Letter to Ms. Caroline Kwan, Remedial Project Manager, U.S. EPA, Region II, from Mr. Perry Katz, Principal Environmental Scientist, McLaren Hart, Inc., re: VICHEM Site, St.…

Collection: Federal Reference
Sub-shelf: EPA SEMS (Superfund, Region 2)
Kind: Government Report
Island: St. Croix
Date: 1994-10-06
Topics: Epstein Usvi
Pages: 75
Text: Native Text

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SDMS Document jmw?' 115547 ***VLi FACSIMILE AND U.S. MAIL*** Inc. December 15, 1997 Ms. Caroline Kwan U.S. Environmental Protection Agency Region n Emergency Remedial Response Division 290 Broadway, 20* Floor New York, New York 10007-1866 RE: VICHEM SITE ST. CROIX, U.S. VIRGIN ISLANDS NOVEMBER 1997 MONTHLY PROGRESS REPORT Dear Ms. Kwan: Tliis Progress Report has been prepared to document activities performed by McLaren/Hart, Inc. (McLaren/Hart) on behalf of Island Chemical Company (ICC) during the month of November 1997, for the Remedial Investigation (RI) of the Virgin Island Chemical Site in St. Croix, U.S. Virgin Islands (Site). This report has been prepared in accordance with the requirements specified in Section Vm of the Administrative Order on Consent (Consent Order) for this project effective October 6, 1994 (EPA Index No. H CERCLA-94-0401) and described in Section 5.1.2 of HLA Work Plan dated March 21, 1994 (including revisions dated August 5,1994, September 19, 1994, May 19,1997, and July 25, 1997). 1.0 COMPLIANCE ACTIVmES This section describes actions taken toward compliance with the Consent Order and describes Work Plan tasks implemented during November 1997. On November 4, 1997, McLaren/Hart forwarded correspondence to EPA to propose the installation of additional borings in the Aboveground-Storage Tank (AST) Area. On November 13, 1997 McLaren/Hart forwarded correspondence to EPA in response of a request by CDM -FPC for a determination of chloroform detection limits of the on-site field gas chromatograph (GC). On November 13, 1997, McLaren/Hart forwarded correspondence to EPA to summarize actions taken to complete the sediment-sampling program in the River, Bethlehem and Fairplain Guts. On November 17, 1997, the Monthly Progress Report for October 1997 was submitted to EPA. H:\GE0\ICOD0CUMENTMCC01S.D0C 25 Independence Boulevard, Warren, NJ 07059 (908) 647-8111 FAX (908) 647-8162 U) o o 00 <T\ IO Ms. Caroline Kwan December 15,1997 On November 18, 1997, McLaren/Hart forwarded correspondence to EPA to summarize historical chloroform concentrations and propose additional borings in the Process Pit Area. 2.0 RESULTS OF SAMPLING AND DATA GENERATED OR RECEIVED This section identifies the results of field sampling, analytical data (validated and/or invalidated), and other information received by the respondents. During the month of November, the data generated by McLaren/Hart as part of the Phase HI Remedial Investigation Activities was received by McLaren/Hart. The data generated included: • Soil sampling and analysis in the AST area, central storm drain areas. River Gut, and background samples; • Sediment sampling and analysis in the River Gut, Bethlehem Gut, and Fairplain Guts; and, • Sediment sampling and analysis in the central and southern storm drains. In addition, preliminary soil boring sampling results for the Process Pit Area and the Lab Pit Area are included for your information. These analytical results are subject to fiirther data validation. These validated results have been included as an attachment to this Monthly Progress Report. If you have any questions, do not hesitate to contact me at (908) 647-8111. lental Scientist Attach. cc: Terry Grimmer, Berlex Biosciences Lori G. Singer, Sills, Cummis, Zuckennan, Radin, Tischman, Epstein & Gross Cecil Williams, Virgin Islands Department of Planning and Natural Resources Syed Syedali, Virgin Islands Department of Planning and Natural Resources Pam Philip, CDM Federal Programs FUe H:\GE0\ICC\D0CUMENTMCC015.: M C i a / ^ * 300863 ENVIRONMENTAL ENGINEERING CORPORATION 0™cc»ap«»f ATTACHMENT NOVEMBER 1997 MONTHLY PROGRESS REPORT LIST OF TABLES Soil Boring Sampling ResuUs - Volatile Organic Compounds Soil Boring Sampling Results - Semivolatile Organic Compounds Soil Boring Sampling Results - Metals Gut and Storm Drain Surface Soil Sampling Results - Semivolatile Organic Compounds Gut and Storm Drain Surface Soil Sampling Results - Metals Gut and Storm Drain Surface Soil Sampling Resuhs - Physicochemical Parameters Gut and Storm Drain Surface Soil Sampling Results - Grain Size Analysis Fairplain Gut/Manning Bay Sediment Sampling Results - Semivolatile Organic Compounds Fairplain Gut/Manning Bay Sediment Sampling Results - Metals Fairplain Gut/Manning Bay Sediment Sampling Results - Physicochemical Parameters Fairplain Gut/Manning Bay Sediment Sampling Results - Grain Size Analysis Soil Boring Sampling Results - Biological Parameters Soil Boring Sampling Results - Physicochemical Parameters Preliminary Soil Boring SampUng Results, Process Pit Area - Volatile Organic Compounds Table 15 Preliminary Soil Boring Sampling Results, Lab Pit Area - Volatile Organic Compounds Table 1 Table 2 Table 3 Table 4 Table 5 Table 6 Table 7 Table 8 Table 9 Table 10 Table 11 Table 12 Table 13 Table 14 H:\GEO\ICC\DOCUMENTyicc015 aJUch.wpd MCiar^^ 300864 ENVIRONMENTAL ENGINEERING CORPORATION W wcycwdp.pef • TABLE 1 VIRGIN ISLAND CHEMICAL SITE SOIL BORING SAMPLING RESULTS VOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Chloromethane Bromomethane Vinyl Chloride Chloroethane Methylene Chloride Acetone Carbon Disulfide 1,1-Dichloroethene 1,1-Dichloroethane 1,2-Dichloroethene(total) Chloroform 1,2-Dichloroethane 2-Butanone 1,1,1-Trichloroethane Carbon Tetrachloride Bromodichloromethane 1,2-Dichloropropane cis-1,3-Dichloropn)pcne Trichloroethene Dibromochloromethane 1.1 ^Trichloroethane Benzene CAS#: 74-87-3 74-83-9 75-01-4 75-00-3 75-09-2 67-64-1 75-15-0 75-35-4 75-34-3 540-59-0 67-66-3 107-06-2 78-93-3 71-55-6 56-23-5 75-27-4 78-87-5 10061-01-5 79-01-6 12448-1 79-00-5 71-43-2 trans-1,3-Dichloropropene 10061-02-6 Bromoform 4-Methyl-2-Pentanone 2-Hexanone Tetrachloroethene 75-25-2 108-10-1 591-78-6 127-18^ 1,1,2,2-Tetrachloroethane 79-34-5 Toluene Chlorobenzene Ethylbenzene Styrene Xylene(total) 108-88-3 108-90-7 100-41-4 100-42-5 1330-20-7 River Gut SBRG-1/6-8 30-Sep-97 Soil 1 11 U 11 U 11 U 11 U 10 U 27 R 11 U 11 U 11 U 11 U 11 U 11 U 7 J 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 u I I U 11 u 11 u 11 u 11 u River Gut SBRG-1/12-14 30-Sep-97 Soil 1 12 U 12 U 12 U 12 U 10 U 34R 12 U 12 U 12 U 12 U 12 U 12 U 7 J 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U River Gut SBRG1/12-14D 30-Sq>-97 SoU 1 12 U 12 U 12 U 12 U 10 U 24 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U River Gut SBRG-2/2-4 26-Sep-97 Soil 1 12 U 12 U 12 U 12 U 13 U 4 R 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 2 J 12 U 12 U 12 U 12 U River Gut SBRG-2/4-6 26-Sep-97 SoU 1 13 U 13 U 13 U 13 U 30 U 150 R 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 4 J 13 U 13 U 13 U 13 U Notes All results reported in ug/kg Analyzed by CLP method OLMO 1.9 U = Analyte was not detected above the referenced reporting limit J = Indicates an estimated value B = Analyte was found in the blank as well as the sanple R = Data is unusable h:\chemhsk\island\soildata\tables\vocs.xls 12/12/97 3 0 0 8 6 5 TABLE 1 VIRGIN ISLAND CHEMICAL SITE SOIL BORING SAMPLING RESULTS VOLATILE ORGANIC COMPOUNDS • LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Chloromethane Bromomethane Vinyl Chloride Chloroethane Methylene Chloride Acetone Carbon Disulfide 1,1-Dichloroethene 1,1-Dichloroethane l,2-Dichloroethene(total) Chloroform 1,2-Dichloroethane 2-Butanone 1,1,1-Trichloroethane Carbon Tetrachloride Bromodichloromethane 1,2-Dichloropropane cis-l,3-Dichloropropene Trichloroethene Dibromochloromethane 1,1,2-Trichloroethane Benzene CAS#: 74-87-3 74-83-9 75-01-4 75-00-3 75-09-2 67-64-1 75-15-0 75-35-4 75-34-3 540-59-0 67-66-3 107-06-2 78-93-3 71-55-6 56-23-5 75-27-4 78-87-5 10061-01-5 79-01-6 12448-1 79-00-5 71-43-2 trans-1,3-Dichloropropene 10061-02-6 Bromoform 4-Methyl-2-Pentanone 2-Hexanone Tetrachloroethene 1,1,2,2-Tetrachloroethane Toluene Chlorobenzene Ethylbenzene Styrene Xylene(total) 75-25-2 108-10-1 591-78-6 127-18-4 79-34-5 108-88-3 108-90-7 10041-4 100-42-5 1330-20-7 River Gut SBRG-3/6-8 30-Sep-97 Soil 1 11 U 11 U 11 U 11 U 12 U 65 R 11 U 11 U 11 U 11 U 11 U 11 U 19 J 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 2J 11 U 11 U 11 U 4U River Gut SBRG-3/8-10 26-Sep-97 SoU 1 11 U 11 U 11 U 11 U 28 U 59 R 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U I I U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 9 J 11 U 11 U 11 U 5U Central Storm Drain SBCSD-1/16-18 23-Sep-97 SoU 1 12 U 12 U 12 U 12 U 13 U 27 U 12 U 12 U 12 U 12 U 12 U 12 U 12 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 1 J 12 U 12 U 12 U 12 U Central Storm Drain SBCSD-1/22-24 23-Sep-97 SoU 1 12 U 12 U 12 U 12 U 13 U 99 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 2 J 12 U 12 U 12 U 12 U Central Storm Drain SBCSD-2/18-20 23-Sep-97 SoU 1 12 U 12 U 12 U 12 U 12 U 230 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 2J 12 U 12 U 12 U 12 U Notes AU results reported in ug/kg Analyzed by CLP method OLMO 1.9 U = Analyte was not detected above the referenced reporting limit J = Indicates an estimated value B = Analyte was found in the blank as well as the sample R = Data is unusable h:\chemrisk\island\soUdata\tables\vocs.xls 12/12/97 3 0 0 8 6 6 TABLE 1 VIRGIN ISLAND CHEMICAL SITE SOIL BORING SAMPLING RESULTS VOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Chloromethane Bromomethane Vinyl Chloride Chloroethane Methylene Chloride Acetone Carbon Disulfide 1,1-Dichloroethene 1,l-Dichloroethane 1 >Dichloroethene(total) Chloroform 1,2-Dichloroethane 2-Butanone 1,1,1-Trichloroethane Carbon Tetrachloride Bromodichloromethane 1,2-Dichloropropane cis-1,3-Dichloropropene Trichloroethene Dibromochloromethane 1,1,2-Trichloroethane Benzene CAS#: 74-87-3 74-83-9 75-OM 75-00-3 75-09-2 67-64-1 75-15-0 75-35-4 75-34-3 540-59-0 67-66-3 107-06-2 78-93-3 71-55-6 56-23-5 75-27-4 78-87-5 10061-01-5 79-01-6 124-48-1 79-00-5 7M3-2 trans-l,3-Dichloropropene 10061-02-6 Bromoform 4-Methyl-2-Pentanone 2-Hexanone Tetrachloroethene 1,1,2,2-Tetrachloroethane Toluene Chlorobenzene Ethylbenzene Styrene Xvlene(total) 75-25-2 108-10-1 591-78-6 127-18^ 79-34-5 108-88-3 108-90-7 100-41-4 100-42-5 1330-20-7 Central Storm Drain SBCSD-2/20-22 23-Sep-97 SoU 1 12 U 12 U 12 U 12 U 13 U 200 U 12 U 12 U 12 U 12 U 12 U 12 U 5U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 2J 12 U 12 U 12 U 12 U Central Storm Drain SBCSD-3/10-12 23-Sep-97 SoU 1 11 U 11 u 11 u 11 u 17 U 130 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 u 11 u 11 u 11 u 11 u 11 u 11 u 11 u 11 u 11 u 4 J 11 u 11 u 11 u 1J Central storm Drain SBCSD-3/18-20 23-Sep-97 SoU 1 12 U 12 U 12 U 12 U 12 U 56 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 26 12 U 6 J 12 U 32 AST Area SBAST5A/20-22 16-Sep-97 SoU 1 12 U 12 U 12 U 12 U 18 U 86 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 75 12 U 130 AST Area SBAST5A/22-24 22-Sep-97 SoU 1 11 U 11 U 11 u 11 u 16 U 27 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 u 11 u 11 u 11 u 11 u 11 u 11 u 130 11 U 1000 Notes AU results reported in ug/kg Analyzed by CLP method OLMO 1.9 U = Analyte was not detected above the referenced reporting limit J = Indicates an estimated value B = Analyte was found in the blank as weU as the sanq>le R = Data is unusable h:\chemrisk\island\soUdata\tables\vocs.xls Page 3 of8 12/12/97 3 0 0 8 6 7 TABLE 1 VIRGIN ISLAND CHEMICAL SITE SOIL BORING SAMPLING RESULTS VOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Chloromethane Bromomethane Vinyl Chloride Chloroethane Methylene Chloride Acetone Carbon Disulfide 1,1-Dichloroethene 1,l-Dichloroethane 1,2-Dichloroethene(total) Chloroform 1,2-Dichloroethane 2-Butanone 1,1,1-Trichloroethane Carbon Tetrachloride Bromodichloromethane 1,2-Dichloropropane cis-l,3-Dichloropropene Trichloroethene Dibromochloromethane 1,1,2-Trichloroethane Benzene CAS#: 74-87-3 74-83-9 75-OM 75-00-3 75-09-2 67-64-1 75-15-0 75-35-4 75-34-3 540-59-0 67-66-3 107-06-2 78-93-3 71-55-6 56-23-5 75-27^ 78-87-5 10061-01-5 79-01-6 12448-1 79-00-5 7M3-2 trans-l,3-Dichloropropene 10061-02-6 Bromoform 4-Methyl-2-Pentanone 2-Hexanone Tetrachloroethene 75-25-2 108-10-1 591-78-6 127-18-4 1,1,2,2-Tetrachloroethane 79-34-5 Toluene Chlorobenzene Ethylbenzene Styrene Xylene(total) 108-88-3 108-90-7 100-41-4 100^2-5 1330-20-7 AST Area SBAST6A/20-22 22-Sep-97 SoU 1 11 U 11 U 11 U 11 U 16 U 28 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 u 11 u 11 u 11 u 11 u 3 J AST Area SBAST6A/22-24 22-Sep-97 SoU 1 12 U 12 U 12 U 12 U 16 U 18 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U AST Area SBAST7/20-22 9/18/97 SoU 1 13 U 13 U 13 U 13 U 21 U ; 87 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U AST Area SBAST7/22-24 9/18/97 SoU 1 12 U 12 U 12 U 12 U 16 U 600 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U Background Samole B-1 9/19/97 SoU 1 11 U 11 U 11 u 11 u 16 U 5U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 u 11 u 11 u 11 u 11 u 11 u 11 u 11 u 11 u 11 u 11 u 11 u 11 u 11 u 11 u Notes AU results reported in ug/kg Analyzed by CLP method OLMO 1.9 U = Analyte was not detected above the referenced reporting limit J = Indicates an estimated value B = Analyte was found in the blank as weU as the sample R = Data is unusable h:\chemrisk\island\soildata\tables\vocs.xls Page 4 of8 12/12/97 3 0 0 8 6 8 TABLE 1 VIRGIN ISLAND CHEMICAL SITE SOIL BORING SAMPLING RESULTS VOLATILE ORGANIC COMPOUNDS • LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: 1 Chloromethane Bromomethane Vinyl Chloride Chloroethane Methylene Chloride Acetone Carbon Disulfide 1,1-Dichloroethene 1.1-Dichloroethane 1,2-Dichloroethene(total) Chloroform 1,2-Dichloroethane 2-Butanone 1,1,1 -Trichloroethane Carbon Tetrachloride Bromodichloromethane 1,2-Dichloropropane cis-1,3-Dichloropropene Trichloroethene Dibromochloromethane 1,1 ^Trichloroethane Benzene CAS#: 74-87-3 74-83-9 75-01-4 75-00-3 75-09-2 67-64-1 75-15-0 75-35-4 75-34-3 540-59-0 67-66-3 107-06-2 78-93-3 71-55-6 56-23-5 75-27-4 78-87-5 10061-01-5 79-01-6 124^8-1 79-00-5 7M3-2 trans-1,3-Dichloropropene 10061-02-6 Bromoform 4-Methyl-2-Pentanone 2-Hexanone Tetrachloroethene 75-25-2 108-10-1 591-78-6 127-18-4 1,1,2,2-Tetrachloroethane 79-34-5 Toluene Chlorobenzene Ethylbenzene Styrene |Xylene(total) 108-88-3 108-90-7 lOO^M 100^2-5 1330-20-7 Background Sample B-2 9/19/97 SoU 1 13 U 13 U 13 U 13 U 20 U 9 U 13 U 13 U 13 U 13 U 13 U 13U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U Background Samnle B-3 ] 9/19/97 SoU 1 12 U 12 U 12 U 12 U 36 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U Background Sample 3-4 (DUP OF B-1 9/19/97 SoU 1 12 U 12 U 12 U 12 U 18 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U Field Blank FB091897 9/18/97 Sou 1 10 u 10 u 10 u 10 u 