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RAC2 EPA Region 2 Final Quality Assurance Project Plan Tutu Wellfield Site Long Term Response Action St. Thomas, U.S. Virgin Island EPA Contract No. EP-W-09-002 WA aaa iced April 2009 125 Maiden Lane, Sth Floor New York, New York 10038 tel; 212 785-9123 fax: 212 785-6114 April 14, 2009 Ms. Caroline Kwan Remedial Project Manager U.S. Environmental Protection Agency 290 Broadway - 20" Floor New York, NY 10007-1866 PROJECT: RAC2 Contract No.: EP-W-09-002 Work Assignment No.: 003-RALR-021D DOC. CONTROL NO.:: 3220-003-00052 SUBJECT: Final Quality Assurance Project Plan Long Term Response Action Tutu Wellfield Site St. Thomas, U.S. Virgin Islands Dear Ms. Kwan: CDM Federal Programs Corporation (CDM) is pleased to submit the above-referenced document for the Long Term Response Action at the Tutu Wellfield Site in St. Thomas, U.S. Virgin Islands as partial fulfillment of Subtask 5.2 of the Statement of Work. If you have any questions regarding this submittal, please contact me at your earliest convenience at (212) 785-9123. Very truly yours, CDM FEDERAL PROGRAMS CORPORATION Demetrios Klerides Project Manager aa PSO: / Ly Enclosure ec: F. Rosado, EPA Region 2 E. Gallerie, CDM L. Mauel, EPA Region 2 J. Oxford, CDM W. Sy, EPA Region 2 RAC2 Document Control S. Syedali, USVI DPNR D. Klerides, CDM consulting - engineering - construction . operations RESPONSE ACTION CONTRACT FOR REMEDIAL RESPONSE, ENFORCEMENT OVERSIGHT, CRITICAL REMOVAL ACTIVITIES AT SITES OF RELEASE OR THREATENED RELEASE OF HAZARDOUS SUBSTANCES IN EPA REGION 2 Final Quality Assurance Project Plan Tutu Wellfield Site Long Term Response Action St. Thomas, U.S, Virgin Islands Work Assignment No. 003-RALR-021D U.S. EPA CONTRACT NO, EP-W-09-002 Document Control No.: 3220-003-00052 April 14, 2009 Prepared for: U.S. Environmental Protection Agency 290 Broadway New York, New York 10007-1866 Prepared by: CDM Federal Programs Corporation 125 Maiden Lane, 5th Floor New York, New York 10038 This document has been prepared for the U.S, Environmental Protection Agency under Contract No. EP-W-09-002. The material contained herein is not to be disclosed to, discussed with, or made available to any person or persons for any reason without prior expressed approval of a responsible official of the U.S, Environmental Protection Agency. Tutu Wellfield Superfund Site Table of Contents Page i of ili Contents QAPP Worksheet #1 Title And Approval Page .....c.ccssessssessssseesessssecsssesssoaenrenssenersnearsersasnessraesoneeaceeees 1 QAPP Worksheet #2 QAPP Identifying INFOrmation wu... ciccccecseesecsseesseeseressecnesereaseessssrneeseaerenenesensesy 2 QAPP Worksheet #3 Distribution List ..........cccccccesssescscsesessseseeceeens Rashad onanasiandencasshanciaslel deahcnhas ldecensl 7 QAPP Worksheet #4 Project Personnel Sign-off SHC... ciccceesssecssecssecseseseesseseseecueesesseeaveneessnagesy 8 QAPP Worksheet #5 Project Organizational Chart... ccccccccseesssesseessssecesensenessesssssesesseseesaereersengeeey 9 QAPP Worksheet #6 Communication Pathways ...........cccceccscccecseneesersssenssecneseesessenestiseeessenssaseneseneesaees 10 QAPP Worksheet #7 Personnel Responsibilities and Qualifications Table... ccc eecescsessessreeseneeeteeesees 12 QAPP Worksheet #8 Special Personnel Training Requirements Table .......ccccsscssceesrnesessscsecsescsseses 14 QAPP Worksheet #9 Project Scoping Session Participants Sheet .......sccccceceeeescsessccecessecsecsssesereseees 16 QAP Worksheets 1D. Problenn DefinibOieccccsscssussyecnviscunyeansticsprasedvecspeaders cuseetenbodeeceunsnacpuaubdereanaeicesenasaagees 18 QAPP Worksheet #11 Project Quality Objectives/Systematic Planning Process Statements .................. 22 QAPP Worksheet #12 Measurement Performance Criteria Table QAPP Worksheet #12a Aqueous TCL VOCS (Trace)... ceceeneseseceeseseseeseesesseeeeteeseeeneeeesneenes 24 QAPP Worksheet #12b Aqueous Chloride, Nitrate, and Sulfate oo... ee eeeeeeeeeerseees 25 QAPP Worksheet #12¢ AQUEOUS TOC .......ccccsscccccsesseccssiensscenceensecsensesssuecteassemseseneserseseussennsaneaes 26 QAPP Worksheet #12d AQUEOUS TSS.........ccceecccsscesccssessesnnseneeesesnsecesnsseessssscsasseasseceeesataseeneeeees 27 QAPP Worksheet #12e Aqueous Ethane & Ethene ........cccesceessccesteenteeeseesceteeeeeeeesneeeeeeseeees 28 QAPP Worksheet #12f PATE ONS Bir cacandneteas ee ncaaascn sans oan ensakh Se ONeh Tats uAT Ge ERMAN eT ovaries 29 QAPP Worksheet #13 Secondary Data Criteria and Limitations Table... ceeeeeeeeeteeereeeeeteeteeeneee 30 QAPP Worksheet #14 Summary of Project Tasks... cece eecceeeteeeeeeceeeeeseeceseeenenensersescseersesessaeeeseneeeres 31 QAPP Worksheet #15 Reference Limits and Evaluation Table QAPP Worksheet #15a Groundwater VOCS .....ccccecccceccscceeeeseeeeeeeeeeesereeeseeeeeseeseteereesseeenieserays 36 QAPP Worksheet #15b Groundwater Wet Chemistry ..........::ccccececceeeereseeeeseeseeeereeenaresteeenseeeenaes 37 GAPP WOrFKSHECEHISG) AIP MOG S iii nossessicszases soaurcamseSrerneene teamed endaesidddapassabandyamornerabennstess 38 QAPP Worksheet #16 Project Schedule/Timeline Table oo... ceccccsesseceseeeeseeeeeesensesnseeeenaeersseaeesnaeres 39 QAPP Worksheet #17 Sampling Design and Rationale ...........c.ccceeceseeceesseeeessenreesensneeserreststesresteseeseseens 40 GAPP Worksh@etghli7a MpbIIZAU ON sc. cccssaceazanss escorts gases aeente rs aeueoera seated duneg nd geadeaabnesd ehaebsyearbaa 41 QAPP Worksheet #17b Operation, Maintenance, and Monitoring ..........cccceeeeresreteerseseeeeenreens 42 QAPP Worksheet #17c Continuous Water Level Measurement. ..........cceeeeeeeeeeeeeesteeeeerseeesenreens 43 QAPP Worksheet #17d Synoptic Water Level Measurements..........cc cece eeesceseseseeseseeereeeererrneees 44 QAPP Worksheet #17e Groundwater SAMPpling wo... ceecseseecceeeeeeeeeseneeerseeeeeaeeetaeessseeeenensenees 45 QAPP Worksheet #17f Process Sampling .........cccccccccsecseeseeeessessseeeeeeeeeesesseeeeeneeerereeserstererenaees 46 QAPP Worksheet #17g Decontamination Procedures ..........ceecscceeeeeseteeeeeeeeseeeetseeersneeeennnnesees 47 QAPP Worksheet #17h_ Investigation Derived WaSte............ cc eecssceeeeereseeteeeeeeeeeeseeerseeeenseseeetnaneges 48 CDM Final Quality Assurance Project Plan Tutu Wellfield Superfund Site Table of Contents Page ii of iii QAPP Worksheet #18 Sampling Locations and Methods/SOP Requirements Table ..........cccccccecseeees 50 QAPP Worksheet #19 Analytical SOP Requirements Table ........::ccccscccseceseesesseecseeeeresseeeeessrssseenseceeesees 51 QAPP Worksheet #20 Field Quality Control Sample Summary Table ............cccccccesseceeesseesseseseneeeeeeneess 52 QAPP Worksheet #21 Project Sampling SOP References Table.........cccccccscseeeueeetsenesnsssessserenesenee 5S QAPP Worksheet #22 Field Equipment Calibration, Maintenance, Testing, and Inspection Table ......... 54 QAPP Worksheet #23 Analytical SOP References Table ........cccccccesecceeecssesesessteceseseseredessssssesensesseees 56 QAPP Worksheet #24 Analytical Instrument Calibration Table oo... cccccccccsecsesscesscsssessesesseeseesensees 57 QAPP Worksheet #25 Analytical Instrument and Equipment Maintenance, Testing, BHA INS pSction Tal Oasis sss csssssevescerssensingcazreavavacatosaa vase sdyaseaaestoscuaecuapasss sivesbeouinieeias 59 QAPP Worksheet #26 Sample Handling System .........ccccccccccccsscsssseecsssecssscesseessesesseessecssseeesseseaaeeesaseneees 60 QAPP Worksheet #27 Sample Custody Requirement ...........c:cccccccccsseesseesessecssecnseseeteecseseaescaesaeensesasens 62 QAPP Worksheet #28 QC Samples Table..is...cssssesessssssesseesessssesssccsscsessesanneasvavsnesesssaseassinnesgensiaasessensstente 63 QAPP Worksheet #28-a Aqueous TCL VOCS (Trace) oo... eecesenseeneetsessessseeesseeseaeensesersnsesseenes 65 QAPP Worksheet #28-b Aqueous Nitrate, Sulfate, and Chloride... ccccceecereecsseeesseesseeenes 66 QAPP Worksheet #28-c AQUEOUS TOC .........ccccccesceesseseecssseessseeceseseccsecssesceusesaesnaeeeeeesseseseees 67 GAPP. Worksheet #28-d). AQUeCOUS TSS: issicsssscciassucesiscaads casdinee hls neages sb eansianas eanndaspaaaasieaaiasavea alae 68 QAPP Worksheet #28-e Aqueous Ethane/Ethene............cccccccssscsessssestsessseesssrseseeseesesesesesnseens 69 QAPP Worksheet#28-f “Alr VOC wveaisd avis accuse avtiicccassensieucsteoi acctanesldttasps Hagieeisssqebaviasiieaiauaats 70 QAPP Worksheet #29 Project Documents and Records Table ......ccccccccccsseeeseeeenenessecssscessscsesseeseseeees 71 QAPP Worksheet #30 Project Analytical Services Table oo... cccccccssesseeerecsecrecseeseetsetsecsesssecseccsseeseeeees 73 QAPP Worksheet #31 Planned Project Assessment Table............ccccccsccectssssscsscsesseeeecceseeecsseesseessseceaeenaye 74 QAPP Worksheet #32 Assessment Findings and Corrective Action RESPONSES ........:cccccccccseeeeseeneeeeees 75 QAPP Worksheet #33 QA Management Reports Table........cccccceccesessersessecsssssesssenssssestseesseessseassnessares 76 QAPP Worksheet #34 Verification (Step 1) Process Table oe... ccceececccsecereeereeeeteeceeeenenesesereenesenseneens 77 QAPP Worksheet #35 Validation (Steps Ila and IIb) Process Table 0.0... cccccecceeeetetseeseeeeeerseeneenseenasnnees 78 QAPP Worksheet #36 Validation (Steps Ila and IIb) Summary Table..........ccceeceeeeceeeeeneeceeseneeeseeneeneee 79 QAPP Worksheet #37 Usability ASSESSMENE).......ccssessccesseecssssvsesenssseeenaetscccosasessscnasssscesaneepoasenasenneenneons 80 Glossary of Abbreviations References CDM Final Quality Assurance Project Plan Tables Table 1 Table 2 Table 3 Figures Figure 1 Figure 2 Figure 3 Figure 4 Appendices Appendix A Appendix B Appendix C Tutu Wellfield Superfund Site Table of Contents Page iii of iti Monitoring Well Construction Sampling and Monitoring Schedule Site-wide Groundwater Monitoring Schedule Site Location Site-wide Groundwater Elevations and CVOC Concentrations Groundwater Treatment Facility #1 Schematic and Sample Locations Groundwater Treatment Facility #2 Schematic and Sample Locations Site-Specific Low Flow Groundwater Purging and Sampling CDM Technical Standard Operating Procedures -2 Sample Custody* -6 Water Level Measurement -8 Vapor Sampling using a SUMMA Cannister -10 Field Measurement of Organic Vapors -1 Packaging and Shipping of Environmental Samples* -2 Guide to Handling of Investigation Derived Waste -1 Control of Measurement and Test Equipment MP hM = = = = * Includes RAC || Contract-Specific Clarification Field Forms Groundwater Sampling Purge Water Data Form Multi-parameter Water Quality Instrumentation Calibration Log Field Change Request (FCR) Form ANSETS Data Requirement System Runtime and Shutdown Log — GWTF#1 System Runtime and Shutdown Log — GWTF#2 Groundwater Influent Monitoring Data - GWTF#1 Groundwater Influent Monitoring Data — GWTF#2 Systems Monitoring Data — GWTF#1 Systems Monitoring Data — GWTF#2 Monthly Operations and Maintenance Activities - GWTF#1 Monthly Operations and Maintenance Activities - GWTF#2 Synoptic Groundwater Levels CAN Oona whys =a - Oo —_ — Final Quality Assurance Project Plan \ Tutu Wellfield Superfund Site Revision Number: 0 April 14, 2009 QAPP Worksheet #1 Title and Approval Page FINAL QUALITY ASSURANCE PROJECT PLAN (QAPP) for Tutu Wellfield Superfund Site ' Long Term Response Action St. Thomas, US Virgin Islands US Environmental Protection Agency (EPA) Region 2 Prepared by; CDM Federal Programs Corporation (CDM) 125 Maiden Lane, 5" Floor New York, NY 10038 (2142) 785-9123 Date; April 14, 2009 CDM Project Manager: Demetrios Klerides, P.E. \ ' ” Signature Lem Bl, le; eile} CDM OA Manager: Doug Updike Signature f EPA Project Manager: CENT , Signature a CDM RAC I] Program Manager: Jeanne Litwin Signature LALA. EPA Region 2 Hazardous Waste Support Section: Linda Mauel Signature bun Document Control Number: 3220-003-00052 Final Quality Assurance Project Plan Tutu Wellfield Superfund Site Revision Number: 0 QAPP Worksheet #2 QAPP Identifying Information Site Name/Project: Site Location: Operable Unit: Contractor Name: Contractor Number: Contract Title: Work Assignment Number: Regulatory Program: Approval Entity: Is QAPP Generic or Project Specific: Dates of scoping sessions: Tutu Wellfield Superfund Site Long Term Response Action St. Thomas, US Virgin Islands Not Applicable (N/A) CDM EP-W-09-002 Response Action Contract Region 2 N/A CERCLA EPA Region 2 Project Specific 11/19/08 and 11/21/08 Dates and Titles of QAPP Documents Written for Previous Site Work, if Applicable: Final Data Quality Assurance Project Plan, Tutu Wellfield Superfund Site: August 19, 2003 Organizational Partners (stakeholders) and Connection with Lead Organization: United States Virgin Islands (USVI) Department of Planning and Natural Resources (DPNR) Data Users: CDM, EPA Region 2, USVI DPNR April 14, 2009 Required QAPP elements and required information that are not applicable to the project, and an explanation for their exclusions: N/A CDM Final Quality Assurance Project Plan QAPP Worksheet #2 QAPP Identifying Information (continued) Tutu Wellfield Superfund Site Revision Number: 0 April 14, 2009 Crosswalk to Required QAPP Element(s) and Related Corresponding QAPP Section(s) Required Information Worksheets Project Management and Objectives 2.1 Title and Approval Page - Title and Approval Page 4 2.2 Document Format and Table of - Table of Contents Contents - QAPP Identifying 2 2.2.1 Document Control Format Information 2.2.2 Document Control Numbering System 2.2.3 Table of Contents 2.2.4 QAPP Identifying Information 2.3 Distribution List and Project Personnel | - Distribution List 3 Sign-Off Sheet - Project Personnel Sign-Off 4 2.3.1 Distribution List Sheet 2.3.2 Project Personnel Sign-Off Sheet 2.4 Project Organization - Project Organizational Chart 5 2.4.1 Project Organizational Chart - Communication Pathways 6 2.4.2 Communication Pathways - Personnel Responsibilities 7 2.4.3. Personnel Responsibilities and and Qualifications Table Qualifications - Special Personnel Training 8 2.4.4 Special Training Requirements Requirements Table and Certification 2.5 Project Planning/Problem Definition - Project Planning Session 9 2.5.1 Project Planning (Scoping) Documentation (including 2.5.2 Problem Definition, Site History, Data Needs tables) and Background - Project Scoping Session Participants Sheet - Problem Definition, Site 10 History, and Background - Site Maps (historical and present) 2.6 Project Quality Objectives (PQO) and | - Site-Specific PQOs 11 Measurement Performance Criteria - Measurement Performance 12 2.6.1 Development of Project Quality Criteria Table Objectives Using the Systematic Planning Process 2.6.2 Measurement Performance Criteria Final Quality Assurance Project Plan Tutu Wellfield Superfund Site QAPP Worksheet #2 QAPP Identifying Information (continued) Revision Number: 0 April 14, 2009 Crosswalk to Required QAPP Element(s) and Related Corresponding QAPP Section(s) Required Information Worksheets 2.7 Secondary Data Evaluation - Sources of Secondary Data 13 and Information - Secondary Data Criteria and Limitations Table 2.8 Project Overview and Schedule - Summary of Project Tasks 14 2.8.1 Project Overview - Reference Limits and 15 2.8.2 Project Schedule Evaluation Table - Project Schedule/Timeline 16 Table Measurement/Data Acquisition 3.1 Sampling Tasks 3.1.1. Sampling Process Design and Rationale 3.1.2 Sampling Procedures and Requirements 3.1.2.1. Sampling Collection - Sampling Design and Rationale - Sample Location Map - Sampling Locations and Methods/SOP Requirements Table 17, Figures 3 & 4 18, Figures 3&4 and Inspection Procedures 3.2.4 Analytical Supply Inspection and Acceptance Procedures Procedures - Analytical Methods/standard 19 3.1.2.2 Sample Containers, Volume, operating procedures (SOP) and Preservation Requirements Table 20 3.1.2.3. Equipment/Sample - Field Quality Control Sample Containers Cleaning and Summary Table 21 Decontamination - Sampling SOPs Procedures - Project Sampling SOP 3.1.2.4 Field Equipment Calibration, References Maintenance, Testing, and Table 22 Inspection Procedures - Field Equipment Calibration, 3.1.2.5 Supply Inspection and Maintenance, Testing, and Acceptance Inspection Table Procedures 3.1.2.6 Field Documentation Procedures 3.2 Analytical Tasks - Analytical SOPs 23 3.2.1 Analytical SOPs - Analytical SOP References 3.2.2 Analytical Instrument Calibration Table Procedures - Analytical Instrument 24 3.2.3 Analytical Instrument and Calibration Table Equipment Maintenance, Testing, | - Analytical Instrument and 25 Equipment Maintenance, Testing, and Inspection Table Final Quality Assurance Project Plan Tutu Wellfield Superfund Site QAPP Worksheet #2 QAPP Identifying Information (continued) Revision Number: 0 April 14, 2009 Crosswalk to Required QAPP Element(s) and Required Corresponding QAPP Section(s) Required Information Worksheets 3.3 Sample Collection Documentation, - Sample Collection 26 Handling, Tracking, and Custody Documentation Handling, Procedures Tracking, and Custody 3.3.1 Sample Collection Documentation SOPs 3.3.2 Sample Handling and Tracking - Sample Container System Identification 3.3.3 Sample Custody - Sample Handling Flow Diagram - Example Chain-of-Custody 27 Form and Seal 3.4 Quality Control (QC) Samples - QC Samples Table 28 3.4.1 Sampling Quality Control Samples | - Screening/Confirmatory N/A 3.4.2 Analytical Quality Control Samples Analysis Decision Tree 3.5 Data Management Tasks - Project Documents and 29 3.5.1 Project Documentation and Records Table Records - Analytical Services Table 30 3.5.2 Data Package Deliverables - Data Management SOPs N/A 3.5.3 Data Reporting Formats 3.5.4 Data Handling and Management 3.5.5 Data Tracking and Control Assessment/Oversight 4.1 Assessments and Response Actions - Assessments and Response 31 4.1.1 Planned Assessments Actions 4.1.2 Assessment Findings and - Planned Project Assessments Corrective Table Action Responses - Audit Checklists N/A - Assessment Findings and 32 Corrective Action Responses Table 4.2 Quality Assurance (QA) Management | - QA Management Reports 33 Reports Table 4.3. Final Project Report CDM Final Quality Assurance Project Plan Tutu Wellfield Superfund Site Revision Number: 0 April 14, 2009 QAPP Worksheet #2 QAPP Identifying Information (continued) Crosswalk to Required QAPP Element(s) and Related Corresponding QAPP Section(s) Required Information Worksheets Data Review 5.1 Overview 5.2 Data Review Steps Verification (Step |) Process 34 5.2.1 Step |: Verification Table 35 5,2.2 Step Il: Validation Validation (Steps Ila and IIb) 5.2.2.1 Step lla Validation Activities Process Table 5.2.2.2 Step Ilb Validation Activities Validation (Steps Ila and IIb) 36 5.2.3. Step Ill: Usability Assessment Summary Table 5.2.3.1 Data Limitations and Actions Usability Assessment 37 from Usability Assessment 5.2.3.2 Activities 5.3 Streamlining Data Review None 5.3.1 Data Review Steps To Be Streamlined Streamlining of 5.3.2 Criteria for Streamlining Data Data Validation Review will not be 5.3.3 Amounts and Types of Data performed Appropriate for Streamlining CDM Final Quality Assurance Project Plan UBlq joalolY aoueJNss, [BND [Bula Jebeuey\| Woo WpPI©{uimy}| VLLO-S8z (ZLZ) v7Sr-LZle (ZLZ) Wad wes6Old Z OVY UIMII] Quuesr JB9INO YO y8lO1d KOWOY) soyeulpso0gD WOd’ Wpo®) w/p1ojxo 7LLO-S8Z (ZZ) 9ESb-ZZE (ZZ) wad VO jeucibey PJOJXO Jayiuer woo wpo®esaayje6 vLL9-Sgz (ZLZ) GZSb-LLE (ZLZ) wad Jesuibul yell Ad ‘avayjes uaz WO UpI® psepiia|} vLLO-S8Z (ZZ) GESp-Z Ze (Z1Z) wad Jabeuew ays} dd ‘sapuay soljewiaq 510'dap-iudpin®peis epahs v616-269 (Ove) Z8OL-ELL (OVE) YNdG IASN Jefeueyy weibold epeks peks AoB ede@uwelj|im As 996¢-2¢9 (Z1Z) 99/%-7E9 (ZEL) Vda JB01NO VO AS WIM sal4YD UOHOaS POoddns Aob ede®epul jenew Lep-Lze (ZeZ) 99/9-Lze (ZEZ) Vd3 aSe\\ sNoplezey jane epuly (INdy) sebeueyy ubwajddy-uemy AOh ede®esurjoseo'uemy 996¢€-L€9 (ZZ) SLZP-LE9 (ZZ) Vda jOal[Old |eIPSWeY Bul|QseD Aob eda@opueussay opeso. 996€-2€9 (Z1Z) OPEr-LEQ (ZLZ) Vd3 JEIUO Palos opesoy opuewe 4 ssolippy |!ew-g dJaquinn xe JOqUINN euoudajel uoljeziuebiC op sjuaidiseay ddvVO 79 40 J abeY 6002 ‘FL dy 0 JOquUNN UOoIsIAgy AUS punyadns pays yn 3SI7] UOHNG!SIG €# JOSYSHION ddVO uel JOa/Oly BOUBINSSY AEN /eulg INGO 99/2-912 (Ove) j0}e18d0 JOJOeBNUODgNS WYLI uosis}ed Gog 9912-272 (Ove) (14) ueloiuyse | plel4 JoyoesjUoNgNS WYLT JaujuEnd suud 1666-718 (E16) Jebeuey| yOalolg 10}OBIUOOGNS WYL7 aoRen\ Ba19 Z6EV-LLE (ZLZ) Jasulbuz yels WdO eBAeISeAUS yUeAeP 6ZSP-ZLE (ZLZ) JaeuiBuz Nels WdO 9a] ueujyeuor SZSp-Z2¢€ (ZZ) JaaulBug yelod Wad SSIES USI SeSPr-ZZe (ZZ) Jebeuey aS NGO saplialy SoUjEweg pesy ddVO eG aunjeubis Jequiny euoudeajaL ontl jauuosiad yOoloig zg 40 g abeY 6002 ‘PL dy 0 uequinN wolsiney SHS punt * PISBIIEM M0 Ja0US HO-uBis jeuuosiad }Daf014 v# }OYSHIOM ddVO iv :uonezIUuebIO uel joalolg aoueinssy AWeNe, ,-ul4 WKS ‘OQu| ‘YoalWaUD — Uoddns S]OJJUOD pue BuluwwesbolYd B (VSaq) }uewssessy Gal — 1esodsiq (Md)) pue soua!9Ss SISEM PsALep uoneBnsenu| | jejuawiuOsAU ‘oul ‘saiBojouyos | JO UOISIAIG 40 (719) OSL — 40}218d0 Jue] dyISUO # weiGoid Arozesoge} OU] BOLWOwy yOeU02 Vda x js0| — Asoyesoge7 jeojAjeuy # $10}9e1}U09qNS UaeS|O epuljayy ‘aHbeueyy esegejeq ! 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Scheduling the process monitoring sampling through the FASTAC process would require a significant effort because the process sampling is on-going and is performed on a weekly basis. In addition, using a subcontract laboratory allows the plant operator greater flexibility in performing the sampling/O&M activities for the week to account for unexpected plant shutdowns due to equipment failure or other plant alarms including severe weather or power outages that frequently occur in the Virgin Islands. The FASTAC policy will be utilized for samples collected during annual sampling events. Action Items: CDM will submit an Analytical Request Form requesting that the process sampling be performed by the LTRA Subcontractor’s subcontract laboratory. CDM Final Quality Assurance Project Plan UP} Joelolg aoUeUNSSY AUjENo jeuly INO} SUL ‘XKILG JO/PUe SOOAD JO S8OINOS INO} payuap! 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Tutu Wellfield Superfund Site, St. Thomas, US Virgin Islands: Operations and Maintenance Manual, Groundwater Treatment Facilities #1 and #2. June. CDM. 2001. Tutu Wellfield Superfund Site, St. Thomas, US Virgin Islands: Final (100%) Remedial Design for Curriculum Center SVE System. September. . 2002, Tutu Wellfield Superfund Site, St. Thomas, US Virgin Islands: Final Remedial Design for Site-wide Groundwater. July. . 2003. Tutu Wellfield Superfund Site, St. Thomas, US Virgin Islands: Final Data Quality Assurance Project Plan. August. . 2003a. Tutu Wellfield Superfund Site, St. Thomas, US Virgin Islands: Final Contractor Quality Assurance/Quality Control Plan. August. . 2004. Tutu Wellfield Superfund Site, St. Thomas, US Virgin Islands: Final Interim Remedial Action Report. September. . 2004a. Tutu Wellfield Superfund Site, St. Thomas, US Virgin Islands: Year 1 Quarter 1 Remedial Action Progress Report. December. . 2005. Tutu Wellfield Superfund Site, St. Thomas, US Virgin Islands: Year 1 Quarter 2 Remedial Action Progress Report. March. . 2005a. Tutu Wellfield Superfund Site, St. Thomas, US Virgin Islands: Year 1 Quarter 3 Remedial Action Progress Report. August. . 2005b. Tutu Wellfield Superfund Site, St. Thomas, US Virgin Islands: Year 1 Quarter 4 Remedial Action Progress Report. December. . 2006. Tutu Wellfield Superfund Site, St. Thomas, US Virgin Islands: July 2005 Quarterly Remedial Action Progress Report. April. . 2006a. Tutu Wellfield Superfund Site, St. Thomas, US Virgin Islands: October 2005 Quarterly Remedial Action Progress Report. June. . 2006b. Tutu Wellfield Superfund Site, St. Thomas, US Virgin Islands: January 2006 Quarterly Remedial Action Progress Report. July. . 2006c. Tutu Wellfield Superfund Site, St. Thomas, US Virgin Islands: April 2006 Quarterly Remedial Action Progress Report. November. . 2006d. Tutu Wellfield Superfund Site, St. Thomas, US Virgin Islands: July 2006 Quarterly Remedial Action Progress Report. December. . 2007. Tutu Wellfield Superfund Site, St. Thomas, US Virgin Islands: October 2006 Quarterly Remedial Action Progress Report. March. . 2007a. Tutu Wellfield Superfund Site, St. Thomas, US Virgin Islands: January 2007 Quarterly Remedial Action Progress Report. June. cDM | Final Quality Assurance Project Plan Reference List . 2007b. Tutu Wellfield Superfund Site, St. Thomas, US Virgin Islands: April 2007 Quarterly Remedial Action Progress Report. October. . 2008, Tutu Wellfield Superfund Site, St. Thomas, US Virgin Islands: April 2008 Annual Remedial Action Progress Report. October. . 2008a. Tutu Wellfield Superfund Site, St. Thomas, US Virgin Islands: Long Term Response Action Subcontract Procurement. November. Environmental Protection Agency (EPA). 1989. Region II Final CERCLA Quality Assurance Manual. .1996, Record of Decision (ROD), Tutu Wellfield Superfund Site, August 5, 1996. .1998. Final EPA Region II] Groundwater Sampling Procedure Low Stress (Low Flow) Purging and Sampling. March 16, ‘ EPA. Drinking Water Contaminants. http://www.epa.gov/safewater/contaminants/index.htmlftorganic. Accessed August 2007. Geraghty and Miller (G&M). 1995. Tutu Wellfield Superfund Site, St. Thomas, US Virgin Islands: Draft Final Feasibility Study. August 1995. . 