USVI Public Records

Document text

SDMS Document # 115569 DRAFT SOIL VAPOR EXTRACTION/AIR SPARGING (SVE/AS) PILOT STUDY REPORT VIRGIN ISLAND CHEMICAL SITE ST. CROIX, U.S. VIRGIN ISLANDS Prepared for : BERLEX LABORATORIES INC PHARMACIA & UPJOHN Prepared by , Colder Associates 304842 PROJECT No. 003-6016 OCTOBER 2000 Golder Associates Inc. 1951 Old Cuthbert Road, Suite 301 g ^ 2 ^ ^ W # Z L r f ^ l ^ / r & - s » Cherry Hili, NJ 08034 i t^^mW VflJMl|^i Telephone (856) 616-8166 ^m^ASSOClMeS Fax (856) 616-1874 - « a » - DRAFT SOIL VAPOR EXTRACTION/AIR SPARGING (SVE/AS) PILOT STUDY REPORT VIRGIN ISLAND CHEMICAL SITE ST. CROIX, U.S. VIRGIN ISLANDS Prepared for; Berlex Laboratories, Inc. 15049 San Pablo Avenue P.O. Box 4099 Richmond, CA 94804 and Pharmacia & Upjohn 7171 Portage Road Kalamazoo, MI 49001 # DISTRIBUTION: 3 Copies 1 Copy 1 Copy 1 Copy 2 Copies 1 Copy 1 Copy 2 Copies October 2000 US Environmental Protection Agency CDM - Federal Programs Corporation Berlex Laboratories, Inc. Pharmacia & Upjohn VIDPNR ERTEC Matrix Environmental & Geotechnical Services Golder Associates Inc. Project No.: ^ f\ A f\ A ^\ 304843 003-6016 OFFICES IN AUSTRALIA, CANADA, GERMANY, HUNGARY, ITALY, SWEDEN, UNITED KINGDOM, UNITED STATES Golder Associates Inc. 1951 Old Cuthbert Rood, Suite 301 Cherry Hill, NJ 08034 » - « ^ = W - M * Fax (856)616-1874 ->WBM»' October 20, 2000 Project No.: 003-6016 Ms. Caroline Kwan Remedial Project Manager U.S. Environmental Protection Agency, Region II Emergency & Response Division 290 Broadway, 20* Floor New York, New York 10007-1866 RE: DRAFT SVE/AS PILOT STUDY REPORT VIRGIN ISLAND CHEMICAL SITE, ST. CROIX, U.S. VIRGE^ ISLANDS Dear Ms. Kwan: On behalf of Berlex Laboratories, Inc. and Pharmacia & Upjohn, Golder Associates Inc. (Golder) is pleased to provide three (3) copies of the Draft Soil Vapor Extraction/Air Sparging (SVE/AS) Pilot Study Report for the Virgm Island Chemical Site located in St. Croix, U.S. Virgin Islands. Copies have also been transmitted directly to the Virgin Islands DPNR and CDM Federal Programs. As discussed during our meeting on October 10, 2000, this report expands upon and replaces Appendix A of the Draft Feasibility Study that was submitted on July 28, 2000. If you have any questions, please do not hesitate to contact Terry Grimmer of Berlex (510-262- 5495), Bill Gierke of P&U (616-833-2017), or either of the undersigned. Very truly yours, GOLDER ASSOCIATES INC. >usan A. Sciarratta, P.E. P. Stephen Finn, C.Eng. Project Manager Principal SAS:bjb G:\PROJECTS\003-60I6\Golder\SVE TS Report\cvrltr.doc Enclosures cc: SyedSyedali, VIDPNR Angela Arnold, VIDPNR Pamela Philip, CDM Federal Programs Norma Eichlin, MATRIX Terry Grimmer, Berlex Laboratories Jose Agrelot, ERTEC William Gierke, Pharmacia & Upjohn 304844 OFFICES IN AUSTRALIA, CANADA, GERMANY, HUNGARY, ITALY, SWEDEN, UNITED KINGDOM, UNITED STATES October 2000 -i- 003-6016 TABLE OF CONTENTS Cover Letter Executive Summary ES-1 Table of Contents i SECTION PAGE 1.0 INTRODUCTION 1 1.1 Purpose 1 1.2 Site Background 2 1.3 Treatment Technology Description 5 1.4 Description of Pilot Study Areas 8 2.0 PILOT STUDY APPROACH 2.1 Study Objectives 2.2 Permit Acquisition 2.3 SVE/AS System Equipment and Materials 2.3.1 Well and Probe Construction 2.3.2 SVE/AS System Equipment 2.4 Experimental Design 6 7 2.5 Data Management 21 3.0 RESULTS AND DISCUSSION 24 3.1 Physical Data '. 24 3.2 Chemical Data 24 3.3 Methods of Analysis 25 3.4 Phase I SVE Step Test 29 3.5 Phase 1 SVE Constant Rate Test 30 3.6 Phase II AS Step Test 33 3.7 Phase II SVE/AS Test 34 3.8 Phase II SVE/AS Extended Test 36 3.9 Groundwater Analytical Results 40 4.0 CONCLUSIONS AND RECOMMENDATIONS 41 4.1 Conclusions •. 41 4.1.1 Comparison to Objectives and Applicability as Potential Remedial Technology 41 4.1.2 Data Limitations and Uncertainties 42 4.2 Recommendations 43 4.2.1 Additional Testing / Monitoring 43 4.2.2 Long Term Operation 44 5.0 REFERENCES 46 Golder Associates -> n /i o yi rr J U 4 O 4 D October 2000 003-6016 TABLE OF CONTENTS (continued) LIST OF TABLES Table 1 Table 2 Table 3 Table 4 Table 5 Table 6 Table 7 Table 8 Table 9 Table 10 Table 11 Table 12 Table 13 Table 14 Table 15 Table 16 Table 17 Table 18 Table 19 Table 20 Table 21 Table 22 Table 23 Table 24 Table 25 Specifications for Pilot Study Wells and Monitoring Points System Testing Field Sampling Summary Comparison of Calculated and Measured SVE Flow Rates Phase I Step Test Results Phase I Constant Rate Test Results Phase I Constant Rate Test Analytical Determination of Well Efficiency, Radius of Influence (ROI), and Air Permeability Phase II Step Test Results - AST Area Phase II Step Test Results - FPP Area Phase II AS/SVE Test - System and Weather Measurements Phase II AS/SVE Test Results - AST Area Phase II AS/SVE Test Results - FPP Area Phase II Extended Test Results - System and Weather Measurements Phase II Extended Test Results - AST Area Phase II Extended Test Results - FPP Area Phase II Extended Test Phase II Extended Test Comparison of Laboratory and Field GC Analytical Data Phase II Extended Test Mass Removal Calculations - Laboratory Analytical Data at the Intake Port Phase II Extended Test Mass Removal Calculations - Field GC Analytical Data at the Intake Port Phase II Extended Test Mass Removal Calculations - Laboratory Analytical Data at the Exhaust Port Phase II Extended Test Mass Removal Calculations - Field GC Analytical Data at the Exhaust Port Groundwater Analytical Results - AST Area Groundwater Analytical Results - FPP Area Groundwater Analytical Results - Trip and Field Blanks LIST OF FIGURES Figure 1 Site Location Map Figure 2 SVE/AS Pilot Test Layout Figure 3 Typical SVE Well Figure 4 Typical AS Well Figure 5 Shallow/Intermediate/Deep VMP Cluster Figure 6 SVE/AS Schematic Figure 7 Phase I SVE Step Rate Test - Flow vs. Vacuum Data Figure 8 Phase I SVE Constant Rate Test, AST Area - Intermediate Probes Figure 9 Phase I SVE Constant Rate Test, FPP Area - Intermediate Probes Figure 10 Phase I Constant Rate SVE Test Contours of Vacuum of Intermediate Probes and SVE Wells, AST Area Figure 11 Phase I Constant Rate Test - Rate of Extraction Figure 12 Phase I Constant Rate Test - Cumulative Mass Removed Figure 13 Phase II AS Step Test- Flow vs. Pressure Data Golder Associates 304846 October 2000 -in- 003-6016 TABLE OF CONTENTS (continued) LIST OF FIGURES (con't) Figure 14 Phase II AS Step Test- Dissolved Oxygen Measurements, AST Area Figure 15 Phase II AS Step Test, Dissolved Oxygen, FPP Area Figure 16 Phase II SVE/AS Test, AST Area - Intermediate Probes - Vacuum Response Figure 17 Phase II SVE/AS Test, AST Area - Deep Probes - Pressure Response Figure 18 Phase II SVE/AS Test, Dissolved Oxygen, AST Area Figure 19 Phase II SVE/AS Test, Dissolved Oxygen, FPP Area Figure 20 Contours of Vacuum Levels for Phase II Extended Test Figure 21 Phase II Extended Test, Dissolved Oxygen, AST Area Figure 22 Phase II Extended Test, Dissolved Oxygen, FPP Area Figure 23 Phase II SVE/AS Extended Test, Total Cumulative Mass Removed - Comparison of Calculation Methods Figure 24 Phase II Extended Test Rate of Mass Extraction, Microseeps Data (Lab) Figure 25 Phase II Extended Test Rate of Mass Extraction, Photovac Data (Field GC) - Intake Port Figure 26 Phase II Extended Test Rate of Mass Extraction, Microseeps Data (Lab) - Exhaust Port Figure 27 Phase II Extended Test Rate of Mass Extraction, Photovac Data (Field GC) - Exhaust Port LIST OF APPENDICES Appendix A Permits Appendix B Boring Logs and Well Construction Diagrams Appendix C Groundwater Sampling Forms Appendix D Chain of Custody Forms Appendix E Form I's and Data Validation Golder Associates 304847 October 2000 ES-1 003-6016 EXECUTIVE SUMMARY A Soil Vapor Extraction / Air Sparging (SVE/AS) Pilot Study was conducted in Spring 2000 at the Virgin Island Chemical Site in St. Croix, U.S. Virgin Islands. The Pilot Study was conducted in order to evaluate the feasibility of SVE and SVE/AS in two study areas of the site: the Former Process Pit Area (FPP Area) and the Aboveground Storage Tank Area (AST Area). The FPP Area is primarily impacted by chloroform, and the AST Area is primarily impacted by ethylbenzene and xylenes. The main objective of the Pilot Study was to provide Site-specific data to evaluate the feasibility and effectiveness of SVE and SVE/AS as potential remedial technologies to remove volatile organic compounds (VOCs) in soil and groundwater in the AST and FPP Areas. A secondary objective of the Pilot Study was to develop design, performance, and cost data for the efficient operation of a full-scale system in one or both areas. The SVE/AS system network included the installation of six SVE wells in the AST Area, one SVE well in the FPP Area, and one AS well in each Area. In addition, clusters of vapor monitoring probes (VMPs), consisting of up to three probes at different depths, were installed at radial distances of approximately 5 feet, 10 feet, 20 feet, and 40 feet from the primary SVE well in each Area. The VMPs were used primarily to monitor pressure responses in the subsurface during system operation. One groundwater monitoring probe (GMP) was also installed within 3 feet of the primary SVE well in each Area in order to monitor water levels, including mounding effects. Pilot testing was conducted in three general phases. Phase I involved testing a single SVE well m each area, and included a step test and constant rate test. Phase II involved testing one SVE well plus one AS well in each Area, and also included a step test and constant rate test. In each case, the results of the step tests were used to determine the optimum operating points for the blower and air compressor for SVE and AS, respectively, during the constant rate tests. The third phase, designated the Extended Phase II test, was subsequently conducted involving the simultaneous operation of the entire SVE/AS system (i.e., all 7 SVE wells and 2 AS wells) over a duration of approximately three days. The test results for the AST Area indicated that a single SVE well located in this area exhibits a radius of influence (ROI) of about 20-25 feet. Due to heterogeneities in the subsurface, specifically intermittent sandy layers , the ROI is expected to vary and could be greater in some Golder Associates 304848 October 2000 ES-2 003-6016 locations within the AST Area, as observed in the field data. The field data and calculations for ROI, air permeability, and mass removal verify that SVE is a viable and efficient technology for removal of VOCs in the vadose zone in the AST area. Further, the observed vacuum responses, together with the calculated ROI, indicate that the existing network of six SVE wells should be adequate for full-scale SVE operation in the AST Area. The AS test results were similarly positive in the AST Area. Based on observed dissolved oxygen levels and pressure responses, AS achieved an ROI of 20 to 30 feet from the sparge well. Very substantial reductions of ethylbenzene and xylene were observed in groundwater during the course of the 3-day test, due to the combined effect of in-situ air stripping and enhanced aerobic biodegradation resulting from the introduction of sparge air. An estimated 70 to 90 pounds of VOCs were removed during all phases of the Pilot Study. It is concluded that SVE and SVE/AS are both feasible technologies for effective VOC removal in the vadose and saturated zones in the AST Area. SVE and SVE/AS testing in the FPP Area yielded inconclusive results as the applicability of mass removal data as an indicator of SVE/AS system performance was severely limited due to the extremely low residual source mass of chloroform that was initially present in soil and groundwater. Although some mass removal of chloroform was obtained during the Pilot Study, no appreciable changes were seen in groundwater conditions for chloroform in the immediate area of the SVE/AS system throughout the course of pilot testing. The physical data (e.g., vacuum/pressure responses, dissolved oxygen) indicated generally weak responses in the subsurface during both SVE and AS. This indicates poor airflow distribution, likely as a result of low air permeabilify and the development of preferential airflow pathways. It is concluded that implementation of an SVE or SVE/AS system in the FPP Area is not warranted due to the very low mass of residual chloroform present in soils and groundwater (i.e. generally below MCLs). Also, chloroform primarily biodegrades anaerobically and natural attenuation parameters measured during the Pilot Study and the RI (Golder, 2000) indicate that natural attenuation processes are important in degrading chloroform in groundwater. Therefore, operation of AS in the FPP area may inhibit existing anaerobic natural attenuation processes, which are addressing residual low-level concentrations that are currently near or below MCLs. Golder Associates 304849 October 2000 -1- 003-6016 1.0 INTRODUCTION This Report describes the pilot-scale Soil Vapor Extraction / Air Sparging (SVE/AS) Pilot Study that was conducted in Spring 2000 at the Virgin Island Chemical (VICHEM) Site located in St. Croix, U.S. Virgin Islands. Figure 1 presents the general location of the Site. The Pilot Study, or Treatability Study, was conducted pursuant to the USEPA-approved Draft Final Treatabilify Study Workplan (McLaren/Hart 1999). The field and laboratory work for the Pilot Study was carried out under the direction of McLaren/Hart, Inc. (McLaren/Hart). This Report was prepared by Golder Associates Inc. (Golder) on behalf of Berlex Laboratories, Inc. (Berlex) and Pharmacia & Upjohn (P&U), with assistance from former McLaren/Hart personnel. This Report is divided into the following sections: • Section 1.0 provides a brief Site background and description of the SVE and AS technologies; • Section 2.0 describes the procedures and methods utilized during the SVE/AS Pilot Study, including deviations from the EPA-approved Workplan (M/H, 1999); • Section 3.0 presents the results of the Pilot Study; and, • Section 4.0 provides an analysis of the results as they relate to the objectives of the study and relevant evaluation criteria. 1.1 Purpose Pilot studies provide site-specific data necessary to evaluate proposed remedial actions. They serve two primary purposes: (1) to aid in the selection of the remedy, and (2) to aid in the implementation of the selected remedy. Pilot studies conducted during the Remedial Investigation/ Feasibility Study (RI/FS) phase indicate whether a given technology can meet the expected cleanup goals for the site and provide important information for remedy selection. Additionally, data collected during this phase can be used to evaluate the design and operating parameters necessary for efficient technology performance and implementation of a sound, cost- effective remedy. Based on the information collected during the RI, two specific areas of concern were identified at the VICHEM Site; namely the Aboveground Storage Tank (AST) Area, primarily impacted with ethylbenzene and xylenes, and the Former Process Pit (FPP) Area, impacted by chloroform. Golder Associates 304850 October 2000 -2- 003-6016 Subsequent to the submittal of the Draft Remedial Investigation Report in January 1999, the potential feasibility of implementing soil vapor extraction (SVE) and air sparging (AS) in each area was discussed with EPA during a February 1999 meeting attended by McLaren/Hart, Berlex, and P&U. The parties agreed that further examination of SVE/AS as a potential remedial technology for source control of Site contaminants was warranted. Subsequently, the Pilot Study was conducted by McLaren/Hart and Environmental Resource Technologies (ERTEC) during the period February through May 2000. The primary objecfive of the Pilot Study at the VICHEM Site was to provide Site-specific data to evaluate the feasibility and effectiveness of SVE and SVE/AS as potential remedial technologies to remove volatile organic compounds (VOCs) in soil and groundwater in the AST and FPP Areas. 1.2 Site Background Site Description This section briefly summarizes data and information regarding the physical setting of the VICHEM Site, past operations, and previous investigative work. Background information included in this section was excerpted from the February 2000 Final Remedial Investigation Report (McLaren/Hart 2000) and the July 2000 Remedial Investigation Addendum (Golder 2000). More detailed informafion on Site history and background can be found in the RI Report. The Virgin Island Chemical (VICHEM) Site is located in the south-central portion of St. Croix in the U.S. Virgin Islands. The VICHEM Site is located on Plot 13Q of Estate Bethlehem Middle Works in the south-central portion of St. Croix, U.S. Virgin Islands (see Figure 1). Site access is via Route 66, which traverses the island east and west and abuts the south-southwest boundary of the Site. The VICHEM Site is bordered to the north and east by an intermittent stream, the River Gut, which originates north of the Site and drains to the Caribbean Sea. The VICHEM Site was initially developed during the early 1970's and a variety of pharmaceutical manufacturing and blending operations, under a number of different corporate entifies, occurred until 1982. However, specific timeframes for the operafion of the manufacturing processes are uncertain. In general, toluene, pyridine, and quinidine (chemicals used by many of the occupants) represent the historically largest volume spills or other releases at the Site. The Site is owned by the Charles H. Steffey Holding Corporation and is currently Golder Associates 304851 October 2000 003-6016 abandoned and overgrown with heavy vegetation. A chain-link fence was installed in Spring 2000 to encompass the Site boundary and secure the area. Over half the Site is covered by buildings and/or process equipment. Several structures remain on-site, including: Laboratory/warehouse building; Maintenance building; Nine reportedly empty (M/H, 2000) Aboveground Storage Tanks identified as T-3 through T-11, an unlabeled AST, and eleven concrete pads at former AST locations; Production area building; Stainless-steel and glass reactor areas (northwest of centrifuge building); Loading dock (former location of laboratory pit); Concrete storage pad adjacent to the loading dock and next to the scalehouse; Cooling towers; Generator building; Generator and fire pump building; and One 250,000-gallon fire water AST. Two storm drains are located on-site. The Central Storm Drain runs beneath the paved area between the laboratory and maintenance buildings. The Southern Storm Drain, where observed, is a concrete-lined depression along the southern wall of the maintenance building and the edge of the reactor area. Both storm drains discharge to the River Gut (M/H, 2000). Two former production wells, P-1 and P-2, also are located on-site. P-1 was sealed during RI field activities conducted in Spring 2000. Site Regulatory History In October 1982, EPA was notified of the facility's impending closure and off-site removal of waste materials. Between 1984 and 1991, several investigations were conducted at the Site by EPA, Island Chemical Company, and the VICHEM Company. The following six areas of environmental concern were identified through this investigative work: Laboratory and Warehouse Building; AST Area; FPP Area; Loading Dock/Former Laboratory Pit Area; Soil Beneath Concrete Pad Near ASTs (northern comer of Site); and Concrete Storage Pad (north of Laboratory and Warehouse Building). During the initial assessment stages of the VICHEM Site by the regulatory agencies, several response activities were conducted by both EPA and Berlex. These activities included soil Golder Associates 304852 October 2000 -4- 003-6016 excavation with on-site treatment (e.g., drying trays) or off-site disposal, drum removals, and off- site disposal of the AST contents. The VICHEM Site was placed on the National Priorities List (NPL) on January 18, 1994. On October 6, 1994, the U.S. Environmental Protection Agency (EPA) entered into an Administrative Order on Consent (AOC), Index No. II CERCLA-94-0401, with Berlex Laboratories, Inc. (Berlex), one of the respondents to the AOC. Pursuant to Section 106(a) of the Comprehensive Environmental Response, Compensation, and Liability Act (CERCLA), as amended, the AOC required the performance of a Remedial Investigation/Feasibility Study (RiypS) at the Site. Site Conceptual Model The VICHEM Site geology is characterized by approximately 85 feet of fill and Alluvial material overlying the clayey marl of the Kingshill Formation. Much of the fill appears to be reworked natural material and so its composition is very similar to the underlying Alluvium which is comprised of olive brown sandy-clay to sandy-silt, to clayey-sand with occasional amounts of clayey-gravel and sand in the upper 30 to 40 feet. Between a depth of approximately 30 to 60 feet below ground surface (bgs), the Alluvium is comprised mainly of a medium brown to gray clay with only occasional traces of fine sand and gravel. From approximately 60 to 90 feet bgs, the Alluvium consists of silty-clay and sand to medium to coarse sand and clay. Underlying the Alluvium is the Kingshill Form.ation, which is the principal water-bearing unit. Below about 100 feet bgs, the Kingshill is described as a light brown to white clay. The water table is typically encountered approximately 10 to 30 feet bgs and is subject to significant fluctuations due to seasonal changes and precipitation. The VICHEM Site hydrogeology is characterized by the presence of a largely unconfined to semi-confmed shallow (approximately 30 feet thick) alluvium aquifer with a predominant flow direction to the south- southeast. Underlying the shallow aquifer is an aquitard or aquitards, comprised of the stiff clay, between 30 and 60 feet bgs, which confines the lower Alluvium and acts as a significant hydraulic barrier isolating the upper Alluvium from the lower Alluvium aquifer and the underlying Kingshill Formation. The lower Alluvium aquifer exhibits a predominant flow direction to the southeast. Golder Associates 304853 October 2000 -5- 003-6016 A brief description of the constituents of concern (COCs) at the two areas of concern at the Site (i.e., FPP and AST Areas) is included in Section 1.4. A complete description of the Site conceptual model, including nature and extent of contamination and associated risks, is found in the RI Report (M/H, 2000), RI Addendum (Golder, 2000), and Draft FS Report (Golder, 2000). 1.3 Treatment Technology Description Technology Description Soil vapor extraction (also known as vacuum extraction, soil venting, or enhanced volatilization) is an accepted and proven technique for removing VOCs from subsurface soil, and is identified as a "Presumptive Remedy" for CERCLA sites with VOCs in soils (EPA, 1993). SVE is generally an in-situ technique by which the volatilization of VOCs is induced in the subsurface and the constituents are removed in extracted vapor. The use of SVE results in the reduction of VOC concentrations in the subsurface and consequently reduces the potential for further transport of contaminants (USEPA, 1991; USEPA, 1995). The transport and removal of VOCs by SVE may be controlled by one or more of the following processes: advection, volatilization, desorption and diffusion. During SVE, as air is drawn through the soil/waste mass, contaminants volatilize and are carried with the air through more permeable regions via advection. Removal induces further volatilization from the source materials. Contaminated areas that are not in contact with the advective flow of air rely on diffusion of contaminants toward zones of enhanced airflow. Diffusion is a much slower, rate- limiting process compared to advection (USACOE, 1995). The effecfiveness of SVE is typically limited to the vadose zone. Air sparging (AS) is an accepted technology for VOC removal in the saturated zone, typically in unconfined aquifers. AS is accomplished by injecting air under pressure below the water table. Consequently, VOCs located within airflow pathways will volatilize or biodegrade. There are two mechanisms that may work individually or together during AS: (1) injected air strips VOCs from soil and groundwater into the vapor flow, and (2) injected air increases the oxygen content of the groundwater, stimulating increased aerobic biodegradation. The sparge air provides a means of transport of VOCs from the saturated zone into the vadose zone, were they biodegrade or can be removed by SVE. Enhancements may include the injection of nutrients to increase biodegradation or heated air to increase volatilization. Golder Associates "^048^4 October 2000 -6- 003-6016 SVE systems generally consists of the following: (1) one or more vapor extraction wells, (2) vapor/liquid separator, (3) vacuum pump or air blower, (4) an impermeable barrier (optional), and (5) monitoring probes. Extracted vapors and liquids are monitored and handled accordingly. AS systems generally includes: (1) one or more air injection (sparging) wells, (2) compressor, (3) oil- coalescing filter, (4) particulate filter, (5) air dryer, and (6) monitoring probes. Vacuum gauges, pressure gauges, regulators, and flow meters are appropriately placed within the systems for monitoring purposes. Depending on emission levels and federal, State and local requirements, off-gas treatment (e.g., carbon adsorption, catalytic or thermal oxidation) may be required prior to atmospheric discharge. Design Considerations The critical factors that determine the viability of a SVE and/or AS system can be divided into three categories: (1) characteristics of the contaminant; (2) properties of the soil; and (3) site conditions. Contaminant Characteristics The extent to which contaminants volatilize is governed by the physical properties of the compounds, notably the Henry's Law constant (H) and vapor pressure (Pv). The Henry's Law constant describes the equilibrium partitioning of a chemical between the vapor phase and aqueous phase. The larger the Henry's Law constant, the more the constituent tends to partition into the vapor phase. The vapor pressure of a chemical describes the tendency of a chemical to evaporate and is described as the pressure exerted by that compound in the vapor phase at equilibrium with the pure compound (in solid or liquid form) in a closed system. Generally, compounds with a vapor pressure greater than 0.5 mm Hg and with Henry's Law constants greater than 0.01 (dimensionless) are amenable to SVE (USEPA, 1991). The physical and chemical properties of the Site COCs (chloroform, ethylbenzene, xylenes) are shown below (USACOE, 1995; NIOSH, 1990). Constituent Chloroform o-Xylene m-Xylene p-Xylene Ethylbenzene H (at 283" 0.074 0.123 0.177 0.181 0.140 K) Pv (mmHe. 298° K) 160 10 10 10 9.5 Water Sol. (mg/l 298° K) 5000 204 173 200 152-208 Golder Associates 304855 October 2000 -7- • 003-6016 Xylene and ethylbenzene are generally very amenable to SVE and AS. Chloroform is also considered amenable to SVE/AS, although to a lesser extent than the other constituents due to its relatively high water solubility and lower Henry's constant. All of the site COCs are considered to be amenable to SVE according to USEPA's presumptive remedy guidance (USEPA, 1993). Soil Properties Soil properties dictate how easily air, and associated contaminants, will move through the vadose zone. Critical soil properties include permeability, porosify, adsorption, and moisture content. The air permeability of a soil is a measure of the ease with which vapors flow through the soil. It is regarded as the most important parameter in the success of an SVE/AS system. Coarse- textured and poorly graded soils will generally have higher permeabilities than fine-textured and well-graded soils. Soils with an air permeability less than 10''° cm^ may not be amenable to SVE (USACOE, 1995). Optimum soil moisture content is also important for air permeability. Too high of a soil moisture content may contribute high volumes of condensate collecting in the SVE system and may reduce the abilify of air vapors to migrate in the vadose zone. Too low of a moisture content, or a desiccated subsurface, will tend to produce airflow channels as well as counteract biodegradation processes. Also, VOCs will tend to adsorb to soils more as the water content decreases. A high organic carbon fraction in the soil will also favor VOC adsorption to the soil rather than partitioning to the soil pore space. The shallow alluvium at the VICHEM Site consists of sandy clay to clayey sand sediments vvith lesser and varying amounts of silt and fine sands. Entrained within the matrix are lenses of gravels and sands. Based on lithologic data collected at the Site, these gravel and sand lenses are more prevalent in the AST Area than in the FPP Area. Fleterogeneities in the subsurface will tend to produce preferential airflow pathways in the more permeable zones. Site Conditions Site conditions that can affect the viability of an SVE/AS system include the depth to water, existence of preferential pathways such as subsurface conduits, and topography. An SVE system alone is not effective in extracting contaminant vapors if the groundwater table is very high (i.e., 5 feet bgs or less). High water levels will cause the system to shut down frequently due to upwelling of groundwater and flooding of screens. Short-circuiting may also occur, resulting in excessive ambient air intrusion via the ground surface. For AS, high water levels may limit Golder Associates 304856 October 2000 -8- 003-6016 compressed air from reaching the vadose zone. The average depth to the water table at the VICHEM Site in both the AST and FPP Areas is approximately 13 feet bgs. Subsurface conduits such as utility lines imbedded in sand, will usually create preferential flow pathways that may reduce the effectiveness of the system. There are no underground utility lines in either area. However, there is a storm drain constructed of polyvinyl chloride (PVC) pipe adjacent to the FPP Area. Prior to the Pilot Test, a concrete surface barrier was applied over the AST Area ground surface to limit short-circuiting of air; a concrete barrier already exists at the FPP Area ground surface. 1.4 Description of Pilot Study Areas AST Area The AST Area is located along the northwestern Site boundary. According to available information, twenty 8,500-gallon ASTs were originally located in this area. Six tanks were reportedly sold locally in the 1980s. Sometime between 1990 and 1994, four additional ASTs were removed and one was relocated within the AST Area. Ten tanks currently remain on-site within the AST Area. Historic analytical results and inspections identified a variety of liquids that were stored in the ASTs. These liquids primarily included toluene, xylenes, para- phenetidine, benzophenone, fluorenone, and ethanol. Soil samples were collected in the AST Area during the various RI field investigations. A total of 22 soil borings were completed in this area, with samples collected at various depth intervals. Likewise, groundwater samples have been collected during the RI from four monitoring wells, one former producfion well, five temporary monitoring wells, and one Geoprobe point located south of the area. The data collected from the AST Area during the RI identified ethylbenzene and xylenes as the predominant COCs impacting subsurface soil and groundwater. The impacted soil encompasses an area between Tanks 3 and 10, existing mainly on-site. The horizontal extent of impacts was conservatively assumed to encompass an area approximately 100 feet by 70 feet.' The zone of impacts is conservatively assumed to encompass a 20-foot interval at approximately 5 to 25 feet ' Based on a comparison of concentrations detected during the Remedial Investigation against USEPA's soil screening levels for migration to groundwater. The layout of the SVE wells was based on this estimated area. Golder Associates ^ . m-m 304857 October 2000 -9- • 003-6016 bgs, extending into the water table interface. The highest concentrations of COCs in subsurface soil were found in the vicinity of Tanks 8 and 9. Concentrations of ethylbenzene and xylenes detected in the two shallow monitoring wells located within the impacted soil area have exceeded federal Maximum Contaminant Levels (MCLs) over the course of several groundwater monitoring events. The horizontal extent of ethylbenzene and xylene contamination in soil and groundwater in the AST Area is depicted in Figures 12 through 14 of the FS Report. FPP Area The FPP Area is located in the central portion of the VICHEM Site. The process pit received wastewater from spills and cooling water from production operations. During plant operations, the contents of the pit were sampled to determine if any product had been released. The water was then reused in the system or, if the sample results did not indicate the presence of product, the water was discharged through the Central Storm Drain. Water and sludge were removed from pit in 1985 for off-site disposal and the pit was reportedly "abandoned and sealed with concrete" (M/H, 2000). However, during Geoprobe sampling conducted during the Phase III RI in March 1998, a large concrete monolith indicative of a subsurface pit was not encountered. Based on accounts from former Site workers provided to McLaren/Hart and Berlex, it is believed that this pit was never actually filled in with concrete. During the Phase III field investigation, a hollow concrete vault (measuring approximately 21.5 feet x 7.7 feet x 7.0 feet) was discovered in the vicinity of monitoring well MW-2. This vault is believed to be the FPP. Soil samples were collected in the FPP Area during the various RI field investigation phases. A total of 20 soil borings were completed in this area, with samples collected at various depth intervals. Likewise, groundwater samples were collected during the RJ from eight monitoring wells including one former production well and its replacement monitoring well, and numerous Geoprobe grab samples. The data collected from the FPP Area during the RI identified chloroform as the predominant COC impacting subsurface soil and groundwater. The impacted soil and groundwater encompasses an area in the vicinity of former RI groundwater sampling point GWPP-27 where the highest chloroform concentration in groundwater was detected historically. An approximate 400 ft^ area in the Former Process Pit (within the vicinity of MW-2) is estimated to be impacted with chloroform. The predominant zone of impacts is conservatively assumed to Golder Associates 304858 October 2000 -10- 003-6016 encompass a 5-foot interval at approximately 20 to 25 feet bgs, around the (fluctuating) water table interface. Chloroform concentrations in the one shallow monitoring well located within the impacted soil area, as well as Geoprobe grab samples collected in the FPP Area, have historically exceeded the federal MCL. The past extent of chloroform impacts in the FPP Area is depicted in Figure 15 of the FS Report. However, groundwater monitoring data from 2000, included herein, show chloroform concentrations above MCLs at only one location in the area of the suspected source of release, and the extent of chloroform impacts has significantly diminished over time. Golder Associates -^ « ,i «,-« 304859 October 2000 -11- 003-6016 2.0 PILOT STUDY APPROACH 2.1 Study Objectives The SVE/AS pilot study was performed at the VICHEM Site to provide Site-specific data to evaluate the feasibility and overall effectiveness of SVE and SVE/AS as potential remedial technologies for the AST and FPP Areas. Specifically, the objectives of the study included: • Verification that SVE and SVE/AS are viable technologies for the reduction of VOCs in subsurface soil and groundwater; and • Development of design, performance, and cost data for efficient operation of a full-scale system in one or both of the impacted areas. 2.2 Permit Acquisition The following permits were obtained" from the Virgin Islands Department of Planning and Natural Resources (VIDPNR) in preparation for the implementation of the Pilot Study: • Earth Change Permit - for intrusive digging such as installation of underground piping; • Well Permit - for installation of the SVE and AS wells, vapor monitoring points (VMPs), and groundwater monitoring points (GMPs); and • Permit to Construct and Operate - for construction of the SVE/AS system and operation of the system (including air emission requirements). Additionally, approval was obtained from the current property owner (Charles H. Steffey Holding Corporation) to install the SVE/AS system. Copies of all permits and approvals are provided in Appendix A. 2.3 SVE/AS System Equipment and Materials 2.3.1 Well and Probe Construction Figure 2 provides a layout of the SVE and AS wells, VMPs, and GMPs installed for the Pilot Study. ERTEC of San Juan, Puerto Rico installed the wells and monitoring points between CERCLA projects are exempt from the administrative requirements to obtain permits, provided the substantive technical requirements are satisfied (CERCLA §121(e)(1) and 40 CFR 300.400(e)(1)). In this instance, VIDPNR elected to issue permits, although they are not strictly required. Golder Associates T n 4 R fi n October 2000 -12- 003-6016 February 1 and 24, 2000. The wells and probes were constructed within the two study areas described in Section 1.4. SVE Well Construction One SVE well was installed in the FPP Area and six SVE wells were installed in the AST Area. For potential cost efficiency, the system was designed and constructed for future operation as a permanent system in the AST Area, with limited modifications. A radius of influence (ROI) of 25 feet was estimated for an SVE well at this Site. This ROI was selected based on ERTEC's previous experience with the design and installation of similar SVE systems in the Virgin Islands. Based on this ROI, it was determined that a total of six SVE wells would be needed to provide a capture zone that would exceed the area of impacted subsurface soil in the AST area. Soil borings were advanced using hollow stem auger (HSA) drilling techniques. Continuous split-spoon samples were collected to evaluate lithological conditions that might affect the pattern of air flow during system operation. Additionally, samples were screened for the presence of organic vapors using an organic vapor monitor (OVM). Each SVE well was constructed of 2-inch diameter, flush-jointed and threaded, 304 Schedule 5, stainless-steel riser. The screen sections were 15 feet in length and consisted of 0.020-inch, wire- wrapped, stainless-steel screen. To account for fluctuating water levels on St. Croix, a 5-foot sump was placed in the bottom of each SVE well to collect condensate or entrained water and to avoid flooding the screened interval. Wells were installed to a total depth of 24.5 feet bgs in the AST Area and 26.5 feet bgs in the FPP Area. Upon reaching the desired depth, the screen and riser was inserted within the augers to the bottom of the borehole. The AST Area SVE wells were screened from 4.5 to 19.5 feet bgs, and the FPP Area SVE well was screened from 6.5 to 21.5 feet bgs. Sand was poured into the annulus around the screen and riser (as the augers were removed) until approximately 2 feet of sand accumulated above the screen interval. After installation of the sand pack, approximately 2 feet of bentonite pellets was poured into the hole. After allowing the bentonite to hydrate/seal, the remaining annular space was filled with cement/bentonite to approximately 2 feet bgs. Each SVE well was completed with an 3-foot square, flush-mount cover that was secured in place with pre-mixed concrete. Golder Associates -^ n yi o r i J U4ot)X October 2000 -13- 003-6016 Downhole packers were placed in each SVE well to prevent groundwater extraction from occurring. The packers were set to a depth of 13-14 feet, as the water table was encountered at approximately 15 feet bgs at the time of the study. Well construction specifications for the SVE wells are provided in Table 1 and illustrated on Figure 3. Boring logs/well construction diagrams also are provided in Appendix B. GMP Well Construction A GMP was installed within 3 feet of one SVE well in each area to measure water levels and evaluate worst-case mounding effects due to AS during the Pilot Study. Hollow stem auger drilling techniques were used to install the two monitoring points to a total depth of 30 feet bgs (i.e., 5 feet below the lowest water level recorded during the RI). Each GMP was constructed of 1-inch diameter, flush-jointed and threaded. Schedule 40, PVC riser with a 1-foot section of 0.020-inch, factory-slotted screen at the bottom. Upon reaching the desired depth, the point was installed and completed in the same manner as the SVE wells. Each GMP was completed as a flush-mount with a PVC cap. Construction specifications for the GMPs are provided in Table 1, and construction diagrams are provided in Appendix B. AS Well Construction One AS well was installed in each area close to an SVE well and associated GMP. The AS location in the AST Area was selected based upon analytical data for both groundwater and soil, where the greatest concentrafions of ethylbenzene and xylenes in each medium coincided at similar locations and depth intervals. To ensure that the AS well was installed to a depth that was sufficient for full capture of the impacted zone through injection of air, the well was installed slightly deeper (50 feet bgs) than the limits of the impacted zone. In order to determine an appropriate location and depth for the AS well in the FPP Area, data collected from the FPP area during the RI were evaluated. The data indicated that chloroform impacts existed at the top of the water table down to approximately 34 feet bgs. Concentrations in deep monitoring well MW-7 (screened from 64 to 74 feet bgs) did not exceed MCLs during the RI monitoring events. Additionally, deeper samples collected in this area during the RI (sample location GWPP-27A) did not indicate that chloroform had migrated vertically in the FPP Area. However, in order to characterize the 35- to 60-foot zone and determine an appropriate depth for the AS well, a temporary well point was initially installed to a depth of 48 feet at the AS well Golder Associates 304862 October 2000 -14- 003-6016 location. A groundwater sample was collected from the 46- to 48-foot depth interval and analyzed for the Site Target Compounds prior to the installation of the AS well. There were no exceedances of MCLs by chloroform or other site target compounds in this sample. Upon approval by USEPA, the final depth of the AS well (48 feet bgs) was extended to the non- impacted zone considerably deeper than the lower limit of chloroform impacts (34 feet bgs). Each AS well was installed using the hollow stem auger drilling techniques described above. Lithologic conditions were similarly logged. However, since the lithology had been evaluated during the installation of the adjacent SVE wells, continuous split-spoon samples were only collected between the total depth of the adjacent SVE well (approximately 25 feet bgs) and the final depth of the AS well in each Area. Each AS well was constructed of 1-inch diameter, flush-jointed and threaded. Schedule 80, PVC riser with a 2-foot section of 0.040-inch, factory-slotted screen at the bottom. The AST Area AS well was screened from 47.5-49.5 feet bgs, and the FPP Area AS well was screened from 45.5- 47.5 feet bgs. Upon reaching the desired depth, the AS well was installed and completed in the same manner as the SVE wells. Each AS well was completed with an 18-inch diameter, flush mount manhole cover that was secured in place with pre-mixed concrete. Well construction specifications for the AS wells are provided in Table 1 and illustrated on Figure 4. Boring logs/well construction diagrams are provided in A.ppendix B. VMP Construction Three vapor monitoring probe (VMP) clusters, consisting of three VMPs each, were installed approximately 10 feet, 20 feet, and 40 feet to the south-southeast (hydraulically downgradient) of the SVE-1 well in each of the AST and FPP Areas. The locations are depicted in Figure 2. At each cluster, the three VMPs were installed to depths of 5 feet bgs (i.e., unsaturated shallow- depth zone), 15 feet bgs (i.e., unsaturated/saturated mid-point/intermediate -depth zone), and 30 feet bgs (i.e., saturated deep zone). These points were used to evaluate the ROI of the SVE well and AS well in each area and groundwater mounding caused by system operation. The deep (30- foot) VMP at each cluster locadon was installed prior to the intermediate (15-foot) and shallow (5-foot) VMPs, with continuous split-spoon samples collected down to depth to evaluate lithologic conditions. Golder Associates 3 0 4 8 6 3 October 2000 -15- 003-6016 Two additional VMPs were installed approximately 5 feet to the south of the SVE wells in the AST and FPP areas. At each cluster, the two VMPs were installed to depths of 15 feet bgs and 30 feet bgs. The intermediate (15-foot) VMP was installed to allow for the verification of a vacuum in the unsaturated zone during the Pilot Study. The deep (30-foot) VMP was installed to provide additional information on the ROI of the AS well, as well as groundwater mounding caused by system operation. As depicted on Figure 2, the VMPs were labeled according to distance from the primary SVE well and depth below ground surface. The "1" Series are located 5 feet from the SVE well. The "2", "3", and "4" Series are located 10 feet, 20 feet, and 40 feet from the SVE well, respectively. Shallow (S), intermediate (I), and deep (D) points correspond to depths of 5 feet, 15 feet, and 30 feet bgs. For example, "VMP-3S" is a shallow point located 20 feet from the SVE well. Each VMP was installed using hollow stem auger drilling techniques and was constructed of 2- inch diameter, flush-jointed and threaded. Schedule 40, PVC riser with a 3-foot section of 0.020- inch, factory-slotted screen at the bottom. Upon reaching the desired depth of each point, the VMP was installed and completed in the same manner as the SVE wells. Each VMP was completed with an 18-inch diameter, flush mount manhole cover that was secured in place with pre-mixed concrete. Construction specifications for the VMPs are provided in Table 1 and illustrated on Figure 5. Boring logs/well construction diagrams are provided in Appendix B. Vapor Barrier A vapor barrier was placed over the SVE/AS study area in the AST Area to prevent short- circuiting of the system. After clearing the area of debris, a steel reinforced concrete mixture was spread over the study area to form an approximate 3- to 4-inch concrete barrier. A 2- to 3-inch concrete layer already existed in the FPP Area, therefore no additional barriers were required. Management of Waste Residuals Primary waste residuals included soil cuttings generated from drilling and groundwater generated from well/probe development and purging. Materials were segregated by area (AST and FPP) and matrix (solid and liquid) and containerized in 55-gallon drums. At the completion of the Pilot Study, composite samples were collected from the drums and analyzed for the Site Target Golder Associates 304864 October 2000 -16- 003-6016 Compounds. All drums are currently staged on-site in each area, pending arrangements for their appropriate disposal. Personal protective equipment and general refuse/debris (i.e., plastic, cardboard, etc.) were disposed off-site in a non-hazardous landfill. 2.3.2 SVE/AS System Equipment As illustrated on Figure 6, the key components of the SVE/AS system were: Collection piping and manifold, including sample ports; Manual bleeder valve (dilution valve); Air/water separator and associated filters and positive displacement pump; Vacuum centrifugal blower; Discharge stack; Air compressor and associated filters; and Instrumentation such as a weather station, vacuum and pressure gauges, flow meters, and pressure regulators. The well head of each SVE well was connected to a manifold system that led to an enclosed treatment trailer located on an adjacent property. This mobile trailer housed the blower and associated equipment. Each SVE well head included a vacuum gauge; sample ports for measuring organic vapors, collecting soil-gas samples, and measuring air velocity; and a control valve to throttle the vacuum applied to the well. Each VMP was equipped with a vacuum gauge, while each AS well was fitted with a pressure indicator. Compressed air was injected into each AS well via a 5 HP air compressor and '/4-inch diameter, flexible tubing. Soil vapor was vacuum- extracted using a Rotron 5 HP EN6F72L regenerative blower. The maximum flow and vacuum of the blower are 225 standard cubic feet per minute (scfm) and 7.3 inches mercury (in Hg). The blower intake line was equipped with a flame arrestor and in-line air filter. The blower was also equipped with an air dilution valve, or bleeder, in order to maximize the operating range of the blower for SVE and to ensure compliance with VOC emission rate limits. Vapors were directed through an underground 2-inch diameter, PVC pipe to the trailer. A 10-gallon air/water separator and 55 gallon storage drum were provided in order to collect any entrained water. However, during the Pilot Study, no excess water accumulated in the separator. Golder Associates o n /i o ,r tr 304865 October 2000 -17- 003-6016 2.4 Experimental Design The Pilot Study was conducted in a phased approach, with results from each phase used to determine specific operating parameters for subsequent phases. The three phases included: • Phase I (SVE Testing) - one SVE well was tested in each area (AST and FPP); • Phase II (SVE/AS Testing) — one SVE well and one AS well were tested in each area; and • Extended Phase II (SVE/AS Testing) - a comprehensive test including all SVE and AS wells simultaneously (one SVE well and one AS well in the FPP Area, plus six SVE wells and one AS well in the AST Area). The specific sequence of events was as follows: Initial baseline monitoring event; Phase I step rate test; Phase I constant rate test; Post-Phase I monitoring event / Phase II baseline event; Phase II step rate test; Phase II constant rate test; Post-Phase II monitoring event / Extended Phase II baseline event; Extended Phase II constant rate test; and Post-Extended Phase II monitoring event. Baseline Monitoring Event The Pilot Study commenced with the collection of baseline samples/measurements in the AST and FPP Areas to evaluate conditions prior to Phase I testing. Specifically, the baseline monitoring included: • Depth to water measurements in all on-site monitoring/production wells, GMPs, and VMPs (if water was present); • Static vacuum pressure measurements from the VMPs in each area; • Weather conditions from the on-site station; • Soil-gas samples from the SVE well and VMPs in each area; • Groundwater samples from monitoring wells MW-1, MW-6, MW-8, MW-10, and the deep VMPs (i.e., 30-foot depth) in the AST Area using a low flow purging technique with a purge rate of about 0.5 liters/minute; and • Groundwater samples from monitoring wells MW-2, MW-3, MW-7, and the deep VMPs in the FPP Area. Golder Associates ? 0 4 8 6 6 October 2000 -18- 003-6016 In addition, ambient air readings were taken regularly with a portable organic vapor monitor (OVM) in the breathing zone downwind of the trailer throughout the pilot testing. Phase I Step Rate Test A step rate test was conducted using one SVE well in each area, to determine the optimal vacuum for the constant rate test. The step test was conducted by initializing the blower at a low vacuum and then increasing the vacuum at pre-determined intervals. Based on the observed ROI and extraction efficiency at the initial position, the next testing condition (i.e., vacuum) was determined. The test was conducted on March 21, 2000. The vacuums tested, in order, were 1.5 inches mercury ("Hg), 3 "Hg, and 5 "Hg measured at the blower. The influence of the different extraction rates on the ROI was monitored through the reading of vacuum gauges installed at the VMPs in each area. Additionally, vacuum and air flow rate measurements were collected at the SVE well in each area. System measurements consisted of air flow rate, vacuum pressure (intake and exhaust points), exhaust temperature, weather conditions, and ambient air concentrations (breathing zone) at a point downwind of the system discharge stack. Constituent removal rates were evaluated during the step test through the analysis of soil-gas samples and OVM readings taken at the SVE well in each area, select VMPs in each area, inlet to the SVE system (i.e., "V-1" as shown on Figure 6), and exliaust manifold (i.e., "V-2" as shown on Figure 6). Depth to water measurements were collected at the GMP in each area to evaluate mounding effects due to vacuum suction and air sparging. Phase I Constant Rate Test After evaluating the results from the step rate test, it was determined in the field that a vacuum of 5"Hg (at the blower) would be the optimum operating condition for the constant rate test. This test was initiated on March 23, 2000 and continued through March 26, 2000 for a total testing period of approximately 72 hours. The same parameters measured during the step rate test were monitored during the course of the constant rate test. The frequency of measurement collection was higher in the beginning of the testing period (i.e., every 1 to 2 hours), when the operating parameters were most variable. By the conclusion of the test, operating parameters reached stabilization, as indicated by the vacuum pressures and SVE air flow rate approaching constant values with minimal variation between successive measurements. Golder Associates 304867 October 2000 -19- 003-6016 Post-Phase I Monitoring Event Upon completion of the Phase I test, the system was turned off and a round of samples/measurements was collected to evaluate the efficiency of the SVE process in addressing the impacts in each area. Samples/measurements were identical to that collected during the initial baseline monitoring event. This event also served as a baseline for Phase II testing. Phase II Step Rate Test Phase II testing was initiated following the collection of post-Phase I samples/measurements. A step rate test was conducted prior to the Phase II test, during which one SVE well and one AS well in each area were on-line. With field concurrence from EPA's oversight contractor, CDM Federal Programs Corporation (CDM Federal), the Phase II step rate test focused on AS only since operating conditions for SVE were determined during the Phase I test. This test was conducted in each area to determine the optimal flow rate for the constant rate test and was implemented by initializing the air compressor at a low flow rate and then increasing the flow at pre-determined intervals. Based on the observed ROI at the initial position, the subsequent testing condition (i.e., flow rate) was determined. The AST Area step test was conducted on April 8, 2000 and began at a pressure of 45 pounds per square inch (psi) at the AS well (at a corresponding air flow rate of 0.8 to 0.9 standard cubic feet per minute [scfm]). Subsequent steps of 55 psi (2.6 to 2.7 scfm) and 64 psi (3.9 to 4.2 scfm) were tested. The FPP Area step test was conducted during the period April 4 through 7, 2000 and consisted of five different steps in order: 17 to 22 psi at the AS well (0.6 scfm), 16 to 19 psi (1.25 scfm), 20 psi (2.5 scfm), 21 to 23 psi (4.5 scfm), and 25 to 29 psi (7.2 scfm). The influence of the different flow rates on the sparging ROI were monitored through the collection of air pressure, depth to water, and dissolved oxygen (DO) measurements at the SVE well and VMPs in each area. Additionally, air pressure and flow rate measurements were collected at the AS well in each area. System measurements consisted of air pressure at the compressor and weather conditions. Constituent removal rates were evaluated during the step test through OVM readings taken at the SVE well and select VMPs in each area. Water levels were collected from the GMPs, and water levels and DO were collected at existing groundwater monitoring wells located in each area. Golder Associates •5n4fifiR October 2000 -20- 003-6016 Phase II Constant Rate Test After evaluating the results from the step rate test, it was determined that a pressure of approximately 50 psi, corresponding to a flow rate of 3.4 scfm, for the AST Area, and approximately 33 psi (7.2 scfm) for the FPP Area would be the optimum operating conditions for the constant rate test. Operating points for the constant rate test were generally determined by the most steady and distant responses at the monitoring points observed during step testing. The points were selected with field concurrence by CDM Federal. The SVE portion of the system was run at a vacuum of 5 "Hg (at the blower), as determined during Phase I testing. The Phase II test was initiated on April 14, 2000 and continued through April 16, 2000 for a total testing period of approximately 48 hours. The same parameters measured during the AS step rate test and the Phase I test were monitored during the course of the Phase II constant rate test. The frequency of measurement collection was higher in the beginning of the testing period, when operating conditions were most variable. Additionally, groundwater samples were collected from select monitoring wells/VMPs in each area during the test. However, holding times were exceeded due to FedEx customs issues and the samples were not analyzed. The Phase II test was concluded once stabilization was attained. Post-Phase II Monitoring Event Upon completion of the Phase II test, the system was turned off and a round of samples/measurements was collected to evaluate the efficiency of the SVE/AS process in addressing the impacts in each area. Sam.ples/measurements were similar to those collected during the initial baseline monitoring event. This event also served as a baseline for extended Phase II testing. Extended Phase II Constant Rate Test To evaluate the effectiveness of the potential full-scale system in the AST Area, an extended Phase II constant rate test was conducted as the final step in the Pilot Study. This test was similar to the Phase II test, except that all six SVE wells in the AST Area were utilized. The extended test was initiated on April 27, 2000 and continued through April 30, 2000 for a total testing period of approximately 72 hours. The same parameters measured during the Phase II constant rate test were monitored during the course of the extended Phase II test. Additionally, groundwater samples were collected from select monitoring wells/VMPs in each area during the test period. The extended Phase II test was concluded once stabilization was attained. Golder Associates '5n4ft6Q October 2000 -21- 003-6016 Post-Extended Phase II Monitoring Event Upon completion of the extended Phase II test, the system was turned off and a round of samples/measurements was collected to evaluate the efficiency of the SVE/AS process, specifically the potential full-scale SVE system in the AST Area. Samples/measurements were similar to that collected during the initial baseline monitoring event. 2.5 Data Management EieldData All raw field data and notes during the Pilot Study were recorded in field logbooks and sampling forms, signed by field personnel. The field data were later tabulated and reviewed for quality control. A summary of the test conditions described above and associated sampling is included in Table 2. Tables 3 through 15 provide the tabulated field data for each phase of testing. These data include weather conditions (i.e., temperature, wind speed, wind direction, relative humidity, barometric pressure, and van temperature ), pressure/vacuum measurements, water levels, dissolved oxygen (DO), and OVM readings. SVE/AS system measurements include: SVE air flow, air velocity, system vacuums (locations depicted on Figure 2), exhaust temperature, and compressed air pressure and flow. Chemistry Data As discussed above, groundwater, waste residual soil, and soil-gas samples were collected during the Pilot Study. Groundwater sampling forms are provided in Appendix C. (Groundwater sampling forms for the initial baseline sampling event in March 2000 were provided in the RI Addendum (Golder, 2000). Groundwater and soil samples were analyzed off-site by Pace Analytical Laboratory (Pace) of St. Rose, Louisiana. Groundwater samples were analyzed for the Site Target Compounds (acetone, chloroform, methylene chloride, ethylbenzene, toluene, and xylenes) using Contract Laboratory Program (CLP) methodology (i.e.. Statement of work for Organic Analysis, Multi-Concentration, Document OLM03.1, USEPA CLP, most current version). Addifionally, samples were analyzed on-site with a Chemetrics field test kit for carbon dioxide (CO2). Soil samples were analyzed for waste classification purposes. The van temperature was considered to be more accurate than the ambient air temperature, which was measured via a weather station on top of the trailer and was biased high due to radiative heat effects during sunlight hours. Golder Associates 304870 October 2000 -22- 003-6016 In order to expedite characterization and optimization of testing parameters, a PhotoVac gas chromatograph (GC) was utilized for on-site analysis of soil-gas samples using Method TO-14. The PhotoVac was equipped with a 10.6 eV photoionization detector (PID) lamp, capable of detecting toluene, ethylbenzene, and total xylenes (TEX) at relatively low concentrations (10 to 20 parts per billion [ppb] range). However, this instrument could not easily detect the remaining Site Target Compounds (acetone, chloroform, and methylene choride) at an adequate concentration range. Therefore, soil-gas samples were additionally analyzed off-site for the Site Target Compounds by Microseeps Laboratories (Microseeps) of Pittsburgh, Peimsylvania using Method AM 4.03. All soil-gas samples collected from the FPP Area were analyzed off-site by Microseeps. Samples collected in the AST Area were analyzed on-site with the PhotoVac, with a percentage of the total number of collected samples analyzed off-site by Microseeps (to confirm the PhotoVac results and to determine concentrations of remaining Site Target Compounds). All laboratory chemical analyses were conducted in accordance with the Draft Final Treatability Study Workplan (M/H, 1999); USEPA Region IPs CERCLA Quality Assurance Manual, Revision I (USEPA 1989); and other applicable EPA requirements (Level I through Level FV), including data validation and quality assurance/quality control (QA/QC). Chain-of-custody records for the samples collected during the Pilot Study are provided in Appendix D. The laboratory analytical Form I's are provided in Appendix E. Data validation summaries are presented in Appendix E. Quality Assurance/Quality Control The primary objective in instituting QC procedures during the Pilot Study was to promote uniformity, consistency, and accuracy in data collection and recording, so that the data could be evaluated and interpreted with greater reliability. In order to collect and record data in a uniform manner, controlling documents that described and specified QA/QC procedures for the Pilot Study were used. The documents used to guide and direct procedures throughout the study included: • Draft Final Treatability Study Workplan (McLaren/Hart 1999); • Region II CERCLA Quality Assurance Manual, Revision 1 (EPA 1989); • Guide for Conducting Treatability Studies under CERCLA, Final (EPA 1992); and Golder Associates 1 0 4 8 7 1 October 2000 -23- 003-6016 • Guide For Conducting Treatability Studies Under CERCLA: Soil Vapor Extraction, Interim Guidance (EVA 1991). The EPA-approved Draft Final Treatability Study Workplan specified and described all QA, QC, analytical, data management, and reporting procedures for the Pilot Study. Additionally, data quality objectives (DQOs) were established for field and analytical data using the DQO levels defined by EPA. By providing a framework for sample collection, decontamination, field QC, sample identification, chain-of-custody, and sample handling procedures, the controlling documents helped to ensure that high quality data were collected and that data comparability was enhanced. All data were collected as specified in the EPA-approved workplan. Field measurements were performed in accordance with procedures ouflined in this plan. All monitoring instruments were calibrated either before each use, at the beginning of each field day, or at the frequency specified for each procedure. All sampling equipment that came in contact with sample media was decontaminated (unless disposable equipment was used), as specified in the workplan, before each sample was collected. All sample collection, chain-of-custody, and sample shipping procedures were carried out as specified in the workplan. As part of the sample collection and analysis effort, field QC samples were prepared to monitor the performance of the analytical laboratories (both on-site and off- site), and to check on field sampling procedures. Data validation was performed by ALPHA Environmental Consultants, Inc. of Latham, New York for all groundwater data under contract to McLaren/Hart. Data validation packages were evaluated by Golder to ensure that data was qualified in accordance with USEPA Region II protocols. The validation process involved review for compliance with holding times, instrument calibration, method and laboratory blanks, instrument tuning and performance data, and constituent quanfification. Results of duplicate, matrix spike, and other QC samples were used to assess precision and accuracy of the analytical data and potential matrix effects. Data qualifiers were applied, where required, so that the qualitative and/or quantitative reliability of the results could be assessed. Validation findings are included in Appendix E as part of the data validation package for each sample delivery group. Golder Associates ?n4R7!? October 2000 -24- 003-6016 3.0 RESULTS AND DISCUSSION 3.1 Physical Data Borehole logs are included in Appendix B. Boring logs from the SVE well installations and VMP installations revealed a significant sandy layers exists in the AST Area. The layers range in thickness from 4 feet to 8 feet, and occurs at depths from 6 feet to 20 feet below ground surface. The shallow probes are screened at 5 feet (i.e., above the sandy layer), the intermediate probes at 15 feet (i.e., within the sandy layer), and the deep probes at 30 feet (i.e., below the sandy layer). In the FPP Area , the boring logs also indicate a sandy layer or layers although it is not as extensively as in the AST Area. Based on the VMP-2D log, the sandy layer in the vicinity of that probe only occurs from 6 feet to 8 feet bgs. In the S,VE well log and the VMP-3D and -4D logs, the sandy layer ranges from 4 feet to 8 feet thick and occurs at 10' to 20' below ground surface. Table 1 provides a summary of the well and probe construction data, as discussed in Section 2. Table 2 provides a summary of all of the field sampling conducted during the Pilot Study. Tables 3 through 17 generally provides results of the field data collected throughout each phase of the Pilot Study. Individual tables are referenced as appropriate in the subsequent sections. 