6BJ 62 B 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u Field Blank FB091997 9/19/97 SoU 1 10 u 10 u 10 u 10 u 4BJ 69 B 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u Notes AU results reported in ug/kg Analyzed by CLP method OLMO 1.9 U = Analyte was not detected above the referenced reporting limit J = Indicates an estimated value B = Analyte was found in the blank as weU as the sample R = Data is unusable h:\chemrisk\island\soUdata\tabIes\vocs.xls 12/12/97 3 0 0 8 6 9 TABLE 1 VIRGIN ISLAND CHEMICAL SITE SOIL BORING SAMPLING RESULTS VOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRK DILUTION FACTOR: ANALYTE: Chloromethane Bromomethane Vinyl Chloride Chloroethane Methylene Chloride Acetone Carbon Disulfide 1,1-Dichloroethene 1,1-Dichloroethane 1 ;j-Dichloroethene(total) Chloroform l-Dichloroethane 2-Butanone 1,1,1-Trichloroethane Carbon Tetrachloride Bromodichloromethane 1,2-Dichloropropane cis-1,3-Dichloropropene Trichloroethene Dibromochloromethane 1,1—Trichloroethane Benzene CAS#: 74-87-3 74-83-9 75-OM 75-00-3 75-09-2 67-64-1 75-15-0 75-35-4 75-34-3 540-59-0 67-66-3 107-06-2 78-93-3 71-55-6 56-23-5 75-27-4 78-87-5 10061-01-5 79-01-6 124-48-1 79-00-5 71-43-2 trans-l,3-Dichloropropene 10061-02-6 Bromoform 4-Methyl-2-Pentanone 2-Hexanone Tetrachloroethene 75-25-2 108-10-1 591-78-6 127-18^ 1,1,2—Tetrachloroethane 79-34-5 Toluene Chlorobenzene Ethylbenzene Styrene Xylene(total) 108-88-3 108-90-7 100-4M 100^2-5 1330-20-7 Field Blank FB092297 9/22/97 SoU 1 10 U 10 u 10 u 10 u 14 B 39 B 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u Field Blank FB092397 23-Sep-97 SoU 1 10 U 10 U 10 U 10 U 4BJ 22 B 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u Field Blank FB092497 9/24/97 Sou 1 10 u 10 u 10 u 10 u 4BJ 40 B 10 U 10 U 10 U 10 U 10 U 10 U 11 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u Field Blank FB092697 26-Sep-97 SoU 1 10 U 10 U 10 U 10 U 3BJ 190 B 10 U 10 U 10 U 10 U 10 U 10 U 4 J 10 U 10 U 10 U 10 U 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 3J Field Blank FB093097 30-Sep-97 SoU 1 10 u 10 u 10 u 10 u 5BJ 92 B 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 3J Notes AU results reported in ug/kg Analyzed by CLP method OLMO 1.9 U = Analyte was not detected above the referenced reporting limit J «Indicates an estimated value B = Analyte was found in the blank as weU as the sanple R = Data is unusable h:\chemrisk\island\soUdata\tables\vocs.xls Page 6 of8 12/12/97 300870 TABLE 1 VIRGIN ISLAND CHEMICAL SITE SOIL BORING SAMPLING RESULTS VOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Chloromethane Bromomethane Vinyl Chloride Chloroethane Methylene Chloride Acetone Carbon Disulfide 1.1-Dichloroethene 1,1-Dichloroethane 1 —Dichloroethene(total) Chloroform 1—Dichloroethane 2-Butanone 1,1,1-Trichloroethane Carbon Tetrachloride Bromodichloromethane 1 —Dlchloropropane cis-l,3-Dichloropropene Trichloroethene Dibromochloromethane 1,1,2-Trichloroethane Benzene CAS#: 74-87-3 74-83-9 75-OM 75-00-3 75-09-2 67-64-1 75-15-0 75-35-4 75-34-3 540-59-0 67-66-3 107-06-2 78-93-3 71-55-6 56-23-5 75-27-4 78-87-5 10061-01-5 79-01-6 124-48-1 79-00-5 71-43-2 trans-l,3-Dichloropropene 10061-02-6 Bromoform 4-Methyl-2-Pentanone 2-Hexanone Tetrachloroethene 1,1,2,2-Tetrachloroethane Toluene Chlorobenzene Ethylbenzene Styrene Xylene(total) 75-25-2 108-10-1 591-78-6 127-18-4 79-34-5 108-88-3 108-90-7 100-4M 100-42-5 1330-20-7 Trip Blank TB091897 9/18/97 SoU 1 10 U 10 u 10 u 10 u 4BJ 11 B 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u Trip Blank TB091997 9/19/97 SoU 1 10 u 10 u 10 u 10 u 25 B 14 B 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u Trip Blank TB092297 9/22/97 SoU 1 10 u 10 u 10 u 10 u 27 B HOB 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u Trip Blank TB092397 23-Sep-97 SoU 1 10 u 10 u 10 u 10 u 4BJ 10 U 10 U 10 U 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u Trip Blank TB092497 9/24/97 SoU 1 10 u 10 u 10 u 10 u 3BJ 7BJ 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u Notes AU results reported in ug/kg Analyzed by CLP method OLMO 1.9 U = Analyte was not detected above the referenced reporting limit J = Indicates an estimated value B = Analyte was found in the blank as weU as the sample R = Data is unusable h:\chemrisk\island\soUdata\tables\vocs.xls Page 7 of8 12/12/97 3 0 0 8 7 1 TABLE 1 VIRGIN ISLAND CHEMICAL SIIE SOIL BORING SAMPLING RESULTS VOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Chloromethane Bromomethane Vinyl Chloride Chloroethane Methylene Chloride Acetone Carbon Disulfide 1,1 -Dichloroethene 1,1-Dichloroethane 1 —Dichloroethene(total) Chloroform 1,2-Dichloroethane 2-Butanone 1,1,1-Trichloroethane Carbon Tetrachloride Bromodichloromethane 1,2-Dichloropropane cis-1,3-Dichloropropene Trichloroethene Dibromochloromethane 1,1—Trichloroethane Benzene CAS#: 74-87-3 74-83-9 75-01-4 75-00-3 75-09-2 67-64-1 75-15-0 75-35^ 75-34-3 540-59-0 67-66-3 107-06-2 78-93-3 71-55-6 56-23-5 75-27^ 78-87-5 10061-01-5 79-01-6 124-48-1 79-00-5 71-43-2 trans-l ,3-Dichloropropene 10061-02-6 Bromoform 4-Methyl-2-Pentanone 2-Hexanone Tetrachloroethene 75-25-2 108-10-1 591-78-6 127^18^ 1,1,2,2-Tetrachloroethane 79-34-5 Toluene Chlorobenzene Ethylbenzene Styrene Xylene(total) 108-88-3 108-90-7 10041-4 10O42-5 1330-20-7 Trip Blank TB092697 26-Sep-97 SoU 1 10 U 10 U 10 U 10 U 4BJ 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u Trip Blank TB093097 30-Sep-97 SoU 1 10 U 10 U 10 U 10 u 5BJ 6BJ 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u Notes AU results reported in ug/kg Analyzed by CLP method OLMO 1.9 U = Analyte was not detected above the referenced reporting limit J = Indicates an estimated value B = Analyte was found in the blank as weU as the sample R = Data is tmusable h:\chemrisk\island\soUdata\tables\vocs.xls Page 8 of8 12/12/97 300872 TABLE 2 VIRGIN ISLAND CHEMICAL SITE SOIL BORING SAMPLING RESULTS SEMIVOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DAli: SAMPLED: MA'IKIX DILUTION FACTOR: ANALYTE: Phenol Pyridine bis-(2-Chloroethyl) Ether 2-Chlorophenol 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene 2-Methylphenol 2,2'-oxybis (1-Chloropropane) 4-Methylphenol N-Nitroso-Di-n-Propylamine Hexachloroethene Nitrobenzene Isophorone 2-Nitrophenol 2,4-Diniethylphenol bis (2-Chloroethoxy) Methane 2,4-Dichlorophenol 1,2,4-Trichlorobenzene Naphthalene 4-Chloroaniline Hexachlorobutadiene 4-Chloro-3-Methylphenol 2-Methylnaphthalene Hexachlorocyclopentadiene 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2-ChloFonaphthalene 2-Nitroaniline Dimethyl Phthalate Acenaphthylene 2,6-Diiiitrotoluene 3-Nitroaniline Acen^hthene 2,4-DinitFophenol 4-Nitrophenol Dibenzoforan 2,4-Dinitrotoluene Diethylphthalate 4-Chlorophenyl-phenyl ether Fluorene h:\chemrisk\island\soildaU\tables\Svocs CAS#: 108-95-2 110-86-1 111-44-4 95-57-8 541-73-1 106-46-7 95-50-1 95-48-7 108-60-1 106-44-5 621-64-7 67-72-1 98-95-3 78-59-1 88-75-5 105-67-9 111-91-1 120-83-2 120-82-1 91-20-3 106-47-8 87-68-3 59-50-7 91-57-6 77-47-4 88-06-2 95-95-4 91-58-7 88-74-4 131-11-3 208-96-8 606-20-2 99-09-2 83-32-9 51-28-5 100-02-7 132-64-9 121-14-2 84-66-2 7005-72-3 86-73-7 River Gut SBRG-1/6-8 30-Sep-97 Sou 1 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 920 U 380 U 920 U 380 U 380 U 380 U 920 U 380 U 920 U 920 U 380 U 380 U 380 U 380 U 380 U Page 1 of River Gut SBRG-1/12-14 30-Sep-97 SoU 1 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 950 U 390 U 950 U 390 U 390 U 390 U 950 U 390 U 950 U 950 U 390 U 390 U 390 U 390 U 390 U 16 River Gut SBRG-2/2-4 26-Sep-97 Sou 1 > 400U 400 U 400U 400 U 400U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400U 400 U 980 U 400 U 980 U 400 U 400 U 400U 980 U 400 U 980 U 980 U 400 U 400U 400U 400 U 400 U River Gut SBRG-2/4-6 26-Sep-97 Sou 1 440 U 440 U 440 U 440 U 440 U 440 U 440 U 440 U 440 U 440 U 440 U 440 U 440 U 440 U 440 U 440 U 440 U 440 U 440 U 440 U 440 U 440 U 440 U 440 U 440 U 440 U 1100 U 440 U 1100 U 440 U 440 U 440 U 1100 U 440 U 1100 U 1100 U 440 U 440 U 440 U 440 U 58 J 12/ 300873 TABLE 2 VIRGIN ISLAND CHEMICAL SITE SOIL BORING SAMPLING RESULTS SEMIVOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: 4-Nitroaniline 4,6-Dinitro-2-Methylphenol N-Nitrosodiphenylamine 4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol Phenanthrene Anthracene Carbazole Di-n-Butylphthalate Fluoranthene Pyrene Butylbenzylphthalate 3,3'-Dichlorobenzidine Benzo(a)Anthracene Chrysene bis(2-Ethylhejtyl)Phthalate pi-n-Octyl Phthalate Benzo(b)Fluoranthene Benzo(k)Fluoranthene Benzo(a)Pyrene Indeno(l,2,3-cd)Pyrene pibenzo(a,h)Anthracene Benzo(g,h,I)Perylene CAS#: 100-01-6 534-52-1 86-30-6 101-55-3 118-74-1 87-86-5 85-01-8 120-12-7 86-74-8 84-74-2 206-44-0 129-00-0 85-68-7 91-94-1 56-55-3 218-01-9 117-81-7 117-84-0 205-99-2 207-08-9 50-32-8 193-39-5 53-70-3 191-24-2 River Gut SBRG-1/6-8 30-Sep-97 SoU 1 920 U 920 U 380 U 380 U 380 U 920 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U River Gut SBRG-1/12-14 30-Sep-97 SoU 1 950 U 950 U 390 U 390 U 390 U 950 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390U 390 U 390 U 390 U 390 U 390 U 390 U River Gut SBRG-2/2-4 26-Sep-97 SoU 1 980 U 980 U 400U 400U 400 U 980 U 400 U 400U 400U 400 U 400 U 400 U 130 J 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U River Gut SBRG-2/4-6 26-Sep-97 SoU 1 1100 U 1100 U 440 U 440 U 440 U 1100 U 440 U 440 U 440 U 440 U 440 U 440 U 440 U 440 U 440 U 440 U 440 U 440 U 440 U 440 U 440 U 440 U 440 U 440 U Notes All results reported in ug/kg Analyzed by CLP method OLMO 1.9 modified for pyridine analysis U = Analyte was not detected above the referenced reporting limit. J s Indicates an estimated value B = Analyte was found in the blank as weU as the sample R = Data is tmusable h:\chemrLsk\islai)d\soildat«\Ubles\Svocs Page2Qfl6 300874 12/12-97 TABLE 2 VIRGIN ISLAND CHEMICAL SITE SOIL BORING SAMPLING RESULTS SEMIVOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Phenol Pyridine bis-(2-Chloroethyl) Ether 2-Chlorophenol 1,3-Dichlorobenzene l,4-Dichlor6benzene 1,2-Dichlorobenzene 2-Methylphenol 2,2'-oxybis (1-Chloropropane) 4-Methylphenol N-Nitroso-Di-n-Propylamine Hexachloroethene Nitrobenzene Isophorone 2-Nitrophenol 2,4-Dimethylphenol bis (2-Chloroethoxy) Methane 2,4-Dichlorophenol 1,2,4-Trichlorobenzene Naphthalene 4-Chloroaniline Hexachlorobutadiene 4-Chloro-3-Methylphenol 2-Methylnaphthalene Hexachlorocyclopentadiene 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2-Chloronaphthalene 2-Nitroaniline Dimethyl Phthalate Acenaphthylene 2,6-Diiiitrotoluene 3-Nitroamline Acenaphthene 2,4-Dinitrophenol 4-Nitrophenol Dibenzofuran 2,4-Dinitrotoluene Diethylphthalate 4-ChIorophehyl-phenyl ether Fluorene h:\cheitirisk\island\soildata^labIes\Svocs CAS#: 108-95-2 110-86-1 111-44-4 95-57-8 541-73-1 106-46-7 95-50-1 95-48-7 108-60-1 106UM-5 621-64-7 67-72-1 98-95-3 78-59-1 88-75-5 105-67-9 111-91-1 120-83-2 120-82-1 91-20-3 106-47-8 87-68-3 59-50-7 91-57-6 77-47-4 88-06-2 95-95-4 91-58-7 88-74-4 131-11-3 208-%-8 606-20-2 99-09-2 83-32-9 51-28-5 100-02-7 132-64-9 121-14-2 84-66-2 7005-72-3 86-73-7 River Gut SBRG-3/6-8 30-Sep-97 SoU 1 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 850 U 350 U 850 U 350 U 350 U 350 U 850 U 350 U 850 U 850 U 350 U 350 U 350 U 350 U 1000 PageSol River Gut SBRG-3/8.10 26-Sep-97 SoU 1 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 920 U 380 U 920 U 380 U 380 U 380 U 920 U 380 U 920 U 920 U 380 U 380 U 380 U 380 U 2600 J •16 River Gut SBRG-1/12-14D 30-Sep-97 Sou 1 400 U 400U 400U 400U 400U 400 U 400U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400U 400U 400U 400 U 400 U 400 U 400U 400 U 400 U % 0 U 400U 960U 400U 400U 400U 960U 400 U 960 U 960 U 400U 400U 400U 400U 400 U Drain SBCSD-1/16-18 23-Sep-97 SoU 1 400 U 400 U 400U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400U 400 U 400 U 400 U 400 U 400 U 400 U 960 U 400 U 960 U 400 U 400 U 400 U % 0 U 400 U 960 U 960 U 400 U 400 U 1100 400 U 400 U 12/ 300875 TABLE 2 VIRGIN ISLAND CHEMICAL SITE SOIL BORING SAMPLING RESULTS SEMIVOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPLED: MAIRIX DILUTION FACTOR: ANALYTE: 4-Nitroaniline 4,6-Dinitro-2-Methylphenol N-Nitrosodiphenylamine 4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol Phenanthrene Anthracene Carbazole Di-n-Butylphthalate Fluoranthene Pyrene Butylbenzylphthalate 3,3 '-Dichlorobenzidine Benzo(a)Anthracene Chrysene bis(2-Ethymexyl)Phthalate Di-n-Octyl Phthalate Benzo(b)Fluoranthene Benzo(k)Fluoranthene Benzo(a)Pyrene Indeno(l,2,3-cd)Pyrene Dibenzo(a,h)Anthracene Benzo(g,h,I)Perylene CAS#: 100-01-6 534-52-1 86-30-6 101-55-3 118-74-1 87-86-5 85-01-8 120-12-7 86-74-8 84-74-2 206-44-0 129-00-0 85-68-7 91-94-1 56-55-3 218-01-9 117-81-7 117-84-0 205-99-2 207-08-9 50-32-8 193-39-5 53-70-3 191-24-2 River Gut SBRG-3/6-8 30-Sep-97 SoU 1 850 U 850 U 350 U 350 U 350 U 850 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U River Gut SBRG-3/8-10 26-Sep-97 SoU 1 920 U 920 U 380 U 380 U 380 U 920 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U River Gut SBRG-1/12-14D 30-Sep-97 Sou 1 960 U 960 U 400 U 400 U 400 U 960 U 400 U 400 U 400 U 400U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400U 400 U 400 U 400U 400 U 400 U 400 U Drain SBCSD-1/16-18 23-Sep-97 Sou 1 960 U 960 U 400 U 400 U 400 U 960 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U Notes All results reported in ug/kg Analyzed by CLP method OLMO 1.9 modified for pyridine analysis U = Analyte was not detected above the referenced reporting limit. J = Indicates an estimated value B = Analyte was found in the blank as weU as the sample R = Data is tmusable h:\cbemrisk\islaiKf\soildataMables\Svocs 12/12/97 300876 TABLE 2 VIRGIN ISLAND CHEMICAL SITE SOIL BORING SAMPLING RESULTS SEMIVOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Phenol Pyridine bis-(2-Chloroethyl) Ether 2-Chlorophenol 1,3-Dichlorobenzene 1,4-Dichlorobenzene l,2-Dichlor6benzene 2-Methylphenol 2,2'-oxybis (1-Chloropropane) 4-Methylphenol N-Nitroso-Di-n-Propylamine Hexachloroethene Nitrobenzene Isophorone 2-Nitrophenol 2,4-Dimethylphenol bis (2-Chloroethoxy) Methane 2,4-Dichlorophenol 1,2,4-Trichlorobenzene Naphthalene 4-Chloroaniline Hexachlorobutadiene 4-Chloro-3-Methylphenol 2-Methylnaphthalene Hexachlorocyclopentadiene 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2-Chloronaphthalene 2-Nitroaniline Dimethyl Phthalate Acenaphthylene 2,6-Dinitrotoluene 3-Nitroaiuline Acenaphthene 2,4-Dinitrophenol 4-Nitrophenol Dibenzofiiran 2,4-Dinitrotoluene Diethylphthalate 4-Chlorophenyl-phenyl ether Fluorene CAS#: 108-95-2 110-86-1 111-44-4 95-57-8 541-73-1 106-46-7 95-50-1 95-48-7 108-60-1 106-44-5 621-64-7 67-72-1 98-95-3 78-59-1 88-75-5 105-67-9 111-91-1 120-83-2 120-82-1 91-20-3 106-47-8 87-68-3 59-50-7 91-57-6 77-47-4 88-06-2 95-95-4 91-58-7 88-74-4 131-11-3 208-96-8 606-20-2 99-09-2 83-32-9 51-28-5 100-02-7 132-64-9 121-14-2 84-66-2 7005-72-3 86-73-7 CcuUal Stuim Drain SBCSD-1/22-24 23.Sep-97 SoU 1 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 960 U 400 U 960 U 400 U 400 