1995a, Tutu Wellfield Superfund Site, St. Thomas, US Virgin Islands: Draft Phase Il Remedial Investigation. January 1995. CDM i Final Quality Assurance Project Plan _ Tables Table 1 Monitoring Well Construction Tutu Wellfield Site, St. Thomas, U.S. Virgin Islands X Y GS Toc TOS BOS TOS BOS AREA NAME (FT AMSL) (FT AMSL) |(FT AMSL)} (FT AMSL) (FT BGS) |(FT BGS) (FT) (FT) BP-1 1036261 187500 202.67 202.67 162.67 143,87 40 58.8 1036260 187490 202.64 202.64 162.64 142.34 40 60.3 Curriculum BP-2 Center/ BP-3 1036259 187481 202.71 202.71 162.71 143.03 40 59.68 Facility #1 IW-1 4036258 187503 202.79 202,79 127.79 107.69 75 95.1 IW-1S 1036251 187508 202.85 202.85 162.85 146.23 40 56.62 IW- 1036266 487505 202,94 202.94 427.94 412.17 75 90.77 IW-2S 1036266 187510 203.77 203.77 163.77 143.22 40 60.55 MW-13 1036477 187456 237.00 236.31 176.01 155.81 60.3 80.5 MW-13D 4036482 487472 236.67 236.60 136.67 116.67 100.0 120,0 4036105 187330 198.04 196.12 170.84 150.84 25.2 45.2 MW-14 MW-15 41035990 187260 178.95 178.95 163.95 142.75 15.0 36.2 MW-16 1036252 187463 203.00 202,33 177.73 157.73 24.6 44.6 13.5 MW-17 1035930 187249 177.18 177.18 168.68 163.68 8.5 MW-10 1036193 187187 195.14 195.14 125.14 105,14 70.0 99.0 RD-10 4036152 487558 196.48 199.18 116.48 91.48 80.0 105.0 RD-14 1036241 187503 202.45 202.46 117.45 92.45 85.0 110.0 RD-12 1036479 187450 235.46 236.71 405.46 80.46 130.0 155.0 RD-13 1036233 187163 195.62 196.44 95.62 70.62 100.0 125.0 RD-9 1036280 187458 203.79 204.41 118.79 93.79 85.0 110.0 RW-6 4036230 187477 202.17 201.04 122.17 72.17 80.00 130,00 RW-7 1036262 187464 203.114 202.56 173.11 123.14 30.00 80.00 RW-8 1036257 187467 202.75 202.75 152.75 97.52 50 105.23 RW-9 1036255 187460 202.27 202.27 162.77 141.97 39.5 60.3 MW-2 1035828 187162 178.31 178.15 171.34 151,31 7,0 Texaco = 27.0 MW-3 1036085 487129 181.85 181.84 AT1AS ~ 151.45 _ 10.4 30.4 MW-4 4035938 487050 175,69 175.66 168.69 148.69 7.0 27.0 _ 128.29 104.99 47.7 71.0 aa MW-4D 1035944 187045 | 175.99 176.02 Fo barf see Te a Ed MW-5 41035972 | 18691 oO} 187.24 487.09 168.24 148.24 49.0 39.0 MW-6D 1035799] 1 86786 171.26 | 171.01 126,26 106.26 _ 45.0 65.0 PS att Son | MW-6R 1035804 | 186802 471.44 ciel FEES ee dt | 474. ‘i 168.74 148.74 27 22.7 MW-7 1035989| 186667 tnt ns el IE 180,30 180.13, 164. 90 144.90 _ 15.4 35.4 RD-5. 1036163 | 186948 | 494,00 | 156.94 146.91 es | a 189.91 a = 33.0 43.0 _ Tillett, Biri Sat a9! PRK A 1035975 186771 | 186.00 paraes __ 186,00 et me | 477. 00_ 88.00 9.00 ~ 98. 00 | TT-1 1036009} 1 87002 |_ 179.00 179.03 169.03 —=— 149,03 10.0 30.0 | 130.50 43.0 __ 53,0 TT-3D 1036076 | 187137 183.50 181.75 140.50 TT-5 41036106 | 187027 482. 50 ~ 182. 34 are) (ESE lt ee 172.50 152.50 10.0 30.0 = TT-6 1035804 | 186672 169.00 169.18 165.50 155,50 3.5 43.5 Esso CHT-1 4035815 ee: 186506. 167.95 167.70 149.45 * 139.45 18.5 28.5 CHT-3 1035795 186321 162.87 161.86 139.87 129.87 23.0 33.0 CHT-4 _ 1035766 186515 166,00 — 166.95 147.95 137.95 19.0 29.0 CHT-7D 4035740) 186233 “159. 00 _ 158.29 138.29 34.29 20.0 124, Oo DW-1 1035805 | 186496 “487. 52 ~ 167. 16 —~—— —_ 102,52 87.52 65.0 80.0 MW-10 1035794 186280 161.36 ~ 164.50 145.76 | 125.76 15.6 35,6 MW-40D 1035799 486278 7 _ 161.52 161.38 406.42 — ~ 86. 42 55.1 — 75.1 MW-2 25 1035632 186489 ~ 168.34 166.34 141.34 421.34 25.0 45.0 —— 5.5 25.5 MW-8 1035812 186494 167.54 167.54 ce ae 162,04 442.04 MW-9 vb Mh 1035694 186368 bs 162.32 162.26 "448.22 - 428.22 nz Aare Pa he 14.1 34.1 MW-9S 1035700. 186377 162.47 162.37 453.77 143.77 8.7 18.7 PW-1 Ebi aS 1035787 186345 167.31 166,00 155.314 129,00 12.00 ee 38.31. sw-10 1035721 486286 160.65 = 160.42 150.65 120,65 10.0 a 40.0 SW-1R 186345 166.69 166.47 154.69 129.47 12.00 37.22 R__| 1035815 | petal fa 3 FE od tote SW-2R 1035782 186371 aes 167.95 167.70 153,95 128,70 14.00 | 39.25 SW-8R | 1035758 186344 167.34 4 467,11 155.34 130.14 42.00 __ 37.23 160.46 150.46 120.46 10.0 40.0 SW-9 | 4035797 “186262 160.46 Table 1 Monitoring Well Construction Tutu Wellfield Site, St. Thomas, U.S. Virgin Islands AREA NAME xX ¥ Gs TOC TOS BOS TOS BOS (FT) (FT) | (FT AMSL) | (FTAMSL) |(FT AMSL)} (FT AMSL) | (FT BGS) |(FT BGS) Facility #2 |DW-2 1035682] 185937 148.00 147.73 82.73 67.73 65.0 80.0 Eglin-1 1035604} 185826 144.00 146.65 - - - - Eglin-3 1035678| 185692 152,00 155.17 95.50 -150.00 56.50 302.00 MW-11D | 1035532] 186025 153.441 153.22 100.11 78.81 53.0 74.3 MW-12D | 1035791] 186063 161.58 161.84 101.08 81,08 60.5 80.5 MW-19 1035617 | 186036 148.78 148.78 436.78 131.78 42.0 17.0 RD-4 1036003} 185650 211.74 212.28 -31.26 -51.26 243.0 263.0 RD-7 1035769} 185996 164.36 164.00 - 94.36 84.35 70.0 80.0 RW-1 1035799] 186102 160.60 160.61 10.60 -39.40 450.00 200.00 RW-1S 1035799} 186091 161.14 161.11 105.11 41.11 56 420 SW-4 41035573] 186137 152.00 152.96 147.96 117.98 5.0 35.0 SW-6 1035680} 185936 148.00 147.60 142.60 112.60 5.0 35.0 Southern |Delegard | 1036722] 183972 741.00 70,00 41.00 1.00 30.00 70,00 Plume Laplace 1035995] 185154 414.00 114.23 94.00 34.00 20.00 80.00 MW-21D | 1035965] 185348 123.48 123.48: 47.48 27.48 76.0 96.0 PZ-4 1037142] 183823 69.11 61.34 51,61 41.61 7.5 17.5: RD-1 1035773] 184965 135.95 436.11 40.95 30.95 95.0 4105.0 RD-14 41036181] 184610 86.67 89.21 6.67 -43,33 80.0 130.0 RD-2 1037256} 183680 55.93 57.56 -2.07 -12,07 58.0 68,0 RD-3 4037247] 183682 56,05 57.95 36.05 26.05 20.0 30.0 RD-6 1036264] 184528 82.69 85.08 52.69 27.69 30.00 55.00 RD-8 1035367 | 185440 141,70 142,46 81.70 71.70 60.0 70.0 Smith 1036154] 184697 30.00 90,00 85,00 30.00 5.00 60.00 Steele 4035647} 185420 177.00 179.33 452.00 62.00 25.00 115.00 Notes: 4. Horizontal coordinates are based on Puerto Rico Coordinate Virgin Island Extension State Plane North American Datum 4927, Vertical elevations are based on the National Geodetic Vertical Datum 1929. Acronyms: AMSL - above mean sea level BGS - below ground surface BOS - bottom of screen Esso - Esso Standard Oil, U.S.A., Inc. FT - feet GS - ground surface GW - groundwater Texaco - Texaco Caribbean, Inc. TOC - top of casing TOS - top of screen Page 20f2 Sampling and Monitoring Schedule Tutu Wellfield Site, St Thomas, U.S, Virgin Islands Table 2 GW Monitoring Sampling Frequency Monitoring or Mesurement Frequency GW Samples Parameters AirSamples} Field Measurements 5 ¢ 3 ¥ 3 3 é ZI 5 ae 3 =| ez |é =| 3 |] 8 e|5 g|e|2 » |alsls z = = 2 < ir = <s a 2 = S| 2) 2) 2 3/8) § +h ay a* mt Si2)/e)])2f)2le2)38)]2)2 13 2 18)o0 e|e|6]s5 Flel ele ¢ S| 8] e| 2 g] 8 o 6 E e| = a 3 fe s § als| Sl els o|6 S| soe fe} ©} 2\ a] o| =z] 3 System or Wells Sampling and/or Monitoring Activity Location =| 5s & 3 €\64 2 Ss 2 3 S ee Gifielo E Sle} elcl}] ol S$ oS Notes Extraction well RW-6 sampling and monitoring RW influent sample port . ° : es OS Ee) . Extraction well RW-7 sampling and monitoring RW influent sample port . , . all (Bi Pek 3 Extraction well RW-9 sampling and monitoring RW influent sample port ° e bd o}. tu, Ss e GW influent (combined) sampling and monitoring EQ tank effluent sample port . . 5 bot ER Pak Bis . GWT system monitoring and field measurements Gauges, meters, instruments . ak eh A a I GWTF #1 GWT system monitoring and field measurements Meters ° ed By Treated water effluent-TPDES permit sampling and monitoring (monthly) Air stripper effluent sample port . d ss Treated water effluent-TPDES permit sampling and monitoring (weekly) Air stripper effluent sample port . . . ele 1 Off-gas treatment system, air permit sampling Stack sample ports i = 2 Extraction well RW-1 sampling and monitoring RW influent sample port . ° s call Ne OR BS : Extraction well RW-1S sampling and monitoring RW influent sample port . bd - bg heal PS = GW influent (combined) sampling and monitoring EQ tank effluent sample port . * . ih a 2 : ' GWT system monitoring and field measurements Gauges, meters, instruments . oo BS Bel EU WO GWTF #2 GWT system monitoring and field measurements Meters ? a Treated water effluent-TPDES permit sampling and monitoring (monthly) Air stripper effluent sample port . a i Treated water effluent-TPDES permit sampling and monitoring (weekly) Air stripper effluent sample port . . J aie Bs - ar Site-wide GW, annual sampling For list of wells, see Table 01730-3 ° * i “g CE SS ah ead al ee 3 GW Monitoring = = = ~ a Wells Site-wide GW, continuous water levels For list of wells, see Table 01730-3 = Site-wide GW, monthly water levels For list of wells, see Table 01730-3 ‘ 2 Notes: 1. Per U.S. Virgin Islands DPNR TPDES Permit Equivalency No VID982272569, effective March 1, 2004 2. Per DPNR Air Pollution Control Permit Conditions, dated July 22, 2003 3, Sampling for TOC, nitrate, sulfate, chloride, and ethane/ethene applies to Southern ae wells only. See Table 01730-3. Acronyms: DO - dissolved oxygen DPNR - Department of Planning and Natural Resources EQ - equalization GW - groundwater GWT - groundwater treatment GWTE - groundwater treatment facility ORP - oxidation reduction potential PID - photo-ionization detector RW - recovery well TOC - Total Organic Carbon TPDES - Territorial Pollutant Discharge Elimination System TSS - total suspended solids VOC - volatile organic compound Page lofi Table 3 Site-wide Groundwater Monitoring Schedule Tutu Wellfield Site St. Thomas, U.S. Virgin Islands AREA WELL | LOCATION SAMPLING *° WATER LEVEL MEASUREMENT Annual Notes Continuous Monthly Notes Curriculum Center/ GWTF #1 BP-14 BP-2 BP-3 IW-1 IW-1S IW-2 IW-2S MW-17 MW-1D MW-13 MW-13D MW-14 MW-15 MW-16 RW-8 RD-9 RD-10 RD-11 x? RD-12 RD-13 > | >< | KK LK OK LK OK | DK | OK | OK | OK | OK | OS | OK | DK | OK | OK | OK | OK Texaco MW-2 MW-3 x? x MW-4 MW-4D MW-5 MW-6R MW-6D MW-7 ~< RD-5 TT-1 TT-3D TT-5 TT-6 Tillett Esso CHT-14 CHT-3 CHT-4 CHT-7D DW-1 MW-8 MW-9 MW-9S MW-10 MW-10D MW-25 P-4 SW-1R SW-2R SW-8R SW-9 SW-10 Site-wide Groundwater Monitoring Schedule Tutu Wellfield Site Table 3 St. Thomas, U.S. Virgin Islands AREA WELL SAMPLING ** WATER LEVEL MEASUREMENT LOCATION Annual Notes Continuous] Monthly Notes GWTF #2 DW-2 x x? X MW-11D x xX MW-12D x xX MW-13 x RD-4 x F | RD-7 Xx xX SW-6 x Eglin | Xx Eglin III x 6 Southern Delegard X 4,6 Plume Laplace Xx 4.6 MW-21D x x! Xx PZ4 Xx Le, RD-1 x YS . X ‘ RD-2 Xx xX RD-3 xX 4 xX RD-6 Xx Xx RD-8 Xx x RD-14 x? x Smith X 48 ~1Steele X 46 1. Notused 2. Notused 3. Sampling includes VOCs, unless othenwise noted. 4. Sampling includes VOCs, TOC, nitrate, sulfate, chloride, and éthane/ethene (intrinsic biodegradation parameters). 5. Field measurements shall be taken for water level, turbidity, DO, temperature, conductivity, pH, and ORP at all wells during sampling. 6. Active supply well. 7. Continuous water levels will be collected by transducers. Acronyms: DO - dissolved oxygen GWTF - groundwater treatment facility O&M - operations and maintenance ORP - oxidation reduction potential RA - remedial action TOC - total organic carbon VOC - volatile organic compound go ,O'HENRY ec gic te =, a oe ee (a a — I 4 + L3@ Osw2r) OWA) : e@rir-4 pase s] red = = eo asd @gyean MEADE = 1s 5, MWR CHT-4 bt & iy ie AS W137 BPD os _f—~ 100 ven? ~y A1889 >) semith S00ugn gps = 727) == 1000 ue FACILITY # \y \ ala yf f FACILITY #4..~ “or : (CURRICULUM Ss CENTER) > ee Ee eee . 4383 \ \ Legend 428.57 Posted Groundwater Elevation < Flow Direction Arrow Fj 2 , (feet above mean sea level) : igure Groandwater Monitoring Well Notes: 1. Groundwater samples were collected in April 2008. : . ; : Total CVOC Concentrations (ug/L) PR Ba a aie a idee 2. Groundwater elevations were recorded in Api 208, Site-Wide Groundwater Elevations and CVOC Concentrations 2 ee {reat mineo Nee Here poh aedolnrett pry ae et re Quality Assurance Project Plan © 10-99.99 elevation iso-contours. . 7 @ 100-499.99 April 2008 Groundwater Total CVOC Concentration Tutu Wellfield Site, St Thomas, USVI Iso-contours (ug/L) @ 500 -999,99 @ 1,000 - 1,060 Baseline (April 2004) Groundwater Total CVOC 0 75 150 ang ‘ CDM i ey @® Not Sampled Concentration Iso-contours (ug/L) ee SVE TREATMENT SYSTEM Ss. OFFLINE S / 7 P< —sg B<- SVE-1 |SVE—7 Sve—iNF SODIUM HYPOCHLORITE MURIATIC SEE NOTE 3 ee CURRENT OFFGAS SYSTEM CONFIGURATION DISCHARGE Y | TO STACK ANTI-SCALANT Si EQUALIZATION TANK Ht GAC #1 PP #1 CURRENTLY BYPASSED pala OFFLINE/ SVE-1 SVE-7 STANDBY SVE WELLS BAG FILTERS LJ AIR STRIPPER se X f “NS “NS “™ GW1-INF VAP—EFF RW-7 RW-9 RW-6 NOTES: 1. THE USE OF RW—9 ONLY OCCURS INTERMITTENTLY WHEN INCREASED FLOW RATE IS NEEDED TO HYDRAULICALLY CONTROL THE CONTAMINATION PLUME. 2. RW—6 OPERATES MANUALLY FOR APPROXIMATELY ONE HOUR PER WEEK, UNTIL THE WELL REACHES A LOW WATER CONDITION. RW-7 RW-9 RW-6 GW1—EFF SEE NOTE 1 SEE GW EXTRACTION WELLS NOTE 2 OUTFALL 001 3. SODIUM HYPOCHLORITE NOT CURRENTLY IN USE, 4. THE SVE AND OFFGAS SYSTEMS ARE CURRENTLY OFFLINE LEGEND AVG — AVERAGE GAC — GRANULAR ACTIVATED CARBON UNIT GPD — GALLONS PER DAY GW — GROUNDWATER MAX — MAXIMUM PP — POTASSIUM PERMANGANATE UNIT RW — RECOVERY WELL Figure 3 Groundwater Treatment Facility #1 Schematic and Sample Locations Quality Assurance Project Plan Tutu Wellfield Site, St. Thomas, USVI SODIUM HYPOCHLORITE DISCHARGE SEE NOTE 2 MURIATIC TO STACK ACID VY ANTI-—SCALANT /\ EQUALIZATION TANK VY CURRENTLY BYPASSED BAG FILTERS AIR STRIPPER Dd Lt RW-1 RW—-1S GW2-INF “™ “|S NOTES: RW—-1 RW-1S GW2—EFF 1 RW-1 IS CURRENTLY NOT IN USE AND SEE NOTE 1 IS NOT LIKELY TO BE USED IN THE OUTFALL FUTURE. GW EXTRACTION WELLS 002 2. SODIUM HYPOCHLORITE NOT CURRENTLY IN USE. LEGEND GPD — GALLONS PER DAY GW — GROUNDWATER RW — RECOVERY WELL Figure 4 Groundwater Treatment Facility #2 Schematic and Sample Locations Quality Assurance Project Plan Tutu Wellfield Site, St. Thomas, USVI CDM Figures CYRIL E. KING AIRPORT 0.75 NILES 0 1.5 MILES Se ee | SCALE IN MILES FACILITY #1 FACILITY #2 fooo" 0 2000" Fee oe | SCALE IN FEET S \ TUTU WELLFIELD SITE ST. THOMAS, USVI CHARLOTTE AMALIE GREAT ST, JAMES ISLAND Figure 1 . Site Location Quality Assurance Project Plan Tutu Wellfield Site, St. Thomas, USVI CDM Appendix A Site-Specific Low Flow Groundwater Purging and Sampling Il. EPA Region II Groundwater Sampling SOP For Tutu Wellfield Site November 7, 2008 U.S. ENVIRONMENTAL PROTECTION AGENCY REGION II GROUNDWATER SAMPLING PROCEDURE LOW STRESS (LOW-FLOW) PURGING AND SAMPLING SCOPE & APPLICATION This Low Stress (or Low-Flow) Purging and Sampling Procedure is the EPA Region II preferred method for collecting groundwater samples from monitoring wells at the Tutu Wellfield Site. The procedure minimizes stress on the formation and minimizes disturbance of sediment in the well. The procedure applies to monitoring wells that have well casing with an inner diameter of 2,0 inch or greater. It is appropriate for groundwater samples that will be analyzed for volatile and semi-volatile organic compounds (VOC and SVOC), pesticides, polychlorinated biphenyls (PCB), metals, wet chemistry parameters, and microbiological and other contaminants in association with any EPA program. This procedure does not address the collection of non-aqueous phase liquid (NAPL) samples and should be used for aqueous samples only. For sampling NAPLs, the reader is referred to the following EPA publications: DNAPL Site Evaluation (Cohen & Mercer, 1993) and the RCRA Ground-Water Monitoring: Draft Technical Guidance (EPA/530-R-93-001), and references therein. METHOD SUMMARY The goal of the Low Stress Purging and Sampling procedure is to collect samples that are representative of groundwater conditions in the geological formation. This is accomplished by setting the intake velocity of the sampling pump to a flow rate that allows a maximum drawdown of 0.3 foot. Sampling at such a low flow rate has three primary benefits. First, it minimizes disturbance of sediment in the bottom of the well, thereby producing a sample with low turbidity (i.e., low concentration of suspended particles). Typically, this saves time and analytical costs by eliminating the need for collecting and analyzing a filtered sample from the same well. Second, it minimizes aeration of the groundwater during sample collection, which improves the sample quality for VOC analysis. Third, in most cases it significantly reduces the volume of Ii. EPA Region II | Groundwater Sampling SOP For Tutu Wellfield Site November 7, 2008 groundwater purged from a well and the costs associated with its proper treatment and disposal. ADDRESSING POTENTIAL PROBLEMS Problems that may be encountered using this technique include a) difficulty in sampling wells with insufficient yield; b) failure of a key indicator parameter to stabilize; c) cascading of water and formation of air bubbles in the tubing; and d) cross-contamination. For wells with insufficient yield (i.e., low recharge rate of the well), care should | be taken to avoid loss of pressure in the tubing line, cascading through the sand pack, or pumping the well dry. Purging should be interrupted before the water level in the well drops below the top of the pump. Sampling should commence as soon as the volume in the well has recovered sufficiently to allow collection of samples. Alternatively, ground water samples may be obtained with techniques designed for the unsaturated zone, such as lysimeters. If a key indicator parameter fails to stabilize after 4 hours, one of two options should be considered; a) continue purging in an attempt to achieve stabilization; or b) discontinue purging, collect samples, and document attempts to reach | stabilization in the log book. The key indicator parameter for samples to be | analyzed for VOCs is dissolved oxygen. The key indicator parameter for all other samples is turbidity. For cascading and air bubbles in the tubing, care should be taken to ensure that the flow rate is sufficient to maintain pump suction. Minimize the length and diameter of tubing (i.e., 1/4 inch ID) to ensure that the tubing remains filled with liquid during sampling. An item that should be checked on a daily basis, is the water within the cooling chamber of the submersible pump. This chamber should always be filled with demonstrated analyte-free water and any leakage from this chamber should be immediately brought to the attention of the person(s) responsible for equipment maintenance so that the appropriate seals can be replaced. Operating the pump with insufficient water in this cooling chamber could result in the pump overheating and/or pump failure. The analyte-free water should be replaced on a daily basis in order to facilitate the mechanical operation of the pump. IV. EPA Region II Groundwater Sampling SOP For Tutu Wellfield Site November 7, 2008 EQUIPMENT O Approved site-specific Quality Assurance Project Plan (QAPP). O ei) Ce i) IE) oe eds feet Ta Ea ed Generally, the target depth corresponds to just above the mid-point of the most permeable zone in the screened interval. Borehole geologic and geophysical logs can be used to help select the most permeable zone. However, in some cases, other criteria may be used to select the target depth for the pump intake. Well construction data, location map, field data from last sampling event. Polyethylene sheeting. Photo Ionization Detector (PID), if required by health and safety plan. Adjustable rate, positive displacement groundwater sampling pump constructed of stainless steel. Interface probe or equivalent device for determining the presence or absence of NAPL. Teflon-lined polyethylene tubing to collect samples for organic and inorganic analysis. Sufficient tubing of the appropriate material must be available so that each well has dedicated tubing. Electronic water level measuring device, 0.01 foot accuracy. Flow measurement supplies (e.g., graduated cylinder and stop watch). Power source (generator). Monitoring instruments for indicator parameters. Redox potential (Eh) and dissolved oxygen must be monitored in-line using an instrument with a continuous readout display. Temperature, pH and specific conductance may be monitored with an in-line monitor. A nephalometer is used to measure turbidity. Decontamination supplies (see Section VII, below). Logs/ Logbook (see Section VIII, below). Sample bottles. Sample preservation supplies (as required by the analytical methods). Sample tags or labels, chain of custody. Other supplies as specified in the EPA approved field sampling plan/QAPP. SAMPLING PROCEDURES Pre-Sampling Activities I: Start at the well known or believed to have the least contaminated groundwater and proceed systematically to the well with the most EPA Region II Groundwater Sampling SOP For Tutu Wellfield Site November 7, 2008 contaminated groundwater. Check well for damage or evidence of tampering. Record observations, Lay out sheet of polyethylene for monitoring and sampling equipment. Measure VOCs at the rim of the unopened well with a PID or FID instrument and record the reading in the field log book. Remove well cap. Measure VOCs at the rim of the well with a PID or FID instrument and record the reading in the field log book. If the well casing does not have a reference point (usually a V-cut or indelible mark in the well casing), make one. Measure and record the depth to water (to 0.01 ft) in all wells to be sampled before any purging begins. Care should be taken to minimize disturbance in the water column and dislodging of any particulate matter attached to the sides or settled at the bottom of the well. If desired, measure and record the depth of any NAPLs using an interface probe. Care should be taken to minimize disturbance of any sediment which has accumulated at the bottom of the well. Record the observations in the log book. Sampling Procedures 9; 10. Install Pump: Slowly lower the pump, safety cable, tubing and electrical lines into the well to a depth midway within the screen interval for that well. The pump intake must be kept at least two feet above the bottom of the well to prevent disturbance and resuspension of any sediment or DNAPL present in the bottom of the well. Record the depth to which the pump is lowered. Measure Water Level: Before starting the pump, measure the water level again with the pump in the well. Leave the water level measuring device in the well. TL; 12, EPA Region II Groundwater Sampling SOP For Tutu Wellfield Site November 7, 2008 Purge Well: Start pumping the well with a rate that varies from 200 to 500 milliliters per minute (ml/min). The water level should be monitored approximately every three to five minutes. Ideally, a steady flow rate should be maintained that results in a stabilized water level (drawdown of 0.3 ft or less). Pumping rates should, if needed, be reduced to the minimum capabilities of the pump to ensure stabilization of the water level. As noted above, care should be taken to maintain pump suction and to avoid entrainment of air in the tubing. Record each adjustment made to the pumping rate and the water level measured immediately after each adjustment. Monitor Indicator Parameters: During purging of the well, monitor and record the field indicator parameters (turbidity, temperature, specific conductance, pH, Eh, and DO) approximately every three to five minutes. The well is considered stabilized and ready for sample collection when the indicator parameters have stabilized for three consecutive readings as follows (Puls and Barcelona, 1996): +0.1 for pH +3% for specific conductance (conductivity) +10 mv for redox potential +10% for DO and turbidity Dissolved oxygen and turbidity usually require the longest time to achieve stabilization. The pump must not be removed from the well between purging and sampling. If pH adjustment is necessary for sample preservation, the amount of acid to be added to each sample vial prior to sampling should be determined, drop by drop, ona separate and equal volume of water (e.g., 40 mls). Groundwater purged from the well prior to sampling can be used for this purpose. Collect Samples: Collect samples at flow rates of between 100 and 250 ml/min or such that drawdown of the water level within the well does not exceed the maximum allowable drawdown of 0.3 ft. Samples should be collected at the same flow rate at which the indicator parameters stabilized. VOC samples must be collected first, at the lower rate, and directly into pre-preserved sample containers. All sample containers should be filled with minimal turbulence by allowing the groundwater to flow from the tubing gently down the inside of the container, EPA Region I] Groundwater Sampling SOP For Tutu Wellfield Site November 7, 2008 14, | Remove Pump and Tubing: After collection of the samples, the tubing, unless permanently installed, must be properly discarded or dedicated to the well for re-sampling by hanging the tubing inside the well. 1B: Measure and record well depth. 