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rra INTERNATIONAL TECHNOLOGY CORPORATION October 25, 1994 Ms. Caroline Kwan Project Manager New York/Caribbean Superfund Branch 2 United States Environmental Protection Agency Region II Jacob K. Javits Federal Building New York, NY 10278-0012 Groundwater Samples From O'Henry Laundry. St. Thomas. US VI Dear Ms. Kwan: This letter is a follow-up to our phone conversation yesterday concerning groundwater data included in the Risk Assessment for the Tutu Wells site, St. Thomas, performed by CDM. From our conversation yesterday and from the fax you sent me indicating which samples are in the data package used by CDM, it appears that CDM only has one of the data packages. Groundwater samples were collected from the four monitoring wells at the O'Henry Laundry on two occasions in 1993, March and May. There were a variety of associated QA samples collected with these samples as indicated in Table 1 (attached). Analytical data packages from both rounds of sampling were transmitted to you in August 1993 and again in February 1994. For you information, I have enclosed Form I's for the package that CDM seems to be missing (May 1993 sampling). If you need me to transmit the entire data package again, please let me know. Sincerely, Belinda K. Price, R.P.G. Project Manager cc: N. D'Anna, Esq. Regional Office 312 Directors Drive« Knoxville. Tennessee 37923 • 615-690-3211 KN \SB\OCT\BPRKTE 001 ™1-1""" IT Corporation is a wholly owned subsidiary of International Technology Cr TUT O06 O965 *64647* 64647 Table 1 Summary of Groundwater Samples Collected by IT Corporation, 1993 O'Henry Laundry, Tutu, St. Thomas March 1 993 Sample # MW-01 MW-02 MW-03-OR MW-03-FD MW-04 MW-03 MS/MSD DRM01 May 1993 Sample # MW-01 MW-02 MW-03 MW-04 Trip Blank PW-1 Samples (7 Water Samples) Sample Description Sample From MW-01 Sample From MW-02 Sample From MW-03 Field Duplicate From MW-03 Sample From MW-04 Matrix Spike/Matrix Spike Duplicate from MW-03 Purge Water Samples (6 Water Samples) Sample Description Sample From MW-01 Sample From MW-02 Sample From MW-03 Sample From MW-04 Trip Blank Purge Water Analysis CLP VOCs CLP VOCs CLP VOCs CLP VOCs CLP VOCs CLP VOCs 601/602 Analysis CLP VOCs CLP VOCs CLP VOCs CLP VOCs CLP VOCs 601/602 KN\SB\OCT\BPR1CE.OOI TUT 006 O966 INTERNATIONAL ANALYTICAL TECHNOLOGY ~£^\jj£Zf?^ CORPORATION SERVICES k CERTIFICATE OF ANALYSIS IT Corporation ^ June 23, 1993 312 Directors Drive Knoxville, TN 37923 Attn: Belinda Price Job Number: ITMK. 34182 P.O. Number: 490440.003 This is the Certificate of Analysis for the following samples: Client Project ID: St. Thomas Date Received by Lab: 05/28/93 Number of Samples: Six (6) Sample Type: Water-five (5); Trip Blank-one (1) I. Introduction * On 05/28/93, five (5) water samples and one (1) trip blank arrived at the ITAS-Knoxville, Tennessee, laboratory from IT Corporation, Knoxville, Tennessee, in support of the St. Thomas project. The list of analytical tests performed, as well as date of receipt and analysis, can be found in the attached report. n. Analytical Results/Methodology The analytical results for this report