3.2 Chemical Data Soil gas laboratory analytical data from the Phase I Constant Rate Test are shown in Table 6. Similar data from the Phase II Extended Test are shown in Table 16, and Phase If field analytical data are shown in Table 17. A comparison of the laboratory and field soil gas data from the Phase II Extended Test is presented in Table 18. More discussion of these results is included in the discussion of mass removal rates later in this section. The validated and qualified laboratory results for the various rounds of groundwater sampling during the Pilot Study are shown in Tables 23, 24 and 25. Natural attenuation parameters, which were measured at the time of certain groundwater sampling rounds, are included in these tables for completeness, but their discussion is beyond the scope of this Report. A detailed discussion of natural attenuation and the associated Site-specific parameters is presented in the FS Report (Golder, 2000). Golder Associates 304873 October 2000 -25- 003-6016 3.3 Methods of Analysis This section describes the methods of analysis that were used to interpret the physical and chemical data from the Pilot Study to evaluate the SVE/AS system performance. The following is a brief review of the analytical methods used. Generally, the results of these evaluations are discussed in the following secfions that are specific to each phase of the Pilot Study. SVE Performance Indicators Flow versus Vacuum Analysis The performance of an SVE system can be measured in a step test by plotting the measured flow rates versus applied SVE well pressures. This analysis provides information for determining optimal operating conditions and indicates the potential viability of a site for SVE. Plan View Vacuum Contour Plots To view the measured responses in the field utilizing the SVE well data in addifion to VMP responses, two-dimensional plots of vacuum contours were constructed using SURFER contouring software. Since the SVE wells were screened from approximately 5-20' bgs, the intermediate-depth probes (i.e., screened from 13-15' bgs) were selected for plotting purposes. These plots reveal the areal extent of the SVE influence. Radius of Influence (ROI) Analysis Two analyses were performed to assess the ROI of the SVE wells. Distance-drawdown plots were consh-ucted which plot measured vacuum at the VMPs versus distance from the SVE well on semi-log axes. Regression lines are fit to the data and the point at which the lines cross the x- axis (i.e., ambient atmospheric pressure) indicates the ROI. An analytical estimate of the ROI from test data was also performed. The analytical solution for ROI is based on the radial steady-state relationship (USACOE, 1995) as follows: R, = Rw exp{[(PA' - P„^) ln(r/R„)]/[Pr - ? J ] ) where: Rw = radius of the extraction well PA = absolute atmospheric pressure Pw = absolute pressure at the extraction well Golder Associates 304874 October 2000 -26- 003-6016 r = radial distance of the VMP from the extraction well Pr = absolute pressure at radial distance r from the extraction well. It is not appropriate to use the measured vacuums in the extraction well in the calculation of radius of influence, or in air permeability calculations, due to the head losses exhibited between the well and its packing. The extraction well pressure, P^, was therefore calculated using the steady-state pressures at two monitoring points within the radius of influence of the well (USACOE, 1995): P.! where: HrJRJP^,'-\n{rJRJP^^' \n{r^lrO Pri = absolute pressure at monitoring point 1 Pr2 = absolute pressure at monitoring point 2 ri = radial distance of the monitoring point 1 to extraction well Xj = radial distance of the monitoring point 2 to extraction well. The values obtained for Pw from the above equation were compared to the actual pressures or vacuums observed at the gas extraction well. The ratios of predicted P^ to actual Pw' provide an estimate of the overall average well efficiency. A low well efficiency indicates a high amount of head loss in the well (e.g., through the well screen). Air Permeability Air permeability (ka) is a measure of the ability of vapor to flow through the air-filled pore space of a medium such as soil. It is a critical parameter to determining the viability of an SVE or SVE/AS system. To calculate ka, which incorporates the estimated radius of influence (ROI), the following steady state radial flow equation was used (Pederson and Curtis, 1991): ka = Q ^l ln(Rw/Rl) / { [ H n Pw][l-(Pa«r/Pw)'} where: Q = volumetric flow rate p, = vapor viscosity Rw = radius of extraction well Ri = estimated radius of influence Golder Associates 304875 October 2000 -27- 003-6016 H = length of extraction well screened through vadose zone Pw = pressure at extraction well Patm = atmospheric pressure. Once again the effective Pw calculated using steady-state pressures at two monitoring points was used, as described above. Determination of Flow Rate and Velocity System flow rates and velocities were determined by two primary means. A flow meter located on the suction side of the blower (Figure 6) measured flow in standard cubic feet per minute (scfm) for the whole system (i.e., AST and FPP areas together). Partitioning of flow rates between the AST and FPP areas was determined by using hand-held anemometers at the SVE well heads through measuring ports (Figure 3). Table 3 compares flow rates determined from velocity measurements and from the flow rate gauge. The results show that velocity measurements in the earlier tests were likely biased low, but measurement accuracy improved markedly in the later tests. Velocity measurements generally were not considered accurate in earlier tests due to inappropriate calibration procedures. Individual flow rates based on the velocity measurements were used minimally in this report (see section 3.2.5), whereas the flow gauge located at the blower was typically used for total system flow rate data. In the future, accurate velocity measurements at individual SVE well heads would be useful in determining the mass removal rates at each SVE well. Air Sparging Performance Indicators Flow versus Pressure Analysis Similar to the flow versus vacuum analysis, this relafionship yields information on the optimal operating condition for the sparge system, and indicates the potential viability of AS at a site. Distance-Pressure Analysis Similar to distance-drawdown analysis, this relationship provides one method for analyzing the areal influence of the sparge system. Pressures measured at monitoring probes are plotted versus distance from the sparge well on semi-log axes, and a regression line drawn to the data. The point at which the regression line intersects the x-axis (i.e., ambient atmospheric pressure) serves as an indicator of the ROI. Golder Associates 3 0 4 8 7 f i October 2000 -28- 003-6016 Dissolved Oxygen Dissolved oxygen (DO) is the most common parameter used for estimating air sparging influence (Marley and Bruell, 1995). After only a few hours of sparging, groundwater DO levels may be observed to increase significantly at one or more monitoring points around the sparge well. The use of DO data is limited, however, in that an observed DO increase may reflect a localized increase in the vicinity of a preferred air channel, resulting in falsely high estimations of ROI. Conversely, DO uptake may occur by abiotic (e.g., oxidation of metals) or biotic (e.g., biodegradation of organics) processes, giving falsely low estimations of sparge influence. Despite these limitations, DO is regarded as an important parameter for the design and monitoring of an air sparging system. Groundwater Mounding In some instances, the groundwater table is observed to "mound"; that is, the water table rises in the vicinity of the sparge well in response to the added volume of injected air. This is sometimes used as an indicator of sparge radius of influence; however, it can overpredict the actual ROI depending on soil conductivity, as mounding may spread laterally beyond the true ROI. Also, concerns have been raised on the validity of measuring mounding in monitoring points open to the atmosphere, as they are thought to exaggerate the effect (Marley and Bruell, 1995). Several monitoring wells were used in the pilot test to record groundwater mounding. Mass Removal Rates The ultimate performance measure of an SVE/AS system is the ability to remove volatile contaminants from the subsurface. Analytical chemistry data is combined with airflow rates developed by the SVE system to quantify mass fluxes and total mass removal. Mass removal rate is calculated from the product of concentration and airflow rate as follows: Mass removal rate [lb/day] = Cone [ppmv] * MW/24.5*(P/Po) * (To/T)*Q [ftVmin] * 28.32 L/ft' * 1440 min/day * 2.2e-9 Ib/ug where MW = molecular weight of compound; P = Pressure of extracted air; Po = Standard pressure (1 atm = 407 "H2O); T = Temperature of extracted air; To = Standard temperature (298.15 K); and, Q = air flow rate. Golder Associates 304877 October 2000 -29- 003-6016 The cumulative mass removed is obtained by first calculating the mass removed over the sampling intervals. The mass removal rate is assumed to be constant for the time interval bounded by the halfway points between successive samples. For example, if samples were taken at 5, 11 and 15 hours after the start of the test, the time interval representative of the 11-hour sample would be from 8 to 13 hours, or 5 hours total. The mass removal rate calculated at the 11- hour sample is assumed to be constant over this time interval. The cumulative mass removed is determined by summing the masses removed over all sampling intervals. Trends in extraction rates over time and cumulative extraction rates were evaluated in order to determine the success of the pilot-scale SVE/AS system and to estimate a future sustainable mass removal rate. Also, the extraction rates were compared to the emission rate stipulated in the air permit (VIDPNR "Permit to Operate" Permit Number: STX-559-A-99-PO) of 13.62 lb/day total VOCs. 3.4 Phase I SVE Step Test The SVE step test provided information to determine the relationship of flow rate to applied vacuum. The flow rates for each area were calculated by apportioning the total system flow, measured at the inlet to the blower, between the AST and FPP Areas. The ratio of AST flow to FPP flow was determined by averaging the velocity measurements taken at the AST and FPP SVE wells over the duration of the test. This procedure resulted in a four to one ratio of AST flow to FPP flow. The data collected during the test is presented in Table 4. Figure 7 shows the flow rate-vacuum data for the AST and FPP areas from the Phase I Step Test. In both Areas, the flow-vacuum relationship is inverted to that which would be normally expected in that the SVE flow rate is lower at higher applied vacuums. Normally, a higher vacuum would be expected to induce a greater flow rate. In the subsequent constant rate test, the flow-vacuum relation was inverted also, with the vacuum level decreasing over the course of the test while the flow rate increased. The levels of vacuum and flow rate achieved were similar in the tvvo tests, as applied vacuums of 5 in Hg induced 90-100 scfm of flow, and 3-3.3 in Fig induced 135-136 scfm of flow. In the Phase II extended test, different operating points were used, so a direct comparison of values is not appropriate, but similar results were obtained in that SVE well head and the blower intake pressures decreased significanfly over the course of the test, while flow Golder Associates , 304878 October 2000 -30- 003-6016 rates increased moderately. Blower intake pressures decreased because the dilution valve at the blower was being opened during the course of this test. An inverted flow vs. applied vacuum relafionship is possible in an SVE system. This effect is typically due to expansion of the saturated zone caused by the induced vacuum. The expansion causes the saturated zone to expand above the natural water table and results in restricted flow to the SVE well. Another explanation for this effect is that leaks may be present in the system, or that higher applied vacuums caused the movement of silts or other fine particles into the screen of the SVE well. The flow rates achieved in the FPP area (i.e., 20-30 scfm) were significantly lower than in the AST Area (i.e., 80-120 scfm), for the same applied pressures. This indicates that the subsurface of the AST Area exhibits a greater air permeability than the FPP Area, probably as a result of the permeable sandy layer that was evident in the soil boring logs. Summary The Phase I Step Rate test resulted in a flow vs. vacuum curve that exhibited an inverted relationship. The test results indicate that the subsurface in the AST Area is generally less resistant to air flow, i.e., more permeable, than the FPP Area. 3.5 Phase I SVE Constant Rate Test The SVE constant rate test provided several important system performance parameters including SVE radius of influence, air permeability, and mass removal estimation from SVE alone. Table 5 presents the data collected during the test. Radius of Influence Analysis Two analyses were performed to assess the ROI of the SVE wells in the AST and FPP areas. Distance-drawdown plots were constructed and an analytical estimate of the ROI from test data was also made. Observed vacuum responses at the VMPs were moderately variable over time. In the AST Area, VMP vacuum levels tended to increase with time, whereas the system vacuum levels decreased with time. In VMP-II, for example, the inifial vacuum was 0.8 "H2O; it decreased to 0.5 "H2O after 5 hours, then increased to 0.8-0.9 "H2O after 11 hours, and increased again to 1.2-1.3 "H2O Golder Associates 304879 October 2000 -31- 003-6016 after 48 hours. VMP-21 exhibited similar results, increasing over the duration of the test. No or poor response (i.e., less than 0.1" vacuum) was observed in the VMP-3 and VMP-4 series probes in the AST Area. Figures 8 and 9 present distance-drawdown data for the intermediate VMPs in the AST and FPP Areas. Data is plotted for steady-state conditions only, represented by the beginning of the third day of the test (March 25, 2000) at 0730. The data are shown in Table 5. The data are presented with logarithmic regression lines fit to each round of measurements. The greatest and most consistent responses were, by a large margin, measured in the intermediate probes VMP-II and - 21 (5' and W from SVE-1) in the AST area, compared with all other VMPs in the AST or FPP areas. Figure 8, which shows the data for the intermediate probes in the AST area, reveals a steady decreasing trend in vacuum response from the 5 foot to 20 foot probes. The regression line crosses the x-axis (i.e., atmospheric pressure) at 30 feet. Assuming that the effective ROI is more likely represented by vacuum readings of 0.1-inch or greater, the plot indicates that the ROI would be about 25 feet. Given the observed responses, the true expected ROI in the AST Area is probably between 20-25 feet. Given the local variability in geology, the ROI for some wells may be greater (e.g. AST-SVE-2). Pressure measurements were taken at the other SVE wells during the test, and these responses are shown along with the VMP-I probes in Figure 10 a contour plot of vacuum levels. The plot represents time after steady state has been reached. A response is measured at SVE-2 but not at SVE-3 or SVE-4, revealing a non-uniform response in different directions from the SVE well. This is indicative of anisotropy within the horizontal plane of the subsurface. In the FPP Area, no consistently strong vacuum responses were obtained in any of the VMPs with the excepfion of VMP-II and VMP-2D. Figure 9 shows that the magnitude of the responses in the FPP area were significanfly less than in the AST area. VMP-II showed responses up to 0.165 "H2O, but no significant responses were ever recorded at VMP-2I, indicating an ROI of less than 10 feet. VMP-2D, which is 10 feet from the SVE well, showed responses up to 0.25 "H2O, despite the general lack of measurable responses at VMP-ID, which is 5 feet from the SVE well. Because the deep VMPs were screened below the water table, much weaker or no vacuum responses would be expected at these probes during SVE operation. Golder Associates 304880 October 2000 -32- 003-6016 In using the analytical prediction method for ROI, a sampling point was chosen after the system reached steady state. One data point for the FPP Area was analyzed since the vacuum response was greater than 0.1 "H2O for only a brief period during the test. The results are presented in Table 7. The calculated ROI values for the AST Area range fi-om 15 to 22 feet, and a value of 10 feet is calculated for the FPP Area. In addition, the comparison of the predicted vacuum at the SVE well to the actual vacuum of the SVE well in each area shows about a 34% well efficiency in the AST Area, which is in the expected range for a typical SVE well. The well efficiency in the FPP Area is less than 1%, which indicates extreme head loss in the SVE well, and suggests that analytical results may be of questionable value. Air Permeability The results of the air permeability calculations are shown in Table 7. The air permeability calculated for the AST area was approximately 10"^-10'^ cm^. A value of approximately 10''' cm^ was calculated for the FPP Area, but is questionable accuracy given the poor performance of the extraction well and very limited responses at monitoring points. Mass Removal Estimation Estimates of the mass removal of ethylbenzene, total xylenes and chloroform are presented in Table 6b, using the Microseeps analytical data presented in Table 6a. The data from the Intake port was used in the calculations. Figure 11 shows the exfraction rates of individual and total COCs at various points throughout the Phase I constant rate test. As expected, the initial mass removal rates were large, followed by a decline. However, the extraction rates increased at the end of the test. Figure 12 shows the cumulative mass removed for the COCs during the Phase 1 constant rate test. The total mass removed over the 72-hour test was about 3.05 lbs. Summary The Phase I Constant Rate test resulted in strong pressure responses in the intermediate vapor probes in the AST Area. This was supported analytically by high estimates of air permeability. The estimated ROI for SVE wells is about 20 feet to 25 feet. The pressure responses in the FPP Area were much lower in magnitude and extent than in the AST Area, and the estimated ROI for an SVE well is less than 10 feet. Golder Associates 7 n 4 f f f t 1 October 2000 -33- 003-6016 3.6 Phase H AS Step Test The Phase II AS Step Tests provided performance information on the flow-pressure relationships and operating set points for the AST and FPP Areas. The AST and FPP sites were tested separately, based on the available equipment, and the field data are presented in Tables 8 and 9. Flow-Pressure Data The sparge flow versus pressure data is presented in Figure 13. The data show a positive relationship between flow and pressure, as flow increases by increasing the pressure from the air compressor. The measured pressures required in the FPP area were significanfly lower than in the AST area, and flows achieved were apparently higher as well. The sparge pressure required to initiate air sparging in the AST area can be predicted as follows (Marley and Bruell, 1995, and Nyer and Suthersan, 1993): Depth of sparge point = 48 ft (top of well screen) Depth to water = 15 ft Specific gravity of sediments = 2.7 Porosity = 0.35 Pressure of soil at sparge point = (48 ft)(l-0.35)(2.7*62.4 lb/ft^)(ftVl44 m^) = 36.5 psi Pressure of water at sparge point = (48-15 ft)(0.35)(62.4 Ib/ft^)(ft^/144 in^) = 5.0 psi Release pressure = 1 psi for evety 3 ft of depth = 48/3 = 16.0 psi Total pressure = 36.5 + 5.0 + 16.0 = 57.5 psi The release pressure accounts for both frictional losses in the system and the capillary entry pressure required to displace the pore water (Nyer and Suthersan, 1993). The calculation indicates that 57.5 psi is required to overcome the pressures at a depth of 50 feet to initiate sparging. The sparge point in the FPP area is 46 feet below ground surface, and the total pressure required to inifiate sparging is 55 psi. These predicted values compare favorably with the pressures measured in the sparge test for the AST area, but not in the FPP area (Tables 8 and 9). There is no ready explanation for this difference. A possibility is that air channeling or short- circuiting (such as along the well annulus) occurred, which would result in higher flows with lower pressures in the FPP area. For example, there may have been channeling via the nearby Central Storm Drain. In later tests, significant bubbling occurred within MW-2, a shallow well Golder Associates 304882 October 2000 -34- 003-6016 near the FPP sparge well, indicating the interception of an air channel. However, bubbling was not observed during the step test. Dissolved Oxygen (DO) DO data for the test are plotted in Figures 14 and 15 for the AST and FPP Areas, respectively. Figure 14 shows that DO increases to saturation levels for AST-VMP-ID, -2D, and MW-1. MW-1 is located approximately 28' from the sparge well, indicating a significant influence. AST- VMP-3D (which is 20 feet from the sparge well) was only moderately affected, indicating the heterogeneous nature of the Site. The magnitude and breadth of the sparging influence in the FPP Area was not as significant as in the AST Area, even though the test was run for over 72 hours (albeit not continuously), compared with 9.5 hours for the AST Area test (see Figure 15). In the closest probe to the sparge well, FPP-VMP-ID, DO reached a maximum of 3.0 mg/L. A greater response was seen in FPP-VMP- 2D, which attained a maximum DO of almost 7 mg/L (compared to 20 mg/L in the AST area), but this level was not sustained. Summary Flow-pressure plots revealed that a normal relationship was observed between flow and applied pressure in both the AST and FPP areas. The analytically predicted pressure agreed with the level attained in the AST area, but was significantly higher than in the FPP area. This indicates that sediment fracturing or short-circuiting may have occurred. In the AST Area, saturated dissolved oxygen levels were measured at a 10 foot radius in the vapor probes, and at 28 feet away in MW-1. The DO results in the FPP Area showed much less effect, as the probes 5 feet and 10 feet from the sparge well attained only 3 mg/L and 7 mg/L, respectively. 3.7 Phase 11 SVE/AS Test The Phase II SVE/AS Test provided information on combined air sparge and SVE performance, and confirmatory information on ROI, air permeability, and DO influence. Field data from this test are presented in Tables 10 to 12. Golder Associates 304883 October 2000 -35- 003-6016 Distance-Drawdown Data (SVE Effects) Vacuum responses were measured in the shallow and intermediate probes, and positive pressures measured in the deep probes. Distance-drawdown data for the intermediate probes in the AST Area during steady state are presented in Figure 16, with regression lines fit to the data. Steady state response was determined fi"om system pressure and flow rate data using the April 15, 2000 data point at 6:15 am. The distance-drawdown plot, in conjunction with the test observations, confirms that the ROI lies between 20-25 feet. In the FPP Area, the VMPs indicated vacuum responses only at the shallow probes, as positive pressures were recorded in the intermediate and deep probes. Furthermore, the responses at the shallow VMPs were very low, achieving a maximum of only 0.03 "H2O. These results confirm the weak influence of the SVE system in the FPP Area. Air Permeability The results of the air permeability calculations are shown in Table 7. The calculated air permeability in the AST area was approximately 10'^-10'^ cm^, consistent with the calculations based on the Phase I test data. Distance-Pressure Data (Sparging Effects) In the AST Area, positive pressures were recorded only at the deep VMPs, reflecting the sparge gas entering the vadose zone from the water table. Data points after 11:25 on April 15, 2000 were used to represent steady-state conditions, which are plotted in Figure 17. VMP-ID recorded the highest pressures, while VMP-3D consistently recorded the second highest pressures, and VMP-2D recorded mostly zero pressure. The same trend occurred in the AS/SVE Extended test, in which VMP-2D recorded lower, but detectable pressures, compared with VMP-3D. Based on these results, there appears to be a preferential air flow pathway in the area of AST-VMP-3D. In the FPP Area, positive pressures were recorded in the deep and intermediate probes. Pressure is distributed among the VMPs fairly uniformly, but the magnitudes are very low (<0.1 "H2O), and a ROI based on this parameter was not discemible. Dissolved Oxygen Figures 18 and 19 show the dissolved oxygen measurements in the AST and FPP Areas, respectively. In the AST Area, saturated or near-saturated conditions were attained at VMP-ID, - Golder Associates , 304884 October 2000 -36- 003-6016 2D, and MW-1 (28 feet from the sparge well), and significant increases were attained in MW-6 (11 feet from the sparge well). Bubbling was observed in VMP-ID, -2D, MW-1, and MW-6, indicating sparge air conduits had been intercepted. No significant increases were measured in VMP-3D or -4D, and no significant increases had been measured in the Phase II Step Test. The DO data reveals significant heterogeneity in the sediments, as VMP-3D (20' from the sparge well) showed no appreciable DO increase, yet bubbling was observed in a monitoring well 28' from the sparge well. In the FPP Area, inconsistent results were obtained. DO levels were initially high in VMP-3D and MW-2, potenfially due to migration of previously sparge-affected water. These DO levels remained high throughout the test. In MW-2 (16' from the sparge well) bubbling was observed during the test, indicating a conduit of sparge air was intercepted. DO increased significantly in VMP-4D, which is the most distant probe from the sparge well, while little or no increases were measured in VMP-ID and -2D, which are more proximate to the AS well. Summary The pressure responses in the VMPs confirmed results from the prior tests. The AST Area showed consistent, significant response to the SVE and AS systems, whereas the FPP Area responses were weak and unpredictable. The analytical ROI calculations for SVE are consistent with the estimates from the previous test. In the AST Area, DO results were similar to the AS Step test results in that points within 10 feet and at 28 feet from the AS well exhibited significant DO concentrations and bubbling, while points at 20 feet and 40 feet from the AS well showed no increases. This revealed the heterogeneous nature of the sediments at the site. DO results in the FPP Area were inconsistent, where increases were measured in the two distant probes, but not in the two closest probes. Overall, the response to air sparging in the FPP Area was weak. 3.8 Phase II SVE/AS Extended Test The Phase II SVE/AS Test provided information on combined air sparge and SVE performance, including areal coverage of the SVE system in the AST area with all six SVE wells operating. Also, the sparge influence via DO measurements and mass removal rates are assessed from this test. Field data from this test are presented in Tables 13 to 15. Golder Associates ^ ^ . ^ 304885 October 2000 -37- 003-6016 Areal Pressure Plots Contour plots of vacuum of the AST Area are presented in Figure 20. The vacuum drawn by each of the SVE wells can be seen as well as the vacuums invoked at each of the intermediate VMPs. The plot shows that at a point nearly equidistant from the SVE wells — VMP-3I - a substantial vacuum occurred (0.2 "H2O). VMP-41 (i.e., the farthest probe from SVE-1) was evidently influenced by both SVE-4 and SVE-1, demonstrated by a strong vacuum of 1.2 "H2O. This test confirms that the SVE well spacing in the existing pilot-scale system is expected to provide adequate vacuum coverage over the impacted zone at the AST Area. Responses of the probes to sparging were similar to the SVE/AS test, where VMP-ID exhibited the highest response followed by VMP-3 D and VMP-2D, reflective of the heterogeneous nature of the sediments at the Site. Vacuum responses in the FPP Area were very low and inconsistent at each probe. Only the shallow probes recorded vacuums, and the highest value recorded vacuum was only 0.05 "H2O. Pressure responses due to sparging were relatively high at the end of the test as VMP-2D, -3D, and -4D all recorded greater than 0.25 "H2O. At the end of the eariier SVE/AS test, VMP-2D had recorded greater than 0.25 "H2O, consistent with these results. These high responses are unexpected in light of the low sparge pressures required for flow. It is possible that air was following a preferential pathway or conduit. Dissolved Oxygen Figures 21 and 22 show the dissolved oxygen measurements in the AST and FPP areas, respectively. The data are more scattered than previous tests, most likely reflecting flow-through of pockets of previously sparge-affected water. However, the same basic results are evident, namely that VMP-ID and -2D became heavily saturated with oxygen while VMP-3D and -4D were generally unaffected. MW-1 (28 feet from AST-AS-1) and MW-6 (11 feet from AST-AS- 1) both started out relatively highly saturated and remained so throughout the test. Bubbling within wells was either not observed or not recorded. The DO data in the FPP Area is inconclusive as all VMPs and MW-2 (which is 15 feet from FPP-AS-1) started out nearly fully saturated and remained so throughout the test. MW-3 (which is 90 feet from FPP-AS-1) was distant enough to be unaffected by sparging. Initial DO levels at MW-3 were low and remained low (i.e., less than 1.0 mg/L) throughout the test. Golder Associates 304886 October 2000 -38- 003-6016 Mass Removal Performance The mass removal rates were calculated from several sampling ports using the on-site and off-site analytical data as described in Section 2. The laboratory data from Microseeps is presented in Table 16 and the Photovac Field GC data is presented in Table 17. These data were not validated, as quality control data were limited. Table 18 presents a comparison of samples taken from the same ports at approximately the same time between the laboratory (Microseeps) data and the field GC (Photovac) data. The relative percent difference between two sets of data, termed "Datal" and Data2", is calculated by the following: Relative percent difference = (Datal - Data2)/(Average of Datal and Data2) The maximum difference that can exist is 200%. As shown in Table 18, there are many cases in which the relative percent differences are greater than 100%. In 48 instances the lab data values were lower than the corresponding field data; in 38 instances, the field data were lower. Therefore, there is no definitive trend to these differences. Two sampling ports used for sampling data that could be used in calculating mass removal. The "Intake" port was located on the suction side of the blower, and the "Exhausf port was located on the discharge side of the blower. The following describes the four tables presenting the mass removal calculations according to the lab data and sampling location used: • Table 19 - Microseeps (laboratory) data and the Intake port; • Table 20 - Photovac (field GC) data and the Intake port; • Table 21 - Microseeps data and the Exhaust port; and, • Table 22 - Photovac data and the Exhaust port. The total cumularive mass removed results are shown in Figure 23. The esfimates for total mass removal of ethylbenzene and xylene combined using the Lab data and the Photovac data at the Intake port are 88 lbs and 7 lbs, respectively. At the Exhaust port, the calculated removals are 60 lbs and 113 lbs, respectively. Chloroform and toluene do not account for a significant amount of mass, consistent with minimal source concentrations observed in baseline (pre-test) sampling. The mass removal estimates based on the Photovac results for ethylbenzene at the intake port are clearly inconsistent with the other estimates. Golder Associates 304887 October 2000 -39- 003-6016 The calculated extraction rates over the course of the test were plotted for the four combinations of sampling port and analytical data, as shown in Figures 24 to 27. The Intake and Exhaust Microseeps data (i.e.. Figures 24 and 26) both show results typical of SVE/AS operations, where higher VOC mass removal rates were obtained early in the test. These rates decline and remain low in the second half of the test. Typically, a sustainable contaminant concenttation in the extracted gas is expected to be I to 10 percent of the initial concentrations (USAGE, 1995). The Photovac data however, as shown in Figure 20, suggests relatively high rates of removal throughout the test, and the final three samples exhibit three of the four highest removal rates. These ttends suggest that the Photovac data may be less reliable. The variability of the data precludes an exact determinafion of total mass removal.. The mass removal calculations also indicate that combined SVE/AS is more efficient at mass removal than SVE alone. The total mass extracted on a per-SVE well basis from the Phase II SVE/AS Extended test was more than double the 3.05 pounds removed in the Phase I Constant Rate test (i.e., SVE only) over the same duration (i.e., 72 hours). The mass removal rates (i.e., gas phase) during the steady-state portion of each test show that about 1-2 lb/day of VOCs were removed per SVE well during the Phase II Extended Test, and about 0.5 lb/day of VOCs were removed during the Phase I Test. Note, these mass removal rates do not include the reduction in mass that would result from enhanced biodegradation in soil and groundwater, due to SVE/AS activities. Groundwater Mounding Depths to groundwater measurements were continually made during the test. The results show that no significant mounding was observed in the vapor probes, GMP wells, or monitoring wells. Summary The results of the test in the AST Area show that the existing network of six SVE wells provided adequate vacuum coverage over the impacted area. Responses of the probes in the FPP Area were low and irregular, confirming a weak overall response to SVE. Pressure responses to sparging were in agreement with previous tests, with diffuse responses measured at all four probes. Dissolved oxygen results in the AST Area were essenfially the same as in previous tests: high DO in the two closest probes and in MW-1 and MW-6, and little response in the two distant probes. In the FPP Area, DO results indicated that the groundwater was oxygen saturated. Golder Associates 304888 October 2000 -40- 003-6016 however, increases were not observed, only that concentrations began high and remained high throughout the test, therefore these results are inconclusive. The mass removal calculations showed that significant mass was removed from the AST Area, probably about 70-80 lbs ethylbenzene and total xylenes. This rate is likely significantly higher than would be achieved by SVE alone. In the FPP Area, significant rates of chloroform removal were not achieved. However, unlike the AST Area, a significant mass of chloroform does not exist in the FPP Area soils or groundwater and thus, significant removal rates would not be expected regardless of SVE/AS efficacy. 3.9 Groundwater Analytical Results Sampling of the groundwater from monitoring wells and deep vapor monitoring probes occurred according to the schedule outlined in Table 2. Analytes included VOCs and natural attenuation parameters. The results are presented in Tables 23 and 24 for the AST and FPP areas, respectively. Table 25 lists the quality control sample results. In the AST Area, there was a marked decrease in concentrations of ethylbenzene and xylene in groundwater between the March 30, 2000 and May 3, 2000 groundwater sampling events, when air sparging was being conducted. These decreases were exhibited most dramatically in AST- VMP-2D. These reductions are likely due to a combination of stripping of VOCs and aerobic biodegi^adation due to the introduction of compressed air. In the FPP Area, no appreciable changes were seen in groundwater conditions for chloroform in the immediate area of the SVE/AS system throughout the course of pilot testing. The minor fluctuations in levels indicate that the groundwater was not significantly affected by the operation of the SVE/AS system. This is supported by the low mass removal rates of chloroform in the extracted soil vapor during combined SVE/AS tests. However, it is again noted that the residual source mass of chloroform in both soils and groundwater in the FPP Area was already very low prior to the commencement of pilot testing. Therefore, mass removal rates in the FPP Area are not considered as good an indicator of system performance as in the AST Area. Golder Associates 304889 October 2000 -41- 003-6016 4.0 CONCLUSIONS AND RECOMMENDATIONS 4.1 Conclusions 4.1.1 Comparison to Objectives and Applicability as Potential Remedial Technology The objectives of the Pilot Study included: • Verification that SVE and SVE/AS are viable potential remedial technologies for source conttol of VOCs in subsurface soil and groundwater; and, • Development of design, performance, and cost data for efficient operation of a full-scale system in one or both of the impacted areas. The Pilot Study demonstrated that SVE or SVE/AS in combination can effectively remove VOCs from the AST Area at this Site. The soil vapor chemistry data indicate that significant mass removals for ethylbenzene and xylene can be sustained over longer-term operation. A secondary evidence of successful demonstration is the decrease in concenttations of Site contaminants in groundwater between the March 30, 2000 and May 3, 2000 sampling events, when air sparging was being conducted. These decreases were exhibited most dramatically in AST-VMP-2D. These reductions are likely due to a combination of stripping of VOCs and aerobic biodegradation due to the introduction of compressed air. Sufficient radii of influence and air permeability were exhibited such that SVE (with or without AS enhancement for groundwater) could provide adequate coverage for the impacted vadose zone in the AST Area. SVE and SVE/AS results were less conclusive for VOC removal in the FPP Area. In the FPP Area, SVE/AS system responses during pilot testing were generally weaker. Field data indicated that the subsurface in the FPP Area is generally less permeable such that good air flow distribudon via SVE and AS is not expected. The total mass removal of chloroform over the three-day extended SVE/AS test in the FPP Area was esUmated at 11 grams, which is not insubstantial given the very low residual source concenttations of chloroform in the FPP Area soils and groundwater.. However, no appreciable changes were seen in groundwater conditions for chloroform in the immediate area of the SVE/AS system throughout the course of pilot testing. It is concluded that implementation of an SVE or SVE/AS system in the FPP Area is not warranted due to the very low mass of residual chloroform present in soils and groundwater (i.e. generally below MCLs). Also, chloroform primarily biodegrades anaerobically and natural attenuation parameters measured during the Pilot Study and the RI (Golder, 2000) indicate that natural attenuation processes are important in degrading chloroform in groundwater. Therefore, Golder Associates 304890 October 2000 -42- 003-6016 operation of AS in the FPP area may inhibit existing anaerobic natural attenuation processes, which are addressing residual low-level concenttations that are currently near or below MCLs. The step tests and constant rate tests for SVE and AS, and SVE/AS in combination, yielded important information for the potential future full-scale design. The information suggests that the existing system in the AST Area could readily transition into a full-scale SVE system with few modifications. However, based on the highly variable pressure and velocity measurements observed during the pilot study, further operafion of the existing-pilot scale system is warranted in order to verify system responses and SVE/AS well efficiencies. These parameters affect the operational pressures, sizing of the blower and air compressor, as well as the layout of the well network and any additional monitoring points. 4.1.2 Data Limitations and Uncertainties Much of the limitations and uncertainties associated with the field data presented and interpreted in this Report stem from issues associated with equipment and instrumentation. In addition, many of the field parameters have inherent limitations in terms of reliability as indicator parameters of radius of influence. For example, dissolved oxygen levels may experience competitive effects due to aerobic biodegradation processes. Such limitations have been discussed in Sections 2 and 3. This section summarizes the limitations and uncertaindes that are most critical to data interpretation to evaluate system performance and future design parameters. Several issues are inherent to site condidons and the limitadons associated with a pilot-scale system. For example, lithologic information from the boring logs in both the FPP and AST Areas reveal the presence of sandy lenses or layers of higher permeability than the surrounding soil. As expected, this heterogeneity affected the responses observed in the probe clusters, with probes screened in the sandy layers generally exhibiting sttonger responses. There is a high degree of uncertainty in the velocity and flow measurements due to inappropriate zeroing procedures at the start of pilot testing. Also, constant flutter in the gauge inhibited accurate readings. It is expected that velocity/flow measurements were under-reported in the earlier phases of tesdng. Soil vapor flows from the AST and FPP Area SVE wells were not measured directly; rather, they were apportioned in a 4:1 ratio based on relative velocity measurements in each area. During the SVE tests, an inverted relationship between applied vacuum and flows was observed at the SVE wells. During the SVE/AS tests, the flow remained Golder Associates 304891 October 2000 -43- 003-6016 fairly uniform despite increases in pressure. An inverted relationship may result from the expansion of the saturated zone above the water table that is induced by the vacuum at the SVE well. The saturated zone may expand enough to resttict air flow into the SVE well screen. Also, higher applied vacuums may cause silts or sands to accumulate on the well screen and resttict air flow into the SVE well. There were also large discrepancies between flows measured at the blower and the sum of individual flows measured at the acdve SVE wells. In light of these uncertaindes, the use of flow data was generally limited to calculadons of mass removal rates, whereas pressure data were more relied upon to evaluate system response, radii of influence, and air permeability. Thus, the uncertainties exhibited by the flow data did not preclude the detailed evaluadon of SVE/AS system performance in each Area. The uncertaindes in the airflow rates also affect the calculated mass removal rates, since mass removals are calculated using constituent concentradons and volumetric flow rates. Additional uncertainties are inherent in the mass removal rates based on the chemistry data. The on-site (PhotoVac) and off-site (Microseeps) analytical data for the constituents of concern were not comparable, as discussed in Section 3. A small difference would be expected since each of the corresponding on-site and off-site air samples was taken at a slightly different time, so these samples are not frue split samples. Also sample procedures different for each type of sample (i.e., Tedlar bag versus syringe/vial). Typically, air samples other than Summa canisters do not transport well in airplanes due to pressure changes in flight. It is possible that leaks occurred in the Microseeps samples, although the inconsistency of the reladve differences between the on-site and off-site sample concentradons suggests that other factors were involved. These factors are likely related to sampling procedures and/or differences in analytical instrumentation. Regardless, the use of either set of chemistry data clearly indicates that significant mass removal of VOCs could be achieved by SVE alone and SVE/AS in combination, notably in the AST Area. 4.2 Recommendations 4.2.1 Additional Testing / Monitoring Should SVE or SVE/AS be selected as the remedial technology for one or both source areas, additional invesdgadons would be conducted prior to the final operation of the full-scale system, including any modificadons to the existing SVE/AS system. Golder Associates 304892 October 2000 -44- 003-6016 Prior to running the system, a full leak-check of the system piping and connections should be performed. Pressure gauges at the wellheads and at the blower can be used to evaluate actual versus expected head losses in the piping. A pilot test on the order of several weeks would assist in the esdmation of sustainable mass removal rates over longer term operation. This, in part, would be used to evaluate the need for any off-gas emission controls. Additional soil vapor samples would be taken during this time. Summa canisters are recommended for any air samples that are sent off-site. In the same vein, a longer-term pilot study would allow the operation and monitoring of the system at steady state rather than transient condidons. Since the water table was at a relatively high level during the Spring 2000 Pilot Study, continuous operation at low water levels would yield important informadon as to the design operating limits of a final system. For any future tests involving air sparging, longer recovery times are recommended to avoid interference by residual dissolved oxygen levels in groundwater from previous tests. Other tests that could be performed in order to design and optimize a full-scale system include cycling the air sparge wells only or cycling the entire SVE/AS system. This would enable a decision as to whether to add conttols (e.g. timers) to the air compressor and/or blower to cycle the system automatically during long-term operation, and determine optimal frequency of cycling. The most beneficial source of additional information on long-term SVE/AS system performance would be gained simply by resumed operation of the system on a continuous basis. Since the SVE/AS system was not decommissioned after the pilot study, the entire system or portions thereof (i.e., SVE only or certain wells only) can be placed on-line at any time, provided that that the appropriate federal and territorial approvals are obtained. 4.2.2 Long Term Operation The extended SVE/AS test in the AST Area indicated that the existing network of SVE wells provides substantial coverage of the vadose zone. Should air sparging be included as a component of the selected final remedy, addidonal sparge wells may be considered for installation. The air sparge wells should be installed within the zone of capture of the SVE well network, but the air sparge wells themselves need not provide overlapping coverage of the impacted groundwater area in the same manner as the SVE wells. Sparge wells can be placed such that groundwater will eventually migrate into the capture zone of an AS well. Golder Associates 304893 October 2000 -45- 003-6016 The long-term operadon of an SVE or SVE/AS system at this Site necessitates careful consideration of operations and maintenance requirements. The system should be designed to operate for periods of regular unattended operation. Alarms with telecommunications would be considered, if needed, to alert a designated local operator of system failure (e.g., motor failure, power outages). Automation and conttol systems would be considered in a final design for long- term operation. Long-term operation would require an operator to visit the site periodically for monitoring purposes. Vacuum/pressure measurements and flow rates would be monitored at each SVE/AS well and at monitoring probes and system balancing may be needed occasionally to ensure coverage of the impacted area. Also, a monitoring program would include vapor concenttations taken at the wellheads, blower, and after any conttol device with a portable meter, as well as periodic gas-samples for laboratory analysis. These data would be used to evaluate system performance in terms of VOC mass removal and compliance with air permit requirements. Golder Associates 304894 October 2000 -46- 003-6016 5.0 REFERENCES Enhanced Landfill Gas Extracdon Pilot Test Work Plan, Keystone Sanitadon Landfill, Union Township, Adams County, Pennsylvania. Golder Associates, August 1998. Focused Feasibility Study, Altemate Remedy for Operable Unit 1, Keystone Sanitation Landfill, Union Township, Adams County, Pennsylvania. Golder Associates, May 2000. Golder 2000. Draft Feasibility Study Report, Virgin Island Chemical Site, U.S. Virgin Islands, July 2000. Marley, M.C. and Bruell, C.J., In Situ Air Sparging: Evaluation of Pettoleum Industry Sites and Consideration for Applicability, Design and Operadon. API Publican #4609, April 1995. McLaren/Hart 1999. Drat Final Treatability Study Work Plan, Virgin Island Chemical Site, May 1999. McLaren/Hart, 2000. Final Remedial Invesdgation Report, Virgin Island Chemical Site, St. Croix, U.S. Virgin Islands, February 2000. NIOSH, 1990. NIOSH Pocket Guide to Chemical Hazards, U.S. Dept. of Health and Human Services, June 1990. Nyer, Evan U. and Suthersan, Suthan S., 1993, "Air Sparging: Savior of Ground Water Remediations or Just Blowing Bubbles in the Bath Tub?" Ground Water Monitoring and Remediation, Fall 1993, p. 87-91. Pederson and Curtis, 1991 USAGE, 1995. Engineering and Design: Soil Vapor Exttacdon and Biovendng. USAGE EM 1110- 1-4001, November 1995. USEPA, 1989. Guide for Conducting Treatability Shjdies Under CERCLA, Mterim Final, EPA/540/2-89/058, December 1989. USEPA, 1993. Presumptive Remedy: Site Characterization and Technology Selection for CERCLA Sites With Voladle Organic Compounds in Soils," USEPA Directive No., 9355.0-48FS, September 1993. USEPA, 1997. Presumptive Remedy: Supplemental Bulletin Multi Phase Exttacdon Technology for VOCs in Soil and Groundwater, USEPA Directive No. 9355.0-68FS, April 1997. G:\Projects\003-6016\Golder\SVE TS Report\revtext.doc Golder Associates ^ ^ . ^ ^ 304895 September lOQQ O 00 VD cn Table 1 Specifications for Pilot Study Wells and Monitoring Points Virgin Island Chemical Site St. Croix, U.S. Virgin Islands 003-6016 bgs: below ground surface NA: not applicable Sch: Schedule PVC; pol>'vinyl chloride SS: stainless-steel Well ID Completion Date Total Depth (feet bgs) Construction Material Screen Interval (feet bgs) Screen Slot Size (inches) Diameter (inches) Design Reference AST Area SVE-1 SVE-2 SVE-3 SVE-4 SVE-5 SVE-6 GMP-1 AS-l VMP-11 VMP-ID VMP-2S VMP-2I VMP-2D VMP-3S VMP-3I VMP-3D VMP-4S VMP-4I VMP-4D 08-Feb-OO 11-Feb-OO 09-Feb-OO 10-Feb-OO 10-Feb-OO 10-Feb-OO 24-Feb-OO 22-Feb-OO 17-Feb-OO 14-Feb-OO 17-Feb-OO 17-Feb-OO 16-Feb-OO 18-Feb-OO 18-Feb-OO 23-Feb-OO 18-Feb-OO 18-Feb-OO 23-Feb-OO 24.5 24.5 24.5 24.5 24.5 24.5 30 50 15 30 5 15 30 5 15 30 5 15 30 304 Sch 5 SS 304 Sch 5 SS 304 Sch 5 SS 304 Sch 5 SS 304 Sch 5 SS 304 Sch 5 SS Sch 40 PVC Sch 80 PVC Sch 40 PVC Sch 40 PVC Sch 40 PVC Sch 40 PVC Sch 40 PVC Sch 40 PVC Sch 40 PVC Sch 40 PVC Sch 40 PVC Sch 40 PVC Sch 40 PVC 4.5- 19.5 4.5-19.5 4.5- 19.5 4.5- 19.5 4.5- 19.5 4.5- 19.5 28.85-29,85 47.5 - 49.5 12.55-14.25 27.55-29.25 2.55-4.25 12.55- 14.25 27.55-29.25 2.55-4.25 12.55-14.25 27.55-29.25 2.55-4.25 12.55- 14.25 27.55-29.25 0.020 0.020 0.020 0.020 0.020 0.020 0.020 0.040 0.020 0.020 0.020 0.020 0.020 0.020 0.020 0.020 0.020 0.020 0.020 2 2 2 2 2 2 1 1 2 2 2 2 2 2 2 2 2 2 2 Figure 3 Figure 3 Figure 3 Figure 3 Figure 3 Figure 3 NA Figure 4 Figure 5 Figure 5 Figure 5 Figure 5 Figure 5 Figure 5 Figure 5 Figure 5 Figure 5 Figure 5 Figure 5 FPP Area SVE-1 GMP-1 AS-l VMP-11 VMP-ID VMP-2S VMP-2I VMP-2D VMP-3S VMP-3I VMP-3D VMP-4S VMP-4I VMP-4D 01-Feb-OO 24-Feb-OO 21-Feb-OO 21-Feb-OO 07-Feb-OO 21-Feb-OO 21-Feb-OO 04-Feb-00 21-Feb-OO 21-Feb-OO 03-Feb-OO 22-Feb-OO 22-Feb-OO 03-Feb-OO 26.5 30 48 15 29.75 5 15 30 5 15 30 5 15 30 304 Sch 5 SS Sch 40 PVC Sch 80 PVC Sch 40 PVC Sch 40 PVC Sch 40 PVC Sch 40 PVC Sch 40 PVC Sch 40 PVC Sch 40 PVC Sch 40 PVC Sch 40 PVC Sch 40 PVC Sch 40 PVC 6.5-21.5 28.85-29.85 45.5-47.5 12.55- 14.25 27.30-29.00 2.55-4.25 12.55- 14.25 27.55-29.25 2.55-4.25 12.55- 14.25 27.55-29.25 2.55-4.25 12.55- 14.25 27.55-29.25 0.020 0.020 0.040 0.020 0.020 0.020 0.020 0.020 0.020 0.020 0.020 0.020 0.020 0.020 2 1 1 2 2 2 2 2 2 2 2 2 2 2 Figure 3 NA Figure 4 Figure 5 Figure 5 Figure 5 Figure 5 Figure 5 Figure 5 Figure 5 Figure 5 Figure 5 Figure 5 Figure 5 G:\0036016\SVE TS Report\tablel&2,xls\Table 1 Golder Associates September 2000 Table 2 System Testing FieUi Sampling Summan Virgin Island Chemical Site St. Croix, U.S. Virgin Islands 003-6016 Phase I (S]'T Testing) Area ut" Concern Chrunology Number of Sample.s Matrix Analysis Laboratory FPP Area 1 SVE Well and 11 V^[Ps Soil-Gas Site Target Compounds Vacuum Pressure MicroSeeps Field Gauge Readings Baseline N'lonitoring (Pre-Pha.se 1} .Ml On-Site Monitoring/Production Wells 1 G\'IP and 11 VMPs Groundwater Depth to Water Field Instmment 3 Monitoring Wells (MW-2, MW-3, MW-7) 4 Dcei? VMPs Gi'ound water Site Target Cornpounds/C02/Field Parameters Pace/Field Test Kits/Field Instruments 1 SVE Well and 11 VMPs (on a regular basis) Soil-Gas Vacuum Pressure/Flow Rate (SVE well only) Field Gauge Readings Step Rale Test 1 SVE Well, VMPs, System Intake, Exluust Manifold, Downwind of System (on a regular basis) Soil-Gas Organic Vapors Site Target Compounds Field Instrument MicroSeeps SVE System - Trailer (on a regular basis) Various Vacuum Pressure (intake/exliaust)/Flow Rale/Exhaust Temperature/Weather Conditions Field Gauge Readings/Weather Station 1 GK-IP (on a regulai" basis) Groundwater Depth to Water Field Instrument 1 SVE Well and 11 VMPs (on a regular basis) Soil-Gas Vacuum Pressure/Flow Rate (SVE well only) Field Gauge Readings Constant Rate Test 1 SVE N\''ell, A''K'IPs, System Intake, Exliaust Manifold, Downwind of System (on a regular basis) SVE System - Trailer (on a regular basis) 1 GKIP (on a regular basis) 1 SVE Well and 11 VMPs Post-Phase I Monitoring All On-Site Monitoring/Production Wells 1 GMP and 11 VMPs 3 Monitoring Wells (MW-2, MW-3, MW-7) 4 Deep VMPs (if water is present) Soil-Gas Organic Vapors Site Target Compounds Field Instrument MicroSeeps Various Vacuum Pressure (intake/exliaust)/Fiow Rate/Exhaust Temperature/Weather Conditions Field Gauge Readings/Weather Station Groujidwater Depth to Water Field Instiiiment Soil-Gas Site Target Compounds Vacuum Pressure MicroSeeps Field Gauge Readings Groundwater Depth to Wate Field Instrument Groundwater Site Target Compounds/C02/Field Parameters Pace/Field Test Kit/Field Instioiments o 00 VD - J Cr:\00?60lD\SVE TS Rejx>n\iablelS:2.xl,s\TabIe 2 Golder Associates .Septembfi- 2000 Table 2 .System Teiiting Field Sampling Summai-)' Virgin Island Chemical Site St. Ci()i-\, U.S. Virgin Islands 003-6016 ASTArea Baseline .Vlonitoring (pre-Pliase I) Step Rale Test Constant Rate Test Post-Phase I Monitoiing 1 .SVE Weil and 11 VMPs All On-Site Monitoring/Production Wells 1 GVCP and 11 VVIPs 4 Monitoring Wells (MW-1, MW-6, MW-8, MW-10) 4 Deep VMPs 1 SVE Well and 11 VMPs (on a regular basis) 1 SVE Well, VK'IPs, System Intake, E.^liaust Manifold, Downwind of System (on a regular basis) SVE System - Trailer (on a regular basis) 1 GK'IP (on a regular basis) 1 SVE Well and 11 VMPs (on a regular basis) 1 SVE Well, VMPs, System Intake, Exliaust Manifold, Downwind of System (on a regular basis) SVE System - Trailer (on a regular basis) 1 GK'IP (on a regular basis) 1 SVE Well and 11 VMPs .\ll On-Site Monitoring/Production Wells I GN'IP and 11 VK'IPs 4 Monitoring Wells (MW-1, MW-6, MW-8, MW-10) 4 Dee|) VMPs Soil-Gas Groundwater Groundwater Soil-Gas Soil-Gas Various Groundwatei' Soil-Gas Soil-Gas Various Groundwater Soil-Gas Groundwater Crtoundwater TE.X /Site Target Compounds (confirmation) Vacuum Pressure Depth to Water Site Target Compounds/COj/Field Parameters Vacuum Pressure/Plow Rate (SVE well only) Organic Vapors TE.X/Site Target Compounds Vacuum Pressure (intake/exliaust)A-"low Rate/Exliaust Temperature/Weather Conditions Depth to Water Vacuum Pressure/Flow Rate (SVE well only) Organic Vapors TEX/Site Target Compounds Vacuum Pressure (intake/exhaust)/Flow Rate/Exliaust Temperature/Weather Conditions Depth to Water TE.X /Site Target Compounds (confmnation) Vacuum Pressure Depth to Water Site Target Compounds/COj/Field Parameters PhotoVac/MicroSeeps Field Gauce Readines Field Instrument Pace/Field Test Kits/Field Instruments Field Gauge Readings Field Instmmcnt PhotoVac/K'licroSeeps Field Gauge Readings/Weather Station Field Instrument Field Gauge Readings Field Insti-ument PliotoVac/K-IicroSeeps Field Gauge Readings/Weather Station Field Listrument Photo Vac/K'IicroSeeps Field Gauge Readings Field Instmment Pace/Field Test Kit.s/Field Instruments to o 00 CD G:\00M016\SVE TS Rcp,jn\tabkI&2.>d5\Table 2 Golder Associates September 2000 Table 2 System Testing Field Sampling Summai7 Virgin Island Clieniical Site St. Cioix, U.S. Virgin Islands 003-6016 Phase II (SV'E/AS Testing) Area of Concern Chronology Number of Samples Matrix Analysis LuboraluPi' FPP Area Baseline Monitoring (Pre-Phase Tl) Transition from Phase I to Phase II wir/.v continuous; therefore, post-Phase I monitoring represented baseline monitoring for pre-Phase II testing. 1 SVE Well and 11 VMPs (on a regular basis) 1 AS Well (on a regular basis) Step Rate Test AS System - Trailer (on a regular basis) 1 SVE Well and 11 VMPs (on a regular basis) 1 GN'IP and Nearby Monitoring Wells (on a regular basis) 1 SVE Well (on a regular basis) 1 AS Well (on a regular basis) 11 VN'IPs (on a regular basis) Constant Rate Test 1 SVE Well, VN'IPs, System bUake, Exliaust Manifold, Downwind of System (on a regular basis) SVE/AS System - Trailer (on a regular basis) Select VMPs and/or Nearby Monitoring Wells 1 GK'IP and Nearby Monitoring Wells (on a regular basis) 1 SVE Well and 11 VMPs Post-Phase H Monitoring .All On-Site Monitoring/Production Wells 1 GMP and 1 1 VMPs 3 Monitoring Wells (MW-2, MW-3, MW-7) 4 Deep VN'U^s (if water is present) Soil-Gas Soil-Gas Various Soil-Gas Groundwater Soil-Gas Soil-Gas Soil-Gas Groundwater Soil-Gas Various Groundwater Groundwater Soil-Gas Groundwater Groundwater Air Pressure/Depth to Water/DO Air Pressure/Flow Rate .Air Pressure (compressor)/Weather Conditions Organic Vapors Depth to WaterDO Vacuum Pressure/Flow Rate .Air Pressure/Flow Rate Pressure (vacuum or air) Depth to Water/DO Organic Vapors Site Target Compounds Vacuum Pressure (intake/exliaust)/Air Pressure (comi)ressor)/Flow Rates/Exhaust Temperature/Weather Conditions Site Target Compounds/C02/Ficld Parameters Depth to Water/DO Site Target Compounds Vacuum Pressure Depth to Water Site Target Compounds/C02/Field Parameters Field Gauge Readings/Field Instmments Field Gauge Readings Field Gauge Readings/Weather Station Field Instrument Field Instruments Field Gauge Readings Field Gauge Readings Field Gauge Readings Field Instiiiments Field Instrument MicroSeeps Field Gauge Readings/Weather Station Pace/Field Test Kit/Field Instruments Field Instruments MicroSeeps Field Gauge Readings Field Instnament Pace/Field Test Kit/Field Instruments O 00 G:\003601d\SVE TS Rtfpoil\tablei&2,xls\Table 2 Golder Associates September 2000 Table 2 System Testing Field Sampling Summary Virgin Island Chemical Site St. CioL\, U.S. Virgin Islands 003-6016 AST Area Baselme Monitoring (ore-Phase R) Step Rate Test Constant Rate Test Post-Phase 11 Monitoring Transition from Phase I to Phase 11 was continuous; therefore. post-Phase I monitoring represented baseline monitoring for 1 SVE Well and 11 VMPs (on a regular basis) 1 AS Well (on a regular basis) AS System - Trailer (on a regular basis) 1 SVE Well and 11 VN/Q^s (on a regular basis) 1 GK'IP and Nearby Monitoring Wells (on a regular basis) 1 SVE Well (on a regular basis) 1 AS Well (on a regular basis) 11 VMPs (on a regular basis) 1 SVE Well, VMPs, System Intake, Exliaust Manifold, Downwind of System (on a regular basis) SVE/AS System - Trailer (on a regular basis) Select VK'IPs and/or Nearby Monitoring Wells 1 GMP and Nearby Monitoring Wells (on a regular basis) 1 SVE Well and 11 VK'IPs ,A11 On-Site K'lonitoring/Production Wells 1 GMP and 11 VK'IPs 4 Monitoring Wells (MW-1, iVIW-6, MW-8, K'IW-10) 4 Deep VMPs Soil-Gas Soil-Gas Various Soil-Gas Groundwater Soil-Gas Soil-Gas Soil-Gas Groundwater Soil-Gas Various Gioundwaler Groundwater Soil-Gas Groundwater Groundwater Air Pressure/Depth to Water/DO Air Pressure/Flow- Rate .Air Pressure (compressor)/Weather Conditions Organic Vapors Depth to Water/DO Vacuum Piessure/Flow Rate .Air Pressure/Flow Rate Pressure (vacuum or air) Depth to Water/DO Organic Vapors TEX/Site Target Compounds Vacuum Pressure (intake/exliaust)/.Air Pressure (compressor),/l^lowRates/Exliaust Temperature/Weather Conditions Site Target Compounds/C02/FieId Parameters Depth to Water/DO TEX /Site Target Compounds (conllrmation) Vacuum Pressure Depth to Water Site Target Compounds/CO^/Field Parameters pre-Phase II testing. Field Gauge Readings/Field Instilments Field Gauge Readings Field Gauge Readings/Weather Station Field Listiument Field Instruments Field Gauge Readings Field Gauge Readings Field Gauge Readings Field Instruments Field Instmment • PhotoVac/N'licroSeeps Field Gauge Readings/Weather Station Pace/Field Test Kit/Field Instruments Field Instruments PhotoVac/KiicroSeeps Field Gauge Readings Field Insti-ument Pace/Field Test Kits/Field Instruments u> o u> o o G:\00J60I6\SVETS R=poi1\tableUt2.xls\Table 2 Golder Associates September 2000 Table 2 System Testing Field Sampling Summary Virgin Island Chemical Site St. Crulx, U.S. Virgin Islands 003-6016 Extended Phase II (SIT/AS Testing) .Area of Concern Chronology Number of Samples Matrix Analysis Laboraton' FPP Area Baselme Monitoring (Pre-Extended Phase E) Transition from Phase II to E.xtended Phase II was continuous; therefore, post-Phase II monitoring represented baseline monitoring for pre-Extended Phase II testing 1 SVE Well (on a regular basis) 1 .AS Well (on a regular basis) 11 VMPs (on a regular basis) Constant Rate Test 1 SVE Well, VMPs, System bitake, Exliaust Manifold, Downwind of System (on a regular basis) SVE/.AS System - Trailer (on a regular basis) Select VK'IPs and/or Nearby Monitoring Wells 1 GK'IP and Nearby Monitoring Wells (on a regular basis) 1 SVE Well and 11 VMPs Post-E.\tended Phase n Monitoring .All On-Site K'lonitoring/Production Wells 1 GMP and 11 VMPs 3 K'lonitoring Wells (MW-2, MW-3, MW-7) 4 Deep VK'IPs (if water is present) Soil-Gas Soil-Gas Soil-Gas Groundwater Soil-Gas Vaiious Groundwater Groundwatei' Soil-Gas Groundwater Groundwater Vacuum Pressure/Flow Rale Air Pressure/Flow Rate Pressure (vacuum or air) Depth to Water/DO Organic Vapors Site Target Compounds Vacuum Pressure (intake/exhaust)/Air Pressure (compressor)/Flow Rates/Exliaust Temperature/Weather Conditions Site Target Compounds/C02/Field Parameters Depth to Water/DO Site Target Compounds Vacuum Pressure Depth to Water Site Target Compounds/COi/Field Parameters Field Gauge Readings Field Gauge Readings Field Gauge Readings Field InstiTJments Field Instrument MicroSeei)s Field Gauge Readings/Weather Station Pace/Field Test Kit/Field Instruments Field Instmments K'licroSeeps Field Gauge Readings Field Instmment Pace/Field Test Kit/Field Instmments o O Cr:\0036016\SVE TS R.eporr\tablel&2.xls\Table 2 Golder Associates September 2000 Table 2 System Testing Field Sampling Summaiy Virgin Island Chemical Site St. Croix, U.S. Virgin Islands 003-601'6 ASTArea Baseline K'lonitoring (pre-Extended Pliase Q) Constant Rate Test Post-Phase 11 K'lonitoring Transition from Phase II to Extended Phase II was continuous; therefore, posi-Pha 6 SVE Wells (on a regular basis) 1 AS Well (on a regular basis) 11 VMPs (on a regular basis) 6 SVE Wells, VMPs, System Intake, Exhaust Manifold, Downwind of System (on a regular basis) SVE/.AS System - Trailer (on a regular basis) Select A'MPs and/or Nearby Monitoring Weili- 1 GK'IP and Nearby K^onitoring Wells (on a regular basis) 1 SVE Well and 11 VMPs All On-Sile K4onitoring/Production Wells 1 GVD^ and 11 VMPs 4 Klonitoring Wells (MW-1, MW-6, K'[W-8, MW-10) 4 Deep VMPs Soil-Gas Soil-Gas Soil-Gas Groundwater Soil-Gas Various Groundwater Groundwater Soil-Gas Groundwater Groundwatei' •>e II monitoring represented baseline monitoring for Vacuum Pressure/Flow Rate Air Pressure/Flow Rate Pressure (vacuum or air) Depth to Water/DO Organic Vapors TEX/Site Target Compounds Vacuum Pressure (intake/exliaust)/Air Pressure (compressor)/Flow Rates/Exliaust Temperature/Weather Conditions Site Target Compounds/C02/Fie]d Parameters Depth to Water/DO TEX /Site Target Compounds (confirmation) Vacuum Pressure Depth to Water Site Target Compounds/COj/Field Parameters pre-Extended Phase II testing. Field Gauge Readings Field Gauge Readings Field Gauge Readings Field Instmments Field Instmment PhotoVac/MicroSeeps Field Gauge Readings/Weather Station Pace/Field Test Kit/Field Instmments Field Instmments PhotoVac/K'IicroSeei)s Field Gauge Readings Field Instmment Pace/Field Test Kits/Field Instmments w o o to C;\00-^60l(i\SVETS Repon\tablel&2,xls\Tal)le 2 Golder Associates September 2000 Table 2 003-6016 System Testing Field Sampling Summary Virgin Lslanri CJiemital .Site St. CroL\, U.S. Virgin Islands Notes: Site Target Compounds: acetone, methylene chloride, chlorofojm, toluene, ethylbenzene, andtotal .xylenes Field Parameters: temperature, pH, conductivity, dissolved oxygen (DO), o.Kidation'reduclion potential, and turbidity TE.X: toluene, ethylbenzene, and total .xylenes SVE: soil vapor extraction AS: air sparging .^ST: aboveground storage tank FPP: fonucr process pit VfvIP: vapor monitoring point COT: carbon dioxide Automatic water level monitoring devices (Telogs or ec|ui\'alcnt) were placed in monitoring \vells MW-6 and .NfW-S at the beginning of Phase I testing. w o o 00 G:\0036016\SVE T.SRe|)ort\iabkli2.-ds\Table 2 Golder Associates Page 7 of? September 2000 Table 3 Comparison of Calculated and Measured SVE Flow Rates Virgin Island Chemical Site St. Croiz, U.S. Virgin Islands 003-6016 Test Phase I Step Area AST FPP AST FPP (1) average average max max Phase I Constant AST FPP AST FPP average average max max Phase II AST FPP AST FPP average average max max Phase II Extended AST FPP AST FPP average of 6 wells average avg of max of 6 wells max Measured Velocity fpm 730 170 1100 180 Calculated Flow Rate cfin 15.9 3.7 24.0 3.9 Calculated Total Flow Rate cfin 19.6 27.9 Measured System Flow Rate scfm 135-150 135-150 1 2000 533 2000 900 43.6 11.6 43.6 19.6 55.3 63.3 90-95 90-95 1 6000 977 6000 4000 130.9 21.3 130.9 87.3 152.2 218.2 126-135 126-135 1 268 1064 533 6000 35.1 23.2 69.8 130.9 58.3 200.7 95-168 95-168 Notes: (I) column denotes average of all data in test, or maximum reading. fpm = feet per minute; cfm = cubic feet per minute; scfm = standard cfin u> o o G:SVE TS Report:table3.xls Golder Associates September 2000 Table 4 Phase I step Test Results Virgin Island Chemical Site St. Croix, U.S. Virgin Islands Date: Tmie: Staee: 21-Mar-OO 1248 Step 1 21-Mar-OO 1442 StepI 21-Mar-OO 1500 Step 1 21-Mar-OO 1537 Step 1 21-Mar-OO 1550 Step 1 21-.Mar-00 1619 Step 2 21-Mar-OO 1645 Step 2 21-Mar-OO 1706 Step 2 21-Mar-OO 1725 Step 2 21-Mar-OO 1745 Step 2 21-Mar-OO 1810 Step 2 21-Mar-OO 1832 Step 3 21-Mar-OO 1857 Step 3 21.Mar-00 1916 Step 3 21-Mar-OO 1933 Step 3 21-Mar-OO 2022 Step 3 21-Mar-OO 2100 Step 3 21-.Mar-00 2145 Step 3 AST Ana (inches H20) AST-SVE-1 .JiST.V.MP-lI AST-VMP-ID AST-VMP-2S AST-VMP.21 AST-V.MP-2D AST-VMP-aS AST-VMP.31 AST-VMP-3D AST-VMP.4S AST-VMP-4I AST-VMP.4D AST-SVE-2 AST.SVE-3 AST-SVE-4 AST-GMP-1 (feet) 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 14.47 20 0.2 0 0 0 0 0 0 0 0,005 0 0 0,02 0 0 14,48 20 0,2 0 0 0 0 0 0,005 0 0,01 0 0 0.01 0 0 14,48 20 0,2 0 0 0 0 0 0 0 0,01 0 0 0,01 0 0 1451 20 0,02 0 0 0 0 0 0 0 0,01 0,005 0 0,01 0 0 14,5 40 0,35 0 0 0 0 0 0,01 0 0,01 0 0 0,02 0 0 14,44 40 0,4 0 0 0 0 0 0,01 0 0,01 0 0 0,02 0 0 14,46 40 0,4 0 0 0 0 0 0,01 0 0 0 0 0,01 0 0 14,4 40 0,4 0 0 0 0 0 0.15 0 0.01 0 0 0,025 0 0 14,43 • 40 0,4 0 0 0 0 0 0,01 0 0,01 0 0 0,025 0 0 1442 40 0,4 0 0 0 0 0 0,01 0 0,005 0 0 0,02 0 0 14,4 67 0.55 0 0 0 0 0 0,015 0 0,005 0 0 0,03 0 0 14,34 66 0,55 0 0 0 0 0 0,015 0 0,005 0 0 0,0325 0 0 14,37 66 0,5 0 0 0 0 0 0,015 0 0,005 0 0 0,0275 0 0 1437 65 0,5 0 0 0 0 0 0.0125 0 0,005 0 0 0,03 0 0 14,31 64 0,5 0,0275 0 0,055 0 0 0,015 0 0,005 0 0 0,0325 0 0 14,28 64 0.5 0,03 0 0,05 0 0 0,15 0 0,005 0 0 0,03 0 0 14,27 64 0,5 0,01 0 0,05 0 0 0,015 0 0,005 0 0 0,03 0 0 14,27 FPP Area finches H20) FPP-SVE-1 FPP-VMP-II FPP.VMP-ID FPP-V,VIP-2S FPP-V,V1P-2I FPP-VMP-2D FPP-VMP.3S FPP-VMP.31 FPP-VMP-3D FPP-VMP-4S FPP-VMP-4I FPP-VMP-4D FPP-GMP-l (feet) 0 0 0 0 0 0 0 0 0 0 0 0 15,16 20 0 0 0 0 0 0 0 0 0 0 0 15,14 20 0,005 0 0 0 0 0 0 0 0 0 0 15,13 20 0,005 0 0,005 0 0 0 0 0 0 0 0 15,13 20 0,005 0 0 0 0 0 0 0 0 0 0 15,13 40 0,02 0 0 0 0,01 0 0,005 0 0 0 0 15,14 40 0,15 0 0 0 0,05 0 0 0 0 0 0 15,13 40 0,15 0 0 0 0,23 0 0 0 0 0 0 15,17 40 0,15 0 0 0 0,05 0 0,005 0 0 0 0 15,17 40 0,15 0 0 0 0,02 0 0,02 0 0 0 0 15,14 40 0,01 0 0 0 0,005 0 0 0 0 0 0 15,17 68 0,0275 0 0 0 0,0075 0 0.005 0 0 0 0 15,17 66 0,0275 0 0 0 0,0125 0 0,01 0 0 0 0 15,17 66 0,0275 0 0 0 0.01 0 0,0075 0 0 0 0 15,16 66 0,0275 0 0 0 0,0025 0 0.005 0 0 0 0 15.15 66 0.0275 0 0 0 0.0125 0 0,0075 0 0 0 0 15,17 64 0,0275 0 0 0 0.005 0 0,0025 0 0 0 0 15,15 64 0,0275 0 0 0 0 0 0,0025 0 0 0 0 15,17 SVS Svs:ern AiTibientTemp, (deerees F) Wind Speed (mpll) Wind Direction Hrmiiditv (%) Bar. Pressure (inches) .Air Flow (SCFM) Velocity (3) AST-SVE-l (film) Velocity 0 FPP-SVE-1 (fpm) System Vacuum ] (" Hs) System Vactiimi 2 {" He) Exhaust Temp, (degiees F) OVM Downerad. (ppm) 80 2 N 52 29.93 0 0 0 SO 0 -- S9 1 NW 56 29,89 152 360 160 1,5 2,1 130 91 6 SE 57 29.89 152 1.5 2,1 130 86 7 SE 55 29,89 135 3 3,5 145 86 3 N 58 29.89 136 1100 180 3 3,5 150 2,4 87 2 NW-W 59 29,9 136 3 3,5 150 78 3 N-NE 58 29,9 136 .. 3 3,5 145 - 1 77 2 N-NW 61 29,9 95 4.9 5,2 185 .- 71 0 67 29,91 100 4.9 5,2 182 74 1 W 71 29,93 too 4.8 5.1 178 - o 1 ^ vo o (Jl G:W036O16\SVETS Repon\ lables.xls (Tabie4] Golder Associates September 2000 Table 5 Phase I Constant Rate Test Results Virgin Island Chemical Site St. Croix, U.S. Virgin Islands 003-6016 Date: Time: 0730 1 0830 0930 1030 1130 1230 1330 23-Mar-OO 1430 1 1530 1630 1730 1830 1930 2030 2130 2230 0130 0430 0630 24-Mar-OO 0830 1 1030 1 1230 1430 1630 1830 0730 0930 25 1130 1 Mar-00 1330 1 1530 1730 1840 26- Mar- 00 0730 ASTArea - Vacuum (inches H20) AST-SVE-1 AST-SVE-2 AST-SVE-3 AST-SVE-4 AST-VMP-11 AST-VMP-ID AST-V1V1P-2S AST-VMP-21 AST-VMP-2D AST-VMP-3S AST-VMP-31 AST-VMP-3D AST-VMP-4S AST-VMP-41 AST-VMP-4D AST-GMP-1 (feet) 67 0.045 <0 <0 0.8 0 <0 0,125 <0 0 0,03 0.035 PL 0.0025 <0 14.5 64 0.045 <0 <0 0.8 0.013 0 0.135 <0 0.03 0.028 0.033 0.005 0.005 <0 14.56 68 0.055 PL 0 0.925 0.013 0 0.16 0 0.02 0.033 0.035 0.005 0 0 14.57 64 0.05 <0 <0 0.8 PH <0 0.15 0.015 0.02 0,03 0.035 0.01 0.01 0.01 14.62 60 0.035 PL PL 0.8 0.1 0 0.195 0 0.01 0.03 0.035 0.01 0.005 0.005 14.67 62 0.038 PL PL 0.45 1.35 <0 0.23 0.02 0 0,02 0.03 <0 L 0 PL 14.71 58 0.033 <0 <0 0.45 0 0 0.125 <0 0 0.025 0.04 0 <0 <0 14.72 60 0.045 <0 <0 0.5 <0 0 0.135 0 0 0.025 0.035 0.005 <0 0.005 14.79 59 0.04 <0 <0 0.5 PL <0 0.135 PL 0 0.02 0.03 0.005 0 <0 14.68 59 0.03 <0 PL 0.45 PL 0 0.13 PL 0 0.02 0.03 0 0 0.003 14.56 54 0.04 PL <0 0.55 <0 0 0.125 <0 0 0.02 0.03 0,003 0 0.008 14.56 50 0.45 PL <0 0.8 1.255 0 0.24 <0 0.03 0,015 0.025 PL <0 <0 14.52 45 0.05 PL PL 0.83 0.1 <0 0.235 PL 0.015 0,01 0.028 PL <0 PL 14.45 42 0.05 PL PL 0.85 0 0 0.245 PL 0.02, 0.015 0.025 0.01 0.01 PL 14.45 40 0.045 PL PL 0.85 0 0 0.245 PL 0.02 0.0.15 0.025 0.01 0.01 PL 14.45 40 0.047 PL PL 0.87 0 0 0,26 PL 0.02 0.015 0.025 0.015 0.01 PL 14.47 35 0.042 PL PL 0.83 <0 0 0.245 PL <0 0.01 0.025 0.01 0.007 PL 14.35 35 0,047 PL PL 0.82 0 <0 0.246 PL <0 0.013 0.025 0.015 0.01 PL 14.31 34 0.058 PL <0 0.85 0.05 <0 PH <0 <0 0.02 0.028 0.02 0.013 <0 14.31 32 0.05 <0 <0 0.9 0.075 0 0.26 <0 0 0.02 0.028 0.015 0.015 PL 14.38 31 O.I PL <0 0.9 0.15 <0 0.27 0 <0 0.025 0.025 0.02 0.02 <0 14.44 30 0.05 PL <0 0.9 0 <0 0.32 PL <0 0.025 0.025 0.015 0.01 PL 14.51 30 0.05 PL <0 0.9 <0 <0 0.32 PL <0 0,015 0.025 0.015 0.015 PL 14.56 30 0.06 <0 <0 0.95 0.05 0 0.32 <0 0 0.025 0.028 0.02 0.02 <0 14.6 30 0,065 PL <0 0.975 0 <0 0.3 PL <0 0,025 0.025 0.023 0.015 PL 14.57 28 0.095 <0 <0 1,25 0.005 <0 0.48 <0 <0 0.045 0.025 0.03 0.02 PL T4.e7 29 0.093 <0 <0 1.35 0 0 0,5 <0 0 0.055 0.025 0.04 0.025 <0 14.7 29 O.i <0 <0 1.35 <0 0 0.48 <0 0 0.045 0.025 0.04 0.025 <0 14.71 28 0.08 PL <0 1.3 <0 0 0.48 <0 0 0,05 0 0,035 0.02 PL 14.71 28 0,1 <0 <0 1.27 0 0 0.49 <0 0 0.045 <0 0.035 0.03 PL 14.69 28 0.11 <0 <0 1.33 0.05 0 0.5 <0 0 0.055 0 0.04 0.025 <0 14.7 26 0.11 PL <0 1.33 0.05 0 0.5 PL <0 0.05 0 0.04 0,025 PL 14.7 25 0.125 PL <0 1.45 PL <0 0.6 PL <0 0.06 0 0.04 0.025 PL 14,7 FPP Area (inches H20) FPP-SVE-1 FPP-VMP-II FPP-VMP-ID FPP-VMP-2S FPP-VMP-21 FPP-VMP-2D FPP-VMP-3S FPP-VMP-31 FPP-VMP-3D FPP-VMP-4S FPP-VMP-41 FPP-VMP-4D FPP-GMP-l (feet) 66 0.025 PL <0 <0 <0 <0 0.01 <0 0 <0 <0 15.17 - 0.033 <0 0 0 PL <0 0.15 0 0.005 <0 <0 15.19 66 0.035 <0 0 0 PL <0 0.01 <0 <0 <0 <0 15.19 63 0.03 <0 0 0 <0 <0 0 0 0 PL <0 15.18 64 0.04 <0 <0 0 <0 PL 0.005 <0 0 PL <0 15.17 61 0.03 PL <0 <0 PH <0 <0 <0 0 PL <0 15.17 59 0,033 PL <0 <0 PL <0 <0 <0 0 PL <0 15.18 62 0.035 <0 0 0 <0 <0 <0 0 0 <0 0 15.2 6! 0.038 <0 <0 <0 0 <0 <0 0 0 PL 0 15.17 58 0,03 <0 <0 <0 0.005 <0 PL <0 <0 PL PL 15.17 56 0.028 <0 <0 <0 0,005 PL <0 <0 <0 PL PL 15.18 50 0.04 <0 <0 <0 0.13 0 <0 <0 0 PL PL 15.19 48 0.038 <0 <0 <0 0.033 0 <0 PL 0 PL PL 15.2 46 0.035 PL <0 <0 0.035 0 <0 <0 <0 PL. PL 15.17 42 0.03 PL <0 <0 0,055 0 PL PL 0 PL PL 15.21 42 0.03 PL PL <0 0.05 0 PL <0 0 PL PL 15.2 39 0.022 PL <0 PL PL PL PL <0 <0 PL PL 15.2 37 0,022 PL PL PL 0 PL PL PL <0 PL PL 15.2 36 0.02 PL <0 <0 0.083 PL PL <0 <0 PL PL 15.19 36 0.02 <0 <0 <0 0.045 <0 PL <0 0 <0 <0 15.2 35 0.045 PL <0 <0 0.225 <0 <0 <0 <0 PL PL 15.19 35 0.09 <0 <0 <0 0.125 <0 PL <0 <0 PL PL 15,19 35 0.09 <0 <0 <0 PL PL PL <0 <0 PL PL 15.19 34 0,05 <0 <0 <0 0.035 <0 <0 0 <0 PL PL 15.19 33 0.02 <0 <0 <0 0.105 <0 PL <0 <0 PL PL 15.19 32 0,165 <0 <0 <0 PH <0 <0 <0 0 <0 ,PL 15.2 32 0,145 <0 <0 0.003 0 <0 <0 0.003 0 <0 <0 15.2 32 0.025 0 0.003 0 PL <0 <0 <0 0.003 <0 <0 15.2 32 0.025 PL <0 <0 <0 PL PL <0 0 PL <0 15.21 32 0.015 <0 <0 <0 PL PL PL <0 0 PL <0 15.19 32 0.025 <0 <0 <0 0.15 PL PL <0 0 PL PL 15.2 32 0.027 <0 <0 <0 0.16 PL PL <0 <0 PL PL 15.21 30 0.017 0.015 <0 <0 0.12 PL <0 <0 <0 PL PL 15.22 SVE System Air Flow (SCFM) Velocity (?