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Table 1. Concentrations of Volatile Organic Compounds in Soil Samples Collected in August 1992 at the Tutu Wells Site, St. Thomas, Virgin Islands. Sample ID: B-14 B-15 B-16 (0-2.01) (0-2.01) (0-2.0') Analyte Date: 14-Aug-92 14-Aug-92 14-Aug-92 Chloromethane Bromomethane Vinyl chloride Chloroethane Methylene chloride Acetone Carbon disulflde 1 , 1 -Dichloroethene 1,1-Dichlorocthane 1 ,2-Dichloroethene (cis/trans) Chloroform 1 ,2-Dichloroethane 2-Butanone 1 , 1 , 1-Trichloroethane Carbon tetrachloride Bromodichloromethane 1 ,2-Dichloropropane cis-1 ,3-Dichloropropene Trichloroethene Dibromochloromethane 1 , 1 ,2-Trichloroethane Benzene trans- 1 ,3-Dichloropropene Bromoform 4-Methyl-2-pentanone 2-Hexanone 1 , 1 ,2,2-Tetrachlorocthanc Tetrachloroethene Toluene Chlorobenzene Elhylbenzene Styrene Xylenes (total) 1,2-Dibromoethane (EDB) tert-Butyl methyl ether 11U 11 U 11 U 11 U 9J 11 U 11 U 11 U II U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11U 11 U 11 U 11 U 72 2J 11 U 11 U 11 U 11 U 5.7 U 11 U 12 U 12 U 12 U 12 U 9J 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 6J 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 170 12 12 U 12U 12 U 12 U 6U 12 U 11 U 11U 11U 1 I U 8J 11U 11U 11U 11 U 11 U 11 U 1 1 U 11U 11U 11U 11 U 11U 11 U 1 1 U 11 U 11 U 11U 11U 11 U 11 U 11U 11U 23 11 J 11 U 11 U 11 U 11 U 5.6 U 11U n-Propylbenzene 5.7 U 6U 5.6 U Analyte concentrations in micrograms per kilogram (parts per billion (ppbl). Analyses were performed by Enseco-East of Somerset, New Jersey, using March 1990 Contract Laboratory Program (CLP) protocols. J Result is detected below the reporting limit and/or is an estimated concentration. U Compound or element analyzed for, but not detected at the corresponding reporting limit. TUT 004 1986 GERAGHTY & MILLHR. INC *64535* 64535 Table 2. Concentrations of Volatile Organic Compounds in the Field Blank and the Trip Blank Collected in August 1992 at the Tutu Wells Site, St. Thomas, Virgin Islands. Sample ID: Field Blank Analyte Date: Trip Blank !4-Aug-92 14-Aug-92 Chloromethane Bromomethane Vinyl chloride Chloroclhanc Methylene chloride Acetone Carbon disulfide 1 , 1 -Dichloroelhene 1,1-Dichloroelhane 1 ,2-Dichloroethene (cis/trans) Chloroform 1 ,2-Dichloroethane 2-Butanone 1,1, 1-Trichloroethane Carbon tetrachloride Bromodichloromcthane 1 ,2-Dichloropropane trans- 1 ,3-Dichloropropcne Trichloroethene Dibromochloromethane 1,1,2-Trichloroethane Benzene cis- 1 ,3-Dichloropropcne Bromoform 4-Methyl-2-pentanone 2-Hexanone 1 , 1 ,2,2-Tetrachloroethane Tetrachloroethenc Toluene Chlorobenzene Ethylbenzene Styrene Xylenes (total) 1 ,2-Dibromoethane (EDB) tert-Butyl methyl ether 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 5 U 10 U 10 U 10 U 10 U 10 U 2J 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 5 U 10 U n-Propylbenzene 5U 5 U Analyte concentrations in micrograms per liter (parts per billion [ppb]). Analyses were performed by Enseco-tast of Somerset, New Jersey, using March 1990 Contract Laboratory Program (CLP) protocols. J Result is detected below the reporting limit and/or is an estimated concentration., U Compound or element analyzed for, but not detected at the corresponding reporting limit. TUT 004 1987 GERAGHTY & MIl.LFR. INC Table 3. Concentrations of Base Neutral and Acid Extractable Organic Compounds in Soil Samples Collected in August 1992 at the Tutu Wells Site, St. Thomas, Virgin Islands. Sample ID: B-14 (0-2.01) B 15 B-16 (0-2.01) (0-2.0') Analyte Date: 14-Aug-92 14-Aug-92 14-Aug-92 Acenaphthene Acenaphthylene Anthracene 9H-Carbazole Benzo(a)anthracene Benzofatayrene BenzoibjiTuoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene 4-Bromophenyl phenyl ether Butyl benzyl phthalate 4-Chloroaniline bis(2-Chloroethoxy)methane bis(2-Chloroethyl)ether bis(2-Chloroisopropyl)ether 4-Chloro-3-methylphenol 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenyl phenyl ether Chrysene Di-n-butyl phthalate Dibenz(a,h)anthracene Oibenzofuran 1 ,2-Dichlorobenzene 1 ,3-Dichlorobenzene 1 ,4-Dichlorobenzene 3 ,3 '-Dichlorobenzidine 2,4- Dichlorophenol Diethyl phthalate 2,4-Dimethylphenol Dimethyl phthalate 