16. Close and lock the well. FIELD QUALITY CONTROL SAMPLES Quality control samples must be collected to determine if sample collection and handling procedures have adversely affected the quality of the ground water samples. The appropriate EPA Program Guidance was consulted when preparing the field QC sample requirements of the site-specific QAPP. All field quality control samples must be prepared exactly as regular investigation samples with regard to sample volume, containers, and preservation. The following quality control samples will be collected for each batch of samples (a batch may not exceed 20 samples). Trip blanks are required for the VOC and ethane/ethene samples at frequency of one per sample cooler containing VOCs and/or ethane/ ethene. im) Field duplicate. Oo Trip blank (VOCs and ethane/ ethene only) In addition, an equipment blank will be collected at a rate of once per day or per decontamination event, whichever is less. However, this is not necessary if equipment is dedicated to the well. Groundwater samples should be collected systematically beginning at wells known or believed to have the lowest level of contamination and proceeding in order to wells known or believed to have the highest level of contamination. VIL. EPA Region II Groundwater Sampling SOP For Tutu Wellfield Site November 7, 2008 DECONTAMINATION Sampling equipment must be decontaminated thoroughly each day before use (daily decon) and after each well is sampled (between-well decon). As noted above, wells should be sampled in order from the least contaminated to the most contaminated. Pumps should not be removed from the well between purging and sampling operations. All non-disposable equipment, including the pump (support cable and electrical wires which are in contact with the sample) will be decontaminated as described below, 17. Prior to Sampling Event Decon Please Note: Steps D through K should only be performed once (for each pump that is to be used) before the commencement of a particular sampling event by a person qualified to disassemble pumps. A) Pre-rinse: Operate pump ina deep basin containing 8 to 10 gallons of potable water for 5 minutes and thoroughly flush other equipment with potable water. B) Wash: Operate pump in a deep basin containing 8 to 10 gallons of a non-phosphate detergent solution, such as Alconox, for 5 minutes and thoroughly flush other equipment with fresh detergent solution. Use the detergent sparingly. C) Rinse: Operate pump in a deep basin of potable water for 5 minutes and thoroughly flush other equipment with potable water for five minutes. D) Disassemble pump. E) Wash pump parts (inlet screen, shaft suction interconnector, motor lead assembly, stator house): Place the disassembled parts of the pump into a deep basin containing 8 to 10 gallons of non-phosphate detergent solution. Scrub all pump parts with a test tube brush. F) Rinse pump parts with potable water for five minutes. G) Rinse the pump parts with demonstrated analy te-free water. 18. EPA Region II Groundwater Sampling SOP For Tutu Wellfield Site November 7, 2008 H) Place impeller assembly in a large glass beaker and rinse with 1% nitric acid (HNOs). 1) Rinse impeller assembly with potable water for five minutes. J) Place impeller assembly in a large glass bleaker and rinse with isopropanol. K) Thoroughly rinse impeller assembly with demonstrated analyte-free water. Daily and Between-Well Decon A) Pre-rinse: Operate pump in a deep basin containing 8 to 10 gallons of potable water for 5 minutes and thoroughly flush other equipment with potable water for five minutes. B) Wash: Operate pump ina deep basin containing 8 to 10 gallons of a non-phosphate detergent solution, such as Alconox, for 5 minutes and thoroughly flush other equipment with fresh detergent solution. Use the detergent sparingly. C) Rinse: Operate pump in a deep basin of potable water for 5 minutes and thoroughly flush other equipment with potable water for five minutes. D) Final Rinse: Operate pump in a deep basin of analyte-free water to pump out 1 to 2 gallons of this final rinse water. VI. FIELD LOGS/LOGBOOK A field log book or field logs must be kept each time ground water monitoring activities are conducted in the field. The field log book or log should document the following: O 0 0 Oo Well identification number and physical condition. Static water level depth, date, time, and measurement technique. Pumping rate, drawdown, indicator parameters values, and clock time, at three to five minute intervals; calculate or measure total volume pumped. Well sampling sequence and time of sample collection. Types of sample bottles used and sample identification numbers. EPA Region II Groundwater Sampling SOP For Tutu Wellfield Site November 7, 2008 Preservatives used, Parameters requested for analysis. Field observations of sampling event. Weather conditions. QA/QC data for field instruments. ENG Ee) & IX. REFERENCES Cohen, R.M. and J.W. Mercer, 1993, DNAPL Site Evaluation, C.K. Smoley Press, Boca Raton, Florida. EPA, 1993, RCRA Ground-Water Monitoring: Draft Technical Guidance, EPA/530-R- 93-001. EPA, 1998, EPA Region II, Ground Water Sampling Procedure Low Stress (Low Flow) Purging and Sampling, March 16. Puls, R.W. and M,J. Barcelona, 1996, Low-Flow (Minimal Drawdown) Ground-water Sampling Procedures, EPA/540/S-95/504. Appendix B CDM Technical Standard Operating Procedures -2 Sample Custody* -6 Water Level Measurement -8 Vapor Sampling using a SUMMA Cannister -10 Field Measurement of Organic Vapors -1 Packaging and Shipping of Environmental Samples* -2 Guide to Handling of Investigation Derived Waste -1 Control of Measurement and Test Equipment POD — a= a a * Includes RAC II Contract-Specific Clarification CONTRACT-SPEGIFIC CLARIFICATION SOP No.: 1-2 Revision: 4 SOP Title: SAMPLE CUSTODY Date: October 10, 2004 QA Review: Milo ff A Approved and et ain lI | ! [ oO Prograta Manager Signature/ Date t Contract No.: RAC II Client: EPA Region I Reason for Clarification: _Make SOP EPA Region If - Specific Add Forms II Lite Procedures; Sample tags requirement not applicable. 1.0 OBJECTIVE, add (to page 1 of 7): For the RAC II contract, the sample custody paperwork will also be supplied to the U.S. Environmental Protection Agency (EPA) Region II Regional Sample Contract Laboratory Program (CLP) Coordinator and the Contract Laboratory Analytical Service Support (CLASS) contact. This will include the combination forms generated using the EPA Field Operations Records Management System II Lite (FORMS II Lite™) software and the hand written combination traffic reports & chain of custody records (TR/COCs). All samples sent through the CLP system are required to be recorded on the FORMS II Lite™ generated combination TR/COC records. Use of hand written TR/COCs must be approved by EPA Regional Sample Control Center (RSCC) prior to use. 4.0 REQUIRED SUPPLIES, add (to page 2 of 7): If using the FORMS II Lite™ software the following additional equipment will be required: e FORMS II Lite™ Software e Computer e Printer 5.0 PROCEDURES 5.1 Chain-of-Custody Field Custody, on page 2 of 7 under item 2, replace: “Complete sample label or tags for each sample, using waterproof ink.”, with, “Complete sample labels for each sample using indelible ink or pre-printed labels.” Add, before 5.2 Sample Labels and Tags (on page 5 of 7): CDM FEDERAL PROGRAMS CORPORATION Technical Standard Operating Procedures TSOP-1-2.RAC Page | of 3 CONTRACT-SPECIFIG CLARIFICATION SOP No.; 1-2 Revision: 4 SOP Title: SAMPLE CUSTODY Date: October 10, 2004 Procedure for Generating EPA’s FORMS II Lite™ Combination Forms FORMS II Lite™ is used to automate printing of sample documentation in the field and facilitate electronic capture of data prior to and during field sampling activities. FORMS II Lite™ can be populated with the general site information, laboratory information, CLP case number, sample locations, CLP sample numbers, analysis, preservatives, etc. prior to the sampling event. Sample labels can then be generated from FORMS II Lite™. The following is a list of items required to be entered into FORMS II Lite™: Site spill number Region number, sampling entity, sampler name and signature Type of activity Date shipped, courier and air bill number Analytical laboratory name, address and contact Case number CLP sample number Sample description (media type) Sample concentration (low, medium, high) Sample type (composite, grab) Preservative used Turn-around time (for organic analysis only) Routine Analytical Services (RAS) fraction(s) Date and time of sample collection Sampler’s initials Corresponding CLP inorganic CLP sample number, if applicable Field QC sample information (information regarding trip or field blanks but not reference to duplicate samples) Whether shipment for case is complete Sample designated for matrix spike laboratory QC purposes The procedures for generating the FORMS II Lite™ combination forms are similar to preparing the CLP RAS combination forms detailed in the next section. The difference is the information will be entered into the FORMS II Lite™ software and the combination forms will be printed out on site instead of filling in the combination forms in by hand. Detailed procedures for using the FORMS II Lite™ software are provided in the FORMS II Lite™ User's Guide supplied with the software. After completing the day’s sampling, the date, time and field QC sample information are entered into the FORMS II Lite™ software. Samples are assigned to the traffic reports, shipping information is entered and CDM FEDERAL PROGRAMS CORPORATION Technical Standard Operating Procedures TSOP-1-2.RAC CONTRACT-SPEGIFIC CLARIFICATION SOP No.: 1-2 Revision: 4 SOP Title: SAMPLE CUSTODY Date: October 10, 2004 the traffic reports are printed, The software generates a Region and a Laboratory copy of the TR/COC record, The Laboratory copies of the TR/COC records are signed and placed in a zip-lock bag taped to the inside cooler lid and shipped with the samples to the laboratory. The Region copies of the TR/COC records are submitted to the RSCC and to CLASS along with the sampling trip report. Examples of TR/COC records that FORMS II Lite™ generates for the Laboratory copies (Figures C1 and C2) and the Region copies (Figures C3 and C4) are attached to this Contract-Specific Clarification. A copy of the sampling trip report is made and retained for the CDM RAC II files. Procedure for Completing EPA CLP RAS Combination Forms A combination Organic or Inorganic TR/COC record is a four-page carbonless form (Figures C5and C6). The information that must be entered in the combination forms is detailed in the Contract Laboratory Program (CLP) Guidance for Field Samplers (EPA/540/R-00/003). A copy of this guidance is to be on site. Field quality control blanks and matrix spike samples will be noted on the combinations forms. Each sample will be assigned a CLP identification number that will be written or pre-printed on the sample label and affixed in the field to each container for CLP analysis. This unique number, which is recorded on |) the combination form, is used by EPA to identify the sample. Notations will be made if the sample is to be used as the matrix spike/ matrix spike duplicate (organics), matrix spike/ duplicate (inorganics), a field (rinsate) blank or trip blank. The same information required to be entered into FORMS II Lite™ is also required on hand written combination Organic or Inorganic TR/COC. After completing the day’s sampling, the bottom two copies of each completed combination form are placed in a zip-lock bag taped to the inside cooler lid and shipped with the samples to the laboratory. The top copy is submitted to the RSCC and the second copy is submitted to CLASS along with the sampling trip report. A copy of each combination form is made and retained for the CDM RAC II files. 5,2 Sample Labels and Tags, (on page 5 of 7) It should be noted that sample tags are no longer required for Region Il CLP samples. Therefore, Figure 2 on page 6 of 7 is not applicable, 7.0 REFERENCES, add (on page 7 of 7): Environmental Protection Agency (EPA). 1989. Region I] CERCLA Quality Assurance Manual. Revision 1. EPA Monitoring Management Branch of the Environmental Services Division. October 1989. . 2002. FORMS II Lite™ User's Guide, Version 5.1. __, 2004. Contract Laboratory Program (CLP), Guidance for Field Samplers, EPA-R-00-003. Final. EPA-540- R-00-003. August. CDM FEDERAL PROGRAMS CORPORATION Technical Standard Operating Procedures TSOP-1-2.RAC Prepared: David O. Johnson Technical Review: _S. Budney Jn, ESigned by Michael C. Malloy P, RIFX* ici ith A I { QA Review: Jo Nell Mullins Approve. i >> SESS |” ~“E-Signed by P. Michael Schwan Signature/Date | PRY giheyysty h apprayelt fre Issued: Signature/Date 1.0 Objective Because of the evidentiary nature of samples collected during environmental investigations, possession must be traceable from the time the samples are collected until their derived data are introduced as evidence in legal proceedings. To maintain and document sample possession, sample custody procedures are followed. All paperwork associated with the sample custody procedures will be retained in CDM Federal Programs Corporation (CDM) files unless the client requests that it be transferred to them for use in legal proceedings or at the completion of the contract. Note: Sample custody documentation requirements vary with the specific EPA region or client. This SOP is intended to present basic sample custody requirements, along with common options. Specific sample custody requirements shall be presented in the project-specific quality assurance (QA) project plan or project-specific modification or clarification form (see Section U-1). 2.0 Background 2.1 Definitions Sample - A sample is material to be analyzed that is contained in single or multiple containers representing a unique sample identification number. Sample Custody - A sample is under custody if: 1. It is in your possession 2, Itis in your view, after being in your possession 3, It was in your possession and you locked it up 4. Itis in a designated secure area Chain-of-Custody Record - A chain-of-custody record is a form used to document the transfer of custody of samples from one individual to another. Custody Seal - A custody seal is a tape-like seal that is part of the chain-of-custody process and is used to detect tampering with samples after they have been packed for shipping. Sample Label - A sample label is an adhesive label placed on sample containers to designate a sample identification number and other sampling information. Sample Tag - A sample tag is attached with string to a sample container to designate a sample identification number and other sampling information, Tags may be used when it is difficult to physically place adhesive labels on the container (e.g., in the case of small air sampling tubes). 3.0 General Responsibilities Sampler - The sampler is personally responsible for the care and custody of the samples collected until they are properly transferred or dispatched, Field Team Leader - The field team leader (FTL) is responsible for ensuring that strict chain-of-custody procedures are maintained during all sampling events. The FTL is also responsible for coordinating with the subcontractor laboratory to CDM Technical Standard Operating Procedures Page 1 of 6 TSOP 1-2 32207 te 2 a ee = Sc a Eh Bh ee ensure that adequate information is recorded on custody records. The FTL determines whether proper custody procedures were followed during the fieldwork. Field Sample Custodian - The field sample custodian, when designated by the FTL, is responsible for accepting custody of samples from the sampler(s) and properly packing and shipping the samples to the laboratory assigned to do the analyses. A field sample custodian is typically designated only for large and complex field efforts. Note: Responsibilities may vary from site to site. Therefore, all field team member responsibilities shall be defined in the field plan or site/quality assurance project plan (QAPP). 4.0 Required Supplies ® Chain-of-custody records (applicable client or CDM forms) = Custody seals = Sample labels and/or tags = Clear tape « EPA Field Operations Records Management System II Lite™ =» Computer (FORMS II Lite™) software (if required) = Printer ® Printer paper 5.0 Procedures 5.1 Chain-of-Custody Record This procedure establishes a method for maintaining custody of samples through use of a chain-of-custody record. This procedure will be followed for all samples collected or split samples accepted. Field Custody 1. Collect only the number of samples needed to represent the media being sampled. To the extent possible, determine the quantity and types of samples and sample locations before the actual fieldwork. As few people as possible shall handle samples. 2. Complete sample labels or tags for each sample using waterproof ink. 3. Maintain personal custody of the samples (in your possession) at all times until custody is transferred for sample shipment or directly to the analytical laboratory. Transfer of Custody and Shipment 1. Complete a chain-of-custody record for all samples (see Figure 1 for an example of a chain-of-custody record. Similar forms may be used when requested by the client). When transferring the possession of samples, the individuals relinquishing and receiving will sign, date, and note the time on the record. This record documents sample custody transfer from the sampler, often through another person, to the sample custodian in the appropriate laboratory. = The date/time will be the same for both signatures when custody is transferred directly to another person. When samples are shipped via common carrier (e.g., Federal Express), the date/time will not be the same for both signatures. Common carriers are not required to sign the chain-of-custody record. ® In all cases, it must be readily apparent that the person who received custody is the same person who relinquished custody to the next custodian. = If samples are left unattended or a person refuses to sign, this must be documented and explained on the chain- of-custody record. Note: If a field sample custodian has been designated, he/she may initiate the chain-of-custody record, sign, and date as the relinquisher. The individual sampler(s) must sign in the appropriate block, but does (do) not need to sign and date as a relinquisher (refer to Figure 1). CDM Technical Standard Operating Procedures Page 2 of 6 TSOP 1-2 32207 2. Package samples properly for shipment and dispatch to the appropriate laboratory for analysis. Each shipment must be accompanied by a separate chain-of-custody record. If a shipment consists of multiple coolers, a chain-of-custody record shall be filled out for each cooler documenting only samples contained in that particular cooler. 3. The original record will accompany the shipment, and the copies will be retained by the FTL and, if applicable, distributed to the appropriate sample coordinators. Freight bills will also be retained by the FTL as part of the permanent documentation. The shipping number from the freight bill shall be recorded on the applicable chain-of- custody record and field logbook in accordance with TSOP 4-1, Field Logbook Content and Control. Procedure for Completing CDM Example Chain-of-Custody Record The following procedure is to be used to fill out the CDM chain-of-custody record. The record provided herein (Figure 1) is an example chain-of-custody record. If another type of custody record (i.e., provided by the EPA Contract Laboratory Program (CLP) or a subcontract laboratory or generated by FORMS I! Lite™) is used to track the custody of samples, the custody record shall be filled out in its entirety. Record project number. Record FTL for the project (if a field sample custodian has been designated, also record this name in the “Remarks” box). Record the name and address of the laboratory to which samples are being shipped. Enter the project name/location or code number. Record overnight courier's airbill number. Record sample location number. Record sample number. Note preservatives added to the sample. Note media type (matrix) of the sample. 10, Note sample type (grab or composite). 11. Enter date of sample collection. 12. Enter time of sample collection in military time. 13. When required by the client, enter the names or initials of the samplers next to the sample location number of the sample they collected. 14. List parameters for analysis and the number of containers submitted for each analysis. 15. Enter appropriate designation for laboratory quality control (e.g., matrix spike/matrix spike duplicate [MS/MSD], matrix spike/duplicate (MS/D]), or other remarks (e.g., sample depth). 16. Sign the chain-of-custody record(s) in the space provided. All samplers must sign each record. 17. If sample tags are used, record the sample tag number in the “Remarks” column. 18. The originator checks information entered in Items 1 through 16 and then signs the top left “Relinquished by” box, prints his/her name, and enters the current date and time (military). 19. Send the top two copies (usually white and yellow) with the samples to the laboratory; retain the third copy (usually pink) for the project files. Retain additional copies for the project file or distribute as required to the appropriate sample coordinators. 20. The laboratory sample custodian receiving the sample shipment checks the sample label information against the chain-of-custody record. Sample condition is checked and anything unusual is noted under “Remarks” on the chain- of-custody record, The laboratory custodian receiving custody signs in the adjacent “Received by” box and keeps the copy. The white copy is returned to CDM. SOAS S GE ON = 5.2 Sample Labels and Tags Unless the client directs otherwise, sample labels or tags will be used for all samples collected or accepted for CDM projects. 1. Complete one label or tag with the information required by the client for each sample container collected. A typical label or tag would be completed as follows (see Figure 2 for example of sample tag; labels are completed with the equivalent information): Record the project code (i.e., project or task number). Enter the station number (sample number or EPA CLP identification number) if applicable, Record the date to indicate the month, day, and year of sample collection. Enter the time (military) of sample collection. CDM Technical Standard Operating Procedures Page 3 of 6 TSOP 1-2 32207 Place a check to indicate composite or grab sample. Record the station (sample) location. Sign in the space provided. Place a check next to “yes” or “no” to indicate if a preservative was added. Place a check under “Analyses” next to the parameters for which the sample is to be analyzed. If the desired analysis is not listed, write it in the empty slot. Note: Do not write in the box for “laboratory sample number.” = Place or write additional relevant information under “Remarks.” 2. Place adhesive labels directly on the sample containers. Place clear tape over the label to protect from moisture. 3. Securely attach sample tags to the sample bottle. On 2.27 liter (80 oz.) amber bottles, the tag string may be looped through the ring-style handle and tied. On all other containers, it is recommended that the string be looped around the neck of the bottle, then twisted, and relooped around the neck until the slack in the string is removed. 4. Double-check that the information recorded on the sample tag is consistent with the information recorded on the chain-of-custody record. 5.3 Custody Seals Two custody seals must be placed on opposite corners of all shipping containers (e.g., cooler) before shipment. The seals shall be signed and dated by the shipper. Custody seals may also be required to be placed on individual sample bottles. Check with the client or refer to EPA regional guidelines for direction. 5.4 Sample Shipping CDM Federal SOP 2-1, Packaging and Shipping Environmental Samples defines the requirements for packaging and shipping environmental samples. 6.0 Restrictions/Limitations Check with the EPA region or client for specific guidelines. If no specific guidelines are identified, this procedure shall be followed. For EPA CLP sampling events, combined chain-of-custody/traffic report forms generated with EPA FORMS II Lite™ or other EPA-specific records may be used, Refer to regional guidelines for completing these forms. The EPA FORMS II Lite™ software may be used to customize sample labels and custody records when directed by the client or the CDM project manager. 7.0 References U. S. Army Corps of Engineers. 2001. Requirements for the Preparation of Sampling and Analysis Plan, EM 200-1-3. Appendix F. February. U. S. Environmental Protection Agency. Revised March 1992, National Enforcement Investigations Center, Multi-Media Investigation Manual, EPA-330/9-89-003-R. p.85. . Region IV. 1996. Environmental Investigations Standard Operating Procedures and Quality Assurance Manual. Section 3.3. May. . 2002, FORMS II Lite™ User's Guide, Version 5.1. . 2002. EPA Guidance for Quality Assurance Project Plans, EPA QA/G-5, EPA/240/R-02/009. Section 2.2.3. December. . 2004. Contract Laboratory Program (CLP), Guidance for Field Samplers, EPA-540-R-00-003. Final. Sectior, 3.2. August. CDM Technical Standard Operating Procedures Page 4 of 6 TSOP 1-2 32207 Figure 1 Example CDM Chain-of-Custody Record 126 Maden Lane, Bh Fleor CDM New York, NY” 10083 CHAIN OF pete P (212) 785-9123 Fax: (212) 785-6114 RECOR || PROVECT ID, FIELO TEAM LEADER LABORATORY DATE SHIPPEO AND ADDRESS | PROJECT NAME/LOGATION AIRBILL HO, H LAB CONTRACT; | EDIA TYPE PRESERVATIVES SAMPLE TYPE 1. Surface Water 1. HCI, pH <2 G « Grab | 2. Groundwater 2, HNOS, pH <2 © = Composite 3 | 3. Leachate 3. NaOH, pH >12 i | 4. Fled OG 4. H2SO4, pH <2 ; |] 5. SdSediment 5. Zino Acetate, pH 29 § 6. O1 6, [ca Only ¥ | 7 Waste 7. N& Preserved | ||| 8. Olbar 8. Other ; SAMPLE LABORATORY |[PRESER: [MEDIA/SAMPLE 20._| TIME REMARKS LOCATION SAMPLE = |VATIVES| TYPE PE | DATE |SAMPLE ; P : ho. HUMBER ALDOED hi sal ni i Nata il SMSO) *, ae ee 2 |—_ 7 ; 2 - A, i 6. i PA a, | % 10. SAMPLER SIGHSTUNES: | ACLISCYUISHLO OY; OATOTIME] RECOMED OY; QATIP ME | ALUNGUSSIEO BY QaTcme | ACCLVLD bY QA FUTINE, joann DAbULF) ree Prem 1 Aaeekd pou 62 boy AELINCUISHEDBY: DATETIVE| FRECEVEDSY: OATETME | REUNOLISHED BY. DATEMME| REGENED Er. DATEMINE SHENTL Damir) prety prety U3 yest pte] nay ney SONMENTE: CISTR BUTION Vino and yobs Coplts zoccmpory sumsde scans oe hsboeatceys yw copy reid ty bbe Tan Pink cosy dso ty rants. Wie Note: |f requested by the client, different chain-of-custody records may be used. Copies of the template for this record may be obtained from the Chantilly Graphics Department. CDM Technical Standard Operating Procedures TSOP 1-2 32207 hee as enn, ik i> ample ustody rR VISION Me 07 ee ee AE Pe ns mu tAES ss a SS ia a es A a Figure 2 Example Sample Tag Preservative: Yes 1) No O ANALYSES BOD Anions Sollds (rss (ros (35) COD, TOC, Nutrlents Phenolics Mercury ' | Metals Cyanide =i Oil and Grease | Organics GC/MS Priority Pollutants Volatile Organics Pesticides | Mutagentclty Bacterlology Remarks; sat Teg No Lab Sample No. 33022215 af Note: Equivalent sample labels or tags may be used. CDM Technical Standard Operating Procedures TSOP 1-2.32207 Prepared: Del Baird QA Review: Jo Nell Mullins Approved: ies ————See ee TE Signed by B. Michagl Schwan Signature/Date PEO MCE SSeS a — Issued: Signature/Date 1.0 Objective Water level measurements are fundamental to groundwater and solute transport studies and are conducted during groundwater sampling events to calculate the amount of groundwater to be purged from the well. This standard operating procedure (SOP) defines the techniques and requirements for obtaining groundwater level measurements. 