^ AST-SVE-1 (fpm) Velocity («! FPP-SVE-1 (fpm) Velocity (a, INTAKE (fpin) Velocity (SJ EXHAUST (fpm) PID (S] AST-SVE-1 (ppm) PID (ft) FPP-SVE-1 (ppm) PID (ai, INTAKE (ppm) PID ((it, EXHAUST (ppin) System Vacuum 1 (" Hg) System Vacuum 2 (" Hg) Exhaust Temp, (degrees F) 90 2000 300 2750 3250 - - - - 4.95 5.2 177 95 2000 900 2800 4000 212 9 256 175 4.8 5.1 180 95 2000 400 2000 3750 - - - - 4.9 5.2 185 95 2500 50 - - — - — - 4,8 5 185 95 - - - - 24 4 232 155 4.9 5.2 190 95 - - - - — - - - 4.8 5.1 186 101 - - - - - - - - 4.6 4.9 182 99 - - - - 52 4 181 166 4.8 5.2 190 95 - - - - 10 6 159 139 4.9 5.2 191 98 - - - - — - - — 4.8 5 186 99 - - - - - - - - 4.6 4.9 176 108 - - - - — — — — 4.4 4.8 170 118 - - - - - - - - 4.4 4.7 165 122 - - - - — — — — 4.2 4.6 160 127 - .. - - — — — — 4.2 4.4 160 127 - - - - — — — — 4 4.4 157 122 - - - - — — — — 3.8 4.2 152 127 - - - - — — — — 3.6 4.1 150 127 - - - - — — — — 3.6 4.1 150 127 - - - - — — — — 3.6 4 152 128 - ~ - - 128 5 135 146 3.6 4 150 126 - - - - — — • — — 3.5 4 150 126 - - - - 123 8 97 143 3.5 4 151 126 - - - - 128 6 97 153 3.4 4 155 126 — - - - — — — — 3.4 4 150 134 - — - - - .,. - - 3.4 3.9 J45 135 - - - - 219 12 264 257 3.4 4 153 134 - - - 237 ,14 252 268 3.4 3.9 155 135 - - - - - - - " 3.4 3.8 150 135 - - - - 203 8 136 239 3.4 3.8 150 135 - - - - - - - - 3.3 3.8 150 135 - - " - - - - 3.3 3.8 148 135 - - - - - - - - 3.3 3.8 140 Notes: PL = Pegged Low PH = Pegged High! <0 = Slight positive pressure — = Not Measured g:\projccis\00.l-6016\goldcr\SVE TS ReponViablc.t.xIs, T.nbleS Golder Associates 304906 Table 5 Page 1 ol' I September 2000 Table 6a Phase I Constant Rate Test Soil-Gas Analytical Laboratory Results Virgin Island Chemical Site St. Croix, U.S. Virgin Islands 003-6016 W o o Client ID: Testing Period/Time: Lab ID Date Sainpled: Matrix: FPP-SVE-I Phase 1/1210 B26 376 23-Mar-OO Soil-Gas FPP-SVE-1 (duplicate) B26 377 23-Mar-OO Soil-Gas FPP-SVE-1 Phase 1/1814 B26 387 23-Mar-OO Soil-Gas FPP-SVE-1 Phase 1/0648 826395 24-Mar-OO Soil-Gas FPP-SVE-1 Phase 1/1741 \V97 97 24-Mar-OO Soil-Gas FPP-SVE-1 Phase 1/0748 W97 101 25-Mar-OO Soil-Gas FPP-SVE-I Phase 1/1742 W97 105 25-Mar-OO Soil-Gas FPP-SVE-1 (duplicate) W97 106 25-Mar-OO Soil-Gas FPP-VMP-II PhaseI/1215 B26 378 23-Mar-OO Soil-Gas FPP-VMP-II Phase 1/1819 B26 388 23-Mar-OO Soil-Gas Site Target Compounds Acetone Chloroform Ethylbenzene Methylene chloride Toluene iricfep-Xylene o-Xylene (ppmv) <2 5.516 <0.07 <2 0.8 0.18 0,09 <2 6.91 <0.07 <2 0.45 0.15 <0.07 <2 13.112 <0.07 <2 0.48 <0.07 <0.07 <2 26.321 <0,07 <2 0.33 <0.07 <0.07 <2 5.85 <0.07 <2 0.19 <0.07 <0.07 <2 16.69 <0.07 <2 0,12 <0,07 <0.07 <2 9.98 <0.07 <2 0.22 <0.07 <0.07 <2 10.17 <0.07 <2 0.12 <0.07 <0.07 <2 2.313 <0.07 <2 0.23 <0.07 <0.07 <2 0.432 <0,07 <2 0.16 <0.07 <0.07 Client ID: Testing PeriodATime: Lab ID Date Sampled: Matrix: AST-SVE-1 Phase 1/1230 B26 372 23-Mar-OO Soil-Gas AST-SVE-1 Phase 1/1800 B26 391 23-Mar-OO Soil-Gas AST-SVE-1 Phase 1/0635 B26 394 24-Mar-OO Soil-Gas AST-SVE-1 Phase 1/1733 W97 95 24-Mar-OO Soil-Gas AST-SVE-1 (duplicate) * W97 96 24-Mar-OO Soil-Gas AST-SVE-1 Phase 1/0739 W97 100 25-Mar-OO Soil-Gas AST-SVE-1 Phase 1/1749 W97 107 25-Mar-OO Soil-Gas Site Target Compounds Acetone Chloroform Ethylbenzene Methylene chloride Toluene m&p-Xylene o-Xylene (ppmv) <2 <0.005 12.73 <2 5.9 48.79 5.64 <2 <0.005 3.69 <2 2.51 12.52 1.55 <2 <0.005 3.58 <2 2.11 12.35 1.59 <2 <0.005 1,98 <2 1.36 6.31 0.82 <4 <0.01 2.02 <4 1.17 6.74 0.89 <2 <0.005 2.58 <2 2.19 8.44 1.07 <2 <0.005 6.94 <2 3.58 26.14 3.16 G:\0036016\Goldcr\SVETS Report tables.xls (Table6) Golder Associates Pane 1 of 2. September 2000 Table 6a Phase I Constant Rate Test Soil-Gas Analytical Laboratory Results Virgin Island Chemical Site St. Croix, U.S. Virgin Islands 003-6016 Client ID: Testing Period/Iime: Lab ID Date Sampled: Matrix: AST-VMP-11 Phase 1/1233 B26 373 23-Mar-OO Soil-Gas AST-VMP-11 Phase 1/1749 B26 392 23-Mar-OO Soil-Gas AST-VMP-21 Phase 1/1239 B26 381 23-Mar-OO Soil-Gas AST-VMP-21 Phase 1/1756 B26 393 23-Mar-OO Soil-Gas AST-VMP-31 Phase 1/1243 B26 374 23-Mar-OO Soil-Gas AST-VMP-41 Phase 1/1248 326375 23-Mar-OO Soil-Gas Site Target Compounds Acetone Chloroform Ethylbenzene Methylene chloride Toluene m&p-Xylene o-Xylene (ppmv) <2 <0.005 O.I <2 0.17 0,39 <0.07 <2 <0.005 0.13 <2 0.2 0.52 <0.07 <2 <0.005 O.I <2 0.23 0.45 0.08 <2 <0.005 <0.07 <2 0.17 <0.07 <0,07 <2 <0.005 <0.07 <2 0.23 0.98 0.11 <2 <0.005 <0,07 <2 0.25 <0.07 <0.07 Sample vial received with less than 3 psi positive pressure. Vial was repressurized with nitrogen, resulting ini a dilution of 2. Client ID: Testing Period/Time: Lab ID Date Sampled: Matrix: fNTAKE Phase 1/1255 B26 379 23-Mar-OO Soil-Gas INTAKE Phase 1/1842 B26 389 23-Mar-OO Soil-Gas fNTAKE Phase 1/0654 B26 396 24-Mar-OO Soil-Gas INTAKE Phase 1/1800 W97 99 24-Mar-OO Soil-Gas INTAKE Phase 1/0756 W97 103 25-Mar-OO Soil-Gas INTAKE Phase I/I807 W97 109 25-Mar-OO Soil-Gas Site Target Compounds Acetone Chloroform Ethylbenzene Methylene chloride Toluene m&p-Xylene o-Xylene (ppmv) <2 0.244 13.02 <2 5.83 49.67 5.72 <2 0.162 3.53 <2 2.68 11.58 1.42 <2 0.107 2,84 •<2 2.06 9.04 1.16 <2 0,091 2,29 <2 1.64 7.43 0.98 <2 0.036 2.93 <2 2.06 9.46 1.2 <2 0.079 5.94 <2 3.24 21.57 2.68 O o 00 Client ID: Testing Period/Time: Lab ID Date Sampled: Matrix: EXHAUST Phase 1/1257 B26 380 23-Mar-OO Soil-Gas EXHAUST Phase 1/1845 B26 390 23-Mar-OO Soil-Gas EXHAUST Phase 1/0657 B26 397 24-Mar-OO Soil-Gas EXHAUST Phase 1/1756 W97 98 24-Mar-OO Soil-Gas EXHAUST Phase 1/0753 W97 102 25-Mar-OO Soil-Gas EXHAUST Phase I/I810 Vv'97 110 25-Mar-OO Soil-Gas DOWNGRAD Phase 1/0655 B26 398 24-Mar-OO Soil-Gas DOWNGRAD Phase 1/0800 W97 104 25-Mar-OO Soil-Gas Site Target Compounds Acetone Chlorofonn Ethylbenzene Methylene chloride Toluene m&p-Xylene o-Xylene (ppmv) <2 0.144 4.49 <2 2.78 15.28 1.85 <2 0.158 5.32 <2 2.88 18.93 2.34 <2 0,103 6,1 <2 2.81 22.81 2.74 <2 0.083 2.26 <2 1.49 7,43 0.98 <2 0.034 2,93 <2 1.93 9.64 1.23 <2 0,072 4.13 <2 2.53 14,54 1.85 <2 <0.005 <0.07 <2 0,34 <0.07 <0.07 <2 <0.005 <0.07 <2 0.09 <0,07 <0.07 O:\0036016\Golder\SVE TS Report tablcs.xis (Table6) Golder Associates Paee2of2 September 2000 Table 6b Phase I Constant Rate Test Mass Removal Calculations Virgin Islands Chemical Site St. Croix, U.S. Virgin Islands 003-6016 Sample Port Start of Test Intake Intake Intake Intake Intake Intake End of Test Sample Date Time 3/23/00 0730 3/23/00 1255 3/23/00 1842 3/24/00 654 3/24/00 1800 3/25/00 756 3/25/00 1807 3/26/00 0730 Compound Ethylbenzene m&p-Xylene o-Xylene Chloroform Ethylbenzene m&p-Xylene o-Xylene Chloroform Ethylbenzene m&p-Xylene o-Xylene Chloroform Ethylbenzene m&p-Xylene o-Xylene Chloroform Ethylbenzene m&p-Xylene o-Xylene Chloroform Ethylbenzene m&p-Xylene o-Xylene Chloroform Molecular V\/eight 106.2 106.2 106,2 119.35 106.2 106.2 106.2 119.35 106,2 106.2 106.2 119.35 106.2 106.2 106.2 119.35 106.2 106,2 106,2 119.35 106.2 106.2 106.2 119.35 Concentration [ppmv](1) 13.02 49.67 5.72 0.244 3.53 11.58 , 1.42 0.162 2.84 9.04 1.16 0.107 2.29 7.43 0.98 0.091 2.93 9.46 1.2 0.036 5,94 21.57 2.68 0.079 Concentration [ug/L] 57.52 219.42 25.27 1.21 15.59 51.16 6.27 0.80 12.55 39.94 5.12 0,53 10.12 32.82 4.33 0,45 12.94 41.79 5.30 0.18 26.24 95.29 11.84 0.39 Flow Rate [ft3/min] 95 95 95 95 108 108 108 108 127 127 127 127 126 126 126 126 134 134 134 134 135 135 135 135 Pressure (in. H2O] -62 -62 -62 -62 -50 -50 -50 -50 -34 -34 -34 -34 -30 -30 -30 -30 -28 -28 -28 -28 -26 -26 -26 -26 Mass Removal Rate [lb/day] 0.42 1.59 0.18 0.009 0.13 0.43 0.05 0.007 0.13 0.42 0.05 0.006 0.11 0.34 0.05 0.005 0.14 0.47 0.06 0.002 0.30 1.08 0.13 0.004 Time from start of test [hours] 0 5.5 5.5 5.5 5.5 11.2 11.2 11.2 11,2 23.5 23.5 23.5 23.5 34.5 34.5 34.5 34.5 48.5 48.5 48.5 48,5 58.5 58.5 58.5 58,5 72 Time Over Interval [hours] 8.4 8.4 8.4 8.4 9.0 9.0 9.0 9.0 11.7 11.7 11.7 11.7 12.5 12.5 12.5 12.5 12.0 12.0 12.0 12.0 18.5 18.5 18.5 18.5 Mass Removed Over Interval [lb] 0.14 0.55 0.06 0.003 0.05 0.16 0.02 0.003 0.06 0.20 0,03 0.003 0.06 0.18 0.02 0.002 0.07 0.23 0.03 0.001 0.23 0.83 0.10 0.003 1 Grand Total: Cumulative Mass Removed [lb] 0.14 0.55 0.06 0.003 0.19 0.71 0.08 0.006 0.26 0.92 0.11 0.008 0.31 1.10 0.13 0.011 0.39 1.33 0.16 0.012 0.61 2.16 0.27 0.015 3.06 Notes: (1) Concentration data from Microseeps Lab analyses (2) Negative pressure indicates vacuum U) O y£> o G:\003-6016\Golder\SVE TS Report\ MassLab.xls\Phas6 I Data Golder Associates Septeinber 2000 Table 7 Analytical Determination of Well Efficiency, Radius of Influence (ROI), and Air Permeability Intermediate VMPs Virgin Island Chemical Site St. Croix, U.S. Virgin Islands TEST SVE Only AS/SVE Time of Readings 3/25/00 9:30 3/25/00 9:30 3/23/00 14:30 4/16/00 7:30 4/16/00 7:30 4/15/00 15:05 Area AST AST FPP AST AST FPP Barometric Pressure, in Ha 29.98 29.98 29.83 30.14 30.14 30.13 rl ID 11 21 11 11 21 11 rl, ft 5 10 5 5 10 5 r2 ID 21 31 21 21 31 21 r2, ft 10 20 10 10 20 10 Predicted Pw, in w.c. gauge -6.4 -3.6 -0.2 -19.3 -4.6 -0.2 Actual "Pw", in w.c. gauge -29 -29 -62 -21 -21 -28 ROI, ft 15 22 10 12 22 10 k, cm2 1.05e-6 2.05e-6 4.69e-6 4.15e-7 1.98e-6 2.18e-6 Notes: ID = identification number in w.c. = inches water colunm ROI = radius of influence See text for equations used in calculations w o yo G:\003-6016\Golder\SVE TS Report\ ROI_anaIyt.XLS, Ana^l ROI Golder Associates September 2000 Table 8 Phase II Step Test Results - AST Area Virgin Island Chemical Site St. Croix, U.S. Virgin Islands 003-6016 Date: Time: Stage: 05-Apr-OO 1630 Baseline 06-Apr-OO 1149 08-Apr-OO 1200 Step 1 08-Apr-OO 1330 Step 1 08-Apr-OO 1500 Step 2 08-Apr-OO 1530 Step 2 08-Apr-OO 1600 Step 2 08-Apr-OO 1630 Step 2 08-Apr-OO 1745 Step 3 08-Apr-OO 1815 Step 3 08-Apr-OO 1900 Step 3 08-Apr-OO 1930 Step 3 ASTArea • Pressure (inches H20) AST-SVE-1 .AST-SVE-2 AST-SVE-3 AST-SVE-4 AS-l (psig) AST-GMP-1 (feet) .AST-VMP-11 AST-VMP-ID AST-VMP-2S AST-VMP-21 AST-VMP-2D AST-VMP-3S AST-VMP-31 AST-VMP-3D AST-VMP-4S AST-VMP-41 AST-VMP-4D Compressor (psig) - - - - - - - - - - - - - - - - - - - - - - .. - - - - - - - - - 0.005 0.04 0.01 0.005 45 - 0 0 0 0,01 0 0 0.005 0.03 0.015 0.01 0.01 45 0.01 0.04 0.02 0.005 45 - 0.075 0.05 0.02 0.02 0 0,02 0,005 0.115 0 0.02 0.06 45 0.02 0.04 0 0 58 ((3,1435) - 0.075 0.075 0.02 0,02 0.03 0 0,015 0,01 O.I <0 0.03 70 ((S,1435) 0 , 0.035 <0 <0 - 0.075 0.075 0.02 0.02 0.03 0 0.015 0.015 0.01 0.005 0.02 0,1 0.035 PL <0 55 ((3,1615) - 0,22 0.21 0.02 0.02 0.03 <0 0,01 0.01 0,01 0.005 0,015 65 ((S,1615) 0,01 0.035 <0 <0 54 - 0.075 0.05 0.02 0.02 0.035 0 0.015 0.01 0.005 0 0,015 70 0.005 0.055 PL <0 - - 0.05 0.05 0.02 0.01 0.015 0 <0 0.05 0 0.01 0.035 - 0,01 0.075 PL >0 64 - 0.05 0.05 0.01 0.03 0.02 0 0 , 0.05 0.005 0.01 0,035 100 0.005 0.09 PL PL 64 .. 0.05 0.05 0.01 0.02 O.ll 0 <0 0.03 0 0.01 0.03 100 0.005 0.1 PL PL 63 .. 0.1 * 0.025 0 0.02 0.065 0 <0 0.03 0.005 0.075 0.03 100 Flow (SCFM) 1 AST-AS-1 1 __ 0,9 0.8 2.0 -- 2,6 2.7 4.2 4.0 ._ 3.9 Weather Conditions Teinp. (detp-ees F) Wind Speed (mph) Wind Direction Humidity (%) Bar. Pressure (inches) Van Temperature (°F) 100 3 SE 56 29.97 - 95 5 N-NE 55 30.06 — 94 10 E 56 30.06 84 97 22 E-SE 53 30.03 84 - - - - - — - ~ - - ~ - - - - - 85 8 E 55 30 81 - - - ~ - - 80 4 N 66 30.02 .. - - - - - _. - - - - __ Depth to Water (feet below TIC) AST-VMP-11 .^ST-VMP-ID AST-VMP-21 AST-VMP-2D AST-VMP-31 AST-VMP-3D AST-VMP-41 AST-VMP-4D AST-GMP-1 SVE-1 MW-! MW-6 - 14.44 - 14.55 - 14.72 - 14,73 15.07 13.4 15.95 16.41 - 14.52 - 14,84 - 14,81 - 14.8 15.24 13.55 16.11 16.58 13,12 13.69 13.61 13,09 13.81 14.21 14,09 14.26 14.64 13.57 15.62 16.55 13.22 13.52 12.61 12.82 13.83 14.11 14.28 14.18 14.45 13.5 15.48 16.51 - - - - - - - - - - - - - - - - ~ - - - - - - - - - - - - - - - 13.06 12.97 13,62 13.12 13.82 13.73 13.28 13.73 13.81 13.33 15.01 16.48 - - - - - - - - 13.12 12.45 13.65 12,9 13.83 13.32 14.16 13.4 13.47 13.32 14.7 16.47 - - - - - - - - - - - - 13.25 12.41 13.65 12.74 13.81 13.29 14.25 13.34 13.27 13.31 14.48 16.47 g:\projects\003-6016\Golder\SVE TS Repon\tables,xls, TableS Golder Associates Page I of2 September 2000 Table 8 Phase II Step Test Results - AST Area Virgin Island Chemical Site St. Croix, U.S. Virgin Islands 003-6016 Dale: Time: Stage: 05-.'=ipr-00 1630 Baseline 06-Apr-OO 1149 08-Apr-OO 1200 Step 1 08-.Apr-00 1330 Step 1 08-.Apr-00 1500 Step 2 08-Apr-OO 1530 Step 2 08-Apr-OO 1600 Step 2 08-Apr-OO 1630 Step 2 08-Apr-OO 1745 Step 3 08-Apr-OO 1815 Step 3 08-Apr-OO 1900 Step 3 08-Apr-OO 1930 Step 3 Dissolved Oxygen (mg/L) AST-VMP-U AST-V.MP-ID AST-VMP-21 AST-VMP-2D .'\ST-VMP-3I AST-VMP-3D AST-VMP-41 AST-VMP-4D SVE-1 MW-1 MW-6 MW-8 MW-10 0.59 - 1.15 - 1.38 - 0.88 8.9 1 0.86 - - - 0.84 - 0,86 - 1.22 - 1.19 0,63 0.52 1.01 - - - 0.2 - 0.27 - 0,21 - 0.26 0.33 0.27 0.24 - - - 0.51 - 0,91 - 0,98 - 1.8 0.5 2 2.25 - .. - - - - - - - - - - - - - - ~ - - - - - ~ - - - - - - - - - - - - - - 8.99 - 15.75 - 1.74 - 1.48 1.19 3.86 5.78 ~ - - - - - - - - - - - - - ~ - 11.82 - >20 - 2.01 ~ 2,58 1.42 6.05 1,86 - .. — - .. - - - - - - - - - - — 12.73 - 15.73 - 1.6 - 0.97 0.99 9.85 2.55 - OVKdReadings (ppmv) AST-SVE-1 AST-SVE-2 AST-SVE-3 AST-SVE-4 .4ST-SVE-5 AST-SVE-6 .^ST-VMP-II .AST-VMP-ID .AST-VMP-2S .AST-VMP-21 AST-VMP-2D AST-VMP-3 S AST-VMP-31 AS'T-VUV-3V> AST-VMP-4S AST-VMP-41 AST-VMP-4D - - - - - - >440 48,8 12.2 170 8.1 2,6 3 17.9 2.6 6.4 2 - - - - - 1.002 23 13.5 209,7 11.8 1.2 7.4 27.2 11.2 7,2 10,4 572 >1.000 7.4 4,9 - > 1,000 93.8 16.4 268 26.6 9.3 8 39,3 8.2 6.1 48.3 >1,000 SSSSSSSsiKggtKS; 22.6 31,6 - - >1.000 38 20,1 442 17.3 14.2 7.4 50 10.2 2.8 5.6 - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 175 7212 22 25 - - >212 17 11 >2I2 >212 17 5 14.1 8 5 5 - - ~ - - - - - - - - - - - - - ~ >212 >212 19 22.6 - >212 11.3 11 >2t2 >2I2 11 5 11.5 8.5 5.6 5.6 - - "- - - - - - - — .. .. - - - >2I2 >212 17 19 — - >212 14 8.5 >212 >212 11 5 11 5.6 5.6 5.8 Notes: PL = Pegged Low PH = Pegged Hight <0 = Slight positive pressure - = Not Measured to O vo M to g:\prqjects\003-601 6\Goldi:r\SVE TS Report\tables.xls, TableS Golder Associates Page 2 of2 September 2000 Table 9 Phase LI Step Test Results - FPP Area Virgin Island Chemical Site St. Croix, U.S. Virgin Islands 003-6016 jDate: Time: IStage: Pressure (inches H20) 1 FPP-AS-1 (psi) FPP-VMP-II FPP-VMP-ID FPP-VMP-2S FPP-VMP-21 FPP-VMP-2D FPP-VMP-3S FPP-VMP-3i FPP-VMP-3D FPP-VMP-4S FPP-VMP-41 FPP-VMP-4D 1 FPP-SVE-1 1 03-Apr-OO 1150 1 Baseline I - - - - - - - - - - - - 1 04-Apr-OO 0900/0930 Step 1 1 ^^ 0 0.01 0.01 <0 0 0 <0 <0 0 <0 <0 0 04-Apr-OO 1000/1015 Step 1 19.5 0,015 <0 0,01 PL <0 0,005 <0 PL 0,0025 0 0,06 - 1 04-Apr-OO 1100/1115 Step 1 17 0.015 0 0.01 PL <0 0,01 0,01 <0 0,005 0,015 0,01 PL 1 04-Apr-OO 1200/1215 Step 1 • 17 0,01 PL 0.01 <0 <0 0.01 0 0.005 0 <0 0,005 PL 1 04-Apr-OO 1300/1315 Step 2 Start 1255 19 0.0125 PL 0.0075 <0 <0 0.01 0 <0 0.0025 <0 <0 PL 1 04-Apr-OO 1400/1415 Step 2 18 0,015 <0 0,01 0 <0 0 0,005 0 0,005 0,01 0.005 PL 1 04-Apr-OO 1500/1515 Step 2 1 ''' 0,015 0.005 0,01 <0 0 0 <0 <0 0,005 0 <0 PL 1 04-Apr-OO 1600/1615 Step 2 17 0,015 PL - 0.01 <0 <0 <0 <o <0 0 <0 PL PL 1 04-Apr-OO 1700/1715 Step 2 1 '^ 0 0 0,0025 <0 0 0,005 <0 0 0 <0 <0 0.0025 1 04-Apr-OO 1800/1815 Step 3 Start 1755 21 0 PL <0 PL 1 ° o.oos PL <0 0 <0 PL <0 1 04-Apr-OO 1900/1915 1 Step 3 1 20 0 0 " <0 <0 I 0,13 0,0025 <0 PL 0 <0 <0 0 1 04-Apr-OO 2000/2015 Step 3 i 20 0 0.005 <0 PL 0 0,005 <0 <0 <0 <0 <0 <0 1 04-Apr-OO 2100/2115 1 Step 3 1 20 0 0 <0 <0 <0 0 <0 <0 0 PL PL <0 1 04-Apr-OO 2200/2215 [ Step 3 1 20 0 <0 <0 <0 <0 0.0025 <0 PL <0 <0 PL <0 1 OS-Apr-00 0730/0745 Step 4 Start 0630 1 ^^ 0,005 0 0 <0 <0 0,005 <0 <0 0 <0 0,005 0 1 05-Apr-OO 0830/0845 Step 4 1 22 0.005 0.005 0 0 0 0,01 0 <0 0,005 0,01 0 0,015 1 OS-Apr-00 0930/0945 Step 4 22 <0 0,005 0 0 0 0,015 0.005 0 0,005 0,005 0.015 <0 1 OS-Apr-00 1030/1045 Step 4 21 0,005 0,01 0 0 <0 0.01 0,0075 <0 0.005 0.0075 0.05 0.02 1 05-Apr-OO 1130/1145 Step 4 21 0.0025 0,01 0.005 0.01 0 0,02 0,0175 0,005 0,01 0,0175 0.005 0,02 1 05-.'Npr-00 1230/1245 Step 4 21 0.0025 0.01 0.005 0.01 0 0.005 0-005 0. 0.01 0.015 0.12 0.03 1 OS-Apr-00 1330/1345 Step 4 21 0,01 0.005 0.005 0,01 0 0,01 0,02 <0 0.01 0,02 0,18 0.04 07-Apr-OO 0830 Step 5 25 0 0 0 0.005 0 0 PL PL 0-0075 0 <0 - 07-Apr-OO 0930 Steps 29 0,0025 0,015 0 0,0075 0 0.0025 0.01 <0 0.01 PL 0,03 - I 07-Apr-OO 1030 Step 5 29 0,01 <0 0 0,01 0 0 0,005 0,005 0.005 0,075 <0 <0 1 07-Apr-OO 1130 Step 5 27 0 0 0.015 0.01 0 0.01 0,02 0 0.005 0 0,005 0 07-Apr-OO 1250 Step 5 28 0,015 0.04 0.01 0,005 0 0,005 0,015 0,005 0.01 0.01 0 0,105 07-Apr-OO 1300 Step 5 - - - - - • 1 - - - - ! - 1 _ Flow (SCFM) : 1 FPP-AS-1 - 0.6 0,65 0,65 0,65 _ L25_ _ _ 1.25 1,25 1.25 __ 1.25 _ 2.5 _ _ 2.5 . 2,5 .. _ 2,5_ 2,55 4,5 .4,5 4.5 _ 4.5 __ 4,3 4.5 4,4 5 7,2 7.2 7,2 7.3 - i Weather Conditions i iTemp, (degrees F) Wind Speed (mph) jWind Direction Humidity (%) |Bar. Pressure (inches) 92 5 NW 68 29,89 90 6 E 62 30 93 8 S-SE 59 30.01 96 4 SE 58 30,01 98 6 SE 56 30 97 8 SE 48 29,96 99 s SE 49 29,96 99 6 SE 51 29,93 95 5 SE 51 29.93 - - - ~ - 93 3 E-SE 50 29,95 80 4 SE 55 29.96 ~ - - - - - - - 84 5 SE 72 29-99 - - 100 5 S-SE 60 30,02 - - - - - - - - - ~i ,.; - - - 105 4 SE 59 29,99 91 8 E 66 30-08 - - - - - 91 7 E-SE 63 30.08 103 7 E 58 30.07 99 8 SE 60 30.06 - - - 1 Depth to Water (feet) IFPP-VMP-ID FPP-VMP-2D FPP-VMP-3D FPP-VMP-4D FPP-GMP-l IFPP-SVE-I MW-2 14,97 15,01 15,18 16.51 15.47 15.63 17.26 15.09 15,09 15.3 15.6 15,48 15.63 17.37 15,08 15.12 15,3 15.54 15.48 15,65 17.37 15.07 15,15 15,29 16.54 15,49 15,65 17.36 15.13 . 15,24 15,27 16,59 15,49 15.61 17.4 15,11 15,24 15,25 16,57 15,54 15.65 17.39 15.09 15,25 15,23 16.56 15,54 15.64 17,36 15,08 15,28 15,24 16,56 15,54 15,64 17,36 15,08 15.29 15.23 16,56 15,55 15,83 17.36 15.09 15,29 15,24 16,56 15.56 15,67 17.37 15.12 15,3 15,27 16.59 15,56 15,63 17,41 15.11 15,32 15,29 16,61 15,56 15.62 17.4 15,11 15.31 15,29 16.6 • 15,56 15,61 17.43 15,11 15,31 15,29 16,61 15-57 15-62 17-4 15,12 15,32 15,31 16,63 15,56 15.61 17.42 1512 15.25 15-3 16,59 15.58 15.61 17-41 15,12 15,28 15,31 16 63 15.57 15.57 17.44 15,12 15,3 153 16,63 15,57 15,53 17,42 15,12 15,31 15,3 1664 15.52 15,53 17,42 15,12 15,32 15,29 16.63 15,59 15,51 17.42 15.12 15,32- 15,29 16-63 15.59 15.51 17.42 15,09 15.34 15,26 16,45 15,58 15.44 17,37 15-14 15-3 1531 16.5 15.68 15,43 17,43 15,15 15,31 15,32 16.57 15,68 15,43 17.44 - - - - - - 15,18 15,33 15,35 16,7 15,7 15.38 17,49 15,18 15,35 15.33 16.7 15,74 15,41 17,45 15-19 j 15.29 15.35 16-69 15.61 15.6 17.49 1 Dissolved Oxygen (mg/L) FPP-VMP-ID |FPP-VMP-2D FPP-VMP-3D FPP-VMP-4D FPP-SVE-I MW-2 1,68 !,22 1,77 2.28 1.08 1.37 0.69 1.47 1,39 2,05 0,63 1,22 1.34 1.35 1,15 1,84 0.66 1,49 1.5 2.2 0,96 1.81 1,13 1,03 106 1,69 0,83 1.54 0,82 0.82 1,21 2 1,01 1,86 0.92 0,77 I.I 2,42 1-39 1,81 1,3 0.84 2,02 2,39 0,82 1,81 0,95 1.25 0.87 2.61 0,95 2.26 0.88 0,82 0,94 2,97 1,08 2,12 0,91 0,82 1,14 2.99 1,18 2.84 1,04 0,87 1,25 2,9 1,8 2,18 0,94 1.19 0 9 2,62 1.25 1,92 093 0,96 1.19 3-03 1-56 2-63 0-83 0-89 0.92 3,02 0.8 2,43 1,01 0,79 1-66 3.75 0,98 1,73 1,08 0.89 1,66 3,1 1,33 2.64 1,3 0,8 1,31 3,69 1,6 3,02 2-38 0,9 1,39 3,85 1,88 2,91 1,98 1,53 1,5 3,2 1,93 2,49 3,04 i-01 1,65 4 22 146 1,95 1 66 0,86 308 4,58 1.77 2,7 1-84 1.14 0,38 1,87 0.83 0.52 4.31 0.34 3,2 3,1 1 15 0,72 7 0,61 - - - - - 0,48 2.1 1.28 0,86 1 0,55 1.29 678 2,9 3.76 1,2 1,6 0,65 2.42 1,11 1,35 0,81 0.7 1 OVM Readings (ppm) FPP-VMP-II FPP-VMP-ID FPP-VMP-2S FPP-VMP-21 FPP-VMP-2D FPP-VMP-3S FPP-VMP-31 FPP-VMP-3D FPP-VMP-4S FPP-VMP-41 FPP-VMP-4D 6,6 3,5 4,5 1,5 4,5 1,5 1.5 1.5 1,5 1,5 0 4 2 0 2 3 2 1 3 1 2.4 0 - - - - - - - — - 3,4 3.2 2,5 2 2.2 1.9 1.4 2.6 1.9 4,7 0 - - - - - - - - _ - - 1 1 0 0 i 0 0 0.5 0 0 0 - — - - - 1,8 1 1 1 2 0 0 0 0 2 0 - - - - - - - - - 1 1 1 1 2 1 1 2 1 2 0 1 2 2 1 1 0 1 1 1 3 0 - — - - — - - 2 1 0 1 1 0 0 1 0 2 0 ~ - — - ,. - - .. - - - - - — - - 3 2 3 2 3 1 1 3 2 4 1 - - — — - - — - - - - 5-7 2 4-3 3 4.5 3,5 1,8 2 34 5,1 0 - - - - - - - - 3 1 0 1.5 1.4 1-5 0 2-2 0 3-7 0 ,. - - - ... - ,- : 1 J 1 2 2 1 0 2 2-4 3-7 0 3 8,3 2 2,3 4.8 0.3 3 2.8 2,3 1,7 2,6 ~ - - ~ - - - - - - - - - - - - - 1,4 1,9 0,3 0.7 1.4 0,5 1.2 1 0.5 2,1 0,7 3,5 2-1 0.5 0.7 3-2 2-1 1.2 2-2 2.1 4-4 2.7 1-2 1 5-2 3.2 5,3 7,1 1 3,1 SI 2 8 • 7 , 9 3,2 1 Notes: PL = Pegged Low PH = Pegged Hight <0 = Slight positive pressure - = Not Measured i!:VTOis':ls\00j-60l6\Gtilder\SVE TS Report\tables,xls. Tabic"} Golder Associates ! 304913 L - - - Table 9 Page 1 of I September 2000 Table 10 Phase II AS/SVE Test - System and Weather Measurements Virgin Island Chemical Site St. Croix, U.S. Virgin Islands 003-6016 Date: Time: 14-Apr-OO 1415 14-Apr-OO 1645 14-Apr-OO 1830 14-Apr-OO 2115 14-Apr-OO 2205 15-Apr-OO 0615 15-Apr-OO 1435 15-Apr-OO 2010 16-Apr-OO 0700 16-Apr-OO 1347 SVE System Air Flow (SCFM) Velocity @ INTAKE (fpm) iVelocity (ai EXHAUST (fpm) PID (0^ INTAKE (ppm) FID @ EXHAUST (ppm) System Vacuum i (" H20) System Vacuum 2 (" H20) Exhaust Temp, (degrees F) 126 >6,000 >6,000 772 728 50 57 160 130 350 750 46 310 48 57 160 135 100 600 5.1 2 47(3.4"Hg) 54 (4" Hg) 150 130 - - - - 46 53 150 130 1,500 1,800 16.2 625 46 (3.4" Hg) 53 149 135 750 2,200 3.5 827 44 (3.2" Hg) 52(3.8"Hg) 145 135 1,500 750 18 827 42(3.1"Hg) 51(3.7"Hg) 150 135 2,000 1,200 332 692 42 50 145 135 2,500 1,800 4.5 1,084 42 50 145 135 2,300 1,500 3.4 1,048 41 49 148 Weather Conditions Temp, (degrees F) Wind Speed (mph) Wind Direction Humidity (%) Bar. Pressure (inches) Van Temperature (°F) PID (a), downgradient (ppm) 93 14 E 52 30.11 85 0 84 9 SE 60 30.09 83 0 81 6 E 58 30.11 — 0 79 5 E-NE 61 30.15 — - 79 7 E 57 30.15 — 0 77 10 E 57 30.14 — 0 87 3 E-SE 56 30,13 — 0 79 6 E-NE - 63 30.15 — 0 77 2 N-NE 67 30,14 __ 0 92 5 E 61 30.11 _. 0 System Vacuum 1 (" H20) Air Flow (SCFM) 50 126 48 130 47 135 46 130 46 130 44 135 42 135 42 135 42 135 41 135 o g:\projects\003-6016\Golder\SVE TS Report\tables.xls, TablelO Golder Associates September 2000 Table 11 Phase II AS/SVE Test Results - AST Area Virgin Island Chemical Site St. Croix, U.S. Virgin Islands 003-6016 .Date: Time; 14-Apr-OO 1530 14-Apr-OO 1725 14-Apr-OO 1930 14-Apr-OO 2045 14-Apr-OO 1300 15-Apr-OO 0750 15-Apr-OO 1125 15-Apr-OO 1540 15-Apr-OO 1920 16-Apr-OO 0730 16-Apr-OO 1520 Flow AST-AS-1 (scfm) AST-SVE-1 (fpm) 3.4 >6.000 3,7 >6.000 3.8 4.000 3.8 6,000 3.8 6.000 4.4 >6,000 3.5 >6,000 4 >6.000 3,7 >6,000 3,8 >6,000 4 >6.000 Vacuum (inches H20) AST-SVE-1 AST-SVE-2 AST-SVE-3 AST-SVE-4 AST-SVE-5 AST-SVE-6 AST-VMP-11 AST-VMP-2S AST-VMP-21 AST-VMP-3S AST-VMP-31 AST-VMP-4S AST-VMP-41 32 - - - - — - <0 - 0 0.02 - 30 - — ~ - — - 0 — 0 - 0,03 ~ 28 - - - ~ - 0,75 0 0,18 0.02 0.035 0.025 0.01 28 0.165 0,025 0 - ~ 3,7 0 0,78 0.02 0.045 0.03 0.12 28 0,16 PL 0,005 - - 3,85 PL 0.6 0.015 0.05 0.025 0.12 24 0.18 <0 0.005 - - 3.85 <0 1 0.035 0.01 0.015 0.01 22 0.18 0.01 0.01 - ~ 3,65 <0 1,55 0,03 0,06 0,015 0,08 25 0.18 0.01 0.005 - - 3.6 <0 0,6 0,015 0,055 0,02 0.1 22 0,22 0,01 0,005 ~ - 3,4 <0 0,55 0,025 0,035 0,02 0,11 21 0,22 0,015 0,005 — — 3.3 <0 0,65 0,025 0,075 0,02 0,075 20 0.2 <0 0 ~ - 3.4 PL 0.6 0.04 0.03 0.005 0.07 Pressure (inches H20) AST-SVE-2 AST-SVE-3 AST-SVE-4 AST-VMP-11 AST-VMP-ID AST-VMP-2! AST-VMP-2D AST-VMP-31 AST-VMP-3D AST-VMP-41 AST-VMP-4D Compressor Pressure (psig) AST-AS-1 (psi) Pressure Regulator (psi) - - - PL 0 PL 0 PL 0.11 PL 0 150 45 59 — - — PL 0 PL 0,03 0 0,05 PL <0 155 44 59 ~ ~ — - 0 - 0.01 ~ 0 ~ 0 150 43 60 - ~ ~ - 0 - 0-0.01 ~ 0.0125 - 0.01 150 42 59 ~ ~ ~ - 0 ~ 0 - 0,04 ~ 0,025 150 41 59 ~ ~ - - 0.05 - <0 - 0.05 ~ 0.015 150 38 60 - - ~ - 0,1 - ,005 - 0,03 ~ 0,055 - 0,025 ~ 26 39 - ~ ~ ~ 0,12 ~ 0 ~ 0,055 ~ 0,015 150 28 36 - - - - 0,18 - 0 - 0,015 - 0,01 150 25 37 — - — - 0,11 - 0,005 — 0 — 0,005 150 25 36 - - - - 0.1 - >.25 - 0 ~ 0.01 150 24 35 to o M en g:\proiects\003-6016\Golder\SVE TS Report\tables.xls, Tablet 1 Golder Associates Paee 1 of 3 Septeinber 2000 Table 11 Phase II AS/SVE Test Results - AST Area Virgin Island Chemical Site St. Croix, U.S. Virgin Islands 003-6016 Date: Time: 14-Apr-OO 1530 14-Apr-OO 1725 14-Apr-OO 1930 14-Apr-OO 2045 14-Apr-OO 1300 15-Apr-OO 0750 15-Apr-OO 1125 15-Apr-OO 15-Apr-OO 1540 1920 16-Apr-OO 0730 16-Apr-OO 1520 Depth to Water (feet below TIC) AST-VMP-11 AST-VMP-ID AST-VMP-2S AST-VMP-21 AST-VMP-2D AST-VMP-3 S AST-VMP-31 AST-VMP-3D AST-VMP-4S AST-VMP-41 AST-VMP-4D AST-GMP-1 MW-1 MW-6 MW-8 13.48 13.79 13.91 13.95 - 14.12 14.48 - 14.5 14.43 14.18 15.4 16.81 - 13,64 13.81 - 13.93 13.95 - 14.11 14.3 ~ 14.51 14.36 14.15 15.51 16,81 - 13,51 13,71 " - 13,93 13,83'' ~ 14,13 14,21 - 14,5 14,22 14.32 15.47'^ 16.84 "^ ~ 13,51 13,71'' 4,53 13,96 13,82" dry 14,13 14,24 dr>' - 14,31 14,28 14,3 15.45" 16.82" 18.2 13.5 14.15 - 13,94 14,19 - ^ 14,13 14,59 - 14,57 14,58 14,85 15,92 16,76 - 13,52 14,23" 4,53 13,93 14,23^ drv 14.14 14,78 dr>' 14,53 14.6 14.86 16,06" 16,82" 18,84 13.57 14,42 dry 14,01 14,41 dry 14,12 14,79 dry 14,54 14,92 15.12 16.16 16,83 19,44 13,54 14,39 4,52 13,95 14,42 dry 14.13 14,74 dry 14,58 14,49 14,95 15,32 16,79 - Dissolved Oxygen (mg/L) AST-VMP-11 AST-VMP-ID AST-VMP-21 AST-VMP-2D AST-VMP-31 AST-VMP-3D AST-VMP-41 AST-VMP-4D MW-1 MW-6 MW-8 - 6.15 - 0.64 - 0,6 ~ 0,8 9,3 3,5 ~ ~ 6,64 - 8,75 - 0,79 ~ 0,71 9,32 4,32 - ~ 9.28 - 10.09 - 0.78 - 0.76 9,34 4,56 ~ 1.97 10.36 ~ 11.17 - 0.75 ~ 0.66 10.64 5,27 0.67 - 10,13 - 11,06 - 0,69 - 0,51 10,48 5,01 ~ - 10,03 - 10.92 ~ 0.52 - 0.63 10,41 5,27 0,85 - 7,66 - 8,37 - 0.41 - 0.69 8.29 4,64 0,56 - - - - - - - - - - - o a:\Droiects\003-6016\Golder\SVE TS ReDort\tables,xls. Tablet 1 Golder Associates Paee2 of 3 September 2000 Table 11 Phase II AS/SVE Test Results - AST Area Virgin Island Chemical Site St. Croix, U.S. Virgin Islands 003-6016 Date: Time: 14-Apr-OO 1530 14-Apr-OO 1725 14-Apr-OO 1930 14-Apr-OO 2045 14-Apr-OO 1300 15-Apr-OO 0750 15-Apr-OO H25 15-Apr-OO 1540 15-Apr-OO 1920 16-Apr-OO 0730 16-Apr-OO 1520 OVM Readings (ppmv) AST-SVE-1 AST-SVE-2 AST-SVE-3 AST-SVE-4 AST-SVE-5 AST-SVE-6 AST-VMP-11 AST-VMP-ID AST-VMP-2S AST-VMP-21 AST-VMP-2D AST-VMP-3S AST-VMP-31 AST-VMP-3D AST-VMP-4S AST-VMP-41 AST-VMP-4D 3 ~ - - - - — - - - - - ~ 7.3 - - ~ 332 - - ~ - - 36.8 - ~ 203.4 ~ — ~ - - - - 269 950 ~ - - - 34 - ~ 147 ~ - — - - 1 - 22.6 666 ~ - - ~ 43 ~ — 107.5 - ~ - - - ~ ~ 5.3 252 ~ - - - 28.1 57,8 — 45,7 ~ ~ ~ - " 1.2 - 3.5 314 - - ~ - 19.2 63,5 - 20,2 - - - - - 0 - 8 341 ~ " - ~ 28,8 130 — 48,8 - - ~ - - - - 3.1 294 ~ - - - 14 386 - 95.7 20 - ~ - - - ~ Notes: PL = Pegged Low PH = Pegged Hight " - Bubbles in well <0 = Slight positive pressure — = Not Measured U) o ,g:\proiects\003-6016\Golder\SVE TS Report\tables,xls, Tablet 1 Golder Associates Paee 3 of 3 September 2000 Table 12 Phase n AS/SVE Test Results - FPP Area Virgin Island Chemical Site St. Croix, U.S. Virgin Islands 003-6016 Date: Time: 14-Apr-OO 1445 14-Apr-OO 1630 14-Apr-OO 1852 14-Apr-OO 2040 14-Apr-OO 2230 15-Apr-OO 0700 15-Apr-OO 1100 15-Apr-OO 1505 15-Apr-OO 1830 16-Apr-OO 1125 16-Apr-OO 1500 Flow FPP-AS-1 (scfm) FPP-SVE-1 (fpm) 7,6 500 7,4 550 7,6 100 7,8 400 7.8 450 7,6 4,000 7,6 350 6,8 400 7,4 500 - 1,000 - 2,500 Vacuum (inches H20) FPP-SVE-1 FPP-VMP-II FPP-ViMP-2S FPP-VMP-21 FPP-VMP-3S FPP-VMP-31 FPP-VMP-4S FPP-VMP-41 38 - PL - 0,01 - 0 38 - 0 - 0,01 PL 0 0 34 - 0.01 - 0 - 0 - 33 - 0,005 - 0,005 - 0,005 - 32 ~ 0.015 - 0 ~ 0 - 30 ~ 0,015 - 0,01 - 0 , - 29 - 0.005 - 0.005 - 0 - 28 - 0,035 - PL - 0 - 28 - 0,01 - 0 - 0,005 23 - 0 - 0 - <0 — 24 — PL — 0,01 — <0 - Pressure (inches H20) FPP-AS-1 (psi) FPP-VMP-II FPP-VMP-ID FPP-VMP-21 FPP-VMP-2D FPP-VMP-31 FPP-VMP-3D FPP-VMP-41 FPP-VMP-4D 26 0.025 0.01 0.075 0.1 0.05 0 0.02 0.001 25 0,005 0,025 0,005 O.I - PL - 0,025 25 0.005 0.015 0 0.08 0.01 0 0.03 0.02 26 0,005 0 - 0 , 7 0.02 0.08 0.02 0.01 <0 0,02 25 0 0.02 0,02 0,04 0,055 0,02 0 0,02 24 O.OI 0.03 0.01 0.07 0.025 0 0 0.045 24 0,005 0,05 0,02 0,005 0,03 0,01 0 0,03 21 0,01 0,03 0,02 0 0,04 0 0,02 0.03 21 0,02 0,01 0,01 PL 0,005 0 - 0,035 0 - 0.02 0.02 10 PL 0.03 0.015 PL 0.005 0.005 PL 0.02 10 PL 0,04 0,025 PL 0,01 0 0,01 0,04 Pressure Regulator (psi) Air Compressor (psi) Depth to Water (feet below 7 FPP-VMP-11 FPP-VMP-ID FPP-VMP-2S FPP-VMP-21 FPP-VMP-2D FPP-ViVlP-3S FPP-VMP-31 FPP-VMP-3D FPP-ViMP-4S FPP-VMP-41 FPP-VMP-4D FPP-GK4P-I MW-2 MW-3 MW-7 59 125 TC) 14.17 15,09 - 14.64 15.3 - do' 15.09 - drv 16.6 15.99 17.39 - 18.54 59 122 - - - - - - - - - - - - — - - 59 122 14,71 15.19 - 14,59 15,32 - dry 15,37 - 15,16 16,77 15,98 17,48 - 18,03 60 125 - - - - - - - - - - - - - - - 60 125 14,7 15,21 - 14,63 15,33 - do' 15,48 - drv 16,83 15,98 17,47" - 17,94 58 121 14,73 15.19 3.98 14.14 15.13 4.75 dr%' 15.39 4.83 dr\' 16.88 15.98 17.45" - 18,29 57 122 - - - - - - - - - - - - — - - 60 122 14.72 15.21 - 14.62 15.36 - dry 15,49 ~ dry 17,01 15,98 17,51 ~ 19,34 60 122 14.72 15.29 4.7 14.68 15.38 4.72 dry 15.57 4.83 dry 17.17 15.98 17.56" - 19.31 - - 14,71 15.33 4,38 14,78 15,49 4,71 dry 15,5 4,73 dry 17 15,98 17,63 - 21,17 — — 14,72 15,32 4.48 14.78 15.48 4,76 dry 15.43 4,82 dry 16.98 15,96 17,61 - 21,1 g:\projecls\003-6016\golder\SVE TS Repon\lables.xls, Tablel2 Golder Associates o yo M September 2000 Table 12 Phase II AS/SVE Test Results - FPP Area Virgin Island Chemical Site St. Croix, U.S. Virgin Islands 003-6016 Date: Time: 14-Apr-OO 1445 14-Apr-OO 1630 14-Apr-OO 1852 14-Apr-OO 2040 14-Apr-OO 2230 15-Apr-OO 0700 15-Apr-OO 1100 15-Apr-OO 1505 15-Apr-OO 1830 16-Apr-OO 1125 16-Apr-OO 1500 Dissolved Oxygen (mg/L) FPP-VMP-II FPP-VMP-ID FPP-VMP-21 FPP-VMP-2D FPP-VMP-31 FPP-VMP-3D FPP-VMP-41 FPP-VMP-4D MW-2 MW-3 MW-7 - 4,8 - 2,1 - 8,3 - 0,8 8,58 — - - - - — - - - - — — - 5,1 2.24 - 9,82 - 1,11 8,91 - - - - - - - - - - — — - - 5.63 - 2.16 - 10.77 - 3.85 8.56 - - - 5.6 - 2.3 - 11.7 6.8 8.3 - 2.8* - - - - - - • - - - - - 6.93 - 2.58 - 12.32 - 10,01 9,38 - - - 6,67 - 2,18 - 11,5 - 9.07 8.93 — 3.69* - - - - - - - - — - - — - - — — — - — - OVM Readings (ppmv) if>0,l"H2O FPP-SVE-1 FPP-VMP-II FPP-VMP-ID FPP-VMP-2S FPP-VMP-21 FPP-VMP-2D FPP-VMP-3S FPP-VMP-31 FPP-VMP-3D FPP.VMP-4S FPP-VMP-41 FPP-VMP-4D 0 - - - 0 0 - - - - - - - - - - - - - - - - - 0 - - ~ - - ~ ~ - - - - ~ - - - - - - - - - - - 0 - - - - - - - - - - - 0 - - - - - - - - - - - - - - - - - - - - - - - 0 " - - - - ~ ~ " - - ~ 0 - - - — ~ - - - — — - ~ ~ - - - - - - - - - - - - - - — - — — - — — " Notes: PL = Pegged Low PH = Pegged Higlit " = bubbles in well <0 = Slight positive pressure — = Not Measured * = D/0 not measured within screened interval !:\projects\003-6016\golder\SVE TS Repon\tables,xls, TablelZ Golder Associates Page 2 of2 September 2000 Table 13 Phase n Extended Test Results - System and Weather Measurements Virgin Island Chemical Site St. Croix, U.S. Virgin Islands 003-6016 Date: iTime: SVE System Air Flow (SCFM) Velocity (al INTAKE (fpin) Velocity (a), EXHAUST (fpm) PID (al INTAKE (ppm) PID @ EXHAUST (ppm) System Vacuum 1 (" H20) System Vacuum 2 (" H20) Exhaust Temp, (degrees F) 27-Apr-OO 0705 27-Apr-OO 0713* FPP SVE-1 Only _ — — - — 94 94 180 46 3.000 2,250 - — 72 76 200 27-Apr-OO 0742** _ — — — — 71 71 225 27-Apr-OO 0805 _ 2.500 *** , — — 69 70 250 27-Apr-OO 0810 AST Only - 4.000 1.500 664 704 30 38 142 27-Apr-OO 0850 145 2.250 2,000 — 30 38 138 27-Apr-OO 0945 27-Apr-OO 1135 Start Extended Phase II Test (J? 145 400 1.500 — — 30 39 140 145 600 1,500 — — 30 39 140 27-Apr-OO 1244 0940 145 2.500 1.250 12 958 30 39 140 27-Apr-OO 1600 145 — — - 30 39 140 27-Apr-OO 2000 155 1.500 3.000 19 870 30 39 135 28-Apr-OO 0930 145 1.000 750 164 798 29 39 140 28-Apr-OO 1230 160 1,500 1,500 221 589- 20 30 135 28-Apr-OO 2040 157 1,000 1,500 158 255 20 30 125 29-.A,pr-00 0908 167 1,500 2,000 7.6 0 18 . 28 125 29-Apr-OO 1646 168 1.000 1.500 20,5 497 18 28 130 29-Apr-OO 2030 168 1.500 1.500 25 636 18 28 130 30-Apr-OO 0730 158 1,250 1,600 7.6 674 18 29 125 30-Apr-OO 0950 115 700 3-000 60 66 150 30-Apr-OO 1125 95 750 1.100 67 71 185 .45 System Air Flow (SCFM) Pressure (psig) — — _ _ - — • — — — - — — — 155 — 107 - 160 — — — 160 — 160 — 160 - 160 - - — - — — - - - - - - Weather Conditions Temp, (degrees E) Wind Speed (mph) Wind Direction Humidiry (%) Bar. Pressure (inches) Air Flow at dilution valve (fpm) — — — — „ ~~ 83 5 E 72 30.1 - .. — — — ~ 87 6 E 67 30.12 - — — _ - - - 94 7 E 61 30.14 - - — — — _ - — — — — - - -_ -.. — — - - — — „ -^ - - 82 7 SE 66 30.09 - 91 10 SE 57 30.13 - 102 8 SE 61 30.11 81 1 N 69 30.1 - 85 5 NE , 71 30.14 - 95 10 E 57 30.05 - 76 2 NE 67 30.08 - 81 7 SE 65 30.08 - 94 8 E 66 30.1 97 6 SE 60 30.09 600 * - Opened dilution valve to deer, vacuum from 1.6 " Hg to 5' Hg ** - Closed dilution valve ***-Can't take-too hot g:>firojccts\003-';ol(5'igolder\SV'E TS Rcport\table.';..\ls, Table! 3 Golder Associates 304920 Table 13 Pace 1 of 1 o to September 2000 Table 14 Phase n Extended Test Results - AST Area Virgin Island Chemical Site St. Croix, U.S. Virgin Islands 003-6016 Date: Time: Flow AST-AS-1 (scfm) AST-SVE-1 (fpm) AST-SVE-2 (fpm) AST-SVE-3 (fpm) AST-SVE-4 (fpm) AST-SVE-5 (fpm) AST-SVE-6 (fpm) AST-AS-1 (fpm) Pressure Regulator (psi) Vacuum (inches H20) AST-SVE-1 AST-SVE-2 AST-SVE-3 AST-SVE-4 AST-SVE-5 AST-SVE-6 AST-VMP-11 AST-VMP-2S AST-VMP-21 AST-VMP-3S AST-VMP-31 AST-VMP-4S AST-VMP-41 27-Apr-OO 27-Apr-OO 0930 AST SVE 1 -6 Only - 550 200 175 100 30 250 - - m " Hg 0.04 ,02 ,08 3 ,08 .04 - - - - 3,5 - - 80 64 10 8 9 3,5 10 10 - - - - - 27-Apr-OO 1400 27-Apr-OO 1715 27-Apr-OO 1905 Started Extended Phase 11 Test (a>, 0940 3,4 525 400 75 50 75 225 44 34 3,6 500 200 150 25 100 200 44 34 3,9 500 250 200 25 75 250 45 34 10 5 10 3,5 12 10 4 0 >2 0 0,17 >,25- >,25 10 4 10 3 12 10 2,7 0,015 3,4 0 >,25 02 0,75 8 6 8 3 10 10 2,7 0,01 3,4 0 0,45 0,15 0,75 27-Apr-OO 2115 3.6 500 400 75 25 75 200 42 34 8 5 8 3,5 8 10 1,6 0 3.2 0 0,2 0,25 0,3 28-Apr-OO 0845 5 1000 400 100 75 125 100 42 31 8 4 8 3 10 7 1,7 0 3,2 0 0,2 0,25 0.35 28-Apr-OO 1145 3,4 750 200 100 50 150 200 33 23 6 3 6 3 8 4 2,15 0 3,35 0.015 0,2 0,15 1,2 28-Apr-OO 1715 3,4 750 1,000 300 100 300 225 33 23 6 3 6 3 6 8 1,1 0 3,4 0 0,5 0,2 0,55 28-Apr-OO 2045 3,8 - - - - ~ - 34 23 6 2 5 3 6 4 1,8 0 3,4 0 0,1 0,12 0,15 29-Apr-OO 1130 4,2 750 200 200 100 100 500 33 22 5 2 4 3 8 4 1,7 0,04 3.3 0 0,15 0,15 0,2 Pressure (inches H20) AST-SVE-2 AST-SVE-3 AST-SVE-4 AST-VMP-11 AST-VMP-ID AST-VMP-21 AST-VMP-2D AST-VMP-31 AST-VMP-3D AST-VMP-41 AST-VMP-4D - - - - - - - - - - - - - - - - - - 0,02 0,15 - 0,005 - 0,01 - - 0,02 - 0,01 - 0,005 - 0,02 - - 0.01 - 0 - 0 0,01 - - - 0 0,06 - 0 - 0 - - - 0.02 - 0,035 - 0 0,01 - - - - 0,02 - 0,01 0,04 - 0,02 - - - 0,02 - 0 0,04 - 0 - - - - 0,03 - 0,005 • - 0,06 - 0 _ - - 0,26 0,02 - 0,06 - 0.005 g:\projects\003-6016\goider\SVE TS Repon\tables,xls, TablsM Golder Associates September 2000 Table 14 Phase II Extended Test Results - AST Area Virgin Island Chemical Site St. Croix, U.S. Virgin Islands 003-6016 Date: Time: Depth to Water (feet below TIC) AST-VMP-11 AST-VMP-ID AST-VMP-2S AST-VMP-21 AST-VMP-2D AST-VMP-3S AST-VMP-31 AST-VMP-3D AST-VMP-4S AST-VMP-41 AST-VMP-4D AST-GMP-1 MW-1 MW-6 MW-8 27-Apr-OO 1410 13,93 13,95 4.32 14.33 14,01 i n 14,59 14,69 dry 14,69 14.66 14,25 15,68 17.25 19.67 27-Apr-OO 1905 13.92 14,36 4,34 14.35 14.33 dry 14,57 14,61 drv 14,69 14,82 14,97 16.08 17.3 19,12 28-Apr-OO 0850 13,95 14,48 4.33 14,41 14,55 dry 14,6 14,93 dr^' 14,69 14,94 15,19 16,2 19,4 17,36 28-Apr-OO 1145 13,9 14.84 4.34 14,41 15.25 dry 14.59 15,27 dry 14,69 15,16 15,34 16.47 17,34 19,65 28-Apr-OO 1715 13,98 14,93 4,33 14,42 14,91 drv 14.59 15.3 dry 14,7 15,3 15,26 16.68 17.24 19,85 29-Apr-OO 1130 14,02 14.94 4.34 14.45 14,88 dr>. 14,61 14,24 dr,' 14,69 15,22 15,7 17,11 17,38 19,68 29-Apr-OO 1345 15,95 15,72 4,33 14,49 15,02 dn,' - 15,29 dry 14,7 15.23 15.85 17.09 17.35 19,67 29-Apr-OO 1900 silt - no h2o 14,91 4,34 14,48 15,04 dry 14,59 15,53 dry 14.69 15.34 15,33 16,81 17.38 19,84 30-Apr-OO 0820 14,5 15 4,31 14,51 15,04 dry 14.57 15.31 drv 14,69 15,27 15,28 16,74 17,41 19,84 30-Apr-OO 0959 30-Apr-OO 1135 Post-packer pulling 13.9 15,05 4,3 14,5 15,01 dry 14.58 15,33 dry 14,69 15,32 15.36 16,82 17,41 19,79 Dissolved Oxvgen (mg/L) AST-VMP-I I AST-VMP-ID AST-VMP-21 AST-VMP-2D AST-VMP-31 AST-VMP-3 D AST-VMP-41 AST-VMP-4D MW-1 MW-6 MW-8 - 0,87 - 14,02 - 0,78 0,51 13,07 6,32 ,59 - 2.36 - 3.87 0,67 - 0.76 13.57 7,11 ,79 5.83 0.59 0,89 13,06 12.18 7,66 1,31 9.66 12,98 0,81 0,95 12.06 7,33 0.87 6,62 13,27 0,76 0,63 12,23 7,15 ,73 13,1 14,31 0,97 0,91 14,65 9.28 1,47 10,89 14,57 0,81 0,71 12.81 8,1 0,82 12,09 14,65 0,57 , 0.77 7.3 7,05 7,19 8,18 9,91 0,48 0,33 9,16 6,28 0,32 to o vo to to g:\projects\003-6016\golder\SVE TS Repon\lables,xls, TableH Golder Associates September 2000 Table 14 P h a s e II Extended Test Results - A S T A r e a Virgin Island Chemical Site St. Croix, U.S. Virgin Islands 003-6016 Date: Time: 27-Apr-OO 1710 27-Apr-OO 1905 28-Apr-OO 0850 2S-Apr-00 1145 28-Apr-OO 1715 29-Apr-OO 1130 29-Apr-OO 1345 29-Apr-OO 1900 30-Apr-OO 0820 30-Apr-OO 0959 30-Apr-OO 1135 o U3 lO CO OVM Readings (ppmv) AST-SVE-1 AST-SVE-2 AST-SVE-3 AST-SVE-4 AST-SVE-5 AST-SVE-6 AST-VMP-11 AST-VMP-ID AST-VMP-2S AST-VMP-21 AST-VMP-2D AST-VMP-3S AST-VMP-31 AST-VMP-3D AST-VMP-4S AST-VMP-41 AST-VMP-4D MW-1 MW-6 - - 3.1 - 22.7 55.2 - 2,1 0 0 - - • - - - - - - - - - - - - 17,7 21,3 3,2 2,2 0 18,3 14,2 3,6 2,1 0 20 65 20,6 14,9 1,5 0 0 636 43,2 3,5 1,1 1,2 26 18 1,2 ,4 ,2 19 16 113 2 2 3 DTW (ft): 14,39 14,54 15,39 15,49 17.88 17,34 g:\projecls\003-6016\golder\SVE TS Report\lables,!<ls, Tablel4 Golder Associates September 2000 Table 15 Phase II Extended Test Results - FPP Area Virgin Island Chemical Site St. Croix, U.S. Virgin Islands 003-6016 * - Was beling bailed; magnahelic was not in place Date: Time: 27-Apr-OO 1335 27-Apr-OO 1840 28-Apr-OO 0800 28-Apr-OO 1915 29-Apr-OO 1105 29-Apr-OO 1900 30-Apr-OO 1415 30-Apr-OO 1745 Depth to Water (feet below TIC) FPP-VMP-11 FPP-VMP-ID FPP-VMP-2S FPP-VMP-21 FPP-VMP-2D FPP-VMP-3S FPP-VMP-31 FPP-VMP-3D FPP-VMP-4S FPP-VMP-41 FPP-VMP-4D FPP-GMP-l MW-2 MW-3 MW-7 14,98 15,1 4,3 14,62 0.35 4,72 dry 12,68 4,84 14,8 15,34 16,02 15.84 18,19 20,08 15,35 15.01 4,39 14,19 1,29 4.73 dry 14.07 4.83 14.77 16.17 16,06 - - - 15,02 15,64 4,48 14.76 1.41 4,74 dry 15,45 4,85 14,8 16,85 16,08 15,85 13.26 18,93 15,68 15.01 4.5 14,75 1.5 4,69 dry 15,21 3,65 14,73 16.5 16,06 15,81 18,23 20,55 15 15.72 4.5 14,66 1,6 4,76 dry 14,81 4,82 14.8 17,3 16,04 15,38 18,21 20,67 15,01 15,87 4,5 14,72 12,97 4,72 dry 14,88 4,84 14,76 17,5 16,08 16,21 18,25 20,91 15,01 15,9 2.35 14.47 15.02 4,71 dry 14.81 4.8 14,73 17,69 16.08 15.62 18.25 21.18 15,01 16,21 2,31 14.8 16,47 4,73 dry 17,18 4.82 14.72 18,85 16,06 17,44 18,3 21.6 Date: Time: Flow FPP-AS-1 (scfm) FPP-SVE-1 (fpm) 27-Apr-OO 0750 FPP-SVE-1 Only - 1,250 27-Apr-OO 0930 7 • - 27-Apr-OO 1325 27-Apr-OO 1710 27-Apr-OO 1830 Started Extended Phase 11 Test (3,0940 7 2,500 7,2 125 7 150 27-Apr-OO 2100 7 100 28-Apr-OO 0745 7 200 28-Apr-OO 1856 7,1 200 29-Apr-OO 1100 7.3 150 29-Apr-OO 1855 7,4 150 30-Apr-OO 1410 6,8 1 6,000 Vacuum (inches H20) FPP-SVE-1 FPP-VMP-11 FPP-VMP-2S FPP-VMP-21 FPP-VMP-3S FPP-VMP-31 FPP-VMP-4S FPP-VMP-41 6.6" Hg - - ~ - ~ - - 12 - - - - - - - 0.15 - 0,01 - 0.03 ~ 0,03 - 12 - 0,01 - 0,01 - 0,01 - 10 - 0.05 - 0 - 0 - 8 - - - - - 10 - 0.01 - 0,005 - 0.02 - 6 0 - 0 ~ 0,02 6 - 0.01 - 0.02 - 0.03 - 7 - 0.005 - 0,02 - 0,03 - 5,2 - 0 - 0,005 - 0.02 - Pressure (inches H20) FPP-AS-1 (psi) FPP-VMP-11 FPP-VMP-ID FPP-VMP-21 FPP-VMP-2D FPP-VMP-3! FPP-VMP-3D FPP-VMP-41 FPP-VMP-4D Pressure Regulator (psi) - - - - - ~ - - - ~ 54 - - - - - - - - 100 29 0.025 0,05 0,04 <0 0,03 0,01 <0 0,15 - 27 0,03 0,02 0,03 <0 0,01 0,01 <0 0.05 100 26 0.02 0.02 0.02 0 0.01 0 0 0.01 100 26 - - ~ - - - ~ - 100 23 0,01 0.015 0,04 0,005 0,04 0,01 ~ 0.02 100 20 0 0.01 0 0 0.05 >.25 0 0,035 100 20 0,01 0.04 0,02 0,02 0,14 0.04 0.02 NA* 100 18 0.03 0,05 0,025 >,25 0.095 >,25 0 0.195 100 - 0,02 0,1 0.22 >.25 0.17 >,25 0,08 >.25 115 O to g:\projecls\003-6016\goider\SVE TS Repon\lables,xis, Table 15 Golder Associates Page 1 of2 September 2000 Table 15 Phase II Extended Test Results - FPP Area Virgin Island Chemical Site St. Croix, U.S. Virgin Islands 003-6016 Date: Titns: 27-Apr-OO 1335 27-Apr-OO \840 28-Apr-OO 0800 28-Apr-OO )915 29-Apr-OO 1105 29-Apr-OO 1900 30-Apr-OO 1415 30-Apr-OO J 745 Dissolved Oxygen (mg/L) FPP-VMP-11 FPP-VMP-ID FPP-VMP-21 FPP-VMP-2D FPP-VMP-31 FPP-VMP-3D FPP-VMP-41 FPP-VMP-4D MW-2 MW-3 MW-7 - 11,46 - 12,7 - 14.27 - 11.31 14,73 ~ 4,74 - 13,41 - 12,05 - 14,17 - 11.74 14.1 - 9.14 - 12.83 - 9.06 - 13,68 - 10,86 13.15 .87 8.29 - 12.47 ~ 8,22 - 13.46 - 9.14 12,76 - 8.09 - 14.49 - 9,03 L 15,41 ~ 13,13 14.91 .92 9.15 - 14,67 14,12 ~ 13.63 - NA*» 15.32 ,81 9.55 ~ 9,57 ~ 9.58 - 10.35 - 9.35 9.89 0,92 6,15 - - - - - - - - - - - OVM Readings (ppmv) if>0,l" H2O FPP-SVE-1 FPP-VMP-11 FPP-VMP-ID FPP-VMP-2S FPP-VMP-21 FPP-VMP-2D FPP-VMP-3 S FPP-VMP-31 FPP-VMP-3D FPP-VMP-4S FPP-VMP-41 FPP-VMP-4D - 3,1 7 3 0 2 0 0 0 0 0 0 - - - ~ - - - - - - ~ - - - - - - - - - - - - ~ ~ - - - - - - ~ - - - - - - 0 - - - - - - - - - 1 - - ,8 - - 1,2 - - - - .8 1.1 - ,1 ,5 - - ,5 - - - - - - - - - - - - to o vo ISJ U1 - Not Measured g:\projecls\003-6016\golder\SVETS Repon\lables,xls, Tablets Golder Associates September 2000 Table 16 Phase II Extended Test Soil-Gas Laboratory Analytical Data Virgin Island Chemical Site St. Croix, U.S. Virgin Islands 003-6016 Client ID: Testing Period/Time: Lab ID Date Sampled: Matrix: AST-SVE-4-Ext#l 1615 B27 232 27-Apr-OO Soil-Gas FPP-SVE-1-Ext #1 1610 B27 233 27-Apr-OO Soil-Gas AST-VMP-ll-Ext#l 1620 B27 234 27-Apr-OO Soil-Gas FPP-SVE-1 #2 1610 827 240 28-Apr-OO Soil-Gas AST-SVE-5 #1 1615 827241 28-Apr-OO Soil-Gas FPP-SVE-I #3 1655 B27 248 29-Apr-OO Soil-Gas AST-SVE-2 2050 827 252 •29-Apr-OO Soil-Gas AST-VMP-2I(PosO 1030 827256 30-Apr-OO Soil-Gas AST-VMP-41(Post) 1040 B27 257 30-Apr-OO Soil-Gas AST-VMP-3(Post) 1050 827 258 30-Apr-OO Soil-Gas Site Target Compounds (ppmv) Acetone Chloroform Ethylbenzene Methylene chloride Toluene m&p-Xylene o-Xylene <2 <0,005 <0,07 <2 0.2 <0,07 <0.07 <2 0.977 <0.07 <2 0.19 <0.07 <0,07 <2 <0.005 0.09 <2 0,18 0.37 <0.07 <2 0.635 <0.07 <2 0.18 <0.07 <0.07 <2 <0.005 <0.07 <2 0.33 0.17 0,36 <2 0.014 <0.07 <2 O.I <0.07 <0.07 <2 0.005 150.07 <2 4.96 669.52 73,3 <2 <0.005 0,99 <2 0.83 1.55 0,33 <2 <0.005 <0.07 <2 0.27 <0.07 <0,07 <2 <0.005 <0.07 <2 0.24 <0.07 <0.07 Cliem ID: Testing Period/Time: Lab ID Date Sampled: Matrix: FPP-SVE-1 #4 1530 B27 259 30-Apr-OO Soil-Gas FPP-SVE-1 (Post) 1715 B27 266 30-Apr-OO Soil-Gas FPP-VMP-ll(PosO 1703 - B27 267 30-Apr-OO Soil-Gas PP-VMP-lD(Pos lFPP-VMP-2S(Posf 1850 827 268 30-Apr-OO Soil-Gas 1650 B27 269 30-Apr-OO Soil-Gas FPP-VMP-2l(Post) 1652 B27 270 30-Apr-OO Soil-Gas P-VMP-2D(Po 1655 827271 30-Apr-OO Soil-Gas FPP-VMP-3S(PosO 1657 B27 272 30-Apr-OO Soil-Gas FPP-VMP-31(Post) 1658 827 273 30-Apr-OO Soil-Gas FPP-VMP-3D(PosO 1700 827 274 30-Apr-OO Soil-Gas FPP-VMP-4S(Post) 1702 827 275 30-Apr-OO Soil-Gas FPP-VMP-4I(PosO 1704 827 276 30-Apr-OO Soil-Gas FPP-VMP^D(Post) 1848 B27 277 30-Apr-OO Soil-Gas Site Target Compounds (ppmv) Acetone Chlorofonn Ethylbenzene Methylene chloride Toluene m&p-Xylene o-Xylene <2 <0,005 <0.07 <2 0.23 <0.07 <0,07 <2 0.016 <0.07 <2 0,37 <0,07 <0,07 <2 39.52 <0,07 <2 0.22 <0,07 <0.07 <2 0.028 <0.07 <2 0,16 <0.07 <0.07 <2 0.011 <0,07 <2 0.31 <0,07 <0,07 <2 44.295 <0,07 <2 0.35 <0.07 <0.07 <2 <0.005 <0.07 <2 0,26 <0.07 <0,07 <2 0.186 <0.07 <2 0.14 <0.07 <0.07 <2 42.284 <0,07 <2 0,19 <0.07 <0.07 <2 0.026 <0,07 <2 0.42 <0.07 <0,07 <2 1.613 <0.07 <2 0.25 <0.07 ; <0,07 ' <2 14.214 <0,07 <2 0,17 <0.07 <0,07 <2 0.414 <0.07 <2 0,27 0,27 <0,07 Client ID: Testing Period/Time: Lab ID Date Sampled: Matrix: Intake-Ext, tt 1 1503 B27 229 27-Apr-OO Soil-Gas Intake #2 1600 B27 238 28-Apr-OO Soil-Gas Intake ff3 2040 B27 249 29-Apr-OO Soil-Gas Intake #4 0758 827 253 30-Apr-OO Soil-Gas Site Target Compounds (ppmv) Acetone Chlorolbrm Ethylbenzene Methylene chloride Toluene m&p-Xylene o-Xylenc <2 0,033 132.22 <2 7,14 576,54 62,58 <2 0,084 107,17 <2 6.09 489.89 55.3 <2 0.19 41,27 <2 3,47 157.94 19,85 <2 0.245 26.62 <2 3.07 95.54 11.33 Client ID: Testing Period/Time: Lab ID Date Sampled: Matrix: Exhaust-Ext. #1 1500 827 230 27-Apr-OO Soil-Gas Exhaust-Ext #2 1900 827 235 27-Apr-OO Soil-Gas Exhaust #3 1035 B27 236 28-Apr-OO Soil-Gas Exhaust #4 1600 827 237 28-Apr-OO Soil-Gas Exhatist #5 1212 827 247 29-Apr-OO Soil-Gas Exhaust #6 2045 B27 2.50 29-Apr-OO Soil-Gas Exhaust #7 0800 827 255 30-Apr-OO Soil-Gas Exhaust #8 1505 827 265 30-Apr-OO Soil-Gas Site Target Compounds (ppmv) Acetone Chloroform Ethylbenzene Methylene chloride Toluene ni&p-Xylene o-Xylene <2 0,027 100,66 <2 5.5 456.89 50.78 <2 0,024 68.09 <2 4.53 290.58 33,55 <2 0.159 132.72 <2 7,15 590,42 65,34 <2 0,032 24,85 <2 1.96 100.67 12.32 <2 0.096 37.98 <2 2.75 152.72 19.51 <2 0.125 37.62 <2 2.66 151,34 19.36 <2 0.177 21.8 <2 2.37 79.47 9.33 <2 0.105 <0.07 <2 0.32 0,16 <0.07 Client ID: Testing Period/Time: Lab ID Date Sampled: Matrix: Dovvngrad-Ext. H1 1505 827 231 27-Apr-OO Soil-Gas Downgrad #2 1605 B27 239 28-Apr-OO Soil-Gas Downgrad #3 2047 B27 25I 29-Apr-OO Soil-Gas Downgrad #4 0805 B27 254 30-Apr-OO Soil-Gas Site Target Compounds (ppmv) Acetone Chloroform Ethylbenzene Methylene chloride Toluene m&p-Xylene o-Xylene <2 <0,005 <0,07 <2 0,2 <0,07 <0,07 <2 <0.005 <0.07 <2 0.27 0,08 <0.07 <2 <0,005 <0,07 <2 0.3 <0.07 <007 <2 <0,005 <0,07 <2 0.24 <0,07 <0.07 g:\projects\OOj-fiOlfAgolderVSVETS ReportMablcsxIs.Tablel 6 Golder Associates 304926 Table 16 September 2000 Table 17 Phase n Extended Test Soil Gas Field Analytical Data Virgin Islands Chemical Site St. Croix, U.S. Virgin Islands 003-6016 Sample ID Lab ID Date Collected Time Collected Matrix MBO1-427 MBOI- 427,gc 4/27/00 soil-gas MB02-427 MB02- 427.gc 4/27/00 soil-gas Intake #1 427-00 l.gc 4/27/00 8:10 soil-gas MB03-427 MB03- 427.gc 4/27/00 soil-gas Exhaust # 1 417-002.gc 4/27/00 8:10 soil-gas MB04-427 MB04- 427.gc 4/27/00 soil-gas Intake #2 427-003.gc 4/27/00 12:44 soil-gas MB05-427 MB05- 427.gc 4/27/00 soil-gas Exhaust #2 427-004,gc 4/27/00 12:44 soil-gas MB06-427 MB06- 427.gc 4/27/00 , soil-gas Exhaust #2 417-005.gc 4/27/00 12:44 (50x dil) soil-gas MB07-427 MB07- 427.gc 4/27/00 soil-gas VOCs (ppm) 1 Toluene Ethylbenzene m,p-Xylene o-Xylene 0.01238 0.02626 ND ND 0.01301 0.03784 0.01994 ND 7.375 3.032 443.1 105 0.01417 0,2268 0,5945 0.1067 8.799 3.289 452.5 119.2 0.02178 0.07431 0.5200 0.2593 0.09927 0.1328 1.002 0.3355 0.009451 0.0156 0.04384 ND 4,317 3,255 580,8 197,3 0.01587 0.577 0.001657 0.001108 0.2777 4.305 13.05 4.983 ND 0.01834 0.03996 ND Sample ID Lab ID Date Collected Time Collected liVIatrix AST-SVE- 1 427-006.gc 4/27/00 16:20 soil-gas MB08-427 MB08- 427.gc 4/27/00 soil-gas AST-SVE- 1 427-007.gc 4/27/00 16:20 (4x dil) soil-gas MB09-427 MB09- 427,gc 4/27/00 soil-gas AST-SVE- 2 427-008,gc 4/27/00 16:25 soil-gas MBlO-427 MBIO- 427,gc 4/27/00 soil-gas AST-SVE- 2 427-009.gc :25 (50x d soil-gas MB 11-427 MBIl- 427.gc 4/27/00 soil-gas MBOl-428 MBOl- 428.gc 4/28/00 soil-gas MB02-428 MB02- 428.gc 4/28/00 soil-gas AST-SVE- 3 428-00 l.gc 4/27/00 16:30 soil-gas MB03-428 MB03- 428,gc 4/28/00 soil-gas AST-SVE- 3 428-002,gc 4/27/00 16:30 (2xdil) soil-gas MB04-428 MB04- 428.gc 4/28/00 soil-gas AST-SVE- 3 428-003.gc 4/27/00 16:30 (lOxdil) soil-gas MB05-428 MB05- 428,gc 4/28/00 soil-gas AST-SVE- 4 428-004.gc 4/27/00 16:35 soil-gas MB06-428 MB06- 428,gc 4/28/00 soil-gas AST-SVE- 4'. 428-005.gc 4/27/00 16:35 (4x dil) soil-gas MB07-428 MB07- 428.gc 4/28/00 soil-gas AST-SVE- 5 428-006.gc 4/27/00 16:38 soil-gas MB08-428 MB08- 428.gc 4/28/00 soil-gas AST-SVE- 6 428-007.gc 4/27/00 16:40 soil-gas MB09-428 MB09- 428.gc 4/28/00 soil-gas Intake #3 428-008.gc 4/27/00 20:00 soil-gas 1 'VOCs (ppm) Toluene Ethylbenzene m.p-Xylene o-Xylene 0.6723 1.339 3,836 1,642 0.1786 0.1528 0.2603 0,356 0,05809 0,1541 1,223 0,6564 0,01201 0,01072 0,03165 ND 4,616 ND 827,5 535,3 0.03085 0.009051 0.0294 0.01116 0.08215 18.13 49,55 17.29 0.009488 0.20250 0.00179 0.002699 0.003917 0.0123 0.02332 0.07909 0.008286 ND 0.01987 0.01693 0.05402 2.046 13,36 2.804 ND 0.7534 0,2343 0.02136 0.02276 0.9711 5,179 2.112 ND 0.3726 0.2366 0.02817 0.01289 1.151 1.904 0.5877 0.009082 0.03539 0,1035 0.09937 0.03507 1,054 6.131 1.243 0,008872 0,1346 0.07001 •ND 0.01393 0.7534 1.506 0.3774 0.007695 0,06243 0.04634 ND 0.06481 0.8182 1.712 0.5112 0.007988 0.02588 0.02807 ND 0.02269 1.099 1.687 0.8515 ND 0.02691 0.03194 ND 0.1482 5.353 14.61 1.866 Sample ID Lab ID Date Collected Time Collected Matrix MB 10-428 MBIO- 428.gc 4/28/00 soil-gas Intake #3 428-009.gc 4/27/00 20:00 (4x dil) soil-gas MB 11-428 M B l l - 428.gc 4/28/00 soil-gas Intake #3 428-0 lO.gc 4/27/00 20:00 (lOxdil) soil-gas MB12-428 MB12- 428.gc 4/28/00 soil-gas Exhaust #3 428-01 l.gc 4/27/00 20:05 soil-gas iMB 13-428 MB13- 428.gc 4/28/00 soil-gas Exhaust tt-2 428-012.gc 4/27/00 20:05 (lOxdil) soil-gas MB 14-428 MBI4- 428.gc 4/28/00 soil-gas Exhaust #3 428-013.gc 4/27/00 20:05 (50x dil) soil-sas MBI5-428 MBI5- 428.gc 4/28/00 soil-gas Intake M 428-014.gc 4/28/00 9:30 soil-gas MB 16-428 MB16- 428.gc 4/28/00 soil-gas Intake #4 428-015.gc 4/28/00 9:30 (20x dil) soil-gas MB 17-428 MB17- 428.gc 4/28/00 soil-gas Intake #4 428-016.gc 4/28/00 9:30 (50x dil) soil-gas MB 18-428 MBI8- 428.gc 4/28/00 soil-gas Exhaust #4 428-017,gc 4/28/00 9:30 (IOx dil) soil-gas MB 19-428 MBI9- 428,gc 4/28/00 soil-gas Exhaust #4 428-018.gc 4/28/00 9:30 (50x dil) soil-gas MB20-428 MB20- 428,gc 4/28/00 soil-gas Exhaust #5 428-019,gc 4/28/00 12:20 (lOxdil) soil-gas MB21-428 MB2I- 428.gc 4/28/00 soil-gas Exhaust #5 428-020.gc 4/28/00 12:20 (50x dil) soil-gas MB22-428 MB22- 428.gc 4/28/00 soil-gas VOCs (ppm) Toluene Ethylbenzene m,p-Xylene o-Xylene 0,01156 0,08574 0.1852 0.01934 0.05472 1.426 3.476 0.5239 0.02261 0.02135 0.04677 ND 0.02565 0.3063 1.781 0.3133 0.009074 0.01682 0.03077 ND 6.951 2.653 451.9 43.42 0.07601 3.407 7.637 0.910 0,9053 33.58 72.68 7.287 0.01070 0.06794 0.1408 ND 0.0806 3.406 7.785 0.8796 0.01283 0.01917 0.03544 ND 0,9877 26.02 46.09 4.495 0.009074 0.01682 0.03077 ND 0.2315 7,836 18,34 1,918, 0,008031 ND 0,01448 ND 0,04745 0,2695 1,206 0.2255 ND ND 0,009371 ND 0,1185 13.21 31.45 3.443 ND 0.01320 0.00349 ND 0.05318 2.982 7.437 1.258 ND ND 20.61 ND 0.4294 12.17 31.99 5.135 ND 0.01353 0.03312 ND 0.05272 2,07 4,802 0,8668 ND ND 0,02006 ND g:\proiects\003-6016\SVE TS Repon\tablcs,xls, Tabid 7 Golder Associates 304927 Table 17 Paee 1 of 3 304928 September 2000 Table 17 Phase II Extended Test Soil Gas Field Analytical Data Virgin Islands Chemical Site St. Croix, U.S. Virgin Islands 003-6016 Sample ID Lab ID Date Collected Time Collected Matrix Exhaust #6 428-02 l.gc 4/28/00 16:05 (lOxdil) soil-gas MB23-428 MB23- 428.gc 4/28/00 soil-gas Exhaust #6 428-022.gc 4/28/00 16:05 (50x dil) soil-gas MB24-428 MB24- 428.gc 4/28/00 soil-gas Exhaust #7 428-023,gc 4/28/00 20:40 (lOxdil) soil-gas MB25-428 MB25- 428,gc 4/28/00 soil-gas Exhaust #7 428-024.gc 4/28/00 20:40 (50x dil) soil-gas MB26-428 MB26- 428.gc 4/28/00 soil-gas MBOI-429 MBOl- 429.gc 4/29/00 soil-gas Exhaust #8 429-00 l.gc 4/29/00 9:08 (lOxdil) soil-gas MB02-429 MB02- 429.gc 4/29/00 soil-gas Exhaust #8 429-002.gc 4/29/00 9:08 (50x dil) soil-gas MB03-429 MB03- 429.gc 4/29/00 soil-gas Exhaust #9 429-003.gc 4/29/00 12:12 (lOxdil) soil-gas MB04-429 MB04- 429.gc 4/29/00 soil-gas Exhaust #9 429- 004a.gc 4/29/00 12:12 (50x dil) soil-gas MBOl-430 MBOl- 430.gc 4/30/00 soil-gas AST-VMP 11 430-00 l.gc 4/27/00 16:42 soil-gas MB02-430 MB02- 430.gc 4/30/00 soil-gas AST-VMP 21 430-002.gc 4/27/00 16:50 soil-gas MB03-430 MB03- 430.gc 4/30/00 soil-gas AST-VMP 31 430-003.gc 4/27/00 16:55 soil-gas MB04-430 MB04- 430.gc 4/30/00 soil-gas AST-VMP 48 430-004.gc 4/27/00 17:00 soil-gas MB05-430 MB05- 430.gc 4/30/00 soil-gas VOCs (ppm) Toluene Ethylbenzene m,p-Xylene o-Xylene 0.2861 11.48 29.9 4.285 ND 0,02396 0,04832 ND 0,05718 2,321 5.388 0.9411 ND ND 0.02059 ND 0.2744 11,13 29,82 4.523 ND 0.0303 0.05234 ND 0.04312 2.113 5,043 0,9054 NS NS NS NS ND ND 0,0291 ND 0,6525 29.69 28.39 8.273 ND 0,1876 0,1453 0.03376 0.1084 1.76 3.368 1.05 ND 0.03758 0.02845 0,001701 0,7108 34,03 30,61 7.314 ND 0.07087 0.05085 ND 0.1208 2.122 4.055 4,462 ND 0.02688 0.01612 ND 0.1255 1.021 0.8243 0.7534 ND 0.02188 0.01532 ND 0.1242 0.2533 0.5108 0,4869 ND ND 0,01463 ND ND 0.09183 0.2249 0.2625 ND ND 0.01337 ND ND 0.0688 0.1757 0.1963 ND ND 0.01347 ND Sample ID Lab ID Date Collected Time Collected Matrix AST-VMP 41 430-005.gc 4/27/00 16:58 soil-gas MB06-430 MB06- 430.gc 4/30/00 soil-gas AST-SVE- • l - # 2 430-006.gc 4/28/00 10:45 soil-gas MB07-430 MB07- 430.gc 4/30/00 soil-gas AST-SVE- l-#2 430-007.gc 4/28/00 10:45 (2x dil) soil-gas MB08-430 MB08- 430.gc 4/30/00 soil-gas AST-SVE- 2-#2 430-008.gc 4/28/00 10:48 soil-gas MB09-430 MB09- 430.gc 4/30/00 soil-gas AST-SVE- 2-#2 430-009.gc 4/28/00 10:48 (50x dil) soil-gas MB 10-430 MBIO- 430.gc 4/30/00 soil-gas AST-SVE- 3-#2 430-0 lO.gc 4/28/00 10:50 soil-gas MB 11-430 MBIl- 430,gc 4/30/00 soil-gas AST-SVE- 3-#2 430-011,gc 4/28/00 10:50 soil-gas MB 12-430 MB12- 430.gc 4/30/00 soil-gas AST-SVE- 4-#2 430-012.gc 4/28/00 10:53 soil-gas MB 13-430 MB13- 430.gc 4/30/00 soil-gas AST-SVE- 4-#2 430-013.gc 4/28/00 10:53 (2xdil) soil-gas MB 14-430 MB14- 430.gc 4/30/00 soil-gas AST-SVE- 5-#2. 430-014.gc 4/28/00 10:58 soii-gas ^ MB 15-430 MB15- 430.gc 4/30/00 soil-gas AST-SVE- 5-#2 430-015.gc 4/28/00 10:58 (2x dil) soil-gas MB 16-430 MB16- 430.gc 4/30/00 soil-gas AST-SVE- 6-#2 • 430-016.gc 4/28/00 11:00 soil-gas MB 17-430 MB17- 430.gc 4/30/00 soil-gas AST-SVE- l-#3 430-017,gc 4/28/00 16:35 (2x dil) soil-gas j VOCs (ppm) Toluene Ethylbenzene m,p-Xylene ,0-Xvlene 0.05051 O.I 339 0.3212 0.3101 ND ND 0,01402 ND 0.5078 2.266 2,186 1.517 ND 0.03435 0.1028 0.1185 0.2943 1.299 1.199 0.9075 ND ND 0.01384 ND 18.88 12.14 396,8 507.5 0.04692 9,116 9,135 6.132 0.2294 15.27 13.85 8.533 ND 0.1406 0.1250 0.1000 0.07557 6.511 6.339 4.078 ND 0.3603 0.2815 0.1868 0.02889 1,793 1.753 1.568 ND 0.09361 0.08567 0,06843 0.1601 2.301 2.005 1.574 ND 0.09724 0.08885 0.06295 0.1 0.6059 1.227 0.9899 ND 0,1127 0.1008 0,06364 0,1899 2,116 1,662 1,92 ND 0.1294 0,1152 0.1033 0,1071 1,195 0.9286 1,14 ND 0.2874 0.2046 0,2092 0.1723 1.467 0.9649 1.991 ND 0.1029 0.08412 0.09403 0.1496 0,3048 0.6725 0.5597 Sample ID Lab ID Date Collected Time Collected Matrix MB 18-430 MBI8- 430.gc 4/30/00 soil-gas AST-SVE- 2-#3 430-018,gc 4/28/00 16:42 (50x dil) soil-gas MB 19-430 MBI9- 430,gc 4/30/00 soil-gas AST-SVE 3-#3 430-019.gc 4/28/00 16:43 (4x dil) soil-gas MB20-430 MB20- 430.gc 4/30/00 soil-gas AST-SVE- 3-#3 430-020,gc 4/28/00 16:43 (lOxdil) soil-gas MB2I-430 MB21- 430,gc 4/30/00 soil-gas AST-SVE- 4-#3 430-02 l,gc 4/28/00 16:50 (2x dil) soil-gas MB22-430 MB22- 430,gc 4/30/00 soil-gas AST-SVE 5-#3 430-022.gc 4/28/00 16:52 (2x dil) soil-gas MB23-430 MB23- 430.gc 4/30/00 soil-gas AST-SVE- 6-#3 430-023.gc 4/28/00 16:54 soil-gas MB24-430 MB24- 430.gc 4/30/00 soil-gas AST-SVE- I-#2D 430-024 4/28/00 10:45 (2x dil) soil-gas MB25-430 MB25- 430.gc 4/30/00 soil-gas AST-SVE- 6-#3D 430-025.gc 4/28/00 16:54 soil-gas MB26-430 MB26- 430.gc 4/30/00 soil-gas AST-SVE- l-#4 460-026.gc 4/29/00 12:26 (2x dil) soil-gas MB27-430 iMB27- 430:gc 4/30/00 soil-gas AST-SVE- I-#4 430-027.gc 4/29/00 12:26 soil-gas MB28-430 MB2S- 430.gc 4/30/00 soil-gas AST-SVE- 2-#4 430-028.gc 4/29/00 12:29 (50x dil) soil-gas MB29-430 MB29- 430.gc 4/30/00 soil-gas AST-SVE- 3-#4 430-029.gc 4/29/00 12:32 (4x dil) soil-gas MB30-430 MB30- 430.gc 4/30/00 soil-gas VOCs (ppm) Toluene Ethylbenzene m,p-Xylene o-Xylene ND 0.04401 0.03561 ND 0.2077 14.23 12,63 7.276 ND 0.06832 0.05132 0.03422 0.1306 4.064 3.507 2.643 ND 0.04049 0.02935 ND 0,05306 1,701 1.489 1.229 ND 0.03676 0.02611 ND 0.0189 0.711 1.555 1.275 ND 0.06947 0.06210 0.04240 0.0202 1.158 0.9507 1.114 ND 0.07188 0.06720 0.07518 0.226 1.472 0.9684 2.014 ND 0.03643 0,02805 ND 0,2955 0.5117 1.167 0.842 ND 0.07013 0,06637 0.04226 0.2291 1,377 0.9667 2.263 ND 0,02808 0,02348 0,03453 0.01497 0.1541 0.3755 0,4291 ND 0,02071 0,01706 ND 0,02827 0.2949 0.7053 0.6715 ND 0.03342 0.02858 ND 0.2286 14.31 12.74 7.89 ND 0.03131 0.01873 ND 0.03749 1.418 2.482 1.969 ND 0.1004 0.08507 0.05118 ^ T < Sample ID Lab ID Date Collected Time Collected Matrix AST-SVE- 3-#4 430-030.gc 4/29/00 12:32 (lOxdil) soil-gas MB31-430 MB3I- 430.gc 4/30/00 soil-gas AST-SVE- 4-#4 430-03 l.gc 4/29/00 12:38 (2x dil) soil-gas MB32-430 MB32- 430,gc 4/30/00 soil-gas AST-SVE- 5-#4 430-032,gc 4/29/00 12:44 (2x dil) soil-gas MB33-430 MB33- 430,gc 4/30/00 soil-gas AST-SVE- 6-#4 430-033.gc 4/29/00 12:42 soil-gas MB34-430 MB34- 430.gc 4/30/00 soil-gas AST-SVE- 4-#4D • 430-034.gc 4/29/00 12:38 (2x dil) soil-gas MB35-430 MB35- 430.gc 4/30/00 soil-gas MB01-5dl MBOl- 50 l.gc 5/1/00 soil-gas AST-SVE- l-#5 501-00 l.gc 4/29/00 19:49 soil-gas MB02-501 MB02- 50 l.gc 5/1/00 soil-gas AST-SVE- 2-#5 50]-002.gc 4/29/00 19:54 (50x dil) soil-gas MB03-501 MB03- 50 l.gc 5/1/00 soil-gas AST-SVE- 2-#5D 501-003.gc 4/29/00 19:54 (50x dil) soil-gas MB04-501 MB04- SOI.gc 5/1/00 soil-gas AST-SVE- 2-#5T 50l-004.gc 4/29/00 19:54 (50x dil) soil-gas MB05-501 MB05- 501,gc 5/1/00 soil-gas AST-SVE- 3-*5- 501-005.gc 4/29/00 19:58 (4x dil) soil-gas MB06-501 MB06- 501,gc 5/1/00 soil-gas AST-SVE- 3-#5 50l-006,gc 4/29/00 19:58 (lOx dil) soil-gas MB07-501 MB07- 50 l.gc 5/1/00 soil-gas AST-SVE- 4-#5 501-007.gc 4/29/00 20:01 (2x dil) soil-gas MB08-501 MB08- 501.gc 5/1/00 soil-gas OCs (ppm) Toluene Ethylbenzene m.p-Xylene o-Xylene 0.01717 0.565 1.139 0.9468 ND 0.02462 0.01814 ND 0.04607 0,6537 1,259 0.9553 ND 0.02690 0.02065 ND 0.2127 0,758 0,5482 0,5971 ND ND 0.01177 ND 0,4943 1,786 1.126 2.047 ND 0.04811 0.03284 ND 0.0188 1.315 1,047 0.7905 ND 0.06072 0.05184 ND ND 0.02518 0.04333 ND 0,01029 0.1452 0.9157 0.6016 ND ND 0.02898 ND 903,7 16.86 43.83 16.85 ND 0.2428 0.5265 0.1510 0.07131 7.103 18.44 5.621 ND 0.09014 0.2038 ND 0.1017 9,356 23.73 5.88 ND 0.09531 0.1916 ND 0.02577 3.102 7.324 2.823 ND 0.0710 0.1814 0.1473 0.02797 0.6059 3.351 1.504 ND 0.03001 0.06246 ND 0.0312 2.077 5.521 2.211 ND 0.02990 0.06927 ND g:\project.';\003-60l6\SVE TS Repon\table5,xls, Tablel? Golder Associates Table 17 Paae 2 of 3 September 2000 Table 17 Phase II Extended Test Soil Gas Field Analytical Data Virgin Islands Chemical Site St. Croix, U.S. Virgin Islands 003-6016 Sample ID Lab ID Date Collected Time Collected Matrix AST-SVE- 4-#5 501-008.gc 4/29/00 20:01 (Sxdil) soil-gas MB09-501 MB09- 50 l.gc 5/1/00 soil-gas AST-SVE- 5-#5 501-009.gc 4/29/00 20:05 (2x dil) soil-gas MB 10-501 MBIO- 501.gc 5/1/00 soil-gas AST-SVE- 6-#5 501-OlO.gc 4/29/00 20:07 soil-gas MBl 1-501 MBII- 501.gc 5/1/00 soil-gas AST-SVE- 6-#5 501-01 l.gc 4/29/00 20:07 (4x dil) soil-gas MB12-501 MBI2- 501.gc 5/1/00 soil-gas Exhaust #11 501-012.gc 4/30/00 7:30 (50x dil) soil-gas MB13-50I MBI3- 50 l.gc 5/1/00 soil-gas Intake #11 50l-013.gc 4/30/00 7:35 soil-gas MB14-501 MBI4- 50 l.gc 5/1/00 soil-gas AST-SVE- l-Post 501-014.gc 4/30/00 10:50 (2x dil) soil-gas MB15-501 MBI5- 50l.gc 5/1/00 soil-gas AST-SVE- l-Post 50l-015.gc 4/30/00 10:50 (50x dil) soil-gas MB16-50I MBI6- 50 l.gc 5/1/00 soil-gas AST-SVE- 2-Post 501-016.gc 5/30/00 10:55 (50x dil) soil-gas MB 17-501 MBI7- 501.gc 5/1/00 soil-gas AST-SVE- 3-Post 501-017.gc 4/30/00 11:00 (50x dil) soil-gas MB 18-501 MB18- 501.gc 5/1/00 soil-gas AST-SVE- 3-Post 501-018.gc 4/30/00 11:00 (lOxdil) soil-gas MB19-50I MBI9- 50 l.gc 5/1/00 soil-gas AST-SVE- 4-Post 50l-019.gc 4/30/00 11:05 (lOx dil) soil-gas MB20-501 MB20- 501.gc 5/1/00 soil-gas AST-SVE- 4-Post 50I-020,gc 4/30/00 11:05 (25x dil) soil-gas VOCs (ppm) Toluene Ethylbenzene m.p-Xylene o-Xylcne ND 0.3323 2.098 1.14 ND ND 0.02455 ND 0.1358 1.242 3.151 1.753 ND 0.05881 0,1587 ND 0,2666 1.884 4,38 4.43 ND 0.05373 0.1186 ND 0,08624 0,2202 1.493 2.127 ND ND 0.03928 0.08924 0.07114 2.968 7,821 4.824 ND ND 0.03414 0.1501 0,05197 0,2027 2,103 3,194 NS NS NS NS 7.663 71.64 187,1 113 0,04683 0.001182 0.003017 0.003021 0.1706 2.669 6,449 4.731 ND 0.03456 0,08782 ND 0,1157 15,19 42,1 21.79 ND 0.05835 0.1374 ND 0.00894 0.1435 0.4983 0.29 ND 0.01948 0,04912 ND 0,03943 0.1735 1.904 1.877 ND ND 0,04617 ND 0.008868 0.7845 5.376 3.761 ND 0,01742 0.04376 ND ND 3248 2.238 1.708 Sample ID Lab ID Date Collected Time Collected Matrix MB21-50 MB21- 501.gc 5/1/00 soil-gas AST-SVE- 5-Post 501-02 l.gc 5/1/00 11:08 (lOxdil) soil-gas MB22-50I MB22- 501.gc 5/1/00 soil-gas AST-SVE- 5-Post 501-022.gc 4/30/00 11:08 (4x dil) soil-gas MB23-501 MB23- SOl.gc 5/1/00 soil-gas AST-SVE- 6-Post 50l-023.gc 4/30/00 11:10 (4x dil) soil-gas MB24-50I MB24- 501.gc 5/1/00 soil-gas AST-VMP 11-Post 501-024.gc 4/30/00 14:30 (4x dil) soil-gas MB25-50 MB25- 501.gc 5/1/00 soil-gas AST-VMP ll-Post 501-025.gc 4/30/00 14:30 (50x dil) soil-gas MB26-50 MB26- 501.gc 5/1/00 soil-gas AST-VMP ID-Post 50l-026.gc 4/30/00 14:35 soil-gas MB27-50I MB27- 501.gc 5/1/00 soil-gas AST-VMP ID-Post 501-027.gc 4/30/00 14:35 (20x dil) soil-gas MB28-50I MB28- 50 l.gc 5/1/00 soil-gas , AST-VMP 2S-Post 50I-028.gc 4/30/00 14:38 soil-gas MB29-501 MB29- 50 l.gc 5/1/00 soil-gas AST-VMP ID-Post 501-029.gc 4/30/00 14:35 (50x dil) soil-gas MB30-501 MB30- 50 l.gc 5/1/00 soil-gas AST-VMP 2S-Post 501-030.gc 4/30/00 14:38 (lOxdil) soil-gas MB31-501 MB3I- SOl.gc 5/1/00 soil-gas AST-VMP 21-Post 502-00 l.gc 4/30/00 14:40 soil-gas MBOl-502 MBOI- 502.gc 5/2/00 soil-gas AST-VMP 21-Post 502-002.gc 4/30/00 14:40 (4x dil) soil-gas MB02-5021 MB02- 502.gc^ 5/2/00 soil-gas 1 VOCs (ppm) Toluene Ethylbenzene m.p-Xylene o-Xylene NS NS NS NS 0.04593 0.2363 0,6405 0,573 ND 0.02806 0,07033 ND 0,06373 0.4584 1.387 1.387 ND ND 0.0430 ND 0.08508 1.03 2.728 2.881 ND 0.02758 0.06583 ND 27.61 9.842 851.4 400.3 0.08534 0.004362 0.01032 0.005053 1.229 22.6 52.76 19.55 0.02722 0,4250 0.002448 0.0103 0.7449 29.95 59.27 29.47 ND 0.3663 0,7546 0.3434 0.02238 0.7767 4.285 8,518 ND 0.08124 0.2047 ND 0.04899^ ,2.779 5.981 9.886 ND 0.1328 0.3042 0.1514 0.02238 0.4057 2.435 5.586 ND 0.02695 0,06410 ND 0.00731 0.1512 1.032 6,111 ND 0,02201 0.07939 ND 0.07666 2.405 3.056 4.21 NS NS NS NS 0.04514 1.087 1.574 3.608 ND ND 0,02068 ND Sample ID Lab ID Date Collected Time Collected Matrix AST-VMP 2D-Post 502-003.gc 4/30/00 14:45 (lOxdil) soil-gas MB03-502 MB03- 502.gc 5/2/00 soil-gas AST-VMP 3S-Post 502-004.gc 4/30/00 14:50 soil-gas MB04-502 MB04- 502.gc 5/2/00 soil-gas AST-VMP 31-Post 502-005.gc 4/30/00 14:53 (2x dil) soil-gas MB05-502 MB05- 502.gc 5/2/00 soil-gas AST-VMP 3D-Post 502-006.gc 4/30/00 14:55 (2x dil) soil-gas MB06-502 MB06- 502.gc 5/2/00 soil-gas AST-VMP 4S-Post 502-007.gc 4/30/00 14:58 soil-gas MB07-502 MB07- 502.gc 5/2/00 soil-gas AST-VMP 41-Post 502-008.gc 4/30/00 15:00 soil-gas MB08-502 502-009.gc 5/2/00 soil-gas AST-VMP 4D-Post 502-0 lO.gc 4/30/00 15:03 (2x dil) soil-gas MB09-502 MB09- 502.gc 5/2/00 soil-gas soil-gas soil-gas soil-gas soil-gas soil-p.as soil-gas soil-gas soil-gas soil-gas soil-gas soil-gas VOCs (ppm) Toluene Ethylbenzene m,p-Xylene o-Xylene 0.03691 0.1726 0.4527 1.843 ND ND 0.01761 ND 1,521 1,462 1.563 2.346 ND 0.03885 0.05286 ND 0.1184 2.25 1.596 1.748 ND 0.07816 0,06959 ND 0,0183 0.2033 0.5146 1.396 ND ND 0.01933 ND 0.08027 0.2706 0.797 1.522 ND 0.03232 0.03827 ND 0.01386 0,5051 0,4542 0,235 ND 0.02753 0.03262 ND 0.01035 0.1993 0.4527 1.087 ND 0.04625 0.05049 ND NS-Not Saved ND - Not Detected g:\prqiects\003-60l6\SVE TS Report'-.tables.xis, Tablet? Golder Associates 304929 Pao Table 17 -.f 3 September 2000 Table t8 Comparison ot Laboratory and Field G C Analytical Data Phase II Extended Test Client ID: Testing Period/Time: Lab ID Date Sampled: Matrix: LAB DATA AST-SVE-4-Ext#l 1615 B27 232 27-Apr-OO Soil-Gas Siie Tarsel Compounds (ppniv) Toluene Ethylbenzene 0,2 <0,07 m&p-Xvlene <0,07 0-Xvlene <0,07 Client ID: Testing Period/Time: Lab ID Date Sampled: Matrix: AST-VMP-2ICPost) 1030 B27 256 30-Apr-OO Soil-Gas Siie Tcir^el Compounds (ppmv) Toluene Ethylbenzene m&p-Xvlene o-Xvletie Client ID: Testing Period/Time: Lab ID Date Sampled: Matrix: 0,83 0,99 1,55 0,33 Intake-Ext, #1 1503 B27 229 27-Apr-OO Soil-Gas Site Target Compounds (ppmv) Toluene Ethylbenzene m<fep.Xylene o-Xvlene Client ID: Testing Period/Time: Lab ID Date Sampled: Matrix: 7,14 132,22 576,54 62,58 Exhaust-ExL si 1500 B27 230 27-Apr-OO Soil-Gas Stle Target Compounds (ppmv) Toluene Ethylbenzene m&p-Xvlene o-Xylene Client ID: Testing Period/Time: Lab ID Date Sampled: Matrix: 5,5 100.66 456,89 50,78 Exhaust #5 1212 B27 247 29-Apr-OO Soil-Gas Site Tarf^el Compounds (ppmv) Toluene Ethylbenzene m&p-Xylene o-Xvlene 2,75 37,98 152,72 19,51 FIELD DATA AST-SVE-4 428-004,gc 4/27/00 16:35 soil-gas 0,03507 1,054 6,131 1,243 AST-VMP-21-Post 502-00 I g c 4/30/00 14:40 soil-sas 0,07666 2,405 3,056 4,21 Intake «2(1) 427-003-gc 4/27/00 12:44 S0i!-ltHS 0,046 N-D 1,275 0,466 Exhaust #2 427-004,gc 4/27/00 12:44 soil-aas 4,317 3,255 580,8 197,3 Exhaust m 429-003,gc 4/29/00 12:12 soil-cas 7,108 340,3 306,1 73,14 Relative Percent DifTerence (%) 140 -175 -195 -179 Relative Percent Difference (%) 166 -S3 -65 -171 Relative Percent Difference (%) 197 199 197 Relative Percent Difference (%) 24 187 -24 -118 Relative Percent Difference (%) -88 -160 -67 -116 LAB DATA AST-VMP-lI-Ext#l 1620 B27 234 27-Apr-OO Soil-Gas 0,18 0,09 0,37 <0,07 AST-VMP-4I(Post) 1040 B27 257 30-Apr-OO Soil-Gas 0,27 <0,07 <0,07 ':0,07 Imake n 1600 B27 238 28-Apr-OO Soil-Gas 6,09 107,17 489,89 55,3 Exhaust-Ext #2 1900 B27 235 27-Apr-OO Soil-Gas 4,53 68,09 290,58 33,55 Exhaust #6 2045 B27 250 29-Apr-OO Soil-Gas 2,66 37,62 151,34 19.36 FIELD DATA AST-VMP-II 430-001,gc 4/27/00 16:42 soil-Eas 0,1255 1,021 0,8243 0,7534 AST-VlvtP-4I-Post 502-OOSgc 4/30/00 15:00 soil-gas 0,01386 0,5051 0,4542 0,235 Intake f)4(l) 428-014,gc 4/28/00 9:30 soil-Eas 0,9877 26,02 46,09 4,495 Exhaust S3 428-01 Igc 4/27/00 20:05 soil-gas 6,951 2,653 451,9 43,42 No Concurrent Sample Relative Percent Difference (%) 36 -168 -76 -166 Relative Percent Difference (%) 180 -151 •147 -108 Relative Percent Difference (%) 144 122 166 170 Relative Percent Difference (%) -42 185 -43 -26 Relative Percent Difference (%) 100 100 100 100 LAB DATA AST-SVE-5 SI 1615 B27 241 28-Apr-OO Soil-Gas 0,33 <0,07 0,17 0,36 AST-VMP-3(Post) 1050 B27 258 30-Apr-OO Soil-Gas 0,24 <0,07 <007 >:0,07 Intake «3 2040 B27 249 29-Apr-OO Soil-Gas 3,47 41,27 157 94 19,85 Exhaust #3 1035 B27 236 28-Apr-OO Soil-Gas 7,15 132,72 590,42 65,34 Exhaust Ul 0800 B27 255 30-Apr-OO Soil-Gas 2,37 21,8 79,47 9,33 FIELD DATA AST-SVE-5 428-006,gc 4/27/00 16:38 soil-eas 0,06481 0,8182 1.712 0,5112 AST-VMP-3I-Post 502-005,gc 4/30/00 14:53 soil-gas 0,2368 4,50 3,192 3,496 No Concurrent Sample Exhaust #5 428-019,gc 4/28/00 12:20 soil-gas 4,294 121,7 319,9 5,135 Exhaust#11 50I-0I2,gc 4/30/00 7:30 soil-gas 3,557 148,4 391,05 241,2 Relative Percent Difference (%) 134 -168 -164 -35 Relative Percent Difference (%) 1 -194 -191 -192 Relative Percent Difference (%) 100 100 100 100 Relative Percent Difference (%) 50 9 59 171 Relative Percent Difference (%) -40 •149 • 132 •185 LAB DATA AST^SVE^2 2050 B27 252 29^Apr-00 Soil-Gas 4,96 150,07 669,52 73,3 Intake »4 0758 B27 253 30-Apr-OO Soil-Gas 3,07 26,62 95,54 11,33 Exhaust #4 1600 B27 237 28-Apr-OO Soil-Gas 1,96 24,85 100,67 12,32 Exhaust #8 1505 B27 265 30-Apr-OO Soil-Gas 0,32 <0,07 0,16 <0,07 FIELD DATA AST^SVE-2-#5 501^002,gc 4/29/00 19:54 soil-gas 45185 843 2191.5 842,5 Intake #11 501-013,gc 4/30/00 7:35 soil-gas 0,05197 0,2027 2,103 3,194 Exhaust #6 428-021.gc 4/28/00 16:05 soil-eas 2,861 11,48 29,9 4,285 No Concurrent Sample Relative Percent Difference (%) •200 -140 -106 -168 Relative Percent DifTerence (%) 193 197 191 112 Relative Percent Difference (%) -37 74 108 97 Relative Percent Difference (%) 100 100 100 100 1 See text for cieschplion of laboratory and fielcj data sources 2, Some samples concurrent only to within 6,5 hours but data presented for informative purposes. to o vo (JJ o G:t00t-6016\Guldcr\SVE TS Repont Data_compare,xl5 (Pliiisc It AS-SV!!) Golder Associates September 2000 Table 19 Phase II Extended Test Mass Removal Calculations Laboratory Analytical Data at the Intake Pert Virgin Island Chemical Site St. Croix, U.S. Virgin Islands 003-6016 Sample Port Start of test Intake Intake Intake Intake End of test Sample Date Time 4/27/00 940 4/27/00 1503 4/28/00 1600 4/29/00 2040 4/30/00 758 4/30/00 950 Compound Ethylbenzene m&p-Xylene o-Xylene Chloroform Ethylbenzene m&p-Xylene o-Xylene Chloroform Ethylbenzene m&p-Xylene o-Xylene Chloroform Ethylbenzene m&p-Xylene o-Xylene Chloroform Molecular Weight 106.2 106.2 106,2 119,35 106,2 106,2 106,2 119,35 106,2 106,2 106,2 119,35 106,2 106.2 106.2 119.35 Concentration [ppmv](1) 132.22 576.54 62.58 0.033 107.17 489.89 55,3 0.084 41,27 157,94 19.85 0.19 26.62 95.54 11.33 0,245 Concentration [ug/L] 584,10 2546,94 276.46 0.16 473.44 2164,16 244,30 0,42 182,32 697,72 87,69 0,94 117,60 422.06 50,05 1,22 Flow Rate [ftS/min] 145 145 145 145 160 160 160 160 168 168 168 168 158 158 158 158 Pressure [in, H2OI -30 -30 -30 -30 -20 -20 -20 -20 -18 -18 -18 -18 -60 -60 -60 -60 Mass Removal Rate [lb/day] 7,0 30,7 3,3 0,002 6,5 29,5 3,3 0,006 2,6 10,1 1,3 0.014 1,4 5,1 0,6 0,015 Time from start of test [hours] 0 5,4 30,4 59.1 70,4 72,2 Time over interval [hours] 17.9 26.85 20 7.45 Mass removed over interval [lb] 5.2 22.9 2,5 0.001 7.2 33.0 3,7 0,006 2,2 8,4 1,1 0,011 0,4 1,6 0,2 0.005 Grand Total: Cumulative Mass Removed [lb] 5,2 22,9 2,5 0,001 12.5 55.9 6,2 0,008 14,7 64,3 7,3 0,019 15,1 65,9 7,5 0,024 88,5 (1) Samples collected by McLaren/Hart (2) Concentration data from Microseeps Lab analyses w o U) G:\003-6016\GolderVSVETS Report\ MassLab.xls\PhE\se II Ext Data - Intake Golder Associates Page 1 of I September 2000 Table 20 Phase II Extended Test Mass Removal Calculations Field GC Analtyical Data at the Intake Port Virgin Island Chemical Site St. Croix, U.S. Virgin Islands Sample Port Start of test Intake Intake Intake Intake End of test Sample Date Time 4/27/00 940 4/27/00 1244 4/27/00 2000 4/28/00 930 4/30/00 735 4/30/00 950 Compound Ethylbenzene mifep-Xylene o-Xylene Ethylbenzene m&p-Xylene o-Xylene Ethylbenzene m&p-Xylene o-Xylene Ethylbenzene m&p-Xylene o-Xylene Molecular Weiglit 106.2 106,2 106,2 106,2 106,2 106,2 106,2 106,2 106,2 106,2 106.2 106,2 Concentration [ppmv] (1) Concentration [ugA-] Flow Rate [ft3/min] Pressure [in, H20] Mass Removal Rate [lb/day] 0,133 1,002 0,3355 5,353 14,61 1,866 26,02 46,09 4,495 0,202 2,103 3,194 0,59 4,43 1.48 23,65 64,54 8,24 114,95 203.61 19,86 0.89 9,29 14,11 145 145 145 160 160 160 168 168 168 158 158 158 -30 -30 -30 -30 -30 -30 -29 -29 -29 -60 -60 -60 0,007 0.053 0,018 0,314 0,858 0.110 1,609 2,850 0,278 0,011 0,112 0171 Time from start of test [hours] Time over interval [hours] Mass removed over interval [lb] Cumulative Mass Removed [lb] 0 3 10,3 24 70 72,2 6,65 10,5 29,85 25.2 0,002 0015 0,005 0,138 0,375 0,048 2,001 3,545 0,346 0,011 0118 0179 Grand Total: 0,002 0,015 0,005 0,140 0,390 0,053 2,141 3,935 0,399 2,152 4.053 0.578 6,8 Notes: (1) Concentration data from Photovac Field GC analyses O vo CO to G:\003-6016\Golder\SVE TS Report\ MassField,xis\Phase il Ext Data - Intake Golder Associates September 2000 Table 21 Phase II Extended Test Mass Removal Calculations Laboratoi7 Analytical Data at the Exhaust Port Virgin Island Chemical Site St. Croix, U.S. Virgin Islands Sample Port Start of test Exhaust Exhaust Exhaust Exhaust Exhaust Exhaust Exhaust Sample Date Compound Time 4/27/00 940 4/27/00 Ethylbenzene 1500 m&p-Xylene o-Xylene Chloroform ' 4 / 2 7 / 0 6 " Bhyibenzene" 1900 m&p-Xylene o-Xylene Chloroform ' 4/28/00 'Ethylbenzene 1035 m&p-Xylene o-Xylene Chloroform ' '4/2'8/bo' '"Ethyltjenzene 1600 m&p-Xylene o-Xylene Chloroform 4/29/00 Ethylbenzene 1212 m&p-Xylene o-Xylene Chloroform 4/29/00 Ethylbenzene 2045 m&p-Xylene o-Xylene Chloroform ' '4/3'0/'do 'Ethylbenzene 800 m&p-Xylene o-Xylene - Chloroform tvlolecular Weight 106.2 106.2 106.2 119,35 106,2 106,2 106,2 119,35 "l0'6',"2 106,2 106,2 119.35 10'6,2 106.2 106,2 119,35 106,2 106,2 106.2 119,35 '106,2 106,2 106,2 119,35 " 106,2 106,2 106,2 119,35 Concentration fPpmvKI) Concentration [ug/L] Flow Rate [ft3/min] Pressure [in, H2OI Press, Corr'n Temp (F] Temp [C] Temp Corr'n l^ass Removal Rate (lb/day] 100.66 456,89 50,78 0,027 68,09 290,58 33,55 0,024 i'3'2,72' " " 590,42 65,34 0,159 '24,85 100,67 12,32 0.032 37.98 152.72 19,51 0.096 3 7 , 6 2 ' 151,34 19,36 0,125 ' "" 2^1,'8 79,47 9,33 0,177 444,68 2018,37 224,33 0.13 's'oci'.'so 1283,68 148,21 0,12 "586,3'i 2608,26 288,65 0,79 i09"'7'8' 444.72 54,43 0,16 167,78 674.66 86,19 0,48 166,"l"9 •668,57 85,53 0,62 ""96,"30 351,07 41,22 0,88 145 145 145 145 155 155 155 "145 145 145 145 160' " 160 160 160 " 167 167 167 167 l"68"" 168 168 168 l'58 158 158 158 39 39 39 39 ""3"9 39 39 39 " 39 "" " 39 39 39 30 30 30 30 28 28 28 28 ""28 28 28 28 • 29- •• • 29 29 29 1,096 1,096 1,096 1.096 ""1,"0"96"" 1,096 1,096 1,096 "i,096"" 1,096 1,096 1,096 "1 ."07"4" 1,074 1,074 1,074 T;06"9 1,059 1,069 1,069 1,069 1,069 1,069 1,069 l','07i 1,071 1,071 1,071 140 140 140 140 135 135 135 135 ' l'4'o" 140 140 140 "'{35 " 135 135 135 125 125 125 125 130' 130 130 130 "125' 125 125 125 60 50 60 60 57' 57 57 57 60 60 60 60 " ' 5 7 57 57 57 ' '52 52 52 52 54 54 54 52 52 52 52 0,895 0,895 0,895 0,895 0!902" 0,902 0,902 0,902 0,895 0,895 0,895 0,895 '6,902 0,902 0,902 0,902 '0,918 0,918 0,918 0,918 0,910 ' 0,910 0,910 0,910 0,918' 0.918 0,918 0,918 5,7 25,8 2,9 0,002 4,1 17,7 2,0 0,002 7.5 33,3 3.7 0,010 1,5 5,2 0,8 0,002 2,5 9,9 1,3 0,007 2,4 9,8 1,3 0,009 1,3 4.9 0,6 0,012 Time from start of test [hours] Time over inten/al [hours] Mass removed over interval [lb] 0 5,4 '"'974" '2'4".'9" ' 30"4 '""sas "^ S'gT " 7b'.4'' 72.2 7,4 "9,'7"5 'l'6,'5 . ,..