HR to o -J HOKS: lUnk ipict - coipound enilyiid for but not diticled I - coepound found in lib bliiik as veil as stipla, indicates possible/probable blink conliAinitioA ( - estiiated value J - estiiated value, coipound present biloK CIQI but above IDl I • analyiii did nol pats ( M OA/QC I - Presuiptive evidence of the presence ol the taterial analyiii nol required Detection liaill elevated if Dilution FiCtor )l and/or percent toisluie >0\ nil \-. FT) t < O • y\m\ H m i U DAI.. ./2I/9I m m i HO.: IS)]) U l HAHE: SItHNEfl IHOICAHtCS Seiple ID lo. Trifflc leport Ko. Iitrli Unttt Dilution Fictor i » 1 1-1 y i-L/w.' ' * SITE INSPECTION SAfi. uiNG RESULTS (cont'd) # 1 i. ) i 1 1 i \- i VI2S-GNIINS/KSDI NBFIOI HUP ug.'l VI25-C1(2 HBril02 NIIER ug/l V125-C»1(DUP1 NBFAOJ HAKI ug/l «I2S-CH KBFA04 •AIEI ug/l VIIS-GVS KBFtOS lAUH U9/1 yi2i-Q«l NBFA06 I t U R ug/L VliS-StOI NSFAOl SEDIHERI ig/kg VI25-St02 HIFAIO SEDINEHI •l/kg »12S-SE01 NBFtll SEOIHEHI ug/kg »12S-S(0IIDUP) KBFAI2 SEDINEHI •g/kg V125-SED5 HeFAII SEOIHEHI •9/kg y|2S-SEOI KBFtll SEDINEHI •g/kg y|2S-SI|NS/NSDl KIFAU SOU • 9 / k | 9125-SJ NIFAU . SOU i | / k | »I25-S1 MFtIS SOU •|/k| lluilnua Intlkony kriinic l i r l u i i i r r l l l u i Cidilui CiUlui Oiroilui Cobilt Copper Iron leid Xi|ieelui Hin|ineee KifCiirif llcMI rotiiiiui tileniui Silver lodlui I l i i l l l g i riaidiiii Ilic WUS: llink ipici - coipound inilyiid for but AOt ditictid ( • i i t i i i t i d vilue J • u t i l l t e d Tilui. coipound present belov CIDl but ibove 101 i - i n i l y i l i did nol piss (PA OA/QC l l - i n i l M i t not riouired J J eiioo J .121 E f (M.I 4|S00 J ^c» ( J J J iUOO i J L>:>4 4^100 .31] J J 14100 J J fltit.l Sl(SOO .400 i J 12^00 i i <.>''3.» itlaoo c ) l f . l J J J iibo J i 0OJ.1 40^00 r J O t . l t J J r/ioo J " C .» t l 00 J " " Q . n ! J 5M' tsioo J 90.3 45100 II.I I 14.f 41.4 2SI00 IS.I fllO 954 10.1 ( J oSO.3 I i J a f . c n . i 53.9 E 32400 J 3.2 E 115 14900 l i . 3 E 23.1 10.5 35100 f.5 lOiOO 1320 13.1 I 1490 (2.1 13.5 E 30100 J 4.1 E I t l J 19900 W . I E 24.1 12 39200 I.i I IIOO IIOO 14.1 E itOO E Jl^doo E Jfl/oO E' 590^00 ( 5 ) 2 ^ E Ij/oOO E J IMO E J 13.2 12.3 E 33(00 3.8 E 122 12100 11.8 E 25.4 il.t 31100 I.t I IIOO 1430 15.2 E IIOO 1150 E ei.i IJ.I E 9400 10100 21.1 E J I E 5.5 E 48.1 35.1 51200 5/,I E 13.1 31/ 113000 4tt 4140 925 41,1 E 4.5 42IQO 110 E tf.3 lOi 121000 - Ill 5000 1120 49.1 E J J J 1500 E irio E 13100 101 11100 I I . I E 13.4 si.r 21500 t M30 135 10.) E l l i o 14.J 142 E 21)00 21000 J l . l E l . l E 131 1)1 11)00 D.i ( 11.1 II.I 44101 n . j )I00 lose 11.1 E 11)0 11.1 31) E 1)100 4) E 21.1 )1.) 11)00 311 )420 91) 31.1 ( 1)20 13.5 312 E U> O O \\ 01/21/91 H SIU fAnr; /I (N(n|('.'. • IDDI: 0:''<I0|-C4 • fUnPllllG DAU: 2 / : ; ' ' l • [PA u s t NO.: 1 ! 1 : J U I : : ' n f ' i ! ( f < • tini'VOlAIIKS • Siaole ID >lo. • I r a l f i c Repo-I Ko. • Kalriit 1 Unit! 1 Dilutio.i faclor/crr C l n . u r n . 