U 400 U 960 U 400 U 960 U 960 U 400 U 400U 400 U 400 U 400 U Drain SBCSD-2/18-20 23-Sep-97 Sou 1 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 990 U 410 U 990 U 410 U 410 U 410 U 990 U 410 U 990 U 990 U 410 U 410 U 410 U 410 U 410 U Drain SBCSD-2/20-22 23-Sep-97 SoU 1 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 1000 U 410 U 1000 U 410 U 410 U 410 U 1000 U 410 U 1000 U 1000 U 410 U 410 U 410 U 410 U 410 U CcuUal Sluiui Drain SBCSD-3/10-12 24-Sep-97 Sou 1 370 U 370 U 370 U 370 U , 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 900 U 370 U 900U 370 U 370 U 370 U 900 U 370 U 900U 900 U 370 U 370 U 370 U 370 U 370 U h:\diemrisk\island\soildala\tables\Svocs 12/12/97 300877 TABLE 2 VIRGIN ISLAND CHEMICAL SITE SOIL BORING SAMPLING RESULTS SEMIVOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DAIE SAMPLED: MAIKIX DILUTION FACTOR: ANALYTE: 4-Nitroaniline 4,6-Dinitro-2-Methylphenol . N-Nitrosodiphenylamine 4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol Phenanthrene Anthracene Carbazole Di-n-Butylphthalate Fluoranthene Pyrene Butylbenzylphthalate 3,3'-Dichlorobenzidine Benzo(a)Anthracene Chrysene bis(2-Ethylhexyl)Phthalate Di-n-Octyl Phthalate Benzo(b)Fluoranthene Benzo(k)Fluoranthene Benzo(a)Pyrene Indeno(l,2,3-cd)Pyrene Dibenzo(a,h)Anthracene Benzo(g,h,I)Perylene CAS#: 100-01-6 534-52-1 86-30-6 101-55-3 118-74-1 87-86-5 85-01-8 120-12-7 86-74-8 84-74-2 206-44-0 129-00-0 85-68-7 91-94-1 56-55-3 218-01-9 117-81-7 117-84-0 205-99-2 207-08-9 50-32-8 193-39-5 53-70-3 191-24-2 Drain SBCSD-1/22-24 23-Sep-97 SoU 1 960 U 960 U 400 U 400 U 400 U 960 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U Drain SBCSD-2/18-20 23-Sep-97 SoU 1 990 U 990 U 410 U 410 U 410 U 990 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 61 J 410 U 410 U 410 U 410 U 410 U 410 U Drain SBCSD-2/20-22 23-Sep-97 SoU 1 1000 u 1000 u 410 U 410 U 410 U 1000 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 55 J 410 U 410 U 410 U 410 U 410 U 410 U CcnUal Stmm Drain SBCSD-3/10-12 24-Sep-97 Sou 1 900 U 900U 370 U 370 U 370 U 900U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 50 J 370 U 370 U 370 U 370 U 370 U 370 U 370 U Notes AU results reported in ug/kg Analyzed by CLP method OLMO 1.9 modified for pyridine analysis U = Analyte was not detected above the referenced reporting limit. J = Indicates an estimated value B = Analyte was fotmd in the blank as weU as the sample R = Data is tmusable h:\cfaemrisk\island\soildata\tables\Svocs 12/12/97 300878 TABLE 2 VIRGIN ISLAND CHEMICAL SITE SOIL BORING SAMPLING RESULTS SEMIVOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Phenol Pyridine bis-(2-Chloroethyl) Ether 2-Chlorophenol 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlor6ben2ene 2-Methylphenol 2,2'-03^is (l-Chloropropane) 4-Methylphenol N-Nitroso-Di-n-Propylamine Hexachloroethene Nitrobenzene Isophorone 2-Nitrophenol 2,4-Dimethylphenol bis (2-Chloroethoxy) Methane 2,4-Dichlorophenol 1,2,4-Trichlorobenzene Naphthalene 4-Chloroaniline Hexachlorobutadiene 4-Chloro-3 -Methylphenol 2-Methylnaphthalene Hexachlorocyclopentadiene 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2-ChloronaphthaIene 2-Nitroaniline Dimethyl Phthalate Acens^hthylene 2,6-Dinitrotoluene 3-Nitroaniline Acenaphthene 2,4-Dinitrophenol 4-Nitrophenol Dibenzofiiran 2,4-Dinitrotoluene Diethylphthalate 4-Chlorophenyl-phenyl ether Fluorene h:\chemrisk\island\soildala\tables\Svocs CAS#: 108-95-2 110-86-1 111-44-4 95-57-8 541-73-1 106-46-7 95-50-1 95-48-7 108-60-1 106-44-5 621-64-7 67-72-1 98-95-3 78-59-1 88-75-5 105-67-9 111-91-1 120-83-2 120-82-1 91-20-3 106-47-8 87-68-3 59-50-7 91-57-6 77-47-4 88-06-2 95-95-4 91-58-7 88-74-4 131-11-3 208-96-8 606-20-2 99-09-2 83-32-9 51-28-5 100-02-7 132-64-9 121-14-2 84-66-2 7005-72-3 86-73-7 Gc-uUal Stuim Drain SBCSD-3/18-20 24-Sep-97 SoU 1 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 940 U 390 U 940 U 390 U 390 U 390 U 940 U 390 U 940 U 940 U 390 U 390 U 390 U 390 U 390 U Page 7 of AST Area SBAST5A/20-22 22-Sep-97 SoU 1 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 930 U 380 U 930 U 380 U 380 U 380 U 930 U 380 U 930 U 930 U 380 U 380 U 380 U 380 U 380 U 16 AST Area SBAST5A/22-24 22-Sep-97 SoU 1 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 990 U 410 U 990 U 410 U 410 U 410 U 990 U 410 U 990 U 990 U 410 U 410 U 410 U 410 U 410 U AST Area SBAST6A/20-22 22-Sep-97 SoU 1 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 910 U 370 U 910 U 370 U 370 U 370 U 910 U 370 U 910 U 910 U 370 U 370 U 370 U 370 U 370 U 12/ 300879 TABLE 2 VIRGIN ISLAND CHEMICAL SITE SOIL BORING SAMPLING RESULTS SEMIVOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: 4-Nitroafliline 4,6-Dinitro-2-Methylphenol N-Nitrosodiphei^lamine 4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol Phenanthrene Anthracene Carbazole Di-n-Butylphthalate Fluoranthene Pyrene Butylbenzylphthalate 3,3 '-Dichlorobenzidine Benzo(a)Anthracene Chrysene bis(2-EtbyUiexyl)Phthalate Di-n-Octyl Phthalate Benzo(b)Fluoranthene Benzo(k)Fluoranthene Benzo(a)Pyrene Indeno(l,2,3-cd)Pyrcne Dibenzo(a,h)Anthracene Benzo(g,h,I)Perylene CAS#: 100-01-6 534-52-1 86-30-6 101-55-3 118-74-1 87-86-5 85-01-8 120-12-7 86-74-8 84-74-2 206-44-0 129-00-0 85-68-7 91-94-1 56-55-3 218-01-9 117-81-7 117-84-0 205-99-2 207-08-9 50-32-8 193-39-5 53-70-3 191-24-2 Drain SBCSD-3/18.20 24-Sep-97 SoU 1 940 U 940 U 390 U 390 U 390 U 940 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U AST Area SBAST5A/20-22 22-Sep-97 SoU 1 930 U 930 U 380 U 380 U 380 U 930 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U AST Area SBAST5A/22-24 22-Sep-97 SoU 1 990 U 990 U 410 U 410 U 410 U 990 U 410 U 410 U 410 U 410 U 410 U 410 U 140 J 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U AST Area SBAST6A/20-22 22-Sep-97 SoU 1 910 U 910 U 370 U 370 U 370 U 910 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U Notes AU results reported in ug/kg Analyzed by CLP method OLMO 1.9 modified for pyridine analysis U = Analyte was not detected above the referenced reporting limit. J = Indicates an estimated value B = Analyte was foimd in the blank as well as the sample R = Data is tmusable h:\cheinri8k\iatand\soilclata\tables\Svocs 12/12/97 3 0 0 8 8 0 TABLE 2 VIRGIN ISLAND CHEMICAL SITE SOIL BORING SAMPLING RESULTS SEMIVOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPLED: MAIRIX DILUTION FACTOR: ANALYTE: Phenol Pyridine bis-(2-Chloroethyl) Ether 2-Chlorophenol l,3-Dichlor6benzene 1,4-DichIorobenzene 1,2-Dichlorobenzene 2-Methylphenol 2,2'-oxybis (1-Chloropropane) 4-Methylphenol N-Nitroso-Di-n-Propylamine Hexachloroethene Nitrobenzene Isophorone 2-Nitrophenol 2,4-Dimethylphenol bis (2-Chloroethoxy) Methane 2,4-Dichlorophenol 1,2,4-Trichlorobenzene Naphthalene 4-Chloroaniline Hexachlorobutadiene 4-Chloro-3-Methylphenol 2-Methylrtaphthalene Hexachlorocyclopentadiene 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2-ChIoronaphthalene 2-Nitroaniline Dimethyl Phthalate Acenaphthylene 2,6-Dinitrotoluene 3-Nitroaniline Acenaphthene 2,4-Dinitrophenol 4-Nitrophenol Dibenzofiiran 2,4-Dinitrotoluene Diethylphthalate 4-Chlorophenyl-phenyl ether Fluorene CAS#: 108-95-2 110-86-1 111-44-4 95-57-8 541-73-1 106-46-7 95-50-1 95-48-7 108-60-1 106-44-5 621-64-7 67-72-1 98-95-3 78-59-1 88-75-5 105-67-9 111-91-1 120-83-2 120-82-1 91-20-3 106-47-8 87-68-3 59-50-7 91-57-6 77-47-4 88-06-2 95-95-4 91-58-7 88-74-4 131-11-3 208-96-8 606-20-2 99-09-2 83-32-9 51-28-5 100-02-7 132-64-9 121-14-2 84-66-2 7005-72-3 86-73-7 AST Area SBAST6A/22-24 22-Sep-97 SoU 1 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 950 U 390 U 950 U 390 U 390 U 390 U 950 U 390 U 950 U 950 U 390 U 390U 390 U 390 U 390 U AST Area SBAST7/20-22 9/18/97 SoU 1 420 U 420 U 420 U 420 U 420 U 420 U 420 U 420 U 420 U 420 U 420 U 420 U 420 U 420 U 420 U 420 U 420 U 420 U 420 U 420 U 420 U 420 U 420 U 420 U 420 U 420 U 1000 U 420 U 1000 U 420 U 420 U 420 U 1000 U 420 U 1000 U 1000 U 420 U 420 U 420 U 420 U 420 U AST Area SBAST7/22-24 9/18/97 SoU 1 400 U 400 U 400 U 400 U 400 U 400U 400 U 400 U 400 U 400 U 400 U 400U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 400 U 980 U 400U 980 U 400U 400 U 400U 980 U 400 U 980 U 980 U 400 U 400 U 400U 400 U 400 U Background B-1 9/19/97 SoU 1 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 900 U 370 U 900U 370 U 370 U 370 U 900U 370 U 900 U 900 U 370 U 370 U 370 U 370 U 370 U h:\chemrisk\island\soildata\tables\Svocs 12/12/97 300881 TABLE 2 VIRGIN ISLAND CHEMICAL SITE SOIL BORING SAMPLING RESULTS SEMIVOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPLED: MAIRIX DILUTION FACTOR: ANALYTE: 4-Nitroaniline 4,6-Dinitro-2-Methylphenol N-Nitrosodiphenylamine 4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol Phenanthrene Anthracene Carbazole Di-n-Butylphthalate Fluoranthene Pyrene Butylbenzylphthalate 3,3'-Dichlor6benzidine Benzo(a)Anthracene Chrysene bis(2-Ethylhexyl)Phthalate Di-n-Octyl Phthalate Benzo(b)Fluoranthene Benzo(k)Fluoranthene Benzo(a)Pyrene Indeno(l,2,3-cd)Pyrene Dibenzo(a,h)Anthracene Benzo(g,h,I)Peiylene CAS#: 100-01-6 534-52-1 86-30-6 101-55-3 118-74-1 87-86-5 85-01-8 120-12-7 86-74-8 84-74-2 206-44-0 129-00-0 85-68-7 91-94-1 56-55-3 218-01-9 117-81-7 117-84-0 205-99-2 207-08-9 50-32-8 193-39-5 53-70-3 191-24-2 AST Area SBAST6A/22-24 22-Sep-97 SoU 1 950 U 950 U 390 U 390 U 390 U 950 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U AST Area SBAST7/20-22 9/18/97 Sou 1 1000 U 1000 U 420 U 420 U 420 U 1000 U 420 U 420 U 420 U 420 U 420 U 420 U 420 U 420 U 420 U 420 U 420 U 420 U 420 U 420 U 420 U 420 U 420 U 420 U AST Area SBAST7/22-24 9/18/97 SoU 1 980 U 980 U 400U 400U 400 U 980 U 400U 400 U 400 U 400 U 400 U 400 U 400 U 400U 400U 400 U 400 U 400 U 400 U 400 U 400 U 400U 400U 400 U Background B-I 9/19/97 SoU 1 900U 900 U 370 U 370 U 370 U 900 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U Notes All results reported in ug/kg Analyzed by CLP method OLMO 1.9 modified for pyridine analysis U = Analyte was not detected above the referenced reporting limit J = Indicates an estimated value B = Analyte was found in the blank as weU as the san:q>le R = Data is tmusable b:\cfaeniiisk\island\sotldata\tables\Svocs 12/12/97 3 0 0 8 8 2 TABLE 2 VIRGIN ISLAND CHEMICAL SITE SOIL BORING SAMPLING RESULTS SEMIVOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Phenol Pyridine bis-(2-Chloroethyl) Ether 2-Chlorophenol 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlor6benzene 2-Methylphenol 2,2'-oxybis (1-Chloropropane) 4-Methylphenol N-Nitroso-Di-n-Propylamine Hexachloroethene Nitrobenzene Isophorone 2-Nitrophenol 2,4-Dimethylphenol bis (2-Chloroethoxy) Methane 2,4-Dichlorophenol 1,2,4-Trichlorobenzene Naphthalene 4-Chloroaniline Hexachlorobutadiene 4-Chloro-3-Methylphenol 2-Methylnaphthalene Hexachlorocyclopentadiene 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2-Chloronaphthalene 2-Nitroaniline Dimethyl Phthalate Acenaphthylene 2,6-Dinitrotoluene 3-Nitroaniline Acenaphthene 2,4-Dinitrophenol 4-Nitrophenol Dibenzofiiran 2,4-Dinitrotoluene Diethylphthalate 4-Chlorophenyl-phenyl ether [Fluorene CAS#: 108-95-2 110-86-1 111-44-4 95-57-8 541-73-1 106-46-7 95-50-1 95-48-7 108-60-1 106-44-5 621-64-7 67-72-1 98-95-3 78-59-1 88-75-5 105-67-9 111-91-1 120-83-2 120-82-1 91-20-3 106-47-8 87-68-3 59-50-7 91-57-6 77-47-4 88-06-2 95-95-4 91-58-7 88-74-4 131-11-3 208-96-8 606-20-2 99-09-2 83-32-9 51-28-5 100-02-7 132-64-9 121-14-2 84-66-2 7005-72-3 86-73-7 Background B-2 9/19/97 SoU 1 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 210 J 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 1100 U 430 U 1100 U 430 U 430 U 430 U 1100 U 430 U 1100 U 1100 U 430 U 430 U 430 U 430 U 430 U Background B-3 9/19/97 Sou 1 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 310 J 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 990 U 410 U 990 U 410 U 410 U 410 U 990 U 410 U 990 U 990 U 410 U 410 U 410 U 410 U 410 U Background B-4 (Dup of B-1) 9/19/97 SoU 1 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 940 U 390 U 940 U 390 U 390 U 390 U 940 U 390 U 940 U 940 U 390 U 390 U 390 U 390 U 390 U Field Blank FB091897 18-Sep-97 SoU 1 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 26 U 10 u 26 U 10 u 10 u 10 u 26 U 10 u 26 U 26 U 10 U 10 U 10 U 10 U 10 U h:\chemrisk\island\soildala\Ubles\Svocs 12/12/97 300883 TABLE 2 VIRGIN ISLAND CHEMICAL SITE SOIL BORING SAMPLING RESULTS SEMIVOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPLED: MAIRIX DILUTION FACTOR: ANALYTE: 4-Nitroaniline 4,6-Dinitro-2-Methylphenol N-Nitrosodiphenylamine 4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol Phenanthrene Anthracene Carbazole Di-n-Butylphthalate Fluoranthene Pyrene Butylbenzylphthalate 3,3'-Dichlorobenzidine Benzo(a)Anthracene Chrysene bis(2-EthyUiexyl)Phthalate Di-n-Octyl Phthalate Benzo(b)Fluoranthene Benzo(k)nuoranthene Benzo(a)Pyrene Indeno(l,2,3-cd)Pyrene Dibenzo(a,h)Anthracene Behzo(g,h,I)Perylene CAS#: 100-01-6 534-52-1 86-30-6 101-55-3 118-74-1 87-86-5 85-01-8 120-12-7 86-74-8 84-74-2 206-44-0 129-00-0 85-68-7 91-94-1 56-55-3 218-01-9 117-81-7 117-84-0 205-99-2 207-08-9 50-32-8 193-39-5 53-70-3 191-24-2 Background B-2 9/19/97 Sou 1 1100 U 1100 U 430 U 430 U 430 U 1100 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U Background B-3 9/19/97 Sou 1 990 U 990 U 410 U 410 U 410 U 990 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U 410 U Background B-4 (Dup of B-1) 9/19/97 Soil 1 940 U 940 U 390 U 390 U 390 U 940 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U Field Blank FB091897 18-Sep-97 SoU 1 26 U 26 U 10 U 10 U 10 U 26 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u Notes All resiUts reported in ug/kg Analyzed by CLP method OLMO 1.9 modified for pyridine analysis U = Analyte was not detected above the referenced reporting limit. J = Indicates an estimated value B = Analyte was foimd in the blank as weU as the sample R = Data is unusable h:\chemrisk\island\soiIdata^tables\Svocs 12/12/97 300884 TABLE 2 VIRGIN ISLAND CHEMICAL SITE SOIL BORING SAMPLING RESULTS SEMIVOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FAC 1 OR: ANALYTE: Phenol Pyridine bis-(2-Chloroethyl) Ether 2-Chlorophenol l,3-Dichlor6benzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene 2-Methylphenol 2,2'-oxybis (1-Chloropropane) 4-Methylphenol N-Nitroso-Di-n-Propylamine Hexachloroethene Nitrobenzene Isophorone 2-Nitrophenol 2,4-Dimethylphenol bis (2-Chloroethoxy) Methane 2,4-Dichlorophenol 1,2,4-Trichlorobenzene Naphthalene 4-Chloroaniline Hexachlorobutadiene 4-Chloro-3-Methylphenol 2-Methylnaphthalene Hexachlorocyclopentadiene 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2-Chloronaphthalene 2-Nitroanilin6 Dimethyl Phthalate Acenaphthylene 2,6-Dinitrotoluene 3-Nitroaniline Acenaphthene 2,4-Dinitrophenol 4-Nitrophenol Dibenzofiiran 2,4-Dinitrotoluene Diethylphthalate 4-Chlorophenyl-phenyl ether Fluorene h:\chenirisk\islaiid\soildata\tables\Svocs CAS#: 108-95-2 110-86-1 111-44-4 95-57-8 541-73-1 106-46-7 95-50-1 95-48-7 108-60-1 106-44-5 621-64-7 67-72-1 98-95-3 78-59-1 