^^..^,_._.,. "' "u'is 9,'9' 7','4'5 " 1,7 7.9 0,9 0,001 " 1.7 7,2 0,8 0,001 ' 3,'3 " 14,6 1.6 0.004 """OS 3.3 0,4 0,001 1,5" 5.9 0,8 0,004 i,'o 4,0 0,5 0,004 a4 1,5 0,2 0,004 Grand Total: Cumulative Mass Removed [lb] 1,7 7,9 0.9 0,001 "••••3.4 15,1 1.7 0.001 ~ 6,7" 29,7 3,3 0,006 7,5 33,0 3,7 0,007 9,6 38,9 4,5 0,011 10,0 43,0 5,0 0,015 16,4 44,5 5,2 0,019 60,1 u> o yo U) OJ (1) Concentration data from Microseeps Lab analyses Notes: Samples taken upstream of blower at unknown location Flow rate measured upstream of blower at unknown location G:\003-6016\GoltlertSVE TS Repoj1\ MassLab,xls\Pnase II Ext Data • Exhaust Golcjer Associates Table 21 September 2000 Table 22 Phase II Extended Test Mass Removal Calculations Field GC Analytical Data at the Exhaust Port Virgin Island Chemical Site St. Croix, U.S. Virgin Islands Sample Pon Stan of test Exhaust Exhaust E.xliatist Exhaust Exhaust' Exhatist Exhausl Exhaust Eitd of test Sample Date Time 4/27/00 940 4/27/00 1244 4/27/00 2005 4/28/00 930 4/28/00 1605 4/28/00 2040 4/29/00 908 4/29/00 1212 4/30/00 730 4/30/00 950 Compoutitj Ethylbenzene tn&p-Xylene o-Xylene Ethylbenzene in&p-Xylene o-Xylene Ethylbenzene in&p-Xylene o-Xylene Ethylbenzene in&p-Xylene o-Xylene Ethylbenzene m&p-Xyleiie o-Xylene Ethylbenzene m&p-Xylene o-Xyieiie Ethylbenzene m&p-Xylene o-Xylene Ethylbenzene m&p-Xylene o-Xylene Molecttlar Weieht 106,2 106,2 106,2 106,2 106,2 106,2 106,2 106,2 106,2 106,2 106,2 106,2 106,2 106,2 106,2 106,2 106,2 106,2 106,2 106,2 106,2 106,2 106,2 106,2 Concentration [ppinv] (1) Concenttation [ug/L] Flow Rate [ft3/iTiin| Pressure [in, H20| Press CoiT'n, Temp, [F] Temp, fC) Temp CotT'n Mass Removal Rale [lb/day] 3,255 580,8 197,3 2653 451,9 43,42 132,1 314,5 34,43 114,8 299 42,85 111,3 298,2 45,23 296,9 283,9 82,73 3403 306 1 73,14 148,4 391,05 241,2 14,38 2565,76 871,50 11,72 199633 191,81 583,57 1389,35 152,10 507,14 1320.87 189,30 491,68 1317,34 199,81 1311,60 1254,17 365,47 1503,32 1352,24 323,11 655,58 1727,52 1065,53 145 145 145 155 155 155 145 145 145 159 159 159 157 157 157 167 167 167 167 167 167 158 158 158 39 39 39 39 39 39 39 39 39 30 30 30 30 30 30 28 28 28 28 28 28 29 29 29 1,096 1 096 1,096 1,096 1,096 1,096 1,096 1,096 1,096 1,074 1,074 1,074 1,074 1,074 1,074 1,069 1,069 1,069 1,069 1,069 1,069 1,071 1,071 1,071 140 140 140 135 135 135 140 140 140 130 130 130 125 125 125 125 125 125 125 125 125 125 125 125 60 60 60 57 57 57 60 60 60 54 54 54 52 52 52 52 52 52 52 52 52 52 52 52 0,895 0,895 0,895 0,902 0,902 0,902 0,895 0,895 0,895 0,910 0,910 0,910 0,918 0,918 0,918 0,918 0,918 0,918 0,918 0,918 0,918 0,918 0,918 0,918 0,183 32,734 11,120 0,161 27,455 2638 7,445 17,725 1,940 7,070 18,413 2,639 6,826 18.288 2,774 19,279 18435 5,372 22,097 19,876 4,749 9,138 24,079 14,852 Time fiom start of test [hours] Time over interval [hours] Iviass removed over interval [lb] Cumulative Mass Reinoved [lb] 0 3 10,3 23,8 30,4 35 47,4 50,4 69,7 72,2 6,65 10,4 10,05 5,6 8,5 7,7 11,15 12,15 0,051 9,070 3,081 0,070 11,897 1,143 3,118 7,422 0,813 1.650 4.296 0,616 2.417 6,477 0,982 6,185 5,915 1,724 10,266 9,234 2,206 4,626 12,190 7,519 Grand Total: 0,05 9,07 3,08 0,12 20,97 4,22 3,24 28,39 5,04 4,89 32,69 5,65 731 39,16 6,63 13,49 45,08 8,36 23,76 54,31 10,56 28,38 66,50 18,08 113,0 (1) Concentration data froin Photovac field gc analyses o w G:\003-6016\Goldet^SVE TS Report\ MassField,xls\Phase 11 Ext Data - Exhaust Golder Associates Table 22 September 2000 Table 23 Groundwater Analytical Results - AST Area Virgin Island Chemical Site 003-6016 iClient ID: Sample Depth: Lab ID Date Sampled: Matrix: AST-VMP-ID 2010021 13-Mar-00 Water AST-VMP-ID 2011123 30-Mar-OO Water AST-VMP-ID 2014007 29-Apr-OO Water AST-VMP-ID 2014130 01-May-OO Water AST-VMP-2D 2010022 13-Mar-OO Water St. Croix, U.S. Virgin Is AST-VMP-2D (duplicate) 2010023 13-Mar-OO Water AST-VMP-2D 2011124 30-Mar-OO Water ands AST-VMP-2D 2014465 03-Mav-OO Water AST-VMP-3D 2010024 13-Mar-OO Water AST-VMP-3D 2011125 30-Mar-OO Water AST-VMP-3D 2014131 1 OI-May-00 ' Water AST-VMP-4D 2010025 13-Mar-OO Water AST-VMP-4D 2011117 30-Mar-OO Water AST-VMP-4D 2014132 OI-May-OO Water Site Target Compounds Acetone Chloroform Ethylbenzene Methylene chloride Toluene Xylene (total) (ug/L) 2000 U 2000 U 8510 2000 U 2000 U 31900 1000 U 1000 U 11100 1000 U • 1000 u 34100 1000 U 1000 U 6150 1000 U 1000 U 26300 1000 U 1000 U 4290 1000 U 1000 U 15300 1000 U 1000 U 5490 1000 U 1000 U 24500 ,1000 U 1000 U 4390 1000 U 1000 U 21300 500 U 500 U 3170 500 U 500 U 12600 40 U 40 U 401 40 U 40 U 907 1000 U 1000 U 7540 1000 U 1000 U 38000 1000 U 1000 U 6850 1000 U 1000 U 35900 1000 U 1000 U 6750 1000 U lOtlO U 24200 10 U 1.9 J 10 U 10 U 10 U 10 U 10 U 2.4 J 1.3 J 10 U 10 U 10 U 10 U 2.1 J 35.5 10 U 10 u 307 Natural A tteniiation Parameters (mg/L) Ammonia Dissolved ox}'gen Iron Nitrate Nitrite Sulfate Sulfide ~ — — — — — - — — — — — — - — — — ~ — — — — — — — — — 5.9 8.2/14.7/15.8 7.3 0.1 0.435 122 0.61 — — — — — - , — — — — — — - — — — — — 119 - — 5 —. — — — - — — — — ~ — „ - ~ — — — — — 0 — — — — - — — — — — — - ~ — — — — — - SVE/AS System Parameter (mg/L) Carbon Dioxide 40 - - - 58 - ~ - 60 - - 50 Client ID: Sample Depth: Lab ID Date Sampled: Matrix: MW-1 209600 09-Mar-OO Water MW-1 2011120 29-Mar-OO Water MW-1 2014006 29-Apr-OO Water MW-I 2014461 03-May-OO Water MW-6 209599 09-Mar-OO Water MW-6 2011128 29-Mar-OO Water MW-6 2014462 03-Mav-OO Water MW-8 209596 08-Mar-OO Water MW-8 (duplicate) 209597 08-Mar-OO Water MW-8 2011122 29-Mar-OO Water MW-8 2014463 03-May-OO Water MW-10 209594 07-Mar-OO Water MW-10 2011121 30-Mar-OO Water Site Target Compounds (ug/L) Acetone Chloroform Ethylbenzene Methylene chloride Toluene Xylene (total) 5000 U 5000 U 19600 5000 U 5000 U 89000 2500 U 2500 U 21600 2500 U 463 J 108000 500 U 500 U 1040 500 U 500 U 8700 1000 U 1000 U 7680 1000 U 155 J 40100 4000 U 4000 U 12400 4000 U 4000 U 60700 1000 U 1000 U 12400 1000 U 146 J 60600 1000 U 1000 U 14500 1000 U 131 J 63000 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u U) u 2.7 J 10 u 10 u 11.6 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u Natural Attenuation Parameters (mg/L) Ammonia Dissolved oxj'gen Iron Nitrate ! Nitrite Sulfate Sulfide 1.1 0 0.9 0 0 10 U 0.51 — ~ — — — ~ ~ — — — — — — ~ — — — — — 25 - , 0.7 0 3.1 0.04 0 47.4 0.11 — — — — — — ~ — — — — — 66.3 - 0 0 0 0.65 O.OI 74.6 0 — — — ~ ~ — ~ — — — — — ~ ~ — ~ - - - 84.9 - 0.4 0 0.1 0.5 0,005 286 0 — - ~ — — — -- SVE/AS System Parameter (mg/LJ 1 Carbon Dioxide | 68 i — 1 - 1 - 1 100 1 - 1 40 1 - 1 - i 80 1 - 1 U: Not detected below method detection limit J: Estimated value G;SVE TS Report'groundwater_rev.xls,'gvv - .-\ST Area Golder Associates 304935 Table 23 SeptembeT 2000 Table 2 4 G r o u n d w a t e r Analytical Results - F P P Area Virgin Island Chemical Site St. Croix, U.S. Virgin Islands 003-6016 ClientlD: Sample Depth: Lab ID Date Sampled: Matri.x: FPP-VMP-ID 2010029 14-Mar-OO Water FPP-VMP-ID 2011237 30-Mar-OO Water FPP-VMP-ID (duplicate) 2011238 30-Mar-OO Water FPP-VMP-ID 2014010 30-Apr-OO Water FPP-VMP-ID 2014014 OI-May-00 Water FPP-VMP-2D 2014011 OI-May-00 Water FPP-VMP-3D 209852 IO-Mar-00 Water FPP-VMP-3D 20IIII5 30-Mar-OO Water FPP-VMP-3D 2014015 OI-Mav-OO Water FPP-VMP-4D 209853 lO-Mar-OO Water FPP-VMP-4D 2011241 31-Mar-00 Water FPP-VMP-4D 2014009 30-Apr-OO Water FPP-VMP-4D 2014013 OI-May-00 Water Site Target Compounds (ii^/L) Acetone Chlorolbrm Ethylbenzene Methvlene chloride Toluene Xylene (total) 10 U 39,8 l O U l O U 10 U 10 U 10 U 25,6 10 U 10 U 10 U 2,1 J 10 U 25,5 10 U 10 U 10 U 3 1 J 10 U 81,6 10 U 10 U 10 U 10 U iO U 137 10 U 10 U 10 U 10 U 10 U 3,7 J 10 U 10 U 10 U 10 U 10 U 11.5 3,4 J 10 U 10 U 15.3 10 U 7.3 J 10 U 10 U 10 U 10 U 10 U 9.8 J l O U 10 U 10 U 10 U 10 U 33,9 10 U 10 U 10 U 10 U 10 U 19,8 l O U 10 U 10 U 10 U 10 U 12,1 10 U 10 U 10 U 10 U 10 u 20,2 10 U 10 U 10 U 10 U Natural Attenuation Parameters (iiig/L^ Ammonia Dissolved oxygen Iron Nitrate Nitrite Sulfate Sulfide - 0 - - - - , - - - - - - - - - ~ - - - - - - - - - - - - - - - - - - - - - - - ~ - - - - - - - ~ - - - - - - - - - - ~ ~ - . - - - - - - - - - - - - SVE/AS System Parameter (mg/L) [Carbon Dioxide 65 70 40 i ClientlD: Sample Depth: Lab ID Date Sampled: Matrix: MW-2 209595 08-Mar-OO Water MW-2 2011239 31-Mar-00 Water MW-2 (duplicate) 2011240 31-Mar-00 Water MW-2 2014469 04-May-OO Water MW-2 (duplicate) 2014470 04-May-OO Water MW-3 209592 08-Mar-OO Water MW-3 2011244 31-Mar-00 Water MW-7 209593 08-Mar-OO Water MW-7 2011242 31-Mar-00 Water MW-7 2014464 03-May-OO Water Site Target Compounds Acetone Chloroform Ethylbenzene Methylene chloride Toluene .Xylene (total) (ug/L) 10 U 37 l O U 10 U 10 U 10 U 10 U 40.7 10 U 10 U 10 U 1,4 J 10 U 38.6 10 U 10 U 10 U 10 U 10 U 16,7 10 U 10 U 10 U 10 U 10 U 21,1 l O U 10 U 10 U 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 1,5 J 10 u 10 u 10 u 10 u 10 u 1.9 J 10 u 10 u 10 u 10 u 10 u 1.4 J 10 u 10 u 10 u 10 u Natural Attenuation Parameters (m^/L} Ammonia Dissolved oxyeen Iron Nitrate Nitrite Sulfate Sulfide 0,7 1 0 0,46 0,01 15! 0,02 - - - - - - - - - - — . - - - 149 - - - - - 179 - 0,4 0,7 4.6 0.02 0 194 0 - - - 0,3 0.7 0 1,71 0,015 195 0 _ - - - - - - - - - 206 - SVE/AS System Parameter (mg/L) [Carbon Dioxide 65 50 70 ClientlD: Sample Depth: Lab ID Date Sampled: Matrix: MW-11 209590 08-Mar-OO Water MW-12 209850 lO-Mar-OO Water MW-13 209421 07-Mar-OO Water MW-14 209851 10-Mar-OO Water MW-15 209420 07-Mar-OO Water Site Target Compounds Acetone 'Chloroform Ethylbenzene Methylene chloride Toluene Xylene (total) (ug/L) lOU 40.4 10 U lOU 10 U 10 U 10 U 10 U 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 9,4 J 10 u 10 u 10 u 10 u Natural Attenuation Parameters (m^/L^ Ammonia Dissolved oxygen Iron Nitrate Nitrite Sulfate Sulfide 0.1 0 0 0.55 0,01 243 0 0,4 0 0 1,05 0,01 194 0 0 0 0 2,73 0 182 0 0 0,5 0 2.81 0,015 207 0 0 0 0 1.48 0.02 186 - SVE/AS System Parameter (mx/L) [Carbon Dioxide 75 35 50 50 26 U: Not detected below method detection limit J: Estimated value G:SVE TS Report:groundwatcr_rev.xls:ji\v - FPP Area Golder Associates 304936 Table 24 Page I of 1 September 2000 Table 25 Groundwater Analytical Results - Trip and Field Blanks Virgin Island Chemical Site St, Croix, U.S. Virgin Islands 003-6016 ClientlD: Sample Depth: Lab ID Date Sampled: Matrix: TB0307G0 N/A 209419 07-Mar-OO Water TB030800 N/A 209591 08-Mar-OO Water TB031000 N/A 209848 10-Mar-OO Water TB031300 N/A 2010020 13-Mar-OO Water TB033000 N/A 2011127 30-Mar-OO Water TB033100 N/A 2011235 31-Mar-OO Water TB042900 • N/A 2014008 29-Apr-OO Water TB050200 N/A 2014133 02-May-00 Water TB050400 N/A 2014467 04-May-OO Water TB050400 N/A 2014471 04-May-OO Water Site Target Compounds Acetone Chloroform Ethylbenzene Methylene chloride Toluene Xylene (total) (ug/L) 10 U 10 U 10 U 1,9 J 10 U 10 U 10 U 10 U 10 U 1.5 J 10 u 10 u 10 u 10 u 10 u 2,1 J 10 u 10 u 10 u 10 u 10 u 4,6 J 10 U 10 U 10 u 10 u 10 u 1,4 J 10 U 10 u 10 u 10 u 10 u 4,3 J 10 U 10 U 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 1,8 J 10 u 10 u 10 u 10 u 10 u 1.6 J 10 u 10 u 10 u 10 u 10 u 1,9 UJ 10 u 10 u Client ID: Sample Depth: Labro Date Sampled: Matrix: FB030800 N/A 209598 08-Mar-OO Water FB030900 N/A 209846 09-Mar-OO Water FB031000 N/A 209849 10-Mar-OO Water FB031400 N/A 2010026 14-Mar-OO Water FB032900 N/A 2011119 29-Mar-OO Water FB033000 N/A 2011126 30-Mar-OO Water FB0330OOA N/A 2011236 30-Mar-OO Water FB033100A N/A 2011245 31-Mar-OO Water FB033100B N/A 2011243 31-Mar-OO Water FB050100 N/A 2014129 01-May-OO Water FB050300 N/A 2014466 03-May-OO Water FB050400 N/A 2014468 04-May-OO Water Site Target Compounds (ug/L) Acetone Chlorofonn Ethylbenzene Methylene chloride Toluene Xylene (total) 10 U 10 U 10 U 1,7 J 10 U 10 U 10 U 10 U 10 U 3,1 J 10 U 10 U 10 U 10 U 10 U 2,4 J 10 U 10 U 8,5 J 10 U 10 U 6 J 3,8 J 1,3 J 10 U 10 U 10 U 1,4 J 10 U 10 U 18,7 J 10 U 10 U 2 J 10 U 1,3 J 16,3 J 10 U 10 U 3,6 J 10 U 10 U 20 J 10 U 10 U 3 J 10 U 10 U 19,8 J 10 U 10 U 2,8 J 10 U 10 U 10 U 10 U 1,9 J 2 J 10 U 7,7 J 10 U 10 U 10 U 1,6 J 10 U 4,2 J 10 U 10 U 10 U 1,2 J 10 U 4.7 J U: Not detection below method detection limit J: Estimated value o CO <l G:SVE TS Report:groundwater_rev,xls:gw - QC Golder Associates Tower ^vB. * V ^ \ W ' I ^ ^ N <• \ ^ 154 <,:"i,n,.'ls/' :-l,3milton Airport .. Ervv'y •4 ,:...:r^-7-.-^-r--V""'"i! Alexanc}et.J:Iamilte5_v-..;,,--.-- .: I"—- ^^ttrpDrt^ it' ^ L^l2:5jp • ; / • rciM 1 50 : MtiiKitng Hay.z-'''-''^ \ Jf- • s i ) W a m i i n g B j y • ~ 2 R.nitrtt.iLli "l S^- IJ .•:j*'>G«tt:- i ' ', :i^--7S' j ^ - " ^ > i : . ' i W ! / / " " % i P 11 V" ' , i > f - J I REFERENCE 1.) MAP TAKEN FROM U.S.G.S. 7.5 MINUTE QUADRANGLE OF CHRISTIANSTED. VIRGIN ISLANDS. 2000 scale 2000 feet 00 n o n OIK BY: REV BY: 003-6016 AM 5A^ ^^S AS SHOWN DATE: 10/05/00 US01-039 DR SUBTlTli: 04 SITE LOCATION MAP VIRGIN ISLAND CHEMICAL SITE 1 3' (S MANHOLE GROUND SURFACE VACUUM GAUGE • MICROSEEPS SAMPUNG PORT- 2" S,S. TEE 2 S.S. RISER • PHOTOVAC AND OVM SAMPLING PORT_ ACCESS FOR ANEMOMETER LU Z o N bJ to O Q LL) < 0 , 6 1/2" 0.0. BOREHOLE- 2" S.S. .020 SLOT WELL SCREEN -20.0'- -25.0'- •S.S. CAP -CONTROL VALVE • 2" PVC PIPE TO BLOWER 12" VAPOR EXTRACTION CEMENT/BENTONITE GROUT BENTONITE SEAL 5.0" 2.0' 3.0" #2 SAND FILTER PACK 20.0 25.0' NOTE: 1.) ACTUAL DEPTHS VARIED BASED ON FIELD CONDITIONS. 2.) MONITORING POINT (GMP) WAS INSTALLED WITHIN 3 FEET OF SVE WELL TO MEASURE WATER LEVELS. 3.) ACTUAL WATER TABLE ENCOUNTERED AT 15 FEET BGS DURING PILOT STUDY. 304940 VIRGIN ISLAND CHEMICAL SITE ST. CROIX, U.S. VIRGIN ISIANDS amRomiBnu. BESOVBCK TSctoioiDciEs - J CHK'D BY: JMV SCALE: NONE DATE; 03/05/99 REV. DATE: 08/31/00 TYPICAL SOIL VAPOR EXTRACTION (SVE) WELL FIGURES 18"0 MANHOLE GROUND SURFACE PRESSURE INDICATOR- 1" PVC TEE AIR INJECTION TUBE (1" DIA. SCH. 80 PVC) • 6 1/2" O.D. BOREHOLE 2 0 - 2 5 ' VARIES T WATER TABLE 50' IN AST AREA 48' IN FPP AREA 2' - r SCH. 80 PVC .040 SLOT WELL SCREEN PVC CAP BALL VALVE 5/16" TUBING TO COMPRESOR INJECTION OF AIR 12 304941 VIRGIN ISLAND CHEMICAL SITE ST. CROIX, U.S. VIRGIN ISLANDS ENVmONUENTAL RISOUKCE TECHNOUlCllS CHK'D BY: JMV SCALE: NONE DATE: 03/05/99 REV. DATE: 08/31/00 TYPICAL AIR SPARGING (AS) WELL FIGURE 4 GROUND SURFACE VACUUM GAUGE SAMPUNG PORT PVC CAP I S " * MANHOLE 2" SCH. 40 PVC RISER 6 1/2" O.D. BOREHOLE • WATER TABLE GROUT/ BENTONITE SEAL BENTONITE SEAL #2 SAN AND RLTER PACK GROUT/ BENTONITE SEAL m tx54 i><^ GROUT/ BENTONITE SEAL BENTONITE SEAL #2 SAND FILTER PACK -2"» SCH. 40 PVC ,020 SLOT WELL SCREEN BENTONITE SEAL #2 SAND FILTER PACK -2"» SCH. 40 PVC .020 SLOT WELL SCREEN -25' -29" - 2 ' t SCH. 40 PVC .020 SLOT WELL SCREEN NOTE: 1) ACTUAL DEPTHS VARIED BASED ON FIELD CONDITIONS. VIRGIN ISLAND CHEMICAL SITE ST. CROIX, U.S. VIRGIN ISLANDS EHVIROiaiEXTAL KZSOUIiCE TZCHMOLDCIES CHK'D BY: JMV DATE: 0 3 / 1 1 / 9 9 SCALE: NONE REV. DATE: 0 8 / 3 1 / 0 0 SHALLOW/INTERMEDIATE/DEEP VAPOR MONITORING PROBE CLUSTER 304942 FIGURES - SEPTUM FOR MICROSEEPS SAMPLES O O O 1 O O 03 6 Q 1.) ACTUAL WATER TABLE ENCOUNTERED AT 15 FEET BGS DURING PILOT STUDY. 2.) SEE WELL^CONSTRUCIION LOGS FOR DETAILS. SOIL VAPOR EXTRACTION/AIR SPARGING SCHEMATIC FIGURES 304943 ^Ro Septemb^TzOOO 003-6016 140 120 u> o l ( ^ \o lt». It^ 1 i 1 u (fl i 5 1 o i u. 100 80 60 Figure 7 Phase I Step Rate Test Flow vs. Vacuum Data Virgin Island Chemical Site St. Croix, U.S. Virgin Islands • AST Area • FPP Area Linear (AST Area) Linear (FPP Area) • 10 20 30 40 Vacuum, in w.c. gauge 50 60 70 g:\proiects\003-6016\GolclerVP(lot Test Rpt\ReportFigs.xls, SVE Step Chart Golder Associates Septemb^^OOO ^reb OOb-6016 Figure 8 Phase I SVE Constant Rate Test AST Area - Intermediate Probes Virgin Island Chemical Site St. Croix, U.S. Virgin Islands Distance From SVE Well, feet 10 100 OJ o Ol 0,2 0,4 ID o> 0,6 ra en 6 S c 0,8 L. 3 tf) V) P 1 (. / \ ) / p r 4 ^ f J \ ^ ^ / y • y / / a -H X — 36610 0730 •36610 1840 -Log, (36610 1530) - O ' — 36610 0930 36611 0730 -Log, (36610 1730) • — , 36610 1130 -Log. (36610 0730) -Log. (36610 1840) m 36610 1330 -Log. (36610 -Log, (36611 0930) 0730) A 36610 1530 -Log. (36610 1130) • X — 36610 1730 -Log, (36610 1330) g:\projects\003-6016\Golder\Pllot Test Rpt\ReportFigs,xls, SVE-AST Int Golder Associates ^Ko SeptemDeTCOOO DC^O 00TB016 u> o Figure 9 Phase I SVE Constant Rate Test FPP Area - Intermediate Probes Virgin Island Chemical Site St. Croix, U.S. Virgin Islands Distance From SVE Well, feet 10 100 0,2 0,4 0) ? 0,6 0,8 1.2 1.4 1,6 { • ^ = === " " . H 1 -I- 36610 0730 X 36610 1840 Log, (36610 1730) - 36610 0930 O 366110730 Log. (36610 1840) 36610 1130 •Log. (36611 0730) •Log. (36610 1130) 36610 1330 -Log. (36610 0930) •Log. (36610 1330) 36610 1530 -Log, (36610 0730) 36610 1730 •Log. (36610 1530) g:\projects\003-6016\Golder\Pilot Test Rpt\ReportF(gs,xls, SVE-FPP Int Golder Associates 304947 AST-SVE-3 Key for Figure: \ST-VMP-4I JVE-4 AST-VMI> AST-VWlP-21 AST-VMP-31 ' - AST-;; Figure 10 Phase I Constant Rate SVE Test, Contours of Vacuum of Intermediate Probes and SVE Wells AST Area Virgin Island Chemical Site St. Croix, U.S. Virgin Islands \\raetallica\document\projects\003-6016\golder\sve ts report\contoursl,doc Colder Associates JKc SeptemC^'ZQOO Db^6016 Figure 11 Phase I Constant Rate Test Rate of Extraction Virgin Island Chemical Site St. Croix, U.S. Virgin Islands 24 35 Hours from start of test D Ethylbenzene a Total Xylenes EH Chloroform H Total "~^ CO o 00 G:\003-6016\Golder\SVE TS Report MassLab.xls\Phl ExtRate Golder Associates \^Ko SeptembSTCOOO ) 0 ^ 0 00T5016 Figure 12 Phase I Constant Rate Test Cumulative Mass Removed Virgin Island Chemical Site St. Croix, U.S. Virgin Islands 3.5 3.0 2.5 •o > o E u 0£ </) in re 2.0 1,5 24 35 Time from Beginning of Test (hours) 49 i ^' 59 ^Ethylbenzene ^ Total Xylenes H Chloroform H Total o yo G:\003-6016\Golder\SVE TS Report MassLab,xls\Phl CumMass Golder Associates b^?0 SeptemtiSrSOOO 003-6016 Figure 13 Phase II AS Step Test Flow vs. Pressure Data Virgin Island Chemical Site St. Croix, U.S. Virgin Islands • AST Area Step Test B FPP Area Step Test Linear (FPP Area Step Test) Linear (AST Area Step Test) 1 5 (/> o 4 LijW. / • 1^ m ^ ^ ^ / B • 10 20 30 40 Sparge Wellhead Pressure, psig 50 60 70 o vo tn o g:\projects\003-6016\Golder\PilotTest Rpt\ReportFigs,xls, AS Step Chart Golder Associates L- SeptembsWDOO j^Rc 13^1 003^16 Figure 14 Phase II AS Step Test Dissolved Oxygen Measurements, AST Area Virgin Island Chemical Site St. Croix, U.S. Virgin Islands «h-AST-VMP-ID ^3~-AST-VMP-2D ^f~-AST-VMP-3D *-AST-VMP-4D ••-SVE-1 -+-MW-1 — MW-6 Baseline 1630 05-Apr-OO StepI 1149 06-Apr-OO StepI 1200 08-Apr-OO Step 1 Step 2 1330 1630 08-Apr-OO 08-Apr-OO Step 3 Step 3 1815 1930 08-Apr-OO 08-Apr-OO G:\003-6016\Golder\SVE TS Report\ DissOxy.xls\Phs II step AST Golder Asssociates Septemb^^OOO ^ K O id^o 003TD16 Figure 15 Phase II AS Step Test Dissolved Oxygen, FPP Area Virgin Island Chemical Site St. Croix, U.S. Virgin Islands o ,«> o -<^ Q. -?> o ..«' Q . .P Q Jt) O .(D o .<i> Q. .,2) O .OJ FPP-VMP-ID * FPP-VMP-2D >t-FPP-VMP-3D *-FPP-VMP-4D •-FPP-SVE-1 -t—MW-2 CO CO CO CO G:\003-6016\Golder\SVE TS Report DissOxy.xIsVPhs II step FPP Golder Associates [Tl^2i SeptemnBr2000 00^016 Figure 16 Phase II SVE/AS Test AST Area - Intermediate Probes - Vacuum Response Virgin Island Chemical Site St. Croix, U.S. Virgin Islands o VD en to 0 -t 0,5 0) 1,5 D) 3 (B U) B •3 u n > 2,5 Distance From SVE Well, feet 10 100 J X / / [ V / A / / ^ / \ V / / ' . / ^ V / / 1 - X 15-Apr-OO, 1125 Log, (15-Apr-OO, 1125) 15-Apr-OO, 1540, •Log, (15-Apr-OO, 1540) -I- 15-Apr-OO, 1920 -Log. (15-Apr-OO, 1920) - 16-Apr-OO, 0730 Log, (16-Apr-OO, 0730) 16-Apr-OO, 1520 •Log, (16-Apr-OO, 1520) g:\proiects\003-6016\Golder\Pilot Test Rpt\ReportFlgs.xls, Phil AS-SVE - AST Int G o l d e r A s s o c i a t e s b ^ C Septembcr2000 O0W0I6 o Ol 0,05 0,1 o at 3 m O) 6 i c 0,15 £ 3 in U) 0) a. 0,2 Figure 17 Phase II AS/SVE Test AST Area - Deep Probes - Pressure Response Virgin Island Chemical Site St. Croix, U.S. Virgin Islands Distance From Sparge Well, feet 10 100 i f t^ ^.-' ^ • ^ ^ ^ ^ ,.-- / . ^ ^ ^ i t > ^ i ^ _,,^ / ^ ^ ^ • ^ ^ ^ ^ ^ ^ " " ^ ^P^ / • ^ ^ ^ ^ ; ^ < ? ^ ^^f^^^---^ • / ^ ' ^ ^^--"^^ \ ^ ^ 1 C X 15-Apr-OO, 1125 e 15-Apr-OO, 1540 4- 15-Apr-OO, 1920 - 16-Apr-OO, 0730 Log, (15-Apr-OO, 1125) Log, (15-Apr-OO, 1540) Log, (15-Apr-OO, 1920) ——Log, (16-Apr-OO, 0730) 16-Apr-OO, 1520 •Log, (16-Apr-OO, 1520) g:\projects\003-6016\Golder\PilotTest Rpt\ReportFigs.xls, Phil AST Deep Golder Associates September 2000 003-6016 Figure 18 Phase II SVE/AS Test Dissolved Oxygen AST Area Virgin Island Chemical Site St. Croix, U.S. Virgin Islands if:*iisf>^" • 1530 14-Apr-OO 1725 14-Apr-OO 1930 14-Apr-OO 2045 14-Apr-OO 1300 14-Apr-OO 0750 15-Apr-OO 1125 1 S-Apr-Od -•-AST-VMP-ID •HB-AST-VMP-2D ~A-AST-VMP-3D •4r"AST-VMP-4D -51^ MW-1 -•-MW-6 -+-MW-8 • & - ^ G:\003-6016\Golder\SVE TS Report\ DissOxy.xls\Phil test AST Golder Associates b ^ O SeptembttTOOOO )0l^0 003^016 Figure 19 Phase II SVE/AS Test Dissolved Oxygen - FPP Area Virgin Island Chemical Site St. Croix, U.S. Virgin Islands 14 ; : CO o i ^ Ul <T» • - 1 en c 0) >» X O T3 ^-FPP-VMP-ID -:^FPP-VMP-2D -^i^FPP-VMP-3D -•-FPP-VMP-4D -I—MW-2 -•-MW-7 2230 14-Apr-OO 0700 15-Apr-OO 1505 15-Apr-OO 1830 15-Apr-OO G:\003-6016\Golder\SVE TS Report\ DissOxy.xls\Phll test FPP Golder Associates Key for Figure: -^AST-SVE-S- ^AST-SVE.3 ^AST-SVE-I ^AST-VMP-11 ^AST-VMP-21 ^AST.VMP-31 ^AST-VMP-41 ^AST.SVE-4 -^AST-SVE-2 ^ - ^ 8 . 0 0.00^ -10.00 -20.00 -30.00 -70.00 -60.00 -50.00 -40.00 -30.00 -20.00 10.00 0.00 Figure 20 Contours of Vacuum Levels for Phase II Extended Test Virgin Island Chemical Site St. Croix, U.S. Virgin Islands 304957 ;:\projects\003-60I6\goldcr\sve ts report\contours2.doc Golder Associates \,r^i SeptembsreoOO ^reo )oWo 00355016 Figure 21 Phase II Extended Test Dissolved Oxygen - AST Area Virgin Island Chemical Site St. Croix, U.S. Virgin Islands CO o vo en O) 16 14 12 10 OJ O Q SS.--:>= *'-"•"::.' ^ . . , , ^ • : f^ 1 '-^ ' - - : • > ~ i ' tw 4 2 J> •0 'ti • \ \ / -A P 1 \ \ , r---^ / / „ ^ / ^ , ^ ^ _ , _ „ . ^ . _ . - ^ - , - ^ AO> / \V / - ^ ^ - ^ ^ ^ - - \ V \ \ \ yi ^^t^yt^—^^ ^^^~:^^ / x / \ / \ \ *=r / / ? 4 \ -A. :.. .--.u^^jji —1 / -rj:—-—y \ \ ^ 0930 J 4 27-Apr-OO 1400 27-Apr-OO 1715 27-Apr-OO 1905 27-Apr-OO 2115 27-Apr-OO 0845 28-Apr-GO 1145 28-Apr-OO 1715 28-Apr-OO -S-AST-VMP-1D --A-AST-VMP-2D -^*--AST-VMP-3D - * - A S T - V M P - 4 D - • - M W - 1 —4—MW-6 MW-8 fA<&i^' G:\003-6016\Goider\SVE TS Report\ DissOxy.xls\Philext AST Golder Associates T^KC Septemc^OOO 0^6016 Figure 22 Phase II Extended Test Dissolved Oxygen - FPP Area Virgin Island Chemical Site St. Croix, U.S. Virgin islands 0750 27-Apr-OO 0930 27-Apr-OO 1325 27-Apr-OO 1710 27-Apr-OO 1830 27-Apr-OO 2100 27-Apr-OO 0745 28-Apr-OO -m- —ir,- • - • M - ^ K - —(_ -FPP-VMP-ID FPP-VMP-2D -FPP-VMP-3D -FPP-VMP-4D -MW-2 -MW-3 -MW-7 G:\003-6016\Golder\SVE TS Report\ DissOxy.xls\PhllextFPP Golder Associates Septembet^WDO ;^R)( 00! Figure 23 Phase K SVE/AS Extended Test Total Cumulative Mass Removed - Comparison of Calculation Methods Virgin Island Chemical Site St. Croix, U.S. Virgin Islands 120 40 Time (hours) • • - Field GC - Exhaust -•-Field GO-Intake HB- Lab - Exhaust -A—Lab - Intake 80 G:003-6016\Golder\SVE TS Report IVlassField.xIsUotal mass Golder Associates September r^JO 003^m6 Figure 24 Phase II Extended Test Rate of Mass Extraction Microseeps Data (Lab) Virgin Island Chemical Site St. Croix, U.S. Virgin Islands OJ o yo 45.0 40.0 35,0 2r 30,0 re B 1^ 25.0 I = ^„ ^ ! .2 20.0 I u S 15.0 1 10.0 ' ] IT- r - ] L i j 5,0 0.0 5,4 30,4 59,1 . Time Sample Taken (Hours from start of test) - \J.>^ .: , '" ' ' ' " / I •*_** , L ' , ' \^ ' 1 . ' * * . - ' ? ' - ' ;; ;* " — - r-- tfl' - ,1 t ' . M • ^ * * 1 <* ' -'". .* - " . - ' • ' ' • * • - ' , - " . • ; ' • ; — - - - • . , . t \ " - - - - --- - - - - - V'"'' * 1 fr ipi^^ppi Pl^ffip^^ i^H I^^B 1 -.'. i^^B „ 70.4 jH Ethylbenzene | I • Total Xylenes i ! • Chloroform | In Total i G:\003-6016\Golder\SVE TS Report MassLab.xls\Phllext ExtRate Golder Associates ^Ko Septemi^reoOO 0(^016 Figure 25 Phase II Extended Test Rate of Mass Extraction Photovac Data (Field GC) - Intake Port Virgin Island Chemical Site St. Croix, U.S. Virgin Islands CO o it^ U3 Ol to _ 1 > ^ • o 3 3 u nj I a: c 1 o ! ^-* ! o 2 ' re •^ 4 - * X LU :-V'i :-^i^* 0 S Ethylbenzene ^ Total Xylenes H Total 12 24 Time Sample Taken (Hours from start of test) 70 G:\003-6016\Golder\SVE TS Report MassField,xls\Phllext ExtRate Golder Associates Septembe nwc 003^^6 Figure 26 Phase II Extended Test Rate of Mass Extraction Microseeps Data (Lab) - Exhaust Port Virgin Island Chemical Site St. Croix, U.S. Virgin Islands CO o vo a\ CO fC/" 50.0 45,0 "^ 40,0 | _ 35,0 >^ i re 1 T3 j 3 30,0 ' re 1(2 25.0 i.i ' "^ 20.0 re X LU 15.0 10,0 5,0 •t i^^i,', 0,0 5,4 9,4 24,9 30,4 50,6 Time Sample Taken (Hours from start of test) 11 Ethylbenzene H Total Xylenes E3 Total 59.1 70,4 G:\003-6016\Golder\SVE TS Report I\/lassLab,xls\Phllext ExtRate - Exh Golder Associates iW2( Septemoir2000 00?6i OOT-6016 Figure 27 Phase II Extended Test Rate of Mass Extraction Photovac Data (Field GC) - Exhaust Port Virgin Island Chemical Site St. Croix, U.S. Virgin Islands CO o 50.0 45.0 40.0 _ 35.0 re S 30,0 0) 4-* a: 25.0 . ^ A m. " 20.0 re u * . » X LU 15.0 ^ 10.0 r'-' ' \ 5.0 10 24 31 36 48 Time Sample Taken (Hours from start of test) H Ethylbenzene a Total Xylenes (1 Total 51 71 G:\003-6016\Golder\SVE TS Report MassField.xls\Phllext ExtRate -Exh Golder Associates APPENDIX A Permits 304965 GOVERNMENT OF THE VIRGIN ISLANDS OF THE UNITED STATES Department of Planning & Natural Resources Division of Environmental Protection W.MER GUT HOMES 1118 CIlRIS'llANSTED, ST. CRODC 00820-5065 (809)773-0565 'PO November 23, 1999 Mr. Kevin M. Walsh Global Envirpiunent and Safety Director Pharmacia & Upjohn 7000 Portage Road Kalamazoo, MI 49001 REF: Soil Vapor Extraction System (New - A/C & P/O) Dear Mr. Walsh: Enclosed please find "Authority to Construct" Permit Number: STX-559-A-99-AC and "Permit to Operate" Permit Number: STX-559-A-99-PO for the construction and operation of a soil vapor extraction system at the former VI Chemical site located at Plot# 13Q Estate Bethlehem, Middle Works, St. Croix, USVI 00840. The above-mentioned permits will be valid for a period of ninety (90) days. The "Authority to Construct" and "Permit to Operate" are issued subject to the following binding conditions: I. GENERAL CONDITIONS A. Pharmacia & Upjohn must notify the Virgin Islands Department of Planning and Natural Resources-Division of Environmental Protection upon completion of construction prior to initiation of operation of the pilot remediation study project. B. "Authority to Construct" and "Permit to Operate" this source does not relieve Pharmacia & Upjohn of the responsibilities for compliance with the provisions of any Federal or Territorial requirements. 304966 STX-559-A-99-AC STX-559-A-99-PO November 23, 1999 n. OPERATING REQUIREMENTS A. The source shall only be operated in accordance with the conditions described in the application dated August 31, 1999 and supporting documents (Draft Final Treatability Study Workplan-May 1999) submitted by Pharmacia & Upjohn to the VIDPNR-DEP. B. The maximum flow rate of air from the soil vapor extraction system operation shall be two hundred and twenty five-standard cubic feet per minute (225 SCFM). An air flow rate meter shall be installed and operated to record and monitor the flow through the operation. C. The emissions from soil vapor extraction unit shall be not exceed the 13.62 lbs/day. D. The monitoring data shall be taken under the operating parameter (flow rate, temperature, air injection, etc.) conditions under which the soil vapor extraction system has been operating. If those conditions are a range, that range shall be recorded and monitoring data shall be taken at worst case conditions. E. Pharmacia & Upjohn must report to the VIDPNR-DEP any physical change or changes in operation which increases the amount of air pollutants or process production. F. Construction of the source must not result in the contravention of any ambient air quality standards, federal or territorial. G. During construction, any source responsible for contravening ambient air quality standards will be required to be modified to bring operation into compliance. H. The VIDPNR-DEP reserves the right to inspect the VI Chemical site. Pharmacia & Upjohn shall give the VIDPNR-DEP whatever aid is necessary to perform said inspections in a safe and timely manner. 3 0 4 9 6 7 STX-559-A-99-AC STX-559-A-99-PO November 23, 1999 m . MONITORING AND RECORDKEEPING A. All monitors, recorders and meters, as required by the permits, shall be installed prior to operation of the equipment. Pharmacia & Upjohn shall maintain and calibrate, in a manner consistent with the manufacturer's specifications, all monitors, meters, portable hydrocarbon analyzers and recorders as required above. All specifications must be made available to representatives of the VIDPNR-DEP upon request. B. Pharmacia & Upjohn must comply with the Monitoring Protocol for all monitoring equipment, which includes the Sampling and Analysis Plan and procedures outlined in the Quality Assurance Project Plan as submitted in the Draft Final Treatability Study Workplan to VIDPNR-DEP. C. The permits require that all monitors, recorders and meters be located in a manner which allows easy access and visibility. D. The readings required for all portable monitors must be recorded and kept as per permit condition III.G. E. Flow rate readings shall be recorded with each set of data and kept as per permit condition III. G. F. Any deviation from requirements of Section II of these conditions shall be recorded. G. All records, required to be kept as part of the permit conditions, shall be entered in a permanently bound logbook with numbered pages, maintained on site for a minimum of two years after collection and shall be made available to representatives of the VIDPNR-DEP upon request. 3 0 4 9 6 8 STX-559-A-99-AC STX-559-A-99-PO November 23, 1999 rv. REPORTING REQUIREMENTS A. Pharmacia & Upjohn shall submit a written report to VIDPNR-DEP within thirty days after completion of pilot test operation. This report must contain the system operating data, measurements of the discharge flow rate of the extracted gas, the measurements of the concentrations of hydrocarbons in the extracted gas and any other pertinent information as a result of the evaluation of this operation. B. Any operation of the equipment which may cause off-property effects, including odors shall be immediately reported to the VIDPNR-DEP by Pharmacia & Upjohn in writing and by phone and/or telefax. C. Pharmacia & Upjohn shall report to the VCDPNR-DEP via telephone and/or telefax immediately upon determination any non-compliance of operating requirements directly related to emission limits, or any non-compliance specified in the conditions of this permit. D. Pharmacia & Upjohn shall submit to VIDPNR-DEP within 7 days a written report detailing the nature of the non-compliance of operating requirements directly related to emission limits, or any non-compliance specified in the conditions of this permit and the corrective measures instituted to bring the system into compliance with the requirements of this permit. IV. OTHER REQUIREMENTS A. Pharmacia & Upjohn shall post the name of the contact person, along with the address and phone number on a permanent, legible location on the work site, prior to beginning the work to be performed in accordance with this permit. B. The Soil Vapor Extraction System shall not cause any air contaminant to be present in the outdoor atmosphere in such quantity and duration which is, or tends to be injurious to human health or welfare, animal or plant life or property or would unreasonably interfere with the enjoyment of life or property, except in areas over which the owner or permittee has exclusive use of occupancy. C. The VIDPNR-DEP issues these permits on the basis of the equipment descriptions and operating procedures presented in the August 31, 1999 Application for Authority to Construct. If final design and operation of the equipment differ from those presented, this permit approval will become invalid. ( - - 3 0 4 9 6 9 STX-559-A-99-AC STX-559-A-99-PO November 23, 1999 D. A person who has been granted a permit under the provisions of the Virgin Islands Rules and Regulations (VIR&R) Title 12, subsections (a) and (b) of 206- 20, shall firmly affix such Authority to Construct Permit, an approved facsimile , or other approved identification bearing the permit number upon the article, machine, equipment or other contrivance in such a manner as to be clearly visible and accessible. In the event that the article, machine, equipment or other contrivance is so constructed or operated that the Authority to construct Permit cannot be so placed, then the permit should be maintained so as to be readily available at all times on the operating premises. E. The "Authority to Construct" permit shall expire ninety days after the date of its issuance, unless an application for extension, in the form of a letter to the commissioner, is made fifteen (15) days prior to the expiration date of the permit. F. Prior to the operation of the Soil Vapor Extraction System, Pharmacia & Upjohn will notify the DPNR-DEP in writing on the completion date of construction and proposed schedule of operation. G. The "Permit to Operate" permit shall expire ninety days after the date of notification of construction completion. Your cooperation in complying with these regulations will be most appreciated. Sincerely, ' ?:yean C. Plaskett, Esq. Commissioner, DPNR Enclosure: (1) Certificate: Authority to Construct (1) Certificate: Permit to Operate cc: Mollis L. Griffin, Director DEP APC Files 3 0 4 9 7 0 Government of The Virgin Islands of The United States V DEPARTMENT OF PLANNING & NATURAL RESOURCES DIVISION OF ENVIRONMENTAL PROTECTION St. Croix, Virgm Islands AIR POLLUTION CONTROL HALFTHORITY TO CONSTRUCT • PERMIT TO OPERATE For PHARMACIA & UPJOHN Permit No.STX-559-A-99-AC Pursuant to the provisions of Title 12, Chapter 9, Section 206, Sub-Section 20 of the Virgin Islands Code. This Permit is issued to: Pharmacia & Upjohn For the operation of the following: One (1) EG & G Rotron DR-6 Regenerative Blower/Compressor Located at: 13Q Estate Bethlehem, Middle Works, St. Croix In accordance with the application dated: August 31,1999 and in conformity with the statements and supporting data entered therein, all of which are filed with the Department and are considered a part of this permit. This permit shall be effective from the date ot-i-November 23, 1999 for a ninety day (90) period ending on: Februaryis, 2000. ^"~^\ / / f Commissioner 3 0 4 9 7 1 r Government of The Virgin Islands of The United States DEPARTMENT OF PLANNING & NATURAL RESOURCES DIVISION OF ENVIRONMENTAL PROTECTION St. Croix, Virgin Islands AIR POLLUTION CONTROL " \ •AUTHORITY TO CONSTRUCT PERMIT TO OPERATE For PHARMACIA & UPJOHN Permit No.STX-559-A-99-PO Pursuant to the provisions of Title 12, Chapter 9, Section 206, Sub-Section 20 of the Virgin Islands Code. This Permit is issued to: Pharmacia & Upjohn For the operation of the following: One (1) EG & G Rotron DR-6 Regenerative Blower/Compressor Located at: 13Q Estate Bethlehem, Middle Works, St. Croix In accordance with the application dated: August 31,1999 and in conformity with the statements and supporting data entered therein, all of which are filed with the Department and are considered a part of this permit. This permit shall be effective from the date of : notification of cprrtpletion of construction for a ninety day (90) period,efTding~oiTHl!larch 31, ^ 0 0 . \ J \ / \ \ ' TEAN C. PLASKETT. ESQ. Commissioner V 304972 '» GOVERNMENT OF THE VIRGIN ISLANDS OF THE UNITED STATES Departmini of Planning <£ Natural Rtsours^j Division of Environmental Prot«clio» WATER QUT HOMES 1118 B n i / A P T . 14-A CHRISTIANSTED, ST. CROIX Oqaao-SO-JS (340) 773-0583 WELL DRILLING PERMIT NEWPBRMtT(a) RENEWAL P£RMIT( ) to accordance with the provisiona of Title 12, Chapter 5, Virpi Islands Code, M air^ded, & Well Drilling p^mut is hereby issued to; (Name of Well Driller) (license Number) RO. Boi 19^3g Sim IMH. P.R. 00919-S336. r7S7V-792-89CW) (MaiHi^ Address & Telephone #) to drill .,gi .; „.„. wdlCs) St. flf|,f P a M J ^ M l ^—. to the plan submitted in application for this permit and approved by the well inspector, This pemut h grgiJtfid with tha follovwng conditiotis: 1. Well log shall be completed and delivered to the Office of the Commissioner of Plinniiig and Natural Resources within thirty (30) days alter the completion of the well drilling operation, for each hole driHed. 2. Each wall diall have aa opening of not less than 3/4 inch m diameter for the measurement of water level by means of a wsttad steel tape. 3. Water samples shall b« fornishad upon tm\\xmX. The Coroirassioaer of the Depanmisit of Piaimii^ and Nstufai Rasourcei shsdi have the p«ww to revoke or suspend this pfnnit upon finding, afier public notice and adequate hsaiing, th^ such revocation or suspension is in the public intsrest; provided, that any p^sons aggrieved by any such 304973 decision, of th« Comnru^sioin^ may appeal such decision to th« Board of Land Use Appeals within ten (10) days of t ^ decision, provided, furdier, tliat all decisions of the Conunissioncr shall ba final except upon findings by the Board of Land Use Appeals that the same was ^rived at by fi'sud or illegal means. This permit is vaEd from S^ttWlNr U, IP99 to S#ntemboir 23,2001 If a renewal is desired, the holder ]$ responsible fi»r making ap{^csti<?n for same without any notice &om dus OSes. In the event of failure to do so, it will be understood that the permit has expired. CoramissJoner i^ % WeM Driiiini Fersaii No. WDP-049-99 Reference: ...MilSg^lSlMMMsLSMm& address, tekpboae) Property Tis Numbar _ M ^ 304974 c^' C0YERNM8NT OP THE VIRCIN ISLANDS OF THS UNITED STATBS DEPARTMENT OF PLANNI^iG ANIl > ? A T U R A L R S S O U R O B S ZiUU Ana*'. Hop«. Chi-isUiJUiei / *S-A SiUte m»to. Chwlotij A a ^ | St, Croljf, g.S. VirgtJJ Ulsads 00680 St. ThomM. U.S. Virgitt teltada OOBqS_ 1 PERMIT APPUCATIOI^ CONTROL FQHM H I N F OR MA T i p N MWWTy J>gOHtWi P R O J E C imai^ . , I . i i i M i m i i i f/t^9 — - ^HOWS! SE AftCNT£CT LiSi. ,IS*l£jtoIl&r2i20. Fnojter lOSA-now — n o t NO,I RSTAnt ^Slyfe4« ^ Sy^UTt* Jlld^iMKi. <XLAMO< ^ T ^ ' ^ ^ sotviNc eitmtcTi TAX .^SaEISQfl't l6tNTir<C*T10N WUMlWi «l*u»tiofl, •(>**ol S4!i»lrke«rort, rflfljw? (ti»»it(«(fl« Willi). »ro4«f. t'»»tm«ftt, «<*^««* lasBNi^*, •!•. T?^^?;'^, /WTA(^ f**^.^ ^i^yy^<te>3^ ^ » ^ -y^tofr < f e ! S ^ ^ > ^ / S < f ^ y t W U C R E Q U I R E M E N T a J H ! R Y ^ERMjTi G MteivisisN D •vitciNa I'enMiT D HJITO/IIS OUTKICY ^ ^ < J O A H Y APPROVALS , *i« M-^LunoN sOfTHet - eoN%if(\>zr M •oujifroN eofiToai. - si>es>n AftNV COS? O'' INBWUftS , •l-itOlNO ^CRMlT S:¥ M A / M ^ M S C2M MIN9N V A M 6 e i U uA,jOm WATS') CSM MiHOa WATtta iAf.TH CHAMCC e!.SCTaCAl»IR«!T CNner cCNn^iANCt ftfit IMvicif ' i . « 3 HAlA«tO 9II0U^ 0»itl.UI«O lAjAWBOvl MATf^lAl. «e*(1£w •'UTo^ie jifTiVrtiT 'lUMSiNQ PS««T »y94.ie WATtn •ij»»i,v »vaT«u (0*9 Axe p^iVlWAf wMiviwoN PSiuiiNAur ivaoivitiON rttiM, ' .f<ajR»ioyNO «To«Aoe TAMK •',y!;;SN»/Kt«K(u7it)/T«ATMStffiw«(aj,?! •»TE« a(fCrt*«af/»oauTieN cowwa.! •.TCf! OMA^irY CtfttlriCATION I i : . sir.:!!)!; / i^Vnoiiiuno*! 1 lltSO'O . [ - , y i j r ^ " > — ^^...~ - \ - „ , — - "- '• 1 JPATC SENT I - —-• p™—*•""-—"• < ^ ^ ; « i — - • - • • —. ; -••- •- 1 • • - - • - • A^PSOVgiS b OdAlTAl. ZONK MANAMMCNT (cijbi) BY • " " " J " " ^ / " j . / j " / ^ •• . • „ J . . ™. . , J . „ . . . . • " " " _ _ _ : " ' • • • " J I CATT ' ^f^'^'fs 1 ^ ', rff J»A5D a' S / ^ i ^ - ^ i . D a F A R T M E N T U S E •*•••"•'" ' • ' ^ " l|ilf'"'r|n '•" ' I "-Tiriiimiir-'-Mpi [-1,1,11 II I.I mrmiKin III iT-riT in rn • - - ^ - - . . . j . , 'Jl '""' ''^"'" " " - r ^ . p * .. ..^ OAni^^icsgivto-.^ € y ^ / > \ ^ ^ _ ' A y ; O V < g Q !>ATi; :cunyt "l*IK..V*WllJ«.I»i." l:!i^ 1: it ^ ' m 3 0 4 9 7 5 m - ? ~ - i 3SS :w ?n77n,ir; p. on n I III Willi II u m i — iiwiii I ynmtiitmtmmmmm*BmmmtmMKmmmmiimMmmx^^ma^ialmSaiBmiiiamm''^IIBaitatiammm'' GorsmumT OP THE VIKGIN ISLANDS OF THKONITBO STATBS DBPARTMSNT OF PLANNINO AND NATURAL. RSSOURCUfi Xoracladsr or Plot 3 KUkj Caaiwr. iulta t i t taitU tA»i.'B Hiit^e. Clu-i«U*nAtad 4Q-A 5ft«t« Nlflcr, Cbtrlotl* iSMtttt Si, Cruiz, U,S. Vlr(la Islaads 00830 St. Thoaa*, U.S. Ylrgla Mtnia OOattt EARTH CHANGE TECHNICAL FORM! P R O J E C T I N F O R M A T I O N D rACAVAiiw n noAC auiLQiiia/RePAift G LANS su»i>iviwwi Q I M S RCMOVA^V^LANTIKU i:ii2i2J£ W!i,'T.r ogtCHiat ^wt TPTAC SCOPS. iNeuiaifia Trie tuo ReauLT OF TVIE Pfto^aao eeveL^M<NT{«)i yrcj^m art. '^^^ItPTfX-t^i'P.. Asonessi th« f i t * lAMtfan (M) dil mSfli, ya avatebi*, • gFF)ci/iu8i;eoiy»'aNMA.p a SITEfl-AH C FjiMA FUUC IMU,<MCi MtP S WATER HESOURCEB iMP D seoa«[^4TnI!aucT)a«l<waMM • TSPCOAMIMBMAP D ae<LM;RV«y.tdlLUAN D dMieiALteMNatUA* O- I / a t h«r»k»> »«.1lfy 1iha< te t h i btat ar Mii" inai/ladgA, all IntaitnaVan •MttmiiUd ta ««aurat« and «urr*nl. SOMATWRE SLDQKi ' / v * ae>!n9wt«agt tns< «h;« G»»i|4ttl*ri ylU ii* rcvftw^l tai* M f M l t U n M i «nil Miisf*<intiy witft U« VA I, Swing Bod* prfor to pR9i,*«t|nf, tt \t alio <Kor«ftl/ asknwvlwigvd ttiat 111* «WTiiT!«n^ af <h* V.), l » l a i l i f a<«,..>.,,«i.., 6Wtrl«« ar* i r j v . r»«r.>rn.»,4di^l*<. \ * •iPiHiIt. nn«l Mkh»rlk> *iiJ r x i x n a b U l l y <«r RSNA'OIRe or CVMH): Blg^tATUM or ACPUOANT/Aoe^ ctfttinoATraN ar AASHITECT,. OATSi OATb /,f/g/?l, •URVBVO* UOCMSe hAMKR: SOMATknCi OATSi E; Dtvi •nipg(»ii OTKW W«Wi(/tTIOf<; V. i. C O N S E R V A T I O N D t e T R I p T ,i/MMirt*rrtjr«fliiUiTtfiii9tinBfvuiiaiiv ^ aATia^AOTOftv 0 ui'iU'naf^Aorony fjHPiN0»/CQ>iei.uaiONS! t M t ^ / ^ k J 9 9i^x/^ r^^^^Ji j^^rr-ji A / ' ^ T- fi^) %, ^^.•^£,Z^^^.m4L^I^.t^4iM^ RCa£MMCNaATiaN3i I 11 iniiiiiniiiniifTiiniiiHiiiiiiiiiMiiiiii niiiiiiiiiiiiiu PAIS l>44« K W r MUIO M TU( ;«t(A HU^, WEU 9> Vi^ir^il ;^ ^M^ikj^ sesitt," wiWsiaiiifTMiuisijan j s w j W T O ^ r v » TKI ii>fa'*«.»M»Ty!»« w Eo^^ {CaCJtiattttywMgvM. MMUBHmnHfiCBQM ^vfK^-nan -ff^MMW^iTAi D E P A R T M E N T U S E * • • ' ' * * * " ' ' * * • " • iniiiMiiimMWii • i m ***!»,> TI.I 1 1 • • • • • • . • • • • • • i.i i n ii.n • n.i •»•»•• iini i »«>^*i^ . i t i i j j i i i v H n m a w ™' " ^ :££k..^^ \(llM<Ji)tAi^ SS-SHATVRS OF *N«PB5TCRi ^^^^^E!^S[ "^mw^. PSAMt FSGl I £g^ oisTwoT o»=tscTo« or piHwira,, < ^ ^ ^ L ^ sswamcMB or A^^ITKOVAI v»fLi Hjiaa' tmif Mmaar l l l l l l l i l l l l l l l l i r H l l i m i l l l M W B H B M ^ M B M a a vo o CO cinren CtlL, Inc. October 5, 1999 Mr. John Steffy 13 Chesapeake Landing Annapolis, MD 21403 RE: VIRGm ISLAND CHEMICAL SITE ST. CROIX, U.S. VIRGIN ISLANDS TREATABILITY STUDY IMPLEMENTATION Dear Mr. Steffy; We have been given approval by the U.S. Environmental Protection Agency to implement a soil vapor extraction (SVE)/air sparging (AS) pilot-scale study at the above-referenced site. Enclosed, you will find an application for a well drilling permit that must be executed by the property owner. The permit will serve as a generail application for all wells to be installed during the upcoming study. Twelve SVE wells, two AS wells, and 11 vapor monitoring points will be installed as part of the upcoming work. Additionally, one of the existing production wells, P-1, will be properly abandoned and replaced for fiiture monitoring purposes. Please sign the attached permit and return to McLaren/Hart in the enclosed pre-addressed FedEx envelope. Please use the airbill provided to ensure that package will be billed to McLaren/Hart. Thank you for your prompt attention to this matter and for your continuing cooperation. If you have any questions do not hesitate to call me at (908) 647-8111. Sincerely, Norma Eichlin Senior Engineer ^o» Attachment cc: Wilfredo Geigel Lori Singer, Esq. - Sills, Cummis, et al Terry Grimm.er - Berlex Kevin Walsh - Parmacia & Upjohn Jose Agrelot - ERTEC ' 304977 ' ,. . . 7 25 Independence Boulevard, Warren, New Jersey 07059 GOVERNMENT 0 ? t H £ VIRGIN ISLANDS OF THE UNITED STATES Dfpsrtmsii tfPkHf^^ Niinrsi Rtfonrca VATSRCirrHOMESIUS CKRBTIANSTID, «T, CROR eottfr-SOH AFFUCATION FOR PERMIT TO BEILL WELL U compUajvcc with Title 12. Cbi^««f 5, Virgin Isltods Code, the imdersisaftd NMOC of DriUa: & Lioease Kumbe ^TL KCffl -- tfflL-D13 ""^To. Box 1^1704 San Juan, ryitlo l i c g " UWiV-UW ~ ~ Miiiios Addr«^ _(2J7) 2n>S§09„_ „ . . ^ _ _ _ _ ^ _ _ _ _ _ _ _ _ _ _ _ _ , Jwr^y ajjplias for 4 permit to: ^ Drill a well 12 soil vapor extraction; 2 a i r sparging; 11 vapor ^ Dft^>«a «a ewsdl^ WdQ monijioring points; 1 TDonitoring well Cl^wuj lad r^uAi^ ta fsckting wsJl Berl«a Laboratori*»/Fhjraaci* Upjoluj 1pS5aj]5lSimberaad lalaad) ""^ ^ (Propely TEC J"iuaib«f) Tt* w»I?will b« drilW ts) Ae eppmximate d«|Kii cf2_3' (so fW lad ^-iii b^ J l i i ' ^ 4 ? 4 is ,., dUm^. It will have 5 f^^cf «sja|. csM^^ictsd of 5 ! i ! ! £ L _ _ _ , _ S T ^ i l i Z _ ^ ^ t o f sc-eaniag of ^'0^^" (desdlptioc ©f 9<af«a3) aad will hivs benict^lt^/cotxcrttg (gft>PQ4^ tvpg of caamg saalV Soil V&1J&S lstTsctioa/(Air Sj«Tgins) l^np^S of "¥,'«BI Thk laacbid sktei d^^Dp^ fflip &om CtdM&aJ S i r ^ } shows locstkia of ppj^sd v«ll i^tive to #dstifls buildis^* ©r oti^ physlal fbimsrffl, ih« k>«loa of s^dug "felHi m lh« pfs^ty or ^uty a^i£^}| propolis, ^ the loation of tU k330WB imsf^' of ssnifemmatlQa la &g vKsid^, 304978 Wen l>nEk| f&ak Afp lia^oa IfpurnpvHnbcifii«a3edbydrilI«,ar^crthcfoU<m«i|:5 ^ blo«*r-v*cuu«. <5H? Po». Pre^a.) CapAcityofPmnp Honepower Si« (QI'M) (HP) Oach«) Ateg AowioQ^ vsshas sixjeSaorfbna«£©ii4 itianHBCtod by tho well, fbrEa*tJofl yields fl£d quality, and cwicg K&d joxjoung ieuJk will be forwiided to the Divkiaa 6f Eoviioamcotd Protertlon within 30 days after ccmpJedon cf drilling operations. F « Cf $10.00 a «ttgd»d. ^died, plesjc make pey^bLe to the Govcnuaeat of the Virgin Islaadi), Si|a6to«cfPiiop«tyOwMr Date • WDL-0I3 Slgoiture of WtU Drills Driller'i Liceme No FOR DEPAJRTMENT USE ONLY: nATK; APPROVED: _ _ _ _ _ „ DISAPPROVED: REMARKS acd/or SPECIAL CONDITIONS; 12 2 11 1 soil vaoor ( air- sparging =xt;;rfic;tinr) wells (40 wp 1 1 =; C ? feet) vapor monitoring points (less monitoring well to rep lace old mnrnv than . .2S fppt - 25 .feet - production well - abov e war«=.,t:.,„^ph1p') various deoths) P-l( 98 feet) SION'ATLmB OF WBLL INSPECTOR: _ DMLLING PERMIT NO. (If approved):" 304979 GOVERNMENT OF THE VIRGIN ISLANDS O F THE UNITED STATES DepartmttisifFhniuni&Natiird Resources DiwiM^EnvlroimeiuaiPrplecUon WATSR GUT KOIiCeS 1118 aiRBTlAKSTBO, ST. CROSS: 00»0«»5 APPLICATION FOR PERMTF TO DRILL WELL In OQixipIiance with Title 12, Ch^ter S, Virgia Islands Code, the und^^sigaed « ' z*^ I - t ^ , I «-OMame of Driller &Lioetifle Number ^ p n ^ /y5J'3K ^^/vTi^'K f^/s. ^Q^/I-JA^X (7f2)7^:L^g?tK) Mailing Address her^y applies for a p^mit to: Telq}hone Number y_Dm.^l T fX f ll f"'"^ '^''^'^ A-V'^5 Deepea an csci^lng well Clean aad refuiblih an odsting wdi on the property: &Ali^ Jfi^^t^^H / Pifi^m^i'^ ( J j i ? ^ ^ 'iO»^ks, ^ ^ P ^ (Eat&te. Lot Kumber aad Jjland) property Tax Numb«r) Th? wdi will b* drilled to the apprcwdmste d^jth of^£jf dkm«t«r. It wQl have _«5 f@3t of cssmg, constmet&d of ^ feet of awi^ilflg of 0»OS'ti" (dwctlpti. 6s<»^>^f^£9^^^^ O^roposed type cf casiisg mi), I , . I . * - . " i . , • • . ! • . . . , . , - . . • • * • " « » - f * v . - . - ~ . - , • • > . , . . - • • , 1 . . . - . - . 3iJig*or-o<hwtphi^ieal_'i'^aftiP^^ E?^ ^1 304980 • • ' . - I * WdQ DdUiog F^asit A|>p!kidSoa Paga2 If pump will be instalW by driller, answer the following: 5 kH i>r^*^ " ^ ^ ^ ^ j (j[M f^ f^^. ) Capacity of Pump. (CffM) .Horsepoww^ Size (HP) (inches) A log showing fee various flrata cr foraoalions intMB««ted by fee well, fofmadon yields and qtiality, and casing aad scrceaiag details will be forwarded to the Division of Environmental Protsctioa within 30 days aft«r completion of driUing op^mtiocs. Foe of 510.00 is attaAed. (If check, please make payable to fee Government of fee Vu-gin Islands). pfrxope^ Owner ^ ^ ^ K rbf Well Driller FOR DEPARTMENT USE ONLY: mLzDLb Diilier's License No DATE: APPROVED: DISAPPROVED: KH^ARKS tnd/of SPECL\L CONDITIONS -A^/- Si^^i^jg^ M O T TT _ J L "E^^^S 2—xktsxx—c *y } - - SI<3jrATURE OF WBLL INSPECTOR; DRTLLJNG PERMIT NO. (If approved): . ;-;ri.-. t,. . . . . : . ' • ' I •;,. ..:•!, I .t;..t." - •-• t — I J ' J ; : . .,| ,. ., ,.^»i »• ,,,i }• • - .. jJ- M k i i : 3 0 4 9 8 1 GOVERNMENT Of THE VIRGIN ISLANDS OF THE UNITED STATES Depisnnttm tifPiMHiiq ^ Saiund Rtuwxa WA7SK CUT HOMES His CKRisn AMrr», JT. CR.o« eeaae-joM APPLICATION FOR PERMTT TO DRILL WELL hi compiiAAC* -with Titla 12, Chaptw 5, Virgin Islands Code, the underUgaed • Nwnc of DriUflr & UOGQM Number 'P.O. Box i^nol STO Jutp, rattU ikttc" w m - u w —" }>iailiafi Addresi i m ) 792-6900 Tel^hooe Numb^ her*y ajfpUea ft>r A p«rmitto: ^ Drill a'Well 12 soil vapor extraction; 2 air sparging; 11 vapor D e ^ s a aa ftajstiag VWdl monij:oring points; 1 monitoring well Cle«o and rt^sibiak tn sclMmg w ^ 031 the nroparty: (Ertsta, Lot Nuaba aad Islind) (Prcjperty Tax Number) th« wtlPvwIl b4 drilled to the appioximau d^^rth ofas' (SofW tad ^U b« J l i i " ^ ^ » , , s dUfflftsr. It will have 5 feetofcaaiag. ooog^ractadof ^ ^ ^^^^^ witirijl _ ^ t of »cr©6S3liijg of O'O^Q" (deaalptioo of scf^a) aad will Er.^ beatoait^/coiicratg (propo»«d typ« of dalag f«ii). Soli Vspor S3itTactioB/(Air S^atging) ?Uip<^ of W^l Hi* lUichsd aketdi (propes^ ma? fitam Cadastral Surv«?^) show* location of proj^aid w«U relative to *!dstla5 buildiaj* or otka" physic f^sturia, the Ip^jios cf editing « ^ i 00 fc« pft^aly or seajfey t^io«tit propaii^, tnd the locstioa of all kisown iouf©^' of oonfesninatjos io die vicbity. 304982 • ., / Wan DriSlai Tstnk Applfeadoa Ifpuiapwi]lb«ifi3tallodbydrill«r,ftn£^cftlicfolk.v«a|:5 "^ blcr«*r-v*cuu=. (5H? Po». Pre^a.) CipachyofPugip . Hongxwcr _ Size (QPM) (HP) OQch«) Alegii>owxc3gth« vsnota sti^iK'£»nu£oiU isim-Mctiekd b^* the well, fw^^ttica yields asd quslky, and casicg aad so^eaing ^i^&Hs vnti ht fonvurded to the Diviiiofi of Hcviroomeotd Protection within 30 dayj aSw cci^letioa cf drilliog op«-«tioiu. F« iifsio}i03itiadx^. (If diack, |H«ae makt payable to fee Govcmiaeat of fee Virgin Iilanda), "^^'^ Date • • WDL-013 Slgaature o^ W«U Drilte-~ Driller's Lic«i»e No FOR DEPAIRTMENT USE ONLY: IX4TE: APPROVED: DISAPPROVED: REMARKS aad/'or SPECIAL CONDITIONS; 12 soil y,^i^n|- extraction welLs fpnprnx ?S fopt- - above, watP.r.^fA] P"! 2 air- sparging wells (40 feet) • " j.1 vapor monitoring poioLS (less than 25 feet - various depths) 1 monitoring veil to replace old production well P-K 98 feet) SIQ^'ATUM or WELL INSPBCTOR: DRILLING PERMIT NO. (If ipproved);] 304983 SENT BY: 3-16-99 ; 11:32AiM ; BERLEX BIOSC i ENCES-* 9086478162;# 2/ 5 WACBSmLS €OVBK LBTTTSR Q MoMSiir • OstUtadMsa Q RaiBkrMiU PATfc ixpII^^JAA. /fe,i?fy J^S U.5J,?,-•,„2,LLdii,3sS>£l. raOMi 3^.^-0 {:!flu£i>H^ RXFEaENCfii JOB NO! f?'0(}V/ |IS(SI4liIL£QU03K& ^ / j L g j : ^ ^ J U L Z J J ^ fl^,,.,3f-g^ ? g^i?- <^^g»- X 4 PBapnosnw i-.«j.-aiMj^ffa»&<igii5Cfr.V.jw»ij>;»T,^ vivf.-vq-.»^n.>c^ -Bi-g-i-y^Tj; irOURBG£!rVBLI^TIiAK IBIS, H.fiASBOOHTAClUi AT (717)7$^ H B Mwgaatea amfifeei i tta!ac}i»h 304984 •pe'd SSSSEBiiB^L £T;3T 888T-9T-aa ^E-^'^ BY-- 9-16-99 ;ll;33AM ; BERLEX B10SC1E.NCES- 9086478162;# 5/ 5 16 8«piamb^, 189$ Mr, Kevin Waish Phtnrifidi & Upjohn Mr. Terry firlmmar Barlox Lai;>orttorit9 Subj#^ VICHSM prejAet St Croix, USV) - Property ownar ai^natura r«quirom«nt on wt>il drilling p«rmil «pf»llefitbn foim, ^nd rcquirsHRARts for dfimoilti^n pmnH Mr. Sy»d Syttdali, of ths USVi Dipt, of Planning and Natural Resourcefi (DPNR)st St. Croix Indicatfd on Sapt 14« 1998 that h]$ Oepfirlmsnt cannot soo^pt th« w«ii drWing permit vppiioiitlon form for the propoMd w^lls and vapor monitoring paints far the Sail Vapor £}(traet!cn lystam ($VE) to b« in8tal)«d at tha ViCHSM slid unieas It is sicnad by it^ prep^tt^ ommr or hii tegai r«pr8aentativ«r». Mr SyiKiaii slao indicated, that a tignod liacaimile Hax") is acceptable for this purpose. I wHI send each of you a oomptstad application form via fax for tHa ownar'a aignatufft. Plaa«« fstum the same as soon as petslbla to tiwi wMi may aubmit n ai e)q)«d)ant!y ae sciaible. Also on Sepi 14, Mr. 8y9«(»!! gniclovftfy trmngsd for 9 e ^ ioapaction with Mr. Gofdan Thomas, Building Parnnita Department DIractor, who is In charga of the evaluation of bom \\m Earth Change Permit (ECP) ind the IDemoiltion Permit <DP) within the DPNR. Mr. Thomas indioated that the ECP may t»e submlttdd with ERTECa algnaturt as representatives. I wi^ submit the £CF doeumentsiksn t&dsy. RdQirdlng the DP, Mr. Thomas Indicated that a detailed plan Is required apeing out the actions and activities that wtil be conducted at alts. H« vxprmmd oonc«rn about the testing and disposal prooadurea for the aboveground tanks, ir\4 aabestoa teatlng. tn addition, both Mr. Thomas and Mr. Syedaii expressed concern about fencing of the property and about a number of efnptlsd 6S-gallon sleet drums in the pramiiis (from previous drilling and sampling). The andilary doaimentation for the OP Is th9 «ame as tbr the ECP, and la already urKier ERT£C's possesion. if you have any qu«»Sonai, p!aas@ contact me at your earliest convenience. Julio §. Cardone Eftvlrommntal Scientist 304985 I I ) APPENDIX B Boring Logs and Well Construction Diagrams 304986 w • Q^ o m CO S Oi ^ o I O LU H- i liJ -J u. 5 < Q: o O il ^ o o o i n CN s o Golder Associates Depth \ in FEET i • 0 ^ J -i - - J ~: 5 ^ -i ^' J — 10-t 15-; H 20 4- -^ 25 t - 30 - Surf, i Elev, • 0 i 0 ' i -5 \ . \ -10 -15 i ! -20 i 1 ] -25 Well: AST AS-1 Elev,: nm •ps^i \-f.\-Concrete ^°i )°'i f:^ N , -j j-J I'M ' ' ] \' ' j i ^; i *J i ' \ \ \ ! 'j 1 ',j 1 \ \ \ , 1 ;'.i l.j i .'i !-'•: j •! ; - v - G r o u t ! '.i i'. 'i ; . ' L -' i • H ' \i ' ' • • ' . : : ".: r, ^ • • M' 1 ' ': 1 0 : "i : 0 :{|M • - : , . - . - LOG OF BORING AST AS-1 : Project f Project Number i Hole Depth \ Date Started '; Date Completed Vichem 003-6016 50' bgs 2/22/00 2/22/00 1 ^ Well Construction Information i i i WELL CONSTRUCTION i Date Started : 2/22/00 1 Date Completed ; Hole Diameter 2/22/00 6.25" ' 1 WELL CASING i Interval ' Material i Diameter i Joints 0' bgs- 47,5' bgs SCH 80 PVC 1" NA 1 WELL SCREEN \ Interval i Material i Diameter : Slot Size 47.5' bgs-49,5' bgs SCH 80 PVC 1" 0,040" i SAND PACK j Interval : 46,5' bgs- 50' bgs ; Type : #2 i BENTONITE SEAL i Interval : 44,5' bgs- 46,5' bgs i NOTES 1 ] • ' • • ~ " " - - (Paget of2) Drilling Company : Ertec Driller : Jose L, Morales Drilling Method : Hollow Stem Auger Geologlist/Office : M. Shorter / Warren Sampling Method : Split Spoon • ' ' ' ~ 1 304987 Golder Associates LOG OF BORING AST AS-1 , Project :i Project Number. I Hole Depth : Date Started : Date Completed Vichem 003-6016 50 ' bgs 2/22/00 2/22/00 (Page 2 of 2) Drilling Company Driller Drilling Method Geologlist/Office Sampling Method : Ertec : Jose L. Morales : Hollow Stem Auger : M. Shorter / Warren : Split Spoon Depth : Surf, in ! Elev, FEET i 0 .Well: AST AS-1 Elev,: 3 0 - ^ -30 3 5 - f - 3 5 40 - + -40 f - G r o u t 4 5 - - - 4 5 50-r-50 -Seal Sand Pack - Screen H— End Cap Weil Construction Information 1 WELL CONSTRUCTION \ Date Started Date Completed Hole Diameter WELL CASING • Interval : Material Diameter • Joints : WELL SCREEN • Interval ; Material Diameter i Slot Size SAND PACK : Interval Type ' BENTONITE SEAL ' Interval : NOTES 2/22/00 ; 2/22/00 6.25" 0'bgs-47,5'bgs SCH 80 PVC 1" i NA 47.5' bgs-49.5' bgs SCH 80 PVC 1" 0.040" 46.5' bgs- 50' bgs I #2 44.5' bgs- 46.5' bgs i Q: m 55-t- -55 6 0 - 304988 Golder Associates Depth : in FEET i 0-t- i 5-f 1 J 1 0 - i - 154 20 4 . 25 -i 30 -'• 35 - Surf. ' Elev. i 0 1 0 j -5 i -10 -15 -20 -25 -30 Well: AST GMP-1 Elev.: jjii ;o'r~Concrete - Grout / / ;--Seal A -A Sand Pack - Screen End Cap LOG OF BORING AST GiVIP-1 (Page 1 of 1) Project Project Number Hole Depth Date Started Date Completed Vichem 003-6016 30' bgs 2/24/00 2/24/00 Drilling Company Driller Drilling Method Geologlist/Office Sampling Method Ertec Jose L. Morales Hollow Stem Auger M. Shorter / Warren Split Spoon Well Construction Information 1 WELL CONSTRUCTION : Date Started \ Date Completed ! Hole Diameter 1 WELL CASING i Interval ; Material i Diameter , Joints j WELL SCREEN i Interval ! Material : Diameter j Slot Size i SAND PACK i Interval I Type : BENTONITE SEAL i Interval I i 2/24/00 2/24/00 6.25" 0' bgs- 28.85' bgs SCH 40 PVC 1" NA 28.85'bgs-29.85'bgs : SCH 40 PVC 1" 0.020" 27' bgs- 30' bgs #2 j 25' bgs- 27' bgs NOTES 304989 Golder Associates LOG OF BORING AST SVE-1 ; Project i Project Number i Hole Depth i: Date Started i Date Completed Vichem 003-6016 50' bgs 2/8/00 2/8/00 (Page 1 of 2) Drilling Company Driller Drilling Method Geologlist/Office : Ertec : Jose L, Morales : Hollow Stem Auger : B, Blum / Warren Sampling Method : Split Spoon • cc o CD T - > rt X <J h~ s - 1 LU <; Q: u o o: ^ IF o o (N OJ Depth in j FEET ; O-T- 5 — 10-4- J 1 5 - - 20 -i- • -j • 2 5 - - I - - 30 : Surf, Elev, 0 O X Q. < a: o O g o m Well: SVE-1 Elev.: DESCRIPTION REMARKS _:. 0 •10 -15 4- -20 -25 0.0 - 0.5': Vegetative debris 0,5 - 2.0': CLAY & SILT, brown and compact, mottled texture MH! MH: 2,0 - 4.0': CLAY & SILT, light brown and compact, mottled texture 4.0 - 6.0': CLAY & SILT, light brown and compact with some SAND • ^ - C L ; 6.0 - 8,0': CLAY, same as above, transition to clay with sand (25%), light brown 8.0 -10.0 ' : CLAY, light brown and compact with 10% sand sweet odor, aromatic transition to ^ clay with 25% ! sand at 7.5', ! odor j odor -2.5 -3.5 -4.5 Gcr:^^? 14 : 10.0 - 1 2 . 0 ' : CLAY, light brown, very compact with sand, gravel, and pebbles 12.0 - 1 4 . 0 ' : same as above ! odor —\ odor : M H i SM; SWi G M ' GM;' SPi ; M H i ML^ M 5 ;; 8 i; 7 ~\ 7 '••'. 1 1 i-Ni '! 4 •i 8 M l \ 8 71 8 J'j 13 '\i 15 l j 2 2 ;;: 15 j I 14 '''^ 17 l i 24 •: 22 i 12 ; 17 : 17 T-; g : 7 /• 11 :: 12 n 5 :' 7 M 9 ' 11 14.0 - 16.0' : CLAY & SILT, olive brown i odor 16.0 - 1 8 , 0 ' : SAND, medium with 10% silt & clay 18.0 - 20.0': SAND, coarse with gravel transition to clay 20.0 - 22.0': poorly sorted mixture of CLAY, SILT, SAND, GRAVEL,and PEBBLES, compact 22.0 - 24.0': same as above, CLAY & SILT dominate matrix wet, odor sand and gravel to clay at 19.75', odor odor odor ,—-rl9.5 24.0 - 26.0': SAND & GRAVEL, with clay and silt to clay, 10% sand compact 26.0 - 28,0': CLAY & SILT, light brown, compact 28.0 - 30.0': SILT, light brown -^ sand & gravel ' transition to ! clay at 25' I slight odor •i slight odor -24.5 - 30 Well Construction Information WELL CONSTRUCTION j Date Started ; Date Completed I Hole Diameter : WELL CASING ; Interval : Material Diameter : Joints WELL SCREEN Interval Material Diameter Slot Size SAND PACK Interval Type BENTONITE SEAL Interval SUMP Interval 2/8/00 2/8/00 6.25" 0' bgs- 4.5' bgs SCH 5,stainless steel 2" NA 4.5'bgs-19.5'bgs : SCH 5,stainless steel 2" 0.020" 3.5' bgs- #2 30' bgs : 2.5' bgs- 3.5' bgs 19.5'bgs-24.5'bgsl NOTES 304990 Golder Associates LOG OF BORING AST SVE-1 (Page 2 of 2) Depth ; Surf, in ; Elev. FEET : 0 30-!--30 ' Project i Project Number f Hole Depth i Date Started ;; Date Completed Vichem 003-6016 50' bgs 2/8/00 2/8/00 Drilling Company Driller Drilling Method Geologlist/Office Sampling Method Ertec Jose L. Morales Hollow Stem Auger B. Blum / Warren Split Spoon Well: SVE-1 Elev.: DESCRIPTION I REMARKS 35- -35 SM SM 40 - f -40 45 -^ -45 SM SM SM SM SM 50 — -50 55- -55 32.0 - 34,0': same as above, wet, brown SILT and SAND to GRAVEL, wet and brown clay & silt, wet plastic slight odor slight odor 34,0 - 36,0': same as above, and brown silt & sand to gravel, dry 36.0 - 38,0': same as above, brown sand & silt to clayey gravel, dry 38,0 - 40,0' : brown S T L T S S A N ' D I O " GRAVEL, wet and brown sandy gravel to silt,dry no odor no odor 40.0 - 42,0' : same as above, wet 42,0 - 44.0': same as above, wet and brown silt & clay, mottling dry 44,0 - 46.0': same as above 46,0-48,0': mottling dry brown CLAY and SILT, 48,0 - 50,0': same as above END OF BOREHOLE Well Construction Information i WELL CONSTRUCTION I Date Started I Date Completed 1 Hole Diameter ! WELL CASING I Interval I Material ; Diameter • Joints : WELL SCREEN Interval Material Diameter Slot Size SAND PACK Interval Type BENTONITE SEAL 2/8/00 2/8/00 6.25" 0' bgs- 4.5' bgs SCH 5,stainless steel 2" NA 4.5'bgs-19.5'bgs ; SCH 5,stainless steel 2" 0.020" 3.5' bgs- 30' bgs #2 Interval SUMP Interval : 2,5' bgs- 3.5' bgs 19,5' bgs-24,5' bgsj NOTES 60 304991 :j i Project i Project Number 1 Hole Depth < Date Started j Date Completed Vichem 003-6016 25 ' bgs 2/11/00 2/11/00 Drilling Company Driller Drilling Method Geologlist/Office Sampling Method (Page1 of 1) : Ertec : Jose L. Morales : Hollow Stem Auger : B. Blum / Warren : Split Spoon Golder Associates LOG OF BORING AST SVE-2 Depth in FEET Surf, Elev, o C/1 (1 V) 3 X Q < a: O o O ^ o m iGM? : M H I M H i i 10- -10 1 5 - f - - l 5 20 -20 MH; ; S P i S P ! S P i SM^ S M ! S M : G M : MH: MH 2 5 - 7 - 2 5 l i 8 :i;! 11 -|J 9 Tl 9 !i 8 M 11 jJ 14 i • 15 I: 15 : M 8 ? 18 h 21 !; 26i ;i 24i •i 24 : •••; 7 i .• 1 1 : ; 8 i J 6 : '\ 4 i ; 8 ; : 6 : : 7 ^ "' 7 ; 8 ; ; 9 i ; 7 ":•' 4 '• ••! 6 !i 10 ; 2 8 ': :•: 4 \ •il 12 i li 15 i !: 22 i n 10: V 17 : n 17; J 13 : !; 4 :" i: 5 i '' 8 : i^ 12^ p 11 i h 13 i ; 13 ' ;: 6 i, 12 DESCRIPTION REMARKS 0.0 - 2.0': reworked CLAY & SILT, mixed with stone, compact : 2,0-4,0' i compact 1 : 4.0-6,0' ; 6.0 - 8.0' CLAY & SILT, light same as above same as above brown, I i Well: SVE-2 Elev,: oi \6^ ^ . ( - ^ 2 odor present odor 8,0 - 10,0' : SANDY GRAVEL, light I present brown, silt (10%) 10,0 - 1 2 , 0 ' : same as above ; odor i present : odor 12.0 - 1 4 . 0 ' : same as above, grading ; present into sand & silt, compact p-l-2.5 r i " 3.5 j-i4-4.5 14.0 - 16.0': SILT and very fine sand, light brown moist 16.0 - 1 8 . 0 ' : SAND, very fine with silt, light brown i wet 18.0 - 20.0': SAND & SILT, light brown 20.0 - 22.0': poorly sorted mixture of SILT and CLAY with fine SAND and trace GFIAVEL 2 ' 2 . 0 ^ ^ . 0 ' T a l A Y &^ILT, brown^nd' olive green, compact —^^ wet wet wet -19.5 24,0 - 25,0': same as above i wet END OF BOREHOLE -24,5 -25 Well Construction Information WELL CONSTRUCTION Date Started Date Completed Hole Diameter WELL CASING Interval Material Diameter Joints WELL SCREEN Interval Material Diameter Slot Size SAND PACK Interval Type BENTONITE SEAL Interval SUMP Interval 2/11/00 2/11/00 6,25" 0' bgs- 4.5' bgs SCH S.stainless steel 2" NA 4.5'bgs-19.5'bgs SCH 5,stainless steel 2" 0.020" 3.5' bgs- 25' bgs #2 2.5' bgs- 3.5' bgs 19.5' bgs- 24.5' bgs NOTES 30 304992 Golder Associates LOG OF BORING AST SVE-3 1 : Project j Project Number j Hole Depth I Date Started ; Date Completed Vichem 003-6016 25' bgs 2/9/00 2/9/00 Drilling Company Driller Drilling Method Geologlist/Office Sampling Method (Page 1 of 1) Ertec Jose L. Morales Hollow Stem Auger B. Blum/Warren Split Spoon Depth ; Surf, i Elev. FEET ; 0 in o CO . 3 O X Q. < CC o O i DESCRIPTION REMARKS Well: SVE-3 Elev,: 10- -10 L0.0^0.5'_;jop-soil 1 0,5 - 2.0': Ct-AY & SILT with trace i sand, brown Topsoil to clay at 0,5 2.0 - 4,0': CLAY, with SILT, very compact with mottled texture, brown -2 2.5 \A\A 4,0 - 6,0': CLAY, with SILT and trace sand, brown 3.5 4.5 6.0 - 8.0 : CLAY with SILT, light brown with 5% sand and gravel 8.0 - 1 0 . 0 ' : same as above 15- -15 20 — -20 CL ! CL " X " / X / \ S M i • .; 1 ;SMi jii;;-! 10.0 -12.0': same as above, transition to poorly sorted mixture of CLAY/SILT with GRAVEL (50%) SM S P ' SP: s < C3 o 25 -; -25 4 8 9 11 3 2 3 5 7 7 9 10 6 7 7 10 5 i 5 '• 11 ; 14 ; 10 j 17 ! 24 I i s ! 30 I 12.0 - 14.0' : CLAY with SILT, light brown, compact 14.0 -16.0' : CLAY, brown to silt and fine sand, olive brown 16.0 - 1 8 . 0 ' : fine SAND & SILT grading into more medium sand and silt 18.0 - 20.0': SAND, fine with SILT (30%) and GRAVEL (15%), olive green 20.0 - 22,0': SAND and SILT grading into clay, with silt, light brown, compact and wet transition from clay to clay and gravel at 11' back to all clay at 12' transition clay to silt and sand at 15' fine sand/silt to medium sand/silt at 17,5' transition to clay at 20,5', wet .H .1 .R-i-19.5 22.0 - 24.0': poorly sorted mixture of SAND, SILT and GRAVEL, olive green odor 24,0 - 25,0': same as above — ; odor END OF BOREHOLE -24,5 -25 m 30 Well Construction Information WELL CONSTRUCTION Date Started Date Completed Hole Diameter WELL CASING Interval Material i Diameter Joints : WELL SCREEN ; Interval ; Material Diameter ; Slot Size i SAND PACK Interval Type BENTONITE SEAL 2/9/00 2/9/00 6,25" 0'bgs-4,5'bgs SCH 5.stainless steel 2" NA 4.5'bgs-19,5'bgs '• SCH 5,stainless steel 2" 0.020" 3.5' bgs- 25' bgs #2 Interval SUMP Interval : 2.5' bgs- 3.5' bgs : 19.5' bgs-24.5' bgs NOTES 304993 Golder Associates LOG OF BORING AST SVE-4 (Page 1 of 1) Project Project Number Hole Depth Date Started Date Completed Vichem 003-6016 25' bgs 2/9/00 2/9/00 Drilling Company Driller Drilling Method Geologlist/Office : Ertec : Jose L. Morales : Hollow Stem Auger : B, Blum / Warren Sampling Method : Split Spoon Depth in FEET Surf. Elev, 0 O CO 3 O I CL < a: o o 5 Well: SVE-4 Elev.: DESCRIPTION REMARKS MHi MHi M H : i S W I 10- -10 I M H i 15- -15 GM iMHI : M H : 20 - f -20 ! M H ; MH: GCf 25- -25 8 6 12 12 15 17 20 15 18 20 i 38 : 31 : 20 18 i 4 ^ 7 i 1 1 ~ 1 7 4 8 ; 11 \ 14 : 16 i 16 • 21 ; 23 11 : 7 ; 11 i 9 \ 7 ; 13 i 15' 15; 15; 17 : 18 : 17 : 5 :" 7 11 • 15i 20 i 18 ; 22 i 24 20 23: '• 0,0 - 2.0': CLAY & SILT, compact, 1 brown 2.0 - 4,0': same as above 4,0 - 6,0': CLAY & SILT with sand (5%),light brown, compact bH-2,5 -3,5 -4.5 6,0 - 8,0': poorly sorted mixture of SAND with angular PEBBLES, SILT & CLAY 8,0-10,0': trace 10.0 -12.0' : CLAY & SILT, brown, (ximpact 12.0 - 1 4 . 0 ' : CLAY & SILT, light brown with 10% sand and 5% gravel 14.0-16.0': CLAY & SILT, compact, : light brown ~r:rz—:'„"^7 '. V- • transition clay 16X1-18,0 : same as above, grading to fine sand at to fine sand with silt, olive green 18,0-20.0': no recovery 20,0 - 22,0' : CLAY & SILT, rusty brown, very compact 22.0 - 24.0': same as above ; 17.25' I ; possibly sand : falling out of spoon i wet — -• wet - - 1 9 . 5 24.0 - 25.0': poorly sorted mixture of CLAY with SAND & GRAVEL (20%) o o wet END OF BOREHOLE 24.5 -25 m 30 Well Construction Information WELL CONSTRUCTION Date Started Date Completed Hole Diameter WELL CASING Interval ; Material Diameter Joints WELL SCREEN Interval Material Diameter Slot Size SAND PACK Interval Type BENTONITE SEAL Interval SUMP Interval NOTES 2/10/00 2/10/00 6.25" 0' bgs- 4.5' bgs SCH S.stainless stee 2" NA 4.5' bgs-19.5' bgs SCH 5,stainless stee 2" 0.020" 3,5' bgs- #2 25' bgs 2.5' bgs- 3.5' bgs 19.5' bgs- 24.5'bgs 304994 Golder Associates LOG OF BORING AST SVE-5 (Page 1 of 1) Project Project Number Hole Depth Date Started Date Completed Vichem 003-6016 25' bgs 2/10/00 2/10/00 Drilling Company Driller Drilling Method Geologlist/Office Sampling Method : Ertec : Jose L. Morales : Hollow Stem Auger : B. Blum / Warren : Split Spoon Depth i Surf, in j Elev. FEET i 0 tn (1 (D 3 O X (L < (t o Well: SVE-5 Elev.: DESCRIPTION REMARKS O H - o M H : SM 5-T--5 MH- :MH SM 1 0 - r - 1 0 MHi MH 15 4-15 M L i S M : M H ; 20- -20 M H : !MH iMHi 25 - - -25 ! 3 i 4 I 5 : 10 •: 6 ':• 8 • 8 i 9 • 10 i 10 : 12 • 12 i 14 ; 11 : 11 i 11 ] 9 : 11 ' 6 ; 10 i 3 ; 12 '\ 14 ; 14 j ; 14 I 20 : 23 i ; 2 5 : : 4 i i 7 i I 14 i i 1 5 : ; 31 i : 25 i ! 15 i i 14 ^ i 5 i i 8 • : 9 i : 13 j • 5 i ; 5 - i 1 1 ' : 16i : 14 : i 15i : 2 3 i 28 : 6 ; 7 • 0,0 - 2.0': CLAY & SILT, brown, compact 2.0 - 4.0': SILT & SAND (fine), light brown, compact 4,0 - 6.6': CLAY & SILT brown and olive green, compact 6.0 - 8,0': CLAY & SILf, brown, compact X' f^r2 ; : ^ 2,5 r - t 3,5 +•^-4.5 8.0 - 10.0' :SAND & SILT, brown to clay, with silt, compact 1 0 , 0 - 1 2 , 0 ' : C L J ^ Y with SILT, compact brown to olive green —• sand & silt to ! clay & silt at 9' — ! odor present 12.0 - 1 4 , 0 ' : same as above transition silt to 14,0 - 1 6 , 0 ' : SILT, olive green, grading ^ gg^d at 15' into fine sand and silt 16,0 - 1 8 , 0 ' : fine SAND with SILT and GRAVEL (15%) transition to 18,0-20,0' : C L A Y & SILT, compact, : ciayat 18'-19' olive green \ •19,5 20,0 - 22.0': C L M & SILT olive green, compact 22.0 - 24,0': same as above, some rusty brown silt and sand in spoon tip wet : dry 24,0 - 25,0': CLAY & SILT with fine sand (15%), light brown END OF BOREHOLE -24,5 25 • Well Construction Information WELL CONSTRUCTION ; Date Started : Date Completed : Hole Diameter WELL CASING Interval Material Diameter Joints WELL SCREEN Interval Material Diameter Slot Size SAND PACK Interval Type BENTONITE SEAL Interval SUMP Interval 2/10/00 2/10/00 6,25" 0' bgs- 4,5' bgs SCH S.stainless stee 2" NA 4.5' bgs-19.5' bgs SCH S.stainless stee 2" 0.020" : 3.5' bgs- 25' bgs :#2 : 2.5' bgs- 3.5' bgs 19.5' bgs-24.5'bgs NOTES 30 304995 Golder Associates LOG OF BORING AST SVE-6 (Page1 of 1) Project Project Number Hole Depth Date Started Date Completed Vichem 003-6016 25' bgs 2/10/00 2/10/00 Drilling Company Driller Drilling Method Geologlist/Office Sampling Method Ertec Jose L. Morales Hollow Stem Auger B. Blum / Warren Split Spoon Depth FEET Surf Elev. 0 CO O CO 3 O X a. < cc o Well: SVE-6 Elev.: DESCRIPTION REMARKS i 5 - r - 5 ; S M ; MH 10- -10 MH: MH: SWi 15- -15 i S W I L L 20-f- 25----25 •SW^ M H ^ -20 i p ice' j G C GC 4 10 14 10 7 7 8 13 6 11 8 8 10 10 11 15 8 8 8 12 5 17 17 21 15 17 23 17 8 9 12 11 15 12 10 25 11 9 10 _ 16 X - , / 36 ? / / / 33 'P/''y 25 •/•y\ 25 7 ^ . 16 '•/"X 20 1 ^ 1 0 A A \ \ 4 -0,0 - 0 5 ' - top sniL 0,5 - 2.0': CLAY & SILT, brown, compact 2.0 - 4.0': CLAY & SILT with trace fine sand, brown, compact vV. 4,0 - 6,0': SAND, with SILT grading into clay with silt --; sand at 4'-5'. : clay at 5' -2,5 -3,5 -4.5 6.0 - 8.0': CLAY & SILT, lighL brown, compact 8,0 - 1 0 , 0 ' : same as above 10,0 - 1 2 . 0 ' : C U \ Y , with SILT transition to sand, fine to medium, orange brown l 2 , 0 - i T o ' : SAND, with GRA'^EL to angular peebles, trace silt 14.0 - 16,0' : SAND, coarse olive green with trace gravel & silt 16.0-^8.0': SAND, fine with silt (10%) and gravel (10%) clay to sand at 10.75' —i moist 18.0 - 20.0': CLAY & SILT, olive brown, compact 20.0 - 22.0': poorly sorted CLAY with SAND & GRAVEL (15%), compact, olive brown -19.5 22.0 - 24.0': same as above, grading to clay and silt, rusty brown and dense wet wet 24,0 - 25,0': same as above END OF BOREHOLE -H-24,S -—25 30- Well Construction Information : WELL CONSTRUCTION i Date Started i Date Completed i Hole Diameter : WELL CASING \ Interval I Material ; Diameter • Joints • WELL SCREEN Interval Material Diameter Slot Size SAND PACK Interval Type BENTONITE SEAL Interval SUMP Interval 2/10/00 2/10/00 6.25" 0' bgs- 4.5' bgs SCH S.stainless stee 2" NA 4.5' bgs-19.5' bgs SCH 5,stainless stee 2" 0.020" : 3.5' bgs- 25' bgs :#2 : 2.5' bgs- 3.5' bgs 19.5' bgs- 24.5' bgs NOTES 304996 Golder Associates Project Project Number Hole Depth Date Started Date Completed LOG OF BORING AST ViVIP-1D : Vichem : 003-6016 : 30' bgs : 2/14/00 : 2/14/00 (Page 1 of 1) Drilling Company Driller Drilling Method Geologlist/Office Sampling Method Ertec Jose L. Morales Hollow Stem Auger M. Shorter / Warren Split Spoon Depth I Surf, in i Elev, FEET i 0 0 ^ 0 Well: AST VMP-ID Elev.: i i fi'i—Concrete 5 - ^ - 5 1 0 - r -10 15-I--1S 20 - i - -20 25 -25 ,—Grout 30 •-• -30 4 - Seal A • - S a n d Pack -f - Screen — End Cap IX. m Well Construction Information ; WELL CONSTRUCTION : Date Started • Date Completed ; Hole Diameter i WELL CASING ! Interval : Material : Diameter ; Joints i WELL SCREEN Interval 1 Material '• Diameter : Slot i SAND PACK ' Interval : Type i BENTONITE SEAL : Interval 2/14/00 2/14/00 ! 