are presented by analytical test. Each set of data will include sample identification information and the analytical results. Please note that the data are not blank corrected. The samples were analyzed for Target Compound List (TCL) volatiles by gas chromatography/mass spectroscopy (GC/MS) in accordance with the EPA CLP 3/90 Statement of Work. The samples were analyzed for halogenated and aromatic volatile organic compounds by gas chromatography based on EPA methods 601 and 602. Reviewed and Approved: Alyce R. Moore Laboratory Manager American Council ol Independent Laboratories International Association ol Environmental Testing Laboratories American Association lor Laboratory Accreditation TUT OO6 O967 IT Analytical Services, 5815 Middlebrook Pike, Knoxville, TN 37921 saneg IT Corporation IT ANALYTICAL SERVICES June 23 1993 5815MIDDLEBROOKPIKE KNOXVILLE. TN * Client Project ID: St. Thomas Job Number: ITEK 54182 ffl. Quality Control Routine laboratory level I QC was followed. The volatiles analyses were performed by purge and trap with a J&W DB-624 megabore column on a Finnigan GC/MS/DS unit. The sample analyses went well. Elevated levels of tetrachloroethene in MW-4 required a two-fold dilution. There were no problems seen in final data review. Data were reported with qualifiers as follows: U - Compound analyzed for but not detected; value given is quantitation limit. E - Compound exceeded calibration range. D - Compound analyzed at a secondary dilution factor. J - Compound detected but below quantitation limit; value estimated. S - Spiked compound. B - Compound found in method blank. A - Suspected aldol condensation product. Y - Indistinguishable isomer in tentatively identified compounds. N - Presumptive evidence of compound presence. The samples were analyzed for halogenated and aromatic volatile organics by gas chromatography/photoionization and electrolytic conductivity (Hall) detection in series using an RTX 502.2 column on a Varian 3400 GC. No problems were encountered. TUT 006 O968 IT Corporation June 23, 1993 Client Project ID: St. Thomas IT ANALYTICAL SERVICES 5815 MIDDLEBROOK PIKE KNOXVILLE. TN Job Number: ITEK 54182 HALOGENATED AND AROMATIC VOLATILE ORGANIC ANALYSIS Results in /tg/liter (ppb) Sample Matrix: Water Client Sample ID: PW-1 Lab Sample ID: XX4810 Compound dichlorodifluoro methane chJoromethane vinyl chloride bromomethane chJoroethane trichlorofluoromethane 1,1 -dichloroethene methylene chloride trans-1,2-dichloroethene 1.1 -dichloroethane cis-1,2-dichloroethene trichloromethane (chloroform) 1,1,1 -trichloroethane carbon tetrachloride benzene 1,2-dichloroethane trichloroethene Analysis Date: 06/03/93 Result Compound 1.8 U 1,2-dichloropropane 0.8 U bromodichloromethane 1.8 U 2-chloroethylvinyl ether 1.2 U cis-l,3-dichloropropene 5.2 U toluene 2.0 U trans-I,3-dichloropropene 1.3 U 1,1,2-trichloroethane 15 U tetrachloroethene 1.0 U dibromochloromethane 0.7 U chlorobenzene 15 ethyl benzene 0.5 U xylenes (total) 0.3 U bromoform 1.2 U 1,1,2,2-tetrachloroethane 2.0 U 1,3-dichlorobenzene 0.3 U 1,4-dichlorobenzene 8.8 1,2-dichlorobenzene Result 0.4 U 1.0 U 1.3 U 3.4 U 2.0 U 3.4 