88-75-5 105-67-9 111-91-1 120-83-2 120-82-1 91-20-3 106-47-8 87-68-3 59-50-7 91-57-6 77-47-4 88-06-2 95-95-4 91-58-7 88-74-4 131-11-3 208-96-8 606-20-2 99-09-2 83-32-9 51-28-5 100-02-7 132-64-9 121-14-2 84-66-2 7005-72-3 86-73-7 Field Blank FB091997 19-Sep-97 Sou 1 11 U 11 U 11 u 11 u 11 u 11 u 11 u I I U 11 u 11 u I I U 11 u 11 u 11 u 11 u 11 u 11 u 11 u 11 u 11 u 11 u 11 u 11 u 11 u 11 u 11 u 27U 11 u 27 U 11 U 11 u 11 u 27 U 11 U 27 U 27 U 11 U 11 U 11 U 11 U 11 U Page 13 0 Field Blank FB092297 22-Sep-97 SoU 1 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 25 U 10 u 25 U 3 J 10 u 10 u 25 U 10 U 25 U 25 U 10 U 10 U 10 U 10 U 10 U fl6 FieldBlank FB092397 23.Sep-97 SoU 1 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 25 U 10 u 25 U 10 u 10 u 10 u 25 U 10 u 25 U 25 U 10 U 10 U 10 U 10 U 10 U Field Blank FB092497 24-Sep-97 Sou 1 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 25 U 10 u 25 U 10 u 10 u 10 u 25 U 10 u 25 U 25 U 10 U 10 U 1 J 10 U 10 U 12/ 300885 TABLE 2 VIRGIN ISLAND CHEMICAL SITE SOIL BORING SAMPLING RESULTS SEMIVOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: 4-Nitroaniline 4,6-Dinitro-2-Methylphenol N-Nitrosodiphenylamine 4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol Phenanthrene Anthracene Carbazole Di-n-Butylphthalate Fluoranthene Pyrene Butylbenzylphthalate 3,3'-Dichlorobenzidine Benzo(a)Anthracene Chrysene bis(2-Ethymexyl)Phthalate Di-n-Octyl Phthalate Benzo(b)Fluoranthene Benzo(k)Fluoranthene Benzo(a)Pyrene Indeno(l,2,3-cd)Pyrene Dibenzo(a,h)Anthracene Benzo(g,h,I)Perylene CAS#: 100-01-6 534-52-1 86-30-6 101-55-3 118-74-1 87-86-5 85-01-8 120-12-7 86-74-8 84-74-2 206-44-0 129-00-0 85-68-7 91-94-1 56-55-3 218-01-9 117-81-7 117-84-0 205-99-2 207-08-9 50-32-8 193-39-5 53-70-3 191-24-2 FieldBlank FB091997 19-Sep-97 SoU 1 27 U 27 U 11 U 11 U 11 U 27 U 11 U 11 U I I U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 4BJ 11 U 11 U 11 U 11 U 11 U I I U 11 U Field Blank FB092297 22-Sep-97 SoU 1 25 U 25 U 10 U 10 U 10 U 25 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 u 3 J 10 U 10 U 10 U 10 u 10 U 10 u 10 u FieldBlank FB092397 23-Sep-97 SoU 1 25 U 25 U 10 U 10 U 10 U 25 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 1 J 10 u 10 u 10 u 10 u 10 U 10 u 10 u FieldBlank FB092497 24-Sep-97 Sou 1 25 U 25 U 10 U 10 U 10 U 25 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u Notes All results reported in ug/kg Analyzed by CLP method OLMO 1.9 modified for pyridine analysis U = Analyte was not detected above the referenced reporting limit J = Indicates an estimated value B = Analyte was foimd in the blank as weU as the sample R = Data is tmusable li:\chenirisk\is!aiM)\soildata\tabIes\Svocs 300886 12/12/97 TABLE 2 VIRGEV ISLAND CHEMICAL SITE SOIL BORING SAMPLING RESULTS SEMIVOLATILE ORGANIC COMPOUNDS LOCATION: SAMPI ,E ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Phenol Pyridine bis-(2-Chloroethyl) Ether 2-Chlorophenol 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene 2-Methylphenol 2,2'-oxybis (1-Chloropropane) 4-Methylphenol N-Nitroso-Di-n-Propylamine Hexachloroethene Nitrobenzene Isophorone 2-NitrophenoI 2,4-Dimethylphenol bis (2-Chloroethoxy) Methane 2,4-Dichlorophenol 1,2,4-Trichlorobenzene Naphthalene 4-Chloroaniline Hexachlorobutadiene 4-Chloro-3 -Methylphenol 2-Methyhiaphthalene Hexachlorocyclopentadiene 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2-Chloronaphthalene 2-Nitroaniline Dimethyl Phthalate Acenaphthylene 2,6-Dinitrotoluene 3-NitroanUine Acenaphthene 2,4-Dinitrophenol 4-Nitrophenol Dibenzofiiran 2,4-Dinitrotoluene Diethylphthalate 4-Chlorophenyl-phenyl ether Fluorene h:\dieinrisk\island\soildata\labIes\Svocs CAS#: 108-95-2 110-86-1 111-44-4 95-57-8 541-73-1 106-46-7 95-50-1 95-48-7 108-60-1 106-44-5 621-64-7 67-72-1 98-95-3 78-59-1 88-75-5 105-67-9 111-91-1 120-83-2 120-82-1 91-20-3 106-47-8 87-68-3 59-50-7 91-57-6 77-47-4 88-06-2 95-95-4 91-58-7 88-74-4 131-11-3 208-96-8 606-20-2 99-09-2 83-32-9 51-28-5 100-02-7 132-64-9 121-14-2 84-66-2 7005-72-3 86-73-7 FieldBlank FB092697 26-Sep-97 SoU 1 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 25 U 10 u 25 U 10 U 10 u 10 u 25 U 10 U 25 U 25 U 10 U 10 U 10 U 10 U 10 U Page 15 0 Field Blank FB093097 30-Sep-97 SoU 1 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 25 U 10 u 25 U 10 u 10 u 10 u 25 U 10 u 25 U 25 U 10 U 10 U 2 J 10 U 10 U ri6 12/12/97 300887 TABLE 2 VIRGIN ISLAND CHEMICAL SITE SOIL BORING SAMPLING RESULTS SEMIVOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPLED: MAIRIX DILUTION FACTOR: ANALYTE: CAS #: 4-Nitroaniline 100-01-6 4,6-Dinitro-2-Methylphenol 534-52-1 N-Nitrosodiphenylamine 86-30-6 4-Bromophenyl-phenylether 101-55-3 Hexachlorobenzene 118-74-1 Pentachlorophenol 87-86-5 Phenanthrene 85-01-8 Anthracene 120-12-7 Carbazole 86-74-8 Di-n-Butylphthalate 84-74-2 Fluoranthene 206-44-0 Pyrene 129-00-0 Butylbenzylphthalate 85-68-7 3,3'-Dichlorobenzidine 91-94-1 Benzo(a)AnthTacene 56-55-3 Chrysene 218-01-9 bis(2-Ethylhexyl)Phthalate 117-81-7 Di-n-Octyl Phthalate 117-84-0 Benzo(b)Fluoranthene 205-99-2 Benzo(k)Fluoranthene 207-08-9 Benzo(a)Pyrene 50-32-8 Indeno(l,2,3-cd)Pyi«ne 193-39-5 Dibenzo(a,h)Anthracene 53-70-3 Benzo(g,h,I)Perylene 191-24-2 FieldBlank FB092697 26-Sep-97 SoU 1 25 U 25 U 10 U 10 U 10 U 25 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u FieldBlank FB093097 30-Sep-97 SoU 1 25 U 25 U 10 U 10 U 10 U 25 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 u I B J 10 U 10 U 10 U 10 u 10 u 10 u 10 u Notes All results reported in ug/kg Analyzed by CLP method OLMO 1.9 modified for pyridine analysis U = Analyte was not detected above the referenced reporting limit } = Indicates an estimated value 6 = Analyte was found in the blank as weU as the sample R = Data is unusable h:\cheinrisk\island\soildata\tables\Svocs 12/12/97 300888 TABLE 3 VIRGEV ISLAND CHEMICAL SITE SOIL BORING SAMPLING RESULTS METALS LOCATION: SAMPLE ID NO: DATE SAMPLED MATRIX DILUTION FACTOR: ANALYTE: Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper jlron Lead Magnesium Manganese Mercury Nickel Potassium Selenium SUver Sodium ThaUium Vanadium Zinc Cyanide CAS#: 7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-O2-O 7440-09-0 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6 57-12-5 River Gut SBRG-1/6-8 30-Sep-97 SoU 12700 0.46 U 0.3 U 59.5 0.02 U 0.14 B 33200 18.8 9.7 B 32.4 J 21800 3.7 J 5550 402 J 0.11 U 8.9 B 1290 J 0.57 U 0.14 UJ 617 B 0.51 U 77.5 39.2 R 0.56 U River Gut SBRG-1/12-14 30-Sep-97 SoU 13800 0.48 U 0.52B BJ 114 0.02 U 0.18 BJ 24200 R 25 13.1 44.5 J 25900 2.1 J 6990 673 J 0.12 U 10.7 1270 J 06 U 0.14 UJ 858 B 0.52 U 88 47 R 0.59 U River Gut SBRG-1/12-14-D 30-Sep-97 SoU 11600 0.48 U 1.3 BJ 114 0.02 U 0.16 B 12900 15.9 13.8 39.9 R 2110 2.8 J 4630 544 J 0.12 U 8.1 B 933 B 0.6 U 0.14 UJ 604 B 0.53 U 786 29.9 R 0.59 U River Gut SBRG-2/2-4 26-Sep-97 SoU 9910 0.49 U 0.81 BJ 46.9 B 0.02 U 0.2 B 5850 12.2 9.8 B 25.8 J 14200 3.7 J 2880 148 J 0.12 U 6.6 B 1060 B 0.61 U 0.15 UJ 389 B 0.54 U 64.8 25.6 J 061 U River Gut SBRG-2/4-6 26-Sep-97 SoU 12100 0.53 U 0.89 BJ 62.2 0.03 U 0.1 B 25900 16 10.6 B 32.7 J 18700 6.2 J 3840 327 J 0.13 U 7.8 B 1530 J 0.67 U 0.16 UJ 548 B 0.59 U 85.3 32.4 J 0.64 U Notes AU results reported in mg/kg Analyzed by CLP method ILMO 3.0 U = Analyte was not deteced above the referenced reporting limit J = Indicates an estimated value B = Result is between the instrument detection limit (IDL) and the contract required detection limit (CRDL) R = Data is unvisable h:\chemrisk\island\soUdata\tables\metals.xls Page 1 of6 12/12/97 300889 TABLE 3 VIRGIN ISLAND CHEMICAL SITE SOIL BORING SAMPLING RESULTS METALS LOCATION: SAMPLE ID NO: DATE SAMPLED MATRIX DILUTION FACTOR: ANALYTE: Aluminum Antimony Arsenic Barium BeryUium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium SUver Sodium ThaUium Vanadium Zinc Cyanide CAS#: 7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-0 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6 57-12-5 River Gut SBRG-3/6-8 30-Sep-97 SoU 11200 0.43 0.52 57.9 0.02 0.26 31700 13.3 10.9 35.1 19400 3.8 5100 440 0.11 106 1460 0.53 0.13 411 0.47 65.8 56.3 0.52 U BJ U BJ J J J U J u UJ B U R U River Gut SBRG-3/8-10 26-Sep-97 SoU 6620 0.46 1.5 41.1 0.02 0.02 27000 7.5 7.8 26.2 12200 3.9 3040 247 0.11 5.2 679 1.1 0.14 377 0.51 47.2 22.7 0.57 U BJ B U U B J J J U B B U B U J U Central Storm Drain SBCSD-1/16-18 23-Sep-97 SoU 11500 0.48 U 0.39 BJ 209 0.02 U 0.13 B 4460 18.3 12.9 41.5 J 23500 2 J 6370 724 J 0.12 U 10.2 1550 J 2.2 0.14 U 1750 J 0.53 U 97 35.5 R 06 U Central Storm Drain SBSCD-1/22-24 23-Sep-97 SoU 8470 U 0.48 U 0.4 BJ 22.5 B 0.02 U 0.09 B 3280 17.6 7.4 B 29 J 18300 0.87 J 3970 139 J 0.12 U 6.3 B 1080 B 0.6 U 0.14 U 810 B 0.53 U 71.1 29 R 0.59 U Central Storm Drain SBSCD2(18-20) 23-Sep-97 SoU 10500 0.49 U 0.32 U 85.3 0.02 U 0.08 B 13300 13.2 11 B 39.7 J 18700 2 J 5340 483 J 0.15 7.9 B 1380 J 0.62 U 0.15 U 697 B 0.54 U 72 29.8 R 0.59 U Notes All results reported in mg/kg Analyzed by CLP method ILMO 3.0 U = Analyte was not deteced above the referenced reporting limit J = Indicates an estimated value B = Result is between the instrument detection limit (IDL) and the contract required detection limit (CRDL) R = Data is unusable h:\chemrisk\island\soildata\tables\metals.xls Page 2 of6 12/12/97 300890 TABLE3 VIRGIN ISLAND CHEMICAL SITE SOIL BORING SAMPLING RESULTS METALS LOCATION: SAMPLE ID NO: DATE SAMPLED MATRIX DILUTION FACTOR: ANALYTE: Aluminum Antimony Arsenic Barium BetyUium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercmy Nickel Potassium Selenium SUver Sodium ThaUium Vanadium Zino Cyanide CAS#: 7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-0 7782^9-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6 57-12-5 Central Storm Drain SBSCD2(20-22) 23-Sep-97 SoU 10400 0.5 U 0.71 BJ 111 0.02 U 0.1 23000 13 12.3 B 36.1 J 19900 2.1 J 5510 1050 J 0.14 8 B 1430 J 1.9 0.15 U 773 B 0.55 U 75 28.8 R 0.62 U Central Storm Drain SBCSD3(10-12) 24-Sep-97 SoU 14000 0.45 U 0.54 BJ 130 0.02 U 0.2 B 24800 19.4 15.8 58.9 J 25500 3.7 J 6250 556 J 0.1 U 12.5 2100 J 1.6 0.13 U 7150 B 0.49 U 97.5 50.3 J 0.56 U Central Storai Drain SBCSD3(18-20) 24-Sep-97 SoU 7830 0.47 U 0.31 U 45 B 0.02 U 0.09 B 7030 126 8.9 B 45.5 J 13500 2.7 J 3400 101 J 0.12 U 6.8 B 645 B 0.59 U 0.14 U 933 B 0.52 U 72.4 29.7 R 0.58 B AST Area SBAST5A/20-22 22-Sep-97 SoU 6520 0.47 0.73 74.5 0.02 0.02 2830 126 8.8 21.9 14200 1.8 3240 404 0.11 56 672 1.4 0.14 480 0.51 63.6 21.4 0.69 U BJ U U R B J J J U B B U B U R B AST Area SBAST5A/22-24 22-Sep-97 SoU 7260 0.49 U 0.93 BJ 59.2 0.02 U 0.02 U 3260 R 10.1 7.3 B 20.3 J 13700 1.2 J 3230 484 J 0,12 U 4.7 B 673 B 0.62 U 0.15 U 538 B 0.54 U 54.8 22.4 R 0.58 U Notes AU results reported in mg/kg Analyzed by CLP method ILMO 3.0 U = Analyte was not deteced above the referenced reporting limit J = Indicates an estimated value B = Result is between the instrument detection limit (DDL) and the ccmtract required detection limit (CRDL) R = Data is unusable h:\cheinrisk\island\soUdata\tables\metaIs.xls Page 3 of6 12/12/97 3 0 0 8 9 1 TABLE 3 VIRGIN ISLAND CHEMICAL SITE SOIL BORING SAMPLING RESULTS METALS LOCATION: SAMPLE ID NO: DATE SAMPLED MATRIX DILUTION FACTOR: ANALYTE: Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercuiy Nickel Potassium Selenium SUver Sodium ThaUium Vanadium Zinc Cyanide CAS#: 7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-0 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6 57-12-5 AST Area SBAST6A/20-22 22-Sep-97 SoU 7510 0.45 U 0.52 BJ 103 0.02 U 0.11 B 3530 R 9.1 15.1 27.6 J 17400 2.3 J 4190 811 J 0.11 U 8.4 B 691 B 0.57 U 0.14 U 541 B 0.5 U 72.5 27 R 0.56 U AST Area SBAST6A/22-24 22-Sep-97 SoU 7850 0.48 U 0.92 BJ 151 0.02 U 0.1 B 3760 R 10.4 15.9 32.7 J 17100 2.7 J 3920 1340 J 0.1 U 8.4 B 795 B 0.6 U 0.14 U 839 B 0.52 U 79.4 27 R 0.59 U AST Area SBAST 7/20-22 9/18/97 SoU 9180 0.51 U 0.45 BJ 77 0.03 U 0.08 B 32600 13.4 9.9 B 30.1 R 18400 2.2 J 4800 482 J 0.12 U 6.9 B 894 B 063 U 0.15 U 705 B 0.56 U 73.1 , 27.9 R 0.62 U AST Area SBAST 7/22-24 9/18/97 SoU 8850 0.49 U 16 BJ 95 0.02 U 0.12 B 4010 15.1 11.5 B 31.5 R 20600 1.7 J 4110 718 J 0.12 U 7 B 794 B 061 U 0.15 U 759 B 0.54 U 95.3 29.9 R 061 U AST Area FB091897 18-Sep-97 SoU 17.8 B 11.5 B 1.3 U 1.4 B 0.1 U 0.1 U 1550 B 2.5 B 0.2 U 82.8 69.2 B 1.1 U 48.5 B 7.2 B 0.2 U 36 B 90.3 B 2.5 J 0.6 U 352 B 2.2 U 0.95 B 166 Notes AU results reported in mg/kg Analyzed by CLP method ILMO 3.0 U = Analyte was not deteced above the referenced reporting limit J = Indicates an estimated value B = Result is between the instrument detection limit (DDL) and the contract required detection limit (CRDL) R = Data is unusable h:\chemrisk\island\soUdata\tables\metals.xls Page 4 of6 12/12/97 3 0 0 8 9 2 TABLE 3 VIRGIN ISLAND CHEMICAL SITE SOIL BORING SAMPLING RESULTS METALS LOCATION: SAMPLE ID NO: DATE SAMPLED MATRIX DILUTION FACTOR: ANALYTE: Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium SUver Sodium ThaUium Vanadium Zinc Cyanide CAS#: 7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-0 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6 57-12-5 Backffround B-1 9/19/97 SoU 12200 0.45 0.29 35.8 0.02 0.23 81700 12 12 31.5 19500 11.5 7010 603 0.13 8.8 1970 0.87 0.13 393 0.49 50.4 106 0.55 U U B U B J J J B J B U B U R U Background B-2 9/19/97 SoU 9790 0.53 1.3 49.7 0.03 0.04 80700 10.9 6.6 19.7 11900 3.1 4620 398 0.14 6.5 3290 0.66 0.16 232 0.58 29.5 45.8 0.65 U BJ B U B B J J J B J U U B U R U Background B-3 9/19/97 SoU 11700 0.49 0.7 119 0.02 0.77 42400 13.6 10.2 44 18800 15.2 5390 497 0.18 7.7 2570 0.62 0.15 365 0.54 59.7 127 06 U BJ U B B J J J B J U U B U R U Background B-4 (Dap of B-1) 9/19/97 SoU 10100 0.47 U 0.76 BJ 31.3 B 0.02 U 0.12 B 65900 9.8 9.3 B 256 J 14900 10.8 J 5430 484 J 0.14 7 B 1800 J 0.59 U 0.14 U 345 B 0.52 U 39 96.7 R 0.57 U FieldBlank FB091997 19-Sep-97 Water 86.2 B 2 U 1.3 U 2.3 B 0.1 U 0.1 U 13000 J 0.5 B 0.2 U 2.5 B 15.1 U 1.1 U 335 B 9.9 B 0.2 U 0.7 U 131 B 2.5 U 0.6 U 175 B 2.2 U 16 B 381 Notes AU results reported in mg/kg Analyzed by CLP method ILMO 3.0 U = Analyte was not deteced above the referenced reporting limit J = Indicates an estimated value B = Result is between the instrument detection limit (IDL) and the contract required detection limit (CRDL) R = Data is unusable h:\chemrisk\island\soiIdata\tables\metals.xls Page 5 of6 12/12/97 3 0 0 8 9 3 TABLE 3 VIRGBV ISLAND CHEMICAL SITE SOIL BORING SAMPLING RESULTS METALS LOCATION: SAMPLE ID NO: DATE SAMPLED MATRIX DILUTION FACTOR: ANALYTE: Aluminum Antimony Arsenic Barium BeryUium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercuiy Nickel Potassium Selenium SUver Sodium ThaUium Vanadium Zinc Cyanide CAS#: 7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-0 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6 57-12-5 FieldBlank FB092297 22-Sep-97 Water 102 B 2 U 1.3 U 2.3 B 0.1 U 0.1 U 16200 J 0.38 B 0.2 U 1.5 U 15.1 U 1.1 U 443 B 12.4 B 0.2 U 0.7 U 175 B 2.5 U 0.6 U 128 B 2.2 U 1.4 B 452 FieldBlank FB092397 23-Sep-97 Water 15.3 B 2 U 1.3 U 1.4 B 0.1 U 0.1 U 2590 B 