6,25" 1 0'bgs-27.55'bgs SCH 40 PVC 2" NA 27,55' bgs-29,25' bgs ; SCH 40 PVC 2" 0,020" : 26' bgs-30' bgs #2 24' bgs-26' bgs NOTES 35- 304997 Golder Associates Depth I Surf, in ' Elev. FEET I 0 0 - ^ 0 4 - r - 4 Well:ASTVMP-1l Elev.: i^j |J:i •pi iii',1—Concrete (?! IC I " - Grout LOG OF BORING AST VMP-11 (Page 1 of 1) ; Project s Project Number : Hole Depth :: Date Started ; Date Completed Vichem 003-6016 15'bgs 2/17/00 2/17/00 Drilling Company Driller Drilling Method Geologlist/Office Sampling Method Ertec Jose L. Morales Hollow Stem Auger M. Shorter / Warren Split Spoon 8 ^ - 8 Well Construction i Information I WELL CONSTRUCTION 1 Date Started ; Date Completed ; Hole Diameter ! WELL CASING i Interval i Material : Diameter : Joints i WELL SCREEN 1 Interval j Material i Diameter ; Slot Size i SAND PACK '• Interval ; Type : BENTONITE SEAL i Interval 2/17/00 2/17/00 6.25" ! ; 0'bgs-12.55'bgs SCH 40 PVC 2" NA 12.55'bgs-14.2S'bgs j SCH 40 PVC 2" i 0.020" 11'bgs-15'bgs '. #2 9'bgs-11'bgs i NOTES A'ln h- Seal \XJ 12 H -12 Sand Pack - Screen - End Cap a; m 16----16 20 304998 Golder Associates -r -10 15- -15 -25 LOG OF BORING AST Vi\/lP-2D (Page 1 of 1) Project Project Number I Hole Depth ' Date Started ; Date Completed Vichem 003-6016 30' bgs 2/16/00 2/16/00 Drilling Company Driller Drilling Method Geologlist/Office Sampling Method ; Ertec : Jose L. Morales : Hollow Stem Auger : M. Shorter / Warren : Split Spoon o s < o 30 --- . 35 tn () cyl _) X n < tr o o O •i o CD DESCRIPTION Well: VMP-2D Elev.: REMARKS MHi MHI .0.0—0^.5'~conGrete-reinforced-witft 9/5'"-rit^F light brown CLAY & SILT, trace sand, dry, plasfic Z b - 4.0': lightirowrTcLAY & SILT,"' trace gravel, plastic, dry, little mottling ( dark to light brown) ;0 ,• ? 16'J ?* ^ ' M - 2 5 - r - 5 : M H ^ 4.0 - 6.0': light brown CLAY & SILT, trace sand, dry, plastic MH SC ' : 6.0 - 8,0': light brown CLAY & SILT, I trac» sand, dry, slight sweet odor 8.0 -10.0' : 1.0' same as above, no odor; 0.7' brown clay, some sand, dry; 0.3' brown SAND, moist M H : iMHi 10,0 - 1 2 . 0 ' : brown / light brown CLAY & SILT, trace sand, dry, slight odor 12.0 - 1 4 . 0 ' : 0.8~brown CLAY& STLT, dry; 1.2' light brown sand & silt trace ^clay, moist to wet 14.0- M H ' SP 20 — -20 ; p-- SCiA S C ; S C : 16.0': brown CLAY & SILT, , trace sand, moist to dry, odor at 15.8' i 16.0 - 1 8 , 0 ' : brown same as above, I dry (0,7'), 1.0' light brown medium to i coarse sand, some clay, wet; trace ;\silt and gravel • 18,0 - 20.0': brown medium to coarse : SAND, some clay, trace gravel, wet, \strong odor, wet • 20.0 - 22.0': 1.0' brown CLAY & SILT, i some medium to coarse sand, wet; \ 1.0' greenish / gray medium to coarse :\SAND, some clay, wet I 22.0 - 24.0': same as above (greenish iVgray), wet, slight odor • 24.0 - 26,0': 0' same as above, moist • to wet; 0,6' brown medium to coarse !\SAND, some silt, trace gravel, moist : 26.0 - 28.0': 1.5' same as above, dry \ to moist (mottling); 0.5' grayish green II fine to medium SAND & SILT, trace i>clay, dry / 1 28.0 - 30,0': same as above, no" odor, i wet END OF BOREHOLE -30 Well Construction Information I WELL CONSTRUCTION Date Started Date Completed Hole Diameter WELL CASING Interval Material Diameter Joints WELL SCREEN Interval Material Diameter Slot SAND PACK Interval Type BENTONITE SEAL Interval 2/16/00 2/16/00 6,25" 0' bgs-27.5S' bgs SCH 40 PVC 2" NA 27.55' bgs-29.25' bg: SCH 40 PVC 2" 0.020" 26' bgs-30' bgs #2 : 24' bgs-26' bgs NOTES i i . h"^^-!- : r-4 24 26 27.55 29,25 304999 Golder Associates I ; . : Project i Project Number i Hole Depth { Date Started i Date Completed LOG OF BORING AST VMP-21 (Paget of 1) Vichem 003-6016 15'bgs 2/17/00 2/17/00 i Drilling Company Driller Drilling Method Geologlist/Office Sampling Method : Ertec : Jose L, Morales : Hollow Stem Auger : M, Shorter / Warren : Split Spoon • oc O d > c^ CO l O r o 1 - trt u. S < Q; o o tK • F o o o I O OJ o I Depth i in FEET I 0 - T j 4 — 8 -; 12 — -; - 1 6 - ; _ ; 2 0 Surf, i Elev. 0 0 j -4 -8 -12 ; -16 Well: AST VMP-21 Elev,: ! " • • fi'j-- Concrete -Grout T-iP-A Seal -, — Sand Pack r-;-- Screen -End Cap Well Construction Information I WELL CONSTRUCTION I Date Started : Date Completed i Hole Diameter i WELL CASING i Interval : Material i Diameter Joints ; WELL SCREEN i Interval ' Material : Diameter i Slot Size ; SAND PACK 1 Interval i Type • BENTONITE SEAL i Interval 2/17/00 2/17/00 6.25" O'bgs-12.55'bgs PVC 2" NA 12.55'bgs-14.25'bgs SCH 40 PVC 2" 0.020" 11'bgs-15'bgs #2 9' bgs-11' bgs NOTES 305000 ^ 9 ^ V on o m e/j Oi a. 5 CM ^ X u LU f - ^ w UJ ul s < Q: O O w in CN s Golder Associates Depth i in FEET i 0-4- J 1 n 1 — ; • '! 2-+ -i _' -i 3 4- -: "^ -4 4 ^ " 5 T H -n —; -1 6 - 1 - ": - j / i 8 -- Surf. Elev, 0 0 -1 : -2 i -3 \ -4 -5 -6 i -7 i Well: AST VMP-2S Elev.: ^- IPi =ti I " ' i ~ Concrete i^"^ '"'I pi/] M/- r^^-Seal M>^ L^L4 ! • • . : • , i , ; :• .', 1- 1 :"'.G- i • • : . - • ' . i . r j f—Sand Pack • R—j—Screen ! • . : • - i i i ^ { : r-f—EndCap ;\_iL_.: LOG OF BORING AST VMP-2S ; Project ; Project Number ; Hole Depth • Date Started ; Date Completed Vichem 003-6016 5 ' bgs 2/17/00 2/17/00 I • i Well Construction Information i WELL CONSTRUCTION Date Started : 2/17/00 i Date Completed i Hole Diameter 2/17/00 6.25" i WELL CASING : Interval Material • Diameter Joints 0' bgs-2.5S' bgs SCH 40 PVC 2" NA WELL SCREEN : Interval ; Material \ Diameter i Slot 2.55' bgs-4.25' bgs SCH 40 PVC 2" ; 0.020" ; 1 SAND PACK : Interval : 1.5' bgs-5' bgs '• I Type : #2 • BENTONITE SEAL : Interval : 0.5'bgs-1.5'bgs . NOTES I ; 1 ' _ _...,_ (Paget of 1) Drilling Company Driller Drilling Method Geologlist/Office Sampling Method Ertec Jose L, Morales Hollow Stem Auger M. Shorter / Warren Split Spoon — . - - . „ . . . 1 305001 Golder Associates LOG OF BORING AST VIVIP-3D (Page 1 of 1) Project Project Number Hole Depth Date Started Date Completed Vichem 003-6016 30' bgs 2/23/00 2/23/00 Drilling Company Driller Drilling Method Geologlist/Office Sampling Method Ertec : Jose L, Morales : Hollow Stem Auger : M, Shorter / Warren : Split Spoon Depth in FEET Surf, i Elev. i w 0 ; tn o I < a: O j O : g i m ; DESCRIPTION REMARKS 0 - i M H I : M H : -5 ^MHi MH S M ; 10- -10 SP 15 -15 ; M H i SMi 20 -20 SMi SMi MHi 2 2 4 4 4 4 3 5 6 7 9 10 14 18 17 15 2 4 5 10 3 11 9 14 19 12 12 12 4 i 11 i 12 : 15 : 4 9 11 19 1 7 11 8 3 10 10 15 7 15 15 19 7 0,0 - 2,0': gray / brown CLAY & SILT, trace gravel, moist 2.0 - 4.0': same as above, mottling 4.0 - 6,0': brown SILT & CLAY, tarce gravel, dry 6.0 - 8.0': same as above, changing to sand & silt at nose 8 . 0 - 1 0 . 0 ' : 1.0' brown / black SILT & CLAY, dry; 1.0' grayish brown SILT & SAND, trace clay, dry 10.0 - 1 2 . ' : 0.6' same as above; 1,0' gray/ brown medium to coarse SANDY GRAVEL, dry no odor no odor no odor no odor no odor I no odor /• no odor 12.0 - 1 4 . 0 ' : no recovery after three attempts 25- o o 30- 25 i SP M L - i i MLii 30 : i 12 - 7 :- :i 8 i i: 7 1 ii 17; i: 11 : ; 11 : : M 3 : _ i J 15 : 14,0-16,0': 1.0'brown SILT & CLAY, trace gravel, dry; 1.0' grayish brown medium to coarse SAND & SILT, trace \ grave I, dry 16.0 - 18.0': same as above 18,0 - 20.0': 1,5' same as above, wet; 0.2' brown SILT & CLAY, trace sand, wet 20.0 - 22,6': grayish brown SILT & fine SAND, trace clay, moist 22,o'-"24'.0'To,9' brown SILT & CLAY, plastic; 1,0' grayish brown medium to coarse SANDY GRAVEL 24,0 - 26.0': 1.5' same as above, wet; 0.2' grayish brown medium to coarse SAND & SILT, trace clay, wet 26,0 - 28.0': grayish brown SILT, mottling, wet 28.0 - 30.0': same as above Well: VMP-3D Elev,: mk no odor no odor slight odor slight odor no odor slight odor no odor slight odor END OF BOREHOLE f^?! I f j - y r 23.4 -25.55 -26 •27.25 -^- 30 Well Construction Information WELL CONSTRUCTION Date Started Date Completed Hole Diameter WELL CASING Interval Material Diameter Joints WELL SCREEN Interval Material Diameter Slot Size SAND PACK Interval Type 2/23/00 2/23/00 6.25" O'bgs-25.55'bgs: SCH 40 PVC 2" NA 25.55' bgs-27.25' SCH 40 PVC 2" 0.020" 26' bgs- 30' bgs : #2 BENTONITE SEAL Interval 23,3' bgs- 26' bgs ; NOTES 35 305002 Depth ; Surf, in ; Elev. FEET ; 0 Well: AST VMP-31 Elev,: yi)- fa'i—Concrete 4 -h-4 -Grout X' • / • V i/1 \/) \. - i i ' • ./. A\ Y\ i/i Seal 12 -12 ; Project \ Project Number : Hole Depth \ Date Started ; Date Completed Vichem 003-6016 15'bgs 2/18/00 2/18/00 Drilling Company Driller Drilling Method Geologlist/Office Sampling Method Ertec Jose L. Morales Hollow Stem Auger M. Shorter / Warren Split Spoon Golder Associates LOG OF BORING AST VMP-3i (Page 1 of 1) Sand Pack - Screen — End Cap 16- -16 20 Well Construction Information i WELL CONSTRUCTION ' Date Started : Date Completed i Hole Diameter ; WELL CASING : Interval \ Material Diameter Joints WELL SCREEN Interval •. Material i Diameter ; Slot Size • SAND PACK • Interval i Type ; BENTONITE SEAL i Interval 2/18/00 2/18/00 6.25" O'bgs-12.55'bgs PVC 2" NA 12.55'bgs-14.25'bgs SCH 40 PVC 2" 0.020" : 11'bgs-15'bgs #2 9'bgs-11'bgs NOTES 305003 Golder Associates Depth in FEET 0 - + 0 Surf Elev. 0 Well: AST VMP-3S Elev,: Concrete i A. 1^--1 -Seal 2 " - 2 3-i- -3 LOG OF BORING AST VMP-3S (Paget of 1) ;; Project : Project Number j Hole Depth i; Date Started \ Date Completed Vichem 003-6016 5' bgs 2/18/00 2/18/00 Drilling Company Driller Drilling Method Geologlist/Office Sampling Method Ertec Jose L. Morales Hollow Stem Auger M. Shorter / Warren Split Spoon 4-r-4 : - Sand Pack ;—:r- - Screen 5 - f - 5 -End Cap Well Construction Information ; WELL CONSTRUCTION : Date Started : Date Completed : Hole Diameter WELL CASING Interval Material Diameter Joints WELL SCREEN Interval Material Diameter ; Slot SAND PACK Interval Type BENTONITE SEAL Interval 2/18/00 2/18/00 . 1 6.25" ! 0'bgs-2.5S'bgs SCH 40 PVC 2" NA 2.55' bgs-4.25' bgs SCH 40 PVC 2" 0.020" 1.5'bgs-5'bgs #2 0.5'bgs-1.5'bgs NOTES 6 -f -6 # 7 — -7 305004 Golder Associates LOG OF BORING AST VMP-4D (Page 1 of 1) ; Project > Project Number : Hole Depth i Date Started ; Date Completed Vichem 003-6016 30' bgs 2/23/00 2/23/00 Drilling Company Driller Drilling Method Geologlist/Office Sampling Method Ertec Jose L. Morales Hollow Stem Auger M. Shorter / Warren Split Spoon Well: VMP-4D Elev,: DESCRIPTION REMARKS 0 - i - 0 i : SM 2 I SM 5 J - - 5 ^MH • SW i -i l O - r J 15 — -10 -15 sw|v ; SM \ I i SM i r : SM :|. i'ii ; 1 M L : i M H ; 20 -''•• -20 IMHM:M i M H i h •; 25H--25 I SMi 1 | S M ; i • SM:; 30 -f -30 6 8 9 9 8 9 8 12 16 17 17 19 26 17 14; 14 ; 6 : 6 • 9 8 j 4 i 6 : 11 ! 10; 11 i 12 '. 14 j 14 i 4 ; 6 i 9 : 15i 6 : 14 ': 18 19 : 6 : 8 ; 9 ; 12i 6 i 10' 12^ 13 4 :' 7 • 11 ': 20 : : 17 I 10' .; 14 : • 17: : 3 : ': 9 ! 8 • ; 9 : • 9 ; 10 • 10 i 25 0.0 -2,0': brown SILT & SAND, some gravel, dry no odor 2.0 - 4,0' : 1.0' same as above; 1.0' brown i throughout / gray SILT & CLAY, mottling, dry \ borehole 4,0 - 6,0': brown SILT & CLAY, trace gravel, dry 6.0 - 8,0': brown fine SAND, some silt, dry 8,0 - 1 0 , 0 ' : brown fine SAND, dry H ^ 2 10.0-12,0': brown SILT & fine SAND, some gravel, dry 12,0 - 14,0' : brown SILT & SAND, trace clay, mottling, dry 14.0 - 1 6 . 0 ' : brown SILT & SAND, trace clay, dry 16.0 - 1 8 : 0 ' : brown SILT, some gravel, dry to moist in nose 18.0 - 20.0': light brown SILT & CLAY, trace gravel, stiff 20,0 - 22,0': gray SILT & CLAY, stiff 22,0 - 24,0': same as above 24.0 - 26,0': brown SAND & SILT, trace gravel, wet A] >- -24 26,0 - 28,0': same as above \A-X^2S.5Z - - ^ > ^ r 2 6 27.25 28.0 - 30.0': same as above END OF BOREHOLE 30 Well Construction Information ; WELL CONSTRUCTION ; Date Started : Date Completed ^ Hole Diameter : WELL CASING : Interval ' Material , Diameter : Joints i WELL SCREEN ; Interval Material Diameter ; Slot Size i SAND PACK ! Interval ; Type 2/23/00 2/23/00 6.25" 0' bgs- 25.55' bgs SCH 40 PVC 2" NA 25.55' bgs-27.25' SCH 40 PVC 2" 0.020" 26' bgs- 30' bgs #2 : BENTONITE SEAL : Interval 24' bgs- 26' bgs NOTES 35- 305005 Golder Associates Project Project Number Hole Depth Date Started Date Completed LOG OF BORING AST VMP-41 (Page 1 of 1) : Vichem : 003-6016 :15'bgs : 2/18/00 : 2/18/00 Drilling Company Driller Drilling Method Geologlist/Office Sampling Method : Ertec : Jose L. Morales : Hollow Stem Auger : M. Shorter / Warren : Split Spoon Depth Surf in : Elev. FEET • 0 Well: AST VMP-41 Elev.: 0 - 0 4 — - 4 8 - ^ - 8 Concrete •y- Grout Well Construction Information i WELL CONSTRUCTION | ! Date Started 1 Date Completed ; Hole Diameter ; WELL CASING ; Interval ; Material ; Diameter • Joints : WELL SCREEN • Interval -. Material Diameter '•: Slot Size 1 SAND PACK i Interval : Type ' BENTONITE SEAL : Interval 2/18/00 ! 2/18/00 6,25" I O'bgs-12,55'bgs PVC 2" NA 12.55'bgs-14.25'bgs i SCH 40 PVC 2" 0.020" j 11'bgs-15'bgs #2 ; 1 9'bgs-11'bgs NOTES Seal 12 -12 Sand Pack Screen -End Cap 16 . -16 Q. 20 305006 Golder Associates Depth : Surf, in : Elev. FEET : 0 1 —-1 Well: AST VMP-4S Elev.: >"°r- Concrete > Seal \.AA/}. 2 - f - 2 3 - • -3 Sand Pack - Screen LOG OF BORING AST ViVIP-4S (Page 1 of 1) ; Project i Project Number i Hole Depth • Date Started Date Completed : Vichem : 003-6016 : S' bgs : 2/18/00 : 2/18/00 Drilling Company Driller Drilling Method Geologlist/Office Sampling Method Ertec Jose L, Morales Hollow Stem Auger M, Shorter / Warren Split Spoon Well Construction Information \ WELL CONSTRUCTION ' \ Date Started : Date Completed ; Hole Diameter : WELL CASING Interval Material Diameter Joints ; WELL SCREEN I Interval i Material i Diameter i Slot ; SAND PACK • Interval i Type ' BENTONITE SEAL Interval 2/18/00 2/18/00 6,25" 0'bgs-2.55'bgs SCH 40 PVC 2" ; NA 2.55' bgs-4,25' bgs SCH 40 PVC ; 2" . 0.020" 1.5'bgs-5'bgs #2 0.5'bgs-1.5'bgs NOTES -^-End Cap 5 -- -5 6 -: -6 7-r -7 305007 k } k f CHI O l CQ (h (O ; X i t o C3 f F If) cn . o 1 Golder Associates Depth in FEET 1 ! °4 -i J 5-1- 1 "1 J 10 — 1 1 5 - r 1 20 -H -: 25 - Surf Elev. 0 0 -5 -10 -15 -20 1 ^ CO : O : CO 1 3 i i O X a s ? Project :i Project Number J Hole Depth |j Date Started l Date Completed i c i 5! DESCRIPTION o : i cn 1 i ': For 0-26.0', see boring log for i FPP-SVE-1 i i ; ; ': ; i i • j : LOG OF BORING FPP AS-1 : Vichem • 003-6016 48 ' bgs 2/21/00 2/21/00 1 REMARKS i : i \ ^ \ (Page 1 of 2) Drilling Company Driller Drilling Method Geologlist/Office Sampling Method Ertec Jose L. Morales Hollow Stem Auger M. Shorter / Warren Split Spoon Well: FPP AS-1 ; Elev,: Well Construction i Information . |j^=; l^y \ WELL CONSTRUCTION l°'= t'°; ! Date Started : 2/21/00 So'j '?'.,: • Date Completed : 2/21/00 hil l/i ! Hole Diameter : 6.25" r r i f:!"^ i WELL CASING ; • . ! ; . ; Interval :. -M • : Material : '.\ ]'. \ : Diameter *. :. ^ ' Joints 0' bgs- 45.5' bgs SCH 80 PVC 1" NA :•.";?.• 1 WELL SCREEN j ; • . ; ' . : Interval ; . • : . • : ! Material ' '.• j ' . i : Diameter *. ;. ' . Slot Size 45.5'bgs-47.5'bgs SCH 80 PVC 1" 0.040" ;•.'! ''. \ ] SANDP/\CK 1 i'.'; L ' interval : 44.5'bgs-48'bgs •. •: i - ; i Type :#2 L'-; ;'• ; ; BENTONITE SEAL '. ': i ' • Interval : 42.5' bgs- 44.5' bgs 1 • ' v K : ; NOTES 1 > ' : i ' i 1 ;. j 1,' i • i.'-il'-! ; •','• 1.' 1 : ;' i ' ' 1 k'' l,M i • • • ^ - - ' ' - 2 5 - - - ... 1 305008 Golder Associates LOG OF BORING FPP AS-1 (Page 2 of 2) • Project ; Project Number i Hole Depth • Date Started : Date Completed Vichem 003-6016 48' bgs 2/21/00 2/21/00 Drilling Company Driller Drilling Method Geologlist/Office Sampling Method Ertec Jose L. Morales Hollow Stem Auger M. Shorter / Warren Split Spoon Depth i Surf. I Elev. FEET i 0 in CO o CO 3 o I Q. < tr o o : O i 5 ; .2 i 00 i DESCRIPTION REMARKS Well: FPP AS-1 Elev,: 2 5 - - - 2 5 30 -i- -30 35 -35 40 - t -40 45 -45 transition to gravel and sand at 27' transition into clay/sand and gravel at 32.5' •42.5 -44.5 - ; - : f 45.5 U i ,S.-i49.5 _U...l.4g Well Construction Information WELL CONSTRUCTION : Date Started : Date Completed \ Hole Diameter • WELL CASING Interval Material Diameter Joints WELL SCREEN Interval Material Diameter Slot Size SAND PACK Interval Type BENTONITE SEAL Interval NOTES 2/21/00 2/21/00 6.25" O'bgs-45.5' bgs SCH 80 PVC 1" NA 45.5' bgs-47.5' bgs SCH 80 PVC 1" 0.040" 44.5' bgs- 48' bgs #2 42.5' bgs- 44.5' bgs 50 305009 • _ • a: s ci. X o liJ 1- 5 5) L U - J < cc o o on CN o Golder Associates i Depth ! in \ FEET 1 0 - - -; 5 — _; 1 0 - r -j I5J- 20 - 25 4 i 3 0 - f 35 -j Surf, : Elev. 0 i 0 i -s - 1 0 [ - 1 5 1 ! -20 I -25 1 -30 Well: FPP GMP-1 Elev.: I 'M •.•; :-1 r]-j • . ; ] . ' • : I'M ['•[ !'•.• hi M ! • ' : : - ^ p - Concrete - Grout -Seal -Sand Pack Screen -End Cap ll LOG OF BORING FPP GIVIP-1 i; il ] Project I Project Number 1 Hole Depth Date Started i Date Completed Vichem 003-6016 30' bgs 2/24/00 2/24/00 j 1 i 1 i i Well Co i Inforr nst Tia ruction ; tion i : WELL CONSTRUCTION i Date Started : 2/24/00 ^ Date Completed : 2/24/00 : : Hole Diameter : 6,25" \ ] WELL CASING \ • Interval i Material ' Diameter ! Joints 0' bgs- 28.85' bgs SCH 40 PVC 1" NA I WELL SCREEN • • Interval ': Material i Diameter 1 Slot Size 28.85' bgs-29.85' bgs : SCH 40 PVC 1" 0.020" ! SAND PACK : Interval : 27' bgs- 30' bgs 1 \ Type : #2 ; BENTONITE SEAL ; Interval : 25.5' bgs- 27 bgs 1 ;NOTES i i i ; 1 ! \ ; '•• • 1 (Paget of 1) Drilling Company Driller Drilling Method Geologlist/Office Sampling Method Ertec Jose L. Morales Hollow Stem Auger M. Shorter / Warren Split Spoon 305010 Golder Associates LOG OF BORING FPP SVE-1 (Page 1 of 1) Project Project Number Hole Depth Date Started Date Completed Vichem 003-6016 48 ' bgs 2/1/00 2/1/00 Drilling Company Driller Drilling Method Geologlist/Office Sampling Method Ertec Jose L. Morales Hollow Stem Auger B. Blum / Warren Split Spoon a: m Depth in FEET 0 - Surf Elev. 0 - 0 10-4--10 15-i--15 20 - r -20 25- -25 30 C/5 o CO 3 O X Q. < (3 o i O i 5 \ _o i CD ; DESCRIPTION REMARKS Well: SVE-1 Elev.: S S S i e L0,0 - 0,5!.:.Concrete FL CL: C L ; C L i C L ; C L ; CL C L ! SPr SC C L i 0.5 - 2.0': Fill, SAND & SILT with gravel 2.0 - 4,0': Fill grading into light brown clay at 2,5' 4.0 - 6.0': CLAY, light brown 6.0 - 8.0': CLAY, light brown, 10% sand & 10% silt; moist @ 7' -: r - r 3.5 -6.5 8.0 - 1 0 . 0 ' : CLAY, light brown, less moist than above, 10% sand 10.0 - 12.0': CLAY, same as above, 10% sand 12.0 -14.0': CLAY, same as above, 10% sand compacted 14,0 -16.0': CLAY, same as above, 10% sand compacted 16.0-18.0': CLAY grading to sand, fine to medium with 40% clay and 5% gravel 18.0 - 20.0' : SAND, GFJAVEL with silt & clay, 40% wet — Transition 20.0 - 22.0': same as above grading • ^^^^^ jg (,|gy g^ into CLAY, light brown with 15% : 20 s' sand, wet 22.0 - 24.0' : CLAY, light brown with 10% sand, wet 24.0 - 26.0': CLAY, same as above with 10% sand, moist -21.5 END OF BOREHOLE 26.5 Well Construction Information WELL CONSTRUCTION : Date Started '• Date Completed i Hole Diameter ; WELL CASING Interval Material Diameter Joints ': WELL SCREEN Interval Material Diameter ; Slot Size : SAND PACK • Interval : Type ; BENTONITE SEAL i Interval : SUMP Interval NOTES 2/7/00 2/7/00 6.25" 0' bgs- 6.5' bgs SCH 5,stainless stee 2" NA 6.5' bgs- 21.5' bgs SCH 5,stainless stee 2" 0.020" 5' bgs- 26.5' bgs #2 3.5' bgs- 5' bgs 21.5'bgs-26.5'bgs 305011 Golder Associates \ LOG OF BORING FPP ViVIP-ID i; Project \ Project Number ;i Hole Depth ; Date Started Date Completed i i Depth ! Surf, i in i Elev. FEET ; 0 o 4 0 J 5 ~r--5 -; j ! 10 T -10 15----15 \ 20-}--20 25 - - -25 I 30 i -30 35 -i Well; FPP VMP-ID Elev,: \ = j i o 1 ; . : ; . • ! i-J -_'J ; - J !-_•]- ': i ' } ' ."i L'-i I: . A ^ - T -Grout -Seal Sand Pack Screen End Cap Vichem 003-6016 30' bgs 2/7/00 2/7/00 i Well Construction Information i WELL CONSTRUCTION i Date Started Date Completed ; Hole Diameter WELL CASING : Interval - Material i Diameter ; Joints WELL SCREEN ; Interval i Material • Diameter : Slot Size i SAND PACK Interval \ Type ; BENTONITE SEAL : Interval : NOTES • The well came up 0.; 2/7/00 2/7/00 6.25" i 0' bgs- 27.3' bgs SCH 40 PVC 2" NA 27.3' bgs- 29' bgs SCH 40 PVC 2" 0.020" ; 26' bgs- 30' bgs #2 24' bgs- 26' bgs !5' during construction (Paget of 1) Drilling Company Driller Drilling Method Geologist/Office Sampling Method Ertec JL. Morales Hollow Stem Auger B.Blum/Warren Split Spoon 305012 Golder Associates Depth in FEET O-M Surf. Elev. 0 Well: FPP VMP-I I Elev.: Jii j6'; -Concrete ,*! ; i ' : -Grout 8 ^ - 8 ^P IZ Seal LOG OF BORING FPP ViVIP-l I (Page 1 of 1) Project Project Number Hole Depth Date Started Date Completed Vichem 003-6016 15'bgs 2/21/00 2/21/00 Drilling Company Driller Drilling Method Geologlist/Office Sampling Method : Ertec : Jose L. Morales : Hollow Stem Auger : M. Shorter / Warren : Split Spoon Well Construction Information WELL CONSTRUCTION Date Started Date Completed Hole Diameter WELL CASING Interval Material Diameter Joints WELL SCREEN Interval Material Diameter Slot Size SAND PACK Interval Type BENTONITE SEAL Interval 2/21/00 2/21/00 6.25" O'bgs-12.55'bgs SCH 40 PVC 2" NA 12.55'bgs-14.25'bgs i SCH 40 PVC 2" 0.020" 11'bgs-15'bgs #2 9'bgs-11'bgs NOTES 12-i--12 - Sand Pack Screen -End Cap 16- -16 m 20 305013 Golder Associates Project Project Number Hole Depth Date Started Date Completed LOG OF BORING FPP VMP-2D (Paget of 1) Vichem 003-6016 30' bgs 2/4/00 2/4/00 Drilling Company Driller Drilling Method Geologist/Office Sampling Method Ertec JL. Morales Hollow Stem Auger B.Blum/Warren Split Spoon Depth ; Surf, in i Elev. FEET ' 0 10 -10 15- -15 20 --i- -20 25 - r -25 o o 30- -30 35 tn o cr) 3 O X CL < tr O 3 : O i ^ o m ; Well: VMP-2D Elev,: DESCRIPTION REMARKS 0 f-. 0.0 - 0,5': concrete 0.5 - 2,0': CLAY, light brown with sand (15%), compacted M - 2 2,0 - 4.0': same as above 4,0 - 6,0': CLAY, light brown with silt & sand (10%), compacted 6,5 sand & C L ' / scK CL^ S P : 6.0 - 8,0': SAND, coarse and gravel ' gravel 6 5-7 5 transitiion to clay, with sand and back to sandy gravel, then clay again clay. 7.5-7.75, sand & gravel, 8.0 - 10.0': CL>\Y, light brown with silt ! 7.75-8 clay &sand(15%) j — I less wet 10.0 -12.0': CLAY, same as above 12,0 -14,0': CLAY, same as above 14,0 - 1 6 , 0 ' : CLAY, same as above less moist with depth moist 16.0 -18,0': CLAY, with gravel and pebbles (20%), compact and moist 18,0 - 20,0': GRAVEL and SAND, poorly sorted with clay(50%) 20,0 - 22,0': GRAVEL and SAND with : clay (50%), transitioning into clay with gravel & sand(25%), compact SWi ^^^'P/'i 15 22,0 - 24,0': CLAY, light brown, compact and mottled with green ^streaks, sand & silt (10%) 24^"-'2aO~~GRAVEL & SAND7brown with 20% clay 26.0 - 28.0': coarse SAND and GRAVEL with silt & clay (10%), clay in tip of spoon i s ' o ^ ^ O ^ C L A Y with'40% S A N D " " " &GRAVEL to clay with 15% sand & gravel, wet transition to sand & gravel at 18' Transition from sand & gravel to clay at 20.5' dry '. moist sand & gravel at 24' \ wet clay at 28' transition to more clay at 29.5' END"OF BOREHOLE 22 -24 -27.S5 -29.25 -30 Well Construction Information WELL CONSTRUCTION j Date Started ; Date Completed i Hole Diameter i WELL CASING '. Interval : Material Diameter Joints WELL SCREEN Interval Material Diameter Slot Size SAND PACK Interval Type BENTONITE SEAL Interval 2/7/00 2/7/00 6.25" 0' bgs- 27.55' bgs SCH 40 PVC 2" NA 27.55' bgs-29.25' bg SCH 40 PVC 2" 0.020" 24' bgs- 30' bgs #2 22' bgs- 24' bgs NOTES 305014 Golder Associates LOG OF BORING FPP VMP-21 (Paget of 1) ; Project \ Project Number > Hole Depth i Date Started ! Date Completed Vichem 003-6016 15'bgs 2/21/00 2/21/00 Drilling Company Driller Drilling Method Geologlist/Office Sampling Method : Ertec : Jose L, Morales : Hollow Stem Auger : M, Shorter / Warren : Split Spoon i Well: FPP-VMP-21 Depth : Surf. I Elev,: in ; Elev, FEET ! 0 ! 5 ^ - 5 - Concrete !• H- -j—Grout I • j i" ' J Well Construction Information i WELL CONSTRUCTION : Date Started ; Date Completed I Hole Diameter i WELL CASING ; Interval • Material ; Diameter I Joints 1 WELL SCREEN 1 Interval '• Material • Diameter Slot Size SAND PACK ' Interval I Type ; BENTONITE SEAL i Interval 2/21/00 ; 2/21/00 6,25" O'bgs-12.55'bgs SCH 40 PVC i 2" NA 12.55'bgs-14.25'bgs ^ SCH 40 PVC 2" 0.020" 11'bgs-15'bgs #2 : 9'bgs-11'bgs NOTES 10-^-10 \/:\A i~Seal 15-f-15 Sand Pack Screen End Cap 20 305015 Golder Associates Depth : in FEET ; 0-i- 1 ~ - 2 - r J 3 ^ - 4--i- 5 ^ 6n- 7 :- Surf j Elev. i 0 i 0 i -1 i i -2 -3 1 -4 -5 -6 -7 i Well: FPP VMP-2S Elev.: ?-" i-A}- Concrete <ii \A\ -Seal - Sand Pack - Screen ;---i— End Cap LOG OF BORING FPP ViVIP-2S (Page 1 of 1) Project I Project Number : Hole Depth J Date Started , Date Completed : Vichem : 003-6016 : 5'bgs : 2/21/00 : 2/21/00 Drilling Company Driller Drilling Method Geologlist/Office Sampling Method : Ertec : Jose L. Morales Hollow Stem Auger M, Shorter / Warren : Split Spoon Well Construction Information : WELL CONSTRUCTION '• Date Started ; Date Completed : Hole Diameter \ WELL CASING i Interval : Material • Diameter : Joints i WELL SCREEN i Interval : Material Diameter Slot SAND PACK Interval : Type : BENTONITE SEAL Interval 2/21/00 2/21/00 6,25" 0' bgs-2,55' bgs ' SCH 40 PVC 2" NA 2,55' bgs-4,25' bgs SCH 40 PVC 2" 0.020" 1.5' bgs-5'bgs #2 O.S'bgs-1.5'bgs NOTES 305016 Golder Associates LOG OF BORING FPP VMP-3D (Paget of 1) Project Project Number Hole Depth Date Started Date Completed Vichem 003-6016 30' bgs 2/2/00 2/2/00 Drilling Company Driller Drilling Method Geologist/Office Sampling Method Ertec J.L. Morales Hollow Stem Auger B Blum/Warren Split Spoon DESCRIPTION REMARKS Well: VMP-3D Elev.: Well Construction Information 15- -15 20 -20 25 -25 30 C L i i^O.O - 0.5': concrete _ i 0.5 - 2.0': CLAY, compact light brown l^with sand (10%) : 2.0 - 4,0': CLAY, compact light brown ; with sand (10%) CL: ! 4 , 0 - 6 , 0 ' : same as above (15%) C L . -10 : -; 6,0 - 8,0': same as above, mottled texture 8.0 -10,0': same as above, mottled texture •; three pictures j taken of this • sample -• two pictures taken of this sample CL 10,0 - 1 2 , 0 ' : CLAY, with sand & silt (25%), compact light brown S C t / - SP SP SP: 12,0 - 1 4 . 0 ' : same as above transition to 14.0 - 1 6 . 0 ' : SAND, coarse and gravel : ggnd & gravel with silt & clay (15%) light brown i gt 14' wet 16.0 -18.0': same as above wet CL CL^ CL^ I 18.0 - 20.0': SAND and GRAVEL as I; above, transition to clay, compaction ' j with sand & gravel(15%), light brown ! 20.0 - 22.0'; CLAY with sand & gravel i: (15%) to clay with silt and fine sand ' 1^(20%) _ _ i 22.0 - 24.0': same as above, clay i: with 15% silt & sand 24,0 - 26.0': CLJOIY with 15% silt & sand, transition to sand & gravel with 25% silt & clay 26,0 - 28,0': SILT and fine SAND, light brown to clay with 20% sand & gravel 2 8 , 6 " ^ , 0 ' ~ : CLAY with 15% siTt and trace fine sand -30 ;- 1 transition to clay at 18,5' CL^Y with less sand & gravel at 20,5' ; transition to sand & gravel at 25,75' transition to silt ; & sand at 26'. thento clay at 27' 'END OF BOREHOLE i- •* : ; " • : \ : '. i 1 A \ • • , J M ' : -r-'-i 22 24 27.55 29.25 30 WELL CONSTRUCTION : Date Started Date Completed I Hole Diameter • WELL CASING Interval Material ; Diameter Joints WELL SCREEN Interval Material Diameter Slot Size SAND PACK Interval Type BENTONITE SEAL Interval 2/3/00 2/3/00 6.25" 0' bgs- 27.55' bgs SCH 40 PVC 2" NA 27.55' bgs-29.25' bg; SCH 40 PVC 2" 0.020" 24' bgs- 30' bgs #2 22' bgs- 24' bgs NOTES 35 305017 Golder Associates LOG OF BORING FPP VMP-31 (Paget oft) ; Project I Project Number : Hole Depth ; Date Started j Date Completed Vichem 003-6016 15'bgs 2/21/00 2/21/00 Drilling Company Driller Drilling Method Geologlist/Office Sampling Method Ertec Jose L. Morales Hollow Stem Auger M. Shorter / Warren Split Spoon Depth ] Surf, in i Elev. FEET ; 0 Well: FPP VMP-31 Elev.: A\— Concrete r-Grout y-- y-: 1/1 i/r-Seal 12-^- -12 Sand Pack Screen End Cap Well Construction \ Information i WELL CONSTRUCTION ; Date Started i Date Completed j Hole Diameter ', WELL CASING Interval Material Diameter : Joints i WELL SCREEN 1 Interval ; Material : Diameter j Slot Size ! SAND PACK ': Interval j Type ' BENTONITE SEAL i Interval 2/21/00 2/21/00 6.25" i O'bgs-12.55'bgs : SCH 40 PVC 2" NA 12.55'bgs-14.25'bgs ^ SCH 40 PVC 2" 0.020" 11'bgs-15'bgs #2 9' bgs- 11' bgs NOTES 16- -16 20 305018 Golder Associates LOG OF BORING FPP VMP-3S (Page 1 of 1) I Project ii Project Number i Hole Depth i Date Started : Date Completed Vichem 003-6016 5'bgs 2/21/00 2/21/00 Drilling Company Driller Drilling Method Geologlist/Office Sampling Method : Ertec : Jose L Morales : Hollow Stem Auger : M. Shorter / Warren : Split Spoon Depth ; Surf, in i Elev. FEET : 0 O^^O Well: FPP VMP-3S Elev.: - Concrete 1 - t - - i -Seal U l u 2 -T -2 3-^- -3 Sand Pack - Screen 4 — - 4 -End Cap 5—-5 6 i- -6 7 A -7 Well Construction Information WELL CONSTRUCTION Date Started Date Completed Hole Diameter WELL CASING Interval Material Diameter Joints WELL SCREEN Interval Material Diameter Slot SAND PACK Interval Type BENTONITE SEAL Interval 2/21/00 2/21/00 6,25" i 0'bgs-2,5S'bgs SCH 40 PVC 2" NA 2,55' bgs-4,25' bgs SCH 40 PVC 2" 0.020" i 1.5'bgs-5'bgs #2 i 0.5'bgs-1.5'bgs NOTES 305019 Golder Associates LOG OF BORING FPP-VIVIP-4D (Page 1 of 1) Project Project Number Hole Depth Date Started Date Completed Vichem 003-6016 30' bgs 2/2/00 2/2/00 Drilling Company Driller Drilling Method Geologist/Office Sampling Method Ertec J.L. Morales Hollow Stem Auger B.Blum /Warren Split Spoon Well: VMP-4D Elev.: DESCRIPTION REMARKS io^--io 15- -15 \ SC isc I SC SP i SP j • SP M ••/(A r~ -". ": • • • • • : 20- -20 i~ 0.0 - 0,5': concrete 0.5 - 2,5': CLAY, light brown with sand (15%) 2,5 - 4.0': CLAY, light brown with 10% sand, compacted 4.0 - 6.0': No recovery, cuttings are CLAY, same as above ; 6.0 - 8.0': CLAY, light brown with ; SILT (20%) and SAND (10%) : 8^0'-10,0': S ' A N D , fine with CLAYsT i SILT (40%), light brown transition into 10,0-12,0': same as above, grading ; medium sand into sand, medium i a t l l ' 12,0 - 1 4 , 0 ' : SAND, medium with silt (10%), light brown 14,0 -16.0': SAND, coarse with gravel (10%) and silt (15%), light brown 16,0 -18,0': same as above grading into clay & gravel (25%) -- moist at 15' transition to ciayat 17,5' 25 - ^ -25 30 -30 18,0 - 20,0': CLAY, compact with sand (15%) 20,0 - 22,0': CL^Y, compact with trace sand, light brown 22.0 - 24,0': CLAY, compact with gravel and pebbles (15%), light brown, mottled 24,0 - 26,0': CLAY, compact with sand (5%) and trace pebbles 26,0 - 28,0 ' : same as above ! wet 28,0 - 30.0': same as above END OF BOREHOLE -22 -24 -27.25 29.25 30 Well Construction Information i WELL CONSTRUCTION : Date Started j Date Completed ! Hole Diameter j WELL CASING : Interval' , : Material Diameter I Joints \ WELL SCREEN Interval Material Diameter Slot Size SAND PACK Interval Type BENTONITE SEAL • Interval 2/3/00 2/3/00 6.25" 0' bgs- 27.55' bgs SCH 40 PVC 2" NA 27.55' bgs-29.25' bg SCH 40 PVC 2" 0.020" 24' bgs- 30' bgs #2 22' bgs- 24' bgs NOTES 35- 305020 Golder Associates Depth : in FEET ^ 0 - ^ I H 4 - 1 ] 8--- 1 1 1 2 - - -i - 16--- 2 0 - : Surf Elev, 0 0 -4 -8 -12 : -16 1 i Well: FPP VMP-41 Elev,: r^f?| 1 .'• •.'-i i •; i ' ' i i".! \A -J r;j n \ . '• : . ' ' ' •:p\L u^:.5—; -Concrete -Grout -Seal -Sand Pack - Screen -End Cap LOG OF BORING FPP VMP-4i • Project ,' Project Number : Hole Depth . Date Started i Date Completed Vichem 003-6016 15'bgs 2/22/00 2/22/00 Well Construction Information 1 WELL CONSTRUCTION \ ' Date Started : Date Completed \ Hole Diameter : WELL CASING : Interval ; Material Diameter : Joints 2/22/00 2/22/00 6.25" O'bgs-12.55'bgs i SCH 40 PVC 2" NA : WELL SCREEN • Interval i Material ; Diameter ; Slot Size 12.55'bgs-14.25'bgs : SCH 40 PVC 2" 0.020" i SAND PACK Unterval : 11'bgs-15'bgs '\ Type : #2 : BENTONITE SEAL i Interval : 9' bgs- 11' bgs \ NOTES i 1 ' ^ (Paget oft) Drilling Company Driller Drilling Method Geologlist/Office Sampling Method Ertec Jose L. Morales Hollow Stem Auger M. Shorter / Warren Split Spoon 305021 Golder Associates Depth '• Surf FEET 0 o 4 o J - A -; 1 -t- -1 i 2 ^ - 2 - •1 3 -- -3 -i 4 4 - 4 5-^- -5 6 A- -6 7 A .7 8 - ' ' Well: FPP VMP-4S i Elev.: : n 1?" i p>: v : ^ \ 'A A\ • \A'^\ : ' • ' : T ' : i i ^ ' - ; !'•, ''• - • • i . - r - i j ^' ' " ; • • : : ;• ; • - . - . L i;n''"'r : ^. •.; f ^ — h " : i ' . • : , : - • - ' — ^ - Concrete -Seal -Sand Pack -Screen • End Cap \ Project :. Project Number \ Hole Depth. ;: Date Started • Date Completed LOG OF BORING FPP VMP-4S (Paget Oft) Vichem Drilling Company 003-6016 Driller S ' bgs Drilling Method 2/22/00 Geologlist/Office 2/22/00 Sampling Method Ertec Jose L. Morales Hollow Stem Auger M, Shorter / Warren Split Spoon Well Construction ' | Information \ WELL CONSTRUCTION | \ Date Started i Date Completed ; Hole Diameter i WELL CASING !Interval i Material Diameter Joints : WELL SCREEN Interval ; Material ; Diameter ; Slot ; SAND PACK 1 Interval i Type : BENTONITE SEAL : Interval '• NOTES i 1 2/22/00 2/22/00 6.25" 0' bgs-2.55' bgs SCH 40 PVC 2" NA 2.55' bgs-4.25' bgs SCH 40 PVC 2" 0.020" 1.5'bgs-5'bgs i #2 0.5'bgs-1.5'bgs : 305022 APPENDIX C Groundwater Sampling Forms 305023 305024 i 5 • ' : • i t ( A m GROUNDWATER SAMPLING FORM Well Number A f / A J - / State Permit No. ,;,^ I C A ^ U J ^ Sampling Date Project Name Urft^T-Jt^t^ ^--^^^^r./S/'^ • Weattier Project Number ^^ ^^n^cu >^ Sampled by: _/?,7'/v ^/^.^, ' -*-^^5>^ ^o-/s»^ ' (initials) ^^^^^^^^^^^^^^^^mmmm^^^^^^^^^^^^^^^m Well Type: ) ( Monitor Other: Well Construction ^ PVC Steel Well Diameter V'*' Well Depth (ft below TIC) Water Level (ft below TIC) Well Notes (Odor, well conditit inches Well Screened Interval to Well Headspace Reading (PID/FID) Other: reet below TIC / ^ . • • ? i Product Level-lf present (ft below TIC) //cjy'* Dn, etc) l^jcl <to>\c/i-/riJn — a c ^ c a , ' i r ' r o i v ^ a ', 0 < / < y r ' ^ / / ' ' ) A ' / ^ / t o / f ^ Volume of Water in Casino (aallons) ( 5 3 . 0 0 ) . ( Well Depth I5.7i O- / J ^ ) * .^V ^f^ '^-*-«:64e&- = aallons water Level Well Diamet'er (in) a > . ~ / G ^ ^ ^ - f ^ ^ ^ ^ O P f i ^ 1 Purging Information " ' ' " Purge Method: K Low Flow NJDEP 3 Well Volume Not Purqed Other: Pump: ^ Submersible Pump ( i? inch) Peristaltic Positive displacement Other: Pump intake depth: 3 i V Purge water discharged to: Ground A" Drum Other: Tubing: Polypropylene X Teflon-line Other: / V New Dedicated Time (HH:MM) 9:^P f y ^ 9."/7 9/5JI 9: h7 lOlO^ /o:ol /OU^i ) 0 . ' i 7 /c ',A^ id ^'Xl a)-3^ my? 1 0 : ^ ^ (0-'i7 )0 x s ^ " ' ' ^ Temp (°6J — ^9.'i9 •iO£>X W3'S ic.V^ J'o.fc-? Jo.cj'o >.Tl '7^.9^ 30.15^ y^.n l o t n ^o.n 3foC U t O ' b 3ir<^9- 3/,9f tA pH (pH units) • - - i.r^L 6,71 Gni 6.7/ 6.70 ^ > ^ io.^'i 6 t 6 9 C 0 i>,Cf U l C6f 6,^9 C.69 ^.i9 ^,€9 D,0, (zaiL ) ^ ^ .3? ,^i Aii '?0 ,a^ 3 \ ,30 , 5 ^ ,37 3/ A'S .X7 ,^Q ,XS Ail tj^ond. (^/"^ ) — . ^ i O i AoC ,7.0C , 3 O ( D ,.?0G ; J 0 O .;?o8 >Xo7 .Xo'tf ,:KO'6 >2oif , ^ 0 7 .IXO'i , ^ t acr? .2fH Turb i / i j O ) 3-2./ i%^ ^9-9 i^.a 5-P.7 6?.^ 57-3 u,l 6^A? €^.9 %or? 3c3 9 2 0 9«.f 9i.H / 3 / DTW (feet) ronH /^;«s I C . 9 7 n.oi n.)t |7,^V \ i . i \ ii.ip n,39 n.H6 n.^^ /7.5^ ;7,55 ;7,S5 M-S5 /Zyg- 1 7 3 9 Rate ( "hi /min) ^oo ilS^ XZO ioo 3K) ^oo — ^yy • — . 3.^5 •— b^o — • • 3^c • — ~ -»?53 -;\$5 -;{s9 ' 3 ( o H - 9 G 7 - J - 7 0 -i'o? -?73 -P.TH ~^73 -;?7$> -;??/ -;?«& ->??/ - ^ 2 ^ ' ^ 7 ? 541 'A . / ^ ,/o ,/^ ,/o JO ,/o 7d ,/tf /tJ JO . 1 ^ ,/o JO JO fO .10 7P^ /.i? 15^ / ^ A i J /.:?J /.7J 1.^3 i.33 1.33 133 1.35 1.33 1.13 'S3 1,3^ L31 Notes Purge Start (licnxL,,r/ e^-.nPl'^ ^ ^ , „ , T 4 l Z n r ) m f / n , / ' y ^.ru^UJ^rl- //.'^y •k ,' Post-sampling Measurements Total Volume Purged Water Quality Meter(s) Hc'i\i<.Q^-^2 ', Sample Information Groundwater Sample Field 1! Sampling Time / / - ^ ^ Sampling Method Bailer Sampling Observations Sampling End Time J l ^ ^ R DTW before Sampling I S . / " (tvoe: ) Same as Above Other: • See Page 2 of 2 for Groundwater Sampling Parameters | 305025 GROUNDWATER SAMPLING FORM ' Well Number MU)- i State Permit No. Project Name Project Number V^fi.fll^l I'^it-^hin C'HfMt Sampling Date lyqL, • Weather ^.iL-CXD Eai^kw Ciu}i,r>v ft£^>-?.»,~ik<P IM £of;,<^F Sampled by: M. (?.',^HUM (initials)' ~ ) . ' 6 ( 1 H M & U - - Well Information ^ - ~ • ! Iwell Type Monitor / Other \ J K \ P Well Construction >/ PVC Steel Well Diameter '~| Well Depth (ft below TIC) Water Level (ft below TIC) inches 3 3 iG.iC Well Notes (Odor, well condition, etc.) Volume of Water in Casino (aallons) Well Depth Water Lev Well Screened interval to 1 Well Headspace Reading (PID/FID) Product Level-if present (ft below TIC) ) * ^ * 0.0408 = el Well Diameter (in) r\Q - /-/A other. eet below TIC gallons Purging Information "~ \ Purge Method: «/ Low Flow NJDEP 3 Well Volume Not Purqed Other: Pump: >/ Submersible Pump ( inch) Peristaltic Positive displacerr>ent Other: Pump intake depth: 2 B Purge water discharged to: Ground v Drum, Other: Tubing: Polvoropylene v/ Teflon-line Other: / / New 1 Time (HH:MM) \ ( < ) ' ^ 105?) M l o c j iiO^ H i t l l i ^ C/ZO 1/25 li-^o 1 ' ^ ^ ii^o j 1 H 6 II e)c> li^OO Temp (°CL) •V^'Ji m.oo 29.0Ch 29. i4 Z'^.Ko ^.H8 29. G 2- 29 7 Z 3o-Oi 3 0 . ^ 6 •^ccl 3o.G£>! ^ • i ^ .^.27 1 pH 1 (pH units) l-2h 7.25 7.2^ •7.Z^ 7.21 1,21 ' I Z o 1/9 7.ip^ rn '7iG 7,!G 7.IG e o..^ 7. R 1 1 D.O, i^na,! i-) -j.n k'sa G.SZ G.lb G.12- G.C.L QAb^ G G5 (^.^A CAO G, iC3 G.5i C.52- X-i-,N C ' ^ 1 f i»n.-, I. C 3o 1 Cond. |W,S/cm) 7.HC 1 2Mn z.^1 z.^n 2.Hb 2.^9 2 •oo 2.51 2.&.3 -^.^H 2.^'b 2,63, 2 . 5 ^ ^., (i,,),-\/' r Turb ( KTTiJL.) ^ T 5 5 5^ 52- Go 5( ^59 < ^ ^ C6 r.P CG G£ ! C>7 ciiU^J b \ 1 -)2.6f)l • 7 ^ DTW (feet) n.i^ / 7 5 8 /7.7*--) 17.^^1 /&.2-5 18 2 7 IB.3 3 IB. 55 lfiS7 l ^ ^J5 18.55 (b-^-^ (&.5o r "U^^\ Ifl.Ofi 1 Rate 1 (m L /min) lOCO 76 O 5oo M20 5 o o 5 6 0 ^ 0 0 ^2x!> H^C ^zo iao ^ 7 0 7^G DAAII.<-^ \ 3 too bj_ TD6 I s l 0-1 |l.S£ oi ir^De 0 1 0.1 \.^: l.bf\ c i jl.to Ol ll Lc o..( h.(.-j Ci il.fe:Z O.i \ \ i 6 O i h i z o.i i\.<oT 0 iii.fci r i A p h j i J 0.(!!-t3 1 *»/ ISo 113 iu> Ii7 i N 115 li.S i()9 107 no lop, io^. ID9 pA(^ Wl I/O 1 _Dedicated 1 Notes |purge Start C t i t j , flojO^tnTo C.Oc) NCTC:'. ( A l t . ' ' (Nj-iiA-vi 1 ,l->)\/ (or-4 f i i n J c J ^ ^ ' o 1 Post-sampling Measurements | Total Volume Purged Water Quality Meter(s) Sample Information 1 broundwater Sample Field 1 ISampling Time (,5=, Sampling Method Bailer Sampling Obsen/ations D MW- i Sampling End Time iZcO DTW before Samp (Ivoe: ) •^ Same as Above Other: linq / 6 . P^ 1 1 - See Page 2 of 2 for Groundwater Sampling Parameters | 305026 GROUNDWATER SAMPLING FORIVI Well Number Q i t U - / State Permit No. Sampling Date Project Name • Weather Project Number Sampled by: ESS^f^ H'2'^'OO s ^ t. 1 ' . . '• T:r (initials) Well Informeficm Well Type: J>(^ Monitor Other._ Well Construction V* PVC Steel Other. jWell Diameter H Well Depth (ft below TIC) Water Level (ft below TIC) inches " r 33 lio.bG' Well Notes (Odor, well condition, etc.) Volume of Water in Casinq (qallons) |( ) - ( 1 Well Depth Well Screened interval to f< Well Headspace Reading (PID/FID) Product Level-if present (ft below TIC) ) * ^ * 0.0408 = Water Level Well Diameter (in) ;et below TIC Q a l l o n s P u r g i n g I n f o r m a t i o n [Purge Method: '•-/ Low Flow NJDEP 3 Well Volume Not Purqed Other IPump; vi Submersible Pump (15 inch) Peristaltic Positive displacement IPump intake depth: " 2 - 8 ' Purge water discharqed to: Ground '4- Drum iTubinq: Polypropvlene Teflon-line Other / 1 Time (HH;MM) 07.^S UMB \o^>5( orss 1 0 1 '•'^'O U'\t? 1 i'^'-1 tt^ 0 =j t7_ k ^ ( 8 oV^^ Temp C C ) 2«.5'-f i2J!.33 .^A}.o:i- yiS.S9' D - i . 2 1 • A ^ . M 9BAiL o^<?.7fc as.77 Xi-S-b pH (pH units) in.-2.'} l-y.^i '7.?jO 7./A6 9. OS 7 2% 7,7? '7.^7 -7, l U 7v>rs Total Volume Purged D.O. \(f^A'^ ) tZ..^)< a . m \ 2. ,M.>- )r>,3! (.>-.^.0 VA i ':> ?.ir./ v^.^>^• i/.-^ok i \ 3 7 Cond. ( s>. ) 0-:^^2 1(7^-^3 c5.20-i? 0 . 2 0 ^ 0.2C7 (;,207 .5.7^/i 0 - i O ? O.iXcl Q ^ ^ i Turb f-»^7^) ^ n 1 — l f c . 7 K . t - -X.h '/.. A. b . ^ 5:5 ^ 5 17 J ' DTW (feet) \ \ n A^o in.sz VAi> h.r^ v i 2 \ Rate (i^-**-/min) 5eo 5 0 0 ^e-D 7.-%t> S < i o tj5(3 ^ c d yvA! i C ] ^S' ~' "2, 1 - ^ s 10 0 )0i 77 It. 'iH ns Water Quality Meter(s) Other Other New Dedicated 5 . ' i r T M o.i h.si- O.t U-3.3 o . , H . 3 3 o^i H.?'^ O.i i i - ^ o> 1 !|,3'' O f !(.7^ o-i : ) B 7.l!i,5, ^ • U i . 3 f i' 1 t Notes Purge Start < 7 J 8 H O PIcx'i! VTs-le ; 50D,-^^/m^ f;4,".XrtrL;i -i-o i't^^ ^ -^ :J,'^.C^: i>.S-t.A -ffj-w .fa-.ii. Stw/^o f<i •^Ti'Y-t. ^ QrslS" 1 D'i.7^^ f^/i-.v,p (^/£. 1 Post-sampling Measurements l^vib:"- 0••'-^) S a m p l e I n f o r m a t i o n Groundwater Sample Field ID [sampling Time ?)'1.^S Sampling Method Bailer Sampling Observations Samp (type: . •VY\lO-t ling End Time O^T-C^ ) yl Same as DTW bef Above Other ore Sampling 1^ ' i 305027 GROUNDWATER SAIVIPLING FC Well Numoer State Permit No. Project Name Project Number i n u : p - « rLs- f a M cke-nC cc-<i> }RM • Sampling Date Weather Sampled by: F J ^ ^ ,T'3-a; S ' c ' . i / i y - ^ ^ t ? Si/Mj-/wA*^ 5<1' , /T/f , U f ' f r ^ (initials) ' H a r t inc. well lnforma{Jon W e l l T v D e : V Monitor O t h e r Well Diameter inches Well Depth (ft below TIC) r | # ; •^^'^ ( y ^ . ^ 9 ) Water Level (ft below TIC) 1 1 1 I ' Z Well Notes (Odor, well condition, etc.) Volume of Water in Casinq (qallons) ( ) - ( Well Depth " Water Lev Well C o n s t r u c t i o n [ y . PVC Steel Well Screened interval to f< Well Headspace Reading (PID/FID) Product Level-if present (ft below TIC) other ;et below TIC ) * ^ * 0.0408 = gal el Well Diameter (in) ons Purging Information i Purqe Method: >Z?Low Flow NJDEP 3 Well V o l u m e Not Purqed O t h e r Pump: ^ Submersible Pump ( 1 inch) Peristaltic Positive displacement O t h e r Pump intake depth: O Z Purge water discharqed to; Ground "KCrum O t h e r Tubinq: Polvpropvlene >> Teflon-line O t h e r / .X?New Time (HH;MM) \ o \ l lo^^ /od~3 / o ^ '031 /OSi- /o3^ l O ' t ^ WAS {o^\ (oS( loss^ Temp ;>?.Sb 3tA^.bl> <;^?..s^' " c k ^ : ^ n^/ ?^%^ X^.13 ^^,-11 Pf)-ll A?.?^ -^9-If 5ii.t1 pH (pH units) n . i ^ ^•/M "7./I 9,13 7.'^ -iix^ in 7.// 7.// 7.// 7 / / 7.|( Total Volume Purged D.O. CAS^/ t ) 1^.;!-^ ii^*^ 11.30 ||.|0 f ^ . ^ j6.3t> / o / t / ' • o ' l ^^.77 ^ . ^ ^ 7 7 'l.fcL^ Cond. 9..0X a.on 3L.01 3<ol ^ . 0 ^ 5.09 ayo .3,.o? ^.o't 5-f^ ^ . 1 0 di-id Turb (^ r^l^ )1X> 3S ^ ^ 7 0 % SS 5-^^ 6 3 6 5 " ^ D Sam Groundwater Sample Field ID Sampling Time (OSS Samp V W L O - ling End Time Sampling Method Bailer (type: ) Sampling Observations D/o ^ t 5 ^ ( DTW (feet) 17.'13 l^.iv U.^3 /^•er Lf.SO^ JS^BA j l d ^ 1%.^^ ;3,9o /X?^ I^T^ Rate ftv^/mln) U>t> 557) ^ o (5(30 5<?6' v$^ i f ^ 45t? HSb Hoo Hoo .^^i7 M1 M ^ )o^ | 0 6 9? f'^ 1.^ 17 % ^5* f r '^n .( 1.33 . 1 . J - / ./ -(^ ol J J i-3> /.3:? 1,^3 /.-3-3 /-3V /3V /.3V /3y , 1 /.3y ' / /.Sf 1 ', 1 j . ( i(-3v Dedicated Notes Purge Start fai3 i 1 i 1 p M - y n ^ 5 / 1 . ^p^^cl ioS9 ! 1 t n • •! ! 1 Post-sampling Wafer Quality Meter(s) 6< -2 2. ^Mr^ii,^,) - pie Infonmatfon 1 J VOP I0S7 [ f o ^ ( ^ - ^ ^ DTW before Same Same as Above Other linq = 0 U Measurements 305028 GROUNDWATER SAMPLiNG FORIV! Well Numtjer Slate Permit No. Project Name Project Number / ^ I t A J ' ^ ^ UirmA 'X&lcLnd d J v w G i l Sampling Date f J c • Weather Sampled by: 3 M J / 0 C > V^^f^. .^,AL. ',-^</:C''>P h.^^r^r o-.^^.a^ / (initials) Well InformeliCMi Well Type: X Monitor Other Well Construction V'PVC Steel other Well Diameter ^ inches Well Screened interval to feet below TIC Well Depth (ft below TIC) . ^ / Well Headspace Reading (PID/FID) 1 J O fi fi i ^ Water Level (ft below TIC) / 7 / 6 ( ^ { . c ( ? j f ^ I ^ A i ) Product Level-if present (ft below TIC) Well Notes (Odor, well condition, etc.) Volume of Water in Casinq (qallons) {!^.(^ <l Ccnri , AIci O d i ^ r / • . • — — f ) - f ) * ^ * 0.0408 = gallons Well Depth - Water Level Well Diameter (in) ^ ^ _ / U i / / / Purging Information Purqe Method: Jjl^Low Flow NJDEP 3 Well Volume Not Purqed Other Pump: X Submersible Pump ( ^ inch) Peristaltic Positive displacement Other Pump intake depth: ^ ( ^ ' ' ^ Purqe water discharqed to: Ground > ^ r u m Other Tubino: Polvcrocvlene Y Teflon-line Other / \ / N e w Dedicated - "^ . / ^ ioto pf/o iO^i /c>^\) ^ Time (HH:MM) 7 3 9 7 ; V ^ 7.H9 7 ; 5 V 7 . 5 ? If.-^v ^^^cf^ 9,\lH 6:i9 6;:?W ^ i p " ) ^-3H ^•39 f -vf '6'.i9 9 ill Temp CCJ a^nH P.'i.^S 30^3^ Si>>30 50.30. 30,HI 303 f i Q t i ' i ^ 9 U 7>o,i^7 2?C,H ^ / . 3 D ^h£C> Tii^i ^ ) M -bini pH {pH units) 5.^? C A l 6.9^ &,9-3. 6.92. 6,7-2 ^,^A ^.93 4.9t C B X Cf9^ ^ ^ 9 ^ f>9^ £.93 C^^ t.93 Total Volume Purged DO. (j!!i/7_) / . / € d.5? 0.^1 QiH4. o . y i ' 0^3") 0.57 O.HI 0.39 o,H^ o,yi 0>3^ 0 , 3 0 0 , ^ 9 ^.a^ 0 > U .ca3 r s a h .7.9^ .AXb .533 . ^ 3 ' / AS.7H .xxc ,^;?s a73 M C /^OsCi ^;m . X : Q '•m >n^ Turb -<6.0 -€.(, -:b,6 7.V 3,9,% -10,6 -JcJfi ~ ( u , 0 - V ~ Q i l ' 9 ^ -<^i% •9J7 -9^ ~(^rh - I D DTW (feet) / 7 / 5 ^ ( 7 . 3 ^ /7.S3 >7..3^ n,3S /7A3:S /7..^S 173$, il,36 (7t5^ 1135 /7/3S H ' ^ p. 3^ /7.55 an Rate ( M/ /min) 3 ^ 3 9 0 - f i O HlO ^/O ^/o 1X0 H?.^ Xoo 15 0 0 ^/y> D / 0 316 ^ ^ ^ -A90 i^S / O ^ 1f^ 73 ^ ^ 5 7 sa VS' ^ 9 y9 3 ^ 3S ^ f i 4 s/ y}> H7 Water Quality Meter(s) 5 ^ .il •11 .d 7P5 f.H5 AW /.W ,11 M^' .n ,11 Jl ,li 'H .Jl M Jl / / / ,/( ill ,// i.l3 h^l / « //<5 /,v/ l i ' H f , ^ i.HS / / ^ 1 . ^ i,H(- IHb Notes Purge Start ^ ^ A t K j ^ k W c ."^co f)A*i/l'^ / ^ S > * / 4 ' ' Post-sampling Measurements //^/,'k /)-32 ^v„;/7cv7''O t; Sample Information I Groundwater Sample Field 1 Sampling Time 6''"^ Sampling Method Bailer Sampling Observations - <^c:o P s n c 0 rxt 0 f n r CI r/M ii-iHiimtor C Sampling Eno Time f ' / { l DTW before Samplina H A S ^ j v (type: ) Same as Above y Other \ / amrvlinn P a r a m o t o r * 305029 GROUNDWATER SAIVIPLING FORM \ A / » I I K l i t r v s K # ^ i > ^ V ^ l j ! 1 Well Number State Permit No. Project Name Project Number 1 / tbXI ^ o i ^ • Sampling Date Weather Sampled by: f^M^kW H-n-'oo 5"l,crvr.t( ,. S ^ S Kf. -' (initials) Weillriforrnfinon Well Type: Sc Monitor O t h e r Well Construction V{. PVC Steel Well Diameter i-/ Well Depth (ft below TIC) Water Level (ft below TIC) Well Notes (Odor, well conditic inches r3l )n, etc.) V o l u m e of W a t e r in C a s i n q (qallons) ( ) - ( Well Depth Well Screened interval to U Well Headspace Reading (PID/FID) Product Level-if present (ft below TIC) other set b e l o w TIC ) * ^ * 0.0408 = qallons Water Level Well Diameter (in) Purging Information Purqe Method: ••/- Low Flow NJDEP 3 Well V o l u m e Not Purqed O t h e r Pump: (XL Submersible Pump ( 2 . inch) Peristaltic Positive displacement O t h e r Pump intake depth: Purqe water discharqed to: Ground X Drum O t h e r Tubinq: Polypropvlene ^i^Teflon-line O t h e r / j ^ N e w Dedicated Time (HH:MM) Temp pH (pH units) - Total Volume Purged D.O. Cond. Turb fK.'Tc{) DTW (feet) , Rate (y^ -'/min) Op.f Water Quality Meter(s) "• Notes Purge Start Post-sampling Measurements Sample Information Groundwater Sample Field ID Sampling Time Sampling Method, Sampling Observa Bailer ions Samp ling End Time (tvDe: ) _Same as DTW before Samp Above Other ling r, ^ -. -,.__ ^ ^.._,*», c ^mr>ti«rt D a r 305030 GROUNDWATER SAIVIPLING FORM Well Number State Permit No. Project Name Project Number ! 1 ] L U ~ c-^ -Xs\ci\^.c\ (Ci-v^tVMf &i/ Sampling Date Weather Sampled by: b ^ t - t /-. R^,- f^WJl^L^rSD -^-oa At^ ^, hr-CC^A^.. SOS (initials) -i^ce^rec] 1 Wen InformalJon Well Type: Monitor Other Well Construction D^PVC Well Diameter inches Well Screened interval 'Well Depth (ft below TIC) 3 1 Well Headspace Reading (PID Wafer Level (ft below TIC) irs^ Well Notes (Odor, well condition, etc.) Volume of Water in Casinq (qallons) ( ) - ( Well Depth Product Level-if present (ft beic ) * ^ * 0.0408 = Water Level Well Diameter (in) Steel to f« ^FID) 3W TIC) other 2et below TIC gallons Purging Information Purge Method: "x Low Flow NJDEP 3 Well Volume Not Purqed Other Pump: "K,'Submersible Pump f2-inch) Peristaltic Positive displacement Pump intake depth: 2(y Purge water discharqed to; Ground x ^ r u m Tubinq: Polypropylene yO Teflon-line Other / ( ^ Time (HH:MM) ! o o 3 i 0 0 6 ! O O J 7o/5— '/OlS' /0/K J o j - t /o^V^ f ' O ^ I 1030 )033 /OVC Temp .S-IMXCX 3o.og 50-dL^ 3 0 . 1 " ) 3c 3 S 3(0.'i-o 3 0 . ^ " ] 3o 3ci So-Vt. 3 0 3 1 3 0.-5V 3 0 . 3 2 pH (pH units) •7o1 n.on 7 - 1 0 7o1 7. JO - 7 . 0 ! 7.0"^ y. on 7-04. 7 - 0 4 7 . 0 4 7 . 0 - } Total Volume Purged D.O. A ^ L ) Z7 ^•H ^ 0 7 3-n 3.7^ 3.^? S . o i o ? . 7 ^ ^.75 c5-fc7 ^ • G i ^ 5. o<-f- Cond. o • ^ ^ 3 OALliy fl.c7J7 D.X>-^/ 0- .7,X7 0'^<)') O ^ ^ l 0 . ^ ^ 0 .r3UJ-9 OAi-30 O A X ^ O 0.,x3o Turb '53. \ ??. 6 ' ^ ^ T ^ ^ ^ <jQ.3: /.^ih-O M - 0 f ' i / O B 7 0 ID-o.o lohAC >J-5 -o 1 DTW (feet) ll/l-^t ' i H i . l l ' \ \ ^ \ / 7 . 5 3 •/%57 /9-^> /7.'f7 /9«^ fQ.t/L| /^•'^'Z /^/.VS /?^^/^ Rate (rv^.^ /mini i^oO "yOO •-loo ir??- 5'^^c) 6 ' o o SDO ^Od ^Cro goo ^ a o £ o ( ) oep •Al\i 3-^3 c 3 6 S ^ 7 / <P-5 7 c;^7 3 J ; 7 i'/'V 3 S S 3 7 7 4'/>3 37a- 3-.S2 Water Quality Meter(s) _Othe 0 >r her New S4t % .V\ . l i •rpS .sA 1.+/ I.'^S ' // i/v{; w/ l/vy ../-' ,7,y,6 . / / w/ . / / -// • / , / .11 A'Vt /.fe /,V7 ' ^'> /,./; 1'/;, j 1 1 ; i ./•' •./.yj Dedicated Notes Purge Start | QOO ^ i ^ - ^ ^ . • • hoih-yi'^ \ s < : o f t • i - r w + u . Rc'-'tscM. -('.--.L'VT^.-k:. s(iqU.4' — u •, D/^ Ajf.4C.ah> •irk.M&y.. Ai.X<.e- 1© / 0 3 5 - Post-sampling Measurements Sample Information Groundwater Sample Field ID Sampling Time l O ' i S Sampling Method Bailer Sampling Observations Samp (type: 0 1 ^ ) ^ 0 ling End Time / O ^ r A ) Same as 7.y,,,,, ' n n ^ J ( 7 ^ , , DTW bef Above Other - • ^ . - » . , ' . .AA.'i.i'-;<A:'.. ore Samplina / 7 - V 6 305031 GROUNDWATER SAMPLING FORM \ A / . . N I I K l i irv-il-mv A . , i i / I <2 Well Numoer State Permit No. Project Name Project Number / 7 f^ -' Sampling Date Weather Sampled by: 3 / ^ / / ^ ) f^'^kw ^.)..;u/ . ^ v:^n^, /^^ --7.7 .>,^ K r/7 A i-'A. (initials) Well Informaticwi Well Type: t( Monitor O t h e r Well Construction V P V C Steel other Well Diameter * / inches Well Screened interval — to """ feet below T I C Well Depth (ft below TIC) r < ? / . ^ 5 ? ( c M e i p . ) . t i Well Headspace Reading (PID/FID) O . O p f , y \ Water Level (ft below T I C ) (7^1 Well Notes (Odor, well condition, etc.) Volume of Water in Casinq (qallons) M> 1 . i>S~ - ) Product Level-if present (ft below T I C ) 7A!3'C-- 1 ' , J ( ^ - - - ' ' " " ' ) - ( : - . . - - ) * .._-^-- ^ * 0.0408 = , . _ Qallons Well Depth Water Level Well Diameter (in) ^ ^ iQ A^ j j j Purging Information Purqe Method: X Low Flow NJDEP 3 Well Volume Not Purqed O t h e r Pump; X Submersible P u m p ( ^xinch) Peristaltic Positive displacement Pump intake depth: i-if^' Purqe water discharged to: Ground V ' D r u m Tubinq: Polypropvlene X Teflon-line O t h e r / V Time (HH:MWI) l|'^^ ii;^^ W-.i)- H'.Hl \\S7 WSl \ M ^ po7 \ M [9~\1 \2y? ,J.7 i.73a i237 \V.<,'^ Temp ( ° e j M i 3d3^ $o.n }d.^:> }0(i^ %5\ ^O.lf m> 36-31 3075^ %H %m Ui^ '^.U -Fi %A1 pH {pH units) ^.^3 b.^3 6.*^ m t.'&'f U 3 ^ h U } i>,V, W3 i,0 i > ^ ^ hfi) i,i} 6.^ DO. {£&/ / ) t,S\ 0.3^ oM 6 M O^i 6^i 6 3 ^ 0.% 0.^! 0.5-1 0.S9- 6.^^ 0,53 OSS' 0,69 Ccnd. ( 5 / / M ) .m ,Hf .i«i .m M6 >iV A^^ AV ,i13 ,1^3 .W .m M'^ .i^r , i % Turb ~ i ^ -lo-o - i n -^.5- -/o.o -13 0.i/ o?.6 2.0 -10.0 'V.o - m '10.0 -10.0 -W^ "l^^ DTW (feet) n^^ il.5(^ OS^ \lS(c 17.^5' i7-5f i1,b6 175'.^ 17.5V ,-7.^r i7^r ^nM as^i 17.57 \im Rate C /•«'' /min) ^io —. vfy — ^ < ? ^ -— ifcr — 37^ ,— V(3y — 5ii^ — /'g'i^ . h ( ; -/^gr - H I -11} -I3n '13^ -/57 -'5r - / > / - / ^ ^ - / ^ f -/p? -'i.i(fi - / ^ ^ -/^r -/AD o t h e r O t h e r N e w Dedicated % \ ^ ^ r o.m\/,7l 'd.(f}\,.7l CC^lUf CQ'\\I.7\ m UJ. o.o1 f.n Off^\l-^i oMi-^ o4 u'/ OJ4I.^3 offiU'^ om>^ 0^\U^ Oi^li'^S' . C ^ \ l , ^ Notes P u r g e S t a r t /Wljjj>W 'clcji /-ft+e., .^ j c r * . ^ . . , ^ fx^*^-, 4 U , « ^ f^}Lo, Post-sampling Measurements T o t a l V o l u m e P u r g e d W a t e r Q u a l i t y M e t e r ( s ) ^ ^ I ^ ^ M \ J ^ ? 2 Sample Infonnation Groundwater Sample Field ID Sampling Time ll^HS Sampling Method Bailer Sampling Observations - See Page 2 of 2 (or G roundwBler S Samp (type: M ' ^ . ^ l M - S / )ling End Time [h^CP ) Same as DTW before Samplinq p M t Above VOther 1 ampling Par ametera \ 305032 1 5 ; i .3 i w 1 GROUNDWATER SAIVIPLING FORM Well Number M l A J ' ^ State Permit No. Project Name Project Number O A ICncaJ"^ U.rjjiA X . / f r t a i (AAertiirJi ESS'^f^" Sampling Date 3 / ^ f f o o yp Weather 3 o / i r t ^ i=f^ ^ V = / 3 ^ u / > ^ Sampled by: ; ^ c '//(oU ' (initials) ; : » ^ B « i i H Well {ftformalim ^ . . . . \ " Well Type: ")( Monitor Other Well Construction X'PVC Steel Well Diameter i / Well Depth (ft below TIC) Water Level (ft below TIC) Well Notes (Odor, well conditi inches Dn, etc.) ^ r Volume of Water in Casinq (qallons) ( . ^ - ^ ^ ) - ( Well Depth Well Screened interval ^ O to 3 C | Well Headspace Reading (PID/FID) Other eet below TIC Product Level-if present (ft below TIC) N t ^ ' ^ f l ^ ' ^ ' ^ " ^ ) * ^ - ^ ^ ^ * 0.0408 = ^ - " " " ' ' ^ a a l l o n s Water Level Well Diameter (in) >•-. Purging {nformatton Purge Method V Low Flow NJDEP 3 Well Volume Not Purqed Other Pump: )Q Submersible Pump (<J^ inch) Peristaltic Positive displacement Other Pump intake depth: ^ S ' ^ Purqe water discharqed to: Ground ^Drum Other Tubing: Polypropylene Teflon-line Other / V New Dedicated Time (HH:MM) /'•^/ol //'.3Z /iS7 1^02 1,7^01 \y.i2 {'•p '^r^ a'S> 11-33 IXHO i^^.HS \vv^ a\3^ l i O O }?i'.o^ Temp cn — 3 0 ^ M).^ 30.%<] 30.10 t ^ ^O.TT ?)I0^ 3 / M 7?} 3 ^ :V'V^ ^/.6<^ 3lh6 %i( • ^ i j J l V4 pH (pH units) ^/(fV 6.P fc.(*3 G.C.^ (p.o.'^ ij.isG U^ as 6,6S 6,^5 6,65 ^>6i a i Ui an D.O. o,73 0.^0 OJ^ 0.)'\ 0.;7 0.57 r-^/ . ; ? ^ .;?o J ^ ,/7 J-$ ,iH fHH s-bl Cond. ( ^ / A ) — T .;?;?7 (p.;';'7 .p;?r .i?pr .m .P3) , ; ^ ; i ^ .^:;\9 ,;u9 . ; i ^ ; ,;;i:3o .W ,;3o >^^c> ,Vbi Turb ( M O ) 9.-^ cif(^ l\ 33 io 10 7^-9 ^ ^ ^ AO,"^ /f.-ir %6lf i ^ M Uf) hh-X Ifif^ DTW (feet) 1 ^ . ^ ^ /4..7^r j^Af] m'] ^.n M ii>.j^ a n l£rA9 UA9 iGXi l i M I h M l ( ) t ^ / ^ . / ^ \m Rate ( * ' /min) J :^90 3Si — JW — .^3^ • — ^ 9 0 5 5 ^ — t,10 — . ^HD — -;?3^ ^^.^y Vi^'i V 7 ^ - ^ 7 7 V ; ^ -;;?<^v' -2TS -^?3 -;^57 -?^9/ -^?S -;?7 -^9f -<^r3 . / / .1) J) .11 M 'il .tl J , / / , / / Jl 7/ .// , / / w/ 7C5 y ^ /.4 /V6 l.li^ /.4 /.f? /,V^ <y7 t^r itT' i.HL iM7 Ml ^.17 i.^ Notes Purge Start (P^ / / - ' f ^ l7)}> d n z « h . - r-in o J ' o ' ^ g ^ j lJ^«/9 tfff /j/f /V/^/* -fvCfOira /j/*«rof«dr Post-sampling Measurements Total Volume Purged Water Quality Meter(s) / / e a h t - U ^ ^ ^ t j i i o A ~ ^ ( ^ Sample Information Groundwater Samp Sampling Time Sampling Method _ Sampling Observa )le Field 1 Bailer ions D MuU'6/\-si9 Sampling End Time . (type: liirJiiL=i tv/tLcri/r/ie/ _Same as DTW before Samplinq / ^- - ^ ^ Above Other: " ' • • J - / - • • " } - See Page 2 of 2 for Groundwater Sampling Parameters Panfi 1 nf 7 305033 GROUNDWATER SAMPUNG FORM Well Number MA)-£ rt^n-l-irsd&i State Permit No. Project Name Project Number raa^wfe" Sampling Wpather mpled b; iformai Well Type Monitor Other Well Diameter inches Construe! Well Bcreene ( Well Depth (ft below TIC) Water Level (ft below Tl Well Notes (Odor, well condition, eto Volume of Water in Casinq (qallgfis) Well Headspace Reading (PID/FID) Product Level-if present (ft below TIC) 0.0408 Well Depth Water Level Well Diameter (in) Purfllng Information. ro^- gallons Purge Method: Low Flow NJDEP 3 Well Volume Not Purged O t h e r _ Pump: Submersible Pump ( inch) Peristaltic Positive displacement Pump intake depth: Purge water discharged to: Ground Drum Tubing: Polypropylene Teflon-line Other / _Other Other: New Dedicated Time (HH:MM) Temp ( ° ^ pH (pH units) D.O. (ft2-/J^) Cond. ( i f H \ Turb ( Nro) DTVJ (feet) Rate ( In' /min) SIC rfff Notes • l3'/o 31^1 6,^'i' 0 , 3 ^ .7y3/ S7,9 /C^f -m /// I, Hi) e'.ih 3Ui C,€i OAbl A 2 ^ I 3 J ^ I L ^ ^ -^30 -^n All m M:D_ 31,'3(6 £JM_ 0,37 ,7.lJ^ J ^ ((\m - ^ 9 ^ •// / ^ 15'AA^ 3i,3C C.CH 0>^6 ^Xbl iCK lin z2JL J I l , ^ l ^ f ^ ^ • 3 1 , ^ A2a. Sanr^/^j^ 7=^/0,^ ^ : ^ o ibHi> i U ^ e>.i7 O.S^ .^dO :M. li^i ^ D •^f/ .-// /.V? Post-sampling Measurements Total Volume Purged Water Quality Meter(s) ^•Groundwater Sample Field ID Sampling Time i2i'?X? Sampling End Time Sample Information m-^/^-^ Tin- aamp Sampling Method Bailer (type Sampling Observations I ' h ' h l DTW before Sampling ) y Same as Above Other: - See Page 2 of 2 for Groundwater Sampling Parameters Paoe 1 of 2 305034 G R O U N D W A T E R SAMPLING FORM Well Number Wl UJ - h State Permit No. Project Name Project Number rcslc^<vok C^-\.a/w^CAx. Sampling Date Weather 1 ^smm ^ , - 3 - 0 0 P ^ H ^ d^.d^'), ^rD5 Sampled by: K { ^ , ^ ^ \ U/ (initials) ^ { - ^ L i a A WeiiJnforrTiation Well Type: Monitor O t h e r Well Construction PVC Steel Well Diameter Well Depth (ft below TIC) Water Level (ft below TIC) inches n.^^ Well Notes (Odor, well condition, etc.) V o l u m e of W a t e r in C a s i n q (qallons) { ) - i Well Depth - Water Lev Well Screened interval .^X> to ^ c ' fe Well Headspace Reading (PID/FID) Product Level-if present (ft below TIC) other et below TIC ) * ^ * 0.0408 = gallons el Well Diameter (in) Purging Information Purge Method: > O L O W Flow NJDEP 3 Well Volume Not Purqed O t h e r Pump: f . i ' S u b m e r s i b l e Pump ( P inch) Peristaltic Positive displacement o t h e r P u m p intake depth: ^ f f Purqe water discharqed to: Ground < . ^ r u m O t h e r Tubinq: Polypropylene y ^ Teflon-line O t h e r ' / ^(i'New Dedicated Time (HH:MM) 0835" ^-^b3t o 8M3. -^^»M6=- 084ft 0?^S3 (^?)S\. 6nc^c> oqolT o^oo> o ^ l l 0 7 ; $ " e^t^c^ a ? a ^ . Temp rC) S^^.|^ X^\.L^ X")"?^ Zi^1S(. 24-26 3f\.''i^ 3-^1 .'li .:>T-^6 ,Xf7o ; L ^ 7 i 3d.o3 & ^ o . o S pH (pH units) (c.n-^ t . ^ f o L . l i - ^ - 9 9 - ( o . l l 6 . 7 7 G.77 b.7^ ( r - ^ ^ ( o - l l G i l 6.77 6-78 D.O. ^ ' d S o S ^ - OHfi H.3^< L(-47 M.04 ^.2Jo 3.53> 3 . 3 3 3 7 V <;<.^5 o.d3 Cond. d . . ^ ^ . 3 1 a.3/ ^ ^ - ^ A . 3 ° ;A.3I ^ • 3 X x^>- 7.3/ ^•3>- 0^^.33 a.34 12.56 Turb (KJyO J \'S \7 "1>^ ^33?0-- 5;s 6 / ^ 1 ^ 1 5^ 5 7 (^J^ ?^ ^ 7 - - DTWx (feet) " X^.po \l:i^O -<^^ \7.(^^ \ 7 o>- 11 t>l 17-^/ p i t a ^ / ? - ^ > i-=?-"T—?~ 1 ^ . \ ^ y - i7.fc3 Rate (-.vl/'niin) 5 5 0 §oo Goo ( c O O ^ 5 ^ ^ <;KO =^M) 57)o " 1 1 ^ - 1 1 ^ -117) ^ l o i -102^ - / o 3 - l o 3 - i o 3 wo3 ' / 6 ^ - l o M - 1 ^ ^ Li_l-41 ./ l i ? J 7.^8 .. / (.46 7 />f8 7 IHC? f \(.^^ 1 H Wil.'^S .7 V.V? -^ !A5t) ? i \ .1 1|.3Z Notes P u r g e S t a r t 0 d 2 ^ Siv-'^^ ~h /«i-v'- S - t o p p e ^ n x A n . V T . ^ u ^ • 0 7 ^ i^CMvA^ S - h f p ^ s u P o s t - s a m p l i n g Measurements Total Volume Purqed Water Quality Meter(s) Sample Information Groundwater Sample Field 1 Sampling Time o ^ 2 o Sampling Method Bailer Sampling Observations - ) - # 1 * — * . - ^ M > . - , * t i r C D rw.io - ( ^ Sampling End Time (type: ) p/n - 0.1 0 ,«!•, Py 013-] ' DTW before Samplinq / / . ^ . ^ Same as Above Other - ' ' ' ' • • ^ ' ' ' ^ J l " ' • ' • 1 ( • • • \ \ a m n t i n n P a am«>tpra 305035 GROUNDWATER SAMPLING FORM \ l \ / . - . l l K i t •r.v.i^j-tp. \ j 4 i 1 t f Well Numoer Slate Permit No. Project Name Project Number r i i A ! y i/fixj f t\ J / A / a t / / ^J3e/ik>- Sampling Date 3 / ^ / / x 5 y . Weather /'^jy,Ay. - ^ ^ Sampled by: / i i . d ' . < r 7 wxm S^A, / j ; . p / . n •' (initials) a r e n i r t tnc. -Srjf^A Wei! Informaijon | Well Type: X Monitor Other Well Construction X P V C Steel other Well Diameter ^ inches Well Screened interval —^ to — feet below TIC Well Depth (ft below TIC) 0 3 , 3 ' ^ } Well Headspace Reading (PID/FID) 0,d>fiA>f^ Water Level (ft below TIC) ^tf, H 3 f i f { r \ p i ^ S(D ' ^ ) ' r o d u c t Level-if present (ft below TIC) Well Notes (Odor, well condition, etc.) Volume of Water in Casinq (qallons) WeH-Depth - Water Lev - . • , 1 - " ^ ) * , ^ - - ^ ^ ^ ^ W S A O f ^ - ^ - " " ^ q a l l o n s el Well Diameter (in) ^ _ ^ ^ ^ M t ^ c ^ U Purging information *" ^ " Purqe Method: V^Low Flow NJDEP 3 Well Volume Not Purqed Other Pump: y Submersible Pump ( ^ i n c h ) Peristaltic Positive displacement Oth er Pump intake depth: 6 7 ' Purqe water discharqed to: Ground yfirum Other Tubinq: Polypropvlene y Teflon-line Other / X New Dedicated Time (HH:MM) 9'W 9-^^ 9iSH 9:59 l l } : 0 ^ x t ^ ^ /c?'/^ lO i9 ( 0 ' . ^ ^ lov2,9 10.3'i 1039 l O : ^ ^ M ^ m^^i J I D H Temp C£A) n H 3 1%'^H •?,^{6L Ui-S^ A l ITS • Mn^ nn^ ^9iB4 ^•i>fi ^1.'J3 5 a 08 5^.o7 ^o>/S 2,0.0^' M ^ pH (pH units) 7 . / ^ l.ol n,o{ i . c i 1,6\ 7,6/ 7/^/ 7;06 1,60 1.06 1,00 1,60 1,00 1,00 I.Ot) Total Volume Purged D.O. I.30 0/7S OiCH C/^3 0 . ^ 0 , 6W> ^/3? 0*37 c^i 039 r>'39 o > M o.rj o.^< G .53 Cond. M f M O ,avA ,^H2. A H 3 >^Hi . A ^ ,^y3 rAH3 .2'^^ .;?V3 , ^ y 5 '?>13 •'V^ .%H3 Turb (An/-) -lOiO ^IdO -ld>0 -i0,6 - ? . 3 -16)0 - / 6 , 0 - 1 ^ -lO'O -10.0 " 0>D - 1 6 6 - i 6 i d -ic.d -/(? 0 DTW (feet) ^o,y %0,<i d.G;Sl ^ 6 . ^ : i 6 , ^ sia^c ^^,5r ^ O i i H 1 6 ^ ^ JO.01 ^ / ^ 3 ^ 0 , ^ ^ 0 } ^ i M ^ ^ . 5 9 Rate ( * / /min) 3/0 ^ / a 3iS ^ J d 7,td h90 3 9 0 />^<^ 3^0> VPo Y^O y / o ^ / O H/0 i^V oRP - a : i -19 ^'h'5 - 1 ^ - Y I y T? f, 7 i < -1 % - 1 Water Quality Meter(s) Ik M .lA ,'7 >a .P j ^ rtA 7^ j ^ 7^ (^ / ^ LHH i m 1.55 r,ss //S< /.&^ A U /<S4 h% /.SC i.s: /.•s^ Tizlir^ A l.^bC 1 • J M I - ^ i|iillllill Notes Purge Start /4/A*t» o/^]^^/ ^£<nfi(^ ^ u ^ / ^ ^ i /<BCf Post-sampling Measu M ^ r k / J - ^ : 2 F n o i f e d Sample Information Groundwater Sample Field 1 Sampling Time l ^ ' - ^ 1 Sampling Method Bailer Sampling Observations - c;cp Panp 9 n( •> fnr n rf^iinH\A/atof ^ D MIM'V3-3/ Sampling End Time U 0^-1 DTW before Samolinq ^ 6 . "S^ (type: ) Same as Above Other amnlinn Par amptprs .fU-- ements ^ O S . '(AAA(A0AAAAA^(AAA<\ 3 0 5 0 3 6 GROUNDWATER SAMPLING FORM Well Number J M i / J " ^ State Permit No. ^ _ _ ^ _ _ Project Name X S u l ^ c l Ci(\.iY\.MCaJi Project Number EH Sampling Date Weather Sampled by: Hart inc. ^ ^ (initials) C A / K C £ ^ r e c ) Well Informslion Well Type: ^ ^ Monitor Other Well Diameter inches Well Depth (ft below TIC) Water Level (ft below TIC) Well Construction .0(f PVC Steel Other Well Screened interval to feet below TIC 7^-y ;)-/7^ Well Headspace Reading (PID/FID) Product Level-if present (ft below TIC) Well Notes (Odor, well condition, etc.) Volume of Water in Casinq (qallons) ( ) - ( _ _ J* 0.0408 = Well Deptt) Water Level Well Diameter (in) gallons Purging Information Purge Method: A'Low Flow NJDEP 3 Well Volume Not Purged Other Pump: TQ Submersible Pump (_^ inch) Peristaltic Positive displacement Other Pump intake depth: C?7 Purge water discharged to: Ground s o Drum Other Tubing: Polypropylene . ^ypTeflon-line Other / v ? New Dedicated l i m e (HH:MM) j 2 | 3 ^--^.o? (:2^is Temp ^ . ^ 3 pH (pH units) 7.iO 7.0b DO. (•vg/t- ) M.zn o-i? Cond. a.scp <3.V3 Turb DTW (feet) 3.3L.O? ^ A % Rate (juf/miD) s^^ - 2 5 - I i'-SY / /.S5 Notes Purge Start I J- V O 13-2K .P^-U 7.0? 0.5S y - ^ ^ T 5 O 13 .( 1.57 i : ^ ^r^i n.i>i 0.31 ^ . ^ y ZiOi.Oo 5^6-0 l b '( 1/-S7 (.3^1 ^ % 3 ^ l . o l <?sz^ 'li.^i' 5a..00 5 5 b ^ / li-SZ 1 , ^ 0 c^')-39. A . O ^ o.^l d.if-J 5^.00 6^0 io I \ l ' ^ 1133 ^ . ^ l.o-X 0.3H c2.47 ^\f\^\ ^57) // n< i/.5S \Vb^ ' ^ . 3 3 7.o>- 0-34 •3.47 <5^.U 5 ^ ^ ./ 7.5s XlAy\ ^ • 1 , ^ 1 . 0 ^ o . y i ^."47 ^ > n ° \ 5 6 0 l-z^ . ( 1/.5S 4 ^ t i ^ - THT?^ -ara=?^- ^M+«- - ^ ^ L J K ^ |l5n P^n ^-j^ ^ppeX l ^ ^ % ^^.35 7 . 0 ^ ^ • ^ ^ a.42 ^( .-'^1 ( ? 0 0 I ] l ^ 1 Post-sampling Measurements Total Volume Purged Water Quality Meter(s) Sample Information fVi.(x)-9- ^^0 4 J p i T l i A n . DTW before Sampling Same as Above Other_ Groundwater Sample Field ID Sampling Time \ 7 ^ 2 . Sampling Method Bailer (type:_ Sampling Observations A ^ r h r Sampling End Time \ 2 J - { ^ J T:>/O -1-3 ^ Fg, " • " > GROUNDWATER SAMPLING FORM well Number State Permit No. Project Name Project Number i i : i t t t o i C i ^ llirciir\ T £ , l o 4 C l C h e . ^ i ' c J Sampling Date '_ Weather Sampled by: 3/^9^/66 3 0 5 0 3 7 ! K H ^ ^ ^ ) (initials) Well Type: )( Monitor Other Well Construction y PVC Steel Well Diameter U ' ' Well Depth (ft below TIC) Water Level (ft below TIC) inches I9.3H Well Notes (Odor, well condition, etc.) Volume of Water in Casinq (qallons) ( ) - f Well Depth He Well Screened interval to 1 Well Headspace Reading (PID/FID) Product Level-if present (ft below TIC) ) * ^ * 0.0408 = Water Level Well Diameter (in) p Q . Purging Information Purge Method: i Low Flow NJDEP 3 Well Volume Not Purqed Other: Pump: V Submersible Pump ( inch) Peristaltic Positive displacement Other: Pump intake depth: f 9 ' Purge water discharqed to: Ground ^'Drum Other Tubing: Polypropylene V^ Teflon-line Other / New .1 ,*'/<: -^K K'O ,t,.4 Time (HH:MM) l',59 2^0i t i l r.i6 7,'.2) s(^U ^ : 3 ( 2 3 i rni rHi- d.-^/ ^ ^^6 V.J 3;oio Vi\ yw^ y 3 i j Temp C ^ ^ ^9/V7 7,^:i^ l7^9,Hh ^9/V3 ;\9,54 2?9/59 t9>hl ;5i^^5 cl9.jr^ ^ • 7 ^ M J Z > ^'{yA am\ d^Xs\ Pii^> m^ pH (pH units) - J M 7,0-^ -V.di 7,o7 1.6C 1.0 b 7,oh l o i l o y TOY ^ • ( ^ ro^ 1,0^ l.o'h 703 1.0^ D.O. \ (tKjl U^, //•SS \ , i i I.O'-l o.'iH <on( 0.60 ,^s wg V7 • V ^ >n .HO .11 (3.U o.^(- o.A^ Cond. \ l ^ j M j J 69 , t c t J6'^ .f6H , l i ^ 7(<3 ^lio ,)^'i . /s-s ^jsrs ./s-Q jn .iSl .150 .ls^ 7CCf Turb ( /VW) —- I h ^ ii9 - 7 / -Co - V . 7 IjJ S;S 9.A ? ? /o- o i O - V "m^fi 10.7 j 6 . i )0S 3^.1 DTW (feet) /M^ i U 9 /939 f 9 , ^ i9,70 nno iht'< i%c% ifci f ^ ^ V /"t^.^y /77^y m^" i^W I W ^ l U i HiH Rate ( A//min) v - . _ _ y ; ? ^ -/s^ — ^ 5 0 hoo r - v?o Y(^V — fOf7 — — 3S'0 Al/ - ^ -n - 9 1 ' 9 ^ ' 9 ^ - 9 3 - 9 ^ -93) - 9 ^ -9cD -89 ' ^ -tG ~t^ •fi< -n -^r SH\rv.^ .c^Jl/yf ,oS- /^^ d,(& ,(H .61 fil >o7 0 7 07 0-? .61 Jbl o l .01 .07 / ^ //57 /;03 l.oH. i.C^ UX i.oA f ^ / o / /.cX. 1.60 1.0b iVO i i * I.OJl H i ^ i ^ ^ ^ l ^ i ^ i i i i i i i M I other eet below TIC gallons =^ 3C ggn ff Dedicated Notes P.r^.s^rf ' i i ) i n Pi^rmp A&4fs /Of/ iofccii STbC fsir^^', (? / S : n Post-sampling Measurements Total Volume Purged Water Quality Meter(s) 0 ' ^ ^ Sample Information Groundwater Sample Field 1 Sampling Time /S'/if Sampling Method Bailer Sampling Observations 3 h'W''^l^^s9 Sampling End Time /JT^O DTW before Samp (type: ) Same as Above Other: inq ni'^i - See Page 2 of 2 for Groundwater Sampling Parameters 305038 GROUNDWATER SAMPLING FORM Well NumDer State Permit No. Project Name Project Number TV! U ) ^ Sampling Date Weather Sampled by: f^^'i^m^ 5--"5-c^r^ (initials) ( / Well information "^ Well Type: ) Q y i o n i t o r O t h e r Well Construction T O P V C Steel Well Diameter ' f Well Depth (ft below TIC) Water Level (ft below TIC) inches 7^-.S-5- ^ . ^ ^ Well Notes: (Odor, well condition, etc.) V o l u m e o f W a t e r in C a s i n q (qallons) f ) - ( Well Depth I Well Screened interval to f« Well Headspace Reading (PID/FID) Product Level-if present (ft below TIC) other =et below TIC ) * ^ * 0.0408 = qallons Water Level Well Diameter (in) Pursing Inform.ation Purqe Method: ^ Low Flow NJDEP 3 Well V o l u m e Not Purged O t h e r Pump: K) Submersible Pump ( 9 inch) Peristaltic Positive displacement O t h e r P u m p intake depth: ( o ^ ^ Purqe water discharqed to: Ground N^yDrum O t h e r Tubinq: Polypropylene y^ Teflon-line O t h e r / yO New Dedicated Time (HH:MtVI) r 3 3 \'6-'ih \^-Hi \^-ii^ $-S7 !8-;5b i'J^-c^f ^^11 Temp •?1.H n-1^ 9^3^ :?^..^i •^i^-so ^f.^'J •:^,h'3 pH (pH units) I f ^ 1 1 1 7,/^ .7/? •7. n- -hi'^ •71$ D.o: (JW<LL ) "^ i.n o^n V ( 1 ^ 1 on2 Otb'K O t h i 0.71. Cond. (#/K) / '^76 7' O.i a 0-lb3 O^C^ 'n/5? 13 '3"^ oJSS Turb f iTlU) 5 / ^ ^;,3^ S.9 & • 0' 0- A^' 0 DTW (feet) ^O-hi \^f^/f 2 ( . ^ ^1.096 •Mw M J I ) H3^ ' ^ ) ^ ' < . € > • ' ., ^\3S Rate (TVA-Amin) 3ticy ^ 0 0 sroo <fm 500 TdO "AOO 66.P 7^^ s> - 3 -•7 ' 7 - t - - 3 Su4t-\ TBS d-O^ O'fJ^ 0 - ^ Ifi?- id- i.oS O^D-?\M 03^101 ^ ^r L^l 5 1 i £^"770/ Notes P u r g e S t a r t cMia') * Post-sampling Measurements Total Volume Purged Water Quality Meter(s) |^fe>^^t& , U ' 2 . ^ ^ V u ^ x i ^ o ^ ' ^ C Sample Information Groundwater Sample Field 1 Sampling Time 7 - (^9— Samplinq Method Bailer Sampling Observations D ^ u J - " ^ 5 Sampling End Time flvoe: ) ( 0 I - ( 9 ^ l u ^'- O'd DTW before Samolina ^ ^ -"e.fc 3 .-tx^-. 1U4. Same as Above Other ' Q , b O - ^fi^:''i ' u^''l^^ntrJ>Q.^J'^!>-} 37/ 305039 I i ; ! •i i w \ \ ^ i \ _ GROUNDWATER SAMPUNG FORM Well Number M U O ' / d Slate Permit No. ^j ^ kv^oco K Project Name Project Number \) I rcj) A J - ^ /^/f y z:^^^.^*/ Sampling Date ^ / ^ • Weather Sampled by: 3/3o/ho B H ' ^ ^ .'^.,^^.,'^^ro^f. o-/on^k /^i)3)L^L ' (initials) Well Infcrmalion . :. .. \ . .^ . . j Well Type Y. Monitor Other Well Construction >(PVC Steel Well Diameter jf Well Depth (ft below TIC) Water Level (ft below TIC) inches / ^ . ^ O Well Notes (Odor, well condition, etc.) Volume of Water in Casino (qallons) f ) - f Well Depth Well Screened inten/al J 2 ^ to S ^ 1 Well Headspace Reading (PID/FID) Product Level-if present (ft below TIC) //c /jy^fs other eet below TIC A 3 f i p i ^ AJr.^ ) * ^ * 0.0408 = gallons Water Level Well Diameter (in) / ^ V ^ -^ / C / ^ Purging Information " ' ' ' 1 Purge Method _X Pump: X Subm Pump intake depth: Tubing: Polypr Time (HH:MM) 7 39 i^n /''sy T.39 V-6i '^^oj i H '^•19 f>-^1 'i-l?) Temp C ^ ri'io zf'^ 7<*Ai9 7,h^9 ^ . ^ 35.^2. 3^.33 •^OMC Low Flow NJDEP 3 Well Volume Not Purqed Other ersible Pump ( inch) Peristaltic Positive displacement Other ^ 1 ' Purqe water discharqed to: Ground )^Drum Other opylene Y Teflon- .1 ICP pH (pH units) U o Gi60 G.el L6i d o e,if Lii L i ^ l ^0.^1 £-63 DO. (JH^I L) .6% .Ci ^CO :hs •^"i ,s¥ ^53 . 5 / .^9 line Other / ^ N e w Dedicated Cond. ;^5? ^ • ^ 9 ,^s9 ;Z^^ .;?s7 ,3.54^ ,^-55 .^S3 Turb ( M f V ) h i 1,3. / S ; & ^S3 H23 H'f>,6 h^.l H ^ i T ,^SV^ x,s.o DTW (feet) I'S,$7 fhf^^ f 9 7 ^ ^9,R t9,lS fhl9 fh^'^ l1,l'^ i 9 , l ^ 19,03 Rate ( »*>//min) 3^0 -hCO HZO HAO HlO ^/O H60 H60 ^ a o 76 70 (^-^ (^^ f3> f:o 5^3 h O ^ Z .i5 .15 Uh i.a 73 f6^ P .6 J3 J:K 'fA 1 : 1 l£S U i /.6i hL3 l a VA\I-^^ Notes Purga Start Ah.,i ptn/>/r. ' • • • - ' — r k/tic ^ / O tul/oiir. ~^ &,.»ple & ' S ' ^ T Post-sampling Measurements Total Volume Purged Water Quality Meter(s) H^r,k I J - X l ^tr.xiul ^ 's Sample Information Groundwater Sample Field II Sampling Time VA3{h Sampling Method Bailer Sampling Observations D / - i o U ' / O / ^ - ^ O Sampling End Time ^'-^9 ^^W before Samplinq / / ' / I f (tvD^ ) Same as Above Jk Other: - See Page 2 of 2 for Groundwater Sampling Parameters | 305040 • 1 * 'I \ • i "•5 • :¥ • • GROUNDW. Well Number State Permit No. Project Name Project Number A.TER SAMPLING FORM Sampling Date Weather Sampled by: ^ 'oannU - 92) "^ K S ^)<?. 1 (initials) :liiii»ii«iiii«iiiliipi« Well Type: Monitor X o t h e r V / ^ T Well Construction ^ P V C Steel Weil Diameter j L inches Well Screened inten/al f l ^ l S ^ o S ^ 3 ? \ Well Depth (ft below TIC) 'J3 ^ 3 Well Headspace Reading (PID/FID) Water Level (ft below TIC) Well Notes (Odor, well conditi( /5^.<?c^ 3n, etc.) Volume of Water in Casinq (qallons) ( Well Depth ) - ( Product Level-if present (ft below TIC) other eet below TIC ) * ^ * 0.0408 = gallons Water Level Well Diameter (in) Purging Information j Purge Method >v Pump: K S u b m Pump intake depth: Tubinq: Polypr Low Flow NJDEP 3 Well Volume Not Purqed Other ersible P u m p f ^ - inch) Penstaltic Positive displacement O t h e r J - 1 - 9 - Purqe water discharqed to: Ground A D r u m Other: opylene X Teflon-line O t h e r Time (HH:MM) 0%^ 0%^ O^Ck C f i ^ mi^ '0" 0 1 ^ iHi ]0>(^ loM io% [ m ^ Temp c€J %.3 <^0.0^ ^ - 0 ? 3ki\ " ^ . ^ %.->^ '^M ^ . ^ * > % : ^ pH (pH units) ^ • | 0 ^.w 10^ 1.(% 1.0-4 l . p ^ 1.0-1 1.01 " t o ^ DO. (tr^/t) O-'fl^ \ 3 \ O.b^ 6 3 1 o.v\ <^-n C-ll 0-1% Cond. (D.>4^ C'.IH^ o.z^^ OlA^ QMh O.V{h O.IM^ om^ -\)^iM^ Turb (NrvA ) (70 Q ^ ^ lOO.C 9^T- "liA n-i icfi '^1 DTW (feet) J f e ^ Poi n"^ . ^ } • iL/Z- %.%^ 11-OV l i c . ^ ^ /(b-<b il^Mh l^.fO | ( . - 2 J 0 -JU+G- Rate ( Tf^i /min) HSo 5oO ^ 0 ^•% (pOO 5oO 6oo ^flT) K o -#e~- / X New Dedicated - ' ( c ( o - | ( ^ ^ -l^-? •-h-2- ' H I "l^i '(^< ' I H - - I t t r - ^90 <<2- 0.