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Di-n-octyl phthalate bis(2-Ethylhexyl)phthalate Fluoranthene 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 910 U 910 U 370 U 370 U 370 U 370 U 370 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 950 U 950 U 390 U 390 U 390 U 390 U 390 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 58 J 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 890 U 890 U 370 U 370 U 370 U 110J 370 U Analyte concentrations in micrograms per kilogram (parts per billion [ppb]). Analyses were performed by Enseco-East of Somerset, New Jersey, using March 1990 Contract Laboratory Program (CLP) protocols. Result is detected below the reporting limit and/or is an estimated concentration. Compound or element analyzed for, but not detected at the corresponding reporting limit. TUT 004 1988 GERAGHTY & MILLHR. INC Table 3. Concentrations of Base Neutral and Acid Extractable Organic Compounds in Soil Samples Collected in August 1992 at the Tutu Wells Site, St. Thomas, Virgin Islands. Sample ID: B-14 B-1S B-16 (0-2.0') (0-2.0') (0-2.01) Aiulyte Dale: 14-Aug-92 14-Aug-92 14-Aug-92 Fluorene Hcxachlorobenzene Hexachlorobutadiene Hexachlorocyclopenladicne Hexachloroethane Indeno( 1 ,2,3-cd)pyrene Isophorone 2-Mcthylnaphthalene 2-Methylphenol 4-Melhylphcnol Naphthalene 2-Nitroanilinc 3-Nitroaniline 4-Nitroanilinc Nitrobenzene 2-Nitrophenol 4-Nitrophcnol N-Nitrosodiphenylamine N-Nitroso-di-n-propylamine Pentachlorophenol Phenanthrene Phenol Pyrene 1 ,2,4-Trichlorobenzene 2,4,5-Trichlorophenol 2,4 ,6-Trichlorophenol 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 910 U 910 U 910 U 370 U 370 U 910 U 370 U 370 U 910 U 370 U 370 U 370 U 370 U 910 U 370 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 950 U 950 U 950 U 390 U 390 U 950 U 390 U 390 U 950 U 390 U 390 U 390 U 390 U 950 U 390 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 890 U 890 U 890 U 370 U 370 U 870 U 370 U 370 U 890 U 370 U 370 U 370 U 370 U 890 U 370 U Analytc concentrations in micrograms per kilogram (parts per billion [ppbll. Analyses were performed by Enseco-East of Somerset, New Jersey, using March 1990 Contract Laboratory Program (CLP) protocols. J Result is detected below the reporting limit and/or is an estimated concentration. U Compound or element analyzed for, but not detected at the corresponding reporting limit. TUT OO4 19S9 GERAGHTY f^ MILLHR. IN( Table 4. Concentrations of Base Neutral and Acid Extractable Organic Compounds in the Field Blank Collected in August 1992 at the Tutu Wells Site, St. Thomas, Virgin Islands. Sample ID: Field Blank Analyte Date: M-Aug-92 Acenaphthene Acenaphthylene Anthracene 9H-Carbazole Benzo(a)anthracene Benzo(b)fluoranthene Benzomfluoranthene Benzofg,h,i)perylene Bcnzo(a)pyrenc 4-Bromophenyl phenyl ether Butyl benzyl phthalate 4-Chloroanilinc bis(2-Chloroethoxy)methane bis(2-Chloroethyl]iether bis(2-Chloroisopropyl)ether 4-Chloro-3-methylphenol 2-ChloronaphthaJcnc 2-Chlorophenol 4-Chlorophenyl phenyl ether Chrysene Dibenz(a,h)anthracene Dibenzofuran Di-n-butyl phthalate 1 ,2-Dichlorobenzene 1 ,3-Dichlorobenzene 1 ,4-Dichlorobenzene 3,3' -Dichlorobenzidine 2,4-Dichlorophenol Diethyl phthalate 2,4-Dimeihylphenol Dimethyl phthalate 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2,4-Dinitrotolucne 2 ,6-Din itrotolucnc Di-n-octyl phthalate bis(2-Ethylnexyl)phthalate Fluoranthene 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 25 U 25 U 10 U 10 U 10 U 47 B 10 U Analyte concentrations in microgramsper liter (parts per billion [ppb]). Analyses were performed by Enseco-East of Somerset, New Jersey, using March 1990 Contract Laboratory Program (CLP) protocols. B Analyte is detected in the laboratory blank. U Compound or element analyzed for, but not detected at the corresponding reporting limit. TUT OO4 199O |0/}T'<n < 71 f-n GERAGHTY & MILLHR. INC Table 4. Concentrations of Base Neutral and Acid Extractable Organic Compounds in the Field Blank Collected in August 1992 at the Tutu Wells Site, St. Thomas, Virgin Islands. Analyte Sample ID: Field Blank Date: H-Aug-92 Fluorene Hcxachlorobcnzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno( 1 ,2,3-cd)pyrene Isophorone 2-Methylnaphthalene 2-Methylphenol 4-Methylphenol Naphthalene 2-Nitroaniline 3-Nitroanilinc 4-Nitroaniline Nitrobenzene 2-Nitrophenol 4-Nitrophenol N-Nitrosodiphenylamine N-Nitroso-di-n-propylamine Pentachlorophenol Phenanthrene Phenol Pyrene 1 ,2,4-Trichlorobenzene 2 ,4 ,5-Trichlorophcnol 2,4,6-Trichlorophenol 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 25 U 25 U 25 U 10 U 10 U 25 U 10 U 10 U 25 U 10 U 10 U 10 U 10 U 25 U 10 U Analyte concentrations in micrograms per liter (parts per billion [ppb]). Analyses were performed by Enseco-East of " " " uiwi yjs«iia Lsv'i isiiuwii Lr|-M-'J/• of Somerset, New Jersey, using March 1990 Contract Laboratory Program (CLP) protocols. B Analyte is detected in the laboratory blank. U Compound or clement analyzed for, but not detected at the corresponding reporting limit. TUT 004 1991 KV21/77 5 J1 !*• GERAGHTY & MILLKR. INC' Table 5. Concentrations of Metals in Soil Samples Collected in August 1992 at the Tutu Wells Site, St. Thomas, Virgin Islands. Sample ID: B-14 (0-2.0-) B-15 (0-2.01) B-16 (0-2.0') Analyle Date: 14-Aug-92 14-Aug-92 14-Aug-92 Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc 25300 7.3 BN 0.46 U 34.5 B 0.23 U 0.7 U 120000 * 13.8 N 20 48.3 N 28000 2.9 26200 757 0.06 U 11.1 161 B 0.46 UW 0.93 B 181 B 0.7 U 95.8 N 50.9 26400 6.4 BN 1.3 B 32. IB 0.23U 0.7 U 89400 * 27.3 N 23.2 65.9 N 32600 12.2 22900 809 0.06 U 16.5 389 B 0.46 UW L I B 281 B 0.7 U 98.8 N 206 18900 6.8BN 11.6 39.9 B 0.22 U 0.99 B 68800 * 36.4 N 19 72.1 N 30600 45.6 N« 16300 599 0.57 15.7 506 B 0.44 U 1.3 B 396 B 0.67 U 79.7 N 459 Analyte concentrations in milligrams per kilogram (parts per million [ppml). Analyses were performed by bnseco-tast of Somerset, New Jersey, using March 1990 Contract Laboratory Program (CLP) protocols. B N U W Duplicate analysis not within control limits. Reported value is between contract required, detection limit (CRDL) and instrument detection limit (IDL). Spiked sample recovery not within control limits. Compound or element analyzed for, but not detected at the corresponding reporting limit. Post-digestion spike for graphite furnace atomic absorption (GFAA) out of controllimits. IWJOTJ jap. TUT 004 1992 GERAGHTY & MII.LI-R, INC Table 6. Concentrations of Metals in the Field Blank Collected in August 1992 at the Tutu Wells Site, St. Thomas, Virgin Islands. Analyte Sample ID: Field Blank Date: 14-Aug-92 Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc 32 U 20 U 2 U 1 U 1 U 3U 73.2 B 4 U 4 U 4 U 9.5 B 1 U 35 U L I B 0.1 U 8U 560 U 2 U 4 U 222 B 3 U 4 U 2U Analyte concentrations in microgramsper liter (pans per billion Ippb]). Analyses were performed by Enseco-East of Somerset, New Jersey, using March 1990 Contract Laboratory Program (CLP) protocols. B Reported value is between contract required detection limit (CRDL) and instrument detection limit (IDL). U Compound or element analyzed for, but not detected at the corresponding reporting limit. TUT O04 1993 GERAGHTY & MILI.I-R. INC Table 7. Concentrations of Total Petroleum Hydrocarbons in Soil Samples Collected in August 1992 at the Tutu Wells Site, St. Thomas, Virgin Islands. Sample ID: B-14 B-15 B 16 (0-2.0') (0-2.0') (0-2.0') Aiulyte Date: 14-Aug-92 14-Aug-92 14-Aug-92 Total Petroleum Hydrocarbons 250 D <24 82 Analyte concentrations in milligrams per kilogram (parts per million [ppmll. Analyses were performed by Enseco-East of Somerset, New Jersey, using U.S. D Analyte identified at a secondary dilution. < Less than. Where an analyte has not been detected, a reporting limit is given. Army Corp of Engineers method CE81-1, ivrnn )Mfm TUT 004 1994 GERAGHTY & MII.LHR. INC Table 8. Concentrations of Total Petroleum Hydrocarbons in the Field Blank Collected in August 1992 at the Tutu Wells Site, St. Thomas, Virgin Islands. Sample ID: Field Blank Analyte Date: 14-Aug-92 Total Petroleum Hydrocarbons <0.5 Analyte concentrations in milligrams per liter (parts per million [ppm]). Analyses were performed by Enseco-East of Somerset, New Jersey, using USEPA Method 418.1. < Less than. Where an analyte has not been detected, a reporting limit is given. TUT 004 1995 GERAGHTY<*MILI,I-:R.IN(