2.0 Background 2.1 Definitions Water Level Indicator - A portable device for measuring the depth from a fixed point (which could be below, at, or above the ground surface) to the groundwater inside a well, borehole, or other underground opening. Measurement Point - An easily located and clearly defined mark at the top of a well from which all water level measurements from that particular well are made. The measurement point shall be as permanent as possible to provide consistency in measurements. Electrical Tape - A graduated plastic tape onto which a water-sensitive electrode is connected that will electronically signal the presence of water (as a result of circuit closure). Immiscible Fluids - Two or more fluid substances that will not mix and, therefore, will exist together in a layered form. The fluid with the highest density will exist as the bottom layer, the fluid with the lowest density will exist as the top layer, and any other fluid layers will be distributed relative to their respective densities. Discharge - The removal/release of water from the zone of saturation. Recharge - The addition of water to the zone of saturation. Static Water Level - The level of water in a well, borehole, or other underground opening that is not influenced by discharge or recharge. Well Riser - A steel, stainless steel, or polyvinyl chloride pipe that extends into a borehole and is connected to the well screen or sealed at the bedrock surface in open-hole wells. The upper portion (approximately 3 to 5 feet) of the well riser is normally enclosed by an outer steel protective casing. Protective Casing - A steel cylinder or square protective sleeve extending approximately 3 to 5 feet into the ground, surrounding the well riser. In flush-mounted wells, the protective casing will extend only high enough so that the well and protective casing can be enclosed by a Christy box or equivalent vault. In above-grade wells, the protective casing will extend above the ground surface approximately 2 to 3 feet. The protective casing protects the well riser. 2.2 Associated Procedures = CDM Federal (CDM) SOP 4-1, Field Logbook Content and Control » CDM SOP 4-5, Field Equipment Decontamination at Nonradioactive Sites 2.3 Discussion The most common uses of static water level data are to determine the elevation of groundwater, the direction of groundwater flow, to identify areas of recharge and discharge, to evaluate the effects of manmade and natural stresses on the groundwater system, to define the hydraulic characteristics of aquifers, and to evaluate stream-aquifer relationships. Specific uses for water level data may include: Determine the change in water level due to distribution or rate of regional groundwater withdrawal Show the relationship of groundwater to surface water Estimate the amount, source, and area of recharge and discharge Determine rate and direction of groundwater movement Static water level measurements shall be obtained from each well before purging, sampling, or other disturbance of the water table. 3.0 General Responsibilities Project Manager - The project manager is responsible for ensuring that measurements are conducted in accordance with this procedure and any other SOP pertaining to site activities related to obtaining groundwater level measurements. Field Team Leader - The field team leader is responsible for ensuring that field personnel obtain water level measurements in accordance with this and other relevant procedures. Note: Responsibilities may vary from site to site. Therefore, all field team member responsibilities shall be defined in the field plan or site/quality assurance project plan (QAPP). 4.0 Required Equipment 4.1 General « Site-specific plans ® Decontamination equipment and supplies, including rinse bottles ® Field logbook and deionized water ® \|ndelible black ink pens ® Tap water and large beaker or bucket = Permanent felt-tip marker (e.g., Sharpie) # Water level meter ] Personal protective equipment 4.2 Measuring Devices The equipment required to obtain water level measurements is dependent on the type of procedure chosen. Measurements may be made with a number of different devices and procedures. Measurements are taken relevant to a permanent measurement point on the well riser. Electrical tapes are preferred over other devices such as steel tape because of the electrical tape's simplicity and ability to make measurements in a short period of time. Many types of electrical instruments have been devised for measuring water levels; most operate on the principle that a circuit is completed when two electrodes are immersed | in water. Examples of electrical tapes that are frequently used include the Slope Indicator Co.° and Solinst® electronic water level indicators. These instruments are powered by batteries that shall be checked before mobilization to the field. Electrical tapes are coiled on a hand-cranked reel unit that contains the batteries and a signaling device that indicates when the circuit is closed (i.e., when the probe reaches the water). Electrodes are generally contained in a weighted probe that Keeps the tape taut in addition to providing some shielding of the electrodes against false indications as the probe is being lowered into the hole. The electrical tapes are marked with 0.01-foot increments. Caution shall be exercised when using electrical tapes when the water contains elevated amounts of dissolved solids. Under these conditions, the signaling device will remain activated after the probe is removed from the water. When the water being measured contains very low amounts of dissolved solids, it is possible for the probe to extend several inches below the water level before activating the signaling device. Both of these conditions are related to the conductivity of the water and in some cases may be compensated for by the sensitivity control, if the device has this option. In groundwater with high conductivity the sensitivity control may need to be turned down, and in groundwater with low conductivity the sensitivity control may need to be turned up to get a proper depth to groundwater measurement. “) SOP/4-6: = a3, 7 6 5.0 Procedures 5.1 Preparation The following steps must be taken when preparing to obtain a water level measurement: =» Assign a designated field logbook to record all field events and measurements according to CDM SOP 4-1. Document any and all deviations from SOPs and site-specific plans in the logbook and include rationale for the changes. = Always exercise caution to prevent inappropriate or contaminated materials from entering an environmental well. » Standing upwind from the well, open the groundwater well. Monitor the well with a photoionization detector, flame ionization detector, or equivalent vapor analyzer as soon as the cap is opened, as dictated by the site-specific health and safety plan. For comparability, water level measurements shall always be referenced to the same vertical (elevation) datum marker, such as a U. S. Geological Survey (USGS) vertical and horizontal control point monument. The elevations calculated from the measurement of static water levels shall be referenced to mean sea level unless otherwise specified in the site- specific plans. The measurement point must be as permanent as possible, clearly defined, marked, and easily located. Frequently, the top.of the PVC riser is designated as the measurement point. However, since the top of the riser is seldom smooth and horizontal, one particular point on the riser pipe shall be designated and clearly marked. This can be accomplished by marking a point on the top of the riser pipe with a permanent marker. To avoid spilling liquids into the well, paints or other liquid marking materials shall not be used. 5.2 Water Level Measurement Using Electrical Water Level Indicators The following steps must be followed when taking water level measurements using electrical tapes: " Before lowering the probe into the well, the circuitry shall be checked by dipping the probe in tap water and checking to ensure that the signaling device responds to probe submergence. The probe shall then be lowered slowly into the well until contact with the water surface is indicated. The electrical tape reading is made at the measuring point. Take a second and third check reading to verify the measurement before completely withdrawing the tape from the well. » |ndependent electrical tape measurements of static water levels using the tape shall agree within 0.01 foot for depths of less than about 200 feet. At greater depths, independent measurements may not be this close. For a depth of about 500 feet, the maximum difference of independent measurement using the same tape shall be within 0.1 foot. = Decontaminate the electrical tape according to CDM SOP 4-5 before proceeding to the next well to minimize cross contamination. It may be necessary to check the electrical tape length with a graduated steel tape after the line has been used for a long period of time (at least annually) or after it has been pulled hard in attempting to free the line. Some electrical tapes, especially the single line wire, are subject to becoming permanently stretched. 5.3 Other Water Level Measurement Methods Although the method cited above (electrical water level indicator) for measuring water levels predominates in the environmental sector, there are a number of other methods available that may be well suited for a particular purpose. 5.3.1 Ultrasonic Method The ultrasonic method electronically measures the amount of time it takes a sound wave to reach and reflect off the water surface and return to the ground surface. These instruments contain electronic microprocessors, capable of performing this measurement many times each second. The actual depth to water, as calculated by the microprocessor, is an average of many individual readings. surement soe Dh ee a ee ee eee 5.3.2 Pressure Gauge Method This method, also called the air-line submergence method, uses a pressure gauge and is the preferred method for obtaining water level measurements in pumping wells. An air line constructed of semi-rigid tubing is inserted into the well below the water table. The tube end at the surface is connected to an air tank or compressor and pressure gauge. Filtered air is then forced through the tube and the resultant pressure is read in pounds per square inch (psi). This reading is converted to feet of water in the column and subtracted from the total tube length to give depth to water. Readings are then converted to groundwater elevation. Results are plotted on a field logging form. Calibration records and the exact procedures used must be maintained. 5.3.3 Acoustic Probe Method The acoustic probe is an electronic device containing two electrodes and a battery-powered transducer. The probe is attached to a tape. The probe is lowered into the well until a sound is detected, indicating the electrodes in the probe have contacted the water surface. This method is similar to the electrical probe method discussed in Section 5.2. 5.3.4 Continuous Recording Method The measurement of groundwater elevations within pumping or monitoring wells can be accomplished by the use of a mechanical or digital analog computerized continuous recording system and shall be performed according to specifications given by the manufacturer of each unit. In general, when using the mechanical or digital system, the pressure or electrical transducer is lowered into the well until it intersects the water surface. The actual depth to water is then measured by one of the methods described above and used to calibrate the continuous recorder. The necessary adjustments and preparations are then completed according to the specifications given for each type of continuous recorder, Proper maintenance of continuous recording devices during water level monitoring shall be performed such that continuous, permanent records are developed for the specified period of time. Records shall be stored on mechanical graph paper or on a microprocessor. Frequent calibrations of equipment shall also be made during monitoring periods of long duration in accordance with the manufacturers’ specifications. 6.0 Restrictions/Limitations 6.1 Groundwater and Miscible Fluids Where water is rapidly dripping or flowing into a well, either from the top of the well or from fractures, obtaining an accurate reading may not be possible. The effect of the water flowing into the well may interfere with an electronic water level measuring device, resulting in a false water level measurement. If water levels must be recorded in wells completed in aquifers that are recharging or discharging, the electronic water level indicator is the preferred measuring device, but shall be used with the awareness of possible false measurements. To minimize the effects of “splashing,” a 1-inch pipe (decontaminated for environmental wells) may be lowered into the pumping well into which the water level indicator would be inserted. This will minimize the effect of “splashing” until the probe contacts the groundwater and protect the probe from becoming tangled in pump wiring or well spacers associated with downhole equipment such as submersible pumps. 6.2 Immiscible Fluids For wells containing immiscible contaminants, the field personnel will need to use special procedures for the measurement of fluid levels. The procedure to follow will depend on whether layers are light immiscibles that form lenses floating on the top of the water table, or dense immiscibles that sink through the aquifer and form lenses over less permeable layers. In the case of light immiscibles, measurements of immiscible fluid and water levels cannot be accomplished by using normal techniques. A conventional electrical tape often will not respond to nonconducting immiscible fluids. Techniques have been specially developed to measure fluid levels in wells containing immiscible fluids, particularly petroleum products. A special paste or gel applied to the end of the steel tape and submerged in the well will show the top of the oil as a wet line and the top of the water as a distinct color change, or an interface probe can be used that will detect { 4 the presence of conducting and nonconducting fluids. Thus, if a well is contaminated with low density, nonconducting immiscible fluids such as gasoline, the probe will first detect the surface of the gasoline, but it will not register electrical conduction. However, when the probe is lowered deeper to contact water, it will detect electrical conduction. Normally, a variation in an audible signal indicates the difference between phases. Both of these methods have disadvantages. These methods are less effective with heavier and less refined petroleum pro- ducts because the product tends to stick to the tape or probe, giving a greater product thickness measurement than it shall. Paste or gel cannot be used when sampling groundwater for the same constituents present in the paste or gel product. Note that water levels obtained in this situation are not suitable for determining hydraulic gradients without further interpretation. To use such data for determining hydraulic gradients, the difference in density between the light immiscible phase and water has to be considered. Measuring fluid levels in wells screened in lenses of dense immiscible fluids resting on a low permeability formation is somewhat easier, provided the immiscible fluid is nonconducting. The top of the dense layer can be identified by simply using an electrical sounder. As an electrical sounder passes from groundwater into the immiscible phase, the detection unit will deactivate because the fluid will no longer conduct electricity. A better method would be to use an interface probe as described above. The variation in the audible signal associated with the detection of differing phase liquids will also allow the user to obtain a groundwater depth and dense immiscible thickness measurement. 7.0 References Camp Dresser & McKee Inc., et al. 1991. Sampling and Analysis Procedures, Geophysical Survey Procedures. May. U. S, Environmental Protection Agency. 1987. A Compendium of Superfund Field Operations Methods, EPA/540/P- 87/001. December. Weight, Willis D. and Sonderegger, John L., 2001. Manual of Applied Hydrogeology. Lewis Publishing Company. 187-190. Westinghouse Savannah River Company. 1997. Standard Operating Procedures Manual, 3Q5, Chapter 13, Revision 2, Hydrogeologic Data Collection Procedures and Specifications. October. Prepared: Del Baird/Chris Koerner Technical Review: _Chris Koerner y Michael C. Malloy i QA Review: Jo Nell Mullins Approved: pit ——— | ESigned by os aay! Signature/Date (PRE githensy ty syfth rqvelt Issued: |! ——_—__——— — Signature/Date 1.0 Objective The purpose of this standard operating procedure (SOP) is to define requirements for collection of vapor using evacuated SUMMA® canister samplers. 2.0 Background Collection of discrete or temporally composited air samples from designated locations on or near a hazardous waste site may be required to characterize and model the nature and extent of ambient or subsurface contamination. The method described in this SOP is adapted from U. S. Environmental Protection Agency Method TO-15 Second Edition 1999. Two types of vapor samples can be collected with SUMMA canisters. The canister can be opened and allowed to fill over a short period to obtain a grab sample or filled slowly by using a flow controller to collect a time-integrated sample. 2.1 Definitions Canister - Leak-free stainless steel pressure vessels of desired volume (e.g., 1 to 6 liters [L]), with valve and specially prepared (SUMMA) nonreactive interior surfaces. The canister is initially evacuated (under high vacuum) at the laboratory to approximately -30 inches of mercury (Hg). The canisters must be properly cleaned at the laboratory before each use by either ultra-pure humidified air in a series of evacuation/pressurization cycles or in a high temperature oven. The canister is then analyzed by GC/MS to verify cleanliness. Note: Canisters previously used for the measurement of high-level contamination may not be suitable for indoor air monitoring, since they may not be able to be adequately decontaminated. Particulate Matter Filter - 2-micrometer (tm) sintered stainless steel in-line filter. A separate laboratory-cleaned filter is used for each canister sample. Stainless Steel Vacuum/Pressure Gauges - A gauge capable of measuring vacuum (0 to -30 inches Hg or -100 to 0 kilo pascals [kPa]) and pressure (0 to 30 pounds per square inch [psi] or 0 to 206 kPa) is needed to verify the initial canister vacuum and to measure sampling progress in the sampling system. Gauges shall be tested clean and leak tight. Sampling Inlet Line/Connectors - Stainless steel, Teflon®, or polyethylene tubing (all usually %-inch diameter) and appropriate air-tight connectors (i.e., Swagelok® tube fittings) connect the canister to the sample inlet. A Swagelok fitting has four parts, the connector body, two ferrules, and the nut. The larger (cone-shaped) ferrule fits into the connector body, small diameter end first. The smaller end of the smaller ferrule fits on top of the cone ferrule, and the nut is screwed on top. The tubing fits through the nut and the two ferrules, and seats firmly in the connector. On newly created fittings, the nut shall be tightened with two wrenches, 1% turns past finger tight to compress the ferrules onto the tubing. (Swagelok makes an inspection gauge that fits between the nut and the connector body if a large number of critical connections are to be made). Connections that have been previously made up will only need a short tighten with the wrenches past finger tight. Stainless Steel Shut-Off Valve - Leak free, for vacuum/pressure gauge. Electronic Mass Flow Controller - This controller, used to collect composite samples, must be capable of maintaining a constant flow rate (+10 percent) over a sampling period of up to 24 hours and under conditions of changing temperature (20 to 40 degrees Celsius [°C]) and humidity. CDM Technical Standard Operating Procedures Page 1 of 5 TSOP 1-8 32707 Auxiliary Vacuum Pump - Continuously draws air through the inlet manifold at 10 L/minute or higher flow rate. The canister vacuum extracts a sample from the manifold at a lower flow rate, and excess air is exhausted. Note: The use of higher inlet flow rates dilutes any contamination present in the inlet and reduces the possibility of sample contamination as a result of contact with active adsorption sites on inlet walls. The auxiliary pump and sampling manifold can also be used to purge vapor monitoring wells. Elapsed Time Meter/Stopwatch - Measures duration of sampling. 2.2 Associated Procedures 2.3 Discussion Ambient air, emission source, or vapor monitoring well samples are collected to determine the type(s) and level(s) of contamination from airborne toxic organic compounds (often important to risk assessment), characterize subsurface vapor contamination, or evaluate vapor intrusion into buildings. These samples may be collected as part of an investigative plan, site-specific sampling plan, and/or as a screen for “hot spots,” which may require more extensive sampling. Sampling will include necessary quality assurance/quality control (QA/QC) samples as documented in the project-specific QAPP, and a field blank shall accompany all sampled media. 3. Site Manager - The site manager is responsible for ensuring that SUMMA canister sampling efforts are performed consistently with this procedure and other project-specific documents such as the QAPP, work plan, sampling plan, and the health and safety plan. Field Team Leader - The field team leader is responsible for ensuring that field personnel collect vapor samples in accordance with this or the project-specific procedure in the field plan and that appropriate documentation is collected. Note: Responsibilities may vary from site to site. Therefore, all field team member responsibilities shall be defined in the field plan or site-/project-specific quality assurance plan. 4. 3. 5.1 Preparation 1. . Check the number on the permanent label/tag attached to the canister against the laboratory-supplied chain-of-custody CDM Federal SOP 1-2, Sample Custody CDM Federal SOP 4-1, Field Logbook Content and Control ' CDM Federal SOP 1-10, Field Measurement of Organic Vapors 0 Responsibilities 0 Required Equipment/Supplies Site-specific plans Adjustable wrenches (two 9/16-inch opened end wrenches for Swagelok fittings) Labels/canister tags (shall be attached to canister) and appropriate laboratory-supplied, individual canister-specific, chain-of-custody forms Field logbook or field forms Documentation for sample shipment Items listed in Section 2.1, Definitions, as applicable Sturdy shipping container(s) 0 Procedures The analysis of vapor samples collected in a canister will have very low detection limits. Canister preparation shall therefore be performed in clean air environments, away from any type of volatile organic contamination. The canisters are expensive, and, although relatively sturdy, valves and connections can be easily damaged. Do not over tighten valves. Use two wrenches to remove and reconnect line caps and attachments. Using a single wrench may cause excessive torque on the fitting/canister connection. form. Verify that the canister number on the form agrees with the label. Note the date the canister was cleaned, preevacuated canister vacuum, and laboratory analysis verification, etc. The supplied paperwork will vary depending o' the laboratory supplying the canister, The objective is to verify that the canister is the correct one, has been cleaned, and has been evacuated to a vacuum approximately -30” Hg. | CDM Technical Standard Operating Procedures Page 2 of 5 TSOP 1-8 32707 3, In aclean environment, use two wrenches to remove the Swagelok cap from the end of the canister and attach a clean vacuum gauge. Verify that the gauge reads zero. Tighten the gauge fitting tightly with the wrenches. Open the canister valve, read the gauge, and record the reading on the chain-of-custody. SHUT THE VALVE TIGHTLY (turn clockwise). The vacuum reading shall agree closely (the field gauge may not be as accurate as the gauge in the laboratory) with the vacuum noted by the laboratory. If the field vacuum is more than 1 inch of Hg less than the laboratory vacuum, then the canister valve has leaked during the time since the canister was evacuated, and a portion of the canister has been filled with an unknown vapor sample. If the vacuum is not sufficient, replace the canister and document the change. If there are questions, call the laboratory that supplied the canister for guidance/to discuss further action. 