(2- O-H o.w d~\i ( 5 . ( ^ O.lZ. o . l l t).a 11?^ A^ i.-a 1 . ^ U'5= f.^ (<5 i.4 i-57 .^ Notes Purge Start B . i 7 ^ \ ^ y 04|V<;K^i^lctP 5)^)^^ l<^ ^ < ^ D C A A ^ »—f>— i fo^i'^W^ie Hiu-'s'n. Post-sampling Measurements Total Volume Purged Water Quality Meter(s) Sample Information Groundwater Sample Field ID Sampling Time ["C^f) Sampling Method Bailer Sampling Observations Samp (type: (\h<^ \;v\MQ ling End Time /OH "3 ) i< Same as DTW before Samolinq Above Other: - See Page 2 of 2 for Groundwater Sampling Parameters i Panp 1 of 2 305041 1 ^ p i GROUNDWATER SAMPLING FORM Well Number A s T ^ / / ^ f ~ i h State Permit No. Project Name Project Number Sampling Date Weather Sampled by: i/io/oo Moi^iy 5v..Y ^ ' = * S3^. r^^ ' (initials) :«iiiiii»»ii«iiilMii«iBiiiil^ Well Type: Monitor 9 ^ 0 t h e r l / « n f Well Construction ? < PVC Steel Well Diameter ^ inches Well Screened interval ,37. I'i to ^ . j 3 f Well Depth (ft below TIC) ^ . t ^ Well Headspace Reading (PID/FID) Water Level (ft below TIC) Well Notes (Odor, well conditic IH.OV 3n, etc.) Volume of Water in Casinq (qallons) ( Well Depth ) - ( ^ Product Level-if present (ft below TIC) Other eet below TIC ) * ^ * 0.0408 = qallons Water Level Well Diameter (in) / » ^ -^ S ] 3 ^ / ) / f / u 1 Purging Information * * Purqe Method: X Low Flow NJDEP 3 Well Volume Not Purqed Other Pump: oCSubmersible Pump (.? inch) Peristaltic Positive displacement Other Pump intake depth: ^ 7 Purqe water discharqed to: Ground ;cDrum Other Tubinq: Polypropylene ^>JC Teflon-line Other / \ ^ New Dedicated Time (HH:MM) y:;w Vbo f . i f r.^o g:Vf ?:si> mf 9^00 ^> ^r/P Temp J 6 M m^ 31^0 h7^n 323'^ i2.0l I Z ' i sj.isr pH (pH units) 1 n l ; l o l I.OS- l.oH lo-i i.o9 i.oi l o i l.of D.O. J 30 M s'i M M ,bi MS- .1^3- Cond. (A5/C/^ ^ . Q l J,l\ ^7^ ^.lU j . n ;?.^l p . i i z ^ Turb ( Arr" ) i ^ o?0 pl 1 0 n 0 0 DTW (feet) \IP(3^ ,f.o^ i i M is.oi iS.O I /irya iS.l3 IS^.O tS.or Rate ( /min) ^So ' — JSO — j e y — JSV — x ^ Scl. L- J 6.( (M O.i oi 0,1 0.1 0.1 9IL 1 I t • ^ . t f H i \M in im lis 137 Illf m OCP -iia^iL V t ' / "jiS^G - J ^ f -2M vv^ vy-2 -^¥J vV Notes Purge Start Post-sampling Measurements Total Volume Purged Water Quality Meter(s) Sample Information Groundwater Sample Field 1 Sampling Time 9 ' 0 O Sampling Method Bailer Sampling Observations Sampling End Time 9:00, DTW before Samolinq l-^- ' ^ ftvoe: ) Same as Above Other: - See Page 2 of 2 for Groundwater Sampling Parameters I Pans 1 nf 2 305042 G R O U N D W A T E R SAMPLING FORM \A/f..li Kfi •rv.«^i.\r ' ^ ^ ^ - - . I . . A 1 T N Well Numt3er State Permit No. Project Name Project Number H O i - V M K ' < -iJ Sampling Date Weather H ' ( ) 0 O F V \ ^ 1 ' ^ ^ ; ^ Ci-cot^'J , foe&.s2V i:60«F 1 Sampled by: |\|. GcticirJ " (initials) ' D ' 6cH/vFi-L- Well Information .] Well Type: Monitor 1 Other V M P Well Diameter ^ inches Well Depth (ft below TIC) 1 - 3 6 i ' . Water Level (ft below TIC) 19.M2' Well Notes (Odor, well condition, etc.) Volume of Water in Casinq (qallons) { ) - i Well Depth ) Water Level Well Construction ^ PVC Steel Well Screened interval27.63 t o 2 9 . ^ 3 f ( Well Headspace Reading (PID/FID) Product Level-if present (ft below TIC) Other ;et below TIC ^ * 0.0408 = qallons Well Diameter (in) Q^Q_^ ._- 7 Q ^ ^ ^ Purging Information ^ ' " . j Purqe Method: 7 LQW Flow NJDEP 3 Well Volume Not Purqed Other Pump: 7 Submersible Pump ( inch) Peristaltic Positive displacement Pump intake depth: 7 ^ 1 Purqe water discharged to: Ground " ^ Drum Tubinq: Polypropvlene ^ Teflon-line Other / v Time (HH:MM) C6H0 OgHS" ag-oo •0 0 ' J -> O'^G'^- 09 OS QSio o^\^ C32si\ 09 Z ^ oS3o o<?35 O^Ho Cf)^6 0 9 5 0 0956 / O o o Temp CCA) ^9.36 29. (oC .ri/^ow^ 1 3o.-2,C ?)0 (?) 3 o . o a 2^.91 2c).^)5 30-IZ 29 £9 3c oo 3o CO 3c 0 ^ 29.'^^ H pH (pH units) 7.5 7,^2. :<.+&At-. 7.15 7-09 7./0 7./0 7 ID 7-0^ 7.10 7.C)9 7 . 0 7,(0 1-.I Total Volume Purged D.O. s-??) M.9M r^fu-v- . . _ v ^ S-.il H 0 ^ -^.32. ^.2)9 ^ . 9 * 0 ^.rl ^.G7 ^ 0 ! ii.6l 2.97 9 . C i Cond. 2.6=6 2 . 8 4 L\/ rviy / 2 , 9 ^ 2.95 z.'-lH .2.S^ 2 . 9 ^ 2 , 9 1 2.96 2.97 2.9'7 2.98 2.97 Turb ( /vTTUJ 7 ^ 9 9 0 - C^rrnt^ ^ 9 9 o P 9 9 0 > T ) 0 9 S G ^ 3 0 8 5 0 C90 <^co 5 ^ 0 ^ 5 0 5 5 0 DTW (feet) 16 . 13 15 33 ^ hc^V• 17. "2)9 |7>^G /7. 3 ^ 17.^=^. 17.35 j7.^0 . ^ ^ 17. 6 & i 7.6Z n . M i 17. 2)S Rale (nnL /min) ^co — ^^5o 5 o o 5oa ( . 0 0 (aOO Ccxj t o o fcOG Goo GO (9 fc^.^' GSC A l i s . 1 1 b3 i J J -1 * 1 , 1 .1 j."t& !.S9 /.g9 '.E9 I,fc9 1.^^ 19c I.TC^ I.Vo A 19/ -1 bo Water Quality Meter(s) other other New Dedicated 0(2-P(r»V Q7. Hfc boc dct cJ-lJlk^-r^t*. U i 3 -1G - 4 - 9 - i o '\^> - I C - j 9 - 2 7 - - 2 4 - Z 2 _ Notes ) Purge Start Icif- f louj . oJ,'ue+rrX Coofrd) m T 'o-Ai.vj— TO be^ ( J J A I L * ^ • 9- ^ ' <-)/v .. . (S f>.tCJU-&T/*JG L)CtLW prciotu ccu-trvu-l-n^coj hcvtrf^afC Poctcompling Meocuromcnts HoClftn I V 2 2 . ^MWiPFN/r - 0 , ^ Sample Information I Groundwater Sample Field 1 Sampling Time IO,'r) Sampling Method Bailer Sampling Observations - See Page 2 of 2 for G roundwater S D fq-jT-\ Sampling End (type: ampling Par ameters Time )G2-"? DTW before Samplina 17.91 ) y Same as Above Other » (0O5 3o.li 7.09 39t Z.99 Hto 17.Zi15o -I 1.91-27 fl.c3U<,T P„t,sa-rH2.i- i c o 30.07 7.,o ^.,7 2.,3 ^ j ^ „ . , ^ ,00 .1 1.91 - 2 3 P I " ; ^ , ^ '0|6 3D. 17 7.io M.oG 2.9'^ 390 I7..MI 5^o . | 1.92 -Z(^ lO^G 30.0H 7.,, ^ r j ^ 2.^^ 330 1738 , .0, , n p ^ ^ 305043 305044 GROUNDWATER SAMPLING FORM Well Number f^.vfA/ n P - X V State Permit No. Project Name Project Number Sampling Date Weather Sampled by: M-Z'1-00 am- (initials) Well Informslion Well T y p e : Monitor - / O t h e r M H ? Well Construction ":/. PVC Steel W e l l Diameter •X Well Depth (ft below T I C ) Water Level (ft below T I C ) inches Well Screened interval ^ 7 1 ) 3 fo.^L'/.JJ f, r:2a.?3 /¥.']9 Well Notes (Odor, well condition, etc.) Volume of Water in Casino (aallons) ( ) - ( WellDepttj Well Headspace Reading (PID/FID) Product Level-if present (ft below TIC) O t h e r ;et below TIC ) * ^ * 0.0408 = aallons Water Level Well Diameter (in) Purging Infonnation Purge Method: / ~ L o w Flow NJDEP 3 Well Volume Not Purqed O t h e r Pump: >>^ Submersible Pump CZ-inch) Peristaltic Positi.'ii iisplacement O t h e r P u m p intake depth: ^ 7 > S ' Purge water discharqed to; Grouiid i V - D r u m O t h e r Tubinq: Polypropylene /V^Teflon-line O t h e r / l ^ . ^ e w Dedicated Time (HH:MWI) i . t ^ a S " ( 3 / S / 3 7 ^ \373' i ' 7 .^ .-N t3i^5~ |B9-^ ^3^5 i "y^'^ j M ^ O VH^AS H\< Temp c ^ 3.x-bT •5S.^9 ,3cl .96 >3.^3 oa.\^ 3i.-^H • • ^ A . S - :-jt. 01 ''3>t-oH 3(M.?_ :>'o.7i SlA^H pH (pH units) -7^9 7..X7 l l H 7. / ! 7.(9 y . i c 7 . ( 0 7 . 0 9 '7.1 o • y . / o '7- il 7.B Total Volume Purged DO. l\3C \ ] • b A /7'fi3 •1-'15- ?/l3 L . i i i (?.^S y-'on l A 7.0 9 7 - ;Za... Cond. rt-^va. 0-^-99 ^•^.^VS" o.c^¥5 o-Av-,- • O . c l H b 0 . ^ 9 6 Q ^ ^ : ^ o.'^^b 0 . 7 A . . [ L Cj'mu n,997 Turb 1 DTW ( ^ ! ' ^ y ' l i ^ ^999 7'?<?9 > 7 9 ? 957 .^6i< '•AS)- 3,3 G 3 i ?- >5n?-,. A?;^. ^39 (feet) ! ? . l ^ ' i'l.ioi \tiA. \i.3i- n-^7 . Rate (i^^rmin) DTTD ()60 9 5 0 557> fccD • l i ^1 ' / / - 7 -12 ^7<-( . . " } • " -23 -2-7: . ' X O ' 2 . / - | i Wafer Quality Meter(s) •ji-t rTtTuS % IH- -.l^fi.55 - i i - M - T l ' / Z l f ^ S / 7 c . \ i . j ? c|2!i.57 . / z i ^ j f ' ( r |;-o'; .129.57 - '^ i/55^ .• i'a.i:!^ . n A i - ^ . n Uiv' • Notes Purge Start ! d v 5 M TVa^A.bfe' ^iXi-v-laA'-Air.o 3 i A v m A ^ ^ ^ ^"ir- K'i-'-Hfej Tn 9M^3e-. I'q f j 3 ^ 7 ^ 7X5 0 f, Cj yM - • i \ \ - n > i > ' . f \ - . r ? M .'-Mf (^-f A- .V , .i U 1H!'0 Sft-Yt'i-^ki; 'fej^»v^.... P o s t - s a m p l i n g Measurements Sample Information Groundwater Sample Field ID Sampling Time Sampling ri/lethod_ Sampling Observa t 9 l . . Bailer ions S a m p m.-^-^ V > ' ' ' f ^ - . i - D ling End Time (tvoe: ) \-s\A _Same as DTW before Samp Above Other ling -* - f -^ . _ . /-- .J....,•«, c a m n l m / 1 P a r :>mpii.T% i ; 1 w k ) GROUNDWATER SAMPLING FORM \ A / o l l M l i m K a r A / " "T" U V V A A ^ T-^ Well NumDer State Permit No. Project Name Project Number ff? 1 - YI'U'- .'v^ Sampling Date Weather Sampled by: ' 5-r- Su..:^.r: ^Ae^ "- (;"%7 3 0 5 0 4 5 l ^ ^ ' ^ W l ^ H: 3)S '' (initials) Weiyhformslion Well Type; Monitor ' / o t h e r ''l'^''*^?' Well Construction X.PVC Well Diameter ' 2 ^ * ^ Well Depth (ft below TIC) Water Level (ft below TIC) Well Notes (Odor, well conditic inches 1^>-H'' jn, etc.) Volume of Water in Casinq (qallons) ( ) - ( Well Depth Well Screened interval ' ^ , t 3 Well Headspace Reading (PID Product Level-if present (ft belc ) * ^ * 0.0408 = Water Level Well Diameter (in) Steel toA^i.?^f* 'FID) wTIC) other set below TIC gallons Purging Infoimstion Purge Method: x Low Flow NJDEP 3 Well Volume Not Purqed Other Pump: X Submersible Pump (2. inch) Peristaltic Positive displacement Pump intake depth: '7^1 . S Purge water discharqed to: Ground VCOrum Tubinq: Polvpropvlene '>.-' Teflon-line Other / V.. Time (HH:MM) 1^52-2 1S2S \5T.V ^^33 [ 5 3 c. ! 5 ^ ^ 1 S'(>- is'M?; 1 9->rh ^65i .55H ! io "•• A Temp C O ) 7'\.2.1 3o.'i.7.. '4=7fc 3 o . ? ' t .-.» O- I j 3o .51-- 3o.'4i^' 1)0 l\h r»'^'5'i 3^.^rt, 3o.At pH (pH units) 7 l 2 '^. eg 7 . 0 6 l - C - ^ i ^ 7. ^2 'J)_, 7.c:> 7.5 4- '7. .o:>- 7.c< ' 7 - c i 7-t^/ 7,Db Total Volume Purged D.O. 2-33 ^•.3r2_ HAjZ M .31 M.f7 M.0'1 H.d<^ i 3 y H.c.l H.c->- •^.^ts M>6'b Cond. (V-) ( > 2 ^ 0 7 7 0 0.275 0 . 2 . 1 5 ri.-XlJ O.J>'7S o..}-/S 0 . * ! ^ 0 ^ ^ ' 7 o c • :>:'.6'' 0 ..'>7/- O.^-l^:: Turb (WtU ) 7c-T H -ZM . I h 3 ' — l 3 \ . 7 A ^ . 5S.7 3;i.s. il^7 "13 ? • ! • DTW (feel) \ i i 3 l r/.'i r7.>^ n-:tH- n-i'i- l7.'i< Rate (r.\C-/min) HG"o H ^ 0 bO'O 3PO 5 3 0 I^W fwV H-Of 30 y-' \6-7 tZO' '"^ 0 & 0 ' - • ^ • Ha- 3'i' >o b •? Water Quality Meter{s) Other Other New Dedicated :;cij ! -rrns 7o i.7L -IH H77 .*H iii6 //^ (i.% . . ( f / i 7 i J4n7fc A-^A-'lh .S^AAi'.. ,)H |(.?i. ,)^M7fo .H i^77 .''1:1.77 i .Nn.-77 Notes Purge Start ( 5 2 7 (\(Xi!,e.A Cf'^i-u .-f.-ki -ASx.'A-M - ^ J ^ X-\:?:0 Slfj.^iiJ. (lvi>Jr\ a r A i S 0 vO v«, , ;SlU^-^+ ^'d-.-r AjiM-M^l • '7 .- >-./ aoz- 5o^/^ Post-sampling Measurements Sample Infomnation Groundwater Sample Field ID p S T • A/f A,P • Sampling Time "\ t QiA Sampling End Time Sampling Method Bailer Sampling Observations - <^l=o P a n « 7 fif 7 fnr O, rnundwater £ (tvoe: ) :?' VT> _Same as DTW bef Above Other amolino Par ameter* ore Samp lino • /' '^3 1 i ; i ;: 1 i i GROUNDW; Well Number State Permit No. Project Name Project Number fl^TER SAMPLING F( 3RM Sampling Date Weather Sampled by: 3 0 5 0 4 6 1 6v^ori^ - *S0-; h)1, v ^ (initials) Well Informalion ^ ; = " ^ Well Type Monitor ^ Other V M ^ Well Construction X PVC Steel Well Diameter " ^ Well Depth (ft below TIC) Water Level (ft below TIC) inches ^ ^ \^A^ Well Notes (Odor, well condition, etc.) Volume of Water in Casino (qallons) ( ) - ( Well Depth Well Screened interval Zl-'^Oto 1 ^ - 0 i Well Headspace Reading (PID/FID) Product Level-if present (ft below TIC) Mix<\^ ,v.)e)lcA^iSV^ vJo^lif-clo\44-ir^o ^;^V other eet below TIC ) * ^ * 0.0408 = gallons Water Level Well Diameter (in) Purging information Purge Method: y~ Low Flow NJDEP 3 Well Volume Not Purqed Other Pump: S^ Submersible Pump (T^-inch) Peristaltic Positive displacement Other Pump intake depth: ?7-ij? Purge water discharqed to: Ground XOrum Other Tubinq: Polypropylene XTeflon-line Other: / ^ New Dedicated Time (HH:MM) i l l ^ Wh 111,^ jfLC. iw^ M^1 jlh^ )im Ii4b 1^1 W ^ iloi (lOio ItH^ Temp ^ . ^ ( ^ ^ . 4 1 -m^ ^.?o ^ . i H •^.01 rUH ^^.<?g ^^o.u pH (pH units) (o.^iA m-^ {^m {,<n^ ( , % &-^5 io9^A Ip^^ (,p\^ DO. ) 13<^ ( y . ^ l.i^ l<l^ 63^ O - l ^ ^^^t' O^t^ ^m Cond. f ^ / r n ) 0.10 0 . I h l ^ Q.W( d-Uo-l Q.m ^.us f).yJi 0-24<? 0.1M^ Turb (JJT(^ ) W m^ q^c^ ip^'b H% 4t>/ 4 ^ ^ H3b ^ i \ DTW (feet) \(\.lh yd3 %\3^ V3^ 707O >-SD i^.^^ \ \ 3 l \%.10 \%3^ ^ ^ - ^ /^-S^ 1%9M^ ' / fi.% Rate (td /min) •3oX) \^(sr) iooO 130 7 1 ^ 1fO ^ ^ 1 ^ 7 ^ T ^ l3b ^ 6 0 1*J '|41 •• ' ( 5 7 AhO A % -151 -I4S -14? -11^ A l ' ^ Q^l OA 0 3 0./3 <5-(3 ai3 m 0.i3 0-1^ iiS> i.b8 /-7 '7) (.1^ Ml ni i.U /.1^ Notes Purge Start \\13 /IcIjVsV H ( ^ 3 3 ^ V \cr\^AoV /)^^^XMA (Ujt^^^Jpov'-K GO^''^y.K. • ylcvJ-TlM dW.-) 4).^>/v •^ / Post-samplinq Measurements Total Volume Purged Water Quality Meter(s) Sample Inforniatlon Groundwater Samf Sampling Time Samplinq Method 3le Field 1 Bailer Sampling Observations 0 f-fbT-^M/'-a Sampling End Time (tvoe: ) A j(? Same as DTW before Samp Above Other [/>A'\,CM^ Lclkdii - f4^1'MWP'ZOP lino 1 - See Page 2 of 2 for Groundwater Sampling Parameters j Paqe 1 of 2 » ^ w J GROUNDW Well Number State Permit No. Project Name Project Number M E R SAMPLING F( 3RM f X I ; 305047 Sampling Date i / ^ o / o o Weather Sampled by: 5o>v>vV - ? © ' ^ , r 2 / ^ ^ (initials) ^ i i i i i i ^ i i l i i i l i i i i i i i i i » l i i l i i i l « ^ Well Type: Monitor '>SDther \ f ' ^ ^ Well Diameter ^ Well'Depth (ft below TIC) W i t e r Level (ft below TIC) Well Notes (Odor, well conditic inches .?o./o H.f^' Dn, etc.) Volume of Water in Casino foallons) ( ) - ( Well Depth M i v ^ ^ l> c/»(.c^ ) * Water Level Well Dian Well Construction ? ^ V C Steel Well Screened interval j 7 . 9 o t o ^ . 6 0 1 Well Headspace Reading (PID/FID) Product Level-if present (ft below TIC) other feet below TIC ^ * 0.0408 = gallons leteron) ^ Q ^ - . ^ J Q , ^ ^ \ 0 , ^ ^ J L C O ^ Purging Information Purge Method Y Low Flow NJDEP 3 Well Volume Not Purqed Other Pump. V - Submersible P u m p ( o ? inch) Penstaltic Positive displacement O t h e r Pump intake depth: ^ 7 Purqe water discharqed to: Ground ?^ Drum O t h e r Tubing: Polypropylene "/-Teflon-line O t h e r / X_ N e w Dedicated Time (HH:MM) /O'l^ /ojo I O J C fOhO a i f /O'/O I09f IO$b 1 0 ^ II00 m3 lU Temp 3MZ ?\.7> l U l 3/.s-\ 3\.si 3 1 ^ % }\M X^o ii5i 3o?x)6 3M^ pH (pH units) 6.71 6.77 In.^^, (p.'S^ U l L ^ (,.10 C.^^ tff.93 fc.'fi G.15' DO. ( f l ^ l l - ) 6.13' o.oi b.^r 0,S3. 6.^^ AV3 o.^lA 0 . ^ ^ 0.^^ OAl 63V Confi. (fi6lcAi) 1 3.0^ j . o r 303 2.0). 3.01 3.0\ 3.0 ( 3.o\ 3>02 3.0^ 3.02 Turb (A/Tv>) 3^ Ho ' K / ^ ^ 1 ^ (o3 11 VV ^3 V3 % Total Volume Purged Sam Groundwater Sample Field ID ft5T-'"^^-'3ti Sampling Time [jOi? Samplinq End Time Sampling Method Bailer Sampling Observations (tvoe: ) - See Page 2 of 2 for Groundwater Sampling Parameters DTW (feet) ]i.^'/' H . l ^ I W H.n 19.70 K i . 1 i i O l mo ii.i.1 H-C'l >M iU$ Rate ( /min) 3^0 — j ^ y — j ^ f — 3V 31(, - ^ — ^ 3 ? S A t 0.) <J./ ^'} oA OA 0.1 o.\ CA ^A [>/ v>s 197 i9r /,?f m i.'^j m 137 )HA Iff} i ^ 04 m oee -c7J3 - a ? ) ^ V)b -PC?') 'PO(^ -70(i> 'ofoH ' a ^ O ^ " o P O O - / ' ? ? - m Notes Purge Start fu//»j'^0 i^s^ll^J Post-samplinq Measurements Water Quality Meter(s) W^Z-sSPr 0 - ^ - 2 ple Information \U0 DTW before Samp Same as Above Other lino 305048 • GROUNDWATER SAMPLING FORM Well Number ^ ^ T \}f\'\ P ^.b State Permit No. Project Name Project Number Ea^#^ Sampling Date Weather Sampled by: "^'-3-00 S v o ^ y , -^ S^<9 ii.n-^lnl..^l•^r<: (initials) Weiliinformalion Well Type: Monitor V Other Well Diameter 'Z^ incf]es Well Depth (ft below TIC) Is^* Water Level (ft below TIC) U I M . P ^3.oi^ JSM. Well Construction j £ . P V C Steel Other Well Screened interval 2 7 ^ ^ to 9^. (t feet below TIC Well Headspace Reading (PID/FID) Product Level-if present (ft below TIC) • Well Notes (Odor, well condition, etc.) Volume of Water in Casinq (qallons) ( ) - ( . 2 * 0.0408 = Well Depth Water Level Well Diameter (in) gallons Purging Inform.ation Purge Method: SA-OW Flow NJDEP 3 Well Volume Not Purged Other Pump: v^Submersible Pump (_2 inch) Peristaltic Positive displacement Other Pump intake depth: ^ 9 J O Purge water discharged to: Ground )^Drum Other Tubing: Polypropylene 77 Teflon-line Other / ^ N e w Dedicated Time (HH:IWM) (OPS iOo'i M3. Temp ( ° ^ n£>6 S9A3^ pH (pH units) 7 3S 7.77 D.O. /&. 3 ^ d.l? Cond. (y"^) l 7 ' ^ / .^.xr? Turb (JJIUJ >f?9 y 9 9 i DTW (feet) /33I n. 33 i i J ^ Rate (^^J/mln) ^TO .no oRP 1 3 3 &2 SdL Tjy m^ L IILL. 0.13 a n f47 U(3 Notes Purge Start ru^l:>,J -,'/3 y mi- n i b l i ' i L^l (P'QS'7 l ^ l " ^ l l ' l l :iTo 1 C-./5 U ^ Sf(\^-hUo j v |-Lut.i? cAc ; ^ JQ_ 10:93 ^tn l.R ^3b o-'^a li'^^'i nx'b ';LS'^ ^1 ( 0 - ^ T \ 3 1 1.(3 2Jzl O-^'^b SM. 0;3\m ujw;-fe-; C r e <*^Hy '^i<iei» iia'2 o^ro Z9 0A,-?3l.b3 cJp(iy')',A ^ /P--33 n 3 2 7 r 8 ^,23. g-js~5 I t J ^ I0-3>S 9^. S3 77'g S^Sk g'.JS'j- ^ 9 2 OM a-vo 3 d o-i2\al 13M. ^XX) • 5 9 C7./-2!A^ [033 mi 3LJ2. S.i^'O 03^"^ JAO O M ^Sro - X 2 m> ib3 M l mm •3m. S3lk 03^'; 3ii n (^ Sy?; ^3 0-33O 3 S'3 m03~ I O l A l T. -:^3 <^-^T% 3&0 l l / O ^S7J - P 7 <MM33l jQ'^r^ 3 P J 3 1 3 b S 3 0 Oc?S<. 3SH' i l o < ; S30 ' 31 ^oW^AP ML -? 0--3G 7/r 3..91 0''^~3b 3 ^ n^( '3^0 - ^ 3^ 0-(3\i7}3 Post-samplirig Measurements Total Volume Purged Water Quality Meter(s) Sample Information Groundwater Sample Field ID / t S T VJmP "2.^^ \;Q-t-ScA^''3ii2- 3~A0O Sampling Time \ \ - f} Q Sampling End Time \ V \ 0 DTW before Sampling Sampling Method Bailer (type: ) Sameas Above Other Sampling Observations C^Oo - 3 ^ ^ ^ . ^ ^ ' O f ) - .^.^fvL<{/L '^ ^^•>^^^-^:io(o'^ 3^ ^^^T? /y>/i— ,r,Hw=ior <;pmnlino Parameters 305049 G R O U N D W A T E R S A M P L I N G F( Well Number /)6T- \}{)r^f- ^ P State Permit No. Project Name Project Number DRM Sampling Date Weather Sampled by: 3SM ^o^rxrU *^H rO^# (initials) ricirL. Inc. Welllnfortrtalion Well Type Monitor ;<( Other ^ M f Well Diameter ' j y inches Well Depth (ft below TIC) ^ O . l 5 Water Level (ft below TIC) /^.^1 Well Notes (Odor, well condition, etc.) Volume of Water in Casinq (qallons) ( Well Depth ) - ( U-. V. fO^jJw-N " ) * Water Level Well Dian Well Construction X P V C Steel Well Screened inten/al'J.1-9^ to W.^-^ f Well Headspace Reading (PID/FID) Product Level-if present (ft below TIC) no o\l+ tclcr Other eet below TIC ^ * 0.0408 = gal leter (in) Ions Purging Information Purqe Method: ) \ Low Flow NJDEP 3 Well Volume Not Purqed Other Pump: y Submersible Pump (2- inch) Peristaltic Positive displacement Other Pump intake depth: p^-1 Purge water discharqed to: Ground V-Drum Other ' Tubinq: Polypropylene \ Teflon-line Other: / 7^ New Dedicated Time (HH:MM) m\ miy m i im \ 3 ^ \h^{j^ 1401 W0(^' H^[ W4G H3\ m^o Temp ^.^^ n^^h^ %Xi3 hb.^V ^;e^> ^ . 1 ^ " h ^ . ^ pH (pH units) (.-"iP l,S<^ b.'f^ fp.^s (^.V <p51 b-^^ D.O. (M-/-L) t30 oi>^ <^?i'\^ ^ 3 \ 0^?^ 6 . ^ / 3 A ^ - . ^ . , • . " 0.^^ Cond. ( ^7r« ) 0 3%> d.vn O.n-t G-tT? d^% b.vu % 33. 331^ Turb (Nm) ^^/ w AhT- "^^^ ^v ")% 133- Total Volume Purged Sam Groundwater Sample Field ID f \ ^ U \j{(\f^ ^Q Sampling Time lMl-4 Sampling End Time Sampling Method Bailer Sampling Observations (type: ) DTW (feet) «.o' ?0 nMh J0,3^ /'?.4q /(.-/< /s-^1 /$flo /^-«) /5.9^ i^/C( ^.u Rate ( rA /min) I'^oo m> 3 ^ I'^OO A 9) 71 <« ?T5^ 1^0 7 ^ ( r ^ 1 ^ -731 - h o - l ^ ( ^ A^3 ^ l ^ ^ 7^1 - j ^ 4 ^ 3 h 0.)4 111 OiH l.-^^ 0,i4 l-TT OJH l.-n 6.11 i'ii D-C* irn Notes Purge Start O A 4 (.1' Post-sampling Water Quality Meter(s) pie Information _Same as DTW before Samp Above X Other linq Measurements i i ^ l M i t t i i J i i i i - See Page 2 of 2 for Groundwater Sampling Parameters ' Panft 1 of 2 305050 G R O U N D W A T E R SAMPLING F O R M ^ Well Number A f y T U M P - 2 ) 0 State Permit No. ,,^ tm»3f\ Project Name {;'/«.>« T^ /aid /^A^m.i^i Project Number —_, _ . . . . Sampling Date C^A^- Weather Sampled by: • Z f 3 o / ^ SiJHH:/ ' ? ^ ' g S ' ' / ^ , ^ ~ 7 0 ^ - f i K (Initials) ^ Wei! Information ^ -- Well Type. Monitor / Other HdAif HiitJoCut Well Diameter ^ Well Depth (ft below TIC) Water Level (ft below TIC) Well Notes (Odor, well conditic 1 - inches •30./^ _ _ j ^ L 3 ^ — m, etc.) Volume of Water in Casino (qallons) ( ) - ( Well Depth Water Lev ) el .w <f / V vVell Construction V PVC Steel Well Screened interval :?? 7 ^ to ^ I C h i Well Headspace Reading (PID/FID) Product Level-if present (ft below TIC) Other eet below TIC ^ * 0.0408 = gallons well Diameter (in) ^ ^ ^ ^ / ^ ^ , ^ ^ ^ ^ / ^ ^ Purging Information Purqe Method \ Low Flow NJDEP 3 Well Volume Not Purqed Other Pump: If Submersible Pump ( ^ inch) Penstaltic Positive displacement Other Pump intake depth: 2 % f 7 t Purge water discharqed to: Ground V^ Drum Other Tubinq: Polypropylene _y_ Teflon-line Other / V New Dedicated Time (HH:MM) IfiZI r.d^.9 1\3H 9-59 f . i i f 9' r9 ^ ; . ^ / 9-^9^ 70] (Pi f o M fO/^i 1^/9^ if, \7)0 Temp CCA) ^ 30,0^ M / l i3>/'/6 z/.a's 31.^1 V3>'^ •3>i:33 3 / . f t ^IMO y , i l i3.Cf pH (pH units) — 7,0^ 6."^% &90 6,91 6.93, MOL iiC.^^ ^.n C^3 6t^3 (.i^iH D.O. (*<j/^:) 5/ I.Oi .35 = 3 3 O i H l O M 3 0 . 5 / O i ^ \ 0,-31 0,<3i Oi^'b 6.U Cond. - ^ ,931 .^75 ,:ai A{9 a o ,2(3 i U S . W l ,^<5 ^^a , XI6 Total Volume Purged Turb ( / V W ) — 3^<^ i^:i ^69.9 /oX chH /oi (31 m ^o3 ^d loS DTW (feet) H 3 ^ ,i,e^ H^"^ H.A^ I^C^ IH,CH IH.63 11,(3 tH.CS li.U ii(^ N33 Rate ( /%/ /min) • ^ ^ 0 ^ 9 ! l ^ 9 0 ^90 ^<)0 X(iO ^90 ^ ' ^ ^ aao ,?lf^ i ' ^ m — -55^ -aBS - ^ H l --Siis -ZH^ ' 2 i 0 -739 -^3T -;B? '739 •^n ^ n //V 73 ,/3 ,3 ,i3 ,13 .il S ,13 ./3 I7PS. — /77 h i i l-lH lA^ in/ ino 1.70 /.el i39 /;/» S /7? Notes e^r^^.3-hrf 3^^pl^P /^'vA.i, / L^ / Post-sampling Measurements Water Quality Meter(s) lAvrihiK Sample Information 1 groundwater Sample Field ID Sampling Time /O'-jiO Sampling Method Bailer Sampling Observations Samf (type: )ling End Time / 5 ^ 7 ) Same as DTW before Samplina H 6^ Above K, Other - See Page 2 of 2 for Groundwater Sampling Parameters | 305051 GROUNDWATER SAMPLING FORM Well Number / s T \ j (Y) ? 3 D State Permit No. Project Name Project Number Sampling Dale Weather Sampled by: ^c^w^y •^SS-90 SC ^ c ^ \ ^ (initials) H a r t tnc. Well Informaljon Well Type: Monitor (/? Other V ^ P Well Construction ^ PVC Steel Well Diameter ^ inches Well Screened interval j2^,4'i'to ^ ^ ^ S ^ f< Well Depth (ft below TIC) e ^ ^ . * ^ ^ ' Well Headspace Reading (PID/FID) Water Level (ft below TIC) / ^ ^ ~ / 3 " Product Level-if present (ft below TIC) Well Notes (Odor, well condition, etc.) Volume of Water in Casinq (qallons) ( 1 Well Depth ) - ( % ^ k t R ] ^ . Other ;et below TIC u )* ^* 0.0408 = gallc Water Level Well Diameter (in) )ns Purging Information Purqe Method: y ' Low Flow NJDEP 3 Well Volume Not Purqed Other Pump: >3 Submersible Pump ^ inch) Peristaltic Positive displacement Oth Pump intake depth: • / ? , & ' Purge water discharged to: Ground /JSrum C er ther Tubinq: Polypropylene Z? Teflon-line Other ' / y ^ New 1 Time (HH:MM) 1 ^ 1 ^ / 5 - - ^ /^-?6 \/Si3l 1^31 /^:Y/ i^^% IS^- $1 Ih-.'Sb 16 ^-01 ly-oi \}U2 Temp (-4) r i ' ^ ^f. DS ni'6 3 i n v-v 3^-0% 3373 ^ 5 . ^ ^ %.y\ 3 a. 3« '3/.s-^^ pH (pH units) 7.0{ (pA2 r^.^^ ^.^f ^-fV h.f'^ ( o i i /..'^r L9<; f ^ ^ ^ ^ (^31, D.O. 3,27" < ? . ^ 0.3G 0<32 0-}0 0 ' ^ o.n o.?S 03H 0^03 ' /?.29 Cond. / 3.;i6 ^ , 5 / ^ . ^ 5 ' 3 3 / 3^:if ^ 3 r ^ y 33?^ 3.^S ^.af $.7^3 \n Turb ( ^-Tt^) >^'?(? -nio y w I W 53D H70 3 3 i 0 ^GO ^ 3 0 ^00 320 1 DTW (feet) 'l^.^l n.w i ^ n /^,7? 1^ ^0 i^m m j o fS 1? mn^ n-hl id.n (^i. ' A A . 1112 Rate (^(?/min) SOD soo '>oo 3DO SCO SOO SCO ^00 SOD SOD f C ^ c O fiP-P MlJ -^/9 -^1>S •'^yi -35-1 - X l ^ -2\o 'ao6 - : i o ^ ' 3 { ? 3 -::ip/p - / 9 7 9", <}•( d-{ &3 l l o3 o3 0.1 a.\ (?l Q-\ \ ^3 , ; t ^ XA M 2.(2 2J0 U^ f-o^ 9-in Xol i-Dl Ol |p-^ Dedicated Notes Purge Start SvC ^ . r j Bffc*-H,iWk8Ru _^/ \—: Post-sampling Measurements Total Volume Purged Water Quality Meter(s) £^,.,v,... ^ LA-ZZ - o ^ fl^.A bo-. Sample Information Groundwater Sam, Sampling Time Sampling Method. Sampling Observa 3le Field 1 Bailer lions D fi#rOMl>3D Sampling End Time 1 ^ O"? DTW before Samp (type: ) Same as Above Other lina 305052 GROUNDWATER SAMPLING FORM Well Number A^3 \JD/\f> 3 b State Permit No. Project Name Project Number EO'V^f^ Sampling Date Weather Sampled by: S^- 3 - o n >^vA (A <y •JL13. S ^ ( (JJ'R - ^ r < X ^ . (Initials) Well Informslion Well Type: Monitor ^ O t h e r \ J (V^ P Well Diameter ZL inches Well Depth (ft below TIC) ^ 1 . 0 4 Water Level (ft below TIC) Well Construction >^PVC ^ F Bteel Other /r^7/ Well Screened inten/al 3 7 , 9 T to 3 ^ ^ f feet below TIC Well Headspace Reading (PID/FID) Product Level-if present (ft below TIC) • Well Notes (Odor, well condition, etc.) Volume of Water in Casinq (qallons) ( ) - ( : 0.0408 = Well Depth Water Level Well Diameter (in) gallons Purging Information Purge Method: _ K £ o w Flow NJDEP 3 Well Volume Not Purged Other Pump: X Submersible Pump Cp'inch) Peristaltic Positive displacement Other Pump intake depth: . ^ S ' Purge water discharged to: Ground vjDrum Other Tubing: Polypropylene .Vcn"eflon-line Other; / %c~pew Dedicated " y j i l l ^ ' Time (HH:MM) i^ \0 [ ^ O Temp CC>> n3^ Sl3il pH (pH units) l.oo D.O. 2.0b Cond. (SfcAA) O . P ^ Turb 7n^ DTW (feet) 13321 n.u Rate (s^x ^/min) 3O0 o^'> zllL ccfl/.n Notes Purge Start {2-1^ hc'lh i.n 0- .3^5 >^f^ /Mil ^ O O ^312 o-i ^ f S Z Oil 2 %n U2. I 09 O'^^n >^n ml too 19S amf-ii Post-sampling Measurements Total Volume Purged Water Quality Meter(s) '^XyA^bk i ) ! - ^ ^ ^ / ^ • c j i J t ' ^ O ^ Sample Information Groundwater Sample Field ID A<>'r \)i'y\P S t 3 ~ \r<3(Ail>0 p*s3AiAl^<^ fc^f Sampling Time ) ^ - ^ | Sampling End Time DTW before Sampling Sampling Method Bailer (type: ) Same as Above Other Sampling Observations 'gQjv^r>6>..v^ f ? 9 f t X7D ^ I . S ^ ^ A C 11— 15'^ W ^ 13 ru^j(. !~Fe Paoe 2 of 2 (or Groundwater Sampling Parameters —A GROUNDWATER SAMPLING FORM \A/all M i i m K a r il\L.-r \ ) l \ P - LiC~) w e n NumDer State Permit No. Project Name Project Number r \ - n ' v / * i i i i y Sampling Date Weather Sampled by; ^^1^-60 3 0 5 0 5 3 KH'T^f^ ^Uo'VWOuj ^50$ N t i US (initials) ;iii«»ii»iiiiiiiiiiiiiiiiiiii^ Well Type: Monitor X o t h e r V M f Well Construction X PVC Steel Well Diameter ^ Well Depth (ft below TIC) Water Level (ft below TIC) inches 30 .11A I3<;(. Well Notes (Odor, well condition, etc.) Volume of Water in Casinq (qallons) f Well Depth ) - ( Well Screened interval J ^ S V t o ^ ° i T l - Well Headspace Reading (PID/FID) Product Level-if present (ft below TIC) other feet below TIC ) * ^ * 0.0408 = aallons Water Level Well Diameter (in) Purging Information Purge Method: V Low Flow NJDEP 3 Well Volume Not Purqed Other Pump: X ^ Submersible Pump ("2^ inch) Peristaltic Positive displacement Other Pump intake depth: T i ^7- Purqe water discharqed to: Ground N Drum Other Tubing: Polypropylene Y- Teflon-line Other / )^ New Dedicated Time (HH:MM) f^^ot i^H )^{>C /'5m I3cf\ /^(( l^^ |S(^ (SVo C^V^ \hh3 ^6^? mh m^ licOl Temp CCJ 3d.i^ <^.3 -h.iA '^•HO •^0(1 'bd.^^ W i ^ 103 pH (pH units) 6.^^ loo 1.00 •1.O0 (.•^^ \ o % ii.'H (f.qi/ D.O. 0.(^0 O.V^ O.U 0-T^ O'V^ O-IM 0-^^ e.v^ Cond. 3\^) 0-Z40 0-%\ o.iw C Z i ^ O.lM G-lipO 07tf D.^O'l Turb (NaV) S^S ^ ^ ) aiz •'ben "hod ^ l ^ 1%^ m DTW (feet) N-1, }m< \^A3 H-O m K3b mz H3b h¥? iit^ M N y^.ig Rate (("^Jl/min) V^oo Z^oo z-^oo ThTP 'fiiOO tSoo ^ 1 ^ ' ' l < b (oOO (oOO (pUV 6in> ^-7'JO 6?W ^ i l t -\\% -M< ' M ~[[V -(0(o •-IO7 - ^ ~ < ^ S d a ^•^<o 0.\i it-f 0 3 {^•^ O.lJ Ibl 0.|3 l.(pt. O i ^ [\i (5.(^ l-t-l 0,1^ )-^ Notes Purge Start 4U4 {co^h^J (lri]ih3 ho^ " A Post-sampling Measurements Total Volume Purged Water Quality Meter(s) Sample Infomiation Groundwater Sample Field ID Sampling Time i S 3 3 Samp Sampling Method Bailer Sampling Observations ling End Time (tvoe: ) _Same as 1 DTW before Samp Above Other inq - See Page 2 of 2 for Groundwater Sampling Parameters | r»««rt •< rtf o 305054 1 ' ' 1 w m 1 G R O U N D W A T E R SAMPLING FORM Well Number A 3 T \ 1 M P ^ 3 3 State Permit No. ookwf...-'v Project Name Project Number Jii^>r^:ts'/<^"C^ C k t : i ^ i c ^ . Sampling Date 5^y^- Weather Sampled by: 3 / 3 0 / 0 0 3^^A./ . 3i^90^7^ . 7C)rji^k d^l^'.h/.. ' (initials) : Well {nformalion Well Type. Monitor ) ^ Other OcO.- r MAAACC:,^ Pf- Well Construction X P V C Steel Well Diameter • j ^ Well Depth (ft below TIC) Water Level (ft below TIC) Well Notes (Odor, well conditi inches /^.^-r 3n, etc.) Volume of Water in Casinq (qallons) { ^ - ^ ) - f •^ell Depth -iO Well Screened interval ^ < i / i h o ^^.9,1^ Well Headspace Reading (PID/FID) Product Level-if present (ft below TIC) 5 i , 7 r ^ r ^ other eet below TIC / ' , .... rtcjKs 7>le3cr/i' •• . _ , u , - " ^ ) * ^ ^ - ^ ^ ^ ^ * 0.0408 = qallons "water Level Well Diameter (in) / ' / O ' J m a / 1 Purging information Purge Method X Low Flow NJDEP 3 Well Volume Not Purqed Other Pump: V Submersible Pump ( .^nch) Peristaltic Positive displacement Other Pump intake depth: ^ ^ i ^ Purqe water discharqed to: Ground X,Drum Other Tubinq: Polypropylene )(Teflon-line Other / V New Dedicated Time (HH:MM) /o:33 tiOO t l -bS l i • i O / / 7 S /•/ 7^0 // -7^3 II-30 i r . ^ ^ ii 30 1133 H-hO •r-33 R-oO /a:o5 l X / 0 Temp cc^ ^ _ 7,^^f 3040 30.59 •?idM 3ociS •ho.Hl ZOt'i) 30.HA. 3c.^l 30 3 ' i SOiiH 30.Hi 30.Si 30>60 -.30 7 y pH (pH units) — 1/b 7,cl 7.t)^ 7,oS 7,oH 7 OH 7>03 7.o3 7,03> 1,0X 7 ^ 7^ OR l.ol l.ol 7.»l D.O. J l O i M 0 , 3 0 d ^ l oaH Oi^Z 6,3.3 0,3.0 0 . ^ 0 0 , 1 ^ 6,iC Q.th O i l l 0 ' ^ 3 .Al Cond. ( i>ff^) _. ,7.(0 A U A39 ••^5T) .^S3 . ^ 3 1 . 3 ^ . ^ ^ ,yi>/d '^i^ ,t^6 a'f^ ,;iv5 ..;?vS z;?^/ Turb ( / V W ) —- i i 3 /%H f.A 3.9 3.7 i'9, h<^ i33 AH^l H0 a.'s 333 167 103 iHO DTW (feet) H53 lA.CJ> H U H.l9 / H i ? H:{9 H T i /H.76 H,^0 /i7( H-7/ / V / 7 / /V-7/ /V/7^ / H , 7 / /^,6~^ Rate ( ^//min) 590 390 390 i7C Hid H70 HCO H60 H70 <7lO -{<S0 ^ ^ 0 i4^6 -7^:0 -506 nti; • A U -173 -/63 - / S C 'li? -/i3 -7^0 757 -/33 '730 3/^1 -/?3, - / ^ ^ -7SIO '-//9 1' .'.i/X ,~ — ,/3 (,(i A3 Wi y3U6S ./w* / ^ A I'CA M ^ ./3. M A ,a 7£0 1,63 i.S9 / ^ i m /,b/ , a 1,37 JT. A57 .A? .7.5? . ^ 1^56 ] Notes euiS^Sl^ Aii^fPar^fT^ P o t ^ - e ^ ' / b i ^ it.QC 3I0VJ h SCOtn 'A'"- Post-samplinq Measurements Total Volume Purged Water Quality Meter(s) Hcf^iWiJ-^'^ B ) ( 3 V T 3 " ^ 3 Sample Information Groundwater Samf Sampling Time Sampling Method _ Sampling Observa )le Field 1 Bailer ions D /\3JVHPHD Sampling End Time (tvoe: ) \ 3 I A - M A)dir iSame as DTW before Samp Above Other inq •' iT"-'—^^ 1 - See Page 2 of 2 for Groundwater Sampling Parameters I 305055 G R O U N D W A T E R S A M P L I N G F O R M Well Number A f ? 7 { l / ^ P 9 D fe/i^^o^'c^/ State Permit No. Project Name Project Number ws'^^m Sampling Date Weather 3mplecW)y: Purge Method: Low Flow NJDEP 3 Well Volume Pump: Submersible Pump ( inch) Peristaltic Positive displacement Other: Pump intake depth: Purge water discharged to: Ground Drum Other: Tubing: Polypropylene Teflon-line Other_^ / New Dedicated TK Time (HH:MM) Temp pH (pH units) DO. C^.") / \ ) Cond. Turb (AiTU) DTW (feet) Rate ( ml /min) 7c rpp Notes 12-15 d i ' O t 1 0 0 0 , ^ 0 AHh i h l iH,77> 300 -//f .72 l,%7 Purge 9SS».Co/t i / / f , h ^ 1^'-^^ 3u^9 1,00 OiAO 7,H5 113 iH.6oi ^90 - i i 9 y5 /,h7 13.35 '3iA3f ^ 0 0 ,/9 <;?y5 9,H i H 6 3 ^90 -//7 7 ^ /S> /Jl-30 3 / 3 7 -7.00 ' l l AH3 l3l H ^ 3oo 3337 a IBA ' ^ 3 3 3 / ^ 7 •7,00 o,/9 .^V5 9.C 1^1 ^^ 1 ) 0 0 ' / i S rR a 7 :?Ay/^f flouj /90i i^ ///^/-c \ t A ^ 7)191 7,0 V o<}.^ 3311. i l ^ i d ^ 190 —i^^ ,1^11^9 Post-sampling Measurements Total Volume Purged Water Quality Meter(s) Sample Information Groundwater Sample Field ID Sampling Time i ' ^ ' l j O Sampling End Time l l V ^ Sampling Method Bailer (type: ) Same as Above Sampling Observations DTW before Sampling Other 33±5S - See Page 2 of 2 for Groundwater Sampling Parameters O^rta 1 nf P 305056 GROUNDWATER SAMPLING FORM \/\//~ll Kli ir>..K<^r TxC'-" l/i'i \ 0 .. i * ' ) Well NumDer State Permit No. Project Name Project Number J^O 1 - V f ii\f i A- Sampling Date Weather Sampled by: h-.. ^.^-... f ^ ' - 0 0 (initials) H c i r t inc Weirjnformafton Well Type: Monitor 'A- O t h e r \ | i\'> V Well Construction H. PVC Well Diameter ^ Well Depth (ft below TIC) Water Level (ft below TIC) inches ! ^ 7 < Well Notes ( O d o r well condition, etc.) Volume of Water in Casinq (qallons) ( ) - f Well Depth Well Screened interval X f . i f ^ i Well Headspace Reading (PID Product Level-if present (ft belc ) * ^ * 0.0408 = Water Level Well Diameter (in) Steel t o i i ^ . 7 ; > f < 'FID) )WT1C) Other set below TIC oal Ions Purging Information Purge Method: X Low Flow NJDEP 3 Well Volume Not Purged O t h e r Pump: 7~- Submersible Pump ('l_inch) Peristaltic Positive displacement P u m p intake depth: Qi^it"^ Purqe water discharged to: Ground :'y D r u m Tubinq: Polyprocylene V' Teflon-line O t h e r / >^ Time (HH:IV1M) \ta^ \kn \{,7>^ ir^^ '(',0 l^H'^ lh^3 \un a (3b M^cPi Temp (°e) 3% 13 l^AM) n n n^i d^.U ^ % ' ) ^ 1931 11.S9 cJ'T.al pH (pH units) 1^.23 7.?^ 1.3^ •1A32 3. %1 331 in 7Al^ 3 9 3 D.O. tt^-^/L ) 0-%'{ e,8D o r i ^ 031 &. 71 (), f>1 6.69 V.h( o-h'l Cond. I D.PS^ n . 3 7 ' i 0.?91 /?. ^ ^ i V- n ^ f^t-m o,nt Q.-n\ a 7'Si Turb 7^'i3i '>999 >^<?^ t^r 53r /f,3^ l^i m • 590 DTW (feet) I ' ^ l ^ 1331 Ib'f^O /^.v\ 1^0'^ Ib^O^ II' •D') IL02 1^03 /S3I Rate (kA-f/min) 3^0 W^ ^ o o 3 0 O • 5 D O • ^00 5'0O roo SOO- oAL/> - 7 § -//v ' / / / A/o:i 301 ~I0\ -19 -loo -"13 Total Volume Purged Wafer Quality Meter(s) _Oth« 0 !r h e r N e w 3 nA \ DJ2 IhH j o-^i W O^l^i ill O-flf fl,i1 DM oii \3'- I'^l) I'K (30 i ] \ \ ;i / a./7?/^C Dedicated Notes Purge Start S'-AfV 1-i-. l^o,2JtC C^ C X I A A . - ^ - t ^ ' < , ^ _ Post-sampling Ct4A^V-^A.^A U-2.lL- Measurements o c Mv^k Sample Information Groundwater Sample Field ID Sampling Time Samplinq Method Bailer Sampling Observations Samf i^/A! ^ 7 , - '.'A-) (ling End Time l"?0"^ DTW bef (tvoe: ) Same as Above Other f l 3 ^ H ( 3 U . I A ore Samp ling 305057 GROUNDWATER SAMPLING FORM Well Number .A37 OM.P ^/) State Permit No. Project Name . Project Number ESS'V^f^ Sampling Date Weather Sampled by: ^ - 3 - On ->>Vlr-> ^ .^£1 g g , U ^ ^ - l ' - ^ f i (initials) Weil Information Well Type: Monitor Y ^ t h e r U l M P Well Diameter \ 3 inches Well Depth (ft below TIC) Water Level (ft below TiC) Well Construction ion y ^ ^ V C Steel i Other ^9.8^ /5"/§r Well Screened interval .3^^02 to ^ ^ 7 ^ f e e t below TIC Well Headspace Reading (PID/FID) Product Level-if present (ft below TIC) • Well Notes (Odor wel| condition, etc.) Volume of Water in Casinq (aallons) ( _ _ _ ) - ( J* 0.0408 = gallons Well Depth Water Level Well Diameter (in) Purging Information Purge Method: ^ L o w Flow NJDEP 3 Well Volume Not Purged Other Pump: y ^ Submersible Pump ( 2.inch) Peristaltic Positive displacement Other Pump intake depth: J ^ d M p ^ t 3 ^ Purge water discharged to: Ground (C3rum Other Tubing: Polypropylene iXDTeflon-line Other / ^^-^ew Dedicated Time (HH:MM) f^asr )3-30 Temp C(13 9.%(ff pH (pH units) 9/^3 D.O. (r}^-L) ^.3.0 Cond. o.^n Turb (_My ^9^- DTW (feet) 13,m /L6'^ Rate (_£u£/mm) WO -fC>2 cfr 1-99 Notes Purge Start \Q 33 g^.^1 1.S3 liH a9A() 7^99 /^, 7^ ^ 0 0 ' 7 ^ M 2 [-3S S23K Q^Sn 7. 33 JLQi aoTf ^76 IL 7 i SCO - R 3 D.12\U( \^3% ^. 3/ l.Pi, C^iO 0.9^-3 9^13 I(/^16 ^OO. - S ^ 3.(7 ICl Post-sampling Measurements Total Volume Purged Water Quality Meter(s) ^ W O ^ Z - £!ti ((J-y.eiA 3 ^ ^ Sample Information DTW before Sampling Other irtoE Groundwater Sample Field ID Sampling Time j 7- 3 ' \ Samplii^ End Time Sampling Method Bailer (type: Sampling Obsep^/ations S?^V..>WM,^Q Same as Above n C f ^ O i r - m i a t a r « 9'-''U4liA.^t Q.1,^^JL.^ 305058 ^ p i ( A P ^ i i GROUNDWATER SAMPLING FORM well Number State Permit No. Project Name Project Number \ryy'V.WY ' i,.. Sampling Date Weather Sampled by: bi^^oo KH'^P^ ^aww-u ^ 4 W4.IQ^ ' (initials) Well {nformalion ^ - Well Type Monitor VL Other V ^ ^ f Well Construction K PVC Steel Well Diameter ' ] / - inches Well Screened interval % A l ^ t o Q'^-^^1 Well Depth (ft below TIC) f ) ^ 3 ^ Well Headspace Reading (PID/FID) Water Level (ft below TIC) Well Notes (Odor, well conditic \^31 3n, etc.) Volume of Water in Casinq (qallons) Product Level-if present (ft below TIC) O t h e r eet below TIC ( ) - ( ) * ^ * 0.0408 = qallons Well Depth Water Level Well Diameter (in) Purfling Information Purge Method X Low Flow NJDEP 3 Well Volume N o t P u r q e d O t h e r Pump: X Submersible Pump ( T ' i n c h ) Peristaltic Positive displacement O t h e r Pump intake depth: i ? 7 - t 9 ' Purqe water discharqed to: Ground S^ Drum Other: Tubinq: Polypropylene ^ Teflon-line O t h e r / V ' N e w Dedicated Time (HH:MM) \m\ fOfiq fH)^ /6Q-7 im (Oil loi^ m i(l3l iov^ m v |G^1 i06'P /n<7 lion WW m Temp CCJ %.ioV % \ ^ ^oni 3:)AP) % - ^ "k)!^ ^f).% %^1 ^ . ^ t ^ . < & ^ pH (pH units) 1.00 A(3) 30D A.Oi 3 0 1 3.01 3.03 7.01 7.0( ao) DO. eL'_L) iio\ I3v \ { i |.!0 .eP/ M 0.^ b.i'i 03V ev^ Cond. (^7<-) O-l^o 0-i^^ 0-W) ().W o.m 0.H1 O.lH'i 044^ 6 ^ 4 ft-'W^ ^°/P'l)i°'"'^?^^T''^-1^. . u { \ 3 , , n r ^ ^\Q3 Turb (U^) 010 ^10 6^0 eix) L|70 9A3) no / ^ Ho _ L ^ DTW (feet) fV^l I'^M ^^1' l ^ ' ^ ^-! /S7^ N'^< ]HA3 M-^ j U 1 W {A 30^ /q.qO H3^ HAd mo IHMi Rate (HvS^/min) (OXTD ^ ' i l w^ t<n 3nj t l ^ 5 ^ 3oo '7'^ 7 ^ TbOt) i6D 1^ 6) CO ( t : ^ ( ^ Water Qua^vJWetf _.';7_ |L/.cJo.-7<0- . "Sample fniuhiation Groundwater Sample Field ID^'"^ " |^F \ h \lfAP- Sampling Time i l j d Sampling End Time Sampling Method Bailer Sampling Observations (type: ) \P _Same as 0 ^ /|H 111 ((f) ((0 m /OV <^7 ^ l-^ 3% o\ i-n (i.\ )-^ 0.1 /.sv 0,1 \ ^ 0.1 '<^ 6j |.^ bl '•? 01 1-^ ( ) • ( ' • ' ^ 54 1."^^ Notes Purge Start 3f!r ( U . ^ o3 ^ C G ' - b / 1 , ^^^ft /)lk,Nf 5 ^ ic^^ fl<^0 /)(;..AJU ' zr Post-sampling Measurements " • ^ ^ ^ 1 , , —/O*^ O-i—Hy^ ^ DTW before Samp Above Other ling - See Page 2 of 2 for Groundwater Sampling Parameters 305059 GROUNDWATER SAMPLING FORM Well Number f f f ' \ / « v t f - \ P Con^''^^'^ State Permit No. Project Name Project Number ^ssi^m 00 o (inrtials) Well Type Monitor C>^ Other Well Diameter J inches Well Depth (ft below TIC) Water Level (ft below TIC) Steel Other Well Screened^teival ^ ^ to Jf^fj'feet below TIC Well Headspf&ce Reading (PID/FID) Q Product Level-if present (ft below TIC) Well Notes (Odor, well condition, etc Volume of Water in Casinq (qallons) ( Well Deptti Water Level Well Diarfieter (inK 0.0408 = gallons lirging Inffjtrpation Purge Method _ ^ L o w Flow NJDEP 3 Well VoHjme Not PurgeH. Other Pump. J::J^ Submersible Pump (_j^ inch) Penstaltic Positive displ^ement Other: Pump intake depth: a?7 Purge wafer discharged to: Ground \ ) < [jrum Other_ Tubing: Polypropylene ^Teflon-line /oihec: V oC New Dedicated Time (HH:MM) Temp pH (pH units) z DTW (feet) '/min) Notes iio^ Purge Start 1333_133_G3I2_M3/J3!3__^ 3(90 1.%' fV/3 ML b . i i 077/ tP.n J O H.13 11^ 3 1 '=4UJ^ 3- ^J ''33PrJ^ /^7S ^\3<< s n ^ 210 IH.'^H y 7 .m li> vicji J^efs (3\-iny ajj- > N7^ T ^ 3l,(i3 - ^ • ^ ^ ^ w. Z l } 3^ 376:^ ( i M iQr'^ ^ :?-77 i ^ HM- 'f7t 177 1 1 V-^\, 6.^ 0.5"^ X l i ^liQ H3f 3 f 2\R> 4.^<P tJL J 3'i ^00 li9J {.fi 3» 37 A l M l Q-5i0 ==)73 9?o IW HOO i n r 3 r 22.01 LM. 6.^3' 7 M . m f9.9^ ^00 a) O i iT Post-sampling Measurements Total Volume Purged Water Quality Meter(s) })o<^l5/< O ' J ^ ' 0v/*fe>/4- ^(7\ Sample Information Groundwater Sample Field ID Sampling Time Sampling End Time D T W before Sampling Sampling Method Bailer (type:. Sampling Observations J Same as Above Other - See Page 2 of 2 for Groundwater Sampling Parameters 305060 G R O U N D W A T E R S A M P L I N G F O R M ) Well Number FPP- \/'^f-lh State Permit No. Project Name Project Number Sampling Date JISOJOV Weather '-i^-my. So'^ Sampled by: ^ L , ^ u l (Initials) Weil Information Well Type Monitor ^ Other \ / ^ ^ Well Construction V PVC Steel Well Diameter ^ inches ^ Well Screened inten/al J t " ^ to-^F-fi" ( Well Depth (ft below TIC) J ^ f l ^ Well Headspace Reading (PID/FID) Water Level (ft below TIC) H . W Well Notes (Odor well condition, etc.) Volume of Water in Casinq (qallons) ( ) - ( Well Depth Water Lev do Product Level-if present (ff below TIC) j(tY u<A^ ) * ^ * 0.0408 = el Well Diameter (in) • ' / V . "^ Purging Information '^^ Purge Method: ^ L o w Flow NJC Pump: -7^ Submersible Pump ( J inc Pump intake depth: J 7 Tubing: Polypr Time (HH:MM) J m3 ^ \^n 1^3' \i^n ^ ^ 3 m% ifciJ b5% m\ \10t ni3 iii^ \V3 n^s 33^ n-H3 Temp ^\32 3\.% 3?.)$ VM 3 J , ^ U V i m 3i.ri 3^.3^ V.13 p-l(/ 3m _J^.5V V.i9 3;?./3 •^.o4 opylene ^^Teflon- pH (pH units) ( ^ ^ m ioM in.n . (o3^ (^i1 i,U fc.n 6,irf ( p . ^ hf\ &,^{? io.V^ (j.n i.^o Ct^o DO. oM 0,52 1?.^^ 0 . ^ 1 0-^y 0,C;0 oM e,s^ 6.^^ 03^ O.Ml lO.'/^ 0.^3 O.VD 0 ^ 0S9 )EP 3 Well Volume Not Purqed Other i) Peristaltic Positive displacement Other Purqewater discharged to: Ground X D r u m Other line Other / New Cond. .?3f ;?-7r I'^'i 3lA ; I A 3 o?.7r Q3^ ^3^ ^ ^ 1 ^ ^M M 9iS ^,id. ^.or ^•a 110 Turb (;vro ) ^P 175 1 ^ d?0"3 ^po ^3o 990 Q30 dAO 3A0 330 3fO 390 W H{6 3^'3 DTW (feet) ) 9 ^ mi l9f\i m^ )i93 l i M \i9i i M H.^S^ m i m i HPII i9.% •330 mi m i i Rate ( ^^/min) yyo — im — • 719i 3^1 3oi . — • ^ 3 0 0 - ^ H f T,/'^ ^ i ^ Sft-lfDi oAliK, o,\ 6\ 0. (1.1 a( O-l oA O.i ^./ ^./ o.\ ^.l rl >/ // l,?fc 1.74' l.lf /.7^ \:ii 1.75 )11 hV i.li pi l1> 130 IMI /,a I'V 3 d^C li (pf 3 1 ^ 1 3^ 3r ';r S>L ^ ^r ^3 i \ l i n 13 13 Total Volume Purged Water Quality Meter(s) }3)i\^A Sample Information Sroundwater Sample Field ID F P P ^ H P I D Sampling Time i l b ' t S Sampling End Time 17-HS DTW bef Samplinq Method Bailer ftvoe: ) Same as Above Other Sampling Observations ore Samp f^^fm ^ . , Other eet below TIC 0 gallons _Dedicated Notes Purge Start s^^pU r/o^' Post-sampling Measurements u 'P;? e ^ i ^ ^ ^cff iiiiiiiiiiiiiiiiiiiiiiiiiii linq / H 9 1 - See Page 2 of 2 for Groundwater Sampling Parameters 1 D o n a 1 o f 9 305061 GROUNDWATER SAMPLING FORM Well Number ^pp- V r ^ . f - / D State Permit No. Project Name Project Number Hart ,nc. Jl\;\!v,^,-A. Cka-Av^<<^{ Sampling Date Weather Sampled by: M -"30-00 S(x^,i;.! °<05 33^ (initials) Weililnformelion Well Type: Monitor y Other V/f''\\-^ Well Diameter 7— inches Well Depth (ft below TIC) r 2^3}'^ Water Level (ft below TIC) _ Well Notes (Odor, well condition, etc.) Volume of Water in Casinq (qallons) ( _ _ ) - ( . Well Construction _ K PVC steel Other \'^A\ Well Screened inten/al 3b.7':r to^.^<<" feet below TIC Well Headspace Reading (PID/FID) Product Level-if present (ft below TIC) • J* 2 * 0.0408 = gallons Well Depth Water Level Well Diameter (in) Purging Inforfnation Purge Method: '/^ Low Flow NJDEP 3 Well Volume Not Purged Other Pump: / Submersible Pump ( X inch) Peristaltic Positive displacement Other. Pump intake depth: 7 l Purge water discharged to: Ground '•'^-Drum Other Tubing: Polyprcpylene y ' Teflon-line Other / /y. New Dedicated Time {HH:MWI) \S't-5, Temp cn • 3 0 . 7 3 pH (pH units) 7.b< D.O. ^.7o "' 7.3T Cond. Turb ^Vi"^} DTW (feet) Rate (£^/min) 5 0 0 \^A Sett' i m s ' I i i.^t. Notes Purge Start \5M,1 •So.-/if 7. S:^- .=10 '^••^^M >n'Vl \io. Z o \ 3 C >il i».5^ »SSC '^c.^?. 7.Mi ^c^.fc-: 0 ." ^ ' ' 7 •-)-7.>i c,oo 13-T . \ \ \ \ 3 \ i'oCiO 50.BU •7.?3 D. L-TAi > ^ q i (5.iS tA)W 57) ^V {\^(A/i 3 0 . 7 ^ 7..XT 7.9.>- O.^MC' >?•}'? 1 iJ-w ^^iiS^ Itoi .fc>.7^ 3. Ah y^B^ 03VA . / / A .y 77.. ZL 1' (O 9 7.7\r^-r A '-^ 7 0 . 7 - ^ 7 . ^ 7&3 o.Jl^/ 7999 /C.^-I •<30 o / 7 7 / 7 i / y ^ ^^J.•^.M•r .vtarn,a-j iv Ae.ilr /fc/? 3 o . l 6 -3H 7-71 Q.7-Y/. >m i'i I j y . i A i i u f fl. liirf-1 I62S 7Q .(3, 7.a3 7.S7 o ^ y H i ~^nii 3 3 1 6 0 0 ;S5 \ b i ! S^7g 7.,"-f /.C3- 0,71% 7 f r n /b-^c^ i^.o (?-i'^- if;;37 ft^^- Post-sampling Measurements Total Volume Purged Water Quality Meter(s) i j ' 2 2 /fer\t.Ao Sample Information Groundwater Sample Field ID ^-V'F -''J (7f'- i r> Sampling Time ]'cAo Sampling End Time ]i£ Sampling Method Bailer (type:_ Sampling Observations DTW before Sampling ) w^'Same as Above Other •^amnltnn Parameters 305062 • •A ' j § ^ i i ^ ^ 9 G R O U N D W A F E R S A M P L I N G F O R M Well Number p P P 1/ m P \ b State Permit No. Project Name Project Number Sampling Date Weather Sampled by: ^ - 1 - oo l . U A n L i 9Qs f « - (initjals) H a r t nc i Well Information Well Type: Monitor V Other '^/ CAx Well Construction / - PVC Steel Other Well Diameter D^ inches Well Screened interval i*-75^to <3l'.vYf« Well Depth (ft below TIC) fil'^t ^ 3 Well Headspace Reading (PID/FID) Water Level (ft below TIC) ( 6 . / t * / Product Level-if present (ft below TIC) Well Notes (Odor well condition, etc.) Volume of Water in Casinq (qallons) I ) - ( Well Depth set below TIC ) * ^ * 0.0408 = oal Water Level Well Diameter (in) ons Purging Information Purqe Method: ) 3 Low Flow NJDEP 3 Well Volume Not Purged Other Pump: X . Submersible Pump ( Z inch) Peristaltic Positive displacement Pump intake depth: 5 7 Purge water discharged to: Ground X O r u m Tubinq: Polypropvlene / ^ Teflon-line Other / .V' Time (HH:MM) \ } { 0 11*3 UHp U l ' ^ (\ 3.7- j i c > 5 (1^5 n--> \ [ ^ i ' L ] 3 3 \ \ H ^ li'4Z Temp CCA o ^ H 3\A'] 3 o . U 3 o - T k> 3C..16 7oA'\ "3 i .CrVJ 3\ • ID 3! :^3' 3!.--fb 3 ] . ^ b 3 o A "i pH (pH units) •74 b 1 , 33 7 . 7 5 - t-.7.3 ( o 3 \ 3 3 % 6.8^t S. k-l S i.tj "^i 5.Hb s.y\ _ s.^z Total Volume Purged D.o. <D 713 7 7 1 7 . 3 t , 7.^:^0 7 ( 5 ' 7 . r p 7 i : ~ - T'-ii 7./O 7.10 1 . 3 \ '.. AK.^ A.OQ Cond. (S/U) a . 5 ^ a.7l 7 . 5 1 7 . t o c i . 6 / ^^•bT) 7.4.3 D..b^: 7 . t ^ 2 • (. IA 7-i.,i- # - ? ? t - Turb ( WTIA) > ^ - 1 G 7 ' n o "^'j'l'O ^T=JO >^'?,9 C->io. 5 10 5 o o M2o H517 '.v'x':' - ^ ^ ^ : 3 , t / > « i ' ^ L ' DTW (feet) lfc.,5<? \fc--3i ! t - ? 4 \L^\ \k..Vb \>,.33 3.7-h V'oA6l lb 3 3 ifo73 - • < 3 ^ . . I t . HO Rate (^"'-/min) Hm 66 0 5 7 0 5'7) 3 ) ^ 0 3 0 O ORP i 33 ns H 3 171 j S l \33 1 5 7 ) 5 t ibO i b o i i, D ! ^ 7 Water Quality Meter(s) Other Other New Dedicated S/xiL 1 TDS 7c i % - -( ii-^3 ^1 K . i s t ,.( U'i'" -f iKt,7 7 n.47 ^ f :/.c^^ .. / 1 U l - i ii.Ci f A . ^ A il7<) .: 1 7.7c > fU.fc? Notes Purge Start )i7-V.^. <:; J •raT<?. , a5 t.v. i ^ ^ A.h.Ac/,: 1 ••' * " > % 7 3 i - . C ^ . . : ^ -f,,v.U .•:tb-'.r "; :S i?t'o-T.A,Y 4- C O ; ~ '- .f .--• / / i ^- .v< / C Post-sampling a - 7 2 (Awr^'o3\ Measurements Sample Information Groundwater Sample Field ID Sampling Time Sampling Method, Sampling Observa 3AA, Bailer lions Samp P P p ~Vmv' ? D ling End Time (tvoe: ) 11 A l _Same as DTW before Samp Above Other lina . "— •^ - • ^ . - - " 1..^*«, c ,,T,r,linn P a r a m o t p n t 305063 • m w 1^ 1 GROUNDWATER SAMPLING FORM well Numoer State Permit No. Project Name Project Number r i r uwr ( u Sampling Date Weather Sampled by: S - i / 0 0 FOTI' ^ k i / v t / v i t . , - . ^ s: ^ (initials) Weil lnform8{icH\ Mciaren H a r t «c :;Ki;i;|;||;:;i:*S;:S;S|:K^ Well Type: Monitor "^-"^ Other / / / > ? / ' ' Well Construction V ^ V C Steel Other Well Diameter Well Depth (ft below 3- TIC) Water Level (ft below TIC) Well Notes (Odor, well conditic inches Well Screened interval c3^ ^ i ^ to 7i}*^"S'feet below TIC 5 * S"' 3 '' Well Headspace Reading (PID/FID) xp n 3n, etc.) Volume of Water in Casinq (qallons) ( Well Depth ) - i Product Level-if present (tt below TIC) ) * ^ * 0.0408 = Water Level Well Diameter (in) aallons Purging Informstic^i Purge Method: Y^Low Flow NJDEP 3 Well Volume Not Purqed Other Pump: ^ Submersible Pump C l i n c h ) Peristaltic Positive displacement Pump intake depth: ' ^ 0 Purge water discharged to: Ground >=0rum Tubinq: Polypropylene ^teflon-line Other / AO Time (HH:MM) 9it/9- ^^33 'I'. 33 3:<;3 1 : ^ I^fi3 Temp c3) sos:) H33 713:) IVyf) pH (pH units) 'llQ 7, r. 1 \z l A l 7 / 0 Total Volume Purged D.O. t^-'jL) ^ Sto^ 3.D3 ^3<: i - 3 ) 33^1 Cond. 3 a 3 h3 3 63 331 331 Turb ( / S V ) >9ro >?9c> 7 3 b 3 U) A>3o DTW (feet) fS9^ /6.A) 1333 3 ( A 3 3 1333 ./133 Rate ( -ij'/min) 7C/) 3sb ^30 1 3 3 -^^33 oR.p . 3 3 / 333 3 3 3 ,331 '>/.5 Water Quality Meter(s) other Other New Dedicated %iL -as i 3 Al^i .• 1 A.<^ '^ 1^3. 31b/-. A ]• U Notes Purge Start ? Post-sampling t4<^,-'.baL'27- - £i(-iVc Measurements eu:j^'.r Sample Infonnation Groundwater Sample Field ID (^~pp i;/V! P Sampling Time it') - <^ ^ Sampling End Time Sampling Method Bailer Sampling Observations - Ceo Dano 7 nf 7 fnr T, rrunriwater S (type: ) i-i3 - Same as DTW before Samp Above Other »7D ^,.k linq •J - ;. ^ / amclinq Par ameters 305064 • .: A m m G R O U N D W A T E R S A M P L I N G F O R M Well Number ( ^ P F - ^ i m P - ^ t ) State Permit No. Project Name Project Number Sampling Date Weather Sampled by: '7vA>.-^M, % ^ ^ - h ^ i i ^ A , ^ 3A}J^ 3cf (initials) lii»il»iii«iiiiiiiiiiiilii^ Well Type: Monitor V Other M M Well Construction X PVC Steel Well Diameter 7 / inches Well Screened interval to f Well Depth (ft below TIC) ^ Well Headspace Reading (PID/FID) Water Level (ft below TIC) Well Notes (Odor well conditic ^ ^ ^ ' )n, etc.) Volume of Water in Casinq (qallons) ( ) - ( Well Depth Product Level-if present (ft below TIC) Other eet below TIC ) * ^ * 0.0408 = qallons Water Level Well Diameter (In) Purging Information Purge Method V Low Flow NJDEP 3 Well Volume Not Purqed Other Pump: y Submersible Pump CT^inch) Peristaltic Positive displacement Other Pump intake depth: Purqe water discharqed to: Ground j>^Drum Other Tubinq: Polypropylene X Teflon-line Other / A New Dedicated Time (HH:MW!) i^l'y m i \3n \ 7 7 \ \ d ^ < 0n ^^3 \3^^ mo Temp ct\ pH (pH units) DO. 1/ Cond. 3\vc^ ) Turb ( M-^) DTW (feet) I5.> \3.^ I ^ < ho j?.^ (17 I'sA ^131' H.^o' Rate ( t A l /min) '7St) ^OD Notes Purge Start ^ 3 P^J^r^ o f f ' \ \\(j ^(}cki.^si. 0 PTf^ ZS.Mi' \ ^ h c ^ \ i ^ Cv,\^rie(\ Post-sampling Measurements Total Volume Purqed Water Quality Meter(s) Sample Information Groundwater Sample Field ID Sampling Time Samplinq Method Bailer Sanipling Observations - See Page 2 of 2 for G roundwater. Samf }ling End Time ftvoe: ) Same as 1 DTW before Samp Above Other inq 1 Sampling Parameters D o n o 1 n f 9 305065 GROUNDWATER SAMPLING FORM//, , j Well Number f ^ P P - \ J M P ~ O . O ' ^ 1 ^ / State Permit No. iiaknr^A Sampling Date Project Name {), r^.A i:J.,»d rAk.^,*'irJ CP ' Weather Project Number ~ — • Sampled by: ^Mo/o^ l^il^kW / R^0,3i- (initials) Well Informai^cwt Well Type: Monitor %. Other \)i,£hr HiAtAat^c^ ^ Well C^'structWi V P V C Steel Other. Well Diameter ^ inches WelP^creened int Well Depth (ft below TIC) Water Level (ft below TIC) J23i i W€fbi .)-{. Depth to —- feet below TIC V^ell Headspace Reading (PID/FID) 7 fifi/n /Vy 7 ^ 3 \ Product Level-if prese\t (ft below TIC) Well Notes (Odor well condition, etc.) 3h'^lsf ^ ' Volume of Water in Casinq (qallons) 0.0408 ^ gallons ^ ^ _2i / / purging Information NJDEB^Well Volume"- Not Purged Other._ Positive displacement Purge Method: J)^ Low Flow . , ^ „ ^ ^ . ._,_..,_. Pump: ^Submersible Pump ( 42 jfich) Peristaltic \ 'Positive displacement Other Pump intake d e p t h : ^ J ^ ^ ^ ^ ^ ^ ? j g r Purge water gischjarged^: Ground VDrum Other Tubing: Polypropylene XTpflon-line Othj^r _^; / _ y New Dedicated H^tlk O AiP. ir/to7../^/;Lg Sample Information Groundwater Sample Field ID FFP{]Mf3l,jl Sampling Time Sampling End Time DTW before Sampling Sampling Method Bailer (type: J Same as Above Other Sampling Observations See Page 2 of 2 for Groundwater Sampling Parameters 3 0 5 0 6 6 G R O U N D W A T E R S A M P L I N G F O R M Well Number T ^ - p P \ } r ' 3 P - A A O State Permit No. "- - Sampling Date Project Name i/-,i':.i;n 'l'...7fA Ahi^mAAJ • Weather Project Number — Sampled by: ESS'^ffr" '3.3:'3-AA C/r-nt.. A : A 7 .••/; ,.„ K :,-i • ' (initials) Weil Informslion Well Type: Monitor < Other |.^'7 f' Well Diameter A A „ inches Well Depth (ft below TIC) f,:7.3 Water Level (ft below TIC) lS.r}7. ( M i e A 3-:... H . H Well Construction X P V C Steel Other Well Screened interval '•— to — C feet below TIC Well Headspace Reading (PID/FID) Well Notes (Odor well condition, etc.) /y Volume of Water in Casinq (qallons) A ^ A - j Product Level-if present (ft below TIC) iA^rc f^' CA>.'\ :'7, .rj,'i\ /•l.^^>ry //A 0.0408 = Well Depth Water Level Well Diameter (in) gallons )-^ / ' t . . ; , • - • ' Purging Information X Low Flow NJDEP 3 Well Volume _Not Purged Other_ Purge Method: Pump: X Submersible Pump (.r>^inch) Peristaltic Positive displacement Other Pump intake depth: AjA J ' Purge water discharged to: Ground V Drum Other Tubing: Polypropylene V Teflon-line Other / y New jo'T' Other ?7F ISI^ Dedicated M » t .•jtcy 'gi Time (HH:MM) Temp (°AJ pH (pH units) DO. Cond. f 7 7 M Turb f 7/70 ) DTW (feet) Rate ( ».f /min) otn- -r: •^7' Notes I3'M ibs07 l(^h hOU ,?9^ ><^3 I t . l 1 ^ o 9 ..^ 07 J I.SA Purge Start / g : 3 3 :^/7^ 63C .39 ,7.i3 ^999 i9.777 J i ^ ^ AT. jASS 13.3^5 31.1^ < . f ^ i X /;iv'^ ^m / ^ i . i o -3? 771 \ l , ^ 5A//loit cj/A.^ 1^3'^ Jh'H3 -^3il 6.91 7 •'A ±7,^AA JML >9n •^1)76 -9 ,11.7/5^ jTlvi^^ f^^iji/,/•••-, ir.H^ 3 3 . ^ 33(3^ ~3 ( C M A l/)Ui. CKO> V_3JJJ373~ 13-37' -rlou.! e . ^ 7 / > » t ^ v ^ ' <^i Ijt f JziL i'77£^td. ^ ^ g? » / o l-P r h f ^Sc> 0''<3 iOO>^ I Post-sampling Measurements Total Volume Purged Water Quality Meter(s) . 3 A 3^ i: .7 lit- Sample Information Groundwater Sample Field ID A f^'^'c •"' '^' '•' > Sampling Time Sampling End Time _ Sampling Method Bailer (type: Sampling Observations DTW before Sampling J Same as Above Other_ See Paoe 2 of 2 for Groundwater Samolina Parameters 305067 G R O U N D W A T E R S A M P L I N G F O R M Well Number f r p - V f k / ^ - 2 D State Permit No. Project Name Project Number Sampling Date Weather Sampled by: (initials) Welllnrormatjon Well Type: Monitor ' / o t h e r " ^ ^ ' ^ Well Construction X PVC Steel Well Diameter 9 . , Well Depth (ft below TIC) Water Level (ft below TIC) inches t \ . ^ 0 Well Notes (Odor well condition, etc.) Volume of Water in Casinq (qallons) \{ ) - ( WellDepth Well Screened inten/al to f« Well Headspace Reading (PID/FID) Product Level-if present (ft below TIC) Other ;et below TIC ) * ^ * 0.0408 = qallons Water Level Well Diameter (in) Purging Information Purqe Method: Low Flow NJDEP 3 Well Volume Not Purqed Other Pump: A) Submersible Pump (iJWfrich) Peristaltic Positive displacement Other Pump intake depth: 7 A 3 Purqe water discharqed to: Ground f>^Drum Other Tubinq: Polypropvlene V Teflon-line Other / \ New ijj*" Time (HH:tVIM) 17 3 ^ \-JS5 ! 7 7S Temp C_A pH (pH units) Total Volume Purged t D.O. ( / ) 1 Cond. ( ) Turb ( ) DTW (feet) K.IS- ^.7? i"s,?''-' Rate ( /min) Water Quality Meter(s) Dedicated Notes Purge Start V"1 ^ 2- K:-.Uif'7 Cis^o -(.Ac • :;v-:--\ <r7<;^^7 •; tc,7 i^ 6 ' ' 1 W C a r . Kea...r lar^',.? c A A r • ' • • ( \ ; ~ ) : A O ^ ' - - : . : - ^ - - P 7 n : .,,.:.•. • ,.-,,j..:..,r:-, c.^ J i,. -Ay ; ^ _ i r r V; '-•'. .•'.. •^ATC'-AI f.?:.iv:.^_/) ^7..^ V '3-7i-,.-;^-,:vC. f.-' • -•- n o ;/.>(V.t-:Jr- <"'Arv:-A-i^.'A]A.^ A A n i^Ai-A^A b^-.hinKi: ..r.-..,, .' '". Post-sampling Measurements Sample Information Groundwater Sample Field ID Sampling Time Sampling Method _ Sampling Observa Bailer ions Samp ling End Time (type: ) _Same as DTW before Samp Above Other ling . C - D ^ « * o ^f o f nf r. .-1 n.>H\A/3(pr *^ amnlinn Par ameters 3 0 5 0 6 8 GROUNDWATER SAMPLING FORM Well Number fPP v;/n P ^ ^ State Permit No. Project Name Project Number ESS'^f^ Sampling Date Weather Sampled by: 3'-l'00 S L L . V , , V ^ -^-ag's 2L (initials) Well informslion Well Type: Well Diameter Well Depth (ft below TIC) Water Level (ft below TIC) Monitor '^^ Other \ J { ^ \ P *— inches • U 3 0 ' Well Construction V^'PVC Steel Other Well Screened interval to feet below TIC Well Headspace Reading (PID/FID) l(p-yS: Well Notes (Odor well condition, etc.) P ^ f t C f ^ S T D (3L 3 ? ^ Volume of Water in Casinq (gallons) ( J-C__ )* Product Level-if present (ft below TIC) 2 * 0.0408 = gallons Well Depth Water Level Well Diameter (in) Purging Information Purge Method: " ^ L o w Flow NJDEP 3 Well Volume Not Purged Other Pump: )'^ubmersible Pump CZ inch) Peristaltic Positive displacement Other Pump intake depth: ^ ^ ~ ^iJ^dti^Jl3 Purge water discharged to: Ground Qf Drum Other Tubing: Polyprcpylene _)Oeflon-line Other / V ^ N e w Dedicated Time (HH:MM) Temp Ct) pH (pH units) D.O. &^I3L. Cond. Turb DTW (feet) Rate (jRp/min) Notes //r^.PO / J : / 7 Purge Start /^>7? 3/./^ PO^ 12X3. 0-7U >9f/ /s,n SCO %'OoTi 1 ^ O.I (33 S'/l>b3/£jS<A!: 5ik^-H3LL:X ..^ ^<^/-A ^ • , 3 3 ' , , , : 3 I0-33 % V 1. "il ML o-M y9f9 n o I M ML n.L;..t3/^.r....33331 3i 7 0 3 % 31.91 in I 33 i/>M 7 9 9 1 Ml. ^-vo I l 3 •^•J>(JA<ji CU^ tf /c^'n^ j>v,-r,p i\b.i4:i'Qymcuaet/.^h 44>1< 70'1< a.ol> nunip S"'fcj.->^/r puwi.pfv(i 11'^ 0 1 Ih. 5$ fe.-'i/jt ivslci. ^m II-U 3l3?> I h ? %.7& D-^17 -m. 7139 SDO % f : i ^ £3 i'3d * i l llLlA 2L31 7. 9L ^31 p. 311 3m. ItM ^ D V M2^ 2l 139 11-30 fltTiLp S'lefip,!cl •piOlUIAC'X-j lMo_ 1L21_ X- ex-sfcu> ^z II'if ^ ./> 36 ~) t i ' i'^ M£ 0'1^3 7999 p.3 9 SVv liS^ 013, J2 o3) t^glJiftfeA U^'^JK.U II'Hi 3All 133 8~Ai9 o. 3c7( >999 17 HI an) W r; i i o D.W/.HI IVA ^ & 3 i 3 g i 2313 L31 to.i^a ''999 QJL ^o(^ io-3 0 v/ % 7? 19'DO lUl i l ujdl'. CLOCul U \ ^ ^ - ^ p liilA 3'i 0 i 7.vr ^ . l O OA^Q 7990 i i M . .22ii 1 3 ^ o-^ia e./ \yiJ2 vc^\ * ^ OiMo-c LiAm a L.XX u u\(i/M^, hiJit K&t ^ Post-sampling Measurements " ^ " ^ Total Volume Purged / - ^ ^ ^ ' i ^ c^-y.nu.^^o/cf ^ ^ ^ ^ ^ ^ ^ ^ ^ ^ ^ ^ ^^^^^^^^ / % . r ) ^ QD-Sl Ctiuy.cuT- ' ^ ^ Sample Information Groundwater Sample Field ID TPP ()fY\P 3 b " VO OAJUI. ^ Z . ^ / i ^ a / i . Sampling Time Sampling End Time /.T-- 0 3 DTW before Sampling Sampling Method Bailer (type: ) Same as Above Other Sampling Observations 3 \ ^ Pc^M4? ^<xiioAi,uLu{ AuW <iC^ fo 7V y3.:-U^di. /^>•i> ~ 30o,3r/mM '• tc\3ti'AA% cii/^ix Sampling Pafametera ^ ,'l'*-'-1 P.iM.<5> 4l<Wrtt,l - See Page 2 of 2 fof GrcuMwater 305069 G R O U N D W A T E R S A M P U N G F O R M Well Number p P p - V n ^ P •- S O State Permit No. Project Name Project Number ras'^f^ Sampling Date Weather Sampled by: 3 AO - D o ••3<.-- r> n ^ 3 r j j ^ yo'-^ (inii itials) 6S Well Information '—' — — " " ;'"•";'—""TT" Well Type Monitor ^^Other V X ^ \ V Well Diameter 3 inches Well Construction V J P V C J^^F Steel Other JH'^ Well Depth (ft below TIC) Water Level (ft below TIC) Well Notes (Odor well condition, etc.) Volume of Water in Casinq (qallons) Well Screened interval ff?7S to ^"j'j.!)^ feet below TIC \ ; 7 - i i u : . : _ Well Headspace Reading (PID/FID) Product Level-if present (ft below TIC) ^Oci'73:^,v^ ^^ -Q.t/S X<a.y3^itkyy\ L J-C J 0.0408 = Well Depth Water Level Well Diameter (in) gallons Purging Information Purge Method: y^' Low Flow NJDEP 3 Well Volume Not Purged Other Pump: •yj Submersible Pump {Jl_ inch) Peristaltic Positive displacement Other: Pump intake depth: 4.7 .M;^ Purge water discharged to: Ground \C Drum Other Tubing: Polypropylene y ^ Teflon-line Other / J-O New Dedicated WxW Time (HH:MM) Temp C £ l pH (pH units) C<^_' DO /c Cond. Turb f >«A7>') DTW (feet) Rate ( /min) Notes • M l Bd<. 3^lm (AUP^I Purge Start liM_ /153 - h t A ' ^ s g ^ / T ^ (_ ^ 7 / a ^ n'^\ ni<: 7.JL M L 0-30 33A3L I^3± SUD. M. m. I l l lUik ^O.dl 7 OH O.^b o.PlI? 913 /3.^3 ^00 1^9 12^ 19 31 3^ P^ ^, f^ ff. r i 6.^09 21.& fSHH 300 IQ m N 36 3g,^^ l,37L 7?.31 O.'^ll 913 /111 ^Shl 7S 3 I3L jloL Mill A.93. 0.59 6. 21 oi nM /^20 5 0 0 4L 3 IAS iSo^l 3PA3 A l l 0.-i9 0.3i30 111.0 MRl y&O / 3 A L31 ISJL ^ . 5 ^ Gr AJi 0.3 A 11231 MJL MB Wl 5 - 0 0 I L ML cui'.j<j,Jl/9wf<^^ 3co l3/h Xll tM. 0.39 9,<i:/f' 23&1. roo 13 4- L^ i ^ % \ •3o,b9 LM- 0^33 o,2/2> 33/; g ^ 3 3 ( i ^od )3 d. LB. IS9^i, 37),-33 Li3. 0 . 2 1 0,1 f'l 3B7.0 /33i ^00 \ 1 i.3i 16 31 3D,9I LU. 0.93 o,2l9 9SS.0 /S'V^ 3 0 0 It lio ^ : t c ± . r , i € ) % A \ o . ^ 7332- P3 n 1331 30, al (,.9 2. 0.2'^ o.-m bno 7^'H^ SOD 1% ff j/.t/qPost-sampling Measurements Total Volume Purged 5 1 - * ^S ' " ^ 5 lApUi Water Quality Meter(s) fhr',iyic.U-^^ Sample Infonnation Groundwater Sample Field ID \ \' j"^ - V (\\ P - 3 h " l 3 ' 3 ^ \7D33i^33~(o337~3 Sampling Time j S 3 3 Sampling End Time DTW before Sampling Sampling Method Bailer (type:__ ) V<35ame as Above Other: Sampling Observations I t 7 -- 3.7'?i.;siA ^ See Page 2 of 2 for Groundwater Sampling Parameters Dcno 1 nf 9 305070 GROUNDWATER SAMPLING FORM well Number State Permit No. Project Name Project Number p f B " V " " l 3 0 ^'t(^,i^'!AbltL*.lChi?^,e3 ^ / A Sampling Date ^ / j « ^ • Weather ' ^ . . , Sampled by: /^uj , J ho K H ' W ^ L (initials) Well Information Well Type- Monitor < Other \ft^9 Well Construction J<PVC Well Diameter ^ Well Depth (ft below TIC) Water Level (ft below TIC) inches liZo-i Well Notes (Odor, well condition, etc.) Volume of Water in Casino (aallons) •Well Depth Water Lev 30^,i Well Screened interval ^ 7 >>' Well Headspace Reading (PID Product Level-if present (ft bel -^ ) * ^ ^ ^ ^ * 0.0408 = el Well Diameter (in) Steel t o ^ - ^ i ' f /FID) 3WT1C) other- eet below TIC S O .--— " gallons C a ^ -fC3o rt^^/l Purginfl Information ^ 1 Purqe Method: > Low Flow NJDEP 3 Well Volume NotPurqed Other Pump: '>^ Submersible Pump ( a inch) Peristaltic Positive displacement Pump intake depth: 7 1 Purqe water discharqed to: Ground /K Drum Tubinq: Polypropvlene >< Teflon-line Other / a<. . / iol/c ^'Vc / w /0,f<i Time (HH:MM) /3.¥'£r / 3 i 3 i 1^39 l i 6H M(3} H 7 9 l<7 /9 H:7.9 iH-73 iH3H H39 /¥:^^ I^:H9 H'.39 N . ^ jiT-cXA Temp C ^ — n.n -31.01 31. i9 3 A as 3i,30 •3/<A^ 3171 31. i i ShTL^S 3 I . X I •NAiH U39 3/,H6 i/or pH (pH units) — ^.^S CH>I L . ^ C,%X 6.^2 C . ^ £,'63 i.H3 L-O c.^3 ^,^3 C33 c¥ (^•6V DO. Q2./_LJ — :i.93- >^H ,H5 , 3 % ,5H 3 1 .U /X\ .19 . / ^ . • / 7 ,IC ,76 i^ Cond. (^//n ) — ,/97 .7^0 .U9 .933 M ' i aiH .Rl3 , ^ ^ 1 . .3.^0. ,773. .^.^'1 , ^ ^ ^ ;^7^ \ . ?-ia Turb (/vrc) . — / / ^ s.? Y^ A3 ^.i lS,l ^1.9 9 Co ^,7 3 ^ ^n f A 6,0 n o DTW (feet) /H.n 1^3"^ i ^ 3 i i ^ 3 i f33.'^ /S.37 r^i^i i3.-iO 13.^0 I D HO / - ^ ^ ^ fS.3'i /S.3'5 IS.3^ /s.-?o Rate ( .n'/min) , — 3 ^ r5l6 :i-60 &.'m '19,0 ^90 r^9^ c^Bc ^ 3 0 ^ ^ 0 2 ^ 1 ^ 7{70 ^7<? ;^/5 Oil/ . — - y ^ -^3 - i 5 -9 •s -C - 7 - i -C ' S ' 3 - r - 3 - ^ other Other New Dedicated ,— ,a - / / . ^ ^ 71 /.fo ,n .// .7/ ,// ..il . / / . / / .11 y / /.W /.vy i.'Ti I.H7> 7^H-5 1.^.1 i,-^ / . ^ LiQ 7/ \7-< // i / ^ ^ \ . t - ^ I 7 / i / ^ Notes Eufie^taft / \ f 9 ^ f P^st^ /"OI^C- S T^i t>Am^l^ f i d , cllS.3l,*f Post-sampling Measurements Total Volume Purqed Water Quality Meter(s) Sample Information Groundwater Sample Field 1 Sampling Time /S:^<j Sampling Method Bailer Sampling Observations Sampling End Time t b ; C3) DTW bef (tvoe: ) V Same as Above Other 3kiii d o t ^^ ^ ^ ^ ^ ^ ^ ^ ^ ^ ^ ^ ^ ^ ^ ore Samplina / S . - ^ - See Page 2 of 2 for Groundwater Sampling Parameters j 305071 GROUNDWATER SAMPLING FORM Well Number Llpp^x/fi-^p . 5 ^ State Permit No. Sampling Date Project Name Ai.&>a-' -A AkA.A.:'i f<-J? • Weather Project Number Sampled by: ESil^kW ZA-I'AJO :AU.-t\AH (initials) V\fe|}:|nformalion Well Type: Monitor r^^ O t h e r \ l / . ' ' r Well Construction V PVC Steel [Well Diameter - l ^ Well Depth (ft below T I C ) Water Level (ft below T I C ) inches ' 3 ^ A 7 ^ ^ n.v.^ Well Notes ( O d o r well condition, etc.) Volume of Water in Casino (aallons) |( ) - ( Well Depth - Water Lev Well Screened interval.-i7-:S*^ to 7 ^ 7 ^ ' i U Well Headspace Reading (PID/FID) Product Level-if present (ft below TIC) O t h e r 2et below TIC ) * ^ * 0.0408 = aallons el Welt Diameter (in) Purging Information Purqe Method: 7 - Lovv Flow NJDEP 3 Well Volume Not Purqed O t h e r Pump: :>^ Submersible P u m p ( ^ inch) Peristaltic Positive displacement Pump intake depth: 177. Purge water discharqed to: Ground v: D r u m O t h e r O t h e r Tubinq: Polyprccylene 7 . Teflon-line O t h e r / V" N e w 1 Time (HH.MIVI) T)^ 0<^~ \x^^iO<' O ' S G S O l 1 ! oi:}.0 1.'.- /cy-' •J^AO 1 !i;'5< 3 A o U.f^^^ A - . ^ ' . .•' --S. Temp CCJ "7.^ .3^ Z £> 3 o 3..GS ' 3 1 • '-• ' f • A t . : ^ 3 ^r?|.. 3^A-y^' 7v \ ^ 3 0 - ^ 1 , ^- ^ '* • r" pH (pH units) AS.XA •3.A\ - 3 7 3 3 - A O •?.'?.' ^A~A7. ^ • y . c < > ' "7- 3 7 7- 7b d - • ^ 3 ? •^C V:'\ I'lASA" Total Volume Purged 0.0. 1(1^/-) I ^Ai 1 . o 3 • ' \ . o 3 A ^ o U 2 . 1 1 . V . * . : V / C 0'-^~- ' t . ? . ; ? - 3 3 1 ' A L o 1 . A i Cond. p-5M •D. H i 7. H I A- 'fW ^ A ^ A. A l -3-11 A . I. A Turb ((\)TiA) \ ' > ^ A \ 0 \AA11A 1-^T;O '••> 1 ••?.:• ' V ' / O il n o >'j-lo 1.7-0 7 1 , 0 {..•• c ^ r ) DTW (feet) [333 l O . / < i?. L!> | 7 • 7 ^ : • 3 i { 3,-A-'-^' 33^ Rate (r'> I'/min) '330 A. .•v-,.~. 55'-^ vSO /-?r''7 v.: A (. :• Tf-.Xf &3 - 7 h '?fc I h 1 1 1 • ArO^ - U 'A' ( 1 < ^ j j ^ _ ,' '•'• •;:.) < Cj% Water Quality Meter(s) .:x"< /• TU:' i^-/^.^ . ' , \ \ . A l A -35 . . ! 7 . A A -.. 1 i-A- ^ 1 '. !.,^t.-. - - / - - M T - i ' i 1^3 - ! \.x.'-l . \ AA7, * • ' ' ' ' • ^ - -./ j.'l,^- Dedicated Notes Purge Start A7h\ ')n I n ^.A: •-_••:.-;-nr:r!..ci:' ••P/-1.1 - n ' 6 ^ : < - b ; O'; ;> 5 D " u - . b ^ : U i ' ' .A;..<r-^.^ [ <Mi..-Yi--^-' • Vi4':.' --". •i</,A /n.> T'~ "'"" J . • ' • • r , {• -.-,.: ^^ .^ . .^ • ' . ; • * ^ ^ . , " T " 1 ; ' - <•••:',<-.K.,t-r.-;:;,. . ( , ' v . i - .:.'Wt^t^'''- ^v'j'. »o2:7,,a.v.:p^.>r. .,f ' i V i ^ V ^ /'•r ( ' Post-sampling Measu A: -'l2--(A'-'r: t-l \ rements Sample Infonnation Groundwater Sample Field ID Sampling Time )' Sampling Method _ Sampling Observa '7 AA Bailer ions Samp pfr-.\/(v\p- -^i, ling End Time (type: ) 6(5,. •- OiS'^-sii L A''- / _Same as DTW before Samp Above Other lina ^^ —- * • a i 1 - C - - D-,r.e 1 ... -> fr>r r. f\ inH\A/:^tpr ? amolina Par ameters 305072 GROUNDWATER SAMPLING FORM Well Number lA?P- ^ n i p • '-ill State Permit No. Project Name Project Number ESS'^ wt . Inc. Sampling Date Weather Sampled by; /x. i n - O ' j S i U A ^ A A -•^-, jUfe, UA) (initials) Well Informalion Well Type Monitor ^ O t h e r Well Diameter ^ inches 31^.^ Well Construction J K ' P V C Steel O t h e r U .1. h h 15.30 Well Depth (ft below TIC) Water Level (ft below TIC) Well Notes (Odor, well condition, etc.) Volume of Water in Casino (gallons) ( ) - ( Well Screened interval J T J i X o i 9 A feet below TIC Well Headspace Reading (PID/FID) Product Level-if present (ft below TIC) J* 0.0408 = gallons Well Depth Water Level Well Diameter (in) Purging {nformation Purge Method: X^'LOW Flow NJDEP 3 Well Volume Not Purged Other: Pump: _ ^ Submersible P u m p (Jj^inch) Peristaltic Positive displacement O t h e r P u m p intake depth: 1 1 1 b Purge water discharged to: Ground A ' D r u m O t h e r Tubing: Polypropylene Teflon-line O t h e r / V N e w Dedicated 3M^ Time (HH:MM) Temp coj pH (pH units) D.O. ( M ^ t U j m3 Cond. s-/ <7\) Turb (<xi;) DTW (feet) Rate ( / W / m i n ) Notes Purge Start ^c3iuj 6>./y? l i S3 7H 37 7 7)/'n A ]13h 79^3 '^*^c n 7 r>A.t A^L>3.^:cAu^.L33'J iTgrS^liy ^ /5 07> l y ) <? M 3 • t v mi 13 0 3 .77. ds 1 <fir /so 1 A3.73 3AX'3 yiltA-'-^'f^ Sa->r^/A^A^'i iLjd. i}.?3-' J 9 - 19 AO ISO /I .- ,J./ i<3^ IS I'd 1 a c^S7 c, 760 99-0 7A -A ^ ML 1? I \ J . ^ ; IS I'i 7 'D 0 3 l 77. 9977 / ./ / J ' ^ I S . •sy J 7 ,^d>cu>f '7t> 3 V O T 1770 3A.^d '770 /hid' 0. u s 993 /t.'TD 300 J73_ , 1 3A< 3l)Ali 7.1.-9 77: S^/ 7?.A60 9 3n 7^:73 SC'O 7. A3I) 3D.(,I API oAL 7J. 773 •10 l'37i .^Vl .!-> \17 5.3S •'hd.(.3 I M o u l 0.76(, - 7 ' < // 90 'OO t l 33131 /A^O 3i)33 ./• i ' S 77 19 /}. 760 7 ¥ 0 / 7 97 >VD a \ 3V-7I I D l oni 77M 130 II /ASO 3f). 1 ! l o l (}' l) 7 - ^ ' X •3 'A . f; V I V ' t i / 1 Ot> O A < J % r 6 / iL2iL 10 30 0 /• r 9 Vil? 5-75- ^^72_ u JJiZ. U i . : l ' < i . ^ . . .yv.. J?:"'. /^, I'y| :3^.V^ ?./T7 7.S7 \ / P , 7 / ^ \ 9 / 0 /7 ^'.^1 ^'^L //'• / : /. 7 Post-sampling Measurements Total Volume Purged :}\3-^ ?l ~ " ^ l ^ l ^ ,'.^ J^Vater Quality Meter(s) m Sample Information roundwater Sample Field ID r-pt>-\/m^ - fO Sampling Time /^, /•-'<f Sampling End Time Sampling Method Bailer (type: ) J^Same as Above Other Sampling Observations 7 \ ^..i; - S.l'^t irtju \ ]'i-.v^^^ x 'i--^in.i -- %i,-5 r n , ^ DTW before Sampling /o, y'x - See Page 2 of 2 for Groundwater Sampling Parameters P a n p 1 n f 2 305073 GROUNDWATER SAMPLING FC \ \A/»ii ^tllml-.<.^r r- n O ,t .^1 y ^ j i i ^ ] well Number State Permit No. Project Name Project Number . r r r ur/t^ -^^ \)^<^n\Ar^3(ih3 C'lu'iyttt DRM l/3.1e Sampling Date 3 / 3 ' 7 < ^ ^ Weather Sampled by: BH^'Me' (initials) Welllnformalion Well Type Monitor X Other l j „ p ^ r / i „ h ^ P f Well Diameter ^ inches Well Depth (ft below TIC) -^9.^' Water Level (ft below TIC) Well Notes ( O d o r well conditic i(,.10' )n, etc.) Volume of Water in Casino (aallons) ( \ - { Well Depth - - )* Water Level Well Dian W e l l Construction V P V C Steel W e l l Screened i n t e r v a l / ' J ^ to S!7.fi^\ Well Headspace Reading (PID/FID) Product Level-if present (ft below TIC) other eet below TIC n M A >o 7"^<!is,^i7 ^ * 0.0408 = aallons Purglnfl Information Purge Method: _ y Low Flow NJDEP 3 Well Volume Not Purqed O t h e r Pump: \ Submersible P u m p ( ^ i n c h ) Peristaltic Positive displacement O t h e r P u m p intake depth: ^ 7 . ^ Purqe water discharged to: Ground X O r u m O t h e r Tubinq: Polypropylene ^ Teflon-line O t h e r / ) ( New Dedicated Time (HH:MM) 1 730 ' -;M6 i : S i l.Si. if.oi ^ ^ ^ ^ rJi %A V^H i A \ 1^3^ ^ 3 ^ r^'i fA"] 3'59 1 3 ^ Temp 31./J W3\ lb.3] y).(^ % 1 ^ Ui'O im V i 3 ylb^- Ul) U 7 \ '^M U(>\ 3 i n DM pH (pH units) 1.10- 7.01 70'I ID'S 7./0 7 ^ ^ 7.01 1.0^ 109, 701 l O i 1.01 701 101 7 0 l DO. ^ 0 3 i 0.^1 o3^ o:r\ 6 I'i oii^ 0.i,l oU- C-Si 0 , ^ D.(JI osi 6.51 c . b l 0.00 Cond. 7?SO J.UO m J.02 J M ^ l.LQ 1.0 fS^ 7.i,K Ji.Ol I b l tl.iil ^.i'C' ^.OV l b 3 J ! . ^ Turb ^31) 370 3(,0 710 3i\0 1^0 lou m no Q^O S-/0 no %o foo S%0 Total Volume Purged Sam Groundwater Samf Sampling Time Sampling Method, Sampling Observa 3le Field 1 Bailer tions D p f P W P i D Sampling End Time (tvoe: ) DTW (feet) /(^.o/ IZ^^ I7J7 \-].\% \X\% j i . n 1170 I7CG I7.i;0 \\^3f \l.h°l 17.(7 i6.^r 175-1 \1S9 Rate ( vhf /min) 31^ — — 77^0 330 — JIO — ^ f / — — sv 377 OiP J 3 n H -^3 'IX 3 0 - / c / ' / 5 - 7 - | C ) -10 - / ( . ')> V ! ^^(^ 0.1 OA C:\ O.i /},] 6,i al 6.1 o.i 0. o.i (}.l o.i IM ti^li i'0 1.41 U9 \.70 1.11 p;j l.7| i.V '-•'1 1.70 oo 6.\ i.io all i n 1 Notes Purge Start A(,V;+"J -h.^ n7<- Post-samplinq Measurements Water Quality Meter(s) pie Information _Same as DTW before Samp Above Other lina 1 - See Page 2 of 2 for Groundwater Sampling Parameters ' D o n a i n f 9 r - - ^ 3 0 5 0 7 4 G R O U N D W A T E R SAMPLING FORM | l \ ^ ^ M ^ l ^ f ^ p D Well Number p f ^ - V m ^ ' V ^ f f o j . ^ r \ A m l H B r t i n c State Permit No. "^^ ' Sampling Date ^hljOo Project Name Weather ^'''7, Project Number Sampled by: (Initials) liiiiiiiiiiiliiiPiiiiiii^ Well Type: Monitor O t h e r Well Construction P V C Steel Well Diameter Well Depth (ft below TIC) Water Level (ft below TIC) inches Well Notes ( O d o r well condition, etc.) V o l u m e of W a t e r in C a s i n o f a a l l o n s ) f ) - ( Well Deptfi Well Screened interval to f Well Headspace Reading (PID/FID) Product Level-if present (ft below TIC) O t h e r eet below TIC ) * ^ * 0.0408 = Water Level Well Diameter (in) gallons Purging Information Purge Method: Low Flow NJDEP 3 Well Volume Not Purqed Other Pump: Submersible P u m p ( inch) Peristaltic Positive displacement O t h e r Pump intake depth: Purqe water discharqed to: Ground Drum O t h e r Tubing: Polypropylene Teflon-line O t h e r / N e w Dedicated Time (HH:M1VI) 910 "i <^m q:H q;il V7i 9'7'\ r-ii ^-.Jif q;H^ ^A") n.s'i lO'.cPl Temp 3?M^ m V.$3 3IIA^ JD.i^O 3119 3;.5^7 31-31 7iAl 3,"?1 ?/>^ M.9ii pH (pH units) 701 7J3^ 7.0^ IM lOi 1 ( ^ % 70l I t i 1.0% l 6 i n.o\ l i t DO. ( / ) t.9l c.u l^'T fl.M(y e?1 0.^1 0. ffC' 0.^3 5.^1 0.3^ ^ 3 ^ <5,b^ Cond. ( ) 7h3 M' J.l^'t 3SL m /6y j . G S ' ^•3% 1.^1 c^.S? a.CI Wl Turb f ) 53C7 Wo 510 Hid 910 ^ 0 ^10 CIO 1^0 110 iHo ^(777 DTW (feet) n.j^ \ i ^ ^ \%i< itW [lA^ \'i.9<r if.oi lf.?p 1771 •r.)^ 17?^ iLlI Rate ( /min) ^ 337 HOO — — ^ — - • ^(?d 3co — - ^ i S O oce ~'f ' H - l l , ~lp -19: -17 -\b ^ $ - / ( -'7\ -\H 1, 5»*<-i7Bj m . i ] <'i\/.7C7 C.]\ 6 \ 0* i \ D.i OA o.i Ol O.i 110 lie l.0$l U9 LU Uf 139 U i IJ;^ o.i \ l P Notes Purge Start Post-samplinq Measurements Total Volume Purged Water Quality Meter(s) Sample Information Groundwater Sample Field ID Sampling Time i t - t b Sampling Method Bailer Sampling Observations Samp (type: )ling End Time \ 0 , \ 0 ) .\Same as DTW before Samplina l<»-7) Above Other 1 - See Page 2 of 2 for Groundwater Sampling Parameters | P a n e 1 of 2 3 0 5 0 7 5 • I GROUNDWATER SAMPLING FORM \ A / ^ l l M l i m l - i n r /-'.y.