0.2 U 0.2 U 1.5 U 15.1 U 1.1 U 59.1 B 2.6 B 0.2 U 0.7 U 60.4 B 2.5 U 0.6 U 119 B 2.2 U 16 B 46.6 FieldBlank FB092497 24-Sep-97 Water 5 B 2 U 1.3 U 1.2 B 0.1 U 0.1 U 1810 B 0.2 U 0.2 U 1.5 U 15.1 U 1.1 U 42.9 B 16 B 0.2 U 0.7 U 29.6 B 2.5 U 0.6 U 42.6 B 2.2 U 1 B 42.8 FieldBlank FB092697 26-Sep-97 Water 8.7 B 6 B 1.3 U 1.3 B 0.1 U 0.1 U 56500 B 0.26 B 0.2 U 1.8 B 27.8 B 1.1 U 15.7 B 1 B 0.2 U 0.7 U 15.7 B 2.5 U 0.6 U 21900 B 2.2 U 1.4 B 5.4 B 8 B FieldBlank FB093097 30-Sep-97 Water 129 B 2 U 1.3 U 1.8 B 0.1 U 0.1 U 11500 J 0.24 B 0.2 U 2 B 15.1 U 1.1 U 34800 B 11.4 B 0.2 U 0.7 U 100 B 2.5 U 0.6 U 804 B 2.2 U 16 B 432 5 U Notes AU results reported in mg/kg Analyzed by CLP method ILMO 3.0 U = Analyte was not deteced above the referenced reporting limit J = Indicates an estimated value B = Result is between the instrument detection limit (IDL) and the contract required detection limit (CRDL) R = Data is unusable h:\cheinrisk\island\soildata\tables\metals.xls Page 6 of6 12/12/97 300894 TABLE 4 VIRGIN ISLAND CHEMICAL SITE GUT AND STORM DRAIN SURFACE SOIL SAMPLING RESULTS SEMIVOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Phenol Pyridine bis-(2-Chlon)ethyl) Ether 2-ChIorophenol 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene 2-Methylphenol 2,2'-oxybis (I-Chloropropane) 4-Methylphenol N-Nitroso-Di-n-Propylamine Hexachloroethene Nitrobenzene Isophorone 2-Nitrophenol 2,4-Dimethylphenol bis (2-Chloroethoxy) Methane 2,4-Dichlorophenol 1,2,4-Trichlorobenzene Naphthalene 4-Chloroaniline Hexachlorobutadiene 4-Chloro-3-Methylphenol 2-Methylnaphthalene Hexachlorocyclopentadiene 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2-Chloronaphthalene 2-Nitroaniline Dimethyl Phthalate Acenaphthylene 2,6-Dinitrotoluene 3-Nitroaniline Acenaphthene 2,4-Dinitrophenol 4-Nitrophenol Dibenzofiiran 2,4-Dinitrotoluene Diethylphthalate CAS#: 108-95-2 110-86-1 111-44-4 95-57-8 541-73-1 106-46-7 95-50-1 95-48-7 108-60-1 106-44-5 621-64-7 67-72-1 98-95-3 78-59-1 88-75-5 105-67-9 111-91-1 120-83-2 120-82-1 91-20-3 106-47-8 87-68-3 59-50-7 91-57-6 77-47-4 88-06-2 95-95-4 91-58-7 88-74-4 131-11-3 208-96-8 606-20-2 99-09-2 83-32-9 51-28-5 100-02-7 132-64-9 121-14-2 84-66-2 Bethlehem Gut BG-l 16-Sep-97 1 SoU 1 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 1200 500 1200 500 500 500 1200 500 1200 1200 500 500 500 U U U U u U U U u U U u u u u u u u u u u U u u U u u u u u u u u u u U u u u Bethlehem Gut BG-2 16-Sep-97 1 SoU 1 350 350 350 350 350 350 350 350 350 350 350 350 350 350 350 350 350 350 350 350 350 350 350 350 350 350 850 350 850 350 350 350 850 350 850 850 350 350 350 u u U u u u u u u u u u u u u u u u u u u U u u U u u u u u u u u u u U u u u Fairplain Gut FPG-1 16-Sep-97 SoU 1 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 1000 430 1000 430 430 430 1000 430 1000 1000 430 430 430 u U U U U u u U u u U u u u u u u u u u u U u u u u u u u u u u u u u U U u u Fairplain Gut FPG-2 16-Sep-97 SoU 1 420 420 420 420 420 420 420 420 420 420 420 420 420 420 420 420 420 420 420 420 420 420 420 420 420 420 1000 420 1000 420 420 420 1000 420 1000 1000 420 420 420 u u U u u u u u u u u u u u u u u u u u u U u u u u u u u u u u u u u U U u u h:\chemrisk\island\data\tables\svocs.xls 12/12/97 3 0 0 8 9 5 TABLE 4 VIRGIN ISLAND CHEMICAL SITE GUT AND STORM DRAIN SURFACE SOIL SAMPLING RESULTS SEMIVOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: [DAIE SAMPLED: MAIRIX DILUTION FACTOR: ANALYTE: 4-Chlorophenyl-phenyl ether Fluorene 4-Nitroaniline 4,6-Dinitro-2-Methylphenol N-Nitrosodiphenylamine 4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol Phenanthrene Anthracene Carbazole Di-n-Butylphthalate Fluoranthene Pyrene Butylbenzylphthalate 3,3'-Dichlorobenzidine Benzo(a)Anthracene Chrysene bis(2-Ethylhexyl)Phthalate Di-n-Octyl Phthalate Benzo(b)Fluoranthene Benzo(k)Fluoranthene Benzo(a)Pyrene Indeno(l,2,3-cd)Pyrene Dibenzo(a,h)Anthracene Benzo(g,h,l)Perylene CAS#: 7005-72-3 86-73-7 100-01-6 534-52-1 86-30-6 101-55-3 118-74-1 87-86-5 85-01-8 120-12-7 86-74-8 84-74-2 206-44-0 129-00-0 85-68-7 91-94-1 56-55-3 218-01-9 117-81-7 117-84-0 205-99-2 207-08-9 50-32-8 193-39-5 53-70-3 191-24-2 Bethlehem Gut BG-l 16-Sep-97 SoU 1 500 500 1200 1200 500 500 500 1200 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 u u u U U U U U U U u U u u U u U u u u u u u u u u Bethlehem Gut BG-2 16-Sep-97 SoU 1 350 350 850 850 350 350 350 850 350 350 350 350 350 350 350 350 350 350 350 350 350 350 350 350 350 350 U U U U U U U U U U U U U U U U U U U U U U u U u u Fairplain Gut FPG-1 16-Sep-97 SoU 1 430 U 430 U 1000 U 1000 U 430 U 430 U 430 U 1000 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U 430 U Fairplain Gut FPG-2 16-Sep-97 SoU 1 420 420 1000 1000 420 420 420 1000 420 420 420 420 420 420 420 420 420 420 420 420 420 420 420 420 420 420 U U U U U U U U U U U U U U U u U u u u u u u u u u Notes All results reported in ug/kg Analyzed by CLP method OLMO 1.9 modified for pyridine analysis U = Analyte was not detected above the referenced reporting limit. J = Indicates an estimated value B = Analyte was found in the blank as weU as the sample h'.\chemrisk\island\data\tables\svocs.xls 12/12/97 300896 TABLE 4 VIRGIN ISLAND CHEMICAL SITE GUT AND STORM DRAIN SURFACE SOIL SAMPLING RESULTS SEMIVOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Phenol Pyridine bis-(2-Chloroethyl) Ether 2-Chlorophenol 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene 2-Methylphenol 2,2'-ojtybis (1-Chloropropane) 4-Methylphenol N-Nitroso-Di-n-Propylamine Hexachloroethene Nitrobenzene Isophorone 2-Nitrophenol 2,4-Dimethylphenol bis (2-Chloroethoxy) Methane 2,4-Dichlorophenol 1,2,4-Trichlorobenzene Naphthalene 4-Chloroaniline Hexachlorobutadiene 4-Chloro-3-Methylphenol 2-MethylnaphthaIene Hexachlorocyclopentadiene 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2-ChloronaphthaIene 2-Nitroaniline Dimethyl Phthalate Acenaphthylene 2,6-Dinitrot61uene 3-Nitroaniline Acenaphthene 2,4-Dinitrophenol 4-Nitrophenol Dibenzofiiran 2,4-Dinitrotoluene Diethylphthalate CAS#: 108-95-2 110-86-1 111-44-4 95-57-8 541-73-1 106-46-7 95-50-1 95-48-7 108-60-1 106-44-5 621-64-7 67-72-1 98-95-3 78-59-1 88-75-5 105-67-9 111-91-1 120-83-2 120-82-1 91-20-3 106-47-8 87-68-3 59-50-7 91-57-6 77-47-4 88-06-2 95-95-4 91-58-7 88-74-4 131-11-3 208-96-8 606-20-2 99-09-2 83-32-9 51-28-5 100-02-7 132-64-9 121-14-2 84-66-2 River Gut RG-3 23-Sep-97 Sou 1 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 1100 430 1100 430 430 430 1100 430 1100 1100 430 430 430 U U U U U U U U U U U U U U U U U U U U U U u u u u u u u u u u U u u u u u u River Gut RG-2 23-Sep-97 SoU 1 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 1100 430 1100 430 430 430 1100 430 1100 1100 430 430 430 U U U U U U U U U U U U U U U U U U U U U u U u u u u U u u u u u u u u u u u River Gut RG-2D 23-Sep-97 SoU 1 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 1000 430 1000 430 430 430 1000 430 1000 1000 430 430 430 U U U U U U U U u u U U U u u U u U U u u U u u u u u u u u u U U U U u u u u River Gut RG-4 23-Sep-97 SoU 1 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 980 400 980 400 400 400 980 400 980 980 400 400 400 U U U U U u u u u u u u u • u u u u u u u u u u u u u u u u u u u u u u u u u u h:\chemrisk\island\data\tables\svocs.xls 12/12/97 3 0 0 8 9 7 TABLE 4 VIRGIN ISLAND CHEMICAL SITE GUT AND STORM DRAIN SURFACE SOIL SAMPLING RESULTS SEMIVOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPLED: M A I R K DILUTION FACTOR: ANALYTE: 4-Chlorophenyl-phenyl ether Fluorene 4-Nitroaniline 4,6-Dinitro-2-Methylphenol N-Nitrosodiphenylamine 4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol Phenanthrene Anthracene Carbazole pi-n-Butylphthalate Fluoranthene Pyrene Butylbenzylphthalate 3,3'-Dichlorobenzidine Benzo(a)Anthracene Chrysene bis(2-Ethymexyl)Phthalate Di-n-Octyl Phthalate Benzo(b)Fluoranthene Benzo(k)Fluoranthene Benzo(a)Pyrene Indeno(l,2,3-cd)Pyrene Dibenzo(a,h)Anthracene Benzo(g,h,I)Perylene CAS#: 7005-72-3 86-73-7 100-01-6 534-52-1 86-30-6 101-55-3 118-74-1 87-86-5 85-01-8 120-12-7 86-74-8 84-74-2 206-44-0 129-00-0 85-68-7 91-94-1 56-55-3 218-01-9 117-81-7 117-84-0 205-99-2 207-08-9 50-32-8 193-39-5 53-70-3 191-24-2 River Gut R:G-3 1 23-Sep-97 Sou 1 430 430 1100 1100 430 430 430 1100 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 U U u u u u u u u u u u u u u u u u u u u u u. u u u River Gut RG-2 23-Sep-97 SoU 1 430 430 1100 1100 430 430 430 1100 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 u U U u U U U U u u u u U u U U U U u U U U u u u u River Gut RG-2D 23-Sep-97 Sou 1 430 430 1000 1000 430 430 430 1000 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 u u u u u u u u u u u u u u u u u u u u u u u u u u River Gut KG-4 23-Sep SoU 1 400 400 980 980 400 400 400 980 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 [ •97 u U u U U U U U U U U U U U u U u U U U u u U u u u Notes AU results reported in ug/kg Analyzed by CLP method OLMO 1.9 modified for pyridine analysis U = Analyte was not detected above the referenced reporting limit. J = Indicates an estimated value B = Analyte was found in the blank as weU as the sample h:\chemrisk\island\data\tables\svocs.xls 12/12/97 300898 TABLE 4 VIRGIN ISLAND CHEMICAL SITE GUT AND STORM DRAIN SURFACE SOIL SAMPLING RESULTS SEMIVOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DAIE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Phenol Pyridine bis-(2-Chloroethyl) Ether 2-Chlorophenol 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene 2-Methylphenol 2,2'-oxybis (l-Chloropropane) 4-Methylphenol N-Nitroso-Di-n-Propylamine Hexachloroethene Nitrobenzene Isophorone 2-Nitrophenol 2,4-Dimethylphenol bis (2-Chloroethoxy) Methane 2,4-Dichlorophenol 1,2,4-Trichlorobenzene Naphthalene 4-ChIoroaniline Hexachlorobutadiene 4-Chloro-3-Methylphenol 2-Methylnaphthalene Hexachlorocyclopentadiene 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2-Chloronaphthalene 2-Nitroaniline Dimethyl Phthalate Acenaphthylene 2,6-Dinitrotoluene 3-Nitroaniline Acenaphthene 2,4-Dinitrophenol 4-Nitrophenol Dibenzofiiran 2,4-Dinitrotoluene Diethylphthalate CAS#: 108-95-2 110-86-1 111-44-4 95-57-8 541-73-1 106-46-7 95-50-1 95-48-7 108-60-1 106-44-5 621-64-7 67-72-1 98-95-3 78-59-1 88-75-5 105-67-9 1II-91-1 120-83-2 120-82-1 91-20-3 106-47-8 87-68-3 59-50-7 91-57-6 77-47-4 88-06-2 95-95-4 91-58-7 88-74-4 131-11-3 208-96-8 606-20-2 99-09-2 83-32-9 51-28-5 100-02-7 132-64-9 121-14-2 84-66-2 River Gut RG-4D 23-Sep-97 SoU 1 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 1100 430 1100 430 430 430 1100 430 1100 1100 430 430 430 U U U U U U U U U U U U U U U U U U U U u U U U U U u u u u u u u u u U u u u River Gut RG-f 23-Sep-97 SoU 1 390 390 390 390 390 390 390 390 390 390 390 390 390 390 390 390 390 390 390 390 390 390 390 390 390 390 940 390 940 390 390 390 940 390 940 940 390 390 390 U U U U U U U U U U U U U U U U U U U U U U U U U u U u u U U u u u u U U U u River Gut RG-< i 23-Sep-97 SoU 1 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 920 380 920 380 380 380 920 380 920 920 380 380 380 U U U U U U U U U U U U U U u u u u u u u U u u u u u u u u u u u u u u u u u River Gut RG-' r 23-Sep-97 | SoU 1 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 1100 430 1100 430 430 430 1100 430 1100 1100 430 430 430 u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u h:\chemrisk\island\data\tables\svocs.xls 12/12/97 3 0 0 8 9 9 TABLE 4 VIRGIN ISLAND CHEMICAL SITE GUT AND STORM DRAIN SURFACE SOIL SAMPLING RESULTS SEMIVOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: 4-ChloTophenyl-phenyl ether Fluorene 4-Nitroaniline 4,6-Dinitro-2-Methylphenol N-Nitrosodiphenylamine 4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol Phenanthrene Anthracene Carbazole Di-n-Butylphthalate Fluoranthene Pyrene Butylbenzylphthalate 3,3'-Dichlorobenzidine Benzo(a)Anthracene Chrysene bis(2-Ethylhexyl)Phthalate Di-n-Octyl Phthalate Ben7X>(b)Fluoranthene Benzo(k)Fluoranthene Benzo(a)Pyrene Indeno(l,2,3-cd)Pyrene Dibenzo(a,h)Anthracene Benzo(g,h,I)Petylene CAS#: 7005-72-3 86-73-7 100-01-6 534-52-1 86-30-6 101-55-3 118-74-1 87-86-5 85-01-8 120-12-7 86-74-8 84-74-2 206-44-0 129-00-0 85-68-7 91-94-1 56-55-3 218-01-9 117-81-7 117-84-0 205-99-2 207-08-9 50-32-8 193-39-5 53-70-3 191-24-2 River Gut RG-4D 23-Sep-97 SoU 1 430 430 1100 1100 430 430 430 1100 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 u u u , u u u u u u u u u u u u u u u u u U u u u u u River Gut RG-3 23-Sep-97 Sou 1 390 390 940 940 390 390 390 940 390 390 390 390 390 390 390 390 390 390 390 390 390 390 390 390 390 390 u u U u u u u u u u u u u u u u u u u u u u u u u u River Gut RG-^ 1 23-Sep-97 SoU 1 380 380 920 920 380 380 380 920 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 U u u u u u u u u u u u u u u u u u u u U u u u u u River Gut RG--1 23-Sep-97 SoU 1 430 430 1100 1100 430 430 430 1100 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 U u u u u u u u u u u u u u u u u u u u u u u u u u Notes All results reported in ug/kg Analyzed by CLP method OLMO 1.9 modified for pyridine analysis U = Analyte was not detected above the referenced reporting limit J = Indicates an estimated value B = Analyte was found in the blank as weU as the sample h:\chemrisk\island\data\tabIes\svocs.xls 12/12/97 300900 TABLE 4 VIRGIN ISLAND CHEMICAL SITE GUT AND STORM DRAIN SURFACE SOIL SAMPLING RESULTS SEMIVOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Phenol Pyridine bis-(2-Chloroethyl) Ether 2-Chlorophenol 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene 2-Methylphenol 2,2'-ojtybis (1-Chloropropane) 4-Methylphenol N-Nitroso-Di-n-Propylamine Hexachloroethene Nitrobenzene Isophorone 2-Nitrophenol 2,4-Dimethylphenol bis (2-Chloroethoxy) Methane 2,4-Dichlorophenol 1,2,4-Trichlor6benzene Naphthalene 4-Chloroaniline Hexachlorobutadiene 4-Chloro-3-Methylphenol 2-Methyln3phthalene Hexachlorocyclopentadiene 2,4,6-TrichIon)phenol 2,4,5-Trichlorophenol 2-Chloronaphthalene 2-NitroanUine Dimethyl Phthalate Acenaphthylene 2,6-Dinitrotoluene 3-Nitroaniline Acen^hthene 2,4-Dinitrophenol 4-Nitrophenol Dibenzofiiran 2,4-Dinitrotoluene Diethylphthalate CAS#: 108-95-2 110-86-1 111-44-4 95-57-8 541-73-1 106-46-7 95-50-1 95-48-7 108-60-1 106-44-5 621-64-7 67-72-1 98-95-3 78-59-1 88-75-5 105-67-9 111-91-1 120-83-2 120-82-1 91-20-3 106-47-8 87-68-3 59-50-7 91-57-6 77-47-4 88-06-2 95-95-4 91-58-7 88-74-4 131-11-3 208-96-8 606-20-2 99-09-2 83-32-9 51-28-5 100-02-7 132-64-9 121-14-2 84-66-2 River Gut RG-S t 23-Sep-97 j Soil 1 390 390 390 390 390 390 390 390 390 390 390 390 390 390 390 390 390 390 390 390 390 390 390 390 390 390 950 390 950 390 390 390 950 390 950 950 390 390 390 U u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u U u u u River Gut RG-S » 23-Sep-97 SoU 1 460 460 460 460 460 460 460 460 460 460 460 460 460 460 460 460 460 460 460 460 460 460 460 460 460 460 1100 460 1100 460 460 460 1100 460 1100 1100 460 460 460 U u U u U U U U U U U U U U U U U U U u u U u U u u U u u u u u u u U u u U U River Gut RG-10 23-Sep-97 