4. If the two vacuum readings agree and the canister is suitable for use, verify that the valve is closed tightly, and remove the vacuum gauge. Attach a clean sample filter (supplied by the laboratory) and replace the Swagelok cap on the filter. 5. If required, build a sampling apparatus using appropriate tubing, connectors, or valves to connect the canister to the sampling location. 6. If a vacuum pump is to be used to purge a soil vapor monitoring well, insert a “tee” fitting between the well and the vacuum pump (upstream of the pump), and a line valve between the tee fitting and the pump. During purging, the line valve is opened and the third leg of the tee is capped, allowing the pump to pull air from the well without short-circuiting through the tee. If a portable photoionization detector, flame ionization detector, or other real-time instrument is to be used to take a field screening reading from the well, a second tee fitting shall be installed on the downstream side of the pump exhaust port. The probe of the instrument is inserted into one leg of the tee, while the other leg is allowed to vent, to prevent pressurizing the instrument and creating false readings. 5.2 Using a Flow Controller for Time-Integrated (Temporally Composited) Sampling 1. To ensure the correct time-integrated sampling rate, the flow controller must be calibrated for the planned sampling duration using a mass flow meter or bubble meter traceable to an American Society for Testing and Materials (ASTM) or National Institute of Standards and Technology (NIST) standard. This measurement will be made by actual calibration by the sampling team, or if calibrated by a laboratory, by checking calibration documentation. A flow control device is chosen to maintain a constant flow into the canister over the desired sample period. This flow rate is determined so the canister is filled (to about 88.1 kPa for subatmospheric pressure sampling or to about 1 atmosphere above ambient pressure for pressurized sampling) over the desired sample period. The flow rate can be calculated by where: F = flow rate, mL/minute P = final canister pressure, atmospheres absolute. P is approximately equal to kPa gauge +4 101.2 kPa V = volume of the canister, mL T = sample period, hours For example, if a 6-L canister is to be filled to 202 kPa (2 atmospheres) absolute pressure in 24 hours, the flow rate can be calculated by: f= 26,000 24 x 60 = 8.3 mL/minute 2. The evacuated canister, flow controller (if required), vacuum gauge, particulate matter filter, and sample inlet need to be assembled (if not already pre-assembled by the offsite laboratory) using two open-end wrenches to tighten the tubing and sampling system components to the canister valve stem. CDN Technical Standard Operating Procedures Page 3 of 5 TSOP 1-8 32707 3. Data entries on the daily sample event data sheet (or equivalent) shall include serial numbers for all numbered sampling components, sample initiation time, sample identification number, sample collection time, separate entries for sub- atmospheric SUMMA canister pressures at sample initiation and completion, sampler initial(s), initiation date, collection date, and sample tag custody number. = 3 Sample Collection . The sample system assembly is transported to the required sample location. Before collecting each sample, confirm that the canister number and sample identification corresponds to the correct sample location. 2. If using a vacuum pump to purge a vapor monitoring well or other space, begin preparing the canister when sufficient purging of the well has been accomplished. Attach a canister with the valve closed to the third leg of the tee upstream of the pump (discussed in 5.1), while the pump continues to pull vapor from the well. Do not connect the canister to the downstream side of the pump, since the pump may contain contaminants that may be introduced into the sample. The sample is drawn into the canister by the vacuum. When it is time to collect the sample, the valve between the canister and the pump is shut off, preventing backflow through the pump if the canister vacuum happens to be stronger than the pump. 3. When collecting a grab (not a temporally composited) sample, check the tightness of all fittings on the sampling apparatus and the connections on the canister. If sampling the ambient air or emission source, position the canister inlet in the intended environment with the inlet line pointed downward to prevent rainwater from entering the canister. 4. To initiate a sample event, gently open (counter clockwise) the canister valve until a hissing noise is heard. Note the initial vacuum reading on the gauge (attached to the canister with a tee) and that the vacuum level begins to drop. There are differing opinions on how long to allow for the canister to fill, and whether there is any negative effect of opening the valve, rapidly. A good compromise is to adjust the valve so there is a slow hiss, allowing the canister to fill in about a half minute. The canister valve can be closed before the hissing stops and the vacuum gauge reaches 0 inches Hg. Record the final vacuum level on the chain-of-custody. Close the valve firmly, without overtightening. 5. Remove the canister from the sampling apparatus, remove the gauge and filter, and replace the canister cap, Do not use the same filter to collect another sample. 6. Record the final vacuum level, duration of sample collection, and any other pertinent sampling information of the chain-of- custody. Complete documentation on the daily event datasheet and the field logbook before leaving each sample location. 7. Place the canister in a sturdy container for shipping. Place all of the used filters in a plastic baggie and return them to the laboratory with the canisters. 6.0 Restrictions/Limitations The nonreactive inner surface of the SUMMA canister may not be compatible for sampling atmospheres with high levels of chlorine or sulfur, Contact the analytical laboratory for guidance when these elements are suspected. For 24-hour time-integrated sampling, sample flow rates through the vacuum gauge of the sample system may not remain stable (within the method flow rate tolerance) at vacuums less than 9 inches Hg (e.g., 8 inches Hg). Caution shall be taken in using 24-hour time-integrated samples where final vacuum is less than 4 inches Hg. Flow rates at this vacuum and below are not constant, yielding potentially nonrepresentative results during the latter portion of the sampling period. Any canister that has reached 0 inches Hg vacuum may not be a representative 24-hour sample. Samples collected at vacuums above 10 inches Hg (e.g., when the canister valve is closed before the gauge reaches 10 inches Hg) may not contain enough sample volume to meet sample volume requirements for high-resolution gas chromatography/mass spectrometry analysis detection limits. Ice crystals can block the flow controller or sampling apparatus at temperatures at or below freezing, Frequent monitoring of canister pressure is recommended during cold periods. CDM Technical Standard Operating Procedures Page 4 of 5 TSOP 1-8 32707 SE a ——————— CT 6} in npl 7) [ Jal V, )/ = Sh Oe a3 = 7.0 References U. S. Environmental Protection Agency. 1999. Compendium of Methods for the Determination of Toxic Organic Compounds in Ambient Air, Second Edition, Compendium Method TO-15, Determination of Volatile Organic Compounds (VOCs) in Air Collected in Specially Prepared Canisters and Analyzed by Gas Chromatography/Mass Spectrometry (GC/MS). January. Air Toxics LTD. Winter 1996. /n The Air. Vol. 1, No. 1. CDM Technical Standard Operating Procedures Page 5o0f 5 TSOP 1-8.32707 Prepared: (Tammy Phillips Technical Review: _ Chris Koerner yr _E-Signed by Michael C Malloy — (2) } VERIFY*au j Approvelt Meld? ig | QA Review: Jo Nell Mullins Approved: : =e lop er foie ccm Signature/Date ‘Fe RY gitnenriftty h ABs rovelt Issued: ~— ———_ ; Signature/Date 1.0 Objective The objective of this standard operating procedure (SOP) is to define the techniques and the requirements for the measurement of organic vapors in the field. 2.0 Background 2.1 Definitions Photoionization Detector (PID) - A portable, hand-held instrument that measures the concentration of gaseous organic compounds through the photoionization of organic vapors. Flame lonization Detector (FID) - A portable, hand-held instrument that measures the concentration of gaseous organic compounds through the flame ionization of organic vapors. 2.2 Associated Procedures =» CDM Federal SOP 1-4, Subsurface Soil Sampling CDM Federal SOP 1-5, Groundwater Sampling Using Bailers CDM Federal SOP 1-6, Water Level Measurement CDM Federal SOP 1-8, Volatile Organic Compound Air Sampling Using USEPA Method TO-15 with SUMMA Canister CDM Federal SOP 3-1, Geoprobe™ Sampling CDM Federal SOP 3-5, Lithologic Logging CDM Federal SOP 4-3, Well Development and Purging 2.3 Discussion The measurement of organic vapors is a required step during numerous field activities. The primary purpose of such measurements is health and safety monitoring to determine if the breathing zone in a work area is acceptable or if personal protective equipment such as a respirator or a supplied air device is necessary for field personnel. In addition to health and safety monitoring, organic vapor measurement is also used in conjunction with sampling activities, including screening subsurface soil samples, soil vapor and indoor air sampling, and groundwater sampling, where measurements are useful for establishing approximate contaminant levels or ranges. The two types of instruments most commonly used to measure organic vapors are PIDs and FIDs. Both instruments first ionize the gaseous compound and then measure the response, which is proportional to the concentration. 2.3.1 PID Operation The PID is preferred when the compound of interest is an aromatic or chlorinated volatile organic compound (VOC). The PID ionizes the sampled vapors using an ultraviolet lamp that emits light energy at a specific electron voltage (eV - labeled on the lamp). The ultraviolet lamp produces photons that are absorbed by the sampled vapor molecule. The molecule becomes excited, producing a positively charged ion and emitting an electron. The number of electrons emitted is proportional to the concentration of the sampled gases. Every organic compound has a specific ionization potential in electron volts. The energy emitted by the lamp must be higher than the ionization potential of the compound for the compound to become ionized and emit an electron. If the ionization potential of the compound is higher than the eV of the lamp, there will be no response on the instrument. Therefore, the ionization potential of the known or suspected compounds shall be checked against the energy of the ultraviolet lamp to verify that the energy provided by the lamp is CDM Technical Standard Operating Procedures Page 1 of 3 TSOP 1-10 32607 = Ce a ara e } 2 I Field Measuremento greater. Additionally, manufacturer’s manuals shall be consulted to obtain the appropriate correction factors for known or suspected contaminants. Water vapor in the vapor sample can interfere with the PID detector and cause the instrument to stop responding. This can be caused by using the PID on a rainy day or when sampling headspace samples that have been in the sun. If moisture is suspected, the calibration gas shall be used to check the instrument response by inserting the gas as a check sample, not by recalibrating. If the response is lower than the gas level, then the probe and the ionization chamber shall be dried out before reusing the instrument. Note: The ultraviolet lamp in the PID is sensitive to shock, especially when using the higher eV lamps. Therefore, they shall be handled and transported carefully. The sampling probe shall not be inserted directly into soil samples or dusty areas, as the instrument vacuum will pull dirt into the ionization chamber. Under particularly dirty or dusty conditions, the lamp may become covered with a layer of dust, If dirty conditions are encountered, or if the instrument response seems to have decreased, then the lamp shall be cleaned. The instrument manual provides instructions on how to remove the instrument cover to access the lamp, and how to clean the screen in the ionization chamber and the surface of the lamp. 2.3.2 FID Operation The FID is preferred when sampling for petroleum hydrocarbons and methane (landfill gases). It responds well to aromatic hydrocarbons but is not as convenient to use as the PID. The FID allows measurement of a wide variety of compounds, but in general its sensitivity is not as high as the PID for compounds where the PID is applicable. The FID ionizes the vapor sample by burning it in a hydrogen/air flame, and measuring the response beyond what is caused by the hydrogen alone. This instrument requires a hydrogen supply, contained in a small tank in the instrument. This hydrogen, including the gas in the instrument tank, is considered a flammable gas and appropriate requirements must be adhered to when shipping. The instrument shall be emptied of hydrogen before shipping. Federal Express Hazardous Material shipping manifests must be completed when shipping the gas. The hydrogen gas in the FID combustion chamber is ignited by pressing a red button on the side of the instrument, which sends electrical current to a small resistance coil igniter in the combustion chamber. This igniter is very sensitive, and if the red button is pressed for longer than 5 seconds, the coil will burn out and the instrument will be unusable unless another igniter is available. If the instrument will not light, check the electrical connections and switches for proper settings. Check that the pump is pumping, and allow fresh air to flow through the combustion chamber for several minutes before lighting. Check to see if the exhaust port of the combustion chamber is dirty. 3.0 Responsibilities Site Manager - The site manager is responsible for ensuring that field activities are conducted in accordance with this procedure and any other SOPs pertaining to the specific activity. Field Team Leader - The field team leader is responsible for ensuring that field personnel conduct field activities in accordance with this and other relevant procedures, Note: Responsibilities may vary from site to site, Therefore, all field team member responsibilities shall be defined in the field plan or site-/project-specific quality assurance plan. 4.0 Required Equipment " Site-specific plans = Calibration gases in a range appropriate for the expected use a Field logbook = 0.5 liter (16-ounce) or “Mason” type glass jar = Waterproof black ink pen = Hydrogen Canister and fill valve and hose (if using FID for a = Personal protective clothing and equipment period of more than 1 day) ® Photoionization detector or flame ionization detector CDM Technical Standard Operating Procedures Page 2 of 3 TSOP 4-10 32607 5.0 Procedures 5.1 Direct Reading Measurement 1. Connect the measurement probe to the instrument and make necessary operational checks (e.g., battery check, etc.) as outlined in the manufacturer's manual. 2. Calibrate the instrument following the applicable manufacturer's manual 3. Make sure the instrument is reading zero and all function and range switches are set appropriately. 4. Insert the end of the probe directly into the atmosphere to be measured (e.g., breathing zone, monitoring well casing, split spoon, etc.) and read the organic vapor concentration in parts per million (ppm) from the instrument display. Apply the appropriate correction factor if necessary. Record the highest instrument response. 5. Immediately document the reading in the field logbook or on the appropriate field form. 5.2 Headspace Measurement 1. Connect the measurement probe to the instrument and make necessary operational checks (e.g., battery check, etc.) as outlined in the manufacturer's manual. 2. Calibrate the instrument following the appropriate manufacturer's manual. 3.' Make sure the instrument is reading zero and all function and range switches are set appropriately. 4. Fillaclean glass jar approximately half-full of the sample to be measured. Quickly cover the top of the jar with one or two sheets of clean aluminum foil and apply cap to seal the jar. 5. Allow headspace to develop for approximately 10 minutes. It is generally preferable to shake the sealed jar for 10 to 15 seconds at the beginning and end of headspace development. Note: When the ambient temperature is below 0°C (32°F), the headspace development and subsequent measurement shall occur within a heated vehicle or building. 6. Remove the jar cap and quickly puncture the foil and insert the instrument probe to a point approximately one-half of the headspace depth. Do not let the probe contact the soil. If using a PID and there is condensation on the inside of the jar, only leave the probe in the jar long enough to obtain a reading. Remove the probe and allow fresh air to flow through the instrument to avoid excess water vapor to build up. 7. Read the organic vapor concentration in ppm from the instrument display. Apply the appropriate correction factor if necessary. Record the highest instrument response. 8. Immediately record the reading in the field logbook or on the appropriate field form. 6.0 Restrictions/Limitations The two methods outlined above are the most commonly used for field measurement of organic vapors but do not apply to all circumstances. Consult project- or program-specific procedures and guidelines for deviations. Both the PID and FID provide quantitative measurement of organic vapors, but generally neither instrument is compound-specific. The typical reading range of the PID is 0 to 2,000 ppm, and the typical reading range of the FID is 0 to 1,000 ppm. The FID will measure methane while the PID will not. Note: The presence of methane will cause erratic PID measurements. In methane rich environments, toxic organic vapors shall be monitored with an FID. If desired, a charcoal filter can be placed temporarily on the FID inlet probe, which will trap all organic vapors except methane. The filtered (methane only) reading can be subtracted from unfiltered (total organic vapors) to provide an estimate of non-methane organic vapors. The reading accuracy of both instruments can be affected by ambient temperature, barometric pressure, humidity, lithology, etc. 7.0 References Martin Marietta Energy Systems, Inc. 1998. Environmental Surveillance Procedures Quality Control Program, ESH/Sub/87-21706/1. CDM Technical Standard Operating Procedures Page 3 of 3 TSOP 1-10 32607 CONTRACT-SPECIFIC CLARIFICATION SOP No.: 2-1 Revision: 3 SOP Title: PACKAGING AND SHIPPING OF ENVIRONMENTAL __ Date: October 20, 2004 _SAMPLES OA Review: Abed, Approved and Issued: ” Of d) / +f L OF ARES 77 Signature, / Date Contract No.: RAC II Client: EPA Region II Reason for Clarification: Make SOP EPA Region II - Specific 1.3 REQUIRED EQUIPMENT Add to the list of equipment: e Paint can-type metal cans with lids, clean (optional) 14 PROCEDURES Under Step 2, add: Clean to the description of the cooler used to transport samples. Under Step 4, add: - If bubble wrap or other wrapping material will be placed around the labeled containers, write the sample number and analysis on the outside of the wrap, and then place wrapped container in a plastic zip-top bag and close the bag. if the sample is known to contain dioxin, all such sample bottles will be placed in waterproof plastic bags and then placed in a metal can (paint can). Vermiculite will be used to secure the bottles within the metal can, and clips or tape will be used to permanently hold the can lid tightly in place. One bottle is packed per can. The metal cans will be labeled as the sample bottle is labeled. High level samples will not be cooled to 49 centigrade, - Note: A labeled cooler temperature blank must be added to each cooler. Under Step 4, remove the sentence: “Optionally, place three to six VOA vials in a quart metal can and then fill the can with vermiculite or equivalent”. - If samples are determined to be of medium or high hazard by visual observation or instrument reading, or CDM FEDERAL PROGRAMS CORPORATION Technical Standard Operating Procedures TSOP-2-1.RAC CONTRACT-SPECIFIC CLARIFICATION SOP No:: 2-1 Revision: 3 SOP Title: PACKAGING AND SHIPPING OF ENVIRONMENTAL Date: October 20, 2004 SAMPLES Under Step 9, add: At least two custody seals must be attached to each cooler at diagonally opposing corners. Under Step 10, add: The outside of the cooler must be marked "Environmental Samples” if the samples are designated “Low- Level.” Bills of Lading (DOT shipping papers) are required only for shipment of medium- or high-level samples. Shipment of medium- or high-level samples are as per the Contract Laboratory Program (CLP) Guidance for Field Samplers (June 2001). 8.0 REFERENCES Remove: U.S, Environmental Protection Agency, Sampler’s Guide to the Contract Laboratory Program, EPA/540/P- 90/006, December 1990. Add: U.S. Environmental Protection Agency. 2004. Contract Laboratory Program (CLP) Guidance for Field Samplers, Final. EPA-540-R-00-003. August. CDM FEDERAL PROGRAMS CORPORATION Technical Standard Operating Procedures TSOP-2-1.RAC Prepared: Krista Lippoldt Technical Review: Chuck Myers TE signed by Michgel Maloy Wales Mat” QA Review: _Jo Nell Mullins Approved: === Sse 4} E-Signed by P. Michagi Schyan > Signature/Date Issued: - —- —! Signature/Date 1.0 Objective The objective of this SOP is to outline the requirements for the packaging and shipment of environmental samples. Additionally, Sections 2.0 through 7.0 outline requirements for the packaging and shipping of regulated environmental samples under the Department of Transportation (DOT) Hazardous Materials Regulations, the International Air Trans- portation Association (IATA), and International Civil Aviation Organization (ICAO) Dangerous Goods Regulations for shipment by air and applies only to domestic shipments. This SOP does not cover the requirements for packaging and shipment of equipment (including data loggers and self-contained breathing apparatus [SCBAs] or bulk chemicals that are regulated under the DOT, IATA, and ICAO. 1.1 Packaging and Shipping of All Samples This standard operating procedure (SOP) applies to the packaging and shipping of all environmental samples. If the sample is preserved or radioactive, the following sections may also be applicable. Section 2.0 - Packaging and Shipping Samples Preserved with Methanol Section 3.0 - Packaging and Shipping Samples Preserved with Sodium Hydroxide Section 4.0 - Packaging and Shipping Samples Preserved with Hydrochloric Acid Section 5.0 - Packaging and Shipping Samples Preserved with Nitric Acid Section 6.0 - Packaging and Shipping Samples Preserved with Sulfuric Acid Section 7.0 - Packaging and Shipping Limited-Quantity Radioactive Samples 1.2 Background 1.2.1 Definitions Environmental Sample - An aliquot of air, water, plant material, sediment, or soil that represents the contaminant levels on a site. Samples of potential contaminant sources, like tanks, lagoons, or non-aqueous phase liquids are normally not “environmental” for this purpose. This procedure applies only to environmental samples that contain less than reportable quantities for any foreseeable hazardous constituents according to DOT regulations promulgated in 49 CFR - Part 172.101 Appendix A. Custody Seal - A custody seal is a narrow adhesive-backed seal that is applied to individual sample containers and/or the container (i.¢., cooler) before offsite shipment. Custody seals are used to demonstrate that sample integrity has not been compromised during transportation from the field to the analytical laboratory. Inside Container - The container, normally made of glass or plastic, that actually contacts the shipped material. Its purpose is to keep the sample from mixing with the ambient environment. Outside Container - The container, normally made of metal or plastic, that the transporter contacts. Its purpose is to protect the inside container. Secondary Containment - The outside container provides secondary containment if the inside container breaks (i.¢., plastic overpackaging if liquid sample is collected in glass). CDM Technical Standard Operating Procedures Page 1 of 17 TSOP 2-1,32607 ee) he ni Excepted Quantity - Excepted quantities are limits to the mass or volume of a hazardous material in the inside and outside containers below which DOT, IATA, ICAO regulations do not apply. The excepted quantity limits are very low. Most regulated shipments will be made under limited quantity. Limited Quantity - Limited quantity is the maximum amount of a hazardous material below which there are specific labeling or packaging exceptions. Performance Testing - Performance testing is the required testing of outer packaging. These tests include drop and stacking tests. Qualified Shipper - A qualified shipper is a person who has been adequately trained to perform the functions of shipping hazardous materials. 