U 0.2 U 49 0.9 U 2.0 U 2.0 U 1.0 U 2.0 U 0.3 U 3.2 U 2.4 U 1.5 U U - Compound was analyzed for but not detected. The number is the detection limit for the sample. TUT OO6 O969 IT Corporation June 23, 1993 Client Project ID: St. Thomas IT ANALYTICAL SERVICES 5815 MIDDLEBROOK PIKE KNOXVILLE, TN Job Number: ITEK 54182 HALOGENATED AND AROMATIC VOLATILE ORGANIC ANALYSIS Results in /tg/liter (ppb) Sample Matrix: Water Client Sample ID: Method Blank Lab Sample ID: B3297 Compound dichJorodifluoromethane chloromethane vinyl chloride bromomethane chloroe thane trichlorofluoromethane 1,1-dichloroethene methylene chloride trans-1,2-dichloroethene i, 1 -dichloroethane cis-1,2-dichloroethene trichloromethane (chloroform) 1,1,1 -trichloroethane carbon tetrachloride benzene 1,2-dichloroethane trichloroethene Result Compound 1.8 U 1,2-dichloropropane 0.8 U bromodichloromethane 1.8 U 2-chloroethylvinyl ether 1.2 U cis-l,3-dichloropropene 5.2 U toluene 2.0 U trans-1,3-dichloropropene 1.3 U 1,1,2-trichJoroethane 15 U tetrachloroethene 1.0 U dibromochloromethane 0.7 U chlorobenzene 1.0 U ethyl benzene 0.5 U xylenes (total) 0.3 U bromofonn 1.2 U 1,1,2,2-tetrachloroethane 2.0 U 1,3-dichlorobenzene 0.3 U 1,4-dichlorobenzene 1.2 U 1,2-dichlorobenzene Result 0.4 U 1.0 U 1.3 U 3.4 U 2.0 U 3.4 U 0.2 U 0.3 U 0.9 U 2.0 U 2.0 U 1.0 U 2.0 U 0.3 U 3.2 U 2.4 U 1.5 U Analysis Date: 06/03/93 U - Compound was analyzed for but not detected. The number is the detection limit for the sample. TUT O06 0970 IT Coiporation June 23, 1993 Client Project ID: St. Thomas IT ANALYTICAL SERVICES 5815 MIDDLEBROOK PIKE KNOXVILLE, TN Job Number: ITEK 54182 WATER SURRCXJATE PERCENT RECOVERY SUMMARY Client Sample ID PW-1 PW-1 Method Blank Lab Sample ID XX4810 XX4810(D1:5) B3297 BCM 110 82 99 VOLATILE OCFB 111 78 93 FB 112 - 117 OFCB 113- - 117 BCM - bromochJoromcthane OCFB - ortho-chJorofluorobenzrihe FB - fluorobenzene OFCB - ortho fluoro chlorobenzene QC LIMITS (60-127%) (65-126%) (64-126%) (73-128%) TUT OO6 O971 1A VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE Lab Namf: ITAS-KNOXVILLE__________ Lab Code: ITSTU Case No.: 54182 Matrix: (soil^-water) WATER Sample wt/vol: 5.0 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. ___ GC-Column: DB-624 ID: 0.530 (mm) Soil Extract Volume: ______ (uL) Contract: SAS No.: MW1 SDG No.: MW1 Lab Sample ID: XX4806 Lab File ID: XX4806 Date Received: 05/28/93 Date Analyzed: 06/01/93 Dilution Factor: ____1.0 Soil Aliquot Volume: ___ CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L 74-87-3——————Chloromethane__________ 74-83-9———————Bromomethane___________ 75-01-4——————Vinyl Chloride_________ 75-00-3———————Chloroethane___________ 75-09-2———————Methylene Chloride______ 67-64-1———————Acetone_______________ 75-15-0———————Carbon Disulfide________ 75-35-4———————1,1-Dichloroethene______ 75-34-3 —————— 1,1-Dichloroethane______ 540-59-0——————1,2-Dichloroethene (total) 67-66-3———————Chloroform_____________ 107-06-2——————1,2-Dichloroethane______ 78-93-3———————2-Butanone_____________ 71-55-6———————1,1,1-Trichloroethane____ 56-23-5———————Carbon Tetrachloride____ 75-27-4———————Bromodichloromethane____ 