1 Percent iloisluie 1 Pentachlorophenol 1 Pheninlhrei^e 1 Anthracene Di-n-butylphlhalate Fluoranthene Pyrene lutylbeniylohlhjIalF J.J'-Dichlorob*niidine leniolalanlhracene Chrysene b i s l } - n h y ) h e i ' y n p h l . j l . . i ( Di-n-octylphlhalale leniolbllluorarlhenr bentolkUluoranthere lentolalpyrene lndenoll,;.3cdloyiei.e Oib'ent|a,hlanlhtac(i>e len(o|g,h,i)oerylen( ; HOKS: Blank space • coapouid aial';e': Jo- tut not delecUd 1 - coipound fruno in lal blani >• mW i : saaple. inditales r o i s i M t / i . i p : a t l f blank contaiination [ • estiialed value ) • estiiated value. (o>noun< o t t i n . l beloM CROl but atovF I U R • analysis lid nol p n ! EP-I OA.'i': H - Presuapli/e evi'ltnc' i-l He ; . ! i n { ( of Ihe a a t e r i i l HR - analysis nol i f o i i i * J Detection l i a i l s e l e v i l ' l i l t'lluH.-r. facloi >l and'or pe'trnl a j i s l m ; K • I . - ' I N : vi:5-uiM BCir- BCl.T KAUP NAUR ug/l ug/l 1 N/A N/A NR NR HR KR HR NR KR NR NR NR N^ NF IIR KR NR NF KR NR i/\BLE ! SITE INSPECTION SAMPLING RESULTS (cont'd) to o -J vn ' ^ 'I \ ] ) j M i l I ri/)i' r I ' ! .• i I i' { #1 V > • :i ;• 1 r DIE HAHE: V] CNEHICU IDOI: ei-)iei-04 tAKPlIlt DUE: 1/21/91 EPA CASE 10.: 15133 U l IIHE: SIIHHEI TABLE 1 SITE INSPECTION SAMPLING RESULTS (cont'd) IIOIMIICS tuple ID Ho. Iriffic Report Ho. Hitrli Uilti Dlltllon fictor Aluiliiiii litliony Ariiiiic l i r l u i I i r r l l l u i Cidalu* • CilcUi Chroilai Cobilt Copper Irta (lid lifaeilui Riniiniia Rerciry lickel rotiiiiui lllver lodlea l l i i l l l i i Yinidin line ; VI25-58 ; KBIA22 SOU : «9/k9 : I92P0 : J 11) • IIOOO 20 ( 19.5 • 43.1 . 25100 9.9 5M0 IPIP 10.3 f 2500 J 81.9 U . l ( VI25-RIHI VI25-RIH2 KBFAII K8FAt9 NAUR NAUR ug/l ug/l J J J J J '^•223 [ J O . ' ^ l . l J J i J 0.21 E J J . J J J 9125-IIUI I/A H/A U|/l III HI HI HI XI XI HI HI HI XI HI XI XI XI HI HI HH HI • HI HI HI Nl Kl XOIES: Hint ipitt - coipound inily;ed lor but •ot detected E - iitliited vilui J - iitlaitid yelue, conpound oresent bilON CROl but ibove IDl I - inilrili did not piss (PA QA'OC HI - inil|iiii not reouired to o M Ul ;o t (t> I < O Appendix N Figures Showing Previous Sampling Locations \WORK\2423l\02\WORKPLA.N.REP HARDING LAWSON ASSOCIATES 301753 Figure 10 ICC Plot Plan: Trenches T r e n c h e s 1-12 301754 > /i > I to o M vJ UT Ul ony RIVER eeo ' aOnitIO LOCATIONS 0 «' • • ' [ = € = : y = y 9 c « l « WAREHOUSE Figure 9 ICC Laboratory Pil U a b o r a l o r y P U 4 " P V C L i n o :((i) ---.-rrr 4 " P V C L i n e LOAOINC DOCK / t - / i fHvina sciCHCes. w c Cll.Ill ! t £ l>i*w»» Ity . . . n . . O J I » . . _ - " tu.uvl (ly ll*f ('<>• l u i i l '-i^tt.ttl. i n . . . . m "1 1 St. Croix, VI DPYING OVEN - toluene contaminated soil v m 80651095 1 1 y Right Side (North Side) NORIH ( Tcp View ) c3oor Coirosite soil sarrple frcm crying oven ° 1087001 - l e f t side (south side) ° #087002 - right side (north side) - 1 1 I I , J - • — door Ijsft Side (South Side) ( Not to Scale ) * Each rectangle represents one bin containing a stack of twenty trays. Figure 4 - Sarple location Map - Drying Oven jse-ft 3 0 1 7 5 6 ^ ^,,,ftr ^ - ' ' ^ ^^'*"" Berlex Laboratories St. Croix, VI VID 80651095 LAB WASTE DRAIJiAGE AREA - pyridine contaminated soil Building ® ® ® • ® ® ® • ® ® (foimer loading dock area) - — I ^ NORTH • ^ ) - Sanple locations for conposite Soil sanple frt^n north side of the lab Waste Drainage Area " Surface - #087003 " Subsurface - #087004 Soil sample fron south side of the lab Waste Drainage Area " Surface,- #087005 » Subsurface - #087006 ( Not to Scale ) Figure 5 - Sanple Location Map - Lab Waste Drainage Area 301757 irc/ri. r^ff-r t t ^ Q r t u t r i x Iy,-t^tt.