1.2.2 Associated Procedures = CDM Federal SOP 1-2, Sample Custody 1.2.3 Discussion Proper packaging and shipping is necessary to ensure the protection of the integrity of environmental samples shipped for analysis. These shipments are potentially subject to regulations published by DOT, IATA, or ICAO. Failure to abide by these rules places both CDM and the individual employee at risk of serious fines. The analytical holding times for the samples must not be exceeded. The samples shall be packed in time to be shipped for overnight delivery. Make arrangements with the laboratory before sending samples for weekend delivery. uf 3 Required Equipment = Coolers with return address of the appropriate CDM office = Bubble wrap (optional) » Heavy-duty plastic garbage bags # Ice # Plastic zip-type bags, small and large = Custody seals » Clear tape = Completed chain-of-custody record or contract labora- ® Nylon reinforced strapping tape tory program (CLP) custody records, if applicable = Duct tape = Completed bill of lading a 5 Vermiculite (or an equivalent nonflammable material that is “This End Up” and directional arrow labels inert and absorbent)* *Check for any client-specific or laboratory requirements related to the use of absorbent packaging materials. 1.4 Packaging Environmental Samples The following steps must be followed when packing sample bottles and jars for shipment: 1. Verify the samples undergoing shipment meet the definition of “environmental sample” and are not a hazardous material as defined by DOT. Professional judgment and/or consultation with qualified persons such as the appropriate health and safety coordinator or the health and safety manager shall be observed. 2. Select a sturdy cooler in good repair. Tape any interior opening in the cooler (drain plug) from the inside to ensure control of interior contents. Also, tape the drain plug from the outside of the cooler. Line the cooler with a large heavy- duty plastic garbage bag. 3. Be sure the caps on all bottles are tight (will not leak); check to see that labels and chain-of-custody records are completed properly (SOP 1-2, Sample Custody), 4. Place all bottles in separate and appropriately sized plastic zip-top bags and close the bags. Up to three VOA vials may be packed in one bag. Binding the vials together with a rubber band on the outside of the bag, or separating them so that they do not contact each other, will reduce the risk of breakage. Bottles may be wrapped in bubble wrap. Optionally, place three to six VOA vials in a quart metal can and then fill the can with vermiculite or equivalent. Note: Trip blanks must be included in coolers containing VOA samples. CDM Technical Standard Operating Procedures Page 2 of 17 TSOP 2-1.32507 5. Place 2 to 4 inches of vermiculite (or equivalent) into a cooler that has been lined with a garbage bag, and then place the bottles and cans in the bag with sufficient space to allow for the addition of packing material between the bottles and cans. It is preferable to place glass sample bottles and jars into the cooler vertically. Glass containers are less likely to break when packed vertically rather than horizontally. 6. While placing sample containers into the cooler, conduct an inventory of the contents of the shipping cooler against the chain-of-custody record. The chain-of-custody with the cooler shall reflect only those samples within the cooler. 7. Putice in large plastic zip-top bags (double bagging the zip-tops is preferred) and properly seal. Place the ice bags on top of and/or between the samples. Several bags of ice are required (dependant on outdoor temperature, staging time, etc.) to maintain the cooler temperature at approximately 4° Celsius (C) if the analytical method requires cooling. Fill all remaining space between the bottles or cans with packing material. Securely fasten the top of the large garbage bag with fiber or duct tape. 8. Place the completed chain-of-custody record or the CLP traffic report form (if applicable) for the laboratory into a plastic zip-top bag, seal the bag, tape the bag to the inner side of the cooler lid and close the cooler. 9. The cooler lid shall be secured with nylon reinforced strapping tape by wrapping each end of the cooler a minimum of two times. Attach a completed chain-of-custody seal across the opening of the cooler on opposite sides. The custody seals shall be affixed to the cooler with half of the seal on the strapping tape so that the cooler cannot be opened without breaking the seal. Complete two more wraps around with fiber tape and place clear tape over the custody seals. 10. The shipping container lid must be marked “THIS END UP” and arrow labels that indicate the proper upward position of the container shall be affixed to the cooler. A label containing the name and address of the shipper (CDM) shall be placed on the outside of the container. Labels used in the shipment of hazardous materials (such as Cargo Only Air Craft, Flammable Solids, etc.) are not permitted on the outside of containers used to transport environmental samples and shall not be used. The name and address of the laboratory shall be placed on the container, or when shipping by common courier, the bill of lading shall be completed and attached to the lid of the shipping container. 2.0 Packaging and Shipping Samples Preserved with Methanol 2.1 Containers » The maximum volume of methanol in a sample container is limited to 30 ml. = The sample container must not be full of methanol. 2.2 Responsibility Itis the responsibility of the qualified shipper to: » Ensure that the samples undergoing shipment contain no other contaminant that meets the definition of “hazardous material” as defined by DOT = Determine the amount of preservative in each sample so that accurate determination of quantities can be made Note: Responsibilities may vary from site to site. Therefore, all field team member responsibilities shall be defined in the field plan or site-/project-specific quality assurance project plan (QAPP). 2.3 Additional Required Equipment The following equipment is needed in addition to the required equipment listed in Section 1.3: Inner packing may consist of glass or plastic jars Outer packaging (for limited quantities) insulated cooler that has passed the ICAO drop test Survey documentation (if shipping from Department of Energy [DOE] or radiological sites) Class 3 flammable liquid labels Orientation labels Consignor/consignee labels CDM Technical Standard Operating Procedures Page 3 of 17 TSOP 2-1.32807 Packaging and Shipping Environmenta 2.4 Packaging Samples Preserved with Methanol The following steps are to be followed when packaging limited-quantity sample shipments: = Tape any interior opening in the cooler (drain plug) from the inside to ensure control of interior contents. Also, tape the drain plug from the outside of the cooler. = All sample containers will be properly labeled and the label protected with waterproof tape before sampling. a Ata minimum the label must contain: Project name - Sample identification number Project number - Collector's initials Date and time of sample collection - Preservative (note amount of preservative used in miscellaneous section of Sample location the chain-of-custody form) = Wrap each container (40-ml VOA vials) in bubble wrap (secure with waterproof tape) to prevent breakage. = Place the bubble-wrapped container into a 2.7-mil zip-type bag, removing trapped air. Place wrapped containers inside a polyethylene bottle filled with vermiculite; seal the bottle. (Maximum of 4 VOA vials will fit inside a 500-ml wide-mouth polyethylene bottle.) Total volume of methanol per shipping container must not exceed 500 ml. Place sufficient amount of vermiculite in the bottom of the cooler to absorb any leakage that may occur. Place a garbage bag in the cooler. Pack the samples appropriately inside the garbage bag (bottles placed upright) to prevent movement during shipment, Place a sufficient amount of double-bagged ice around the samples to maintain the required temperature during shipment. Seal the garbage bag by tieing or taping. The maximum weight of the cooler shall not exceed 30 kg (66 Ibs) for any limited-quantity shipment of dangerous goods. Secure the chain-of-custody form (placed inside a zip-type bag) to the interior of the cooler lid. If the shipment is from a DOE or other facility, place the results of the radiation screen and cooler/sample survey with the chain-of-custody. « Wrap strapping tape or duct tape around both ends of the cooler and around the cooler lid. = Affix custody seals to opposite sides of the cooler lid. Cover the custody seals with clear waterproof tape. » Mark the outside of the cooler with the proper shipping name of the contents, corresponding UN number, and LTD. QTY. (as shown below), Methanol Mixture UN1230 LTD. QTY. = Place a label on the front of the cooler with the company name, contact name, phone number, full street address, and state with zip code for both shipper and recipient. a Affix a Flammable Liquid label to the outside of the cooler. » Affix package orientation labels on two opposite sides of the cooler. = Secure the marking and labels to the surface of the cooler with clear waterproof tape to prevent accidental removal during shipment. = An example of cooler labeling/marking locations is shown in Figure 1. Note: No marking or labeling can be obscured by strapping or duct tape. Note: The inner packaging of dangerous goods must be placed into the designated cooler for shipment. Other nonregulated environmental samples may be added to the cooler for shipment. 8 When shipping from a DOE facility, the cooler will be surveyed by a qualified radiation control technician to ensure that radiation flux on exterior surfaces does not exceed 0.5 mrem/h on all sides. This survey will be documented and the results reviewed by the qualified shipper. « Complete the Dangerous Goods and Hazardous Materials Inspection Checklist for Shipping Limited-Quantity (Appendix A). =" Complete a Dangerous Goods Airbill. CDM Technical Standard Operating Procedures Page 4 of 17 TSOP 2-1.32807 Figure 1 Example of Cooler Label/Marking Locations Address Label Tt =F ee Strapping—_ | [To: x pa TT) Tape From: -. Methanol Mixture UN1230 LTD. arg \ Taped \ Drain Orientation Labels \ Proper Shipping Name anh Number ~ Hazard Class Label 3.0 Packaging and Shipping Samples Preserved with Sodium Hydroxide 3.1 Containers The inner packaging container (and amount of preservative) that may be used for these shipments includes: Excepted Quantities of Sodium Hydroxide Preservatives Pi HR ee AS jer ree 8) eee cue Specified Ce ar ARIS} pH Conc. 40m! | 125ml | 250ml | 500ml | 1L NaOH | 30% >12 | 0.08% 25 0.5 1 2 5 drops = 1 ml 3.2 Responsibility It is the responsibility of the qualified shipper to determine the amount of preservative in each sample so that accurate determination of quantities can be made. Note: Responsibilities may vary from site to site. Therefore, all field team member responsibilities shall be defined in the field plan or site-/project-specific quality assurance project plan (QAPP). 3.3 Additional Required Equipment The following equipment is needed in addition to the required equipment listed in Section 1.3: Outer packaging (for limited quantities) insulated cooler that has passed the ICAO drop test Inner packings may consist of glass or plastic jars no larger than 1 pint Survey documentation (if shipping from DOE or radiological sites) Class 8 corrosive labels Orientation labels Consignor/consignee labels CDM Technical Standard Operating Procedures ; Page 5 of 17 TSOP 2-1,32807 3.4 Packaging Samples Preserved with Sodium Hydroxide Samples containing NaOH as a preservative that exceed the excepted concentration of 0.08 percent (2 ml of a 30 percent NaOH solution per liter) may be shipped as a limited quantity per packing instruction Y819 of the IATA/ICAO Dangerous Goods Regulations. The following steps are to be followed when packaging limited-quantity samples shipments: = Tape any interior opening in the cooler (drain plug) from the inside to ensure control of interior contents. Also, tape the drain plug from the outside of the cooler. » All sample containers will be properly labeled and the label protected with waterproof tape before sampling. = Ataminimum the label must contain: Project name - Sample identification number Project number - Collector's initials Date and time of sample collection - Preservative (note amount of preservative used in miscellaneous section of Sample location the chain-of-custody form) This step is optional; wrap each container in bubble wrap (secure with waterproof tape) to prevent breakage. Place the bubble-wrapped container into a 2.7-mil zip-type bag, removing trapped air. Place glass containers inside a polyethylene bottle filled with vermiculite; seal the bottle. The total volume of sample in each cooler must not exceed 1 liter. Place sufficient amount of vermiculite in the bottom of the cooler to absorb any leakage that may occur. Place a garbage bag in the cooler. Pack the samples appropriately inside the garbage bag (bottles placed upright) to prevent movement during shipment. Place sufficient amount of double-bagged ice around the samples to maintain the required temperature during shipment. | Seal the garbage bag by tieing or taping. The maximum weight of the cooler shall not exceed 30 kg (66 Ibs) for any limited-quantity shipment of dangerous goods. Secure the chain-of-custody form (placed inside a zip-type bag) to the interior of the cooler lid. If the shipment is from a DOE or other facility, place the results of the radiation screen and cooler/sample survey with the chain-of-custody. Wrap strapping tape or duct tape around both ends of the cooler and around the cooler lid. Affix custody seals to opposite sides of the cooler lid. Cover the custody seals with clear waterproof tape. = Mark the outside of the cooler with the proper shipping name of the contents, corresponding UN number, and LTD, QTY. (as shown below). Sodium Hydroxide Solution UN1824 LTD. QTY. = Place a label on the front of the cooler with the company name, contact name, phone number, full street address, and state with zip code for both shipper and recipient. = Affix a Corrosive label to the outside of the cooler. " Affix package orientation labels on two opposite sides of the cooler. = Secure the marking and labels to the surface of the cooler with clear waterproof tape to prevent accidental removal during shipment. = An example of cooler labeling/marking locations is shown in Figure 1. Note: Samples meeting the exception concentration of 0.08 percent NaOH by weight may be shipped as nonregulated or nonhazardous following the procedure in Section 1.4. Note: No marking or labeling can be obscured by strapping or duct tape. Note: The inner packaging of dangerous goods must be placed into the designated cooler for shipment. Other nonregulated environmental samples may be added to the cooler for shipment. CDM Technical Standard Operating Procedures Page 6 of 17 TSOP 2-1,32807 = When shipping from a DOE facility, the cooler will be surveyed by a qualified radiation control technician to ensure that radiation flux on exterior surfaces does not exceed 0.5 mrem/h on all sides. This survey will be documented and the results reviewed by the qualified shipper. " Complete the Dangerous Goods and Hazardous Materials Inspection Checklist for Shipping Limited-Quantity (Appendix A). » Complete a Dangerous Goods Airbill. 4.0 Packaging and Shipping Samples Preserved with Hydrochloric Acid 4.1 Containers The inner packaging container (and amount of preservative) that may be used for these shipments includes: ric Acid Preservatives |) Quantity of Preservative (ml) HCl | 2N <1.96 0.04% 2 5 1 5 drops = 1 ml 4.2 Responsibility It is the responsibility of the qualified shipper to: ® Determine the samples undergoing shipment contain no other contaminant that meets the definition of hazardous material as defined by DOT = Determine the amount of preservative in each sample so that accurate determination of quantities can be made Note: Responsibilities may vary from site to site. Therefore, all field team member responsibilities shall be defined in the field plan or site-/project-specific quality assurance project plan (QAPP). 4.3 Additional Required Equipment The following equipment is needed in addition to the required equipment listed in Section 1.3. Inner packing may consist of glass or plastic jars no larger than 1 pint. Outer packaging (for limited quantities) insulated cooler that has passed the ICAO drop test. Survey documentation (if shipping from DOE or radiological sites) Class 8 corrosive labels Orientation labels Consignor/consignee labels 4.4 Packaging Samples Preserved with Hydrochloric Acid The following steps are to be followed when packaging limited-quantity sample shipments: ® Tape any interior opening in the cooler (drain plug) from the inside to ensure control of interior contents. Also, tape the drain plug from the outside of the cooler. # All sample containers will be properly labeled and the label protected with waterproof tape before sampling. =» Ata minimum the label must contain: Project name - Sample identification number Project number - Collector's initials Date and time of sample collection - Preservative (note amount of preservative used in miscellaneous section of Sample location the chain-of-custody form) = Wrap each container (40-ml VOA vials) in bubble wrap (secure with waterproof tape) to prevent breakage. « Place the bubble-wrapped container into a 2.7-mil zip-type bag, removing trapped air. = Place wrapped containers inside a polyethylene bottle filled with vermiculite; seal the bottle. (No more than 4 VOA vials will fit inside a 500-ml wide-mouth polyethylene bottle.) CDM Technical Standard Operating Procedures Page 7 of 17 TSOP 2-1.32607 ipping E =hvironmen ital Sample 3S Total volume of sample inside each cooler must not exceed 1 liter. Place sufficient amount of vermiculite in the bottom of the cooler to absorb any leakage that may occur. Place a garbage bag in the cooler. Pack the samples appropriately inside the garbage bag (bottles placed upright) to prevent movement during shipment. Place sufficient amount of double-bagged ice around the samples to maintain the required temperature during shipment. Seal the garbage bag by tieing or taping. The maximum weight of the cooler shall not exceed 30 kg (66 Ibs) for any limited-quantity shipment of dangerous goods. Secure the chain-of-custody form (placed inside a zip-type bag) to the interior of the cooler lid. If the shipment is from a DOE or other facility, place the results of the radiation screen and cooler/sample survey with the chain-of-custody. = Wrap strapping tape or duct tape around both ends of the cooler and around the cooler lid. s Affix custody seals to opposite sides of the cooler lid. Cover the custody seals with clear waterproof tape. Mark the outside of the cooler with the proper shipping name of the contents, corresponding UN number, and LTD. QTY. (as shown below). Hydrochloric Acid Solution UN1789 LTD. QTY. Place a label on the front of the cooler with the company name, contact name, phone number, full street address, and state with zip code for both shipper and recipient. a Affix a Corrosive label to the outside of the cooler. u Affix package orientation labels on two opposite sides of the cooler. " Secure the marking and labels to the surface of the cooler with clear waterproof tape to prevent accidental removal during shipment. An example of cooler labeling/marking locations is shown in Figure 1. Note: Samples containing less than the exception concentration of 0.04 percent HCI by weight will be shipped as nonregulated or nonhazardous following the procedure in Section 1.4. Note: No marking or labeling can be obscured by strapping or duct tape. Note: The inner packaging of dangerous goods must be placed into the designated cooler for shipment. Other nonregulated environmental samples may be added to the cooler for shipment. When shipping from a DOE facility, the cooler will be surveyed by a qualified radiation control technician to ensure that radiation flux on exterior surfaces does not exceed 0.5 mrem/h on all sides. This survey will be documented and the results reviewed by the qualified shipper. Complete the Dangerous Goods and Hazardous Materials Inspection Checklist for Shipping Limited-Quantity (Appendix A). # Complete a Dangerous Goods Airbill. 5.0 Packaging and Shipping Samples Preserved with Nitric Acid 5.1 Containers The inner packaging container (and amount of preservative) that may be used for these shipments includes: excepted Quantities of Nitric Acid Preservatives PS ee | a Pesired int Final] 1a he re: - Quantity of Preservative (ml), for Nis _ Preservative Sample | Specified Container Ah et pH Conc. 40 ml 125 ml 250 ml 500 ml 4L HNO; | 6N <1.62 | 0.15% 2 4 5 8 5 drops = 1 mg/L CDM Technical Standard Operating Procedures Page 8 of 17 TSOP 2-4 32807 5.2 Responsibility It is the responsibility of the qualified shipper to: ® Determine the samples undergoing shipment contain no other contaminant that meets the definition of hazardous material as defined by DOT » Determine the amount of preservative in each sample so that accurate determination of quantities can be made Note: Responsibilities may vary from site to site. Therefore, all field team member responsibilities shall be defined in the field plan or site-/project-specific quality assurance project plan (QAPP). 5.3 Additional Required Equipment The following equipment is needed in addition to the required equipment listed in Section 1.3: Inner packings may consist of glass or plastic jars no larger than 100 ml. Outer packaging (for limited quantities) insulated cooler that has passed the ICAO drop test. Survey documentation (if shipping from DOE or radiological sites) Class 8 corrosive labels Orientation labels Consignor/consignee labels 5.4 Packaging Samples Preserved with Nitric Acid Samples containing HNO; as a preservative that exceed the excepted concentration of 0.15 percent HNO; will be shipped as a limited quantity per packing instruction Y807 of the IATA/ICAO Dangerous Goods Regulations. The following steps are to be followed when packaging limited-quantity sample shipments: " Tape any interior opening in the cooler (drain plug) from the inside to ensure control of interior contents. Also, tape the drain plug from the outside of the cooler. # All sample containers will be properly labeled and the label protected with waterproof tape before sampling. # Ataminimum the label must contain: Project name - Sample identification number Project number - Collector's initials Date and time of sample collection - Preservative (note amount of preservative used in miscellaneous section of Sample location the chain-of-custody form) This step is optional; wrap each container in bubble wrap (secure with waterproof tape) to prevent breakage. Place the bubble-wrapped container into a 2.7-mil zip-type bag, removing trapped air. Place glass containers inside a polyethylene bottle filled with vermiculite; seal the bottle. Place sufficient amount of vermiculite in the bottom of the cooler to absorb any leakage that may occur. Place a garbage bag in the cooler. “Pack the samples appropriately inside the garbage bag (bottles placed upright) to prevent movement during shipment. Place sufficient amount of double-bagged ice around the samples to maintain the required temperature during shipment. Seal the garbage bag by tieing or taping. The maximum volume of preserved solution in the cooler must not exceed 500 ml. The maximum weight of the cooler shall not exceed 30 kg (66 Ibs) for any limited-quantity shipment of dangerous goods. Secure the chain-of-custody form (placed inside a zip-type bag) to the interior of the cooler lid. If the shipment is from a DOE or other facility, place the results of the radiation screen and cooler/sample survey with the chain-of-custody. « Wrap strapping tape or duct tape around both ends of the cooler and around the cooler lid. » Affix custody seals to opposite sides of the cooler lid. Cover the custody seals with clear waterproof tape. » Mark the outside of the cooler with the proper shipping name of the contents, corresponding UN number, and LTD. QTY. (as shown below). CDM Technical Standard Operating Procedures Page 9 of 17 TSOP 2-1.32507 Nitric Acid Solution (with less than 20 percent) UN2031 Ltd. Qty. = Place a label on the front of the cooler with the company name, contact name, phone number, full street address, and state with zip code for both shipper and recipient. " Affix a Corrosive label to the outside of the cooler. s Affix package orientation labels on two opposite sides of the cooler. = Secure the marking and labels to the surface of the cooler with clear waterproof tape to prevent accidental removal during shipment. = An example of cooler labeling/marking locations is shown in Figure 1. Note: Samples meeting the exception concentration of 0.15 percent HNO by weight will be shipped as nonregulated or nonhazardous following the procedure in Section 1.4. Note: No marking or labeling can be obscured by strapping or duct tape. Note: The inner packaging of dangerous goods must be placed into the designated cooler for shipment. Other nonregulated environmental samples may be added to the cooler for shipment. = When shipping from a DOE facility, the cooler will be surveyed by a qualified radiation control technician to ensure that radiation flux on exterior surfaces does not exceed 0.5 mrem/h on all sides. This survey will be documented and the results reviewed by the qualified shipper. = Complete the Dangerous Goods and Hazardous Materials Inspection Checklist for Shipping Limited-Quantity (Appendix A). » Complete a Dangerous Goods Airbill. 