78-87-5 ——————— 1,2-Dichloropropane_____ 10061-01-5————cis-1,3-Dichloropropene__ 79-01-6———————Trichloroethene________ 124-48-1——————Dibromochloromethane____ 79-00-5———————1,1,2-Trichloroethane____ 71-43-2———————Benzene________________ 10061-02-6————trans-i/3-Dichloropropene_ 75-25-2———————Bromoform_____________ 108-10-1——————4-Methyl-2-Pentanone____ 591-78-6——————2-Hexanone____________ 127-18-4——————Tetrachloroethene_______ 79-34-5———————1, l,2,2-Tetrachloroethane_ 108-88-3———————Toluene_________________ 108-90-7 ———— —Chlorobenzene__________ 100-41-4——————Ethylbenzene___________ 100-42-5——————Styrene_______________ 1330-20-7—————Xylene (total)__________ 10 10 10 10 1 10 10 10 10 22 10 10 10 10 10 10 10 10 6 10 10 10 10 10 10 10 15 10 10 10 10 10 10 FORM I VOA U U U U BJ U U U U U U U U U U U UJ U U U U U U U U U U U U U .(uL) 3/90 TUT 006 0972 IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS Lab Name: ITAS-KNOXVILLE_________ Contract: Lab Code: ITSTU Case No.: 54182 SAS No.: Matrix: (soil/water) WATER Sample wt/vol: 5.0 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. ___ GC'Column: DB-624 ID: 0.530 (nun) Soil Extract Volume: ______ (uL) Number TICs found: _Q EPA SAMPLE N2.1 MW1 SDG No.: MW1 Lab Sample ID: XX4806 Lab File ID: XX4806 Date Received: 05/28/93 Date Analyzed: 06/01/93 Dilution Factor: ____1.0 Soil Aliquot Volume: CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L .(UL) CAS NUMBER COMPOUND NAME RT EST. CONC. Q FORM I VOA-TIC 3/90 TUT 006 0973 1A VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE Lab Name: ITAS-KNOXVILLE_________ Contract: Lab Code: ITSTU Case No.: 54182 SAS No.: Matrix: (soil^yater) WATER Sample wt/vol: 5.0 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. ___ GC Column: DB-624 ID: 0.530 (mm) Soil Extract Volume: ______ (uL) MW2 SDG No.: MW1 Lab Sample ID: XX4807 Lab File ID: XX4807 Date Received: 05/28/93 Date Analyzed: 06/01/93 Dilution Factor: ____1.0 Soil Aliquot Volume: ___ CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L 74-87-3——————Chloromethane__________ 74-83-9———————Bromomethane___________ 75-01-4——————Vinyl Chloride_________ 75-00-3——————Chloroe thane__________ 75-09-2———————Methylene Chloride______ 67-64-1———————Acetone_______________ 75-15-0———————Carbon Disulfide________ 75-35-4 ——————— 1,1-Dichloroethene______ 75-34-3———————1,1-Dichloroethane______ 540-59-0——————1,2-Dichloroethene (total) 67-66-3———————Chloroform_____________ 107-06-2——————1,2-Dichloroethane______ 78-93-3——————2-Butanone____________ 71-55-6———————1,1,1-Trichloroethane____ 56-23-5——————Carbon Tetrachloride____ 75-27-4———————Bromodichloromethane____ 78-87-5———————1,2-Dichloropropane_____ 10061-01-5————cis-1,3-Dichloropropene__ 79-01-6———————Trichloroethene_________ 124-48-1——————Dibromochloromethane____ 79-00-5——————1,1,2-Trichloroethane___ 71-43-2———————Benzene________________ 10061-02-6————trans-1,3-Dichloropropene_ 75-25-2——————Bromoform_____________ 108-10-1——————4-Methyl-2-Pentanone____ 591-78-6——————2-Hexanone_____________ 127-18-4——————Tetrachloroethene_______ 79-34-5———————1,1,2,2-Tetrachloroethane_ 108-88-3——————Toluene______________ 108-90-7——————Chlorobenzene__________ 100-41-4——————Ethylbenzene___________ 100-42-5——————Styrene_______________ 1330-20-7—————Xylene (total)__________ 10 10 10 10 1 10 10 10 10 20 10 10 « -*• 10 10 10 10 10 35 10 10 10 10 10 10 10 200 10 10 10 10 10 10 FORM I VOA uuuu BJ U U U U U U f* U U U u u uuu uuuu u uu uuu .