\. Figure 3 flap qt .sarrpiincj_points 1 :3 J • a •I •a i *i O^S-SSS CD OD CD CD OD CD CD LAB..; '•^' IST ^ - - 7 L •«4-rt-«>..«r « . * « C*«wiCAl. h.OT fvwe M MC tJ^ PW M •-•—* X = Sanpiing point • = Production %^ell 301758 K o t t n c - a 1 , ^ C H I7.l1fl<- 5«^t«- t*C*Tl*rv^ CHEMICAL, ST. CROIX, U.S.V.l cnRprTr=f ATirvM Appendix O Compendium of Groundv^^ater Data \WORK\24231\02\WORiCPLAN.REP HARDING LAWSON ASSOCIATES 301760 n\ DATE: JECT: FROM: TO: UNITED STATES ENVIRONMENTAL PROTECTION AGENCY OCT 1 8 1990 REGION II Virgin Island Chemical Co. (VIChem) - Well Water Data John Higgins, P.E., On-Scene Coordinator Response & Prevention Branch Sherrel Hemy, Remedial Project Manager Eastern New York/Caribbean Remedial Action Branch Please find attached the, "Compendium of Well Water Data Collected at the Virgin Island Chemical Co. by the USEPA (1986-1990)." Thank you for reviewing the draft version. As we agreed, I am sending this report to Ms. Yvette Canegatta of the Virgin Island Department bf Natural Resources. This repon will also be appended to the VIChem OSC Report I can be contacted at (FTS) 340-6194, should you have any questions regarding the removal action ar VIChem. Attachment cc: Yvette Canegatta, VIDPNR ^ 301761 ^\r-/^i*^»t tt r- f^r^t t 4 o^s^v 4 ff^ in F \ COMPENDIUM OF WELL WATER DATA COLLECTED AT THE VIRGIN ISLAND CHEMICAL CO. BY THE USEPA (1986-19901 FOREWORD The piirpose of this report is to summarize pertinent sampling data and information regarding the volatile organic, well water data coUected by the United States Envirormiental Protection Agency (EPA) during various sampling events at, and in the vicinity of the Virgin Island Chemical Co. (VIChem) Hazardous Waste Site in St Croix during and prior to the 1990 Superfund Removal Action. Summary repons of ezch of these sampling events are included in the VIChem Removal Action Site Files. A review of the data indicates that Chloroform was consistently the dominant contaminant during each of the sampling events. For this reason, Chloroform results are included herein and are plotted in the attached graph, "Chloroform Contamination in Well Water - Virgin Island Chemical Co. Site, St. Croix". Since the purpose of this repon is to merely assemble pertinent data, and not to interpret the data or make recommendations based on the data, all analyzed data, including qualified and rejected data, are included in this report. It should be pointed out that the Drinking Water Maximum Contaminant Level for total trihalomethanes is 100 ug/l (See 40 CFR §141.12) and the 1980 Federal Water Quality Criteria for Chloroform (as revised), based on a carcinogenicity of IO"*, is 5.70 ug/l for human exposure from contaminated water and fish. COMPENDIUM •j 1. RCRA Enforcement (3/13/86) The Environmental Services Division (ESD) of Region 2 conducted a RCRA Enforcement Inspection of the VIChem facUity, then known as Berlex