6.0 Packaging and Shipping Samples Preserved with Sulfuric Acid 6.1 Containers The inner packaging container (and amount of preservative) that may be used for these shipments includes: Excepted Quantities of Sulfuric Acid ese ates esired in. ; 7 antity of Preservative e (mi) f for. ; Re ive > ni ey 3 Specified. ee ainer 7 Conc. 40 ml 125 ml 250 ml 500 ml 4L H2SO4, | 37N mai a | 0.35% yi BS 0.5 1 2 5 drops = 1 ml 6.2 Responsibility It is the responsibility of the qualified shipper to: « Determine the samples undergoing shipment contain no other contaminant that meets the definition of hazardous material as defined by DOT = Determine the amount of preservative in each sample so that accurate determination of quantities can be made Note: Responsibilities may vary from site to site. Therefore, all field team member responsibilities shall be defined in the field plan or site-/project-specific quality assurance project plan (QAPP). 6.3 Additional Required Equipment The following equipment is needed in addition to the required equipment listed in Section 1.3: CDM Technical Standard Operating Procedures Page 10 of 17 TSOP 2-1 32807 Inner packings may consist of glass or plastic jars no larger than 100 ml. Outer packaging (for limited quantities) insulated cooler that has passed the ICAO drop test. Survey documentation (if shipping from DOE or radiological sites) Class 8 corrosive labels Orientation labels Consignor/consignee labels 6.4 Packaging of Samples Preserved with Sulfuric Acid Samples containing H,SO, as a preservative that exceed the excepted concentration of 0.35 percent will be shipped as a limited quantity per packing instruction Y809 of the IATA/ICAO Dangerous Goods Regulations. The following steps are to be followed when packaging limited-quantity samples shipments: ® Tape any interior opening in the cooler (drain plug) from the inside to ensure control of interior contents. Also, tape the drain plug from the outside of the cooler. = All sample containers will be properly labeled and the label protected with waterproof tape before sampling. » Ata minimum the label must contain: Project name - Sample identification number Project number - Collector's initials Date and time of sample collection - Preservative (note amount of preservative used in miscellaneous section of Sample location the chain-of-custody form) Wrap each glass container in bubble wrap (secure with waterproof tape) to prevent breakage. Place the bubble-wrapped container into a 2.7-mil zip-type bag, removing trapped air. Place glass containers inside a polyethylene bottle filled with vermiculite; seal the bottle. Place sufficient amount of vermiculite in the bottom of the cooler to absorb any leakage that may occur, Place a garbage bag in the cooler. Pack the samples appropriately inside the garbage bag (bottles placed upright) to prevent movement during shipment. Place sufficient amount of double-bagged ice around the samples to maintain the required temperature during shipment. Seal the garbage bag by tieing or taping. The maximum volume of preserved solution in the cooler must not exceed 500 ml. The maximum weight of the cooler shall not exceed 30 kg (66 Ibs) for any limited-quantity shipment of dangerous goods. Secure the chain-of-custody form (placed inside a zip-type bag) to the interior of the cooler lid. If the shipment is from a DOE or other facility, place the results of the radiation screen and cooler/sample survey with the chain-of-custody. Wrap strapping tape or duct tape around both ends of the cooler and around the cooler lid. " Affix custody seals to opposite sides of the cooler lid. Cover the custody seals with clear waterproof tape. » Mark the outside of the cooler with the proper shipping name of the contents, corresponding UN number, and LTD. QTY. (as shown below). Sulfuric Acid Solution UN2796 LTD. QTY. ® Place a label on the front of the cooler with the company name, contact name, phone number, full street address, and state with zip code for both shipper and recipient. a Affix a Corrosive label to the outside of the cooler. « Affix package orientation labels on two opposite sides of the cooler. = Secure the marking and labels to the surface of the cooler with clear waterproof tape to prevent accidental removal during shipment. = An example of cooler labeling/marking locations is shown in Figure 1. CDM Technical Standard Operating Procedures Page 11 of 17 TSOP 2-4 32807 Note: Samples containing less than the exception concentration of 0.35 percent H2SO, by weight will be shipped as nonregulated or nonhazardous in accordance with the procedure described in Section 1.4. Note: No marking or labeling can be obscured by strapping or duct tape. Note: The inner packaging of dangerous goods must be placed into the designated cooler for shipment. Other nonregulated environmental samples may be added to the cooler for shipment. = When shipping from a DOE facility, the cooler will be surveyed by a qualified radiation contro! technician to ensure that radiation flux on exterior surfaces does not exceed 0.5 mrem/h on all sides. This survey will be documented and the results reviewed by the qualified shipper. " Complete the Dangerous Goods and Hazardous Materials Inspection Checklist for Shipping Limited-Quantity (Appendix A). ® Complete a Dangerous Goods Airbill. 7.0 Packaging and Shipping Limited-Quantity Radioactive Samples 7.1 Containers The inner packaging containers that may be used for these shipments include: « Any size sample container 7.2 Description/Responsibilities a The qualified shipper will determine that the samples undergoing shipment contain no other contaminant that meets the | definition of hazardous material as defined by DOT, = The qualified shipper will ship all samples that meet the Class 7 definition of radioactive materials and meet the activity requirements specified in Table 7 of 49 CFR 173.425, as Radioactive Materials in Limited Quantity. The qualified shipper will verify that all packages and their contents meet the requirements of 49 CFR 173.421, Limited Quantities of Radioactive Materials. = The packaging used for shipping will meet the general requirements for packaging and packages specified in 49 CFR 173.24 and the general design requirements provided in 173.410. These standards state that a package must be capable of withstanding the effects of any acceleration, vibration, or vibration resonance that may arise under normal condition of transport without any deterioration in the effectiveness of the closing devices on the various receptacles or in the integrity of the package as a whole and without loosening or unintentionally releasing the nuts, bolts, or other securing devices even after repeated use. " Ifthe shipment is from a DOE facility, radiological screenings will be completed on all samples taken. The qualified shipper will review the results of each screening (alpha, beta, and gamma speciation). Samples will not be shipped offsite until the radiological screening has been performed. 8 The total activity for each package will not exceed the relevant limits listed in Table 7 of 49 CFR 173.425. The A: value of the material will be calculated based on all radionuclides found during previous investigations (if any) in the area from which the samples are derived. The A2 values to be used will be the most restrictive of all potential radionuclides as listed in 49 CFR 173.435. = The radiation level at any point on the external surface of the package bearing the sample(s) will not exceed 0.005 mSv/hour (0.5 mrem/hour). These will be verified by dose and activity monitoring before shipment of the package. # The removable radioactive surface contamination on the external surface of the package will not exceed the limits specified in 49 CFR 173.443(a). CDM will apply the DOE-established free release criteria for removable surface contamination of less than 20 dpm/100 cm? (alpha) and 1,000 dpm/100 cm? (beta/gamma). It shall be noted that these values are more conservative than the DOT requirements for removable surface contamination. # The qualified shipper will verify that the outside of the inner packaging is marked “Radioactive.” u The qualified shipper will verify that the excepted packages prepared for shipment under the provisions of 49 CFR 173.421 have a notice enclosed, or shown on the outside of the package, that reads, “This package conforms to the conditions and limitations specified in 49 CFR 173.421 for radioactive material, excepted package-limited quantity of material, UN2910.” CDM Technical Standard Operating Procedures Page 12 of 17 TSOP 2.132207 Note: Responsibilities may vary from site to site. Therefore, all field team member responsibilities shall be defined in the field plan or site-/project-specific quality assurance project plan (QAPP). 7.3 Additional Required Equipment The following equipment is needed in addition to the required equipment listed in Section 1.3: Survey documentation/radiation screening results (if shipping from DOE or radiological sites) Orientation labels Excepted quantities label Consignor/consignee labels 7.4 Packaging of Limited-Quantity Radioactive Samples The following steps are to be followed when packaging limited-quantity sample shipments: " The cooler is to be surveyed by a qualified radiation control technician to ensure that radiation flux on exterior surfaces does not exceed 0.5 mrem/h on all sides. This survey will be documented and the results reviewed by the qualified shipper. # Tape any interior opening in the cooler (drain plug) from the inside to ensure control of interior contents, Also, tape the drain plug from the outside of the cooler. » All sample containers will be properly labeled and the label protected with waterproof tape before sampling. a Ataminimum the label must contain: Project name - Sample location Project number - Sample identification number - Date and time of sample collection - Collector's initials " This step is optional; wrap each container in bubble wrap (secure with waterproof tape) to prevent breakage. » Place sufficient amount of vermiculite, or approved packaging material, in the bottom of the cooler to absorb any leakage that may occur. a Place a garbage bag in the cooler. » Pack the samples appropriately inside the garbage bag (bottles placed upright) to prevent movement during shipment. " If required, place a sufficient amount of double-bagged ice around the samples to maintain the required temperature during shipment. » Seal the garbage bag by tieing or taping. » Place a label marked Radioactive on the outside of the sealed bag. » Enclose a notice that includes the name of the consignor or consignee and the following statement: “This package conforms to the conditions and limitations specified in 49 CFR 173.421 for radioactive material, excepted package-limited quantity of material, UN2910.” Note that both DOT and IATA apply different limits to the quantity in the inside packing and in the outside packing. The maximum weight of the package shall not exceed 30 kg (66 Ibs) for any limited-quantity shipment of dangerous goods. Secure the chain-of-custody form (placed inside a zip-type bag) to the interior of the cooler lid. If the shipment is from a DOE or other facility, place the results of the radiation screen and cooler/sample survey with the chain-of-custody. » |facooler is used, wrap strapping tape or duct tape around both ends of the cooler and around the cooler lid. « Affix custody seals to opposite sides of the cooler lid. Cover the custody seals with clear waterproof tape. » Place a label on the front of the cooler with the company name, contact name, phone number, full street address, and state with zip code for both shipper and recipient. a Affix package orientation labels on two opposite sides of the cooler/package. » Affix a completed Excepted Quantities label to the side of the cooler/package. » Secure any marking and labels to the surface of the cooler with clear waterproof tape to prevent accidental removal during shipment. » An example of the cooler labeling/marking is shown in Figure 2. Note: No marking or labeling can be obscured by strapping or duct tape. CDM Technical Standard Operating Procedures Page 13 of 17 TSOP 2-1.32607 and Ship ping E Envir ronme ?r = Complete the Shipment Quality Assurance Checklist (Appendix B). Note: Except as provided in 49 CFR 173.426, the package will not contain more than 15 grams of “°U. Note: A declaration of dangerous goods is not required. Figure 2 Radioactive Material — Limited-Quantity Cooler Marking Example ZZ p \ Strapping [= £ Tape °° ——. ra From This package conforms to the éonditions and limitations specified in 49 CFR 173.421 for Radioactive Material, excepted package - limited quantity of material, UN2910. Taped AN & Drain \ \ Orientation Labels Limited Quantity Notice Exempted Quantities Label 8.0 References U. S. Environmental Protection Agency. Region IV. February 1991 or current. Standard Operating Procedures and Quality Assurance Manual. . 1996 or current. Sampler’s Guide to the Contract Laboratory Program, EPA/540/R-96/032. Title 49 Code of Federal Regulations, Department of Transportation. 2005 or current revision. Hazardous Materials Table, Special Provisions, Hazardous, Materials Communications, Emergency Response Information, and Training Requirements, 49 CFR 172. Title 49 Code of Federal Regulations, Department of Transportation. 2005 or current revision. Shippers General Requirements for Shipments and Packagings, 49 CFR 173. CDM technical standard Operating Procedures Page 14 of 17 TSOP 2-1.32607 Sample Packaging Yes No WNA O QO Oo QO QO Q QO QO Q QO O QO ooo oo Air Waybill Completion Yes No QO oO oO O Oooo oOo DOO oa QO Oo oO D DeoDU Oo ooo oo N/A QO oe 2D DEGoO Oo Appendix A Dangerous Goods and Hazardous Materials Inspection Checklist for Shipping Limited-Quantity The VOA vials are wrapped in bubble wrap and placed inside a zip-type bag. The VOA vials are placed into a polyethylene bottle, filled with vermiculite, and tightly sealed. The drain plug is taped inside and outside to ensure control of interior contents. The samples have been placed inside garbage bags with sufficient bags of ice to preserve samples at 4°C. The cooler weighs less than the 66-pound limit for limited-quantity shipment. The garbage bag has been sealed with tape (or tied) to prevent movement during shipment. The chain-of-custody has been secured to the interior of the cooler lid. The cooler lid and sides have been taped to ensure a seal. The custody seals have been placed on both the front and back hinges of the cooler, using waterproof tape. Section 1 has the shipper’s name, company, and address; the account number, date, internal billing reference number; and the telephone number where the shipper can be reached. Section 2 has the recipient's name and company along with a telephone number where they can be reached. Section 3 has the Bill Sender box checked. Section 4 has the Standard Overnight box checked. Section 5 has the Deliver Weekday box checked. Section 6 has the number of packages and their weights filled out. Was the total of all packages and their weights figured up and added at the bottom of Section 6? Under the Transport Details box, the Cargo Aircraft Only box is obliterated, leaving only the Passenger and Cargo Aircraft box. Under the Shipment Type, the Radioactive box is obliterated, leaving only the Non- Radioactive box. Under the Nature and Quantity of Dangerous Goods box, the Proper Shipping Name, Class or Division, UN or ID No., Packing Group, Subsidiary Risk, Quantity and Type of Packing, Packing Instructions, and Authorization have been filled out for the type of chemical being sent. The Name, Place and Date, Signature, and Emergency Telephone Number appears at the bottom of the FedEx Airbill. The statement “In accordance with IATA/ICAO” appears in the Additional Handling Information box. The Emergency Contact Information at the bottom of the FedEx Airbill is truly someone who can respond any time of the day or night. CDM Technical Standard Operating Procedures Page 15 of 17 TSOP 2-1,32€07 Hydrochloric Acid UN1789 II 1 plastic box x 0.5L Y809 Ltd. Qty. Solution Nitric Acid Solution UN2031 I] 1 plastic box x 0.5L Y807 Ltd. Qty. (with less than 20%) Sodium Hydroxide UN1824 I 1 plastic box x 0.5L Y809 Ltd. Qty. Solution Sulfuric Acid UN2796 I 1 plastic box x 0.5 L Y809 Ltd, Qty. Solution Methanol! UN1230 iH} 1 plastic box x 1L Y305 Ltd. Qty. Sample Cooler Labeling Yes No WNA Eb Bs ob ooo oO oOo Dep, Bb eo The proper shipping name, UN number, and Ltd. Qty. appears on the shipping container. The corresponding hazard labels are affixed on the shipping container; the labels are not obscured by tape. The name and address of the shipper and receiver appear on the top and side of the shipping container. The air waybill is attached to the top of the shipping container. Up Arrows have been attached to opposite sides of the shipping container. Packaging tape does not obscure markings or labeling. CDM Technical Standard Operating Procedures TSOP 2-1.32807 Appendix B Shipment Quality Assurance Checklist Date: Shipper: Destination: Item(s) Description: Radionuclide(s): Radiological Survey Results: surface mrem/hr 1 meter Instrument Used: Mfgr: Model: S/N: Cal Date: Limited-Quantity or Instrument and Article Yes No 1. Strong tight package (package that will not leak material during conditions normally incidental to transportation). 2. Radiation levels at any point on the external surface of package less than or equal to 0.5 mrem/hr. 3, Removable surface contamination less than 20 dpm/100 cm? (alpha) and 1,000 dpm/100 cm? (beta/gamma). Outside inner package bears the marking “Radioactive.” Package contains less than 15 grams of *°°U (check yes if *°°U not present). Notice enclosed in or on the package that includes the consignor or consignee and the statement, “This package conforms to the conditions and limitations specified in 49 CFR 173.421 for radioactive material, excepted package-limited quantity of material, UN2910.” 7. Activity less than that specified in 49 CFR 173.425. Permissible package limit: Package Quantity: 8. Onall air shipments, the statement Radioactive Material, excepted package-limited quantity of material shall be noted on the air waybill. SOU Ss Qualified Shipper: Signature: CDM Technical Standard Operating Procedures Page 17 of 17 TSOP 2-1 32607 Prepared: Tim Eggert Technical Review: Matt eee os " ager C. Malloy 4 wy | QA Review: Jo Nell Mullins Approved: = [anes er signed by P. Micnasl wan eonotunbate. | ese pny gaurenupk the Pee “| Issued: <——— —s | Signature/Dale 1.0 Objective This standard operating procedure (SOP) presents guidance for the management of investigation-derived waste (IDW). The primary objectives for managing IDW during field activities include: Leaving the site in no worse condition than existed before field activities Removing wastes that pose an immediate threat to human health or the environment Proper handling of onsite wastes that do not require offsite disposal or extended aboveground containerization Complying with federal, state, local, and facility applicable or relevant and appropriate requirements (ARARs) Careful planning and coordination of IDW management options Minimizing the quantity of IDW 2.0 Background 2.1 Definitions Hazardous Waste - Discarded material that is regulated listed waste, or waste that exhibits ignitability, corrosivity, reactivity, or toxicity as defined in 40 CFR 261.3 or state regulations. Investigation-Derived Wastes - Discarded materials resulting from field activities such as sampling, surveying, drilling, excavations, and decontamination processes that, in present form, possess no inherent value or additional usefulness without treatment. Wastes may be solid, sludge, liquid, gaseous, or multiphase materials that may be classified as hazardous or nonhazardous. Mixed Waste - Any material that has been classified as hazardous and radioactive. Radioactive Wastes - Discarded materials that are contaminated with radioactive constituents with specific activities in concentrations greater than the latest regulatory criteria (i.e., 10 CFR 20). Treatment, Storage, and Disposal Facility (TSDF) - Permitted facilities that accept hazardous waste shipments for further treatment, storage, and/or disposal. These facilities must be permitted by the U. S. Environmental Protection Agency (EPA) and appropriate state and local agencies. 2.2 Discussion Field investigation activities result in the generation of waste materials that may be characterized as hazardous or radioactive waste. IDWs may include drilling muds, cuttings, and purge water from test pit and well installation; purge water, soil, and other materials from collection of samples; residues from testing of treatment technologies and pump and treat systems; personal protective equipment (PPE); solutions (aqueous or otherwise) used to decontaminate nondisposable protective clothing and equipment; and other wastes or supplies used in sampling and testing potentially hazardous or radiologically contaminated material. Note: The client’s representatives may not be aware of all potential contaminants. The management of IDW must comply with applicable regulatory requirements. 3.0 General Responsibilities Site Manager - The site manager is responsible for ensuring that all IDW procedures are conducted in accordance with this SOP. The site manager is also responsible for ensuring that handling of IDW is in accordance with site-specific requirements. Project Manager - The project manager is responsible for identifying site-specific requirements for the disposal of IDW in accordance with federal, state, and/or facility requirements. Field Crew Members - Field crew members are responsible for implementing this SOP and communicating any unusual or unplanned condition to the project manager's attention. Note: Responsibilities may vary from site to site. Therefore, all field team member responsibilities shall be defined in the field plan or site/project specific quality assurance plan. 4.0 Required Equipment Equipment required for IDW containment will vary according to site-specific/client requirements. Management decisions concerning the necessary equipment required shall consider: containment method, sampling, labeling, maneuvering, and storage (if applicable). Equipment must be onsite and inspected before commencing work. 4.1 IDW Containment Devices The appropriate containment device (drums, tanks, etc.) will depend on site- or client-specific requirements and the ultimate disposition of the IDW. Typical IDW containment devices can include: ® Plastic sheeting (polyethylene) with a minimum thickness of 20 millimeters " Department of Transportation (DOT)-approved steel containers " Polyethylene or steel bulk storage tanks Containment of IDW shall be segregated by waste type (i.e., solid or liquid, corrosive or flammable, etc.) and source location. Volume of the appropriate containment device shall be site-specific. 4.2 |IDW Container Labeling A “Waste Container’ or “IDW Container” label or indelible marking shall be applied to each container. Labeling or marking requirements for onsite IDW not expected to be transported offsite are: 8 Labels and markings that contain the following information: project name, generation date, location of waste origin, container identification number, sample number (if applicable), and contents (drill cuttings, purge water, PPE, etc.). ® Each label or marking will be applied to the upper one-third of the container at least twice, on opposite sides. ® Containers that are 5 gallons or less may only require one label or set of markings. = Labels or markings will be positioned on a smooth part of the container. The label must not be affixed across container bungs, seams, ridges, or dents. ® Labels must be constructed of a weather-resistive material with markings made with a permanent marker or paint pen and capable of enduring the expected weather conditions. If markings are used, the color must be easily distinguishable from the drum color. = Labels will be secured in a manner to ensure the label remains affixed to the container. Labeling or marking requirements for IDW expected to be transported offsite must be in accordance with the requirements of 49 CFR 172. 4.3 IDW Container Movement Staging areas for IDW containers shall be predetermined and in accordance with site-specific and/or client requirements. Arrangements shall be made before field mobilization as to the methods and personnel required to safely transport IDW containers to the staging area. Transportation offsite onto a public roadway is prohibited unless 49 CFR 172 requirements are met. | SES FOSS == = = a ee a 4.4 IDW Container Storage Containerized IDW shall be staged pending chemical analysis or further onsite treatment. Staging areas and bulk storage procedures are to be determined according to site-specific requirements. Containers are to be stored in such a fashion that the labels can be easily read. A secondary/spill container must be provided for liquid IDW storage and as appropriate for solid IDW storage. 