SoU 1 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 1000 430 1000 430 430 430 1000 430 1000 1000 430 430 430 U U U U U U U U U U U U U U U U U U U u u U u u u U u U U u u u u u U u u u U River Gut RG-II 23-Sep SoU 1 410 410 410 410 410 410 410 410 410 410 410 410 410 410 410 410 410 410 410 410 410 410 410 410 410 410 990 410 990 410 410 410 990 410 990 990 410 410 410 -97 U U U U U U U U U U U U U U U U U U U U u u u u u U u u U u U U u U U u u u u h:\chemrisk\island\data\tables\svocs.xls 12/12/97 300901 TABLE 4 VIRGIN ISLAND CHEMICAL SITE GUT AND STORM DRAIN SURFACE SOIL SAMPLING RESULTS SEMIVOLATILE ORGANIC COMPOUNDS LOCATION: SAMPI F I D NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: 4-Chlorophenyl-phenyl ether Fluorene 4-Nitroaniline 4,6-Dinitro-2-Methylphenol N-Nitrosodiphenylamine 4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol Phenanthrene Anthracene Carbazole Di-n-Butylphthalate Fluoranthene Pyrene Butylbenzylphthalate 3,3 '-Dichlorobenzidine Benzo(a)Anthracene Chrysene bis(2-Ethylhexyl)Phthalate Di-n-Octyl Phthalate Benzo(b)Fluoranthene Benzo(k)Fluoranthene Benzo(a)Pyrene lndeno( 1,2,3 -cd)Pyrene Dibenzo(a,h)Anthracene Benzo(g,h,I)Perylene CAS#: 7005-72-3 86-73-7 100-01-6 534-52-1 86-30-6 101-55-3 118-74-1 87-86-5 85-01-8 120-12-7 86-74-8 84-74-2 206-44-0 129-00-0 85-68-7 91-94-1 56-55-3 218-01-9 117-81-7 117-84-0 205-99-2 207-08-9 50-32-8 193-39-5 53-70-3 191-24-2 River Gut RG-i I 23-Sep-97 Sou 1 390 390 950 950 390 390 390 950 390 390 390 390 390 390 390 390 390 390 390 390 390 390 390 390 390 390 U U U U U U U U U U U U U U U U U u u u u u u u u u River Gut RG-S » 23-Sep-97 SoU 1 460 460 1100 1100 460 460 460 1100 460 460 460 460 91 86 460 460 460 460 460 460 460 460 460 460 460 460 U U U u u u u u u U u u J J u u u u u u u u u u u u River Gut RG-10 23-Sep-97 SoU 1 430 430 1000 1000 430 430 430 1000 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 u u U u u u u u U U u u U u u u u u u u u u u u U u River Gut RG-11 23-Sep-97 SoU 1 410 410 990 990 410 410 410 990 410 410 410 410 410 410 410 410 410 410 410 410 410 410 410 410 410 410 u U u u U U U U U U U U u U U U u u u u u u u u u u Notes AU results reported in ug/kg Analyzed by CLP method OLMO 1.9 modified for pyridine analysis U = Analyte was not detected above the referenced reporting limit. J = Indicates an estimated value B = Analyte was found in the blank as weU as the sample h:\chemrisk\isIand\data\tables\svocs.xls 12/12/97 300902 TABLE 4 VIRGIN ISLAND CHEMICAL SITE GUT AND STORM DRAIN SURFACE SOIL SAMPLING RESULTS SEMIVOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FAC iOR: ANALYTE: Phenol Pyridine bis-(2-Chloroethyl) Ether 2-Chlorophenol l,3-Dichlor6benzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene 2-Methylphenol 2,2'-oxybis (1-Chloropropane) 4-Methylphenol N-Nitroso-Di-n-Propylamine Hexachloroethene Nitrobenzene Isophorone 2-Nitrophenol 2,4-Dimethylphenol bis (2-Chloroethoxy) Methane 2,4-Dichlorophenol l,2,4-Trichlor6benzene Naphthalene 4-Chloroaniline Hexachlorobutadiene 4-Chloro-3-Methylphenol 2-Methylnaphthalene Hexachlorocyclopentadiene 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2-Chloronaphthalene 2-Nitroaniline Dimethyl Phthalate Acenaphthylene 2,6-Dinitrotoluene 3-Nitroaniline Acenaphthene 2,4-Dinitrophenol 4-Nitrophenol Dibenzofiiran 2,4-Dinitrotoluene Diethylphthalate CAS#: 108-95-2 110-86-1 111-44-4 95-57-8 541-73-1 106-46-7 95-50-1 95-48-7 108-60-1 106-44-5 621-64-7 67-72-1 98-95-3 78-59-1 88-75-5 105-67-9 111-91-1 120-83-2 120-82-1 91-20-3 106-47-8 87-68-3 59-50-7 91-57-6 77-47-4 88-06-2 95-95-4 91-58-7 88-74-t 131-11-3 208-96-8 606-20-2 99-09-2 83-32-9 51-28-5 100-02-7 132-64-9 121-14-2 84-66-2 River Gut RG-12 16-Sep-97 SoU 1 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 980 400 980 400 400 400 980 400 980 980 400 400 400 u u U u u, u U U U U U U U U U U U U U u u u U u u u U u u u U u u u U u u u U River Gut RG-13 16-Sep-97 Sou 1 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 930 380 930 380 380 380 930 380 930 930 380 380 380 U U U U U U U U U U U U U U U U U U U u u u u u u u u u u u u u u u U u u u u River Gut RG-14 16-Sep-97 SoU 1 690 690 690 ' 690 690 690 690 690 690 690 690 690 690 690 690 690 690 690 690 690 690 690 690 690 690 690 1700 690 1700 690 690 690 1700 690 1700 1700 690 690 690 U U U U U U U U U U U U U U U u U U u U u u u U u U u u u u U u u U u U u u U River Gut RG-15 16-Sep-97 SoU 1 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 920 380 920 380 380 380 920 380 920 920 380 380 380 u U U U u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u h:\chemrisk\island\data\tables\svocs.xls 12/12/97 3 0 0 9 0 3 TABLE 4 VIRGIN ISLAND CHEMICAL SITE GUT AND STORM DRAIN SURFACE SOIL SAMPLING RESULTS SEMIVOLATILE ORGANIC COMPOUNDS LOCATION: ^L^^^F ^ ^ A ^ ^ . ^ ^i^ * ^ 9 SAMPLE ID NO: DATE SAMPT-ED: MATRIX DILUTION FACi OR: ANALYTE: 4-Chlorophenyl-phenyl ether Fluorene 4-Nitroaniline 4,6-Dinitro-2-Methylphenol N-Nitrosodiphenylamine 4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol Phenanthrene Anthracene (Taibazole Di-n-Butylphthalate Fluoranthene Pyrene Butylbenzylphthalate 3,3'-Dichlorobenzidine Benzo(a)Anthracene Chrysene bis(2-EthyUiejtyl)Phthalate Di-n-Octyl Phthalate Benzo(b)Fluoranthene Benzo(k)Fluoranthene Benzo(a)Pyrene Indeno(l,2,3-cd)Pyrene Dibenzo(a,h)Anthracene Benzo(g,h,I)Perylene CAS#: 7005-72-3 86-73-7 100-01-6 534-52-1 86-30-6 101-55-3 118-74-1 87-86-5 85-01-8 120-12-7 86-74-8 84-74-2 206-44-0 129-00-0 85-68-7 91-94-1 56-55-3 218-01-9 117-81-7 117-84-0 205-99-2 207-08-9 50-32-8 193-39-5 53-70-3 191-24-2 River Gut RG-12 16-Sep-97 SoU 1 400 400 980 980 400 400 400 980 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 U u U u u u u u U U U U U U U U u U U U u u U U u U River Gut RG-13 16-Sep-97 SoU 1 380 380 930 930 380 380 380 930 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 U U U U U U U U U U U U U U U U U U U U U U U U u U River Gut RG-14 16-Sep-97 SoU 1 690 690 1700 1700 690 690 690 1700 690 690 690 690 690 690 690 690 690 690 690 690 690 690 690 690 690 690 U U U U U U U U U U U U U U U U u U U u u u u U u U River Gut RG-15 16-Sep-97 SoU 1 380 380 920 920 380 380 380 920 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 U U u U u u U U u u u u u u u u u u u u u u u u u u Notes AU results reported in ug/kg Analyzed by CLP method OLMO 1.9 modified for pyridine analysis U = Analyte was not detected above the referenced reporting limit. J = Indicates an estimated value B = Analyte was found in the blank as weU as the sample h:\chemrisk\island\data\tables\svocs.xls 12/12/97 300904 TABLE 4 VIRGIN ISLAND CHEMICAL SITE GUT AND STORM DRAIN SURFACE SOIL SAMPLING RESULTS SEMIVOLATILE ORGANIC COMPOUNDS ^r ^^ ^v a M*^r^^^T LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Phenol Pyridine bis-(2-Chloroethyl) Ether 2-Chlorophenol 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene 2-Methylphenol 2,2'-oxybis (1-Chloropropane) 4-Methylphenol N-Nitroso-Di-n-Propylamine Hexachloroethene Nitrobenzene Isophorone 2-Nitrophenol 2,4-Dimethylphenol bis (2-Chloroethoxy) Methane 2,4-Dichlorophenol 1,2,4-Trichlorobenzene Naphthalene 4-Chloroamline Hexachlorobutadiene 4-Chloro-3-Methylphenol 2-Methylnaphthalene Hexachlorocyclopentadiene 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2-Chloronaphthalene 2-Nitroaniline Dimethyl Phthalate Acenaphthylene 2,6-Dinitrotoluene 3-Nitroaniline Acenaphthene 2,4-Dinitrophenol 4-Nitrophenol Dibenzofiiran 2,4-Dinitrotoluene Diethylphthalate CAS#: 108-95-2 110-86-1 111-44-4 95-57-8 541-73-1 106-46-7 95-50-1 95-48-7 108-60-1 106-44-5 621-64-7 67-72-1 98-95-3 78-59-1 88-75-5 105-67-9 111-91-1 120-83-2 120-82-1 91-20-3 106-47-8 87-68-3 59-50-7 91-57-6 77-47-4 88-06-2 95-95-4 91-58-7 88-74-4 131-11-3 208-96-8 606-20-2 99-09-2 83-32-9 51-28-5 100-02-7 132-64-9 121-14-2 84-66-2 River Gut RG-16 16-Sep-97 SoU 1 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 1100 430 1100 430 430 430 1100 430 1100 1100 430 430 430 u u U u U U U u u U U U U U U U U U U u u u U U U U U U u u u u U u U U u u u Central Storm Drain SDCSD-2 07-Oct-97 SoU 1 510 510 510 510 510 510 510 510 510 510 510 510 510 510 510 510 510 510 510 510 510 510 510 510 510 510 1200 510 1200 570 510 510 1200 510 1200 1200 510 510 510 U U U U U U U U U U U U U U U U U U U U U u U u U u U u u u u U u U u u U u u Central Storm Drain SDSCD-3 07-Oct-97 Sou 1 460 460 460 460 460 460 460 460 460 460 460 460 460 460 460 460 460 460 460 460 460 460 460 460 460 460 1100 460 1100 160 460 460 1100 460 1100 1100 460 460 460 U U U U U U U U U U U U U U U u u U u u u u u U U u u u u u u u u u U U u u u Southern Storm Drain SDSSD-1 07-Oct-97 Sou 1 370 370 370 370 370 370 370 370 370 370 370 370 370 320 370 370 370 370 370 370 370 370 370 370 370 370 910 370 910 370 370 370 910 370 910 910 370 370 370 U U U U U u u U U U U u u J u u u u u u U u u u u u u u u u u u u u u u u u u h:\cheinrisk\island\data\tables\svocs.xls 12/12/97 300905 TABLE 4 VIRGIN ISLAND CHEMICAL SITE GUT AND STORM DRAIN SURFACE SOIL SAMPLING RESULTS SEMIVOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: 4-Chlorophenyl-phenyl ether Fluorene 4-Nitroaniline 4,6-Dinitro-2-Methylphenol N-Nitrosodiphenylamine 4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol Phenanthrene Anthracene Carbazole Di-n-Butylphthalate Fluoranthene Pyrene Butylbenzylphthalate 3,3'-Dichlor6benzidine Benzo(a)Anthracene Chrysene bis(2-EthyIhexyl)Phthalate Di-n-Octyl Phthalate Benzo(b)Fluoranthene Benzo(k)Fluoranthene Benzo(a)Pyrene Indeno(l,2,3-cd)Pyrene Dibenzo(a,h)Anthracene Benzo(g,h,I)Perylene CAS#: 7005-72-3 86-73-7 100-01-6 534-52-1 86-30-6 101-55-3 118-74-1 87-86-5 85-^1-8 120-12-7 86-74-8 84-74-2 206-44-0 129-00-0 85-68-7 91-94-1 56-55-3 218-01-9 117-81-7 117-84-0 205-99-2 207-08-9 50-32-8 193-39-5 53-70-3 191-24-2 River Gut RG-16 16-Sep-97 SoU 1 430 430 1100 1100 430 430 430 1100 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 430 U U U U U U U u U U U U U U U U U u u u U u u u u U Central Storm Drain SDCSD-2 07-Oct-97 Sou 1 510 510 1200 1200 510 510 510 1200 510 510 510 510 510 510 2100 510 510 510 7800 510 510 510 510 510 510 510 U U U U U U U U U U U U U U U U U U DJ U U U U U U U Central Storm Drain SDSCD-3 07-Oct-97 SoU 1 460 460 1100 1100 460 460 460 1100 460 460 460 460 460 460 790 460 460 460 1800 460 460 460 460 460 460 460 U U u U u u u u U U u u u U u U U u U u u U U u u U Southern Storm Drain SDSSD-1 07-Oct-97 SoU 1 370 U 370 U 910 U 910 U 370 U 370 U 370 U 910 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U Notes All results reported in ug/kg Analyzed by CLP method OLMO 1.9 modified for pyridine analysis U = Analyte was not detected above the referenced reporting limit. J = Indicates an estimated value B = Analyte was foimd in the blank as weU as the sample h:\chemrisk\isIand\data\tables\svocs.xls 12/12/97 300906 TABLE 4 VIRGIN ISLAND CHEMICAL SITE GUT AND STORM DRAIN SURFACE SOIL SAMPLING RESULTS SEMIVOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUllON FACTOR: ANALYTE: Phenol Pyridine bis-(2-Chloroethyl) Ether 2-Chlorophenol 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene 2-Methylphenol 2,2'-oxybis (1-Chloropropane) 4-Methylphenol N-Nitroso-Di-n-Propylamine Hexachloroethene Nitrobenzene Isophorone 2-Nitrophenol 2,4-Dimethylphenol bis (2-Chloroethoxy) Methane 2,4-Dichlorophenol 1,2,4-Trichlorobenzene Naphthalene 4-(^hloroaniline Hexachlorobutadiene 4-Chloro-3-Methylphenol 2-Methyln^hthalene Hexachlorocyclopentadiene 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2-Chloronaphthalene 2-Nitroaniline Dimethyl Phthalate Acenaphthylene 2,6-Dinitrotoluene 3-Nitroaniline Acen^hthene 2,4-Dinitrophenol 4-Nitrophenol Dibenzofiiran 2,4-Dinitrotoluene Diethylphthalate CAS#: 108-95-2 110-86-1 111-44-4 95-57-8 541-73-1 106-46-7 95-50-1 95-48-7 108-60-1 106-44-5 621-64-7 67-72-1 98-95-3 78-59-1 88-75-5 105-67-9 111-91-1 120-83-2 120-82-1 91-20-3 106-47-8 87-68-3 59-50-7 91-57-6 77-47-4 88-06-2 95-95-4 91-58-7 88-74-4 131-11-3 208-96-8 606-20-2 99-09-2 83-32-9 51-28-5 100-02-7 132-64-9 121-14-2 84-66-2 Southern Storm Drain SDSSD-2 07-Oct-97 Sou 1 380 380 380 380 380 380 380 380 380 380 380 380 380 2500 380 380 380 380 380 380 380 380 380 380 380 380 930 380 930 380 380 380 930 380 930 930 380 380 380 U U U U u u u u u u u u u u u u u u u u U u u u u u u u u u u u U u u U U U Field Blank FB100797 07.Oct-97 Water 1 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 25 10 25 10 10 10 25 10 25 25 10 10 10 10 u U U u u U u u u u u U u u u u u u u u u u u u u u u u u u u u u u u u u U U h:\cheinrisk\isIand\data\tables\svocs.xls 12/12/9^ 300907 TABLE 4 VIRGIN ISLAND CHEMICAL SITE GUT AND STORM DRAIN SURFACE SOIL SAMPLING RESULTS SEMIVOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: 4-Chlorophenyl-phenyl ether Fluorene 4-Nitroaniline 4,6-Dinitro-2-Methylphenol N-Nitrosodiphenylamine 4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol Phenanthrene Anthracene Carbazole Di-n-Butylphthalate Fluoranthene Pyrene Butylbenzylphthalate 3,3'-Dichlorobenzidine Benzo(a)Anthracene Chrysene bis(2-Ethylhexyl)Phthalate Di-n-Octyl Phthalate Benzo(b)Fluoranthene Benzo(k)Fluoranthene Benzo(a)Pyrene Indeno(l,2,3-cd)Pyrene Dibenzo(a,h)Anthracene Benzo(g,h,I)Perylene CAS#: 7005-72-3 86-73-7 100-01-6 534-52-1 86-30-6 101-55-3 118-74-1 87-86-5 85-01-8 120-12-7 86-74-8 84-74-2 206-44-0 129-00-0 85-68-7 91-94-1 56-55-3 218-01-9 117-81-7 117-84-0 205-99-2 207-08-9 50-32-8 193-39-5 53-70-3 191-24-2 Southern Storm Drain SDSSD-2 07-Oct-97 Sou 1 380 380 930 930 380 380 380 930 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 380 u u u u u u u u U U U u U U U u U u u u U U U u u u FieldBlank FB100797 07-Oct-97 Water 1 10 25 25 10 10 10 25 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 u u u u u u u u u u u u u u u u u u u u u u u u u Notes AU results reported in ug/kg Analyzed by CLP method OLMO 1.9 modified for pyridine analysis U = Analyte was not detected above the referenced reporting limit. J = Indicates an estimated value B = Analyte was found in the blank as weU as the sample h:\chemrisk\island\data\tables\svocs.xls 12/12/97 300908 TABLES VIRGIN ISLAND CHEMICAL SITE GUT AND STORM DRAIN SURFACE SOIL SAMPLING RESULTS METALS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium SUver Sodium Thallium Vanadium Zinc Cyanide CAS#: 7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-tl-7 7440-t3-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-0 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6 57-12-5 Bethlehem Gut BG-l 16-SCP-97 SoU 15400 0.61 U 0.39 U 101 0.03 U 0.16 B 39800 19.7 11.4 BJ 49.3 J 20400 12.9 J 5380 534 J 0.14 U 11.7 B 3310 J 0.76 U 0.18 U 660 B 0.67 U 68.2 58.7 J 1.5 U Bethlehem Gut BG-2 16-Sep-97 Soil 3990 0.43 U 0.43 BJ 63 0.02 U 0.02 U 19800 4.6 5.4 BJ 11.2 J 5300 2.4 J 1150 339 J 0.1 U 3.2 B 582 B 0.53 U 0.13 U 423 B 0.47 U 29.9 13.1 J 1.1 U Fairplain Gut FPG-1 16-Sep-97 Sou 10200 0.52 U 1.4 BJ 67.4 0.03 U 0.09 B 36600 13.9 8.2 BJ 33.1 J 14300 8.8 J 3680 267 J 0.13 