(UL) 3/90 TUT 006 0974 IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS Lab Name*: ITAS-KNOXVILLE_________ Contract: _ Lab Code: ITSTU Case No.: 54182 SAS No.: EPA SAMPLE MW2 SDG NO.: MW1 Matrix: (soi]^water) WATER Sample wt/vol: 5.0 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. ___ GC'Column: DB-624 ID: 0.530 (nun) Soil Extract Volume: ______ (uL) Number TICs found: _0 Lab Sample ID: XX4807 Lab File ID: XX4807 Date Received: 05/28/93 Date Analyzed: 06/01/93 Dilution Factor: ____1.0 Soil Aliquot Volume: CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L .(uL) CAS NUMBER COMPOUND NAME RT EST. CONC. Q FORM I VOA-TIC 3/90 TUT OO6 O975 1A VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE >ab Name: ITAS-KNOXVILLE_________ Lab Code: ITSTU Case No.: 54182 Matrix: (soil/tatter) WATER Sample wt/vol: 5.0 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. ___ GC'column: DB-624 ID: 0.530 (nun) Soil Extract Volume: _______ (uL) Contract: SAS No.: MW3 SDG No.: MW1 Lab Sample ID: XX4808 Lab File ID: XX4808 CAS NO. COMPOUND Date Received: 05/28/93 Date Analyzed: 06/01/93 Dilution Factor: ____1.0 Soil Aliquot Volume: CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L 74-87-3———————Chloromethane___________ 74-83-9———————Bromomethane___________ 75-01-4———————Vinyl Chloride_________ 75-00-3———————Chloroethane___________ 75-09-2———————Methylene Chloride______ 67-64-1———————Acetone_______________ 75-15-0———————Carbon Disulfide________ 75-35-4———————1,1-Dichloroethene______ 75-34-3———————1,1-Dichloroethane______ 540-59-0——————1,2-Dichloroethene (total) 67-66-3——————Chloroform____________ 107-06-2——————1,2-Dichloroethane______ 78-93-3————————2-Butanone______________ 71-55-6———————1, l, 1-Trichloroethane____ 56-23-5———————Carbon Tetrachloride_____ 75-27-4———————Bromodichloromethane_____ 78-87-5———————1,2-Dichloropropane_____ 10061-01-5————cis-1,3-Dichloropropene__ 79-01-6———————Trichloroethene_________ 124-48-1——————Dibromochloromethane_____ 79-00-5———————1,1,2-Trichloroethane____ 71-43-2———————Benzene_______________ 10061-02-6————trans-1,3-Dichloropropene_ 75-25-2———————Bromoform_____________ 108-10-1——————4-Methyl-2-Pentanone____ 591-78-6——————2-Hexanone_____________ 127-18-4——————Tetrachloroethene_______ 79-34-5——————l,l,2/2-Tetrachloroethane_ 108-88-3——————Toluene________________ 108-90-7——————Chlorobenzene__________ 100-41-4——————Ethylbenzene___________ 100-42-5——————Styrene_______________ 1330-20-7—————Xylene (total)_________ 10 10 10 10 1 10 10 10 10 7 10 10 10 10 10 10 10 10 3 10 10 10 10 10 10 10 6 10 10 10 10 10 10 u uuu BJ Uu u u Juu uuuuuu J uu uuuuuJuuuuuu .