5.0 Procedures The three general options for managing IDW are (1) collection and onsite disposal, (2) collection for offsite disposal, and (3) collection and interim management. Attachment 1 summarizes media-specific information on generation processes and management options. The option selected shall take into account the following factors: Type (soil, sludge, liquid, debris), quantity, and source of IDW Risk posed by managing the IDW onsite Compliance with regulatory requirements IDW minimization and consistency with the IDW remedy and the site remedy In all cases the client shall approve the plans for IDW. Formal plans for the management of IDW must be prepared as part of a work plan or separate document. 5.1 Collection and Onsite Disposal 5.1.1 Soil/Sludge/Sediment The options for handling soil/sludge/sediment IDW are as follows: 1. Return to boring, pit, or source immediately after generation as long as returning the media to these areas will not increase site risks (e.g., the contaminated soil will not be replaced at a greater depth than where it was originally so that it will not contaminate “clean” areas). 2. Spread around boring, pit, or source within the area of contamination (AOC) as long as returning the media to these areas will not increase site risks (e.g., direct contact with surficial contamination). 3. Consolidate in a pit within the AOC as long as returning the media to these areas will not increase site risks (e.g., the contaminated soil will not be replaced at a greater depth than where it was originally so that it will not contaminate “clean” areas). 4. Send to onsite TSDF - may require analytical analysis before treatment/disposal, Note: These options may require client and/or regulatory approval. 5.1.2 Aqueous Liquids The options for handling aqueous liquid IDW are as follows: 1. Discharge to surface water, only when IDW is not contaminated. 2. Discharge to ground surface close to the well, only if soil contaminants will not be mobilized in the process and the action will not contaminate clean areas. If IDW from the sampling of background upgradient wells is not a community concern or associated with soil contamination, this presumably uncontaminated IDW may be released on the ground around the well. 3. Discharge to sanitary sewer, only when IDW is not contaminated. 4. Send to onsite TSDF - may require analysis before treatment/disposal. Note: These options may require analytical results to obtain client and/or regulatory approval. ES to Handling Inv n 2007 5.1.3 Disposable PPE The options for handling disposable PPE are as follows: 1. Double-bag contents in nontransparent trash bags and place in onsite industrial dumpster, only if PPE is not contaminated. 2. Containerize, label, and send to onsite TSDF - may require analysis before treatment/disposal. 5.2 Collection for Offsite Disposal Before sending to an offsite TSDF, analysis may be required. Manifests are required. In some instances, a bill of lading can be used for nonhazardous solid IDW (i.e., wooden pallets, large quantities of plastic sheeting). Arrangements must be made with the client responsible for the site to sign as generator on any waste profile and all manifests or bill of ladings; it is CDM's policy not to sign manifests. The TSDF and transporter must be permitted for the respective wastes, Nonbulk containers (e.g., drums) must have a DOT-approved label adhered to the container and all required associated placard stickers before leaving for a TSDF off site. These labels must include information as required in 49 CFR 172. Bulk containers (i.e., rolloffs, tanks) do not require container specific labels for transporting off site, but must include appropriate placards as required in 49 CFR 172. 5.2.1 Soil/Sludge/Sediment When the final site remedy requires offsite treatment and disposal, the IDW may be stored (e.g., drummed, covered ina waste pile) or returned to its source until final disposal. The management option selected shall take into account the potential for increased risks, applicable regulations, and other relevant site-specific factors (e.g., weather, storage space,, and public concern/perceptions). §.2.2 Aqueous Liquids When the final site remedy requires offsite treatment and disposal, the IDW may be stored (e.g., mobile tanks or drums with appropriate secondary containment) until final disposal. The management option selected shall take into account the potential for increased risks, applicable regulations, and other relevant site-specific factors (e.g., weather, storage space, and public concern/perceptions). §.2.3 Disposable PPE When the final site remedy requires offsite treatment disposal, the IDW may be containerized and stored. The management option selected shall take into account potential for increased risks, applicable regulations, and other relevant site-specific factors (e.g., weather, storage space, and public concern/perceptions). 5.3 Collection and Interim Management All interim measures must be approved by the client and regulatory agencies. 1. Storing IDW onsite until the final action may be practical in the following situations: - Returning wastes (especially sludges and soils) to their onsite source area would require reexcavation for disposal in the final remediation alternative. - Interim storage in containers may be necessary to provide adequate protection to human health and the environment. - Offsite disposal options may trigger land disposal regulations under the Resource Conservation and Recovery Act (RCRA). Storing IDW until the final disposal of all wastes from the site will eliminate the need to address this issue more than once. - Interim storage may be necessary to provide time for sampling and analysis. 2. Segregate and containerize all waste for future treatment and/or disposal. - Containment options for soil/sludge/sediment may include drums or covered waste piles in AOC. - Containment options for aqueous liquids may include mobile tanks or drums. - Containment options for PPE may include drums or roll-off boxes. 6.0 Restrictions/Limitations Site Managers Shall Determine the Most Appropriate Disposal Option for Aqueous Liquids on a Site-Specific Basis. Parameters to consider, especially when determining the level of protection, include the volume of IDW, the contaminants present in the groundwater, the presence of contaminants in the soil at the site, whether the groundwater or surface water is a drinking water supply, and whether the groundwater plume is contained or moving. Special disposal/handling may be needed for drilling fluids because they may contain significant solid components. Disposable sampling materials, disposable PPE, decontamination fluids, etc. will always be managed on a site-specific basis. Under No Circumstances Shall These Types of Materials Be Brought Back to the Office or Warehouse. 7.0 References Environmental Resource Center. 1997. Hazardous Waste Management Compliance Handbook 2nd Edition. Karnofsky (Editor), Academy of Certified Hazardous Materials Manager. May 1999. Hazardous Materials Management Desk Reference. Cox. Title 49 Code of Federal Regulations, Department of Transportation. 2005 or current revision. Hazardous Materials Table, Special Provisions, Hazardous, Materials Communications, Emergency Response Information, and Training Requirements, 49 CFR 172. U. S. Environmental Protection Agency. 1987. A Compendium of Superfund Field Operations Methods, EPA/540/P-87/001.1. . August 1990. Low-Level Mixed Waste: A RCRA Perspective for NRC Licensees, EPA/530-SW-90-057. . May 1991. Management of Investigation-Derived Wastes During Site Inspections, EPA/540/G-91/009. . January 1992. Guide to Management of Investigation-Derived Wastes, 9345.3-03FS. . Region IV. November 2001. Environmental Investigations Standard Operating Procedures and Quality Assurance Manual. . t Fe alan Ate &' > Handling Invesi ® Borehole drilling = Soil sampling = Return to boring, pit, or source immediately after generation ® Spread around boring, pit, or source within the AOC = Consolidate in a pit (within the AOC) = Send to onsite TSDF Offsite Disposal ™ Client to send to offsite TSDF Interim Management " Store for future treatment and/or disposal Sludge/Sediment ™ Sludge pit/sediment sampling Onsite Disposal ® Return to boring, pit, or source immediately after generation ® Send to onsite TSDF Offsite Disposal ® Client to send to offsite TSDF Interim Management ™ Store for future treatment and/or disposal Aqueous Liquids (groundwater, surface water, drilling fluids, wastewaters) ™ Well installation/development ® Well purging during sampling = Groundwater discharge during pump tests ® Surface water sampling ™ Wastewater sampling Onsite Disposal ® Pour onto ground close to well (nonhazardous waste) = Discharge to sewer = Send to onsite TSDF Offsite Disposal ® Client to send to offsite commercial treatment unit ® Client to send to publicly owned treatment works (POTW) Interim Management ® Store for future treatment and/or disposal Decontamination Fluids " Decontamination of PPE and equipment Onsite Disposal " Send to onsite TSDF 4 Evaporate (for small amounts of low contamination organic fluids) = Discharge to ground surface Offsite Disposal ® Client to send to offsite TSDF m Discharge to sewer Interim Management ® Store for future treatment and/or disposal Disposable PPE and Sampling Equipment =" Sampling procedures or other onsite activities Onsite Disposal = Place in onsite industrial dumpster = Send to onsite TSDF Offsite Disposal ® Client to send to offsite TSDF Interim Management ® Store for future treatment and/or disposal Adapted from U. S, Environmental Protection Agency, Guide to Management of Investigation-Denived Wastes, 9345-03FS, January 1992. ee +S Prepared: Dave Johnson Technical Review: Steve Guthrie ““E-Signed by Michael C. Malloy QA Review: Jo Nell Mullins Approved: = =e F ~“e-Signed by P. Michagl Schwan Signature/Date hengi h I pep ees. Z an Issued: —————————— Signature/Date 1.0 Objective The objective of this standard operating procedure (SOP) is to establish the baseline requirements, procedures, and responsibilities inherent to the control and use of all measurement and test equipment (M&TE). Contractual obligations may require more specific or stringent requirements that must also be implemented. 2.0 Background 2.1 Definitions Traceability - The ability to trace the history, application, or location of an item and like items or activities by means of recorded identification. 2.2 Associated Procedures = CDM Federal Technical SOP 4-1, Field Logbook Content and Control = CDM Quality Procedures (QPs) 2.1 and 2.3 = Manufacturer's operating and maintenance and calibration procedures 2.3 Discussion M&TE may be government furnished (GF), rented or leased from an outside vendor, or purchased. It is essential that measurements and tests resulting from the use of this equipment be of the highest accountability and integrity. To facilitate that, the equipment shall be used in full understanding and compliance with the instructions and specifications included in the manufacturer's operations and maintenance and calibration procedures and in accordance with any other related project-specific requirements. 3.0 Responsibilities All staff with responsibility for the direct control and/or use of M&TE are responsible for being knowledgeable of and under- standing and implementing the requirements contained herein as well as any other related project-specific requirements. The project manager (PM) or designee (equipment coordinator, quality assurance coordinator, field team leader, etc.) is responsible for initiating and tracking the requirements contained herein. Note: Responsibilities may vary from site to site. Therefore, all field team member responsibilities shall be defined in the field plan or site-/project-specific quality assurance plan. 4.0 Requirements for M&TE Determine and implement M&TE related project-specific requirements The maintenance and calibration procedures must be followed when using M&TE Obtain the maintenance and calibration procedures if they are missing or incomplete Attach or include the maintenance and calibration procedures with the M&TE Prepare and record maintenance and calibration in an equipment log or a field log as appropriate (Figure 1) Maintain M&TE records Label M&TE requiring routine or scheduled calibration (when required) Perform maintenance and calibration using the appropriate procedure and calibration standards Identify and take action on nonconforming M&TE CDM Technical Standard Operating Procedures Page 1 of 4 TSOP 5-1 31997 re 5.0 Procedures 5.1 Determine if Other Related Project-Specific Requirements Apply For all M&TE: The PM or designee shall determine if M&TE related project-specific requirements apply. If M&TE related project-specific requirements apply, obtain a copy of them and review and implement as appropriate. 5.2 Obtain the Operating and Maintenance and Calibration Documents For GF M&TE that is to be procured: Requisitioner - Specify that the maintenance and calibration procedures be included, For GF M&TE that is acquired as a result of a property transfer: Receiver - Inspect the M&TE to determine whether maintenance and calibration procedures are included with the item. If missing or incomplete, order the appropriate documentation from the manufacturer. For M&TE that is to be rented or leased from an outside vendor: Requisitioner - Specify that the maintenance and calibration procedures, the latest calibration record, and the calibration standards certification be included. If this information is not delivered with the M&TE, ask the procurement division to request it from the vendor. 5.3 Prepare and Record Maintenance and Calibration Records For all M&TE: PM or Designee - Record all maintenance and calibration events in a field log unless other project-specific requirements apply. For GF M&TE only (does not apply to rented or leased M&TE): If an equipment log is a project specific requirement, perform the following: Receiver - Notify the PM or designee for the overall property control of the equipment upon receipt of an item of M&TE, PM or Designee and User: - Prepare a sequentially page numbered equipment log for the item using the maintenance and calibration form (or equivalent) (Figure 1), - Record all maintenance and calibration events in an equipment log. 5.4 Label M&TE Requiring Calibration For GF M&TE only (does not apply to rented or leased M&TE): If calibration labeling is a project specific requirement, perform the following: PM or Designee: - Read the maintenance and calibration procedures to determine the frequency of calibration required. - Ifan M&TE item requires calibration before use, affix a label to the item stating “Calibrate Before Use.” - lfan M&TE item requires calibration at other scheduled intervals, e.g., monthly, annually, etc., affix a label listing the date of the last calibration, the date the item is next due for a calibration, the initials of the person who performed the calibration, and a space for the initials of the person who shall perform the next calibration. 5.5 Operating, Maintaining or Calibrating an M&TE Item For all M&TE: PM or Designee and User - Operate, maintain, and calibrate M&TE in accordance with the maintenance and calibration procedures. Record maintenance and calibration actions in the equipment log or field log. 5.6 Shipment For GF M&TE: Shipper - Inspect the item to ensure that the maintenance and calibration procedures are attached to the shipping case, or included, and that a copy of the most recent equipment log entry page (if required) is included with the shipment. If the maintenance and calibration procedures and/or the current equipment log page (if required) is missing or incomplete, do not ship the item. Immediately contact the PM or designee and request a replacement. CDM Technical Standard Operating Procedures Page 2 of 4 TSOP 5-1.31907 a ’ ‘ 7 For M&TE that is rented or leased from an outside vendor: Shipper - Inspect the item to ensure that the maintenance and calibration procedures and latest calibration and standards certification records are included prior to shipment. If any documentation is missing or incomplete, do not ship the item. Immediately contact the procurement division and request that they obtain the documentation from the vendor. 5.7 Records Maintenance For GF M&TE: PM or Designee - Create a file upon the initial receipt of an item of M&TE or calibration standard. Organize the files by contract origin and by M&TE item and calibration standard. Store all files in a cabinet, file drawer, or other appropriate storage media at the pertinent warehouse or office location. Receiver - Forward the original packing slip to the procurement division and a photocopy to the PM or designee. PM or Designee and User: - Maintain all original documents in the equipment file except for the packing slip and field log. - File the photocopy of the packing slip in the M&TE file. - Record all maintenance and calibration in an equipment log or field log (as appropriate). File the completed equipment logs in the M&TE records. Forward completed field logs to the PM for inclusion in the project files. For M&TE rented or leased from an outside vendor: Receiver - Forward the packing slip to the procurement division. User: - Forward the completed field log to the PM for inclusion in the project files. - Retain the most current maintenance and calibration record and calibration standards certifications with the M&TE item and forward previous versions to the PM for inclusion in the project files. 5.8 Traceability of Calibration Standards For all items of M&TE: PM or Designee and User: - When ordering calibration standards, request nationally recognized standards as specified or required, Request commercially available standards when not otherwise specified or required. Or, request standards in accordance with other related project-specific requirements. : - Require certifications for standards that clearly state the traceability. - Require Material Safety Data Sheets to be provided with standards. - Note standards that are perishable and consume or dispose of them on or before the expiration date. 5.9 M&TE That Fails Calibration For any M&TE item that cannot be calibrated or adjusted to perform accurately: PM or Designee - Immediately discontinue use and segregate the item from other equipment. Notify the appropriate PM and take appropriate action in accordance with the CDM QP 2.3 for nonconforming items. - Review the current and previous maintenance and calibration records to determine if the validity of current or previous measurement and test results could have been affected and notify the appropriate PM(s) of the results of the review. 6.0 Restrictions/Limitations On an item-by-item basis, exemptions from the requirements of this SOP may be granted by the Headquarters health and safety manager and/or Headquarters quality assurance director. All exemptions shall be documented by the grantor and included in the equipment records as appropriate. 7.0 References CDM Federal Programs Corporation. 2007. Quality Assurance Manual. Rev. 11. CDM Federal Programs Corporation. 2005. Government Property Manual. Rev. 3. CDM Technical Standard Operating Procedures Page 3 of 4 TSOP 5-1 31907 ———_—__ 3} | Control Vieasurement and Test Home ah IS 007 EEsarias el Mee! ee eee a Figure 1 CDM A subsidiary of Camp Dresser & McKee Inc. Maintenance and Calibration Date: Time (a.m./p.m.) Employee Name: Equipment Description: Contract/Project: Equipment ID No.: Activi LSS —— Sn Equipment Serial No.: ee ace SE La alae Malt entra ance ee Gaiiennane aaanad Comments: Date Si va eee aces 3 & Sate Dsl ge ERE El fi libration/Field oe Eee Cc ok es sili ed bk Calibration Standard: Guneceinratian of Standard: Lot No. of Calibration Standard: Expiration Date of Calibration Standard: Pre-Calibration Reading: Post-Calibration Reading: Additional Readings: Additional Readings: Additional Readings: Additional Readings: Pre-Field Check Reading: Post-Field Check Reading: Adjustment(s): Calibration: ao Passed o Failed Comments: Signature: Date: CDM Technical Standard Operating Procedures TSOP S-1.31997 ONCOL) DOr PO NON Appendix C Field Forms Groundwater Sampling Purge Water Data Form Multi-parameter Water Quality Instrumentation Calibration Log Field Change Request (FCR) Form ANSETS Data Requirement System Runtime and Shutdown Log — GWTF#1 System Runtime and Shutdown Log — GWTF#2 Groundwater Influent Monitoring Data —- GWTF#1 Groundwater Influent Monitoring Data — GWTF#2 Systems Monitoring Data —- GWTF#1 . Systems Monitoring Data - GWTF#2 . Monthly Operations and Maintenance Activities - GWTF#1 . Monthly Operations and Maintenance Activities - GWTF#2 . Synoptic Groundwater Levels ssqy 01g | 12D ju (Aw) (7/3) (N.LN) (wi3/Su) do De Sd}0N sajen 0} yjdag awNjoA a3ind do ZosiG “quan *puo dway Hd Sully ‘S3]ON isajaweig suse) :pouralA) Suryjdwes :adA, Suised aulea\\ Julog Sulnsealj jauUOSJag Buryjdwes :u}3ua] uaesS :ajeq SUWUINIJOD Ja}e/\ 2123S JO JYUsIAH “ON JAM dajyeM 0} ujdeg :8US :Yy3daq [19M ON YefO1d w4o04 eyeq Ja1e/ aSiNg Zuydwes sa}empunosy psepuers Suipeay | psepueys | Suipeay uoljeuqije> Jaya | uoesquyey | saieyy psepueys duipeay vonesque) | salay 4. 9. | paepuers | Suipeay out uoleigie> JaIW Sd]0N (Aw) d¥O AUNEIO ayisads (1/3) SOL (%) Ajuyes (1/8u4) ZOs!d (N.LN) qan (w9/Stu) puod dway Hd :paepueys uoieiqued J2poW sdaunqoegnueyy Juawnsysu| Ag pa329]/0D 80] uoRneiqued UONeUsUNIYSU] Aen sazem sazowesed-ninw ‘SOON TaWeEN alo aquinn alos :01eg TUTU WELLFIELD SITE FIELD CHANGE REQUEST (FCR) FORM REQUEST NO: FCR TITLE: DATE: DESCRIPTION: REASON FOR DEVIATION: RECOMMENDED/MODIFICATION: IMPACT ON PROJECT OBJECTIVES: Signatures: Field Technician (FT) Date Subcontractor Project Manager (PM) Date CDM Site Manager (SM) Date Distribution: EPA Remedial Project Manager CDM SM CDM Quality Assurance Coordinator Subcontractor PM Field Team Project File United States Environmental Protection Ni Agency ANSETS Data Requirement Date: Sampling Start Date Sampling End Date: Project Numbers Project Regional Account DAS Assoc. Number: Number: Number: CLP Case No: Site Information Site Name: City: State: CERCLIS ID: Operable Unit: Action: Funding Lead: Responsible EPA Sampling Organization Project Individual: Analytical Services Information If field analytical services are used during this project write “field COST analysis” in the Laboratory Name Column. If fixed laboratory is used write the name of the laboratory in the Laboratory Name Column. Please specify in this box all field analytical techniques used, Laboratory Name (include No. Requested location if multiple lab locations) Samples Matrix Analysis Turnaround (Days) Completed by: Organization: Date: Table 1 - System Runtime and Shutdown Log - GWTF #1 yh) ES; fh ae ee DUSTER has Tht é Es weil gk re AST a at ate i Dis. ilure/ y as Pas oo ates | 2 aginer |e aye arm Yeseri eee ion LE tart e ce utes =E ae | Maint. _ = (abe gts 4 sre = A as Total Minutes Run Time Total Available Minutes Percent Uptime Page | of 8 Table 2 - System Runtime and Shutdown Log - GWTF #2 k hive yster wi D ned ¥F re (m ID Total Minutes Run Time Total Available Minutes Percent Uptime Table 3 - Groundwater Influent Monitoring Data - GWTF #1 Z RW-61 + RW. 7. Copihived J fluent u 4 Influent RW: influent Date ‘ “Time Totalizer: | Flowrate Press, ENS Totalizer ; Flowrate Press. | Tolslizer , Fiowsle Press. “Totalizer Flowrate (gal.)— (gpm) (psi) (gpm) | (psi). (gal) (gpm) (psi) (gal.) (gpm) Table 4 - Groundwater Influent Monitoring Data - GWTF #2 PF 7 ax RW: Influent y o Combined J foent } Date Time: t 2 Totalizer Wry Flowrate Press 4 “‘Totalizer i Flowrate ‘rast Flowrate (gal (gpm) | (psi) (gal.) (gpm) | (psi) (gal) _| (gpm) Table 5 - Systems Monitoring Data - GWTF #1 Transfer Pump] = ~ | Transfer | TALS, Blower} © A,S. | A'S, Blower ty EAS. [Gen ; | Discharge | Bag Filter |~ Pump) |: Air Stripper, 7 > | "Inlet. Blower |/ Disch. | A.S. Blower |) Sump | Treated Water Date (|) Press... Diff.Press. |, Flowrate | | Influent Totalizer =} Vacuum | Flowrate. | Press. Temperature} Press, | Effluent pil’ REP | 25% (psi) = (psi) |/_ (gpm) Gal) | (in. H20) | (scfm) | (in. H20) | (Deg. F) | (in. H20)| (pH units). Table 6 - Systems Monitoring Data - GWTF #2 AS, AS. Pit Do Transfer f “e » ‘raoster Punip | Bag Filter | Blower | Blower AS, Blower As Blower Sump - Treated Water es ate Discharge Press. | Diff. Press. | ‘ . fluent Totalizer- | |) Inlet | Flowrate. |Disch. Press.| Temperature “Press, 9}. EMueot pH (psi) ‘ (psi) | (gpm) (¢ (gal.) (in. H20) (scfm) ‘| (in. 1120)_| (Deg. F) | Gn. 1120)| (ptt units) Table 7 - Monthly Operations and Maintenance Activities - GWTF #1 po Operation and Maintenance Events. — Sy Cee te ae ee ed tek ae Beata ice ae le tere BLT AG & M Performed -. Chemical Usage Amount Batched Date Muriatic Acid Caltrol 100 Voltage / AMP Draws Date Equipment TP-1 TP-2 AS B-1 SVE B-2 HX-1 A-B/A A-C/B B-C/C Table 8 - Monthly Operations and Maintenance Activities - GWTF #2 -. Operation and Maintenance Events Date O & M Performed - Chemical Usage Amount Batched Date Muriatic Acid Caltrol 100 Voltage /AMP Draws Date Equipment TP-1 AS B-1 A-B/IA A-C/B B-C/C Table 9 - Synoptic Groundwater Levels GWTFE #1 GWTF #2, a - Southern Plume : Well Time DTW Well Time DTW Well =| Time- DTW BP-1 DW-2* MW-21D* BP-2 MW-11D PZ-4 BP-3 MW-12D RD-1 IW-1 MW-19 RD-2 IW-2 RD-4 RD-3 IW-1S RD-7 RD-6 IW-2S SW-6 RD-8 MW-1D Eglin-1 RD-14* MW-13 MW-3* MW-13D MW-14 MW-15 MW-16* MW-17 RD-9 RD-10 RD-11* RD-12 RD-13 RW-8 Date Collected: * Well with pressure transducer (continuous water level measurements) Page | of 1