U 7.7 B 2150 J 1.1 B 0.16 U 570 B 0.57 U 54.6 39.4 J 1.3 U Fairplain Gut FPG-2 16-Sep-97 Sou 9750 0.51 U 2.8 J 70 0.03 U 0.2 B 25300 13.9 8.6 BJ 33.2 J 14800 5.7 J 3670 332 J 0.12 U 6.9 B 1940 J 0.63 U 0.15 U 887 B 0.56 U 56.5 34.2 J 1.2 U River Gut RG-2 23-Sep-97 SoU 15500 0.53 U 1.6 BJ 70.6 0.03 U 0.19 BJ 24500 16.1 14.8 J 40.5 J 26800 5.9 J 7650 594 J 0.13 U 9.4 B 2230 J 0.68 B 0.16 U 543 B 0.58 U 69.2 140 J 1.3 U Notes All results reported in mg/kg Analyzed by CLP method ILMO 3.0 U = Analyte was not deteced above the referenced reporting limit J = Indicates an estimated value B = Result is between the instrument detection limit (IDL) and the contract required detection limit (CRDL) R = Data is tmusable h:\chemrisk\island\data\tables\metals.xls Page 1 of6 300909 12/12/97 TABLE 5 VIRGIN ISLAND CHEMICAL SITE GUT AND STORM DRAIN SURFACE SOIL SAMPLING RESULTS METALS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Aluminum Antimony Arsenic Barium BeryUium Cadmium (Dalcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Pota.s,sium Selenium Silver Sodium Thallium Vanadium Zinc Cyanide CAS#: 7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-O 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6 57-12-5 River Gut RG-2D 23-Sep-97 SoU 17700 0.52 U 0.34 U 89 0.03 U 0.3 B 28700 19.4 16.8 J 54.4 J 30900 8.2 J 9070 675 J 0.13 U 13.8 J 3300 J 0.65 U 0.16 U 697 B 0.57 U 81 263 J 1.3 U River Gut RG-3 23-Sep-97 SoU 14900 0.53 U 0.86 BJ 53.8 0.03 U 0.31 B 39300 14.8 13.8 J 38.8 J 27300 4.1 J 8600 792 J 0.13 U 10.3 B 1500 J 0.66 U 0.16 U 525 B 0.58 U 59.6 54.4 J 1.3 U River Gut RG-4 23-Sep-97 Sou 14400 0.49 U 1.2 BJ 58.4 0.02 U 0.21 B 51000 12 12.8 J 33 J 22700 14.1 J 6920 726 J 0.33 9.8 J 1310 J 0.61 U 0.15 U 639 B 0.54 U 49.2 50.8 J 1.2 U River Gut RG-4D 23-Sep-97 SoU 9210 0.53 U 0.34 U 36.3 B 0.03 U 0.11 B 30700 8 8 BJ 19.6 J 14500 3.1 J 4700 445 J 0.19 J 6.1 B 754 B 1 B 0.16 U 509 B 0.58 U 32.7 42.6 J 1.3 U River Gut RG-5 23-Sep-97 SoU 11200 0.47 U 0.91 BJ 43.5 B 0.02 U 0.15 B 81100 14.6 10.3 BJ 32.9 J 22300 26.1 J 7630 598 J 0.13 J 9.6 J 1290 J 0.98 B 0.14 U 580 B 0.52 U 48.1 67.8 J 1.2 U Notes AU results reported in mg/kg Analyzed by CLP method ILMO 3.0 U = Analyte was not deteced above the referenced reporting limit J = Indicates an estimated value B = Result is between the instrument detection limit (IDL) and the contract required detection limit (CRDL) R = Data is unusable h:\cheinrisk\island\data\tables\metals.xls Page 2 of6 300910 12/12/97 TABLES VIRGIN ISLAND CHEMICAL SITE GUT AND STORM DRAIN SURFACE SOIL SAMPLING RESULTS METALS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Aluminum Antimony Arsenic Barium BeiyUium Cadmium Calcium Chromium Cobalt Copper Iron I^ad Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc Cyanide CAS#: 7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-0 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6 57-12-5 River Gut RG-6 23-Sep-97 SoU 10500 0.46 U 0.36 BJ 43.5 B 0.02 U 0.13 B 57000 14.4 9.5 BJ 29.6 J 19800 11.4 J 6700 513 J 0.22 J 10.6 J 1250 J 0.57 U 0.14 U 474 B 0.51 U 51.4 45.9 J I.I U River Gut RG-7 23-Sep-97 SoU 11500 0.53 U 0.92 BJ 68 0.03 U 0.19 B 42900 13.6 11 BJ 34.1 J 21100 5.9 J 6040 531 J 0.11 U 8.2 B 1750 J 0.66 U 0.16 U 479 B 0.58 U 63.8 43.4 J 1.3 U River Gut RG-8 23-Sep-97 SoU 10200 0.48 U 0.31 U 53 0.02 U 0.03 B 48700 10.8 8.1 BJ 25.1 J 15800 4.5 J 5320 408 J 0.19 J 6.5 B 1910 J 0.6 U 0.14 U 522 B 0.52 U 44.8 34.9 J 1.2 U River Gut RG-9 23-Sep-97 Sou 15400 0.56 U 1.1 BJ 98.5 0.03 U 0.32 B 56200 20.2 14.4 J 47.2 J 27500 6.3 J 8270 708 J 0.34 J 12.4 J 3540 J 0.69 U 0.17 U 668 B 0.61 U 85.9 155 J 1.4 U River Gut RG-10 23-Sep-97 Sou 9500 0.52 U 1 BJ 52.6 0.03 U O.ll B 56700 13.9 7.4 BJ 23.7 J 16000 8.2 J 4610 431 J 0.25 J 7.6 B 1650 J 1.1 B 0.16 U 599 B 0.57 U 46.3 44 J 1.3 U Notes All resiUts reported in mg/kg Analyzed by CLP method ILMO 3.0 U = Analyte was not deteced above the referenced reporting limit J = Indicates an estimated value B = Result is between the instrument detection limit (IDL) and the contract required detection limit (CRDL) R = Data is unusable h:\chemrisk\island\data\tables\metals.xls Page 3 of6 300911 12/12/97 TABLE 5 VIRGIN ISLAND CHEMICAL SITE GUT AND STORM DRAIN SURFACE SOIL SAMPLING RESULTS METALS LOCATION: SAMPLE ID NO: DAIE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Aluminum Antimony Arsenic Barium BeiylUum Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium ThaUium Vanadium Zinc Cyanide CAS#: 7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-0 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6 57-12-5 River Gut RG-11 23-Sep-97 SoU 7680 0.49 U 0.38 BJ 50.6 0.02 U 0.05 B 32000 10.1 6.7 BJ 22 J 12700 3.4 J 3590 297 J 0.39 J 5.6 B 1410 J 0.62 U 0.15 U 329 B 0.54 U 44.5 26.4 J 1.2 U River Gut RG-12 16-Sep-97 SoU 6210 0.49 U 0.48 BJ 47 B 0.02 U 0.12 B 23900 9.9 6.1 BJ 18.1 J 12500 4.7 J 2560 313 J 0.11 U 4.2 B 1010 B 0.61 U 0.15 U 293 B 0.54 U 53 39.1 J 1.2 U River Gut RG-13 16-Sep-97 SoU 14400 0.47 U 1.1 BJ 112 0.02 U 0.86 B 57400 21.6 11.9 J 43.8 J 23100 22.2 J 6600 560 J 0.11 U 11.5 J 3020 J 1.6 0.14 U 561 B 0.51 U 70.2 174 J 1.2 U River Gut RG-14 16.Sep-97 SoU 7220 J 0.83 U 1.5 BJ 36.5 BJ 0.04 U 0.04 U 97500 J 39 J 4.9 BJ 10.2 BJ 9160 J 3.4 J 3190 J 222 J 0.18 U 17 J 706 BJ 1 U 0.25 U 215 BJ 0.92 U 28.6 J 21.8 J 2 U River Gut RG-15 16-Sep-97 SoU 3500 0.46 U 0.3 U 23.1 B 0.02 U 0.02 U 800000 4.7 2.2 BJ 11.8 J 4330 1.6 J 1600 173 J 0.11 J 1.3 B 665 B 0.57 U 0.14 U 255 B 0.51 U 15 136 J 1.1 U Notes All results reported in mg/kg Analyzed by CLP method ILMO 3.0 U = Analyte was not deteced above the referenced reporting limit J = Indicates an estimated value B = Result is between the instrument detection limit (IDL) and the contract required detection limit (CRDL) R = Data is unusable h:\chemrisk\island\data\tables\metals.xls Page 4 of6 300912 12/12/97 TABLE 5 VIRGIN ISLAND CHEMICAL SITE GUT AND STORM DRAIN SURFACE SOIL SAMPLING RESULTS METALS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Merciuy Nickel Potassium Selenium SUver Sodium ThaUium Vanadium Zinc Cyanide CAS#: 7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-0 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6 57-12-5 River Gut RG-16 16-Sep-97 SoU 5200 0.53 U 0.34 U 21.6 B 0.03 U 0.08 B 46400 5.9 3.1 BJ 19.9 J 5780 2.2 J 1660 196 J 0.12 U 4.2 B 803 B 0.66 U 0.16 U 492 B 0.58 U 17 25.9 J 1.3 U Central Storm Drain SDCSD-2 10/7/97 Sou 8390 0.62 UJ 8.8 70.3 0.03 UJ 3.9 76900 J 32 9.4 BJ 280 J 58800 35.2 4090 595 J 0.15U 23.5 838 B 0.94 BJ 1.5 B 675 B 0.68 U 34.3 336 Central Storm Drain SCSD-3 10/7/97 SoU 8890 0.56 UJ 3.7 44 B 0.03 UJ 3.9 56300 J 22.7 7.5 BJ 121 J 19700 25.4 4840 311 J 0.14 U 14.5 1060 B 0.69 UJ 1.2 B 659 B 0.61 U 39.5 346 Southem Storm Drain SDSSD-1 10/7/97 Sou 14600 0.45 UJ 0.81 B 68.9 0.02 UJ 0.52 B 56400 J 13.9 10 BJ 30.7 J 19100 3.9 5870 503 J 0.11 UJ 9 B 3650 0.57 UJ 0.98 B 373 B 0.5 U 52.1 40.5 R Southem Storm Drain SDSSD-2 10/7/97 SoU 13500 0.47 UJ 0.87 B 59.2 0.02 UJ 0.72 B 53600 J 14.6 9.4 BJ 35.2 J 18800 7.3 6170 494 J 0.12 U 8.3 B 3400 0.58 UJ 0.92 B 453 B 0.51 U 50.1 74.4 Notes All results reported in mg/kg Analyzed by CLP method ILMO 3.0 U = Analyte was not deteced above the referenced reporting limit J = Indicates an estimated value B = Result is between the instrument detection limit (IDL) and the contract required detection limit (CRDL) R = Data is unusable h:\chemrisk\island\data\tables\metals.xls 3 0 0 9 1 3 12/12/97 TABLES VIRGIN ISLAND CHEMICAL SITE GUT AND STORM DRAIN SURFACE SOIL SAMPLING RESULTS METALS LOCATION: SAMPLE ID NO: DAIE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Aluminum Antimony Arsenic Barium BeiyUium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium SUver Sodium Thallium Vanadium Zinc Cyanide CAS#: 7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-0 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6 57-12-5 FieldBlank FB100797 10/7/97 Water 30.3 2 1.3 1.6 0.1 0.1 4240 0.28 0.2 1.5 15.1 1.1 84.5 2.5 0.2 0.7 35.2 2.5 0.6 7.8 2.2 0.2 63.7 B U U B U U B B UJ U U u B B U u B UJ u u u u Notes AU results reported in mg/kg Analyzed by CLP method ILMO 3.0 U = Analyte was not deteced above the referenced reporting limit J = Indicates an estimated value B = Result is between the instrument detection limit (IDL) and the contract required detection limit (CRDL) R = Data is unusable h:\chemrisk\island\data\tables\metals.xls 12/12/97 300914 TABLE 6 VIRGIN ISLAND CHEMICAL SITE GUT AND STORM DRAIN SURFACE SOIL SAMPLING RESULTS PHYSICOCHEMICAL PARAMETERS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: AUcalinity (Total) Oxidation/Reduction Potential pH Specific Conductance Total Organic Carbon Total Solids Units: mg/kg none none umbos mg/kg mg/l Bethlehem Gut BG-l 16-Sep-97 SoU I 524 197 8.02 147 27800 66 Bethlehem Gut BG-2 16-Sep-97 Sou 1 319 184 8.7 69.6 12900 94.9 Fairplain Gut FPG-I 16-Sep-97 SoU 1 530 181 8.12 154 27700 72.9 Fairplain Gut FPG-2 16-Sep-97 Sou 1 528 169 8.39 148 19100 79.5 Analytical methods: EPA Method 310.1 (aDcalinity), SM 2580 (oxidation/reduction potential), SW-846 9045A (pH), SW8-W46 9050 specific conductance, EPA 415.1 modified (total organic carbon), EPA 160.3 M (total solids) h:\chemrisk\island\data\tables^{)cparams.xls 12/12/97 300915 TABLE 6 VIRGIN ISLAND CHEMICAL SITE GUT AND STORM DRAIN SURFACE SOIL SAMPLING RESULTS PHYSICOCHEMICAL PARAMETERS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Alkalinity (Total) Oxidation/Reduction Potential pH Specific Conductance Total Organic Carbon Total SoUds Units: mg/kg none none umhos mg/kg mg/l River Gut RG-2 23-Sep-97 SoU 1 427 207 8.66 91 17800 78.3 River Gut RG-3 23.Sep-97 SoU 1 962 203 8.27 123 21300 74 River Gut RG-4 23-Sep-97 Sou 1 425 188 8.32 108 22400 86.6 River Gut RG-5 23.Sep-97 Sou 1 4680 172 8.65 70.1 29600 92.9 Analytical methods: EPA Method 310.1 (alkalinity), SM 2580 (oxidation/reduction potential), SW-846 9045A (pH), SW8-W46 9050 specific conductance, EPA 415.1 modified (total organic carbon), EPA 160.3 M (total solids) h:\chemrisk\island\data\tables\pcparains.xls Page 2 of6 12/12/97 300916 TABLE 6 VIRGIN ISLAND CHEMICAL SITE GUT AND STORM DRAIN SURFACE SOIL SAMPLING RESULTS PHYSICOCHEMICAL PARAMETERS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Alkalinity (Total) iOxidation/Reduction Potential pH Specific Conductance Total Organic Caiiran Total Solids Units: mg/kg none none umhos mg/kg mg/l River Gut RG-6 23-Sep-97 SoU I 640 175 8.3 95.9 24300 88.7 River Gut RG-7 23-Sep-97 Sou 1 530 174 8.3 71.5 30500 85.9 River Gut RG-8 23-Sep-97 SoU 1 1180 177 8.22 106 37900 84.4 River Gut RG-9 23-Sep-97 SoU 1 428 181 7.97 139 19600 86.9 Analytical methods: EPA Method 310.1 (alkaUnity), SM 2580 (oxidation/reduction potential), SW-846 9045A (pH), SW8-W46 9050 specific conductance, EPA 415.1 modified (total organic carbon), EPA 160.3 M (total solids) h:\chemrisk\island\data\tables\pcparams.xls Page 3 of6 12/12/97 300917 TABLE 6 VIRGIN ISLAND CHEMICAL SITE GUT AND STORM DRAIN SURFACE SOIL SAMPLING RESULTS PHYSICOCHEMICAL PARAMETERS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: AUcalinity (Total) Oxidation/Reduction Potential pH Specific Conductance Total Organic Carbon Total Solids Units: mg/kg none none umbos mg/kg mgA River Gut RG-10 23-Sep-97 SoU 1 631 169 8.35 154 30800 87.6 River Gut RG-11 23-Sep-97 SoU 1 1070 174 8.29 104 15000 84.1 River Gut FPG-2 16-Sep-97 SoU 1 630 228 8.28 80.7 26800 82.4 River Gut RG-13 16-Sep-97 SoU 1 636 196 7.95 167 28600 85.6 Analytical methods: EPA Method 310.1 (alkalinity), SM 2580 (oxidation/reduction potential). SW-846 9045A (pH). SW8-W46 9050 specific conductance, EPA 415.1 modified (total organic carbon), EPA 160.3 M (total solids) h:\chemrisk\island\data\tables\pcparains.xls Page 4 of6 12/12/97 300918 TABLE 6 VIRGIN ISLAND CHEMICAL SITE GUT AND STORM DRAIN SURFACE SOIL SAMPLING RESULTS PHYSICOCHEMICAL PARAMETERS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FAC 1 OR: ANALYTE: AUcaUnity (Total) Oxidation/Reduction Potential pH Specific Conductance Total Organic Carbon Total SoUds Units: mg/kg none none umhos mg/kg mg/l River Gut RG-14 16-Sep-97 SoU 1 4340 26.3 12.1 1920 49500 49.3 River Gut RG-15 16-Sep-97 SoU 1 417 200 8.71 133 22500 86 River Gut RG-16 16-Sep-97 SoU 1 422 156 8.51 124 18300 78.4 Central Storm Drain SDCSD-2 07-Oct-97 SoU 1 758 206 7.54 123 48500 62.1 Analytical methods: EPA Method 310.1 (aUcalinity), SM 2580 (oxidation/reduction potential), SW-846 9045A (pH), SW8-W46 9050 specific conductance, EPA 415.1 modified (total organic carbon), EPA 160.3 M (total solids) h:\chenirisk\island\data\tables\pcparams.xls Page 5 of6 12/12/97 300919 TABLE 6 VIRGIN ISLAND CHEMICAL SITE GUT AND STORM DRAIN SURFACE SOIL SAMPLING RESULTS PHYSICOCHEMICAL PARAMETERS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: AUcaUnity (Total) Oxidation/Reduction Potential pH Specific Conductance Total Organic Carbon Total Solids Units: mg/kg none none umhos mg/kg mg/l Central Storm Drain SDCSD-3 07-Oct-97 Sou 1 636 190 7.81 87.9 45400 70.5 Southem Storm Drain SDSSD-1 07-Oct-97 SoU 1 544 211 7.83 104 35400 88.3 Southem Storm Drain SDSSD-2 07-Oct-97 SoU 1 456 207 7.71 120 41700 85.6 Analytical methods: EPA Method 310.1 (alkalinity), SM 2580 (oxidation/reduction potential), SW-846 9045A (pH), SW8-W46 9050 specific conductance, EPA 415.1 modified (total organic carbon), EPA 160.3 M (total soUds) h:\chemrisk\island\data\tables\pcparams.xls Page 6 of6 12/12/97 300920 TABLE 7 VIRGIN ISLAND CHEMICAL SITE GUT AND STORM DRAIN SURFACE SOIL SAMPLING RESULTS GRAIN SIZE ANALYSIS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Gravel/Sand SUt Clay Units: % % % Bethlehem Gut BG-l 16-Sep-97 Sou 38.3 22.9 38.9 Bethlehem Gut BG-2 16-Scp-97 SoU 94.5 0.0 5.5 Fairplain Gut FPG-1 16-Sep-97 SoU 66.4 10.9 22.6 Fairplain Gut FPG-2 16-Sep-97 Sou 54.8 20.5 24.6 Aniyzed by ASTM Method D-422 h:\chemrisk\island\data\tables\pcparams.xls Page 1 of6 12/12/97 300921 TABLE 7 VIRGIN ISLAND CHEMICAL SITE GUT AND STORM DRAIN SURFACE SOIL SAMPLING RESULTS GRAIN SIZE ANALYSIS LOCATION: SAMPLE ID NO: DAIE SAMPLED: MAIRIX DILUTION FACTOR: ANALYTE: Gravel/Sand SUt Clay Units: % % % River Gut RG-2 23-Sep-97 Sou 12.7 74.7 12.6 River Gut RG-3 23-Sep-97 SoU 4.0 86.5 9.5 River Gut RG-4 23-Sep-97 SoU 18.8 80.3 0.9 River Gut RG-5 23-Sep-97 Sou 59.4 20.0 20.6 Aniyzed by ASTM Method D-422 h:\chemrisk\island\data\tables\pcparams.xls Page 2 of6 12/12/97 300922 TABLE 7 VIRGIN ISLAND CHEMICAL SITE GUT AND STORM DRAIN SURFACE SOIL SAMPLING RESULTS GRAIN SIZE ANALYSIS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Gravel/Sand SUt Iciav Units: % % % River Gut RG-6 23.Sep-97 Sou 75.8 3.9 20.3 River Gut RG-7 23-Sep.97 SoU 64.7 18.9 16.4 River Gut RG-8 23-Sep-97 SoU 59.0 16.2 24.8 River Gut RG-9 23-Sep-97 Sou 50.9 25.7 23.4 Aniyzed by ASTM Method D-422 h:\chenirisk\island\data\tables\pcparams.xls Page 3 of6 12/12/97 300923 TABLE 7 VIRGIN ISLAND CHEMICAL SITE GUT AND STORM DRAIN SURFACE SOIL SAMPLING RESULTS GRAIN SIZE