(uL) FORM I VOA 3/90 TUT OO6 O976 IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS Lab Name: ITAS-KNOXVILLE_________ Contract: Lab Code: ITSTU Case No.: 54182 SAS No.: EPA SAMPLE MW3 SDG No.: MW1 Matrix: (soi^/water) WATER Sample wt/vol: 5.0 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. ___ GC-Column: DB-624 ID: 0.530 (mm) Soil Extract Volume: ______ (uL) Number TICs found: Lab Sample ID: XX4808 Lab File ID: XX4808 Date Received: 05/28/93 Date Analyzed: 06/01/93 Dilution Factor: ____1.0 Soil Aliquot Volume: CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L .(UL) CAS NUMBER COMPOUND NAME *• RT EST. CONC. Q FORM I VOA-TIC 3/90 TUT 006 O977 1A VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE Lab Name: ITAS-KNOXVILLE_________ Lab Code: ITSTU Case No.: 54182 Matrix: (soil</vater) WATER Sample wt/vol: 5.0 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. ___ GC'Column: DB-624 ID: 0.530 (mm) Soil Extract Volume: ______ (uL) Contract: SAS No.: MW4 SDG No.: MW1 Lab Sample ID: XX4809 Lab File ID: XX4809 Date Received: 05/28/93 Date Analyzed: 06/01/93 Dilution Factor: ____1.0 Soil Aliquot Volume: ___ CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L 74-87-3———————Chloromethane__________ 74-8 3-9 ———————Bromomethane___________ 75-01-4———————Vinyl Chloride__________ 75-00-3——————Chloroethane__________ 75-09-2———————Methylene Chloride______ 67-64-1———————Acetone________________ 75-15-0———————Carbon Disulfide________ 75-35-4- —————— 1,1-Dichloroethene______ 75-34-3 ——————— 1, l-Dichloroethane______ 540-59-0——————1,2-Dichloroethene (total). 67-66-3———————Chloroform_____________ 107-06-2——————1,2-Dichloroethane______ 78-93-3———————2-Butanone_____________ 71-55-6———————1,1, l-Trichloroethane____ 56-23-5———————Carbon Tetrachloride____ 75-27-4——————Bromodichloromethane____ 78-87-5———————1,2-Dichloropropane_____ 10061-01-5————cis-1,3-Dichloropropene__ 79-01-6——————Trichloroethene________ 124-48-1——————Dibromochloromethane_____ 79-00-5———————1,1,2-Trichloroethane____ 71-43 -2 ———————Benzene_______________ 10061-02-6————trans-1,3-Dichloropropene_ 75-25-2——————Bromoform_____________ 108-10-1——————4-Methyl-2-Pentanone_____ 591-78-6——————2-Hexanone______________ 127-18-4——————Tetrachloroethene_______ 79-34-5———————l,l,2,2-Tetrachloroethane_ 108-88-3——————Toluene_______________ 108-90-7——————Chlorobenzene__________ 100-41-4——————Ethylbenzene__________ 100-42-5——————Styrene_______________ 1330-20-7—————Xylene (total)_________ 10 10 10 10 2 10 10 10 10 25 10 10 10 10 10 10 10 10 26 10 10 10 10 10 10 10 240 10 10 10 10 10 10 U U U U BJ U U U U U U U U U U U U U U U U U U U E U U U U U U .(UL) FORM I VGA TUT OO& 09 78 3/90 IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS 74 EPA SAMPLE NO. Lab Name: ITAS-KNOXVILLE__________ Lab Code: ITSTU Case No.: 54182 Matrix: (soil^water) WATER Sample wt/vol: 5.0 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. ___ GC'Column: DB-624 ID: 0.530 (mm) Soil Extract Volume: ______ (uL) Number TICs found: _Q Contract: SAS No.: MW4 SDG No.: MW1 Lab Sample ID: XX4809 Lab File ID: XX4809 Date Received: 05/28/93 Date Analyzed: 06/01/93 Dilution Factor: ____1.0 Soil Aliquot Volume: ___ .