^ /">— I IT-.. Well NumDer State Permit No. Project Name Project Number V 1 ' \ ^ - V i J • Sampling Date Weather Sampled by: KSSl^f^ ^ ' j ^ ' o a (initials) Well Informelion Well Type: Monitor O t h e r Well Diameter Well Depth (ft below TIC) Water Level (ft below TIC) inches r Well Notes ( O d o r well condition, etc.) Volume of Water in Casino (aallons) f ) - ( Well Depth Well Construction PVC Steel Well Screened interval to fe Well Headspace Reading (PID/FID) Product Level-if present (ft below TIC) Other ;et below TIC • ) * ^ * 0.0408 = qallons Water Level Well Diameter (in) Purging Information i Purqe Method: Low Flow NJDEP 3 Well V o l u m e Not Purqed O t h e r P u m p : Submersible P u m p ( inch) Peristaltic Positive displacement P u m p intake depth: " 2 ^ 7 Purqe water discharqed to; Ground D r u m Tubinq: Pclvprccvlene Teflon-line O t h e r / Time (HH:fWM) s f^r, \ lA3^ lA^i) m'i Temp C_3 ^'1,33 l o - l ' - '•iA-A.' 3'. AAf 3 ' A^i pH (pH units) l . ' i U H i * ' . \ * " • • , I.I'.. 773 ' Total Volume Purged D.O. L_/ ) 'A-)AA3 =7 3 3 t-<i7 A-. ->...-, A f i o Cond. ( ) n M i ..._. '-'.A -I Z. AH 7-. S 3 0 C<' * - . .J ! Turb ( ) >71^ 7A'A >7'> - f f t ' DTW (feet) l A l i A • Rate ( /min) OKP CA^ "7/ 7.< ^AA OA Water Quality Meter(s) 1 other 1 O t h e r I N e w Dedicated S-^A 7^6 J h5^ - • f';S • ' • ^ c - t • / -UA Notes Purge Start \ ( ^ A 3 V € V l . i <A- l-^M • t r J A ' i ' i J AAr^-'.i^ u .:•:• 'f /i',^A?.i.-(r> , ,.., — . — . — (<5-43; h--,-."^J A'^-'^-^J A.-c' \ — j . — f . 7.-'A f S / : - 0 0 3A:>.,'<^-7 otx^r-^.. {]liv^.>)i.e- r n M.'i.<.-.-f;-Uv_ C,.V:J t'iiv.' 1 - f ^ . - Post-sampling Measurements Sample Information Groundwater Sample Field ID Sampling Time Sampling Method, Sampling Observa Bailer lions - See Pace 2 o t 2 f o r G roundwater S Samf )ling End Time (fvoe: ) _Same as DTW before Samp Above Other linq ampling Par ameters 305076 GROUNDWATER SAMPLING FORM \ A //.^ 11 K i l l rr., ^ r ^ r C .\ i". . .... O . .- A Well NumDer State Permit No. Project Name Project Number r (• r i/*»i r 6/ u Sampling Date Weather Sampled by: 3-70, ..o^- (initials) f^^mWE Weil Inforrneljon Well T y p e : Monitor O t h e r Well Construction PVC Steel Well Diameter Well Depth (ft below TIC) Water Level (ft below TIC) inches , n , o h - ^ Well Notes ( O d o r well condition, etc.) Volume of Water \n Casino (aallons) { ) - f WellDepth Well Screened interval to f« Well Headspace Reading (PlD/FlD) \ 1 3 0 Product Level-if present (ft below TIC) , ) * ^* 0.0408 = Water Level Well Diameter (in) O t h e r 2et below TIC qallons Purging Information Purqe Method: L o w Plow NJDEP 3 Well Volume Not Purqed O t h e r Pump: Submersible P u m p (8t'inch) Peristaltic Positive displacement P u m p intake depth: o?7. S Purqe water discharqed to: Ground D r u m O t h e r O t h e r Tubinq: Polvpropvlene Teflon-line O t h e r / New Time (HH:MM) / T ^ Ml /1<3 [133 ' "'37 13 / i l^.'S I t 13 i9r 19 1 ^ ' ^ /V3/ Temp (°_) / f^V/A.'? ; -J pH (pH units) i%i-l37loi Total Volume Purged D.O. ( / ) Cond. ( ) -Mcf Turb DTW (feet) ih-n PC ^31 3^^A d37 IL ^il 13 36 Rate ( /min) ajJAi^l -.c 7 ly'^A-.^, ^~y Water Quality Meter(s) ^ ' ^ . Dedicated Notes Purge Start S'/(Ju7, y / ^ < ^ i ^ ^ A - <;o.%',i.ta ^ ' y v y ) Af''^-v77'b.'0:.yJl-VLAAt^.^ r , , A y - 33,1/- . . j ' ^ ^^:-^^Ar cVK^'f'ApA-r /-.I ;A'^A7A s ' ' • • - . . A y o ' /-•• "^•"m^d ac/^l^ ls^A,±3(r^Ayi t / / 3r'i>fY^d/(/<:,4cA., •37 ;/ . ., 7 3 y i , r - A 'i^X.^OeC/' fe A A ^ 7 f.' ' r P o s t - s a m p l i n g Measurements Sample Information Groundwater Sample Field ID Sampling Time Sampling Method. Sampling Observa Bailer lions Samp ling End Time (tvoe: ) _Same as DTW before Samp Above Other lina Ccfl Pano •? nf •? ir\r (^rr.iinf^wstpf *^amclina PafafTieters 305077 GROUNDWATER SAMPLING FORM Well Number f ? ? - </fnP ^ ^ State Permit No. Sampling Date Project Name • Weather Project Number Sampled by: ESS^ art Inc. H-3c^oc7 i^•..:.^.\r>../ -?o Sd. (initials) Weirinformaiion Monitor Other 3 inches Well Type: Well Diameter Well Depth (ft below TIC) Water Level (ft below TIC) Well Notes (Odor well condition, etc.) Volume of Water in Casing (gallons) Well Construction PVC Steel Other Well Screened interval to feet below TIC n. 19 Well Headspace Reading (PID/FID) Product Level-if present (ft below TIC) 3lr&.r..u.fL S7(l Sjdvyfi^nji ^ i / ^ ii-..^^^fcw.&g--^ L J - C ScV: UAJ i\ijf~( ^ 0.0408 = Well Depth Water Level Well Diameter (in) 3 7iLi^ gallons l/i^ Purging Information Purge Method: ) 0 Low Flow NJDEP 3 Well Volume Not Purged Other Pump: :^ Submersible Pump ( Z-inch) Peristaltic Positive displacement Other Pump intake depth: 3 V , S" " Purge water discharged to: Ground 7^ Drum Other_ Tubing: Polyprcpylene "jQ Teflon-line Other / J ^ N e w Dedicated I ime (HH:MM) Temp cL> pH (pH units) D.O. (.^'s' L) Coryd. .ytS^ct.*: Turb (J£OZ) DTW (feet) EM Rate l_j^lrnm) oep ^dL r£<, Notes 1333 Purge Start IS 3 1 .m3 1.93 3313 3J2. 7990 mu. .7Sc /.?Q OA 7.6S ili%i A^jA Aiurt. i s l ^ 7%1% A.3% -7-9^ 2J23 >r1f) IS. 90 ^.fi'i.-' .1 j L IO /Si% Q i 3 t 7. 35 A.'JA •0 .66 > 9 9 D }%'5) :;i^6o I O \ i \n] il^ 10.b3 1 39 3% A 3 I d 2311 I3M J3Sc 1 3 \iP3 \3S3 ' i . ) 0 ! 7.3.3 1-77 X 2 i 7 ^ 1^0 J3M :J6C' ^g a i A-li' H.;03> •V/-73 7.31 7 77 .? 77 •>9 90 /8.H .^So 11 0- i \ 1:7} ] i 0 ^ 3 \ 1 ^ 130 7 10 3 1 9 79 97 li-. 7 b =3 s i ; 9 ^ "7 US i b l 1 p . ' y i 1 . 3 2 I 7 1 ^ \ ' 2 1 3 \ "^'^f7^ I / ? • 3 3 1 1 ^ 7 3 I 1 9 W - 1 //-^IPost-sampling Measurements Total Volume Purged Water Quality Meter(s) Wc:)^, U;-)a ^^,^>v^,.j^ ^ 0 ^ 7 Sample Information Groundwater Sample Field ID Sampling Time Sampling End Time fp?-V,Y|P -^D Sampling Method Bailer (type:_ Sampling Observations S^ Akl5_ DTW before Sampling /S^/'^ 3 _2_Same as Above Other_ ?ce Psce 2 of 2 for Groundwater Sampling Parameters 305078 G R O U N D W A T E R SAMPLING FORM Well Number f ^ f U f l t P ^ [ ) State Permit No. Project Name Project Number ESS'V^ffr" Sampling Date Weather Sampled by: § . ^-i-va SA. ^ SO (initials) Well Informslion Well Type: Monitor .^o Other [ I f C l P Well Diameter ^ ^ - inches I^yfif Well Depth (ft below TIC) Water Level (ft below TIC) Well Notes (Odor, well condition, etc.) Volume of Water in Casing (gallons) Well Construction ' y ^ M C Steel Other Well Screened interval ol 7-5 Mo 7^- //feet below TIC Well Headspace Reading (PID/FID) Product Level-if present (ft below TIC) • c J-C 0.0408 = Well Depth Water Level Well Diameter (in) gallons Purging Information Purge Method: ^ ^ L o w Flow NJDEP 3 Well Volume Not Purged Other Pump: yjSubmersible Pump (_2 inch) Peristaltic Positive displacement Other Pump intake depth: al7^ 3 3 Purge water discharged to: Ground Drum Other Tubing: Polypropylene Teflon-line Other / New Dedicated lime (HH:f^M) 1-GO Temp pH (pH units) D.O. • ^ iL.) Corid. Turb u!^n7_) DTW (feet) /^.? Rate {lAJtylmm) T Ozp ^,^A5S5- Notes Purge Start y / ^ ^ / 5 ; / / g 4 a < - tmr*A'7u^ 10< 3aj3 7J^ r j 3 cm >M. 1(7^03 3 ^ 2 . J03L 0.13 1,7a ^tAc ttu y^^Uri iio 33.5V iJK 9^^e Or 9 69 7^99 im. Jso. ^3L^&3L71,Z^IMU^3%SAM f e r 3/£ ^liM9 3L1A. L 3 3 0'7hl W- 3313 11V 13bL O r T - l l mi. 10.19: QSO I Q ^(3 hjo n99 i%9^ a.^o fz ^ m n 17LTL«ZO^. l A ^ 33 2\ 339' IftL ^LM- ^991 M/i ^30 o d im %M 3 3(^9 III. lai 0.221 mt im. 3519 9131 11% ^ . : a ^ . ^ ^ v o ^ ^ r / A " ^ ? m. 3lf^ 138 211 OAllO im. Ml ^w V ^ U l m- ^3\\ 737) "^.01 0^933 \y9^c^ ^0,21 \ 30O \ro9 w 7-7T Post-sampling Measurements Total Volume Purged Water Quality Meter(s) Jb^.M'uw^-M^-llq 072 - 0 ^ Sample Information Groundwater Sample Field ID l^/T ] / ^ ? ^ ! > -h-^UQ^CO, Sampling Time Sampling End Time ^ 3 S ' DTW before Sampling Sampling Method Bailer (type: ) Same as Above Other, Sampling Observations C.(\ t f < y ^ . ( g f i y - ?f p Faoe 2 of 2 for Groundwater Sampling Parameters APPENDIX D Chain of Custody Forms t 305079 -A::^>9A^.- P a c ^ Analytical . ^ . ^ ^ ^ ^ ' a . . . - . . ^ , . . .-..^.'t i'" iftf,t;iiyii iiw'iiMt-. The Right Chemistry, The Right Solution"' Required Client Intormation: SeCtlon A Required Client Information: SeCtlon B GHAIN-OF-eUSTODY/Analytical Request Document The Chain-of-custody Is a LEGAL DOCUMENT. A l l relevant fields must be completed accurately. Page: of Company f^^JA.H.A:a / N Bl. Reporl To: MfjtlMH EiC\W:iti. 517694 To Be Completed by Pace Analytical and Client S e c t i O D C Quote Reference; Client Infonnation (CtiecK quote/contract) .^h J^i'tfl'^Ni i tu.. i i U H J - Invoice To: Requested DuaOate: •irrcY_ 'TAT: Proiect Manager: (.,)i¥i^.fsl. N T 07069 Phone Project Name:. ^()Sfei7-8i^A Project Number: 6L/)NL f\,^.-., ^ mA * Turn arourtd times less ttian 14 days subject to laDoratory-and contractual obligations and may result In a . Rusti Turnaround Surcharge; ' Turn Araund Time (TAT) in calendar days. Project #: Requested Analysis: Section D Required Client Information: S A M P L E I D One character per box. (A-Z, 0-9/.-) Sample IDs MUST BE UNIQUE %&' 'im i i 11* m -mm tmi tm W T •^rTT vJr : . . I l l : O o mm I d6lyy O - & - 0 O 9-^'5a.. W l 3-S-Qo 3 •6-06 3 . g>. Oo m ^ o u titirmm a/p B-CJQM z ir-<b^ ..^ 'J. • -; ^£^S Preservatives / / / </ 7: ^ i^«4< 'i ^': Remarks/Lab ID ,-*!: S ^ v£r 3-7-0O ? : ) 5 ^ 3 i J i m m WT 3-6-00 5i06t / « gi '''^•^p!' m M A l 3 A : 0 Q33x 1 7 '"AM m m v j t 3-b'-<30 / 4 ^ ¥• * ^ g v\^i T: jg. f 3 y S ^M ^'' pis 1 ^ fm m«- \.vr v. Go aific VV'f ^ • " I ' A K <i.^l-|^Jll:J»I-|^,•e^^4. %'- mi m WT 3-9-o<i / eW !-^'ICliLi m t-C lIC-i-rt'iTltJu^ruO K' ^ •~!^i ;®5; Iteriii No. Relinquished By / Company |f^ ii'ii" rAjl. Time Accepted By / Company t | - 4 . vi..n".l-i Irv.^ KAtXr-ia^/Hiitj 3'S-oo N t o ^gt^a..-iu GJ''E •'li/'..6tj Date Time a,.' 3-<Lid Nop f-^oxti^i, C:'<.(ia£€,<, Additional Comments: 'Dv..ti.'"'V'-v>o^" 0;fvvpf u/r>do : ';>£ji:Tcr, ^ULtcrrvi. I cTmiV-)|j;L'^-*- C-l.h>>urU--; Q-hlcics-vtiTA SAMPLER NAME AND SIGNATURE PRINT Name of SAMPLER: " H t u i ; > \ 2 . , v£t^•|vJib.&^,•'.,J^,^X__ ,4tf^^ YVj U > \ a o SEeflEVERSE SIDE FOR INSTRUCTIONS SIGNATURE of SAMPLE: _, . DATE Signed: (MM / DD / YY) 3-9.OO Pace Analytical Services, Inc. Fom^i COC01 .XLS 12/99 SJ i-oce Analytical The Right Chemistiy, The Right Solution® -i^;iiiiil CHAIN-OF-CUSTOPY/Ahialytlcal Request Document The Chain-of-Custodyls a LEGAL DOCUMENT. All relevant fields must be completed accurately. Required Client Information: Section A Required :Client Information: Section B Page: Company Report To: 4- of 517695 To Be Completed by Pace Analytical and Client S e C t l O H C Quote Reference: Client Information (GhecK quote/contract) Requested Due Date: Project Manager Project«: Temp in °C: EGEfc*?trtyn2E5B~ i2>-oo \yM Received on ICE: '..Ot^UHU iZ'i^\'U^&3 LO O Ln 00 Sealed Cooler: Y / N Samples Intact: Y / N Additional Comments: '-^V.i 1 f: 1 c 3 V '.-w -h- t,Kx.i..-,u!_., •^33; vJ I hui/rx'^^, , , * - . ) . ' C c c D c i / c D c c cknc SAMPLER NAME AND SIGNATURE PRINT Name of SAMPLER: NJfu Mft i . PicULiM JURE of SAMPLCFl: . ^ I »- i f i SIGNATURE ^EE REVERSE SHciE FORINSTRUCTlONS 4 noN t. i..-i->^a., GS vA.lnL ^ DATE Signed: (MM / OD / YY): 3 . In.r'in Pace Analytical Services, Inc. Fonn COC01.XLS 12/99 ^ , ace^nalytical The Right Chemistry, The Right Solution'^ Required Client Information: Sectlon A Required Client Information:. SectlOn B CHAIN-OF-CUSTODY /Analytical Request Document The Chain-of-Custody Is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Page: Of 517697 To Be Completed by Pace Analytical and .Client - S G C t l O f l C Company p. U=AS- Report To: Mri 'c.K..Hl>r4 Client tntormation (Check quote/contract): Quote Reference: Address M*i i U A i j ^ j^cX HLA/CJ Invoice To: "A:r-i.c ii Requested Due Date: ^yi:.KU:T , b ^ ^ l R z C Project Manager: ^f-L.£fi M T G'/Qg^ Ptione 3LM3M. A\\\ Project Name: Project Number: -Ci ^ . . 'yttir'iL, 0\tl\ji.'•• ^'Tfc * Turn around times less than 14 days subject to taboratOTy and contractual obtigations and may result In a Rush Turnaround Surcharge. Turn Around Time (TAT) in calendar days. Project #; C A j f r ^ l - A G Z 'Section D R e q u i r e d Cllenl information: S A M P L E I D One ctiaracter per box. (A-Z, 0-9 /.-) Sample IDs MUST BE UNIQUE Valid Matrix Codes A MATRIX WATER SOIL OIL WIPE- AIR TISSUE OTHER CODE WT SL OL WP AR TS OT LU o o mm / dd / yy Q HI 2 LU f=zl O U hti:mm a/p i-Cf- I0:60a • M . M r^ A -?-Oij IO-/5fv Jiu.1 -f(LLP\/C(l6 ^ ) 4iii. /Q:2IQC^ / 1 7% •® •M^^ >-C0. ^1373333336333(10 iii i . ;«;< * 2L. ^, ) 00 UHilB. <»— / J 'i/i 3i- M!» %1 ti>l W5? Ul t -^ ^ n j -..M 7'.. m m ^r5 litH SS» lE'l <^f Itn iA}. * * 4' ¥ • 4 P7 ^ ^ :M m .p-v M * i Relinquished By / Company Time Accepted By / Company Date Time .W:^^ ^-t -.ji--'~.-'^nv^—f^L-u-<t-;:t- Mdi^i-;;M|l\iKr •^KT Uicfir 4 •'J4JCJ-HL. C-><t'Cdb.:> Sloci m^ w o Ln o 00 to vf.D"i:.>u., v i y C££S£j Additional Comments: SAMPLER NAME AND SIGNATURE PRINT Name of SAMPLER: k^ SIGI >^S •j) i H f V b — DATE Signed: (MM / DD / YY) 37-i oo SEE REVERSE SjeE^FOR INSTRUCTrONS"' " ^ " ^ Pace Analytical Services, Inc. Fomn COC01 .XLS 12/99 fij Pace^^nalytical Tlte Right Chemist^The Right Solution® CHAIN-OF-CUSTODY 7 Analytical Request Docu: The Chaln-of-Custody Is a LEGAL DOCUMENT. All relevant fields must be completed accurately. '''.>jr-:.~ Required Client Information: Section A Required Client Information: Section B Page: Of Company Ku A u A i ^ /)l>u--i Report To: ^.ic:..: ^-^•Mi £ i ^ lU iN, Client Informalion (Check quote/contract): 517698 To Be Completed by Pace Analytical and Client S G C t i O H C Quote Reference: i ^ ^ -T'VN/i •••':f-vr/^jr-c^f-|^ "'i'h/.UD. '3<:f^(^ /"V,>T(rnr ("gCTigg) Requested Due Date: 'TAT: Project Manager: 1 i.,)r^L^-i-N. K PO. ^_L. _LV Project Name; . ,iv Vlfcfiir^i | 6 L * S N D C'jitM. >ri£. " Turn around times less than 14 days subject to laboratory and contractual obligations and may result in a Rush Turnaround Surcharge. Turn Around Time (TAT) in calendar days. Project *»: Profile #: Temp in °C: Received on ICE: Sealed Cooler: Samples Intact: Y / N Y / N Y / N ^ A . p ^ - A i h - ' Mc'- 'r*j>-i>rti_ c7fc/^.-^fs , i-Yi-l/llnT ' ^V .!> p-'/Oft Ti'OO f-f-C^i.o/ ^ y pf> p^C fe-/.0/) sy^'^ LO O Ln o 00 LO Additional Comments: SAtiflPLER NAME AND SIGNATURE PRINT Name of SAMPLER: N'0t..MH / , . GcHL [fl SIGNATURE of SAMPLEp; c- t'>TVA.^."'y SEE REVERSE SIDE FOR INSTRUCTIONS IGNATUF CTiSr y. <3L3J3^—- DATE Signed: (MM/DD/YY) 5' 7. oo —jg Pace Analytical Services, Inc. Form COC01.XLS;i2/99 A na lytic a I The Right Chemistiy, The Right Solution'^ Required Client Information: SeCtlon A CHAIN-OFrCUSTODY/Analytical Request Document The Chaln-of-Custody is a LECSAL DOCUMENT. All relevant fields must becompleted accurately. Additional Comments 53c Toiyi CcmfcwTb '.Aceic^^ ^ flr^kj^me chktU ^ c.ll^io4c(/n ' A / C o o ( r \ 3 / 3 3 h ' p ^ m e P / SEE REVERSE SIDE FOR INSTR SAMPLER NAME AND SIGNATURE PHIMjT Name ol SAMPLER: i , DATE Signed: (MM / DD / YY) / 3/io/ao 'ace Analytical Services, Inc. Form COC01 .XLS 12/99 I % Pace'Analytical The Right Chemistry, The Right Solution®'" CHAIN-pF-GUSTOpY7^AnalytiGal Request Document The Chain-of-Custody is a LEdAL DCicuMENf/Aliivleyantflelds must t>e completed accurately. • Reqiili^d Clierit Information: Section A Company .:-' A,A^ Required Client Information: Section B Page: / o f / 517700 To Be Completed by Pace Analytioal and Client S e C t i o n C (fn Address ' ' l3iJrrl> /M,d Report To: Afcr/wA j^,^A7, 2A_ Client.Information (Check quote/contract): Quote Reference: ./ r(Tg/?encffK n /3kcl j ^ a-7(^.'39 Q o ^ Arucloi - BiHrC Requested Due Date; ^ k ^ TAT: Project Manager: JAii liiiEL. Phone / Fax / <70pi/O77- W l \96^/€V7-m^ Project Name: > # t I ProjecHVIumber;. * Turn around tirnes (ess than 14 days subject to laboratory and contractual obtigations and may result in a Rush Turnaround Surcharge. Tum Around Time (TAT) in calendar days. Project #: Requested Analysis; Section D Required Client Information: S A M P L E n D One character per Box. (A-Z, 0-9 /.-) Sample IDs MUST BE UNIQUE Valid Matrix Codes * MATRIX WATER ;• SOIL OIL WIPE AIB TISSUE OTHER CODE WT SL OL WP AR TS OT UJ o o mm / dd / yy , 5 UJ f=d O O titi:mm a/p Preservatives Remarks / Lab ID .ft if 3" WT ^ AJ m ^r u j f ?kk )fe/^T Hi {oT /I3t 'X^ 0 fel ""^pui M/' iW y m ^A u hrr 3]i) Oo <^:Si m it 4 ^ V ?«,,« fM h- tUT f;od i il !H« urr 1030 m ST, 41 k j f tl(}0 % ^ 3 m ^4 H/T IIOO **/* AT ur I D l ^ M 7S f t L2tt 1 J * . «/r >i/ 1^30 1 & &_ ^7- R e l i n q u i s h e d B y / C o m p a n y m m- P^oyWenTc/ ///^7vrv-y/^,/^ IS ^Vff / ^ ^ / t > / B S B 03 .7^^/** Date T i m e ^ /T-ad w o Ln o 00 Ln Additional Comments: 3>/Pc 7'of'^^lO^^f'^^^O^ A ac<iiQiie ] /^e7K^/:p/te .!-fii>ri7f e ^ 7 y 7 t e A 7 , » , e j 7016 7xy/<P/i<?^ SAMPLER NAME AND SIGNATURE PRlflT Name ol SAMPLER: . SEE REVERSE SIDE FOR INSTRU SIGNlWJRE ol SAMPI 3/AJ ^ ICA-lk/p DATE Signed: (MM / DD / YY) 'V DATE Sianed: m i I '3/3//d6 Pace Analytical Services, Inc. Form COC01.XLS 12/99 « Pace'AnalytJGal The-Right Chemistry, The Right Solution® Required Client Information: S e C t i o n A Required Client Information: S e C t l O H B CHAIN-OF-CUSTODY/Analytleal Request Document The Chaln-of-Custody Is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Page: of 517766 To Be Completed by Pace Analytical and Client S C C t J O n C Company Address / ' . ' . / }|.^A^ . - i - , \ r : i n . ^ f : A l A i : : . . (0,^::-;W.i ^J•'-^ A ' 7 t ^ f ^ S Phone 7.:f,ii.,>-i''!- Jr?in 4t S UJ 1 2 3 4 5 6 7 8 9 10 11 12 Fax . U)Ac.-n-7nA2. Report To: f4... ».i|-i ; - | f H I + 1 ^'•'i/hl • nvoice To: .. .J ' * RO.." "" ' ' 1 •"• Project Name: ^^ . ,. . Project hJtjmber: - ' S e c t i o n D Required Client Information: S A M P L E ID One character per box. (A-Z, 0-9 / . - ) Sample IDs MUST BE UNIQUE J -'i M Tl 3 W 4 Sv, " ? A ! n 1 ^ K ^1/ 54;?* ^ 37 i ^ I V (3 M^ !< ' i ' T- jr f3 i t '•*. .^ l4fj »% t-cf ( i^ r,'- -4 4 ^ '3 r. i" «t ^^^ 1 ir- 3)^ '. f i3. K s -/ ? 4^ Til v ? (=^ -1 •f- A J » ' 'K, V ^ % ^ A # ^ << "'.If ttl( ^> Valid Matrix Codes A MATRIX CODE WATER WT SOIL SL OIL OL WIPE . WP AIR AR TISSUE TS OTHER OT r. 1*. y ^ ^3 .1^ "^ X ii' h k r» t A '^^ ^ Pi fp V 3^ "ft. ^:/ ^ /- f> ?t •?' * « J * I4 UJ Q O O X DC !; 5 w w W Client Infonnation (Check quote/contract): Requested Due Date; • *TAT- • Tum, around times less than 14 days subject to : laboratory and contractual obligations and may result in a , Rush Turnaround Surcharge. Tum Around Time (TAT) in calendar days. 3 DATE a COLLECTED 3 \i • (X. ' I - A ' ( A , 'AU-.-<yA a t (. hti:mm a/p ' •-A.) A,-. :. hAi-A... t 11". b •• >r-. . i- Preservatives ? 1 2 Ui. : Q} I & i ' X O z X o I 1 7 / ; Sample Condition | Sample Notes Item No. 1 Relinquished By / Company |D< Temp in °C: Received on ICE: Sealed Cooler: Samples Intact: Y / N Y / N Y / N -.M,..,:-:'u^*;J-.iu™' M(i4 1 A I X o ra z d (0 z Quote Reference: Project Manager: Project •: Profile #: Requested Analysis: O f / • / / / / / / / / '•y P / P P P P P P P Remarks / Lab ID y / / 3te Tim( W c i } ^ g M ^1 ttrt 1 ^ m .f3h ^ rk%j 3 A ) ^ ¥f r •« '#i 1^ ^4 ^ , 5 5 4^3 m ^^? l l ^ , 3, M a >«'i # Cf s p * % ft > Xf i if t i . s ^ fl 3R f f r - 3 i % ^i w A: > : i(? ^3^ ^ ' 4^ ?. 1 , ^Jl C^i-nl^a, ,f,'c..iiO., 1 1.'^ I fK>yUj«Ot.'^,,,i:_>i.- X f l".rsi_' Date Time w o Ln o 00 Additional Comments: SAMPLER NAME AND SIGNATURE PRINT Name of SAMPLER: . SIGNATURE ol SAMPLER: SEE REVERSE SIDE FOR INSTRUCTI A.k,r.,-.^AA: - ^ J A U L ;TI6NS DATE Signed: (MM/DD/YY) Pace Analytical Services, Inc. Form COC01.XLS 12/99 « Pac^TXnalytical The Ri^ht Chemistry, The Right Solution® - ^ Required Client Information: S e C t i O n A Required Client Information: SeCtiOM B CHAIN-OFrCUSTODY/Analytical Request Document The Chaln-of-Custddy Is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Page: ± o f ^ 517528 To Be Completed by Pace Analytical and Client S e C t l O n C Company ..•, ; / ; Address ' _ .. A t u ( a v \ 3 3 n1c7=;'^ Phone. s UJ 1 2 3 4 5 6 7 8 9 10 11 12 AiJAu3l-llhQ Report To: Invoice To: ^^{iJfV.'Vd- C i c U l / i Aare\or('fr:^lk-e\ P.O. " - ^» - - . ^^ Project Name:. ProjecvA) umber: . S e c t i o n D Required Client Information: S A M P L E I D One character per box. (A-Z, 0-9 /.-) Sample IDs MUST BE UNIQUE w w w w w w w 3 Iv' 'A y w T£ d CA t t t t t A (}_^ L B t l R T /! h h P\ fi / /I A l\ r f- 3 5 S S S s s S' s V - ^ l ' ?7 smp in °C: { T T f r r r r r r P Received on ICE: Sealed Cooler: Samples Intact: A B c p & / ^ $ H X ; ! ' 5' 33 / - ; ^n .*^.- / > Y / N ,Y / N Y / N ET^ 1 • ^ •if f -< ^ i 1 f> 'L. ' ^ ^ *f -% 3^ ^ ^ U - I , 2 ^ ^ »j '< ft ... -^ 3, yfi Valid Matrix Codes <—~—:.-.._ MATRIX CODE WATER WT SOIL SL OIL OL WIPE WP AIR AR TISSUE TS OTHER OT ? ,* i . -t >? * u' H *' A^^ ^ !'f H H2; h ^ 1^ I# s i I V I •4, rp 6 ' » 1 .. 1^ \ X sl t i l l LU Q 8 X i 5 A\ 3 (.. -•L L >L - L >L SL Client Information (Check quote/contrac Requested Due Date: t): 'TAT: " Turn around times less than.14 days subject to laboratory and contractual obNgatiphs and may result in a Rush Tumaround Surcharge. \ + Turn Around Time (TAT) in calendar days. i DATE a COLLECTED O^/ypx ^/yloo ^iho/oi) 3:-Apa 1 <i 3.3.. .As J ^l]oho • ' . I I I '1 lA '\IVJhiO O •( " I hti:mm a/p ' li '^0 il l 3 w i o H ^ V i l ' ^ l !!>i \A3S WSH \ AiO^ 120"] Moo mo Preservatives \ I 5 S t 3 X IX >x ^y ix h J , V K * ^ « K a O CO, 3? o" z r . — o I Iff o ra z 17!^ c? ... m —f—it^ Quote Reference: Project Manager • Project«: Profile*: Requested Analysis: • / / / / / / / / / / / / / / / / / / / / Remarks / Lab ID X ^ f ")(-. r ' $ ^% 'f ni .t' %^ % ' 1 7-' 3 . 5 1'* ' i. . 1\ H fo 0- M i * n •;• ^^ 'S 14 3it ! | ' ^ i n fcpeeAL £xf- V *l f !!j;' j f ^ C; r.^ ^ fS U <f 3 i f '-,! >> ^ ' f 1 ^ • ! • R£S3 Additional Comments: SAMPLER NAME AND SIGNATURE PRINT Name ol SAMPLER: OJ O U l O 00 SIGNATURE of SAMPLER: DATE Signed: SEE REVERSE SIDE FOR INSTRUCTIONS [MM I DD / pSo/o YY) OO Pace Analytical Services, Inc. Form COC01 .XLS 12/99 % Pace'Analytical The Right Chemistry, The Right Solution® CHAIN-OF-CUSTODY /Analytical Request Document The Chain-of-Custody Is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Required Ciier^t Information: S O C t l o n A Required Client Information: S e c t i O f l B . Company . • , : K : • i...--:<rA A / A r , . s - A Address •' , . A 3 /.-.-A.'.-.A.-3cA.,c ' 3 s J \ 3 ' A ' <• AA;\ 3 3 A 7 0 S H Phone ''''A<i 1 i A i l '%iLL At S UJ t Fax A A ^ ) T i l l >;M2 Report To: /". . | : Invoice To: \ / \ P.O. ' J ^ / Project Name: ^ T i •; --^ PrbjecUfiurnber: ' S e c t i o n D Required CHent information: S A M P L E I D One ctiaracter per box. (A-Z, 0-9 /.-) Sample IDs MUST BE UNIQUE ! ^J. w i ^, • i , W w VI w AL' iSi \ a (I tl, c c v.- e. e e. <h f- ^ - c /-' F r r D m rvi ^ v'.» 9 P p. P P P e W w w w '$" t p p p p c / 1 V \ • ^ D £ F Cr H £)• -? ,5 5- 5 /f /v /4 f3 0 p j ' ^ . t '' s-' • A J - ' , '/, i l w f ' . ' > 1 - i , ", . .- ^ * .^ '"7 '; Y r> / . t-' ; : ,v £. " \ ^ 1 . ^ > .-- r - v ' ' f •r? Valid Matrix Codes < __ MATRIX CODE WATER WT SOIL SL .OIL • OL WIPE WP AIR AR TISSUE TS OTHER OT -«- ,'' " .' ! . \ ) "•'.r j " " • " W W '' 1 ' '•\ * C. J »v /\ T'^i i '^:^' ^ » ^r^ Z '• ? 1 '.'- A ^A .. y.1. "~«». Ul 8 o X i 5 1 ^>L •:>L -•u- 31- 3 - ^ -^L i s t ^ Page: Q of ^ Client Information (Check quote/contractj: Requested Due Date: C t - 7 C O Q •TAT: ' ' Turr^ around times less than 14 days subject to laboratory and contractual obligations and may result in a Rush Tumaround Surcharge. Tum Around Time (TAT) in calendar days. 3 3 DATE a COLLECTED *< -< H / l 3 t 7 A <i A A A A7o m''.3r,0 ipPJoo ^•piOlOO ' 1 ' / '••; A l A i A ^ H/>a//;?/:) w ^ Q LU O 'i U 1 t hh: mm a/p ; "i lHh' H A l 1 /•7.37 r?3'^ nw 11 i s Preservatives l l .^' V 1 y 0^ ! ^ '/ nr^i^ i«/7oS !*ft!3S i^.)C5 /;<'^(:3 -~~..,iim^^ y U . k."" iL^ ft Jt.WP w " 0 I */, .\ 0" 2 -P To Be Completed by Pace Analytical and Client S e C t i o n C • . .' Quote Relerence: / / / . Project Manager: Proisct tt-. Profile #: Requested Analyslfi: / / / / / / / / / / p y / / / / / / / / Remarks / Lab ID ' W ^ 3. •^. ;# y- ')^ f ^ ic^ ff 'A^!A^: y y > V - * "' 1 -'•f t*. 1- i 3 - * '!•* •it ^n, ^ •' '4^; -^ ^-^ s^ fV A ^ \» t;; * * ? ^ ' A "i A. f i 1-^ ik A'^"' J . . ^ »6 1 • ^ 4 T^ ' It . • ; ' ' 3 7.: f3 r i 1: • - * *• ' p» Sample Condition i Sample Notes . Item Np. 1 Relinquished By / Company JDate (Time 1 Accepted By / Company {Date Temp in °C: Received on ICE: Sealed Cooler: Samples Intact: Y / N Y / N Y / N • S? 3 A 1 ^ A / 3 ' t i ^ - i y ' fM-U/k fC:'k:.AJf---rA'7 W Pf,i>f^/5L t M m i ' > Time Additional Comments: SAMPLER.NAME-AND SIGNATURE. PRINT Name of SAtiUPLER: OJ o cn o 00 00 SIGNATURE 0) SAMPLEFj <3~r-'37- SEE REVERSE SIDE FOR INSTRUCTIONfS DATE Signed: (MM/DD/YY) Pace Analytical Services, Inc. FofrnCOC01.XLS 12/99. SJ Ks Pace analytical The Right Chemistry, The Right Solution'^ CHAIN-OF-CUSTODY/Analytical Request Dcfc^^ The Chain-of-Custody is a LEGAL DOCUMENT. All relevant fields must t)e completed accurately. Required Client Information: Section A Required Client Information; Section B Page: J_ of rj^ Company McJAre^/HaH- Report To: Klorm^ £'>cU{ i'>^ 517530 To Be Completed by Pace Analytical and Client S e C t i o n C Client Information (Check quote/contract) 2'^: j:-nHgp«>n4enCg.-•&iv4 f ivoice To: / - Requested Due Date: ^hone Fax , Project Name: |VAr^;.x 'XS\aYN4 rv^^r^iifal C.-ff 3je<^j>j! * Tum around times less than 14 days subject to laboratory and contractual obligations and may result in a Rush TumaroundSurcharge. Tum Around Time {TAT) in calendar days. Proje<^Vj umber:. Section D Required client information: S A M P L E I D One character per box. (A-Z, 0-9 /.-) Sample IDs MUST BE UNIQUE Valid Matrix Codes •«- MATHIX WATER SOIL OIL WIPE AIR • TISSUE OTHER CODE WT SL OL WP AR TS OT D UJ <:' Q • o o mm I 661 yy ''il vi-r 5/l/ 60 WT ?/(IcQ v ^ ^ / l / < 3 0 ^% nr 5P/D0 • > * • w\ #.f m fi * ,4.' Item No. Relinquished By / Company # ^ tjJ O cn o 00 Additional Comments: / ^ I » ToUAei-^e, E+v.jl^><?'>""^c«^/^f<^^ Xjlf-«e.5 SAMPLER NAME AND SIGNATURE PRINT Name ol SAMPLER: ^ T f A H A A r ; ! ; . ClIOtA) SlGt^ATUREplSAIvflPLEB:.. ; . • • • • : : , / /.-.^/.A DATE Signed: (MM / pD / YY) SEE REVERSE SIDE FOR INSTRUCTIONS '•) .P//on Pace Analytical Services, Inc. Form COC01.XLS 12/99 f, Pace'Analytical The Right Chemistry, The Right Solution® Required Client Information: SeCtion A CHAIN-OF-CUSTODY/ Analytical Requestl>v^^ The Chaln-of-Custody Is a LEGAL DOCUMENT. All relevant fields must be completed accuratelyA Required Client Information: Section B Company YV\rUren I H c r t Report To: Moirn^a £:ichim T Page: 3 . o^ 517527 To Be Cornpleted by Pace Analytical and Client S e C t l o n C QuoVa RelaT&nce-. Client Infomialion (Ctieck quote/contract): 25 l-hdco^ndAnCe h f . Requested Due Date: Project Manager: \N,irfe^) iMT ^ 1 0 ^ ^ one ,^ . rax> _ * ^ Project Name: . • : Djeot-Ni • Turn around.times less than 14 days subject to laboratory and contractual obtigations and may result in a Rush Turnaround.Surcharge, Tum Around Time (TAT) in calendar days. Project #: Projeot-Number: Requested Analysis S e c t i o n D R e q u i r e d Cllent information: S A M P L E I D One character per box. (A-Z, 0-9 / . - ) Sample IDs MUST BE UNIQUE o UJ ad o o mm 1661 yy 5 UJ O o hh:mm a/p Preservatives m Remarks / Lab ID WT HMl0i> on^cL y ^ 9 " t^/i^/oo \H10 p x -7f' %i WT H / I % / D O osoo*- 1 )( M i, * vn*^/WQo I k l O % V l i t . i-vl ^T^/30/61> |fc3o 4?' Zf- WT V t / g o ^ 0 8 €< t, 1 • ^ * ^ f/T f Z L ^ olM.^ ^a#' ,%!• %£ W l g/l/<30 lii££. .^ C J i MifAm. Mil :?< l / r ' • ^ i l ' t %:x ^ i% ?.< A'i- Item No. Relinquished By / Company *M> Time Accepted By / Company Date Time CO O U l o vo o Additional Comments: » v- • , A I i ; tract Covv.Dunds: ftcrt^v. ^'Wlly^^/K: CM^r.^le , Chbr^fBrwi, Sr-^ Tot -Toivtev^e/Ffhylbeiaen'^^ -tef^l Xy'f''>e5 SAMPLER NAME AND SIGNATURE PRINT Name ot SAMPLER: • . / . . 3-" '-'Ai C.-''^V- " > 1";vi/ ! f SIGNATURE of SAMPLER:. . 1. DATE Signed: (MM/DD/YY). ] - / • V SEE REVERSE SIDE FOR INSTRUCTIONS Pace Analytical Services, Inc. Form COC01 .XLS 12/99 « nalytical The Right Chemistry, The Right Solution'^ Required Client Informalion: Sectlon A . Required Client Information: CHAIN-OF-CUSTODY/Anaiytical Request Document The Chain-of-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Additional Comments: SEE REVERSE SIDE FOR INSTRUCTIcJiNS Pace Analytical Services, Inc. Form COGOI .XLS 12/99 « Pace'Analytical The Right Chemistry, The Right Solution® Required Client Information: S e C t l O n A Required Client Information: CHAIN-OF-CUSTODY/Analytical Request Pocumet;: The Chain-of-Custody Is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section B Page: of 517902 To Be Completed by Pace Analytical and Client S O C t l o n C Company -Mi ddresE •.ui / M r ^ e T Report To: kXUt Client.Information (Check quote/contract) Quote Reference: ^ iN&Pif^itXf-K'^ f ) t . \ i r i , it*_ r,r.\ Nio' C3r()&=) Invoice To; Requea^d Due Dete: TAT. •0 PTol©t\ Manager-. Project Name; Phone l(±kiVlA,\U I C<k ^rq|i 'iC-hlCAl' f'iC>2- N&T Project Numtwr: !£,<alti \3iLfitiQ Ll-fcM (L. ."Siif. • Turn around times less than 14 days subject to tatwratory and contractual obligations and may result in e Rush Turnaround Surcharge. Tum Around Time (TAT) In calendar days. Profile ft: Requested Analysis: S e c t i o n D Required Client Information: S A M P L E I D One character per box. (A-Z, 0-9 /.-) Sample IDs MUST BE UNIQUE Valid Matny ..Codes •• MATRIX: WATER ' SOIL OIL WIPE AIR TISSUE OTHER COUE WT SL OL WP AR TS OT Q LU o o mm 1661 yy S LU O o tihimm a/p Preservatives Project It: Remarks / Lab ID Q. WT 3 iXcA- IO:CK-..X 7 W Wr iJSu:^ iO-HOr. / P. rla -k:^ >uf),|t t.crii\:..0 *.-, M WT S • 13- ^y i^.tS^ ^ y / g^ / m hS i.j MAA^ C':iC\Arvi_, 7i D fl w WT •i3-D0 12-15. / % •ifA, If. ntCtV>.|U.-\,«, i.3\S' <m,<iti 2i ID \ ft% ' f . » ^ ^•tS-At'l Z:25 y iia. u:t) 1^ }l:i«.n SM.<.«_ 4- * . . ? * 3 3< ^ WT 5-l^-On-):^^-.^ 1 i t t{^'-^3 /sU.>u^ ^ .Oj% f/v/T 3-l'iftc. r>".Z(''ifv. 2 y ^ . ill «!/ !,<*' **,« ,%** WT?-.-|^..n'i >l-2.&c^ y - ^ ^sf ^i^M. .iJlchlgiCT^j.-) ' t l >jVi L.A 4" 5^. 1^ 1 l^ H 9 tA e f ' ^ k l "i.!? \m OK ^ ^ I f #'? Item No. Relinquished By/Company I ;:ii.vfji:VJ..,- M.j'•''•• <'>i/t|i'^'r :s^tea- ' t o : , Pfrtf.t.Ru"^vPf-'/^.s IS i#4 llffi Date Time im^ti. iLm. o Ln o vo Y / N hiitfvA(,C.)ay?v6<^ MSnii ISOo Y / N Y / N Additional Comments: '^:>aelnc:^T (JcMfti^JO^: oc.d>'tvi^ va-Tsa:^w|Ui^, ^ 3 : \ c u ^ ^ eKlci<^^v»rv, ..V V . . i . t . l \ . . . t i l . ,:. 1 SAMPLER NAME AND SIGNATURE PRINT Name ol SAMPLER: * ' J ' SEE REVERSE SIDE FOR INSTRUCTIONS SIGNATURE Ol SA(i/IPL^B: 7: ^^'IW.- DATE Signed: (MI^/DD/YY) 3-iM-rn Pace Analytical Services, Inc. Form COC01.XLS 12/99 7^f4ce Analytical • L . CHAIN-OF-CUSTODY / Analytical Request Document The Chain-of-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. 529258 Required Client Information: Section A Required Client Information: Section B Page: J . of ^ To Be Completed by Pace Analytical and Client S e C t i O D C Company U'f r p i.\ / f ( !,. Report To; 'A^'- t.(M. Quote Reference: Client Information (Check quote/contract): M M I L . 3 Requested.Due Date: Project Manager: [3:,frA^^. 0 ' 3 A'-y}:A3 Project Name: • Turn around times less than 14 days subject to tat»ratory and contractual obligations and may result in a Rush Turnaround Surcharge. ^ Turn Around Time (TAT) in calendar days. Project #: Profile tt: Temp in °C: Received on ICE: Sealed Cooler: Samples Intact: Y / N Y / N Y / N -v.,->U.. . ' v , - , . -n}AA.....A.,r- 7-1-p •t ' 'if/oo ! 1 Additional Comments: 0 'ivK.^.j,--\A5 '• 33iA%7'--- AvAAA^i U^^..i iA-\iof 3 ^ AWuAjf SEE REVERSE SIDE FOR INSTRUCTIONS SAMPLER NAME AND SIGNATURE PRINT Name ol SAMPLER: SIGNATlIRE of SAI^PLER: 7 ^ o Ln o LO LO M Pace Analytical Services, Im DATE Signed: (MM / Dp / YY) t. Fori orm COC01 02/00 5i Pace* Analytical The Right Chemistry, The Right Solution'^ CHAIN-OF-CUSTODY7 Analytical Request Document The Chaln-of-Custody Is a LEC^AL DOCUMENT. All relevant fields must be completed accurately. Required Client Information: Section A Required Client Information: Section B Page: ^ of 517767 To Be Completed by Pace Analytical and Client S e C t i o n C Company c J c\^Ar,•^....,^ i/c'j,, -f Addreis ._ ' A ' ^ '> :-., / jv - O N A , A 7 . - A A . t 3 - . i . t A i ^ A 3 \ :.-'\ \-..7,:, t -A..\ 3 ) 3 r ) 7 i ) K : i • Phone 3 ^ 3 7 7 / 7 ^ / / / 1 2 3 4 5 6 7 8 9 10 11 12 Fax 7r)i'M7?i:/A7 RepOrt^o: . / I : { • n v o i c e T o : . <•' '•-•-- - • - . . - V '- -..^ ... ^.i / . ..... r ^ \ A.'iC- As i t r c i -{.>-{ 1 rirA-V... \ RO." . ' V ^ ^ . 7 Project Name;... . p. ^ , i U., c^,./^ VAf^. .3{'YV'a. .r4\At Project Number:. S e c t i o n D Required Client Information: S A M P L E I D One character per box. (A-Z, 0-9 / . - ) Sample IDs MUST BE UNIQUE F pi D 3 Ui (J (J OJ OJ * v^ U> (3 B J a c° c c J.V 0 -^ P (> f f f K K \ S': Q V "C f- p: T Pi UJ u) ! C> 1 o 9 P P 1 1 4 a ^ 3h A ^ ^ ^ 5 5 > " i t% ) / ,o F) e> C. M to o V. r(7 Cf i f ^ f^ fl (^ ft r r J , ¥ ^ ! # i t 3 If 1^ i^ ^J 1 A ^Y'- f3 ¥ l t % K i f «?1 V 51' « f . & M 5H %' v" t- . ^ 3' Valid Matrix Codes .« • — MATRIX CODE WATER WT SOIL SL OIL OL WIPE . WP AIR AR TISSUE TS OTHER OT V *-. •> ^ f^ 3. % ,^] Pi t * • * * t- " • ^ 14. 7^ -.! .? ^.\--^ / / 'i 5 •r "• il 3 .. 4 .11 s LU Q 8 tL It^' uT l^/ urr L J T W T tor UJT • A Client Information (Ctieck quote/contrac Requested.Due Date: .••.''.-.' • ^: 'TAT:\ • Tum, around times less than 14 days subject to laboratory and contractual obligations and may result in a , Ftus •J Tun h Turnaround Surcharge. Around Time (TAT) in calendar days. Q < ^ a d O . o mm / dd / yy '3/Joo H^l^l(h, ' / ' 1 ( 3 / ^ • ' ^ j l i i l 4lC:V t > r 6 A - Q 0 > f , Q 2 til ! Pd I O c c c tih:mm a/p ' r •/t^^C ' L 1 I I 1 0 .^ ll 13) 2 J i i ^ : l2o7 : 1^00 : Preservatives 5 S rl \ i h^ 5 i i i i i d I i O Y • < Y N- X X K X X Sample Condition 1 Sample Notes Item No. 1 Relinquished By / Company I D . Temp in °C: Received on ICE: Sealed Cooler: Samples Intact: Y / N Y / N Y / N '•; ;-.";ij r.i ,:- , .>' : \.:, . . f -l.'i AAf.';!, A-fi ,' z 3te v./: Quote Relerence; Project Manager: Project*: Profile It: Requested Analysis: / s / / / / / / / / / PcA/' y P P P P P P P Remarks / Lab ID Timi >f^ If ^K t % ^ ^ M 7 ^ f ~i *, 1 J Y't *4 «! 4i A^ Jl.. " • f t cfSBB] '^l^ t s V t^l 1 ^ 3 %^ s ^ ,^4 i4 • • 1 T f i K to 4v 4 % | t i S^ 'M'w' ^*! ' ^ i ^^ »1^ 4- .%^ S' 1», ^r any p a t e Time /^„i5i^f •.',-;,/' •^•'i-v;>fv^^C? 7 v / ^ Additional Comments: =U: ^•x,e> SAMPLER NAME AND SIGNATURE PRINT Name ol SAMPLER; ^r,A'A-^i^Af:7 r/>//)/. SIGNATURE of SAMPtER; .... ,"-, A'..-SLi> to O Ul O SEE REVERSE SIDE FOR INSTRUCTIONS 33i^ DATE Signed; ^(MM/DD/YY) \/OpO0 Pace Analytical Services, (nc. ' Form COC01:XLS 12/99 r - ; " •^'^ MICROSEEPS, Inc. 220 WiUiam Pitt WaV, Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 Company Name: Mc.U"lCy./4 /l-JAi,-r Prqj. Manager: NJ.yMA F'lf i-u..tN h't..^7 3f-^^\ft(rr i'(:i3TtL) Proj. Location: \j(v.^ii4 K>A^if< ("\.lfiU . "St-T^: Proj. Number: CHAIN-OF-CUSTODY RECORD Note: Enter proper letten in Requeued AmUyiet cohimni below. A n a l y s i s O p t i o n s Note: if anslyni D,E,or K u lelected, Kt^tch (opiioa) NOTT wtnled. Phone tt: -1 -JOBiC pA'l^H 3\ F«#: qnf^ fe/,!7- Ai(;2^ iiii i i « ill Mi: m C1-C4 Hydrogen & Helium Pennanent Gases (CH4, co, co2, N2.02 ) Mercury (SoU) or (Air •• > TO-14 by GC/MS (Ambieia ) or ( Source •• ) £01 & 602 Compounds o K Chlorinated HC BTEX BTEX & C5 - CIO T M (C5-C10)or(C4-C12) L CU - CI8 Otber Specify below. Sampler's signature : A- i i/iW.. at- • ; J . uu. * An additional 22 ml vial of sample ia required when requested in combination with another analysis. ** Available upon request. .') vor.. li-<ilC£.7' K^i.%\\'f;yt-iO'-'•'• caht\«... (^77 L VI S«llipi» in lV^Ult«>«l W11«U &««jUBDl«W 111 bUlllUllKIUUll WIUI BIHJ ^PTJ t.'tva_ ' h|r-|< ci-jii. C ^V•^37vy'\ i tW. Collection Date Time Number of Containen 'Summa* # if Can. used Sample Type Sample Identification Requested Analyse <Otb«r^ Remarks v l ' j . « . j /C^'7 3cu-4ias A6T-:->Vif^-1 trVi-:.^ StTe:"lHi!,^T {\, ^Jt^^•^^^r^J|-><> K'.ii' fK^r-V;MP-VT r>fe^ IC2JO A ^ T - U N P - rf) P.fej: •P-iJO Ed ASP V^<P-2b Kri-;v 15-1^-1 \Y'A'^kXv-AAX H A V Ifiikii f\-vr- \jrafi Z'D irW-,^.. rt--jr- vird^>--^--, hiyv:. )C<y. A^rr \j^.^P- :-H'r nH-.f .405 i\^x.\^tM''AA>Y^^.t IC,o-9 nf)-VMP--^-!"-) hi-iv ['"^Lri^ ^)^H^T-\l^4t^^•^'-i•L <-/t^>> L /i''.T- \j(a('- d-ih 3AA:. iiiiiiinMiiiMiiiiiiiiiiitiiiiiiiMiiiiiiiiiiiiiitiiiiniiiiiiiiiiiiiiiniiniiiitMiiiiiuiniiiiiiiiMiiitiiiiiiiiiiniiiiiiiiiiuiiiiiMiiiiiiiiiiiMiiniiMniiiiiiiiiiiiMiiinMiMiiiiiiiiiiiiiiiiiiinii^ Resulu to : lllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllll Relinquished by : 1 • • ; * i Relinquished by : Relinquished by : iL.''it:.i.'>J7 \\i\A\ lllllllllllllllllllllllllllllllllllllllllllllllllllll Company : Company: ' Company : llllllllllllllllllllllllllllll Date : Date : Date : llllllllllllllllllllllllllllll Time : )'70O Time: Time : Invoice to : 3:^:AA f U : „ . c L c r , i^XTScL liiiiiiiiiNiiNi iiiiiiiiiiiiiiiii mil iiiiiiiiiiiiiiiiiiiii Received by : Received by : Received by : iiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiniiiiiiiiiiiiiiiiiii Company : Company : Company : 1 iiiiiiiiiiiiiiiiiiiiiiiiiiiii Date: Date: Date : llllllllllllllllllllllllllllllll Time : Time : Time: O cn o vo cn WHITE COPY : Laboratory to return. YELLOW COPY : Uboratorv PINK COPY : Subminer m MICROSEEPS, Inc. 220 William Pitt Way, Pittsburgh, PA 15238 Phone: (412)826-5245 Fax: (412)826-3433 1 \'^^t. z.^pp2^ C H A I N - O F - C U S T O D Y R E C O R D •i\c i.'^^^^-^f'ill-ifir:;! Analysis Options Note: EoUr proper letters in Requeued Analyse* cohinmi below. Note: If analysis D,E,or K is selected, scratch (opiioa) N O T waited. Company Name: Address: '•)A^, U(s^,y.Kh>/vJCr hlllf^ i^W.l^^lsl^ K!3" 0 ^ ^ 6 5 9 Proj. Manager: ^ M H \3C \K\ \\A jVSl. H^^f I f f (f^AiSd) Proj. Location: VJiy-Cihl I-Sj AM f)^ ( S^PMU'f^l " P H S Proj. Number: Phone tt:-'^C:fi,fcM"/-Vit li Fax tt : ^ n h | ( ; ^ n - H l A Z . iilil mm Iiii 9m iil iiii*j;i;i: C 1 - C 4 Hydrogen & Helium ' Permanent Gases (CH4. CO. co2. N2,02 ) Mercury (SoU)«(Air • • ) TO-14 by GC/MS ( Ambient) or (Source • • ) £01 & 602 Compounds i»l Iiii iipi mm |::;|il!j|sS: iiii^ Chlorinated HC BTEX BTEX & C5- CIO T P H (C5-C10)or(C4-C12) C l l - C18 Specify below. Sampler's signature : Collection Date Tmie 3-HrX-, iG3() •"1. 'cvri'v. Coolainen 2 . llllllllllllllllllllllllllllllllNllllllilillllll 3 s 3 • S u m m a ' 0 if Can. uoed llllllllllllllllllllllllllll .3. - 'An A3 Sample Type AK^L.Q-\i> 7\e.4,f:T C.tw>^(\\t4DS:<-K Sample Identiflcation A6T-6vt-iO \^'v\Af iiiiiilllllllliimill II iiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiii iiiiiiiiiii Reiulu to : 4.;.i;.-Mi\ £l.-1.11 UN, 5\iQ^ij\t(iA 1KAcT llllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllll Relinquished by.: Relinquished by : Relinquished by : llllllllllll Illlllllllllllllllllllllllllllll Company : Company : ' Company : IIIIIIIIIIIIIIIIIIIIIIIIIIIII Date : •5-uA.oo Date : Date : llllllllllllllllllllllllllllll Time : T i m e : Time : •• Available upon request. \\\< h ^ l ' - "-'.n K-ir-/-.("i Y> 1 liillilillH^^ iiiiiiiiiiiiii .;?*" IIIIIIIIIIIIII IIIIIIIIIIIIII IIIIIIIIIIIIII Vlllllllllllll 3 \ A \ t \ t f ^ - T Q Remarks >»J\ffctsh(DS 'iiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiii iiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiii 1 iiiiiiiiii Invoice to : iiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiifiiiifiiiiiiiiiiiiiiiiiiiiniiiiiiii Received by : Received by : Received by : llllllll IIIIIIIIII llllllllllllllllllllllllllll! Company : C o n ^ a n y : Company : lillllllllllllllllllll 1 D a t e : D a t e : Date : III IIIIIIIIII IIII Time : Time : Time : o cn o vo W H I T P r n P Y • I j>hnr«tnru tn r^tiim VPT t n w m w . r .k« ntxjv /...-vnv . €>..! !— — MICROSEEPS, Inc. 220 William Pitt Way, Pittsburgh, PA 15238 Phone: (412)826-5245 Fax: (412)826-3433 , CHAIN-OF-CUSTODY RECORD V Note: Enter proper letten in Requested Analyses cotunma below. A n a l y s i s O p t i o n s Note: if analyns D,E,orKis selected, scratch (op&n) NOT waited. Company Name: Uc-j r,i,(.A jUtAx Address: 2 3 \,.M'^cc..rMY.^M3\^v ^r>^ />V;^g.^:/sl^ M T ' CYlA^l ,^ Prqj. Manager: fA^uM-i fir HI it-l /.'"'vr.;-. fkGi^.fL^r (^ixTcA^ Proj. Location: \hi? f•.^t^ Ur f^NfV (IH.^M tbAt. "Onji. Proj. Number: Phone tt: ^(.^,^17-AiU Fax# = 3oy^. j(rAAl-rMCtT- iiii iil 111 ^ iiii iiii Cl -fc4 . HydrogMi & Helium < Permanent Gases (CH4, cx), co2, N2,02 > Mopcury ( SoU > or ( Air • • ) TO-14 by GC/MS ( Ambieia ) or ( Souice •• ) 601 & 602 Compounds •1 iiii Iiii 111 IHlii Chlorinated HC BTEX BTEX & C5 - CIO T H I {C5-C10)or(C4-C12) Cll - C18 Specify below. . i. Sampler's signature : '••\A:'-\r\. .'A. ^-A.ni.) * An additional 22 ml vial of sample is required when requested in combination with another analysis. • • Available upon request. Collection Date Time Ntmd>er of Coolainen 'Summa* t if Can. used Sample Type Sample Identification Requested Analysts <Other) Remarks •ViS-o( 2ai 7 .MtU Cv^aS hii^isvL- JZOi. 3in:3f\Cj:^f:.7 t^PoUtylOS LUii i'fp-NJMP-ti: A,A-,t \ Z 3 hfl-'-VjMf- I t ) An<.t 10'^ hH^XlMj^-^D &,v ili£L P?p.- VMf^ Z : L 3 ¥ . t ii_a. f\3A3A333LA7YA .#»*- ivfl i-"pp..\fMp- A 3 Bftst 1^3 fpP-\J^^[^. s r feK,i- H?q^? fPP-VMp- '^I) Hyfet IC^-^fe fi'p- \i^Ap- HS hifef. ^fUlQ ppp-vjMj'^ ^g: feas^ fin l(V ii ID ii f vf- \ i M p - ^-1^^ £y6£ mmm. Resulu to : Invoice to : AkA^i- f\cAa.LaT (t^-red.) llllllll iiiiiiiiiiiiiiii Ill iiiiiiiiiiiiiiiiiiiiiiir CO o cn o vo - J Relinquished by : Company : ^••lc.l/IC£>^/'i4/U'-t, r Date : 3-15-OC; TinK : IGOO Received by ; Company : Date : Time : Relinquished by : Company ; Date : Time ; Received by : Company : Date : Tune : Relinquished by : Company : Date ; Time ; Received by : Company : Date : Time : _ _ J T WHITE COPY : Laboratorv to remm. YP.I .t OW r n P V • T >kAF.i.sr» Diuv n n n v . «;..w«:«— •? ¥ ^ f r?.*r.ft.7^vw5i'tT;:f?'?-TrT7:^"T^*';TT'' MICROSEEPS, Inc. 220 William Pitt Way, Pittsburgh, PA 15238 Phone: (412)826-5245 Fax: (412)826-3433 l]\3...aA.^.x nhu r CHAIN-OF-CUSTODY RECOIO^ V* Note: Enter proper letten in Requested Analyaea cotumna below. A n a l y s i s O p t i o n s Note: if analysts D.E.or K is selected, scratch (option) NOT wanted. Company Name: Address: A^A \,^iai^A,J.(vA('.L..A9->i\ii\ iAiUU7.,^^ ^43^ 0 7 6 ^ 9 Prqj. Manager: fsi'viiAiH 3 \ r Hl.i^/ /"1()6& fk^&^Lar (<:A13C:') Proj. Location: \iu/.(c.)f4 \3lfiHbP3A>Mv:'I\{33rr:^. Proj. Number: Phone tt: q(3:',j{313A\ Fax tt: Sampler's signature • . . . / LAA ""KP.M'A M3-~ mm mm iiii m Cl -C4 Hydrogen & Helium Permanent Gases (CH4, CO, C02, N2.02 ) Mercury (Soil) or ( Air •• ) TO-14 by GC/MS ( Ambient) or (Source •• ) 601 & 602 Compounds mm Chlorinated HC BTEX BTEX & C5 - CIO TPH (C5-CI0)or(C4-C12) Cll - C18 Specify below. An additional 22 ml vial of sample is required when requested in combination with another analysis. .'ri'fa ..•'^~V '^•AlJ.'.n A • • Available upon request. , • S u m n u * f S i m n l e . S i U n o l e ' ^ > C_J ' Collection Date Time Number of Containen 'Summa* f if Can. used San^le Type Sample Identification ReytfiSt0d Analyse (Others Remarks •oo 9 :;<u<-t.:>n6 R'P-SVC' io t3)i:t ':>\TE. |ftfcCg.T .ti^^Po,vhiO-'' vB^oe ILZL Fft03lS0Q ssaf*"" iiiiiiiiiiiiiiiiiiiiOiiiiiiiiiiiiiiiiiiiiiiiiiiiniiiiNiiiiiiiiiiiiiiiiiiiiiilliiiiiiiiiiiiiiiiiiiiiiilliiiiiiiiiiiN m Resulu to : Invoice to : t^ti^i.] (:,.!(..ML iM i Mc.[.8i;'t^!/l4/1e.T iiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiHiMnnm J&S6 A(,e<saJi", S31H3. o cn o vo 00 Relinquished by : Company : ; Mcd-/\eew/Hi^£..T Date : Time : Received by : ivoo Company : Date : Time: Relinquished by : Company : Date : Time : Received by : Company : Date I Time i Relinquished by : Company : Date ; Time : Received by : Company : Date ; Time ; J WHITE COPY : Labontoiy to return. YELLOW COPY : Ubontory PINK COPY : Submitter MICROSEEPS, Inc. 220 William Pitt Way, Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 Company Name: Mc^La<cr^/l-lprJ Address: ^^TS Tn<jfi)PgAcJ.?,nc^ glud?, lU^rfcn iVO' 0 7 ( 3 3 l Proj. Manager: Proj. Location: Proj. Number: Phoned': 90'^ • C U - ' S / / / ^'^'*' I C ^ - C Y I - ' ^ / C ^ rcxj^t^. I d f 3P CHAIN-OF-CUSTODY RECORD Analysis Options Note: Eater proper letten ia Requested Analysea cotunms below. Note: If analyns D,E,or K is selected, scntch (option) NOT wsiried. — r 7 . iJiVoiifs 'T.rflana ^Ke.mic3 $.r<r- Sampler's signatxire : •/yO-AA'.^, mm ill ill Iiii iiii ' ^ ^ Cl -C4 Hydrogen & Helium Permanent Gases (CH4, CO. C02, N2,02 ) Mercury (SoU) or (Air ••) TO-14 by GC/MS ( Ambient) or ( Source •• ) 601 & 602 Compounds iiiiii Iiii iiii •ii iiiii iini Chlorinated HC BTEX BTEX & C5 - CIO T P H (C5-C10)or(C4-C12) C l l • C18 Specify below. ,,73: * An additional 22 ml vial of sample is requited when requested in combiiution with another analysis, • • Available upon request. e.H//hffA-Z.d^*'/ ' ^ ' ^ ^ > ' y / < ^ - ^ ^ Collection Date Time 3 - 7 1 OO 5-71 Oc I - 7 1 - 0 0 Z--.2I-CC . ^ 7 h C ^ 5ai-0o ^Al'oo }> AhOO o ' 2 i 0 0 •3-7.100 ,^••.21-00 : > - ^ \ 6 0 'illlllllllllllllllll! /VfS'i /5'3'V /•i'./o -70 \ M •J'.cifb l^'iXi / £ ; s ^ :?©•// 7,070 /% '07 / 5 '07 tb'.^Tj Number of Containen I l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l "Summa" # if Can. used IIIIIIIIIIIIIMIIIIIIIIIIIII Senile Type StAU^ \ K / Sample Identification rPP5)Jel--S.^5E rffSi/E.-L- /-S f^PP^^^l- 3 . 0 F3f6\IB^- h ' O r'PP7 7 £ . l - S . b 7i6T5i/ai~ -5.75a AST.50B.-1-- h h 7t5T.^\/B.t~ S.O .7^5r3\la.t~ S.3 Asr^iSRi- s . o XNLBr-(3.'^5<£. Zr^t-i^r ' /-S iiiiiiiiiiiiiiiiiiinn IIIIIIIIIII IIIIIIIIIIIIIIIII iiiiiiiiiiiiiiiiiiiiiiii Resulu to: ^ ^ ^ ^ ^ B , ^ h h ^ . 7 ^ 1 J ^ Ce ^ P l - f a d lllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllll Relinquished by : Relinquiihed by ^ Rclinquiahed by : 1I1I1IIIIIIIIIIIIII1IIIIIIIIIIIIIIIIIIIIIIIIII1IIIIII C o m p a n y : C o m p a n y ; C o m p a n y : llllllllllllllllllllllllllll! D a l e : 3-7a'0O Date : Date : iMiiiiinimnim™ Time : f7 O O Time : Time; w7mm!^mfmm^mmmWM^mMM7Am&m7fMM». IIIIIIIIIIIIII IIIIIIIIIIIIII IIIIIIIIIIIIII IIIIIIIIIIIIII Remarks 5y7<i To rye./ <A(. />»/fcv/!'«^ 1 1 1 I / 1 V lllllllllllllllllflllllllllllllllllllllllliiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiniin^ voice to. ^ ^ ^ J ^ ^ ^ j ^ ^ ^ i ^ / c ? C _ lllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllll Received by : Received by : Received by : llllllllllllllllllNllllllillllillll C o m p a n y : C o m p a n y : C o m p a n y : llllllllllllllllllllllllllllll Date : Date : Date: lllllllllllllllllllllllllllllllll Time : Time : Time: w o cn o vo vo MICROSEEPS, Inc. 220 William Pitt Way, Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 t(i-CJ e /R. OT = 3 "-3 CHAIN-OF-CUSTODY RECORD Company Name; 73c L a ^ OKP3a 3 Analysis Options Note: Enter proper letten in Requested Analyaea cotumna below. Note: If analyais D.E,or K is selected, s c n t c h (option) N O T wanted. Address: .^S T^Up.»rK(iatu^^ S h d . t^c^rre-A . N-T O 7 0 3 ' 9 Proj. Manager: /s/prnM^ ^icklAf\ 17o<-,<f- A^{it. l o t ( B r I c P ) Proj. Location: i^\fG,in •'H.-AUA/ CAA/TMCUI S'/T^JT- Proj. Number: Pkone # : ^ O ' j - C J l - ^ / l l F« * '• 9 o 1 f - ^ ^ ? - ^ / C 2 /3 • A *B *C D E F Cl -C4 Hydrogen & Helium Pennanent Gases (CH4, CO, co2, N2,02 ) Mercury (soU) or (Air ••) TO-14 by GC/MS ( Ambient) or (Source •• ) 601 & 602 Compounds iil iifti iiii •i iiiii liH Chlorinated HC BTEX BTEX & C5 - CIO T P H (C5-C10)or(C4-C12) Cll - CIS Specify below. Sampler's signat\ire : V p 6 L ^ / / j 3 ^ ' 3 * An additional 22 ml vial of sample is required when requested in combination with another analysis. • • Available upon request. •I^c7u<'jl&^ c^f-Ay / b<:AZe.,i<t ^ ; ^ ^ ^ 7xy7<iA.e^, Collection Dale Tune Number of Comoioen "Summa" I if Can. used Sample Type Sample Identification Requested Analyses (Others Remarks 5'7i'00 / ^ • • O ' ^C:.' Lcu J ^ L £ 7 ' - ^ , 0 5//c- 7iry^-7'<^ '/•it.AM^</> .b-7i'60 XO!A± Z A ' i . f Z J ' ^ . O 3 ^i 00 i^:/o ^T-HAO^^r - 8 / 6 £ :X"0O iy>.'77 7^y/iAU.i>T- 7,S .3--7J 00 l^'-OA ^//yy^a^r- 3 . 0 3 3 Xtoo 20 Ah 3 ^ ) ( / / A ^ ' j l ~ 3 ' 0 •^•"'"•"^ /Porm.^ B,c.hl,r.y , - ^ 7 j ^ f e ^ / l 7 ^ 3 iiiiiiiiiiiiillllllilllllllliilliiiiliiliiiliiilllllilllllilliiilllllllll '•""'"^,£./?- R e l i n q u i s h ^ by ; '' Relinquiihed by : IIIIIIIIIIIIIIIIIIIIIIIIHIIIIIIIIIIIIIIIIIIIIIIIIIII C o n ^ a n y : Company : Company : IIIIIIIIIIIIIIIIIIIIIIIIIIIII Date : Date : Date : IIII lillllllllllllllllll Time : 7 7 : 6 6 T i m e : Time : ' ^ ' ' ' ' ' ' ' ' • : 3 ' o 5 ^ A 5 r ^ l c i , e r i - c c lllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllll Received by : Received by : Received by : lllllllllllllllllllllllllllllllllllllll IIIIIIIIIIIH C o m p a n y : Company : Company : llllllllllllllllllllllllllllll Date : D a t e : Date : lllllllllllllllllllllllllllllllll Time : T i m e : Time : O cn M o o MICROSEEPS, Inc. 220 William Pitt Way, Pittsburgh, PA 15238 Phone: (412)826-5245 Fax; (412)826-3433 •A'\AA..:A::.;,3*i:^-j: Z J ' ^ CHAIN-OF-CUSTODY RECORD A/a /OO/ t33.cu-,-./)~}6<3 Analysis Options Note: Elder proper letten in Requested Analyaea cofainms below. Note: If analyaia D,E,or K is selected, scratch (optioo) N O T waitfed. Company Name: Address: ;^r,T,,r4-y?rrrt,xt./.7?)u.V. {l)r.,,^r. N 3 A^^y^.^A Proj. Manager: Mmm^ /^..r/.A/v^/vTn^<-- J n ^ f c l c j Proj. Location: |/,m,r. T-^.lor.J 7"k^r^t^iJ^.^,/r~ Proj. Number: P*»°°« * = 9 7 n / 7 7 7 ^ ^ 3 7 l F " * = 9oi<-T^^-Zy-"^7/3 iiiii iiii i i p iiii C1-C4 Hydrogen & Helium Permanent Gases (CH4, co, co2, N2,02 > Mercury (SoU) or (Air ••) TO-14 by GC/MS ( Ambient) or (Source • • ) HI 601 & 602 Compounds 11 Chlorinated HC BTEX BTEX & C5 - CIO TPH (C5-C10)or(C4-C12) Cll - C18 11111: Specify below. Sampler's signature : / " </c7 9^ b3aTh i>/ 'Al' * An additional 22 ml vial of sample is required when requested in combination with another analysis. • • Available upon request. ^ . ^ / y / b t f ^ Z e / j e ^ V t A / v y / i P / ; ^ ^ A <3 r,\po^*c& ' of<'7o/\CA iK^3 Ple>tp ci/oil J IT I c/lvic3enii>. ."/c/nf/tf Collection Date Tune Number of Containen "Summa" I if Can. used Sample Type Sample Identification Rei^[uested Ajnalyses (Othw) Remarks 3£7376<A 17 70 n p ^ ^iaJA^ rP/.5\/f3 ^iir76IT'l /*tmf f 7 , i PAiX fPPS )7hi-A 1775 rfiPdTiP ID rAT-33.i //w(7 iiu'./i J n ^ ..•fi/i^^,-/.>r^ •; p:/7> f f f l / M p AT. j:La. yr'Air ^r.rma FPPW7P .^S '7^)9^- ^V7 ^77J jO. '.26 r3Pi)/AP Alb^A \'l'l% rPP'j7^iP -20 a :7k rPf i/T^iP 3 5 2'7.i fpp^TiP 3 r E a'^7 rPp\)riP 3 0 Ni' 3?53'> T t / U FPP\7.'7p v5 Resulu to : lllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllll '^^377^-' Relinquished b y ' : Rsliivjuiabed by : iiiniiiiiiiiiiiiiiiiiii IIIIIIIIIIIIIIIII Company : Company : Company : IIIIIIIIIIIIIIIIIIIIIIIIIIIII D a t e : 3/A73P7>6 D a t e : "' D a t e : mil Illlllllllllllllllll Time : /7:00 T u n e : Time : Invoice to : iiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiii Received by : Received by : Received by : llllllllllllllllllllllllllllllllllllllllllllllllllllllllll Company : Company : Company : IIIIIIIIIIIIIIIIIIIIIIIIIIIII D a t e : Date : Date : lllllllllllllllllllllllllllllllll Time : Time : T u n e : W H I T E C O P Y : Labontorv to return. V E U J O W C O P Y .. I..h«r>tnFV onov r>nDV . . c u - I'.'yffiPvTtlT?*.'" • 'T;'TV';W.';!y.)iy(UWi'W-'*W",-'^''j'^ "TTlfWf'-lti^^Xjfl-^--((^ W J - l f . ^ , ^ : ; ^ ^ MICROSEEPS, Inc. 220 William Pitt Way, Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 /4<^e y^3^ ^ CHAIN-OF-CUSTODY RECORD No. /<:>CJ '•™!;rr5w«<n«»ws^ Analysis Options Note: Elder proper letien in Requested Analyses cohinms below. Note: If analyns D,E,or K is selected, scntch (option) N O T wanted. Company Name: Address: Proj. Manager: Proj. Location: Proj. Number: Phone tt: Sampler's signature: .-- 1 K3 r - n p \ n I- Faxtt: JAJAJJ.^A'' *A * 1% • c D E Cl -C4 Hydrogen & Helium • Pennanent Gases (CH4, co, co2, N2,02 ) Mercury ( Scril ) or (Air • • > TO-14 by GC/MS ( Ambient) «(Source • • ) 601 & 602 Compounds mm •ill ^ i mm H Chlorinated HC BTEX BTEX & C5- CIO TPH (C5-C10)oc(C4-C12) Cll - C18 Specify bdow. * An additional 22 ml vial of sample is required when requested in combination with another analysis. * * Avsilable upon request. Collection Date Time 3/.A3P}Ct \ "l It JPJ-M 17'.Xl l^'.hS I7'S7 a39 . / . - K - ^ /.t'.50 N u m be r of 3. 4^ A llllllllllllllllllllllllllll "Summa" 1 if Can. used l l l l l l l l l IIIIIIIIIIIIII Type . ^ ' / & 5 ' \| V l l Sample Identification FPP 077 P VZ P P f { i M P ' / 0 TNTAIcP ^7/13057 /\S7 V71P TTIJ: /:>7 o 7 i P ¥ 3 f 3/737^0-e/_ J AIM Results to : 3AC9 / J f C lllllllllllll!lll)llll!lli!lllllllliillllllllllllllllll!lllllllllllllllll Relinquished by .n 1 xi ^-./ ReU^uished by : '^ Relinquished by : IIIII IIIII Illllll IIIIIIIIIIIIIIII " " ' " > / / / / Company : Company : IIIII II IIIIIIIIII D a t e : 3/7^/60 D a t e : Date : II IHI m m Time : 7 7 (7^ T i m e : T i m e : Requested Atk(tlys4» (Odur )t IIIIIIIIIIIIII lllllllllllllll 5,/'^ Tai'^f-/ Ce, 4/ Remarics t/}ci>/> o i Invoice to : A 3 » ^f^f ^ lllllllllilllllillllllilllllllllllllillllllllllllllllllllllllllllllllllllllll Received b y : Received b y : Received by : III iiiiiiiiiiiiiiiiiiiiiiiiniiiiiiiiiiiii nil C o m p a n y : C o m p a n y : C o m p a n y : iiiiiiiiiniiiii II Date : Date : Date : IIIIIIIIIIIIIIII llllllll T i m e : T u n e : T u n e : W H I T E C O P Y : L a b o n t o r y to return. Y E L L O W COPY : U b o r a t o r v pnov rripv . cvm-.n*. MICROSEEPS, Inc. 220 William Pitt Way, Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 Company Name: P l c L o \ c r \ / P l o ( 1 Address: :?,J, 7"/..Vrvg«?//-/(^/v e /?/</</ LAr^Kfrs 7^/3 C ) 7 o ' s 9 Proj. Manager: M , mo / M A J J ^ / . J r ^ s ^ M t e Is/ Proj. Location: {}uyr^ A A l o a J «^}>f->v)f^/ Proj. Number: CHAIN-OF-CUSTODY RECORD A/o. / 0 0 3 { Analysis Options Note: Eater proper letten in Requested Analyaea cohumii below. Note: If analyaia D,E,or K ia aelected, acrateh (option) NOT waited. Phone #: QO% P y y - " ' / / / / Fax ^ : ' 9 o % \ i : ^ 7 ~ ' B / C S Sampler's signature : pH'^l^ P7-\Jj.J. 3o ^ \ *A • B »C D E F Cl -C4 Hydrogen & Helium > Pennanent Gases ( CH4, CO, co2, N2,02 > Mercury (soU) or (Air ••) TO-14 by G C / M S ( Ambient) or (Souice • • ) 601 & 602 Compounds nil ini iiii Hili Chlorinated HC BTEX BTEX & C5 - CIO T H I (C5-C10)or(C4-C12) Cll - C18 Specify below. ^ £,/'^ ^ < 9 £ ^ * An additional 22 ml vial of sample is required when requested in combination with another analysis. • • Available upon request. e ' / k y l h o n t e f i - ' / ~ * C T / O > ^ y / e n - t /.ofvhCorQ^ ' atr-^c/t"! ihf't^/T^'i^cllofiJf) c/lctaToif^ , -A/u^n-p Collection Date . . Tune Number of Containen "Summa" I if Con. used Sample;, Type Sample Identification Requested Analyises (Other) Remarks 3x3<!0 )2^:5o ^ Sc/Qc A575\7P± $ 3 A l c i ^ ^ 7 ^< t),pc^t^.d )7 A75 .A57mS'l'/^Pl^ HOLD M/TJT 1732 A77 vnP /O a'.si A'5r\7/iP ^ 5 cj / o^r\ A i...3kni lio 3/t :/\ /^ ^ i A57H/lP ^ 0 •//o n/1/^/ys'- b y A57 17/7P 3 5 '^/mA .. )im A^rmP gx / i V O r J ^ . " ^ / / D A 2 TM 17 Al A<>r\7HP30 .£-£. g/,/^'"-^ Al >.i% A57\77iP »7- 7-90^-€97 -zT/// Jl f7Ai: TAI \J AyjVTiP ^771 _1£ CO o cn M o CO IDM mnM Resulu to : /Po/'hO- 7Ai7khrs - //c/*>ieh//7on Invoice to : C7^^€> As^^f^i - ^ r i ^ \m Rslinquislted l)y i^A Relbiquiahed \ ^ Company :, Date : /;B/7>O trr— Time : Received by : Company : Date : Tune: Company : Date : Time I Received by : Company : Date : Time : Relinquished by : Company : Date : Tune : Received by : Company : Date : Time : WHITE COPY : I-aboratoty to return. YELLOW COPY : Laboratory PINK COPY: Submitter MICROSEEPS, Inc. 220 William Pitt Way, Pittsburgh, PA 15238 Phone: (412)826-5245 Fax: (412)826-3433 Company Name: pi3..r,(crs^//„ 3 ' Address: A}^.rrr.^.p^rtn/^rt.-^ PT/LV U . U , . ^ ^ klAT 7\7r\-r.Q Proj. Manager: ^,^^_ 7^,.^/.^ / . T h ^ X . , - / , / / r , / ^ ) Proj. Location: |J.Q,,V - X - . ^ ^ r / / ^ ii^».^^.//^^ < A U Proj. Number: . P^°°«^-- QC^-7:^/7- -7^777 Fax#: ^^f? .yf^/-•g/^g' CHAIN-OF-CUSTODY RECORD AP / 0 C 3 Analysis Options Note: Ester proper letten in Requested Analyses cohimna below. Note: If analyais D,E,or K is selected, scnteb (opiioa) NOT wanted. Sanq>ler's signature * A *B *C » E F C1.C4 Hydrogen & Helium < Permanent Gases {CH4, co, co2, N2,02 ) Mercury (Soa)or(Air»») TO-14 by GC/MS ( Ambient) or ( Souice • • ) 601 & 602 Compounds mm lip •ii Hi Chlorinated HC BTEX BTEX & C5- CIO TPH (C5-C10)or(C4-C12) Cll - C18 Specify below. * An additional 22 ml vial of sample is required when requested in combiiution with another analysis. . • • Available upon request. t r / l ' ' y / h ^ t l T e ^ & f ' 7 r s t v 7 ) C y P ' ' ^ ^./^7^.r^t^i r^A'/cono^:^ y ^A^^/c^c-: /^r/h7<^^ <7-H73''' f^pJ^.^^ ./^/^^^fc^- (Others Collection Date Tune Number of Containen "Summa" # if Con. used Sample Type Sample Identification Rei^uested At»ilya» Remarks 3/73/00 i l - l H a. ^ [ ^ rPP6vfAL ^37i'{^f Gift ft wL imio vo IB-19 EIIMEJI- 3 ) K A O O 19'H2 XNlAM- -TAT-^yT/ooL^ m^joo tS'tf.5 f^wAOf^r ' P I ^ r v anry/^OftT' IplJpo lffW(> A^n\^tm/ r ^ / / Alnlf>.A 4Z24M /7.'»9 AAJ- ^11 P U ^ 90% P.V7i777l •AIA3}OO 17'.'^^ A.5rilr1Pg.T :ipAiioo i'' 1..'^. A^TT.'^O^/ %i7>.llf» ^W-eT 7^PP.^>l/£7 6'.5V T T / r M B 30/£O_ 6:S7 p:x3A05r T 1 \ / • ^ Vo(JoNsP.D Resulu to : Alo(Ar^ PPli^l^ltn iHcLofer^///<'''' Invoice to q-o,^ AQ>'^/OP'I ^//<^A Relii ishe^ by : , RfcUnquished^: Con^any: Company': Date : 3/7.^/^ Difte: Time : / 7 : 0 c Received by : Company : Date : Time : Time : Received by : Company : Date : Tune : Relinquished by ; Company : Date : Time : Received by : Company : Date : Time : WHITE COPY : Laboratory to nluro. YELLOW COPY : Uboratorv PINK C O P Y : .tiiKmtft... '5f""^'?'T MICROSEEPS, Inc. 220 William Pitt Way, Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 7 7 ^ ^ J '•' A . / . ™'»*T^'!!Fy*?PWr™w)» -A^m CHAIN-OF-CUSTODY RECORD Ni-^/OOf Note: Eitfer proper letten in Requested Analyaea cofaimna below. A n a l y s i s O p t i o n s Note: if analysis D,B,or K u selected, scnteh (optioa) NOT waited. Company Name: / / • /,?y..;.v //A..- / Address: ,2.^- Z,...-..-. '^A-A.^'A B / W - A,A,,......^ //J^A^.-r^-y Prqj. Manager: M>...-A. A,.-77.^- / X.:c d r . A / A^XJlAA ) Prqj. Location: 7.,-.-: ..^'Ao ^ A A7....... r~.J 1^3- Proj. Number: Phone # : ^.-f. ^^^yy. f}/^/ Fax # : y^-.f.; ^ 6 9 7 • A7-73- Sampler's signature : - ^ M - ^ / ^ / / / S ' • A •B *C D E i F C1-C4 Hydrogen & Helium Permanent Gases (CH4, co, C02, N2, o2 ) Mercury (SoU)or(Air«) TO-14 by GC/MS ( Ambient) or (Stfiroe •• ) 601 & 602 Compounds •il • 1 :|i|| WM. ilil iii Chlorinated HC BTEX BTEX & C5- CIO T r a (C5-C10)or(C4-C12) Cll - C18 Specify below. Af if- ! ^ • 3 Z...- * An additional 22 ml vial of sample is required when requested in combination with another analysis. * * Available upon request. ,' -'- 'Xy''''-' ^^fMrm^^rt^mmmfmmfmmmmmmmmmmmmmm , Collection Date TisK Number of CotOainen "Summa* S if Can. uaed Sample Type Sample Identification Reipested Analyse iQ^bxst} Remarks ..i^ / 7 A -'• •) /;s/^A V.A J A/r I.,.,./-./... ,. MMI 3 7 ^ Aspsvc. 1 -/i i:7f 7 ./•* ~377^'-'-' / / • v / ^'-VW.: 7'/3.:<V£ X UZ^^Tjl 337^333333 ".?/i^'/v a^££. I.A7A:. £ A ^ < r s / ^ 7 f //,.•..'/ r- ^,,..,„..: -'^•^r „•'--• ^,VJA'3->I /(•' 77/.••-.(, ^ ^ ^ ^ • - A - ^ r - '/-'/7 A/<...-^A / . A '&/Ar/e-( 7-^9 ••-•their 4:Ar^VS7 ^/^^.„>/C-^.^:,. 7.-/^-. .A.'// .Uki. .y-y;- SAAiJAS.r 7 / 7 7 iA£ jf ^ A ' ^ •••f/i\ :.-/>>-'"/'• V 7-i-'- ^-./v>f 3,i^AA3" ^/PtAj:.^.....,. ,M^ Z- Z-ipKi. ^33:7^,.^.... •••u. Af/' ^' C:,rf'' .y-''-••••'.* '•/,. Z-.j.'/ru.........., H I Resulu to : A.->-.•//? Invoice to : / • - A / r 'iiiiiiiiiiiiiiiiiniiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiim!!^^ ^ //,...• / -^';r/^ / ' t (-':/ r A' .7 Ac. ( Relinquiahed by : ^ ReU^uished b v / Company .A^<£uiCr /IL TL Date : •:^S.17J60 Time : 77 00 Received by : Company ; Date : Time : CtRBpfoy : Time : Received by : Company : Date : Time : Relinquished by : Company : Date : Time : Received by : Company: Daw : Time; WHITE COPY : Labontory to return. YELLOW COPY : Ubontorv PINK r . ( \ W • «..k.ni«.> ^:rr^ y^f^r.'W^^.:i^''^.---''.y.~^: •; .•^..^yv^.'^ -;jji!ry^>,i<ij.;^j!).;i|iV»'j'iiuf's MICROSEEPS, Inc. 220 William Pitt Way, Pittsburgh, PA 15238 Phone: (412)826-5245 Fax: (412)826-3433 ";? -. ') -..A CHAIN-OF-CUSTODY RECORD Alo./O&j Note: Enter proper letten in Requested Analyses eohunna below. A n a l y s i s O p t i o n s Note: if analysU D,E,or K is selected, scrateh (optioa) NOT waited. \ Company Name: /./. / : .,,/At.. 7 Address: • • i ' .•; .-^ -• .,. <^ A://:.,-/, fi/u,...,,., / / J f , ' ' ^ : - Prqj. Manager: ^: . , „., /.-,, ..J /.,.. / j : , _ , , - , /A,., / / / / , , • , / / . ' Prqj. Location: 7..-,..A r.-A.„7 :'Pf'^-.-..I/ A / < 2 Proj. Number: Phone tt: -/^-n • . f.,/;.- - <.</// Fax tt: ;^J /v . ^ f//- Sampler's sinmture : " 3 ^ 3 3 3 7 / 7 . ' 3 ^7A9^ wm i i P iiii m Wi C1-C4 Hydrogen & Helium Permanent Gases (CH4, co, C02, N2. 02 ) M o x u r y ( SoU ) or ( Air •• ) TO-14 by GC/MS ( Ambient) or ( Souice •• ) 601 & 602 Compounds o K Other Chlorinated HC BTEX BTEX & C5- CIO TPH (C5-C10)or(C4-CI2) Cll - C18 Specify below. i^ S/7t3'-f7^ * An additional 22 ml vial of sample is required when requested in combination with another analysis. ** Available upon request. t.-'/^>v.. / *' 7/,/ / •' .> / ' ' , , , , P ^ / A A . " . J 7 : iL. Collection Date Tune Number of Containen "Summa" f if Can. uaed Sample Type Samjple IdentiHcation Reipested Analyses (Othec^ Remarks > / r / . /7-/-- A^/Ap- ^77^7/^2 f/e 7«< 7 3^- /A'/'/ 7 <^A/7A>jt 77P.A71 : ! - / } ^:7i7*.ri-7C'-.-. «^./,.,.-yi * * s i ^ A/A: 7 /A 79 <7AA^.r 4i/AV£.J .'Aft.. /^,~*-/i'A..-'y.'r':'/ •-'> 3 A 7 U 77-/7 -^ ../fcjf 37A..ic-7/7S- ^pPr/^A,... A/prP. ^,/fA JAP ^, i l ^ A - A / , . /f-A/n -JSM £iA. ^Pf3'^rf:- 'iiiiiii iiiiiiiiiiiiiiiiniiiiiiiiiiiiiiii IIIIIIIIIIIIIIIIIIIIIIIIIII iiiiiiiiiiiiiiiiiiiiiiiiiiiiir Results to : 77..'-:'^A P . - / A , . ' / .••^•&7.'-- -•../ / / / A . - Invoice to : iiii m 3'-M: A,A/-7 mmhmmmm i n Relinquished by : /MA/A-^T <y '4r<7A^7/ Relinquished by/^ Company : A / / / / Date ^/o Tune : A7:O0 Received by : Company : Date : Time : Company : DAe: Time : Received by : Company : Date : Time : Relinquiahed by : Company : Date : Time : Received by : Company : Date : Time: WHrre COPY : Labontorv to return. YF.i.inw rnpv • t .>u»>i/. vnjv r^f\tw . d-.i—:—- M Company Name: Address: AIA: MICROSEEPS, Inc. 220 William Pitt Way, Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 /f<'.'iL.<< >'>">'' 7 ^ 7 a I i ' Ac,c Vofms ''3 <A^) CHAIN-OF-CUSTODY RECORD Ak/OO 5 i " .-I , . „ i Note: Eater proper letten in Requested Analyaea cblumna below. A n a l y s i s O p t i o n s NOM: if analysis D,E,or K is aelected, scrateh (option) NOT waited. Proj. Manager: Proj. Location: Proj. Number: Phone tt: '-p AT-.? ??Vi F'l.-^///••./ja^-;<:t. Ac.t^i.'/ryi P f ^ ~ 7 f ^ 3 -A77-7i7/7 Yaxtt: 'Ayi-pvT-AnAp *A * B *C D E F C1-C4 Hydrogen & Helium Permanent Gases (CH4, co, C02. N2,02 ) Mercury (SoU) or (Air »•) TO-14 by GC/MS ( Ambient) or (Souice •• ) 601 & 602 Compounds ill mm •ii •• •n iiii Chlorinated HC BTEX BTEX & C5 - CIO TPH (C5-C10)or(C4-C12) Cll - C18 Specify below. Sampler's signature : jA/i 4 / .f-^73 * An additional 22 ml vial of sample is required when requested in combination with another analysis. • • Available upon request. er7Aj</bt?-nZeyi^ / Ao'/o / y / / r / i ' ~ i > Aw-^- ^^•'''^-tt^'^PinA.»fm,.«,/'^ ' ^'^'^p.f.Cj.f?'''A.P^:P.'\'°.... .P:^'^.'. f"^' •*'^i:ifc3i-}rt^., "/.'.AJJ^A f Collection Date Time Number of Containen "Summa"! if Can. uaed Sample Type Sample Identification Requested A n a l y ^ (Other) Remarks A/->Ai-, 77. t l P^7C^' r^ffisuP/ 5 i P 7 i i ( U r f c ^ gAjdaA iuA^L. <3A7 •y> r.t. l^lANP - V7P -^3iP i^PP V7-1P /X A/AP fA^ PPP771P/0 :>/,-:A7. '7{';.ac rP7i/AiP^^^5 T / T - r?V/A..>s ^ TAAS- 3PfVMpAT- 3^ i4.-..y f, „.'•.... A'^•.- •'• •^7:/7P- .^.'.SM-. •T^-pPttH-f^-^—A- t (T rr' 3 NAima •A/AA AT i •;» I P-PPi/nP ^ B 9n'K~^^n--7^./7/ M2C FPP\7MPnS .-3 l^.,,'' t:Am T^PP I/.MP S J np <iS7 i / ~w F P P i7Tip ^u7 '-^AA>P A:P77 liiiiiiiiiiiiiii'iiiiiiiliiiiiiiiii'iiiiiiiiiifliiiiiiiiiiiiiiiiiiiii iiiiiiiiiiiiiiiiiiiiiiiiiiiiifiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiM F P P m P ¥.3 oiiiiiiiiiiiiiiiiiiiiiifiir Resulti to : pic 1 fn <K Bick jt.'\ ( ' ' 3 1 o' rr./po (1) Invoice to : JOS-C- / ^ / w r ^ / ( ^ f P < ^ 3 CO o cn M o Relinquished by,: i ,, ^/37/K.AJ--5'' Relialquished by./>^ Company : AP/PA Date : Time : Received by : Company : Date : Time : •:5/::mt 7 7 0 0 Company : Date : Time : Received by : Company : Date : Time '. Relinquished by : Company : Date : Time : Received by : Company : Date : Time I WHITE COPY : Labontoiy to return. YELLOW COPY : Laboratory PINK COPY: Submitter r ^ H ^ ^ a t Company Name: Address: ; . j ! . j ! Proj. Manager: Proj. Location: Proj. Number: Phone tt : ^^yX - ^;^/ y- -,?/// MICROSEEPS, Inc. 220 William Pitt Way, Pittsburgh, PA 15238 Phone: (412)826-5245 Fax; (412)826-3433 A3..h>irn P/Prl oW-z-^.g/gri'-f P;7i>i7. itk>He--r\, 74J' d~A-'S7 .J^-.r/-nii. lAi7\/jt\ Pjhiic- ,A<4/C7AP P F l f r ^ } Us1Mir\ ir.*jik./•'7 7ht?./n...f.i:r/ A:.'>/7r- •^Jje 3 fP/n; CHAIN-OF-CUSTODY RECORD AJo/ooX^ Analysis Options Note: Enter proper letten in Requested Analysea cotunms below. Note: If analyaia D,E,or K is selected, scnteb (option) NOT waited. Sampler's signature : ./ ..^7,/i A~* J 7 -~A '^' • A • B »C D E F C1-C4 Hydrogen & Helium Pennanent Gases (CH4, co, co2, N2,02 ) Mercury (SoU)or(Air") TO-14 by GC/MS ( Ambient) or ( Source •• ) 601 & 602 Compounds ipi •iil IIIII iiii Chlorinated HC BTEX BTEX & C5 - CIO T P H (C5-C10)or(C4-Ci2) Cll - C18 Specify below. i.'' P/-Ah An additional 22 ml vial of sample is required when requested in combination with another analysis. • Available upon request. e/j?y/tS«».7«/^e* . -7lls7^/ yyi7<-» O A'\(.j/.A.> 1 Of *-7tM*. . /•Hj--/^v/g-^^.>'» f ftA\rtAf I Ch76f(i7c.djPA^ i -i '/aPue-jt. Collection Date Tune Number of Coolainen 'Summa' f if Can. used Sample Type Sample IdentiHcation Reqttested Ajcalyses <Otha>jt Remarks •A I -'•> A ^ ' 3 1 • r < .5fv/d 5 pfpmp 9X- 53e%i>4r7P'/: i ^ ^^"•"fe iPTLP ^ S ^ 3PP\7r7P30 77 •A. h 7 ;• 57 AAAI vnP^.~L :^/7P 7 : P 3 AS7 i/MP.7^.r-A - r . / 7 - P-.-A PPCXJCJ A h P T l A'^ 57v3iAr/ A t f j <^t>i^--yAfm^j' A.^n .->7P }-.A i'£//7 AT-nrtlu 7AAI..P f > . A t > ' AS77=,7F/ 9C>'P~/C¥7-^AA/ •?MP 7fP,9t ASLJUALEJJL 3 I A P zm. .A^,l-\/MP /P) u. pp. 7;5/C A.'77i//rP' ?^5 •^^;^6 P<(A^f 7 s r \ 7 n P 7?..0 $;cw. A f nil ./:ST' l/7i/^ 7^, S llllllllllllllllllllllllllll^lllllllllllllllllllllllflllll'l'lllll lilOlllllflllllllUlllllllllllllllllllllff m llllllll lllllllllllllllllllllllllllllllinilllllllllllllfllllllllllllllllllllllllllllllllllllllllllllllllllllllllllOlllllllN Resulu to : p7'f<3o I ct\/7ft' <' y Invoice to : to: \ CO o cn M o 00 Relinquished by : -'^'^ M^ U 3-/-3J Company : M ' / / / / Date : yp.t/i'id Time : J 7 ' 0 0 Received by : Company : Date : Time ; R^mqi^shedbyX Coiiq>sny : Date : Time : Received by : Company ; Date I Time : Relinquished by : Company : Date : Time : Received by : Company : Date: Time : WHITE COPY : Labontory to return. YELLOW COPY : Ubontory PINK COPY : Suhmtter /it/e 3 dri o MICROSEEPS, Inc. 220 William Pitt Way, Pittsburgh, PA 15238 Phone: (412)826-5245 Fax: (412)826-3433 CHAIN-OF-CUSTODY RECORD /^^. /00_^ Company Name: //C^^O ff*^\ / /•/r? ( t Analysis Options Note: Eater proper letten in Requested Analyses cohinms below. Note: If analysis D,E,or K is selected, acnteh (option) NOT waited. Address: •v"y-' ['•>•. P Proj. Manager: Proj. Location: Proj. Ntimber: Phone tt: :::rt An i,- J^iU2lf- •>(, >')-•. <••' Faxtt: Sampler's signature : 33/..P^/P^^'^ * A *B *C D E F C1-C4 Hydrogen & Helium ' Permanent Gases ( CH4, co, co2, N2,02 ) Mercury ( Soil) or ( Air •• ) TO-14 by GC/MS ( Ambient) or (Source •• ) 601 & 602 Compounds SHi IMI iiiii iiiii Chlorinated HC BTEX BTEX & C5 - CIO TPH (C5-CI0)or(C4-C12) Cll - C18 Specify below. * An additional 22 ml vial of sample is required when requested in combination with another analysis. ** Available upon request. Collection Date Tune SIA^P AiUP -3/AlP • 7 . h P 3/a A <i'.o7 "PiOP, <7:AP7 9U39 77^6? Number of Containen 3 3.. 3L Pi "Summa" # if Can. uaed Sample Type £f\llPtAt \ \ / Sample Identification A-TTurlPP^T A'77rU7-ip-30 A.^TMnP t/5 A S r A , ^ P ' / T A'--.riJHP'7D IIIIIHIIIIIIIIIIIIIIIIlllllNIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIII IIIIIIIIIIIIIIIII Results to: , ; ^_ A/ppfn^' I^/c'km iiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiii Relinquishedb^f :/,} / / y r j C - 3 3 0 3 P M A Relii^Ued by : / Relinquished by : 1 lllllllll Illlllllllllllllll Company : , A-/7/I Compail^ : Company : IIIIIIIIIIIIIIIII llllllll Date : 3/.3r Doie: Date : IIIIIIIIIIIIIIIIIIIIIIIIIIIII Time ; Time : Time : Rei|uested Aitalys^ (OtW \ liiiPilllllll iiiiiiiiimi lllllllllllllll IIIIIIIIIIIIII lllllllllllllll S3c7nf(,fiA 1 w." i/ Remarks •.n,/J •17AIL>A -TAA lllllllllllllllllllllllllllllllllllllllllliiiiiiiiiniiiiiiiiiiiiiiiiiii iiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiii Invoice t o : / . j Vose yfcj7e/d7 iiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiii Received by : Received by : Received by : llllllll mil IIIIIIIIIIIH Company : Company : Company : Illllll 1 II Date: Date : Date : lllllllllllllllllllllllllllllllll Time : Time: Time: WHITE COPY : Labontory to return. YELLOW COPY : Labontorv pmif rriPV. sukmin... MICROSEEPS, Inc. 220 William Pitt Way, Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 CHAIN-OF-CUSTODY RECORD Analysis Options Note: Eater proper letten in Requested Analyaea cohimna below. Note: If analysis D,E,or K is selected, scnteh (optioa) NOT wanted. company iName: { -i Address: ._•--: vc.;;-,.-!-- ?.,-,- Prqj. Manager: ;\i, Proj. Location: J . ,, LA-... • ..( ; \--iA. T •-.~A-A r i .•-/;::.. i A u . . , r,A,- 77:,,A.,A. f i < •• •- „ A . : . l ^ : - . , . ) A - / i . . i . . > -..,4 ^r,: i T ; <'/V - • > • Proj. Number: Phone # : yA.A.y-;.. >.. ,,. Sampler's signature : -^ L Faxtt: '::,^yi, .-....:, . A. • /,.i:i,. : ' - : ' ' ' / • • . ! : i W i l l iffl • i l l C1-C4 Hydrogen & Helium Permanent Gases (CH4, co, C02, N2,02 ) Mercury (SoU) or (Air ••) T O - 1 4 b y G C / M S (Ambient) or (Source • • ) 601 & 602 Compounds o K lu OOter Chlorinated HC BTEX BTEX & C5- CIO TPH (C5-C10)or(C4-C12) Cll - C18 Specify below. •;4s!xc:. * An additional 22 ml vial of sample is required when requested in combination with another analysis. • • Available upon request ~" i(» ^j *-*7.>'-M ?!,!. M > , Z"^' '>-i'^^.t3 WHITE COPY : Labontoiy to retuni. YELLOW COPY : Labontory PINK COPY : Submitter Collection Date Tune • : A A : - i 1 ! 1 A . i . . ; • • • • . • A \ i , ^ - : -, X: iniiiiiiiiiiiiiiiiii U--;.",- i iA-A, •: I , ; , . • ! ' • • - , • :••"'• i " / i ic-. 'V; 1 : .'f.-.'i -,.,-; . . :., - \-3r2 Illlllllllllllllllll Number of Containen > : • ! , ! 1 ^;, i IIIIIIIIIIIIIIIIIIIIIIIIIII Resulu lo : lllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllll Relinquished by : ' . . A v,i,;l-,i -•• Relinquished by : Relinquished by : "Summa" * if Con. uaed Sample Type ".-^"tV{J. - b ( ' ; i ' ^ 1 i 1 J. Sample Identification r/.r^-V.\t\.-i \ :',.i.-:-:e.'.A.-A-TA,A-f^i T- r., ^,;,.,--,^ '•< lA-^u.'^A'n {,-AA\A^. '-- l-~ I'UrA-AlT f-f-f-VMf^Zf)-^ I f).,A ffi"''AVf.i~ ^ i fAA'-A f^T-VMriT-«i A m ]-:...AA<A.:-.-:.A-^ " ••• i \ .-f- .•.......^-,T ^ a , . A..,,y7A A .;>....-.vr 'i2-AA.>"^-:r.. /AAf:.\;(vlA-7A- iiAAT Vi>. AA-r-A^-AA ! - ' i 0 A u-. llllllllllllllllllllllllllll IIIIIIIIII IIIIIIIIIIIIII Illlllllllllllllllll IIIIIIIIIIIIIIII 3\..-ArA:..^^A |U;ic.r iiiiiiiiiiiliiiiiiiiillliliiiiiiiiiiiiiiiiiiiiiiiiiil Company : h.