ANALYSIS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Gravel/Sand SUt Clay Units: % % % River Gut RG-10 23-Sep-97 SoU 52.6 31.1 16.3 River Gut RG-11 23-Sep-97 SoU 54.7 19.1 26.2 River Gut RG-12 16-Sep-97 SoU 54.5 19.7 25.8 River Gut RG-13 16-Sep-97 Sou 51.0 18.2 30.9 Aniyzed by ASTM Method D-422 h:\chemrisk\island\data\tables^>cparams.xls Page 4 of6 12/12/97 300924 TABLE 7 VIRGIN ISLAND CHEMICAL SITE GUT AND STORM DRAIN SURFACE SOIL SAMPLING RESULTS GRAIN SIZE ANALYSIS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Gravel/Sand SUt Clay Units: % % % River Gut RG-14 16-Sep-97 SoU 39.4 51.1 9.5 River Gut RG-15 16-Sep-97 SoU 80.0 12.7 7.3 River Gut RG-16 16-Sep-97 SoU 87.2 4.0 8.8 Central Storm Drain SDCSD-2 07-Oct-97 Sou 66.3 19.3 14.5 Aniyzed by ASTM Method D-422 h:\chemrisk\island\data\tables^)cparams.xls Page 5 of6 12/12/97 300925 TABLE 7 VIRGIN ISLAND CHEMICAL SITE GUT AND STORM DRAIN SURFACE SOIL SAMPLING RESULTS GRAIN SIZE ANALYSIS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Gravel/Sand SUt Clay Units: % % % Central Storm Drain SCSD-3 07-Oct-97 SoU 71.2 14.7 14.1 Southem Storm Drain SDSSD-1 07-Oct-97 SoU 28.7 28.1 43.2 Southem Storm Drain SDSSD-2 07-Oct-97 Sou 42.9 21.8 35.3 Aniyzed by ASTM Method D-422 h:\chemrisk\island\data\tables\pcparams.xls Page 6 of6 12/12/97 3 0 0 9 2 6 TABLE 8 VIRGIN ISLAND CHEMICAL SITE FAIRPLAIN GUT/MANNING BAY SEDIMENT SAMPLING RESULTS SEMIVOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Phenol Pyridine bis-(2-Chloroethyl) Ether 2-Chlorophenol 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene 2-Methylphenol 2,2'-oJc^is (1-Chloropropane) 4-Methylphenol N-Nitroso-Di-n-Propylamine Hexachloroethene Nitrobenzene Isophorone 2-Nitrophenol 2,4-Dimethylphenol bis (2-Chloroethoxy) Methane 2,4-Dichlorophenol 1,2,4-Trichlorobenzene Naphthalene 4-Chlotoaniline Hexachlorobutadiene 4-Chlon)-3-Methylphenol 2-Methyhiaphthalene Hexachlorocyclopentadiene 2,4,6-Trichlonq)henol 2,4,5-Trichlorophenol 2-Chloron2q)hthalene 2-NitroanUine Dimethyl Phthalate Acen^hthylene 2,6-Dinitrotoluene 3-Nitroaniline Acenaphthene 2,4-Dinitrophenol 4-Nitrophenol Dibenzofiiran 2,4-Dinitrotohiene Diethylphthalate CAS#: 108-95-2 110-86-1 lll-W-4 95-57-8 541-73-1 106-46-7 95-50-1 95-48-7 108-60-1 106-44-5 621-64-7 67-72-1 98-95-3 78-59-1 88-75-5 105-67-9 111-91-1 120-83-2 120-82-1 91-20-3 106-47-8 87-68-3 59-50-7 91-57-6 77-47-4 88-06-2 95-95-4 91-58-7 88-74-4 131-11-3 208-%-8 606-20-2 99-09-2 83-32-9 51-28-5 100-02-7 132-64-9 121-14-2 84-66-2 Fairplair I Gut FPG-3 16-Sep-97 Sediment 1 510 510 510 510 510 510 510 510 510 510 510 510 510 510 510 510 510 510 510 510 510 510 510 510 510 510 1200 510 1200 510 510 510 1200 510 1200 1200 510 510 510 U U U U U U U U U U U U U U U U U U U u u u u u u u u u u u u u u u u u u u u Manning Bay MB-1 16-Sep-97 Sediment 410 410 410 410 410 410 410 410 410 410 410 410 410 410 410 410 410 410 410 410 410 410 410 410 410 410 990 410 990 410 410 410 990 410 990 990 410 410 410 1 U U U U U U U u u u u u u u u u u u u u u u u U u u u u u u u u u u u u u u u h:\chemrisk\island\data\tables\svocs.xls Page 1 of2 12/12/97 300927 TABLES VIRGIN ISLAND CHEMICAL SITE FAIRPLAIN GUT/MANNING BAY SEDIMENT SAMPLING RESULTS SEMIVOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPI-ED: MATRIX DILUTION FACI OR: ANALYTE: 4-Chlorophenyl-phenyl ether Fluorene 4-Nitroaniline 4,6-Dinitro-2-Methylphenol N-Nitrosodiphenylamine 4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol Phenanthrene Anthracene Carbazole Di-n-Butylphthalate Fluoranthene Pyrene Butylbenzylphthalate 3,3'-Dichlor6benzidine Benzo(a)Anthracene Chrysene bis(2-EthyUiexyl)Phthalate Di-n-Octyl Phthalate Ben2o(b)Fluoranthene Ben2o(k)Fluoranthene Ben2o(a)Pyrene Indeno(l,2,3-cd)Pyrene Dibenzo(a,h)Anthracene Ben2o(g,h,I)Perylene CAS#: 7005-72-3 86-73-7 100-01-6 534-52-1 86-30-6 101-55-3 118-74-1 87-86-5 85-01-8 120-12-7 86-74-8 84-74-2 206-44-0 129-00-0 85-68-7 91-94-1 56-55-3 218-01-9 117-81-7 117-84-0 205-99-2 207-08-9 50-32-8 193-39-5 53-70-3 191-24-2 Fairplain Gut FPG-3 16-Sep-97 Sediment 1 510 510 1200 1200 510 510 510 1200 510 510 510 510 510 510 510 510 510 510 510 510 510 510 510 510 510 510 U U U U U u u u u u u u u u u u u u u u u u u u u u Manning Bay MB-1 16-Sep-97 Sediment 1 410 410 990 990 410 410 410 990 410 410 410 410 410 410 410 410 410 410 410 410 410 410 410 410 410 410 U U U U U U U U U U U U U U U U U U U U U U U u u u Notes AU results reported in ug/kg Analyzed by CLP method OLMO 1.9 modified for pyridine analysis U = Analyte was not detected above the referenced reporting limit. J = Indicates an estimated value B = Analyte was found in the blank as weU as the sample h:\chemrisk\island\data\tables\svocs.xls Page 2 of2 12/12/97 300928 TABLE 9 VIRGIN ISLAND CHEMICAL SITE FAIRPLAIN GUT/MANNING BAY SEDIMENT SAMPLING RESULTS METALS LOCATION: SAMPLE ID NO: DATE SAMPLED: MAIKIX DILUTION FACTOR: ANALYTE: Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc Cyanide CAS#: 7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0, 7440-09-0 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6 57-12-5 Fairplair Gut FPG-3 16-Sep -97 Sediment 9150 0.62 1.3 61.4 0.03 0.05 17900 13.7 9.3 25.8 15200 5.6 4210 197 0.15 7 2720 1.2 0.18 21100 0.68 69.4 29.3 1.5 U BJ B U B BJ J J J U B J B U B U J U Manning Bay MB-1 16-Sep-97 Sediment 2770 0.49 U 1.7 B 8.7 B 0.02 U 0.02 U 21300 3 3 BJ 6 B 4320 2.6 J 1850 64.6 J 0.12 U 1.5 B 493 B 0.62 U 0.15 U llio B 0.54 U 16.6 12.2 J 1.2 U Notes All results reported in mg/kg Analyzed by CLP method ILMO 3.0 U = Analyte was not deteced above the referenced reporting limit J = Indicates an estimated value B = Result is between the instmment detection limit (IDL) and the contract required detection limit (CRDL) R = Data is unusable h:\chemrisk\island\data\tables\METALS-Gut Sediments Page 1 of 1 3 0 0 9 2 9 12/15/97 TABLE 10 VIRGIN ISLAND CHEMICAL SITE FAIRPLAIN GUT/MANNING BAY SEDIMENT SAMPLING RESULTS PHYSICOCHEMICAL PARAMETERS LOCATION: SAMPLE ID NO: DATE SAMPLED: MAIRIX DILUTION FACTOR: ANALYTE: Units: AUcalinity (Total) mg/kg Oxidation/Reduction Potential none pH none Specific Conductance umhos Total Organic Clarbon mg/kg Total SoUds mg/l Fairplain Gut FPG-3 16-Sep-97 Sediment 1 1050 96 8.25 1550 17200 65.7 Manning Bay MB-1 16-Sep-97 Sediment 1 317 116 8.63 337 9910 80.9 Analytical methods: EPA Method 310.1 (alkalinity), SM 2580 (oxidation/reduction potential), SW-846 9045A (pH), SW8-W46 9050 specific conductance, EPA 415.1 modified (total organic carbon), EPA 160.3 M (total soUds) h:\chemrisk\island\data\tables\pcparams.xls 12/12/97 300930 TABLE 11 VIRGIN ISLAND CHEMICAL SITE FAIRPLAIN GUT/MANNING BAY SEDIMENT SAMPLING RESULTS GRAIN SIZE ANALYSIS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Units: Gravel/Sand % SiU % Clay % Fairplain Gut FPG-3 16-Sep-97 Sediment 76.0 3.9 20.1 Manning Bay MB-1 16-Sep-97 Sediment 99.0 0.3 0.6 Aniyzed by ASTM Method D-422 h:\chemrisk\island\data\tables\pcparams.xls 12/12/97 300931 TABLE 12 VIRGIN ISLAND CHEMICAL SITE SOIL BORING SAMPLING RESULTS BIOLOGICAL PARAMETERS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Units: total populations (mean) cfii/gm (DSW) degrader populations (mean) cfii/gm (DSW) AST Area SBAST-8 (8-10) 24-Sep-97 Sou 1.80E-K)3 2.00E-K)2 AST Area SBAST-9 (10-12) 24-Sep-97 SoU 3.10E-K)4 1.00E-K)4 Notes Analyzed by method SM 9215C M (hydrocarbon utilization bacteria (HCU)) cfii/gm (DSW) = colony forming units per gram of dry soU weight L h:\chemrisk\island\soildata\tables^^>cparams.xls 12/12/97 300932 TABLE 13 VIRGIN ISLAND CEtEMICAL SITE SOIL BORING SAMPLING RESULTS PHYSICOCHEMICAL PARAMETERS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Gravel Sand SUt or Clay Moisture Content Total Organic Carbon Porosity Alkalinity (Total) Iron Ammonia Nitrite Nitrate Ortho phosphate Sulfate Sulfide Atterberg Limits - Liquid Limit Atterberg Limits - Plastic Limit Atterberg Limits - Plasticity Index Hydraulic Conductivity Units: % % % % mg/kg mg/l mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg cm/s AST Area SBAST-8 (6-8) 24-Sep-97 SoU 11 40 49 17 5900 0.38 40 17 23 e.i^io-* AST Area SBAST-9 (8-10) 24-Sep-97 SoU 13 32 45 13 23000 0.32 50 19 31 2.9*10-' AST Area SBAST-8 (8-10) 24-Sep-97 SoU 17 1650 1350 20500 ND ND ND 133 ND ND AST Area SBAST-9 (10-12) 24-Sep-97 SoU 17 2790 998 14800 ND ND ND 97.8 ND ND Analytical Methods: ASTM D422 (grain size). ASTM D4318 (Moisture content), EPA-600 Method 415.1 (TOC), ASTMD5084 (porosity), SW 6010 (iron), EPA 310.1 (alkalinity-total), EPA 350.2 (ammonia), EPA 353.2 (nitrate), EPA 353.2 (nitrite), EPA 365.3 (ortho-phosphate), SW 9036 (sulfate), SW 9030 (sulfide), and SW 9060 (total organic carbon) h:\chemrisk\island\soUdata\pcparams.xls Page 1 ofl 12/12/97 300933 TABLE 14 VIRGIN ISLAND CHEMICAL SITE PRELIMINARY SOIL BORING SAMPLING RESULTS PROCESS PIT AREA VOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Chloromethane Bromomethane Vinyl Chloride CWoroe thane Methylene Chloride Acetone Carbon Disulfide 1,1-Dichloroethene 1,1 -Dichloroethane 1,2-Dichloroethene(total) Chloroform 1,2-Dichloroethane 2-Butanone 1,1,1-Trichloroethane Carbon Tetrachloride Bromodichloromethane 1,2-Dichloropropane cis-1,3-Dichloropropene Trichloroethene Dibromochloromethane 1,1,2-Trichloroethane Benzene CAS#: 74-87-3 74-83-9 75-01-4 75-00-3 75-09-2 67-64-1 75-15-0 75-35^ 75-34-3 540-59-0 67-66-3 107-06-2 78-93-3 71-55-6 56-23-5 75-27-4 78-87-5 10061-01-5 79-01-6 124-48-1 79-00-5 71-43-2 trans-l,3-Dichloropropene 10061-02-6 Bromoform 4-Methyl-2-Pentanone 2-Hexanone Tetrachloroethene 1,1,2,2-Tetrachloroethane Toluene Chlorobenzene Ethylbenzene Styrene Xylene(total) 75-25-2 108-10-1 591-78-6 127-18^ 79-34-5 108-88-3 108-90-7 lOO^M 100-42-5 1330-20-7 Process Pit SBPP-1/11-13 04-Dec-97 Soil 1 10 U 10 u 10 u 10 u 24.4 All 6120 10 U 10 U 10 U 10 U 52.6 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u Process Pit SBPP-1/25-27 04-Dec-97 Soil 1 10 u 10 U 10 u 10 u 15.9 All 10 U 10 U 10 U 10 U 10 U 37.2 10 U 10 U 10 U lOU 10 U 10 U 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u Process Pit SBPP-2/10-12 04-Dec-97 Soil 1 10 u 10 u 10 u 10 u 37.4 Al 1 48.8 All 10 U 10 U 10 U 10 U 52.5 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u Process Pit SBPP-2/23-25 04-Dec-97 Soil 1 10 u 10 u 10 u 10 u 27.8 All 10 U 10 U 10 U 10 U 10 U 13.2 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u Process Pit SBPP-3/8-10 04-Dec-97 Soil 1 10 u 10 u 10 u 10 u 26.2 All 10 U 10 U 10 U 10 U 10 U 34.9 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u Notes: All results reported in ug/kg Analyzed by semiquanititative screen on a wet weight basis Results are preliminary and subject to further evaluation U = Analyte was not detected above the referenced reporting limit. Al 1= This analyte is a common solvent. Its presence in field samples may be an artifact of sample collection, transport or analysis. h:\chemrisk\isIand\soildata\tables\VOCS-PROCESS PIT 12/15/97 300934 TABLE 14 VIRGIN ISLAND CHEMICAL SITE PRELIMINARY SOIL BORING SAMPLING RESULTS PROCESS PIT AREA VOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Chloromethane Bromomethane Vinyl Chloride Chloroethane Methylene Chloride Acetone Carbon Disulfide 1,1-Dichloroethene 1,1-Dichloroethane 1,2-Dichloroethene(total) Chloroform 1,2-Dichloroethane 2-Butanone 1,1,1-Trichloroethane Carbon Tetrachloride Bromodichloromethane 1,2-Dichloropropane cis-1,3-Dichloropropene Trichloroethene Dibromochloromethane 1,1,2-Trichloroethane Benzene CAS#: 74-87-3 74-83-9 75-OM 75-00-3 75-09-2 67-64-1 75-15-0 75-35-4 75-34-3 540-59-0 67-66-3 107-06-2 78-93-3 71-55-6 56-23-5 75-27-4 78-87-5 10061-01-5 79-01-6 124^8-1 79-00-5 7M3-2 trans-1,3-Dichloropropene 10061-02-6 Bromoform 4-Methyl-2-Pentanone 2-Hexanone Tetrachloroethene 75-25-2 108-10-1 591-78-6 127-18-4 1,1,2,2-Tetrachloroethane 79-34-5 Toluene Chlorobenzene Ethylbenzene Styrene Xylene(total) 108-88-3 108-90-7 100-41-4 100-42-5 1330-20-7 Process Pit SBPP-3/24-26 04-Dec-97 Soil 1 10 U 10 U 10 U 10 U 24.7 All 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u Process Pit SBPP-4/8-10 04-Dec-97 Soil 1 10 u 10 u 10 u 10 u 25.9 All 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 U 10 U 10 u 10 U 10 U 10 u 10 u 10 u 10 u 10 u Process Pit SBPP^/21-23 04-Dec-97 Soil 1 10 u 10 u 10 u 10 u 21.4 All 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u Process Pit SBPP-4/21-23D 04-Dec-97 Soil 1 10 u 10 u 10 u 10 u 20.4 All 10 U 10 U 10 U 10 U 10 U 60.9 10 U 10 U 10 U 10 U 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u Notes All results reported in ug/kg Analyzed by semiquanititative screen on a wet weight basis Results are preliminary and subject to fiirther evaluation U = Analyte was not detected above the referenced reporting limit. Al 1= This analyte is a common solvent. Its presence in field samples may be an artifact of sample collection, transport or analysis. h:\chemrisk\island\soildata\tables\VOCS-PROCESS PIT 12/15/97 3 0 0 9 3 5 TABLE 15 VIRGIN ISLAND CHEMICAL SITE PRELIMINARY SOIL BORING SAMPLING RESULTS LAB PIT AREA VOLATILE ORGANIC COMPOUNDS LOCATION: SAMPLE ID NO: DATE SAMPLED: MATRIX DILUTION FACTOR: ANALYTE: Chloromethane Bromomethane Vinyl Chloride Chloroethane Methylene Chloride Acetone Carbon Disulfide 1,1 -Dichloroethene 1,1 -Dichloroethane 1,2-Dichloroethene{total) Chloroform 1,2-Dichloroethane 2-Butanone 1,1,1 -Trichloroethane Carbon Tetrachloride Bromodichloromethane 1,2-Dichloropropane cis-1,3-Dichloropropene Trichloroethene Dibromochloromethane 1,1,2-Trichloroethane Benzene CAS#: 74-87-3 74-83-9 75-OM 75-00-3 75-09-2 67-64-1 75-15-0 75-35-4 75-34-3 540-59-0 67-66-3 107-06-2 78-93-3 71-55-6 56-23-5 75-27-4 78-87-5 10061-01-5 79-01-6 12448-1 79-00-5 7M3-2 trans-1,3-Dichloropropene 10061 -02-6 Bromoform 4-Methyl-2-Pentanone 2-Hexanone Tetrachloroethene 1,1,2,2-Tetrachloroethane Toluene Chlorobenzene Ethylbenzene Styrene Xylene(total) 75-25-2 108-10-1 591-78-6 127-184 79-34-5 108-88-3 108-90-7 1004M 100-42-5 1330-20-7 Lab Pit SBLP-1/8-10 lO-Dec-97 Soil 1 10 U 10 U 10 u 10 u 19.4 All 27.7 All 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 U 10 u 10 U 10 u 10 u 10 u 10 u 10 U 10 u Lab Pit SBLP-1/15-17 lO-Dec-97 Soil 1 10 u 10 u 10 u 10 u 20.1 All 33.7 All 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 u .10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u Lab Pit SBLP-2/8-10 lO-Dec-97 Son 1 10 U 10 u 10 u 10 u 20.9 All 29.1 All 10 U 10 U 10 U 10 U ' 10 U 10 U 10 U 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u Lab Pit SBLP-2/13-15 lO-Dec-97 Soil 1 10 u 10 u 10 u 10 u 20.2 All 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u Notes: All results reported in ug/kg Analyzed by semiquanititative screen on a wet weight basis Results are preliminary and subject to further evaluation U = Analyte was not detected above the referenced reporting limit. Al 1= This analyte is a common solvent. Its presence in field samples may be an artifact of sample collection, transport or analysis. h:\chemrisk\island\soildata\tables\VOCS-LABPIT 12/15/97 300936