(uL) CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L CAS NUMBER COMPOUND NAME " RT EST . CONC . Q FORM I VOA-TIC TUT OO6 O979 3/90 1A VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE Lab Name: ITAS-KNOXVILLE__________ Lab Code: ITSTU Case No.: 54182 Matrix: (soil/water) WATER Sample wt/vol: 5.0 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. ___ GC' Column: DB-624 ID: 0.530 (mm) Soil Extract Volume: ______ (uL) Contract: SAS No.: MW4DL SDG No.: MW1 Lab Sample ID: XX4809 Lab File ID: XX4809DL CAS NO. COMPOUND Date Received: 05/28/93 Date Analyzed: 06/03/93 Dilution Factor: ____2.0 Soil Aliquot Volume: CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L 74-87-3———————Chloromethane__________ 74-83-9———————Bromomethane___________ 75-01-4——————Vinyl Chloride_________ 75-00-3———————Chloroethane___________ 75-09-2———————Methylene Chloride______ 67-64-1———————Acetone_______________ 75-15-0———————Carbon Disulfide________ 75-35-4——————1,1-Dichloroethene______ 75-34-3———————1,1-Dichloroethane______ 540-59-0——————1,2-Dichloroethene (total) 67-66-3———————Chloroform_____________ 107-06-2——————1,2-Dichloroethane______ 78-93-3———————2-Butanone_____________ 71-55-6———————1, l, 1-Trichloroethane____ 56-23-5———————Carbon Tetrachloride____ 75-27-4———————Bromodichloromethane____ 78-87-5——————1,2-Dichloropropane_____ 10061-01-5————cis-1,3-Dichloropropene__ 79-01-6———————Trichloroethene_________ 124-48-1——————Dlbromochloromethane____ 79-00-5———————1,1,2-Trichloroethane____ 71-43-2———————Benzene_______________ 10061-02-6————trans-l,3-Dichloropropene_ 75-25-2———————Bromoform_____________ 108-10-1——————4-Methyl-2-Pentanone____ 591-78-6——————2-Hexanone____________ 127-18-4——————Tet rachl oroethene_______ 79-34-5——————l,l,2,2-Tetrachloroethane_ 108-88-3——————Toluene______________ 108-90-7——————Chlorobenzene__________ 100-41-4 ——————Ethylbenzene___________ 100-42-5——————Styrene_______________ 1330-20-7—————Xylene (total)_________ 20 20 20 20 6 20 20 20 20 25 20 20 20 20 20 20 20 20 23 20 20 20 20 20 20 20 210 20 20 20 20 20 20 U U U U J U U U U U U U U U U U U U U U U U U U U U U U U U .(uL) FORM I VOA TUT OO6 O980 3/90 IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS 92 EPA SAMPLE NO. yab Name: ITAS-KNOXVILLE_________ ^^' Lab Code: ITSTU Case No.: 54182 Matrix: (soil/water) WATER Sample wt/vol: 5.0 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. ___ GC'Column: DB-624___ ID: 0.530 (mm) Soil Extract Volume: ______ (uL) Number TICs found: _0 Contract: SAS No.: MW4DL SDG NO.: MW1 Lab Sample ID: XX4809 Lab File ID: XX4809DL Date Received: 05/28/93 Date Analyzed: 06/03/93 Dilution Factor: ____2 .0 Soil Aliquot Volume: ___ .(uL) CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L CAS NUMBER COMPOUND NAME RT EST . CONC . Q FORM I VOA-TIC TUT OO6 O98.1. 3/90 1A VOLATILE ORGANICS ANALYSIS DATA SHEET '.ab Name*: ITAS-KNOXVILLE________ Contract: _ Lab Code: ITSTU Case No.: 54182 SAS No.: _ EPA SAMPLE TRIPBLANK SDG NO.: MW1 Matrix: (soi^water) WATER Sample wt/vol: 5.0 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. ___ GC Column: DB-624 ID: 0.530 (mm) Soil Extract Volume: ______ (uL) Lab Sample ID: XX4805 Lab File ID: XX4805 Date Received: 05/28/93 Date Analyzed: 06/01/93 Dilution Factor: ____1.0 Soil Aliquot Volume: ___ GAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L 74-87-3———————Chloromethane__________ 74-83-9———————Bromomethane___________ 75-01-4——————Vinyl Chloride_________ 75-00-3———————Chloroethane___________ 75-09-2———————Methylene Chloride______ 67-64-1———————Acetone_______________ 75-15-0———————Carbon Disulfide________ 75-35-4———————1,1-Dichloroethene______ 75-34-3——————1,1-Dichloroethane______ 540-59-0——————1,2-Dichloroethene (total) 67-66-3———————Chloroform____________ 107-06-2——————1,2-Dichloroethane______ 78-93-3———————2-Butanone_____________ 71-55-6———————1,1,1-Trichloroethane____ 56-23-5———————Carbon Tetrachloride____ 75-27-4———————Bromodi Chloromethane____ 78-87-5——————1,2-Dichloropropane_____ 10061-01-5————cis-1,3-Dichloropropene__ 79-01-6———————Trichloroethene_________ 124-48-1——————Dibr omochl oromethane______ 79-00-5———————1,1,2-Trichloroethane____ 71-43-2———————Benzene_________________ 10061-02-6————trans-l,3-Dichloropropene_ 75-25-2———————Bromoform_____________ 108-10-1——————4-Methyl-2-Pentanone____ 591-78-6——————2-Hexanone____________ 127-18-4——————Tetrachloroethene_______ 79-34-5———————1/1/2,2-Tetrachloroethane_ 108-88-3——————Toluene_______________ 108-90-7——————Chlorobenzene______________ 100-41-4——————Ethylbenzene__________ 100-42-5——————Styrene_______________ 1330-20-7—————Xylene (total)_________ 10 10 10 10 8 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 uuuu BJ uuu uuuuuuuuuu uuuuuuuuuuuu uuu .(uL) FORM I VOA TUT OO6 0982 3/90 IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS EPA SAMPLE HcJ.l Lab Name*: ITAS-KNOXVILLE_________ / Lab Code: ITSTU Case No.: 54182 Matrix: (soil^water) WATER Sample wt/vol: 5.0 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. ___ GC'Column: DB-624 ID: 0.530 (nun) Soil Extract Volume: ______ (uL) Number TlCs found: Contract: SAS No.: TRIPBLANK SDG No.: MW1 Lab Sample ID: XX4805 Lab File ID: XX4805 Date Received: 05/28/93 Date Analyzed: 06/01/93 Dilution Factor: __ 1.0 Soil Aliquot Volume: CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L .(UL) CAS NUMBER COMPOUND - NAME RT EST. CONC. Q FORM I VOA-TIC TUT OO6 0983 3/90 KNATIONAL .HNOLOGY CORPORATION Project Name/No. 1 3r". Sample Team Members 2 Profit Center No. 3 Project Manager4 Purchase Order No.6 Required Report Date 11 M f*< / - Ppc* ANALYSIS R( JEST AND CHAIN OF CUSTODY RECORD* f /Wy&*s7moles Shipment Date 7 Lab Destination j* Lab Contact 5. Project Contact/Phone l2.lLjV>t< Carrier/Waybill No.t3 //<W Reference Document^ Page 1 of / Bill to:5 _TT <: £ 6 £0 10 occ 0 ONE CONTAINER PER LINE SpeciaJJnstructions: 23 Possible Hazard Identification: 24 Non-hazard I Jl Flammable J Skin Irritant Poison B J| Unknown Sample Disposal: 2S . Return to Oient' J Disposal by Lab Archive (mos.J Turnaround Time Required: 26 Normal ffi. Rush IJ________ 1. Relinquished by (Signature/Affiliation) Date: Time: Project Specific ( 1. Received by 28 Qignatura/AffHiation) 2. Relinquished by (Signature/Affiliation) Date: Time: 2. Received by (Signature/Affiliation) Date:. Time: 3. Relinquished by (Signature/Affiliation) Date: Time: 3. Received by (Signature/Affiliation) Date: Time: Comments:29 TUT O06 Oc?84 MCA »1 VII