Laboratories, on March 13, .1986. The inspection included 3 soD samples taken from the intermittent stream, or "gut", on the site perimeter, 2 soil samples obtained from the laboratory water drainage pit, and one sample taken from Lhe production well in the northwest comer of the property. The results of the organic analysis from the production well indicated Chloroform contamination at a level of 130 ug/l. 2. St. Croix Well Survey Phase I (3/7/88-3/10/88) The Response and Prevention Branch (RPB) conducted well sampling for volatile organic constituents at 21 locations in St. Croix, including four wells in the vicinity of the VIChem Site. The data was rejected by the Monitoring Management Branch (MMB) due to excessive holding times. Chloroform contamination was indicated in the October 25, 1988 repon. 'Si. Croix Well Survey", prepared by Weston - TAT, as shown below: Well Name - Fairplains #6 Fairplains #9 . VIPA #1 VIPA #2 Chlorofonn (ug/l) 24 75 &70 11.5 11.3 3. St. Croix Well Survey Phase I (10/31/88-11/2/88) RPB resampled wells at eight locations, including four wells in the vicinity of the VIChem Site. Chloroform contamination was indicated as shown below: Well Name Fairplains #6 Fairplains #9 Fairplains #8 VIPA #2 Chloroform (ug/l)' 35.9 10.4 & 9.7 12.4 1.6U" "* Chloroform was not detected at the detection level of 1.6 ug/l. 3 017 62 4. VIChem Removal Action Phase I (1/17/90) During Phase I removal action activities at VIChem, three off-site wells and the on-site water tank were sampled for volatile organic contamination. Analytical services were provided by a private laboratory procured by the TAT. In addition to the routine QA/QC required for Level 2 Removal Program sampling, two performance evaluation samples and one blind duplicate sample were analyzed. TAT validated the data and, although QA/QC discrepansies were slight and few, the data was qualified as estimated. Once again, Chloroform was the most dominant compound in each sample; the data for this contaminant are shown below: Well Name Fairplains #6 Fairplains #9 Fairplains #8 Water Tank Chlorofonn (ug/I) 39.0 25.0 5.0 23.9* * This is an average of Chloroform contamination in the three tank samples (Water tank sample = 23.9 ug/l, Water tank drain sample = 22.7 ug/l. Water tank pump sample = 25.0 ug/l). 5. VIChem Removal Action Phase I f6/25/90) During Phase II removal action activities at VIChem, four off-site wells were sampled and analyzed for volatile organic contaminants. When detected, Chlorofonn was the most dominant compound in each sample and in 3 out of 4 samples the only VOC detected. Analytical services were provided by the Contract Laboratory Program and the data was validated by MMB. The only data qualified was for a QA/QC sample for a single compound. The Chloroform data for this sampling event are shown below: Well Name Fairplains #6 Fairplains #9 ' VIPA #1 VIPA #2 Chloroform (ug/l) 11 39 2J* ' 5U* * An estimated value of 2 ug/l was reported. ** Chloroform was not detected at the detection level of 5 ug/l. T** 301763 ll. t V - I Chloroform Contamination (ug/l) in fell Water • ^ -^a 00 o it^ <y^^kk ^ Vkg/n Island Chemical Site, St. Croix