\:7l \:uj^..l h-pAT Company : / Company : Illllllllllllllllllllllllllllll Date : Date : Date : II IN Ill Time: Time : Time : iiiiiiiiiiW^^ (AfA- lA-rj- i\ ••: : g : ^"^ 'iP ~ An\ 'A:-% IIIIIIIIIIIH ^ • • . X lllllllllllilll IIIIIIIIIIIIII IIIIIIIIIIIIII lllllllllllllll ' .If i n . . 7 \ ' , t \ \ I Remarks .;,;";••,, vfeiCvS IIIIIIIIIIIIIIIIIIIIIIIIIIINIIIIIIIIIIIII IIIIIIIIIIIIIIIIIIIIIIIIIII Illlllllllllllllllllllllllllllllllllllllllllllll Invoice to : 'A33.'-/^i~ \A:7.&.u^r,7SZ7\£C^ niiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiii Received by : Received by : Received by : II llllllll iiiiiiiiiiiiiiiiiniiiiiiiiiiiiiiiiiii Company : Company :' Company : iiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiniiiiiiiiiiiiiiiiiiiii Date : Date: Date: Time : • Time : Time: A ^ CO o cn o '^•^^••••:'\'y^.]y-VI'<---''^-'-)-'''^-'^.f'ltfi;^y^^^^^ MICROSEEPS, Inc. 220 William Pitt Way, Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax; (412) 826-3433 CHAIN-OF-CUSTODY RECORD > Uvf t Analysis Options Note: Enter pioper letten in Requested Analyaea cohinms below. Note: If analysis D,E,or K is selected, scnteh (option) NOT watted. Company Name: Address: i..P, "jj- Proj. Manager: Proj. Location: Proj. Number: Phone # : ' ;;>-;, | :;, Sampler's signature : \P:L^: irAA7.f}.A p3.y\ tAA< P V M''(;; A -i? - ^n\ '•- A. p.. A t \ j \-A,(A. % A o^-A . W;. ^('.",'1 Kjj OKyAi -AA-A / 3 A A A-.ok'.t ( 7 7 ( 3 ) "AAj(,fA' {p{-^\ APf, Faxtt: '-f;')'-^ iu'--;'!._ V j ; , ; / . AA U-.-xkJx _, •A " JJ *C D E :i||p| C1-C4 Hydrogen & Helium Penhkhent Gases (CH4, co, co2, N2,02 ) Mercury (SoU) or (Air ••) TO-14 by GC/MS ( Ambient) or ( Souice •• ) 601 & 602 Compounds W mi :lii W ^ Chlorinated HC BTEX BTEX & C5 - CIO T P H (C5-C10)or(C4-C12) C l l - C18 Specify below. * An additional 22 ml vial of sample is required when requested in combination with another analysis. • • Available upon request. (iiviil.. C < . \ , 'ck<i Vj'iCi>r;'i *'l'?!#wff^'??!lff?w i^. Collection Date Time Number of Containen "Summa" I if Can. uoed Sample Type Sample Identincation Requested Analyses (Other) Remarks H->'?-00 AA/i) A- OiAL A^'-^ t.v;i0.^a- yi Tr.' i i^'i.tyf~: (. •<i^fv^ 7APi 'rA''{iiiA- h I V33 i X:A-^f'(\^i.:. }! . . < Afe't-VV'r-H -V.-4 AAAi'.A, i C • 'I J ! ii,"i'0 PA IfAA- j I - v,j. , ',i ) mo y y'-.Ay'.KA'^- - '-''y. i • • > * 1 f-i-Vfc-o: \ ( j. -'Si-.;. ;.yh(!;i<i -• B. IJpbd A,j'j hr, i K-J - "•• P IteOD - r .-vf.' v' i- iivOb li ''. — » — i^ \u3 Ar P/A -.v^.--\ •• - ^ 7 . Results to : 'lllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllll Relinquished by : . A . ' ' r v & i • A-- ' ;i-\XyM„->..v.... Relinquished by : Relinquished by : l l l l l l l l l l l l I l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l Company : - Un.v,(-.-A\AA.3 Company : Company ; IIIIIIIIII 1 Date : 3nAP) Date : Date : llllllll 1 lllllllll Time : Time: Time: Inyoice to : ZwA At;i^CLOT ' Z . A 3 C . lllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllllll Received by : Received by : Received by : lllllll!lllllini!llllllillllilllll!llllllllllllilllllllllllllllllllllllllllllll!lilllllllillllillllllllllllllll!lllllllli|i Company : Company : Company : Date : Date : Date : Time: Time : Time ; WHITE COPY : Labontory to return. YELLOW COPY : Lshonitorv PtMV cnov . Ci.k.^:*.. j Company Name: Address: j Proj. Manager: j Proj. Location: i Proj. Number: Phone tt: A, c MICROSEEPS, Inc. 220 William Pitt Way, Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 fv'U. i . ( u ? a j \-'-iiiX. -^ A.AAUm:3H7f h A \Aui,i:i^, P\S AVpp A'Ai/C'x Virhi.,T / 3v-si h ( , , ' P 3 - i A \ f i 3 u*- CHAIN-OF-CUSTODY RECORD Note: Emn proper letten in Requested Analyses ciduams below. A n a l y s i s O p t i o n s Note: if analysU D,E,or K u aelected, acnteh (option) NOT wanted. 1 - ^ i t \ Fax#: C AA.UrX\\A\Wl :iW iiii m^ C1-C4 Hydrogen & Helium Pennanent Gases (CH4. co. co2, N2,02 ) Mexury (SoU)or(Air*») TO-14 by GC/MS (Ambient) or (Souice •• ) 601 & 602 Compounds 6 K Chlorinated HC BTEX BTEX & C5 - CIO TPH (C5-C10)or(C4-CI2) Gil - C18 Other Specify below. Sampler's signature : 4^ Cy3...k^. * An additional 22 ml vial of ssn^le is required when requested in combination with another analysis. • • AvaiUble upon request. f H.>^AV>C>llC I'li; 3 7 A ypCAi-^S WHITE COPY : Labontorv to return. Y E L L O W COPY • I^hnr-lnrv Ditjir nriDv . c..k_:~.. Collection Date Tune 3n.-.m i i i i i i i i i i i m i i i m n i . ; • • • • ' ' Number of Comoioen 'A liiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiii "Summa" # if Con. uaed Sample Type ':iC'i4.. 6t"*'- A Ah ' l . v Sample Identification i¥-P-AJ£-P'*\ Results to : IIIIIIIIIHHIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIi Relinquished by : Pj^Aitr- P ^"3.33- Relinquished by : Relinquished by : III IIIIIIIIIII llllllllllllllllllllllllllll Company : Company ; Company : 1 IIIIIIIIIIIIIIIII D a t e : A--]7A-(7) Date : Date : iimniiiiniiiiiiiiiiiiiiiii Time : \r^ip> Time : Time : S-f s fv'-fl iH',/. lu Cf A ' U \ S. ) I M V ' V ! ( \ - \ \ t 11 Requested Analyisi^ < Oth^^) iiiiiiiiP'nii iiiiniiiiiiiii IIIIIIIIIIIIII IIIIIIIIIIIIII IIIIIIIIIIIH A\ rA pAmhf.r • . r X ,(Af.r^. 7^ . <!>At(? Remarks ri:*v,.Yi.(4=>'> lllllllllllllllllllllllllllllllllllllllllll IIIII IIIIIIIIII IIIIIIIIIIIIIIII IIII Illllllllllllllli Invoice to : 3i7P PhAAiiP ySp^c iiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiii Received by : Received by : Received by : llllllllllllllllllllllllllllllllllllllllllllllllllllllllll Company : Company : Company : IIIIIIIIIIIIIIIIIIIIIIIIIIIII lllllllllllllll IIIIIIIIIIIH Date : Date : Date: Time: Time: Time: MICROSEEPS, Inc 9 220 William Pitt Way, Pittsburgh, PA 15238 Phone: (412)826-5245 Fax; (412)826-3433 Company Name: f\Aft^Tt'A / Rg-Vt' Proj. Manager: [V\Kfvy>f, E-IcKim, / T M . . ^ f^qff t ftr (ERlFrC) Prqj. Location: V\/AJ^ J.3a^d Chf'... 'AliP' Proj. Number: '"^ Phone ft: {q r p ) l , H l . t Hi ^ " * = ( P O K \ 1 ' M 7 - R-K>2 Sampler's signature : j'f^ <yiiA.. i^. K-M^.-t^ CHAIN-OF-CUSTODY RECORD Note: Enter pioper letten in Requeoted Analyaea cohimna below. A n a l y s i s O p t i o n s Note: if analyals D,E,or K is selected, acrateh (optioa) NOT waited. •A *B • C D iiiiji lilil Cl -C4 Hydrogen & Heliimt Pennanent Gases (CH4, CO. co2, N2,02 ) Mercury (SoU)or(Air") T O - 1 4 b y G C / M S ( AnAient) or (Source • • ) 601 & 602 Compounds •1 •I ilp iiii Chlorinated HC BTEX BTEX & C5 - CIO T P H (CS-C10)or(C4-C12) C l l - C18 Specify below. * An additional 22 ml vial of sample is required when requested in combination with another analysis. • • Available upon request. f l i V u e v^e / ^ ^'"^''^ t>*:>,Xt;. te. j "fvi-jU ^ i p e A i ^ S Collection Date Tune lU-pAm ^4^ «'';.(> OD \ ] \ t i i r l . 1 A 3 pAil/S ••*i . . " • ' " .'. 'A.'AAA VAA-i': 7A. j ' ' ; i ; (risB t):\0^ bpoo 'iG'>f^> ID H 5 !0^-6 • • Containen . . L V . " '. \ 1 t 1 1 ,! . ^ iiiniiiiiiiiiiiiiii IIIIIIIIIIIIIIIIIIIIIIIIIIIII "Summa" # if Can. uaed Sample Type Svir^as ' i ! • i 1 i .i 4- iiiiiiiiiiiiii'iiiiiiimiiiiiiiiiiiiiiiiiiiiiiiiiii Resulu to : iiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiii Relinquished by : /, Reliivquished by : Relinquished by : Illlllllllllllllll nil lllllllll Company : Company ; Company : .;" r c \iXYa*i^ Sample ' Identification PfpAPP,-\A3 • ^ A A ' i A i •• ^ - P "C'viVlUV^ - T^l- i'.l)isjrK^vai •• ^^'7y .:-A..A!7.-'Z :x.MaV.ii ' M 4 tX-AUnafft'-f • t t H- EYhnuM "M'J ftst-v^'Vf-di^^^zi: ASr-VHf-i|X.-H>v,r ftST-SVE-3 -^H^ fiififiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiriifiiiiiii rP /K r'P llllllllllllllllllllllllllllll Date : Date : Date : imiiimmniiiiiiiiiniiii Time : ' ii.i7''- Time: Time : • '.v.. v^ nr.'i V-vvlS . ac f'Tftn r . IVW' ' l . i i t ' . V - ••illillilliilillililii^ * > • • , > • • : • • • ; • ' IIIIIIIIIIIIII IIIIIIIIIIIIII: IIIIIIIIIIIIII IIIIIIIIIIIIII lllllllllllllll S'f^ 7>irn.o- / t s/^ CMI h t t d c . r i i/in>f-Ar»v^ Remarks •• C.(-^<rv\;AOu o H < 1 . ' - ' lllllllllllllllllll lllllllllililllllllll IIIIIIIIIIIIII Illllllllllllllllllllllllllllllllllllllllllllllllllilllllllllll Invoice to : Toi.e V\t\xe\iyf / E R T E C llllllll iiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiitiiii™ [((Ill Received by ; Received by : Received by : lllllllllllllllllllllllllllllllllllllllll Illllll Company : Company : Company : IIIIIIIIIIIIIIIII Illllll Date : Date : Date : lllllllllllllllllllllillllllilllll Time : Time : Time : o Ol IP WHTTE COPY : Laboratorv to return. Y E L L O W C O P Y r I..hr.r«Inr. vnov n n n v . c..u« MICROSEEPS, Inc. 220 William Pitt Way, Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 CHAIN-OF-CUSTODY RECORD Analysis Options Note: Enter proper letten in Requeated Analyaea cohinms below. Note: If analyais D,E,oT K is selected, scrateh (option) NOT watted. Company Name: M cU'.! Tifvt J-07 f t Address: , ? S 3::y..a^p^ncU'nca., % W 4 U)?lrriJ.>A KH' OlO'5''| Prqj. Manager: ^:!Cv-t\-\i.\ £;jCt->^: i^ / 3oiC.. -f^nre.\ m (t:-^^^tC) Proj. Location: V••io^^'^.- Xsift.-..-t QU P ».•• "^SU^. ..J Proj. Number: Phone<y:/qg^|fcH1.g|» Fax tt: /^jc.g)4-^-|. S'lfeT^-, Sampler's signature : j;-'?.•fet.i.,- K ¥^-(^— •A •B • C D E F C1-C4 Hydrogen & Helium Permanent Gases (CH4, co, co2, N2, 02 ) M e r c u r y ( Soil) or ( Air • • ) T O - 1 4 b y G C / M S (Ancient) or (Source • • ) 601 & 602 Compounds mm mm Ml iiiii 111 WK Chlorinated HC BTEX BTEX & C5 - CIO T P H (C5-C10)or(C4-C12) Cll - C18 Specify below. * An additional 22 ml vial of sample is required when requested in combination with another analysis. • • Available upon request. "I»i ui+?>A<2 , € t i v . j ! b*') .; t'n<i , /.^'f^^u/ 'Xyl'/nt'.J. 1 f -• » K Collection Date Tune u-5>:.-oo 1 1 1 / •1 ] ^ V I S 3 0 s ^ ^ \-7^ po3 \i>3^> t(«50 kSZ. ^^3S |i*'C7 \13I \7iP) r;o2_ —t N u m b e r of C o n t a i n e n 2, pA- y {iliniiiiiiiiiiiiii IIIIIIIIIIIIIIIIIIIIIIII Results lo : H ( ; V m i \ E ' C i \ l V llllllllllllllllllllllillllllllllllllllllllllllllllllllllllllllllllllilll Relinquiahed by : Relinquished by : Relinquished by : i f C a n . u a e d Sample Type S^ar-i-vs ( t 1 V' -^ P>t& Thfqi Sample IdentiHcation •ffp:.yji.:\..'^.{ V'':.hay'v4- - •^^V i3>AAA> \ A,-,^ CA^ j^juA \r-pcAr fff v^^'^-IB fr>s^ Ffp-\jN?-25- f'6iP fPpUU--"7ZA'0S-i FPP wp-ro-P^jsr ppf.yfAf-^S- PoS-t F fp. VW?-3X !^£'5-r FPf-VH/^-3D-p<^Sr pP?-\/HP~HS-F;'S+ . IIIIIIIIIIIIIIIIIIIIIIIIIII I l l l l l l l l l l l l l l l l l I l l l l l l l l l l l l l l l l l IIIIII I l l l l l l l l l l l l l l l l l IIII '. y MctArPi^-./ff'.'r-f- iiiiiiiiiiiiiiiiiiiiiiiiiimiiiiiininiiiiniiiiii! Con^any : Company : Company : llllllllllllllllllllllllllllll Date : Date : Date : iMniiimiMiiiiniimi Time : AAA) Time : Time : A C '-,1- lie , • - . ( - ' - : <•> ^efpne., Wxeih iiiiiillMKliiililKll llllllOPIll IIIIIIIIIIIH IIIIIIIIIIIIII lllllllffl'll'll lllllllllllllll Sitt. T«.rtrc.-t \ \ \ '%k iiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiii "t-.tr- Ptrid.. i Ch( ;..'V?.>-f'-0 r iA^ Remarks 0 c i r t . . . ^ D u ' ' \ . : | 3 Invoice to : iiiiiiiiiii IIIIIIIIIIIIII iiiiiiiiiiiiiiimiMiimniinini Received by : Received by : Received by : iiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiii Company : Company : Company : iiiiiiiiii 1 ii|iiiiiiiiiiiiiiiiiiiiiiiniiimi] Date : Date : D a t e : T i m e : T i m e : T i m e : WHITE COPY : Labontory to return. YELLOW COPY : Lahontnrv piiMV r n n v . «..k_:H.. MICROSEEPS, Inc. 220 William Pitt Way, Pittsburgh, PA 15238 Phone: (412)826-5245 Fax: (412)826-3433 CHAIN-OF-CUSTODY RECORD Company Name: Mct-ft5"<ei'^ / H a ' " " * " Analysis Options Note: Enter proper letten in Requested Analyaea cohumu below. Note: If analyna D,E,or K is aelected, acrateh (optioa) NOT watted. Proj. Manager: ^J. ov-yy.a. f„tC\A iW. / T o S * - R<%re I j-.t (i. RT£f^ Proj. Location: Proj. Number: •^::t-<xv^-^ Z£-.'3a-<\A Ct^'.^'i,-^ ' y i T Phone tt: ^^,y^^\fe H - ^ . . ; ? ! ! ) F'^^ = C'^A^Hm-g\c-.-2 • A *B • C D E F C1-C4 Hydrogen & Helium Pennanent Gases (CH4, co, co2, N2,02 ) Mercury (SoU) or (Air ••) TO-14 by GC/MS ( Ambiett ) or (Source •* ) 601 & 602 Compounds •1 111 i ^ l l iiiii iiiiii « Chlorinated HC BTEX BTEX & C5 - CIO T P H (C5-C10)or(C4<:i2) Cll - C18 Specify below. * An additional 22 ml vial of sample is required when requested in combination with another analysis. Sampler's signature : Collection Date Time MV>-OC H--3€*s |i|IIIIIIIII|i!i|||l!l H r M \m^ ,f Illlllllllllllllllll P(\M« , Number of Containen 0- 4-.-: Kv-i< "Summa" t if Con. uaed 'Illllllllllllllllllllllllllliiiiiiiiiiiiiiiiiiiiiii 1 Sample Type PvPieaS ^ S'lif. Sample Identification fpp-vHs^-Hx- (-''> si FPP-VMP-M'r>'pA"i+ lillllllllllllllllllll IIIIIIIIIIIIIIIIIIIIIIIIIII 1 iiiiiiiiiiiiiiiiiiiii Results to : / lllllllllllllllllllllHlllllllllllllllllllllllllilllllHIllllllllllllllll Relinquished by : ,V }. i -../.-. r -/' -A. .A'. Relinquished by : Relinquished by : lllllllllllllllllllllllllllllllllllllllllllllllllllll|lllllllllllllllllllllllllllllll Con^any : Company : Company : Date : A- ^ 7y . Date : Date : lllllltlllllllllllllllllllllll T i m e : T i m e : T i m e : Available upon request. Reipested Anftlyis^ <Otfa^> IIIIIIIIIIIIII IIIIIIIIIIIH IIIIIIIIIIIIII IIIIIIIIIIIIII lllllllllllllll Si+e JarvfQ ^ ^ 2 e-vu:-., P>A^ " r v » Remarks + C o t ' i , lOiJu n d S 1 • llllllllllllllillllllllllllllllllllllllllliiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiii iiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiii Invoice to : iiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiifiiiiiiiiiiiiiiiiiiiii Received by : Received by : Received by : iiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiii C o m p a n y : C o m p a n y : C o m p a n y : IIIIIIIIIIIIIIIIIIIIIIIIIIIII D a t e : Date : Date : lllllllllllllllllllllllllllillll. T i m e : T i m e : T i m e , : WHrrp. rnpv • t .Knr.tnrv m »•«..« vet I n w rrinv . r .i.._.— p o VVilliaA Pitt WWlE^fsbj^r^/pA 1^38 Phqne: (412) 826-5245 / Faw' (412) 826^433 A / / / ' • / . ' • ' ^ / A^7cU«;.^/Hi,rA P\ I fpcTo [}(yc- CHAIN-OF-CUSTODY RECORD Analysis Options Note: Enter pioper letten in Requested Analyaea columns below. Note: If analysis D,E,or K is selected, scnteh (optioa) N O T watted. Company Name: Address: 7P7^ T A A r r f i e J e ^ ^ / P l i j 3 . L/A/TeA P J J Proj. Manager: Mar/r\o. B f a h l/r. Proj. Location: !/./&/A T ^ / o r t d C 7 c . m c ^ / 5/-7^- Proj. Number: Phone tt: Sampler's signature : Vy Fax* x/PM iiii Wk iffl • w C1-C4 Hydrogen & Helium Permanent Gases (CH4, co, co2, N2,02 ) Mercury (Soil) or ( Air •• ) TO-14 by GC/MS ( Ambiem ) or (Source •• ) 601 & 602 Compounds * An additional 22 ml vial of sample is required when reque * * Available upon request. i l l Chlorinated HC BTEX BTEX & C5 - CIO TPH (C5-C10)or{C4-C12) Cll - C18 Ililli Specify below isted in combination with another analysis. W H r r E COPY : Laboratory to return. Y E L L O W COPY : U b o n t o i y PINK COPY ; Submitter Collection Date Tune 7)-AlOO \ i A llllllllllllliiiiiiiiii /v;v3 iH'.-hi l i i S ^ pAO'o )CA)0 ic'.oX /^•,A0 i'i 7 0 i-i7S A6'.73 %o:il M'-lT. Illlllllllllllllllll Number of Containen / / / / / / / • / J I / I IIIIIIIIIIIIIIIIIIIIIIIIIII "Summa" f if Can. uaed Sample Type So/lCc^ \ \ \ 1 '•> V Sample Identification A5T.50B7,- BA3a TNLBX" 8A^F JEYPAb5T' 8AS£ A5r6UE7i~ / . 5 Z^LBT- XS ^^LPAO^T - A S A6rp)U£3' s . o X/^L^7'' 3 . 0 ^XpA05F' 3 . 0 3675 y e t - SAP) riHLar' ^.0 £x/7Aapy7 - 6 , 0 I I I I I M I I I I I I I I I I I I I I I I I I I I M I I I I I I I I I I I I I I I I I I I I I I I I I I M I I I I I I I I I I I I I I I I I I I I I I I I M I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I '^""'"°-' P/ortr^o. B/c/tliA - H c U i ^ ^ / ^ a d IIIII llllllllllllllllllllllllllll Illlllllllllllllllllllllll Relinquished by : , AijA Relinquished by : Relinquiahed by : lllllllllllllllllllllllllllllllllllllllllllllllllllll Company : Company : Company : llllllllllllllllllllllllllllll Date : Date : D a t e : lllllllll IIIII Time : Time : T i m e : Rei^uested Ai^yses < Oth^} IIIIIIIIIIIIII IIIIIIIIIIIIII IIIIIIIIIIIIII • IIIIIIIIIIIIII IIIIIIIIIIIIII 5//t7Sr<,«/J i ^ Remarks "o^n/^ooy ci> iiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiii I n v o i c e t o : ^ ^ ^ IIIIIIIIII Illllllllllllllllllllllllllllllllllllllllllllllllllllllllllll Received by : Received by : Received by : iiiiiiiiiiiii lillllllllllllllllllll IIIIIIIIIII Company : Company : Com{iany : llllllllllllllllllllllllllllll mil IIIIIIIIIIIIIIIIIIIIIIII Date : Date : Date : Tune : T i m e : T i m e : (JJ o cn M M Ot 3/73/06 Pa^c /o73 ESS'^F MOBILE LABORATORIES PROGRAM Field Services Division - Warren, N7 N9 03205 CHAIN OF CUSTODY RECORD f O n LABORATORY USE ONLY Latwratbry Project No.: A - -' . Storage Refrigerator ID: '..' • Storage Freezer ID: ___^ Secured: Yes No Proiect Name; - i - ^ fiwi CK.£»w>«. Relinquished by; {Slgnalur* and Prinlad Nan>«) Relinquished by: isignatuo and Piimad Namal Relinquished by; ISignalura and Pnnix) Namal Relinquished by: (Slgnalura and Printad Nama) Project #: Samoler: H e c e i v e a Dy: ISijnatura and Ptinlad Nama) R e c e i v e d by; (Signalura and Pnnlad Nama) R e c e i v e d by; (Signaluta and Prinlad Nama| R e c e i v e d by; ISignatura and Primad Namal (PiinMd Namal Date: Date: Date: Date: (Slenatural Time: Time: Time: Time: —— Fixed Based Location: 1 <n Ml nxh^l Q A Warren. NJ 07059 (908) 604-8900 1(908)604-2352 Sample ID Number 1 11 2 3 4 5 6 7 .8 . 9 10 MT-ivf-l ^n^P-):^^ - 1 ^ - c 2 5 --2 1 - ; ? b - S S -311 . -3i> ]/]/ -V5 Method of Shipment: Shipment ID: Sample Description Date yjiyloo \ 1 Time l i o 7 lOH i j ' / r 1.318" pao i^:^<7 p^o , 3 ? ^ p36 13^3? Description / ^•>l^t/M>OfL/lMft. > ( \ \A ADalysis(es Requested A / ' / / ? ? ? ? ? ? ' / ' / ? ' / ' / A V, Z a) Identify specific metals / / / / / / / y A / / / / / / / / / / y ^ / Instnjctlons A A A A A A A A A A A A A A A A A A 7 7 4^///////////////// c )/ . / / /TAT « \ j ontalner(s) '^*'ffl # \ \ J - - i-^^ FOR LABORATORY USF ONLY Lab ID • / - / • • - / — - • / / / - - - •• / / / ' • • • - • / - / - - : - - / - — / -/--:-y-^-:-- • - - / • / • • • • • • • ¥ • • . - . • • • • • • • / : / ' • / — : • / / • • • • / • • / / • / -7 / — / Special Instructions/Comments:. Sample Archive/Disposal: n Latxjratory Standard D Other FOR LABORATORY USE ONLY. Sample Condition Upon Receipt: TAT (Analytical Turn-Around Times) i • 24 hours 2 > 48 houra 3 - 1 week 4 > 2 weeks Container Types: B^BrassTube, V-VOA Vial, A« 1-Liter Amber, Q-Qlass Jar, C-Cassette, O-Other 'V^l>\.f» Qi^C SEND DOCUMENTATION AND RESULTS TO (Check one): D Project Manager/Office: - • D Client Name: ' • ' - • Company: ,__ ' •' •"•••;.' • • ' Address: • '• • '•• •. "•;'.-'••.:•' • ^ ; - • Phone: ( ) -;/•• ••• .•;;;; '.' • Tax:: ;•: O tJl M M K T W ^ M ^ H y ! ^ MOBILE LABORATORIES PROGRAM N9 03205 Field Services Division - Warren, NJ CHAIN OF CUSTODY RECORD FOR LABORATORY USE ONLY Laboratory Project No.: • Storage Refrigerator ID: u . _ _ _ Storage Freezer ID; Secured: Yes No. . Project Name: X s U ^ < i CWet^^c^l Project #:. Sampler:. Heceive^yMSiJialu'^Bn^^l'tladNamal (Pnnla<) Namal Date: ISIgnalura) Tf Relinquished by; ISignalura and Primed Namal ime: R e c e i v e d by; (SIgnatura and Printad Nama) Data: Time: Relinquished by: ISIgnalura and Prinlad Nama) Date: Time: Relinquished by; (Stgnatura end Pnmad Nama) R e c e i v e d by; ISIgnaura and Primad Namal Date: Time: Relinquished by; (Signalura and Pnntad Nama) R e c e i v e d by; (Signauira and Prinlad Nama) Fixed Based Locatioi i: Wdrren, NJ 07059 (908) 604-8900 (908) 604-2352 Sample ID Number 7^7 / 2 ^mP-'^X J , - w r ^ 3h l^ ' ^ 4 5 6 A$r5Q^ I AsrvPP/T h5nMPiD_ 7 bTDHPTO 8 9 10 TibnPIPTX AsrudP^D AbnPI?35 Method of Shipment; Shipment ID: Sample Description Date S\P3)X > / •3137) ( i>- Time \n^ laix {?-7^ m t 7 I%'.i7 )VP IV77(^ n.77> 1^.19 IVIB Description / Vffoz. / Ai e — ' —r— 4^ ^a^flhrA 1 1 • / V N Analysis(es) Re<iuested / / ? / "} V ' / . ? ' / . ' / . ? ^ ' / . ? ' / . y. / / Z / / / / / / / / / / / / / / / / / ^ ^ ^ / / / / / / / / / / / / / y / / jA y / J ^//////////////////ZT / i y • Container(s) « \ I 4^ .•.!*r^' TyPf PA O \ / 1: ^.,.r A a) Identify specific metals requested under Spedal Instructions FOR LABORATORY USE ONLY Lab ID • • • • • • / • • • - • / - • / — - / / - / - • / / • / • • — • • / / • / • • • • • • • / / • • - • • • / • / - - - / - - - / / - / • / • • • • • • • / • • • • / • • / • • - - / - - H - - / - / • / • • • • • • • • • • / Special Instructions/Comments:- Sample Archive/Disposal: n Laboratory Standard D Other FOR LABORA TORY USE ONL Y. Sample Condition Upon Rocoipl:. TAT (Analytical Turn-Around Times) 1 - 2 4 hours 2 - 4 8 hours 3 - 1 week 4 « 2 weeks Container Types: B-Brass Tube, V-VOA Vial, A-1 -Liter Amber, Q-Qlass Jar, C«Cassetta, O-Other -TCA^^ o^<^ SEND DOCUMENTATION AND RESULTS TO (Check one): n Project Manager/Office:; • '/••''. ': D Client Name: •'• ''A -' ' A ^ • Company: • • • • / - " A / p ' ' - .,. Address: • • ' • •' •' ' •••-y''A':-7' -' ^ • Phone: I ) - -7'----': " ; ' ' ' ' ; - Fax: CO o cn H H 00 • A A .•A..'AM'ik-Ai!&A.AA:y^i,-. / A s AO Paa,e 3<^3 , / CHAIN OF CUSTODY RECORD MOBILE LABORATORIES PROGRAM F i e l d Services Division - Warreri, N J ? 03205 FOR LABORA TORY USE ONL Y Laboratory Project No.: Storage Refrigerator 10: Storage Freezer ID: Secured:: Yes Na Proiect Name: R e l i n q u i s h e d by; (Slgnattjra and Printad Nama) Relinquished by; (Signatuta and Priniad Namal R e l i n q u i s h e d by; {Signalura and Printad Nama) R e l i n q u i s h e d by; (Signalura and Printad Nama) Project #: Sampler: H e c e i v e d by; (Slgnalura and Printad Nama) R e c e i v e d by; ISignaltxa and Pnnlad Nama) R e c e i v e d by; (Slgnatuia and Printad Nama) R e c e i v e d by; (Signalura and Piintad Narrta) (Piintad Nama) ' Date: Data! Date: Date: (Slgnat»a| Time; Time; Time: Time: Fixed Based L.ocatior l < n kit* D « * h « l TtA : Warren, NJ 07059 (908) 604-8900 1(908) 604-2352 Sample ID Number pTisrmPp/x ^\ASPDPlP3P 3 AuruTfP^P P 7167 \! PIP HZ 7 8 9 10 A^np/pMD Date 3l73> 1/ Method of Shipment: Shipment ID: Sample Description Time lis'3/ l<i.7$ 1^.34. /9'39 l<s'HX Description ]la.fi.=( l A i f \ / V ADalysis(ei Requested / ' / ? ' / ? ? / ? ? ? ? ? ? ? ' / V, / / / / a) Identify specific metals / / / / / / / / / / / / / / / / / / / A y j y y y y y y y y y y y y y y y y y y J /y/////////////////Zt \ • " / ContaJner(s) „f, • ••'vi« Tvoe •; iffjl,'. FOR LABORATORY USE ONLY Lab ID — / -A---f-.-:.. : • • • • • • / • • • / . . . . . . . . / • • • : • . . • • • / / • • • • - / • . , • . . • : • / - / - - - • / - ^ • . - > - .......:/ J........ .A..:..... P A ••/••••••'• / ./.......'A... / / / / --/--.-^-A-:-.- ^ / • • ' / - / - • • : - - / - - / ; • • / / • : / / Special Instructions/Comments:. Sample Archive/Disposal: G Laboratory Standard D Other - FOR LABORATORY USE ONL Y. Sample Condition Upon Receipt: TAT (Analytical Turn-Around Times) 1 - 2 4 hours 2 - 4 8 hours 3 -1 week 4 - 2 weeks Container Types: B-Bras8 Tube, V-VOA Vial, A-1 -Liter Amber, Q-Qlass Jar, C-Cassette, O - Other • . - . ' , ' ,. SEND DOCUMENTATION AND RESULTS TO (Check one): D Project Manaoer/OfHce: • ._^ D Client Name: " •' -A. :A-' • . ^ ^ Company: ; •• • • " ' •".••"'- '''-_'. / Address: '• ' ' ' '--' ' • '-AAAA/A.. . PfHjne: _L J_ -F«. CJ o cn vo .K..kii'niSja;fei*;!?a4&&*;iiS.Si^^ ;,',i^.<2Liiu<>k ESS«F 3)7,7/do PkAdoac. CA:A7X MOBILE LABORATORIES PROGRAM Field Services Division - Warren, NJ N? 03205 CHAIN OF CUSTODY RECORD FOR LABORATORY USE ONLY Laboratory Project No.: - - • Storage Refrigerator ID:_ Storage Freezer ID: ' Secured: Yes No Proiect Name; "XsltiAif L l ^ e \ ^ \ c A Relinquished by; iSignatura and Printed Nama) Relinquished by; (Slgnalura and Pnnlad Nama) R e l i n q u i s h e d by; iSignatura and Pnntad Nama) R e l i n q u i s h e d by; (Signature and Printad Nama) Project #; Samoler: H e c e i v e a b^. (Signature and Printad Nama) R e c e i v e d by; (Signature and Printad Name) R e c e i v e d by; (Slgnaluta and Printed Name) R e c e i v e d by; (Signature and Printad Nama) I (Printad Name) Date: Data) Date: Date: Time: Time: Time: Time: Fixed Based Location: 14n XA. D.»k.l D.I Waircn, NJ 07059 (908) 604-8900 1(908) 604-2352 Sample ID 1 ;AsT'5Vi'-i 2 AiT-jive-l 3/|iT--SV6~lA 4 5 6 7 8 9 10 Method ol Shipment: Shipment ID; Sample Description Date ^|p^ '1 J/ Time Ci-^:> rXiP 17. V9 Description ^ c \ \ t,iA5 \ ' -.* Aiialysis(esJ Requested / P ? / / ? ? ? ? ? ? ? ? ? ? 7. / VV a) Identify specific metals 7 / 7 7 7 7 7 / 7 7 7 7 7 7 7 7 7 7 7 7 ro^osteo unoer opooai 7 / ^ / / / ^ / / / / / / ^ / 7 / / / / / / / Instructions / / / / / / / / / / / / / / / / / / / / / / / / / / / / / / / / / / / / / / / / A//////////////////AT A I- . / Contalner(s) # V • i N ''^VM <rf i ; . ; ' • ' FOR LABORATORY USE ONLY UbID - • / / / - — / • / • • • • / • •• / -/-^ / : • • • - / / • • • / • • • • - / / / — / - / - : - : - / - - - - - - / - - - : - / / / / - • / • - - ^ - / - - - / / • • • • • • / / - ^ / Special Instructions/Comments:. Sample Archive/Disposal: '^^'^ (Analytfcal Turn-Around Times) 1-24 hours 2-48 hours 3 -1 vwek 4 - 2 weeks Container Types: B-Brass Tube, V-VOA Vial, A-1-Liter Amber, Q-Qlass Jar, C-Cassette, O - Other " V e ^ ^ f i ^ 0 ^ 0 D Laboratory Standard D Other FOR LABORATORY USE ONLY. Sample Condition Upon Receipt: SEND DOCUMENTATION AND RESULTS TO (Check one): D Project Manager/Office: ' • . D Client Name: • -• : - 7 Company: • - / • ''•'' ; Address: .- A '/•' • ' '• CJ o cn H» to o Phone: _L J- Fax: ^ W F MOBILE LABORATORIES PROGRAM Field Services Division - Warren, NJ N9 03205 CHAIN OF CUSTODY RECORD FOR LABORATORY USE ONLY Laboratory Project No.: Storage Refrigerator ID: Storage Freezer ID: Secured: Yes No Proiect Name; ! H i 'u>xJ C K £ w i c c a R e l i n q u i s h e d b y ; (Signature and Primed Nama) R e l i n q u i s h e d b y ; ISignatura and Printed Namal R e l i n q u i s h e d b y ; ISrgnalura and Printed Namal R e l i n q u i s h e d b y ; (Signature and Printed Name) Project #; Samoler: MecetveO by; (Signature and Printed Name) R e c e i v e d b y : ISignalure ana Printed Name) R e c e i v e d by; (S«nalure and Printed Namal R e c e i v e d by: (Signature and Pnntad Namal (Pnntad Name) - Date: Data: Date: Date: Time: Time: Time: Time; Fixed Based Location: i<n iL4t a . t k . i DA Warren, NJ 07059 (908) 604-8900 1(908)604-2352 Sample ID Number 1 '^v:.T-5\;e -1 2|A5T-j,vr-i 3 4 5 6 7 8 9 10 (KT-->Vin/^ Method of Shipment: Shipment ID; Sample Description Date TI^S^O 4" Time 7:'yj '•''5.V ns'p Description SctJ <'r^:> >. y Analysis(es) Requested / ' / / ' / ? ? ' / ? ? ' / ? ' / ^ ? / 7/ y7. / a) Identify specific metals / ^ / y / / ' / / / ^ / / / / / / / / / / y A y instructions / / / / / / / / / / / / / / / / / / / / A ^ / / / / / / / / / / / / / / / / A A v<. p . / / ^ / Coritainer(s) /TAT ^ ' • . • Typ^ 3/ \ \ V- • A -•: f FOR LABORATORY USE ONLY UbID / / / • : • • • ; ; • • • • • • / -/--.-/--A / - / - - : - / - - , • / 7 •/-:-:•: / - / - - - : / - : - - / / - / - - ^ / / - - - : - / - : : : : : - / / • ' / / / - - / / / • / Special Instructions/Comments:. Sample Archive/Disposal: D Laboratory Standard n Other FOR LABORATORY USE ONLY. Sample Condition Upon Receipt: TAT (Analytical Turn-Around Times) 1 - 2 4 hours 2 - 4 8 hours 3 - 1 week 4 - 2 weeks Container Types: B-Brass Tube, V-VOA Vial A-1-Liter Amber, Q-Qlass Jar, C-Cassette, O-Other -TThUH. P,4o SEND DOCUMENTATION AND RESULTS TO (Check one): n Project Manager/Office: ; D Client Name: : Company: • • • :'.•:' Address: - '• ' ' / A Pfione: ( 1 .'''• • . • ' ' . • • Fax: CJ O cn M lo ^sm /A<>Pooc. 3/^^/00 M CIciren MOBILE LABORATORIES PROGRAM cirC Field Services Division - Warren, N J 0 ^ ^ N? 03205 Vr CHAIN OF CUSTODY RECORD FOR LABORATORY USE ONLY Laboratory Project No.:' Storage Refrigerator ID:.; Storage Freezer ID; _^ Secured: Yes No Project Name: (Jifbyy\ "XTJ lanri P}\.ei^ta3 Project #: Relinquished by; IS^natura and Printed N«nal y ^ P ^ J / ^ / ^ / J ^ A Q O 7 ^ ' OO ^eceiveSIByn&gnatuSTi^rinledNamel Sampler: I A O ^ H T ^ ^ A A T - U P I ' (Printa^ama) Date: bata; (Signalura)" Time R e l i n q u i s h e d b y ; (Signature and Prinlad Name) ^ / ^ R e c e i v e d b y ; (Slgnetura and Prinlad Name) Time! bate: R e l i n q u i s h e d b y ; (Signature and Printed Name) R e c e i v e d b y ; (Signature and Printed Name) Time Time R e l i n q u i s h e d by; ISignatura and Printed Name) R e c e i v e d b y : ISIgnatuca and Primed Name) Date: Fixed Based Location: Wanen, NJ 07059 (908)604-8900 (908) 604-2352 Sample ID Number '\A&r3o^l "'/^pp/iP/J i^TOPlP/V 'A^u/fpj^ ^hrmFTo: ^Wy/iF^^ y^i//iP^5 ^,wmP3T ^7bru/iP3D ^^hfl/p/PH5 Method of Shipment: Shipment ID: Sample Description Date d j ^ A 3(71P ^A=r ^ 3/^C 3lM SiTiC ^IM £l74 Time %'.n ^79 ^:7.l i-2H i'.7a f-jK 'BAA' 'i<3i r:59 t^iS Description vS>y Go.5> \ . . \l J Analysis(es] Requested / / ' / / T ? ? ' / ? ? ? ? ? ? ' / 7. / 7 a) Identify specific metats / ^ / ^ / A A A / / A / / / A / / / A / / ^ / Instructions 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 - 7 7 7 7 7 / / \ 7 / / / / / / / / / / / / / / / / / d /y//////////////////,, X X X X X X K X X X . : . - . • A Container(s) IP -H TVM ' - " • • • - - ' • FOR LABORATORY USE ONLY Lab ID • • • • • / / / • - • • • • • • • / • • / / - ^ - - • • / ^ - / ; / • — • ^ / - / / • • ; - • / / v / - ^ - - : / • / • • — / - • • • • • • • / / • • • • • • • : / - • ; . / • ; / - / • • • / - ' • • / - / • • - - - / - - - - / : - - / Special Instructions/Comments:. Sample Archive/Disposal: D Laboratory Standard D Other FOR LABORA TORY USE ONL Y. Sample Condition Upon Recoipl: TAT (Analytical Turn-Around Times) 1 > 24 hours 2-48 hours 3-1 week 4 - 2 weeks Container Types: B-Brass Tube, V-VOA Vial, A-1-Liter Aimber, Q-Qlass Jar, C-Cassette, 0-Other ; SEND D(X;UMENTATION AND RESULTS TO (Check one): n Project Manager/Offtoe: ' • ' ^ ' D Client Name: ' •'-^'- ' • ' ' Company: ;•'•-•-;. -A/ ' Address: ] ' A-^- •':''• :•'.'- Phone: ( J ; ' . ' , ''• y'-'-'Fax: O cn l-> t o t o KTW^ MClcif^n MOBILE LABORATORIES PROGRAM y \A m 1 tlctrC Field Services Division - Warren, NJ CHAIN OF CUSTODY RECORD N? 03205 FOR LABORATORY USE ONLY Laboratory Project No.: • Storage Refrigerator ID:; Storage Freezer ID: Secured: Yes No \ . y • ^ IPrinledNi^l ISkinalucal R e l i n q u i s h e d by; (Signature and printad ^ ^ " ^ ^ r < p 7 / ' t A R e l i n q u i s h e d b y ; (Signature and Printed Name)^^ R e l i n q u i s h e d by; (Signature and Printed Namal R e l i n q u i s h e d b y ; (Signature and Pnnted Name) 3jp/'^ :?hjAxi' J A D y y \ H e c e i v e a by; (Signature and Printed Name) R e c e i v e d by; (Signature and Printed Nama) R e c e i v e d by: (Signature and Primed Namal R e c e i v e d by; (Signature and Primad Nama) Date: Datej Date: Date: Time: Time: Time: Time; Fixed Based Location: Wanrn, NJ 07059 (908) 604-8900 (908)604-2352 Sample ID Number ''/^pu7/P'Pi: "^•M/AP^T) 3^57mP^77 4 5 6 7 8 9 10 Method of Shipment: Shipment ID: Sample Description Date '3/pt.C 7>iP^, 3lS!£ Time ^13?- 5W-2 <3 3t> Description PXA \l/ Ana]ysU(es] Requested / ? / ? ? ? / ' / . ' / . ' / ' / ' / ' / ' / / y. / 7 a) Identify specific metals / / / / / / / / / / / / / / / y / / / / Instructions / / / / / / / / / / / / / / / y / / y y y X / / X X X y X X X X X y / X y A y > A///////////////////,, K K > . ' . -A ' . . Conlalner(s) # , u. TVD^ . . > ! • FOR LABORA TORY USE ONL Y Lab ID / / / • • • • • • • / / / • • • • - • / • / • / ^ / / ^ • / — / • / • • / / / • • • / / • • • / • • • - • / • • • • • - / - • • • / • / • • • • • / / / • • • • / / • / Special Instructions/Comments:. Sample Archive/Disposal: n Laboratory Standard D Other FOR LABORATORY USE ONLY. Sample Condition Upon Receipt:. TAT (Analytical Turn-Around Times) 1 - 24 hours 2 - 4 8 hours 3 -1 week 4 - 2 weeks Container Types: B-Brass Tube, V-VOA Vial, A-1 -Liter Amber, Q-Glass Jar, C-Cassette, O - Other SEND DOCUMENTATION AND RESULTS TO (Check one): D Project Manager/Office: -_ D Client N a m e : _ _ , , . / • - ' - , Company: v__ .""•• . - - Address:. '•-.'. . .-.. ^' ..• - - Phone: ( > •.": .-i "- ' -- Fax: UJ O (Jl M to CO ESS WF Prt<5t \ S ^ MOBILE LABORATORIES PROGRAM Field Services Division - Warren, NJ N? 03205 CHAIN OF CUSTODY RECORD FOR LABORATORY USE ONLY Laboratory Project No.: • Storage Refrigerator ID: Storage Freezer ID: Secured: Yes No Project Name; \/i£.g,iJ l6LOMr^ L H S M I U Q U Project # Sampler: _Nla£MSi£cJdLl.fcL Printed Namal _M^a M ^()^j.1L Special InstructionsyComments:. Sample Archive/Disposal: D Laboratory Standard D Other FOR LABORA TORY USE ONL Y. Sample Condition Upon Receipt: TAT (Analytical Turn-Around Times) 1-24 hours 2-48 hours 3-1 week 4 - 2 weeks Container Types: B-Brass Tube, V-VOA Vlal, A-1-Liter Amber, Q-Qlass Jar, C-Cassette, O-Other . SEND DOCUMENTATION AND RESULTS TO (Check one): n Project Manager/Office: , • .-^ • , D Client Name: • " • ' --. .-: A : - - ' Company: , • ••: ' -• '7p'-A -. ' Address: '• • •• . ' A; '/'•"•/^AA-'. / ' Phone: ( ) '' •;. ^ T '/.-AAA'pi.Fix: ' U) o cn to A i j-rf'ifeSfei •itJ;!.i;;i>iH!i' ^im 6, CIciren MOBILE LABORATORIES PROGRAM cirC Field Services Division - Warren, NJ 2 0^3 N9 03205 CHAIN OF CUSTODY RECORD FOR LABORATORY USE ONLY Laboratory Project No.: Storage Refrigerator ID: Storage Freezer ID: • Secured: Yes No Project Name: Aiex-,,\ri \<^~.i lq^^lr^ ljK€MIPi^) Project #;. Sampler:. n q ^ l y e d ^ ; ( S . n a ^ ^ P r | . a ^ N a m ^ ^ M ^ O f U ^ P . n H , , A r\Qii\shea'tn: iSignatute and Pnnlvd Nama) TTeceiveSTTMSionatuiTandPTJ^^ R e c e i v e d by: (Signatura and Phniad Nama) (ftrinfdfama) '\7avryn. ( p ^ ^ T ^ °^'°^'Ml4oo ;["^°^ ie,Or) Date: Date: Relinquished by; (Signature and Printed Name) R e c e i v e d by; (Signature and Prinlad Name) Time: Relinquished by; (Signature and Printed Name) Fixed Based Location: 1 50 M l Rethel Rd Watren, NJ 07059 (908) 604-8900 (908) 604-2352 Sample ID Number - •• :fl-sr-VMP-2X - 2j,:^.VMp-3:l. ' 3^T-VMP-m •• '»ter-VMP-\D "• 5Jfl^..SVE.( ~ 8 7 8 9 A=r7-\)MP-:^' Samp Date H Jcoo PlLo^. M l tec M/t-6Ci '^•)(,•(X^ D '^ Ikct Time 17?,^ 1723 17)7 1739 tmz nz\ Method ol Shipment: Shipment ID; le Description Description pMoSf.T PHR.'=)fnr; PH(\'O(-:.ZSL PNttStTC PHG^ZK. pMA6e.TT. R e c e i v e d by; (Signature and Printed Name) D a t e : T i m e : Requested / ^ / / / / / / / / / / / X / / / / / / a) Identify specific metals / 4J/ A A A A A A A A A A A A / / 7 7 / / ra«|uesteo unoer special / ^ ^ / / / / / / / / / / / / / / / / / / Instructions XCA^r / / / y X y y X / / X y X X y / / X / Y ^ X / X X X X / X X X X / / / / / / / /^f/////////////////A, 7 A J A J y <?( imni n Arr -hlvfi /nk nnsB 1- • TAT (Analytteal Tum-Around Times 1 i ' • Contalner(s) # 1 1 1 1 1 1 -p'-t- - 24 hourt """"PI Gfl5 3 - ' • . • . - : . - \ I FOR LABORATORY USE ONLY Lab ID m\'P-3y^%/- /••••••• mftPoi'i-P /• M-fiiPm}^--!/^^-^^^--- OM-;y^'0Mk-/6'qA"/"'- cym^^t^^Z-cv^r-/--- MA'y^--n^--a?H/- • • • • / • - - / • / • : • / - ^ - : - : - / - ^ - - - / :/ ,./ /...,... / / / 2-48 hours 3 -1 week 4 - 2 weeks Special Instructions/Comments:- D Laljoratory Standard D Other FOR LABORATORY USE ONLY. Sample Condition Upon Receipt:. Container Types: B-Brass Tube, V-VOA Vial, A-1-Llter Amber, Q-Qlass Jar, C-Cassette, O-Other •_ SEND DOCUMENTATION AND RESULTS TO (Check one): D Project Manager/Office: ^ D Client Name: ^ ^ '• '•'-[•' ' Company: ^ . .,/. :7:7 - - - Address:. Phone:. ( ) j & i i i i s * Jj^f^ili,;' P 7 7 A p i : • • ' - ' • • ' ; - - - ^ : ; * ; : - > a x : - • • 3 3 P 3 ' : p : : 3 . 3 ^ :: „.•;., . • . , . . • li•:^/!^i7^ii^3Mp••:MPA3i^3j7'':•A:.y •.:, . .. >..p. :7^r\.lJtfi .•d.PtitiaiA CO o cn to cn KSWF MOBILE LABORATORIES PROGRAM Field Services Division - Warren, NJ N9 03205 CHAIN OF CUSTODY RECORD FOR LABORATORY USE ONLY Laboratory Project No.: • Storage Refrigerator ID: Storage Freezer ID: Secured: Yes No Sampler: ^'^'^:f^ ^ f , ^ ^ ^ ^ Aj^nrry^n . 7 ^ / ' ^ ^ J ^ A . '""'•^''•"•' Bate:/! J T T " Time: Project Name; \Ji&fc.)f4 I 5 L Q M D LHgM^^Ln(- Project #: R e c e i v e d by; (Signatur^n^rtntefl^ame) Wp^3^Zt\ ire ind Printed Nama) hL £±m_ P^^<r^ Ll 4 M I60O •geSe^ H3Q R e t i n c ^ u i S h ^ by; tSignatura and Printad Namal R e c e i v e d by; (Slgnalijre and Printed Namal Date: Date: "Tlrneir^^^ T l ^ ime: Time: Relinquished b y ; iSignatura and Printed Namal R e c e i v e d by; (Signature and Printed Name) Date: Relinquished by; (Signature and Pnnted Name) R e c e i v e d by: (Slgnatuia and Printed Name) Fixed Based Location: K n M i n»>h.i Drf Wanen, NJ 07059 (908)604-8900 (908)604-2352 Sample ID M^5T-6vill-*l 2 3 4 5 6 7 8 9 10 A^-SV<£2-'I RST-VIAPIX-- etCtAfiU'-M ^ 1 IMTOHJS.* 1 '^iuP,cf.n-*2 iNJTflliJi * 2 //sTTfltiA 7) & . M R L ) 6 T "3, Method of Shipment: Shipment ID: Sample Description Date HKJOO "1 i 1 1 MigcG "^.(500 Mlfc.OD ^•Itoc Time il50 MMO 1125 lOMO )0^6 2o2o 2^25 JHQf^ iii.6 Description Pmt^AS^ \ / Pi-(«6^. 3J1 '( '' pHflfjf. :iL pHROe. X AnalysU(es Requested A, ^ w~ ? ^ / ? / ' / / ? ' / ? ' / / / y > ; / z / a) Identify specific metals / . ^ ^ / / / / / / / / / / / / / / / / / / io«|uosnKj unaer opeciai -; / / ^ / ^ / / / / / / / y y y y / / / y y / Instructions / r ^ X / / / / / / / / / / / / / / - / / / / / '7 / / / / / / / / / / / / / 7 / / / y /f/////////////////A 7 A A 7 V 7 / y / - -- r / i. 1 \ 1 \ 1 1 / • • • Container(s) ''ff X \K \ ^ ^ ^ X X .-T*( TVM (^p5 \ 7 ' Qf^ <. '. *i >; '/ ' 1 . A.,A^ \ FOR 1 ARnnATonv lltP rVtJI V Lab ID •O'^^^-QOS- /•-'•• OHi^-oo^o^reT^zt- OHt^-OOg A-/---: OMI:^-00J^o«=flft^cih.«7. o-^ti^-ooi/^-•••••••/••••-t oMr8l-oti"/or^>/viq- O'+IR-06-76bw/ rtMi'l/DoM-;-:^^^^ (34i<^/mt;'-/6oY-c2fTO-o • • • : - / - - / - - / - ^ - -<JI5 017 Special Instructions/Comments:, Sample Archive/Disposal: n Laboratory Standard D Other FOR LABORATORY USE ONLY. Sample Condition Upon Receipt:. TAT (Analytical Turn-Around Tlnfies) 1-24 hours 2 - 4 8 hours 3-1 week 4 - 2 weeks Container Types: B-Brass Tube, V-VOA Vial, A-1 -Liter Amber, Q-Qlass Jar, C-Cassette, O - Other SEND DOCUMENTATION AND RESULTS TO (Check one): D Pnsject Manager/Office: ' D Client Name: -7[ — .Company: •• •. ',, P P p . . _ . - Address: •• : • '•' - .AAyA-.'A ., • Phone: I Y - . - - A - '- •' ''•' • Fax: '• --.AAAAriiky: U) O cn to A ^ ESS'WF MOBILE LABORATORIES PROGRAM Field Services Division - Warren, NJ N9 03205 CHAIN OF CUSTODY RECORD FOR LABORATORY USE ONLY Laboratory Project No.: . Storage Refrigerator ID: Storage Freezer ID: Secured: Yes No (Signature) Project Name; X 5 1 (T'.yx c\ ChCwiA C.jy-l Project #:. Sampler: Leb6YTx-U •ScKv^^>i,| .eceiveooy;(S^..^^Prp^^^^^ i k ^ i m f J . -R ^ U A ^ Relinquished by; (Signature and Pnmed Nama) °"'°-U-7Jl-0G "^^^ \ ^ R e l i n q u i s h e d b y ; (signature and Printed Name) Received by; (Signature and Printed Name) Date: Date: Time: R e l i n q u i s h e d b y ; (Signature and Printed Nama) Received by; (Signature and Prirtted Name) Data: Time: Time: R e l i n q u i s h e d b y ; (Signature and Printed Name} R e c e i v e d by-. (Signature and Pnntta Utma) Fixed Based Location: Wanen, NJ 07059 (908)604-8900 (908) 604-2352 Sample ID 1 :lnVtxVi?-^iV>l 2 U-i\,aPA^\ ^AoM-<iiy-*'l "Pxl^ia^i-til.-''^ m^-^.AhA^ 6^T-4Ht.'l-?.V-* 7(k.^rr-^-f*i,M 8!^'.';^!?,^-f•\v>l ^ter.Si^-f.vVVi ^° ^A''^7r,-<^-'r-h\^ Method of Shipment; Ai Rl Shipment ID; Sample Description Date M-11-03 I \ \ / Time O^IQ GSiO I3-4M i9-MH iblO (foiS \PbO iws i b3K \ M 0 Description / %j\\.fhir-..-3qd7x.7h& "A ! "^ 1 \ \ \ ' Y A 7 naXyiisies) Miuested / ; - ; > / / ? ; > : > / ' / ? ? ; ^ ' / ' / 7A ^ z a) Identify specific metals / / ^ > / / / / / / / / / / yA / / / / / / Instructions ^^7//////////// 7- 7. ) _ L i yijf t s'l '-^ y <^ i ^^ / / ^ / Container(s) /TAT « 1 Tv(?e D ^ ^ \ - V 0 FOR LARORATORY U t F OfJI V Lab ID ^W^-CXSPP- ••/• •427/©02-/ /••••••• H-2-9/-D03'/ ••••/-••••• M2:V0CH-/^C)0<^-/ • ^7AptX)•t7p•^t}r/• ^y^../,^Q^../.,^^0^./.... t|?.^/OG-t • • p O O T . ' -/OO-S mtPmtvp:-CP)<p- • m.«/-oot/ ••••/• •• m-/^^nP- / •• Special Instructions/Comments:, Sample Archive/Disposal: D Laboratory Standard D Other TAT (Analytical Tum-Around Times) 1 - 24 hours 2 - 4 8 hours 3-1 week 4 - 2 weeks Container Types: B-Brass Tube, V-VOA Vial, A-1-Liter Amber, Q-Qlass Jar, C-Cassatte, O-Other '7i&\aA FOR LABORATORY USE ONLY. Sample Condition Upon Receipt; SEND DOCUMENTATION AND RESULTS TO (Check one): D Project Manaoer/Office: tv\)t rmO- acUJU'^ • Client Name: M d i U l U v / \M^P Company: _ ; _ _ „ _ _ Address: • • Phone: ( ) Fax:, CJ O cn M to -J EHWF CHAIN OF CUSTODY RECORD MOBILE LABORATORIES PROGRAM Field Services Division - Warren, NJ N? 03205 FOR LABORATORY USE ONLY Laboratory Project No.: • • Storage Refrigerator ID: ^ Storage Freezer ID: ' - Secured: Yes No .^sduJA , Project Name; ^ ^ ^ S \ g.v^d. C\fle^wu C^4' Project tt: Sampler: bdlp D r a . p S c \ n r\<U( (Printe^lamel R e c e i v e d by; (Slgrialura and Printed Name) D a t e ! J ^ R e l i n q u i s h e d by; (Signature and Prinlad Name) %1oo"^'"'"^)(oir) R e l i n q u i s h e d by; (Signature and Printed Name) Date: Time: Time: R e l i n q u i s h e d by; (Signature and Printed Namel R e c e i v e d by: (Signature end Printed Name) R e l i n q u i s h e d by: (Signature and Printed Namal R e c e i v e d by; (SIgnatura and Primed Namal D a t e : T i m e : Fixed Based Location: ISO ML Bethel Rd. Warren, NJ 07059 (908) 604-8900 (908) 604-2352 Sample ID 1 Vmr-vMp-jl 2jftf,-,VMf-ZX 3 4 = B 7 (PP^B 9 10 AST-VMf • i-T- Ai't-VIMf'-Hi AiT-VMP-45 f^HitiU-n !:'VwuAV--^3 t x h i l u s H ^ Ey'-x.ius^^ii £ihnmA1 Method of Shipment: Analy Reque Shipment ID: Sample Description y 3 Date 'A/zipt 4 / V ^ / i B / s 1 V Time U,-4 2. Ifco-o !b-.?r |b-.5S \ro^ Zoeo T/TO^ (i2L0 vboS :^D4O Description / / ^ 6ciL G i ^ y- ~X 4/ v t><1X sted / / / / / / / / / / / / / / / / / / / / / / / / / / / / / / / / / / / / / / / requested unoer special / / ^ L / W / / / / / / / / / / / / / / / / Instructions 17S/^w'^\X 7 7 7 7 7 7 7 7 7 7 / / / / / WY/////^^ \ x y kk \K Mixt ' / / ^ / Container(s) /TAT d 1 • ; ' ^*M 3 • ^ 4 • - A / i ^ . "1 6 FOR LABORATORY USE ONI Y Lab ID <^3£)/Oer|-/---/ m-cy^'OOTp /• • H ^ n / n c ^ - / •/•••• 6 | - 2 ; Q / A O < - / - " - / ' - - m&-m^P •/•• ^nP^Q(Hp-0(fi;-iy{c>-- ^2<^/OH--:V-|T-oA M2'?yofi--i<-7o--/ • ^^^•/0•2i1•j•/o^:-^:.;•/••••:••• MTi'/o-Vi-/--(jrMP- Special Instructions/Comments:. Sample Archive/Disposal: D Laboratory Standard D Other FOR LABORATORY USE ONLY. Sample Condition Upon Receipt; TAT (Analytical Tum-Around Times) 1-24 hours 2-48 hours 3 -1 week 4 - 2 weeks Container Types: B-Brass Tube, V-VOA Vial, A-1-Liter Amber, Q-Qlass Jar, C-Cassette, O-Other - r p a i a r B o s . SEND DOCUMENTATION AND RESULTS TO (Check one): ; D ProjectManaoer/Offlce: f^trY/iH E.l(i^•il^^^- D Client Name: H c l & . f t v ^ / \ ^ r 7 Company: Address: ;_ Phone: (___)_ Fax:. O cn i-» lo 00 BSl'WP MOBILE LABORATORIES PROGRAM Field Services Division - Warren, NJ m 03205 CHAIN OF CUSTODY RECORD FOR LABORATORY USE ONLY Laboratory Project No.; -J_ Storage Refrigerator ID: '.^^ Storage Freezer ID: Secured: Yes , N o . Project Name; 7 : < i a . ^ P Ck£iAA,i r.J-f Project #: Heceive<!Tynsigneiurr! Sampler: i J ^ b t ^ m K i- • SQkA&ij IPr«j2dN-lS[ 'CT'or a. ^Ui ?»wvnu ^w..A ^^3-7^-(77> ^^^^31^ R e l i n q u i s h e d by; (Signature end Printed Nafnel Received by; (Signature and Printed Name) R e l i n q u i s h e d by: (Signature and Printed Namal Date: Time: Time: R e l i n q u i s h e d by; ISignalure and Primed Namel R e c e i v e d by; (Signatufe and Printed Name) R e l i n q u i s h e d by; (Signature and Primed Name) R e c e i v e d by; (Signeture end Primed Name) D a t e : T i m O : i ' : . Fixed Based Location: 150 ML Bethel Rd. Warren, NJ 07059 (908) 604-8900 (908) 604-2352 Sample ID ^ ^ ( ^ I ^ T n t a k * w / H _ 2 j e x h r t i t s t i i / a 4 5 6 7 8 9 10 •fPfri>v»;-4- nir-svE-l-' (^sr-svt-tO,- AiT-^-vE'S- mT-5Vfc--M- A&T-^-ye-^" jo^T-sve-fe- fl^T-'S./f,-)- Method of Shipment: Shipment ID: Sample Description Date y/^A ^ ^ I, U I ^ 2- h 1 ; Time 0130 0^)30 ^-dHfr- I6H5 104}^ loSo iOS3 \o5S IIOO (t^-^ Description / '' „ . „ - . . » . „ » - . — — - . \ > Aiuiyiii(es) / A A A A A A A A A A A A A A 7 7 7 / X Requejted / / / / / / / / / / / / / / / / / / / / A "' ^'^^^'^ epeciflc metals X 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 X ^ ' requested unoer opeoiai / y / , / / ^ / y y' / / y y / y y y y y / / Instructions /n./P/A/AATA / / / / / / / / / / / / A A A /P/XJA'/ PA A A / A A A A A A A / / / / / W3AA4///////////////A, i X ! -=-_j.. " / ^'; kp y o ^__ 1 1 i i 1 i \ K > < / 1 - ..-^. . ^ - ^ • ^ • . , ^ : 1 • . — Z' Container(8) .fn, 'i •iw' Tvoe •9S V — — Asi^ : FOR LABORATORY //<JP ONI V Lab ID *f2<?>4);tt-r/<|<^-^t/tfe Hvp/an-.^M-:-/-'--' ~ ^ 3 M : W ' r ^ 6 r — HWoofe/^rfr)y^-nTH ^^•(m'/ncPlP- M^Po[o'/^-[-\/ ^^^^Pc)r;P"/^<!)-(^-p- M'^At)iMA^n\<-p- • 4'wn'it;-^-""-/-"- McvD/ovn ••/•••••••/• ••• Special Instructions/Comments:. Sample Archive/Disposal: D Laboratory Standard D Other TAT (Analytical Tum-Around Times) 1 - 2 4 hours 2 - 4 8 hours 3 - 1 week 4 - 2 weeks Container Types: B-BrassTUbe, V-VOA Vial, A-1-Liter Amber, Q-Olass Jar, C-Cassette, FOR LABOFIATORY USE ONL Y. Sample Condition Upon Receipt:. O - Other ' T e i d t r b A i SEND DOCUMENTATION AND R E S ' U L T S T O (Check one): D Project Manager/Office: p l i y ^ n H £ i ^ K ( i i > . . D Client Name: f^cUre.i-- / Hn-t-f Company: Address: Phone: ( )_ J=Bx:. CO O cn M to Earn ^CIciren MOBILE LABORATORIES PROGRAM 'cirC Field Services Division - Warren, NJ N9 03205 CHAIN OF CUSTODY RECORD FOR LABORATORY USE ONLY Laboratory Project No.: •' Storage Refrigerator ID: Storage Freezer ID; •. •-•. •• • Secured: Yes ; No Project Name; ^Siavvi::^ ( 3 \ t m 7 : ( 3 . Project #: T?ece!ve3Ty!TsignanIre»!d'pr!nle7Nam^ Sampler: "Deb^ro-K L-. OC-kng^i . . 7 . ^ ^ (Printed Name) _ ISIonaHael R e l i n q u i s h e d by: iSignatur* tnd Printed Nam*) Received by: (Stenaturt and Phmtd N«m«) !m Date: R e l i n q u i s h e d by; (Signature and Printed Nanta) Time: Date: Date: R e l i n q u i s h e d by; (Signature and Primed Name) R e c e i v e d by; (Signature and Prinlad Namel Time: R e l i n q u i s h e d by; (Signature and Printed Nama) R e c e i v e d by; (Signalixa and Printed Nama) Time: Fixed Based Location 1 <n k.f* l].*k.i D.4 Warren, NJ 07059 (908) 604-8900 (908) 604-2352 Sample ID Number ^; i\^r-^Mi'Vi Jj()'i'yh^i.7>P 3 4 5 8 7 8 9 W t'Hr.'3.;^.-V-3 m\77i.'<P iY^XAA^ A.'P Method of Shipment: Shipment ID: Sample Description Date 4-5'<ic \ IN y Time ll^M^- 1UM5 lU-^'l) W7i^ Ifn^ Description / \ / > Analysis(es) Requested / / ? ? ? ? / ? ? ? ? ^ / ' / ' / / ^ y z a) Identity iBpieciflc metals / a . / i X A S \ -\/ / / / / / / / / / / / / / / / 7 A/Ar 7^p7\ / / / / / / / / / / / / / / / ATvAp/^ 3/xpA ^ / / / / / / / / / / / / / / / Oontainer(s) x V ^ y A A A A A A A A / / A A / A A XAT 1 i / \ y "^ Y \ \ 7 X / V- • ' •"•^Rf 1 : l P- A ! ^5^1 ^ • • ; 3'3) -.:. FOR LABORA ibRY USE ONL Y Lab ID H W m p A / • • - • • H ^ n i S T ^ n t G / - - I\(^(m-P;—P-' ^\^CA]Al:/-:-r-/--A mc/~oi>¥--m^- • • • • • • • / • / • . • • . . . . . / . • • - • - r - / - - - / - : - . - / - / — / - / - r - / - r - . - ^ - : - ^ . - - / - : - • • • / • • • • • • • / 7 Special Instructions/Comments:. Sample Archive/Disposal: D Laboratory Standard D Other TAT (Analytk^l Tum-Around Times) 1 • 24 hours 2 - 48 hours 3 -1 week 4 - 2 weeks Container Types: B-Brass Tube, V-VOA Vial, A-i-Utar Amber; Q-Qiass Jar, C-Cassette, FOR LABORATORY USE ONLY. Sample Condition Upon Receipt; O - Other J l i J / y i _ £ l 3 ^ SEND DOCUMENTATION AND RE^LTS TO (Check one): n Project Manaoer/Offtee: H 6Y M t - 8 '> tP f I'irv. • D Client Name: M C - ^ ' ^ ' ' ^ / H^i^t Company: .-' ' •'. ''• •• ':-• Address: :;•• • • ' :-• • :A-:--A-^ Phone: _L J - Fax: OJ O cn l - > CO o . .—..'^.•.,A:iA^-'t^A^^':k-ArA-\^AA..A . ESaWF MOBILE LABORATORIES PROGRAM Field Services Division - Warren, NJ N9 03205 CHAIN OF CUSTODY RECORD FOR LABORATORY USE ONLY Laboratory Project No,: Storage Refrigerator ID: _ _ _ _ _ Storage Freezer ID: • Secured: Yes No Proiect Name: X ^ I O - ^ i r i CMtWviClC^ R e l i n q u i s h e d by; (Signature and Prinlat) Nama) R e l i n q u i s h e d by; (Signature and Printed Neme) R e l i n q u i s h e d by; ISignalure and Printed Name) R e l i n q u i s h e d by; (Signature and Printed Name) Project*: Samoler.'behDmM U. S c / m d i d e c e i v e d by; (Signature and Printed Nama) Received by; (Signalura and Printad Namel . Received by; (Signature end Printed Name) R e c e i v e d by; (Signature and Printed Name) Date: Date: Date: Date: (Signature) T i m e : ' " " " " " ^ Time: Time; Time: Special Instructions/Comments: Sample Archive/Disposal: D Laboratory Standard D Other _ ^ FOR LABORATORY USE ONLY. Sample Condition Upon Receipt: TAT (Analytical Tum-Around Times) 1-24 hours 2-48 hours 3-1 week 4 - 2 weeks Container Types: B-Brass Tube, V-VOA Vlal, A-1-Liter Amber, Q-Qlast Jar, C-Cassette, 0-Other/4€d.lrir Wag-: SEND DOCUMENTATION AND RESULTS TO (Check one): ;•; : n Project Manaoer/Office: / A . . -.. O Cllent Name: • •"'' - A - -- ::-:--/• -- '\ -. . " . ' " • i i ^ . M M . . i — •••mm*m t i l l 1 1 . 1 1 1 1 l i . - i i . M I i i - . i . - — i i — I .1 I I I I Company; •;•. ' '. . . '\;: •,.?•. :-}. Address: ': '. ; •... : - A - : . A A A A p Phona:' (• - 3 - • •3'-'.-Vp3'PA-^':tp:ftx: ' • ' *• i i w i i»ip.ini «wi HP»»I IT .. " " • m OJ o cn i-> CO l - > ii^iSiilliii..« KSS'WF MOBILE LABORATORIES PROGRAM Field Services Division - Warren, NJ N? 03205 CHAIN OF CUSTODY RECORD FOR LABORATORY USE ONLY Latwratory Project No.: -_^ Storage Refrigerator ID; Storage Freezer ID: •' ' Secured: Yes No Proiect Name; H ^ S l a n c ^ Che-ryvicoJ? R e l i n q u i s h e d b y ; (Signature and Printad Nama) R e l i n q u i s h e d b y ; ISIgnalura and Primed Name) R e l i n q u i s h e d b y ; (Signature and Printed Name) R e l i n q u i s h e d b y ; (Signature and Printad Nama) Project #: Sampler: T V J o A m ^ L . S c k ^ ^ R J H e c e i v e a by; (Signature and Printed Name) R e c e i v e d by; (SIgnatura and Printed Name) R e c e i v e d by; (Signature and Prinled Nama) R e c e i v e d by; (Signature anl Print-1 Name) Date: Data: Date: Daie: Time: Time: Time; Time: 150 ML Bethel Rd. Wairen. NJ 07059 (908) 604-8900 (908) 604-2352 Sample ID Number Sample Description Date Time Description a) Identify specific metals rflquested Undelr Special Instructions FOR LABORATORY USE ONLY Lab ID !fi3T-^£-2-5 ^x. (7~--y- • f j Q i y l ^ ^ - ^ ^ - / ^ 3o\-/mip/p fl^T-5Vg . 3 i - \ ^ S l ft<;r^sv£'t-S Z ^ o l mSS^l <\ir-s^E-^:-s Z o o i ^tSff)-/—-^ fVSr-S«5'6'S Z o o l ^- "A Ni' V m^^S^ml EKkdMi-^X' s y 2.o3o v- A~~- A \k vy. It / - / - - / / •-/ 7 7---/-- / 10 Special Instructions/Comments;. Sample Archive/Disposal: D Laboratory Standard D Other FOR LABORATORY USE ONLY. Sample Condition Upon Receipt:. TAT (Analytical Tum-Around Times) 1-24hour8 2-48hour8 3-1 week 4-2weelw^! Container Types: B-BrassTube, V-VOA Vlal, A^l-Liter Amber, Q-Qlass Jaf. C-Cassette. / O-Other . ^ A J r L r b(x.j / , SEND DOCUMENTATION AND RESULTS TO (Check one): D Project Manager/Office: • ' ' : -' . - ( D Client Name: / • • . / . • . . Company: .• • - ..:.AAiA : . _ _ 7 A d d r e s s : ' - ' '> -:"••:. •:;- . A - . A A : - - • ' • : : ' i Phone:; ( ) :.-''AA.'"A'\:'-::Fax: '. - ,| OJ o cn M OJ l o -AieAfVX.!.dixAA:'.r!iSAii:A.J ..-I'^ii- I'iiii'iii'i'iHiiiitr ESS^WF MOBILE LABORATORIES PROGRAM Field Services Division - Warren, NJ N? 03205 CHAIN OF CUSTODY RECORD FOR LABORATORY USE ONLY Laboratory Project No.: Storage Refrigerator ID:, Storage Freezer ID: • Secured: Yes No Proiect Name; '-l-IGl a.'V^ A CptQArvvi o.aSI R e l i n q u i s h e d by; (Signature and Printed Name) R e l i n q u i s h e d by; (Signature erid Printed Name) R e l i n q u i s h e d by; (Signature and Printed Name) R e l i n q u i s h e d by; (Signature and Primed Namel Proiect #; Samoler: feefe>nyi5-K L-• ScUt^eLl Heceivea by; (Signature and Printad Name) R e c e i v e d by; (signature and Primed Name) R e c e i v e d by; (Signalura and Printad Name) Date; Data: Date: Date: Time: Time; Time: lime: Special Instructions/Comments:. Sample Archive/Disposal: D Laboratory Standard D Other TAT (Analytnai Tum-Around Times) 1 - 2 4 hours 2 - 4 8 hours 3 - 1 week 4 - 2 weeks Container Types: B-Brass Tube, V-VOA Vial, A-1-Liter Amber, Q-Qlass Jar, C-Cassette, 0 - Other +-tdicW ha. FOR LABORA TORY USE ONL Y. Sample Condition Upon Receipt: SEND DOCUMENTATION AND RESI D Project Manager/Office: D Client Name: • Company: •' Address: "' A : Pttone: ( > utrs TO (Check one); J=«: u> o cn M OJ OJ ^'7y-.7iM7. ^ m Clsiren MOBILE LABORATORIES PROGRAM cll C Field Services Division - Warren, NJ N9 03205 CHAIN OF CUSTODY RECORD FOR LABORA TORY USE ONL Y Laboratory Project No,: - Storage Refrigerator ID: _ _ _ _ _ Storage Freezer ID:. Secured: Yes No Proiect Name; - A S \ c ^ n c [ ( 3 \ e f V \ A C c 3 R e l i n q u i s h e d by; (Signature and Printed Nentel R e l i n q u i s h e d by; (Signature and Primed Name) R e l i n q u i s h e d by; iSignalura and Pririted Nama) R e l i n q u i s h e d by; (Signature and Primed Namel Project*: Samoler; Heceivea by; (Signature and Printed Namal R e c e i v e d by; (Signature and Printad Name) R e c e i v e d by; (Signature and Printed Neme) (Printed Name) S c K n P . I I Date; Data: Date: Date: (Sionalm) Time: Time; Time: Time: - Special Instructions/Comments:. Sample Archive/Disposal: D Laboratory Standard D Other. FOR LABORA TORY USE ONL Y. Sample Condition Upon Receipt:. TAT (Analytical Tum-Around Times) 1 - 24 hours 2 - 48 hours 3 ail week 4 - 2 w e e k s Container Types: B-Brass Tuba, V-VOA Vial, A-1-Liter Amber, Q-Qlass Jar, C-Cassette, O-Other -fg-ij \ 0 . r bfl<| SEND DOCUMENTATION AND RESULTS TO (Check one): D Project Manager/Otfk»:_ •'; ' "~ _ ' DCllentName: .• . ' • ' " • p ' ' - ' - ' ' . ' : - A ' ,. .• Company: ^ ;'. --.. A i • ' ' ' • Address: '•'- '••""• ^t'',;•• - • "" - • .-'.- Phone: ( ) • ' ' '. '•- '/ - J'"- •• Fax: ' ' 00 o c n f-> 00 •Ui^MiMtSTAM.. >:,--A- Aii^s-:ii&>A. ^ i^m MOBILE LABORATORIES PROGRAM Field Services Division • Warren, N J N? 03205 CHAI^I OR CUSTODY RECORD FOR LABORATORYUSE ONLY Laboratory Project No.: •'; Storage Refrigerator ID: _ _ _ _ _ Storage Freezer ID: - Secured: Yes No Proiect Name; ::S75[ a ^ A {C3\^rvPc.£3 ': Relinquished by; (Signature and Printed Namel R e l i n q u i s h e d by; (Signature and Primed Name) Relinquished b y ; (Signature and Printed Namel Project #: Samoler: Heceivea b y ; ISIgnalura and Prinlad Name) R e c e i v e d by; (Signature and Printed Name) R e c e i v e d b y ; (Signature and Printed Nemel R e c e i v e d by; (Signature and Pnmed Name) hehond^ L. Sckr\dA - " • • —(lissidNissr^—— Date: Data; Date: Date: ( S i B n - « ) Time: Time: Time: Time: Fixed Based Location; t e n VAt D * M . . i D.I Warren, NI 07059 (908) 604-8900 1(908) 604-2352 Sample ID Number i;AST-irmf-33.'fi JJ 3 4 5 6 7 8 9 10 Mr-\mf-^D-R Asr- I'MP -^5^ tisr-\w?-Hi7c Pfi,r-vw-MD'<^ Method of Shipment: Shipment ID; Sample Description Date ;;t H-Zoi 'X l^i-/ •.r )it y Time > H53 IH5^ H5i tsoo Itp3 Description • Aiialysts(e>) Requested / ' / ^ / ? ^ ? ' / . ? ? ' / . ' / . ' / . / / 7. 7 / / / a) Identify specific metals y ' / ^ T y ^ A y 7 y 7 y 7 y 7 y ^ / / y 7 / / / / y 7 / X / Instructions /0W///////////////. X ? * • V <.x'_. 1 1 ' A- 7^ I ^ <5. •+ilvfl /nk nn<iit 1- TAT (Analytteal Tum-Around Times 1 / Contalner(s) ff, I k • % Tvoe (?• ' • i , ' i : . 7 • - 24 hours FOR LABORATORY USE ONLY UbID .cC/><.-7...,n^X7. y.... ... bOP-PXM ;••/•••.-. 6er2l-f^ •/•• 6W-m¥- •/• ..p^Q^^QOf^.:...:.../.......- ^ ^ / - o \ o ^ - •••••/••• • - / / • • • " • • • • / " • • • / / • • • • / • • ^ ' / • • : • • - / • • / • • • • • • • —/"•"•:••/•••• / • • • • • • • / • • • • • • • • / • • • • / 2 - 48 hours 3 - 1 week 4 - 2 weeks Special Instructions/Comments:. n Laboratory Standard D Other FOR LABORA TORY USE ONL Y. Sample Condition Upon Rocoipl:. Container Types: B-Brass Tube, V-VOA Vial, A-1-Liter Amber, Q-Qlass Jar, C-Cassette, O-Other -rCAjx-r ' h / t a SEND DOCUMENTATION AND RESULTS TO (Check one): D Project Manaoer/Offtee: . D Client Name: ': • -' •';•'.- ..:A:-...'r.A:i,-/ ,. / Company: , -: : -:.A:Ay7-:7\' ^ 7 Address: : . ..; : . A : : A - A : A A . ' . - ; • Phone: ( V ' A A'PAPAp CO o cn M 00 cn APPENDIX E Form I's and Data Validation 305136 y a c e Analytical Pace Analytical Services, Inc. 1000 RIverbendBlvd, Suite F St. Rose. LA 70087 Tel: 504-469-0333 Fax: 504-469-0555 Sample Data Summary Package SDG: 201382 Project(s): 201382 Presented to: Norma Eichlin McLaren Hart 25 Independence Boulevard Warren. NJ 07059 Presented By: Pace Analytical Services, Inc. 1000 RIverbendBlvd Suite F St. Rose, Louisiana 70087 April 17.2000 3 0 5 1 3 7 (Pace Analytical Services, Inc. SDG:201382 McLaren Han Narrative The McLaren Hart project consisted of twenty-four (24) water samples which were received by Pace Analytical_ Services, Inc. on March 31 and April 3, 2000 and logged in as Project 201382. The samples were identified on the attached Sample Cross Reference report. The s£imples were analyzed for volatile orgainics according to CLP methodology. Sample Management/Login Narrative Temperature for the samples included in this repon ranged from 1.0-4.0''C upon receipt. Nojjroblems were encountered with the login process. ^^:^3P33±=_Zh/oo Cindy Ofavesen Date Project Manager Volatiles # Manual integrations for volatile organics are occasionaUy necessary due to co-elution, interferences and/or inadequacies of the software; these integrations are indicated by an "m" on the quantitation list and the inclusion of an extracted ion current profile indicating the integration of the rget. Samples 2011120, 2011123, 2011124, 2011125, and 2011128 were dUuted prior to analysis based upon screening information. Sample 2011128 required further dilution. Methylene chloride and acetone are common solvents; their presence in field samples may be an artifact of sample collection, transport, or analysis. A surrogate exciarsion was noted for the laboratory control sample, which was included as additional information for batch 02231. The matrix spike recoveries were within QC linuts; therefore no further action was taken. No problems were encountered with these analyses. The pH measurement for each of these water samples was 1. ''^/tT/oi Shelley Afltoine Date Operation Manager Quality Assurance This data package has been reviewed for both completeness and technical specifications. The data were reviewed for overall QA/QC requirements of precision, accuracy, and consistency in data presentation. The data were evaluated for compliance against the CLP Method. These guidelines were used Ln the preparation of our technical narratives. The release of this data package has therefore been authorized by the Laboratory Manager through Quality Assurance review. QA Reviewer Date 305138 j^F^ce Analytical , , ^ w Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s . Inc 1000 Rivertierid Blvd. Suite F Sninl Rose. LA 70087 Phone: 5 0 4 . ^ 9 0333 Fax: 504.469.0555 CUentID: FPPVMP3D Project: VIRGIN ISLAND Lab ID: 2011115 Description: None Method: CLP Volatile Organics Prep Factor: I Leached: n/a CUent: ERTEC Site: None Project No.: 201382 Matrix: Water Prep Level: Water Units: ug/1 CoUected: 3Q-Mar-00 Prepared: Sample Qu: % Moisture: n/a Batch: 02231 Target List: SR61SMVW.\T Received: 31-Mar-OO Analyzed: 06-Apr-OO 16:48 ACA CAS Number 67.M-I 67-66-3 100-41-4 75-09-2 IO«-88-3 1330-20-7 Parameter Acetone (2-Propanone, Dimethyl keto Chlorofomi Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (toial) Dilutioa Result ND 7.30 J ND TiTo—r- ND -2:10-—J- Qu —Att -ti- ij- ID i -• I D v Reporting Limit 10.0 10.0 10.0 10.0 10: ./ 10 V Reg. Limit 6 compoundd) reported ND draotn Not Detected at or ibovc A t uljssted reponlDg lioilL DF denotes DBution Ftctor of extract. T V Prep Ftctor Kcoaiits for a aoo-roatlae sample lizc- Reportiog Uinit is corrected for tanpk sac. dBation and owlsturc content if applkabk. Qu Ibu quaiificn. Specific qnallfWri are dcOfted at the end of tbe report For motstnce results, wet denotes resah b mM corredeil for motsture and a/t denotes not applicable. 305139 4.1*00 U;10:9 Report of Laboratory Analysis 7 - ^ a c e Analytical New Orleans Laboratory _ ClientlD: TB031300 Project: VIRGIN ISLAND Lab ID: 2010020 Description: None Method: CLP Volatile Organics Single Sample - Protocol Pace Analytical Services, Inc. 1000 Riverf>er^cf SfvrJ. Si/To = Saint Rose. LA 7C0S7 P h o n e 5 0 4 . 4 6 9 . 0 3 3 3 F a x : 5 0 4 . 4 6 9 . 0 5 5 5 Prep Factor: I Leached: n/a Client: ERTEC Site: None Project No.: 201156 Matrix: Water Prep Level: Water Units: ug/1 Collected: 13-Mar-OO Prepared: Sample Qu: % Moisture: n/a Batch: 01908 Target List: SR615MVWAT Received: 16-Mar-OO Analyzed: 16-Mar-OO 13:00 KCg Reporting Reg. CAS Number 67-64-1 67-66-3 100-4M 75-09-2 108-88-3 1330-20-7 Parameter Acetone (2-Propanone, Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (total) Dilution Result ND ND ND 4.60 ND ND ••-, iiX Qu All Limit 10.0 10.0 10.0 10.0 10.0 10.0 Limit 6 cotnpound{s) reported v.k- AS.- AA „ ,., >i. 305140- ND denotes Not Detected al or above the adjusted reporting limiL DF denotes Dilution Factor of estract. Tbe Prep Factor accounts for a non-routine sample size Reporting Limit is corrected for saapic size, dilution and moisture content if ippUcable. On lists qualifiers. Specific qualifiers are defined at the end of the report. ::S00 16;40:57 A^^^Ct Report of Laboratory Analysis ^ace Analytical New Orleans Laboratory ClientlD: FB031400 Project: VIRGIN ISLAND Lab ED: 2010026 Description: None Method: CLP Volatile Organics Prep Factor: 1. Single Sample - Protocol P a c e A n a l y t i c a l Services, Inc. 1000 Rivertjonci Blvcl Suito F Saint Rosa. t..4 700S'' Phone: 504.469.0323 Fax: 504 469.0555 Leached: n/a CUent: ERTEC Site: None Project No.: 201156 Matrix: Water Prep Level: Water Units: ug/1 Collected: 14-Mar-OO Prepared: Sample Qu: % Moisture: n/a Batch: 01908 Target List: SR61SMVWAT Received: 16-Mar-OO Analyzed: 23-Mar-OO 1 6 : 3 7 P E I CAS Number 67-64-1 67-66-3 100^1-4 75-09-2 108-88-3 1330-20-7 Parameter Acetone (2-Propanone. Dimethyl keto Chloroform Ethylbeiuene Methylene chloride (Dichloromethane Toluene Xylene (total) Dilution Result 8.50 ND ND 6.00 3.80 1.30 J i J J Qu All All Reporting Limit 10.0 10.0 10.0 10.0 10.0 10.0 Reg- Limit 6 con)pound(s) reported 305141 ND denotes Not Detected at or above the adjusted reporting limit. DF denotes Dilution Factor of e i t r a c t Tbe Prep Factor accounts for a non-routine sample size Reporting L i m i t is corrected for sample size, dilution and moisture content if applicable. Qn lists qualifiers. Specific qualifiers are defined at the end of the report. 3'28'00 16:40:59 /'L>/^6 ^ace Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol Pace Analytical Services, Inc. 1000 Rivertiend Blvd. Suite F Saint Rose. LA 70OS7 Phone. 504 4690333 Fax: 504.469.0555 ClientlD: TB030700 Proiect: VIRGIN ISLAND Lab ID: 209419 Description: None Method: CLP Volatile Organics Prep Factor: I Leached: CAS Number Parameter 67-64-1 Acetone (2-Propanone, Dimethyl keto 67-66-3 Chloroform 100-4M Ethylbenzene 75-09-2 Methylene chloride (Dichloromethane 108-88-3 Toluene 1330-20-7 Xylene (total) 6 conipound(s) reported n/a Client: Site: Project No.: Matrix: Prep Level: Units: CoUected: Prepared: ERTEC None 201156 Water Water ug/I 07-Mar-OO Dilution Result ND ND ND 1.90 J ND ND Qu All Sample Qu: % Moisture: n/a Batch: 01745 Target List: SR615MVWAT Received: 08-Mar-OO Analyzed: 10-Mar-OO 19:41 KCB Reporting Reg. Limit Limit 10.0 10.0 10.0 10.0 10.0 10.0 305142 ND denotes Not Detected at or above the adjusted reporting l i m i t DF denotes Dilutioa Fictor of extract. The Prep Factor accounts for a non-routine sample size. Reporting Limit is corrected for sample size, dilution and noisture content if applicable. Qu lists qualifiers. Specific qualifiers arc defined at the end of the report. 3.:8.0O 16:40:59 *2o. P'^^ace Analytical New Orleans Laboratory ClientlD: MW-IS Project: VIRGIN ISLAND Lab ID: 209420 Description: None Method: CLP Volatile Organics Prep Factor: I Report of Laboratory Analysis Single Sample - Protocol CUent: ERTEC Site: None Project No.: 201156 Matrix: Water Prep Level: Water Units: ug/1 Collected: 07-Mar-OO Leached: n/a Prepared: Pace Analytical Services, Inc. 1000 Riverticnd Blvcl Suite P Saint Raser L.^ 7COS'' Phone: 504.469.0333 Fax: 504 469 0555 Sample Qu: % Moisture: n/a Batch: 01745 Target List: SR615MVWAT Received: 08-Mar-OO Analyzed: 10-Mar-OO 20:11KCB CAS Number 67-64-1 67-66-3 I00-4M 75-09-2 108-88-3 1330-20-7 Parameter Acetone (2-Propanone, Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (total) Dilution Result Qu ND 9.40 J ND 2m--}^-kPMi R ND ND Reporting Limit 10.0 10.0 10.0 ; ( ) 10.0 10.0 10.0 Reg. Limit 6 compound's) reported 305143 ND denotes Not Detected al or above the adjusted reporting limit. DF denotes Dilution Factor of eitract. The Prep Factor Kcounts for a non-rontinc sample size;. Reporting Limit is corrected for sample sixe, dilation and moisture content if applicable. Qu lists qualifiers. Specific qualificn are defined at the end of the report. 3/28.00 16:41:00 0 J 4 C I 'ace Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Inorganic Parameters P a c e A n a l y t i c a l S e r v i c e s , Inc. 1000 Riv(}rt>*?nd Blvrl Sm'f^ F Saint Rosf^. LA 70.0B'^ P h o n e : 304.469.0333 Fax: 504.469.0555 Client ID: MW-15 Project: VIRGIN ISLAND Lab ID: 209856 Description: None Client: ERTEC Site: None Project No.: 201156 Matrix: Water CoUected: 3/7/00 ParameterName Method Batch DF Result Qu Reporting Lnits Limit %Moisture: n/a Received: 3/14/00 Prep. Analysis Reg. Limit Sulfate EPA 375.2 1 pararacterts) reported 02155 186. mg/1 50.0 29-Mar-OO 12:03 LAK 305144 ND denotes Not Detected at or at>ove the adjusted reporting limlL DF denotes Dilution Factor of final sample. PF denotes sample Prep Factor which accounts for a non-rontlne sample size. Reporting Limit is corrected for sample size, dilution and moisture content If applicable. Qn lisis qualifiers. Specific qualifiers are defined at the end of the report For moisture results. we< denotes result is not corrected for moisture and n/a denotes not applicable. ' 3.'30 00 13:23:30 f^^ce Report of Laboratory Analysis ^ace Analytical New Orleans Laboratory _ ClientlD: MW-13 Project: VIRGIN ISLAND Lab ID: 209421 Description: None Method: CLP Volatile Organics Prep Factor: 1, Leached: n/a Single Sample - Protocol P a c e A n a l y t i c a l Services, Inc. 1000 Rivertiend Btvd, Suite F Saint Rose. LA 700S7 Phone: 504 469.0333 Fax: S04.469 0555 CUent: ERTEC Site: None Project No.: 201156 Matrix: Water Prep Level: Water Units: ug/1 CoUected: 07-Mar-OO Prepared: Sample Qu: % Moisture: n/a Batch: 01745 Target List: SR615MVWAT Received: 08-Mar-OO Analyzed: 10-Mar-OO 20:42 KgB CAS Number 67-64-1 67-66-3 100-4M 75-09-2 108-88-3 1330-20-7 Parameter Acetone (2-Propanone, Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (total) Dilution Result ND ND ND t780- ND ND Qu J -tMii- \ Reporting Limit 10.0 10.0 10,0 D U '0-0 10.0 10.0 Reg. Limit 6 compound(s) reported \^S VA- 305145 ND denotes Not Detected at or above tbe adjusted reporting UmiL OF denotes Dilution Factor of ciCract. The Prep Factor accounts for a non-routine sample size. Reporting Limit is corrected for sample size, dilation and moisture content if applicable. Qu lists qualifiers. Specific qualifiers are defined at the end of the report. For moisture results, wet denota rcsalt b not corrected for moisture and n/a denotes not applicable. i.23:00 16:41:00 ^ . Report of Laboratory Analysis /"^^ace Analytical New Orleans Laboratory Single Sample - Inorganic Parameters P a c e A n a l y t i c a l S e r v i c e s , Inc. 1000 Rivertiend Blvd. Suite F Saint Rosf^. LA 7008^ Phone. 504.469.0333 Fax: 504 469.0555 ClientlD: MW-13 Proiect: VIRGIN ISLAND Lab ID: 209857 Description: None ParameterName Method Batch OF Sulfate • EPA 375.2 02155 5 1 p>rain«n-(s) irponed Result 182. Qu CUent: ERTEC Site: None Proiect No.: 201156 Matrix: Water CoUected: 3/7/00 Reporting Units Limit mg/1 50.0 Prep. %Moisture: n/a Received: 3/14/00 Analysis 29-Mar-OO 12;03 LAK Reg. Limit 305146 ND denotes Not Detected at or above the adjusted reporting limit DF denotes Dilution Factor of final sample. PF denotes sample Prep Factor which acconnts for a oon-roallne sample size Reporting Limit is corrected for sample size, dilutioa and moisture content if applicable. Qu lists qualifier!. Specific qualifiers arc defined at the end of the report. Vttr mni^turr results, wet deaot«s resnh k ant mrrcvted for moisture and n/a denotes not aoDlicable. 3.30 00 13:23:31 ^ J ^ c e ^ace Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s , Inc. 1000 Rivertiend Blvd. Suite F Saint Rose LA 70087 Phone: 504.469.0333 Fax: 504.469.0555 ClientlD: MW-11 Project: VIRGIN ISLAND Lab ID: 209590 Description: None Method: CLP Volatile Organics Prep Factor: I Leached: n/a Client: ERTEC Site: None Project No.: 201156 Matrix: Water Prep Level: Water Units: ug/1 CoUected: 08-Mar-OO Prepared: Sample Qu: % Moisture: n/a Batch: 01745 Target List: SR615MVWAT Received: 10-Mar-OO Analyzed: 10-Mar-OO 21:12 Kgg CAS Number 67-64-1 67-66-3 100^1-4 75-09-2 108-88-3 1330-20-7 Parameter Acetone (2-Propanone, Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (total) Dilution Result ND 40.4 ND -1.80 ND ND Qo IUAU., \ • Reporting Limit 10.0 10.0 10.0 j \ J 10.0 10.0 10.0 Reg. Limit 6 compound(s) reported ^^:;-^ \ V-i 305147 ND denotes Not Detected at or above the adjusted reporting UmiL DF denotes DQutlon Factor of extract. Tbe Prep Factor accooots for a non-routine sample size. Reporting Limit h corrected for sample size, dilution and moisture content if applicable. Qn lists qualifiers. Specific qualifiers are defined at the end of the report. 3/:S.0O 16:41:00 W^ce Report of Laboratory Analysis ^ace Analytical^ New Orleans Laboratory Single Sample - Inorganic Parameters Pace Analytical Services, Inc. 1000 Rivertiend Blvd Suite F Saint Rose. LA 700S7 P h o n e : 5 0 4 . 4 6 9 . 0 3 3 3 F a x : 5 0 4 . 4 6 9 . 0 5 5 5 ClientlD: MW-11 Project: VIRGIN ISLAND Lab ID: 209858 Description: None ParameterName Method Batch DF Result Qu Client: ERTEC Site: None Proiect No.: 201156 Matrix: Water CoUected: 3/8/00 Reporting l/nits Limit Prep. %Moisture: n/a Received: 3/14/00 Analysis Reg. Limit Sulfate EPA 375.2 I parameter(s) reported 02155 243. mg/I 50.0 29-Mar-OO 12:03 LAK 305148 ND denotes Not Detected at or above tbe adjusted reporting limit. DF denotes Dilution Factor of final sample. PF denotes sample Prep Factor which acconnts for a non-routine sample size. Reporting Limit is corrected for sample size, dilution and oMHSture content if appUcabtc: Qu lists qualifiers. Specific qualifiers are defined at the end of the report. For moisture results, wet denotes resoh is not corrected for aonturc and n/a denotes wM applicable. 3 3000 i3::3;31 . ^ ^ c t Report of Laboratory Analysis ^ace Analytical New Orleans Laboratory CUent ID: TB030800 Project: VIRGIN ISLAND Lab ID: 209591 Description: None Method: CLP VolatUe Organics Prep Factor: 1_ Leached: n/a Single Sample - Protocol Pace Analytical Services, tnc. 1000 Rivertiend Blvd. Suite F Saint Rose. LA 70OS7 Phone: 504 469.0333 Fax: 504.469.0555 Client: ERTEC Site: None Project No.: 201156 Matrix: Water Prep Level: Water Units: ug/1 CoUected: 08-Mar-OO Prepared: Sample Qu: % Moisture: n/a Batch: 01745 Target List: SR615MVWAT Received: 10-Mar-OO Analyzed: 11-Mar-OO 14:26 J<CB CAS Number 67-64-1 67-66-3 100-41-4 75-09-2 108-88-3 1330-20-7 Parameter Acetone (2-Propanone, Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (total) Dilution Result ND ND ND 1.50 J ND ND Qu All Reporting Limit 10.0 10.0 10.0 10.0 10.0 10.0 Reg. Limit 6 compound(s) reported ND denotes Not Detected al or above the adjusted reporting limit DF denotes Dilution Faaor of extract The Prep Factor accounts for a non-routine sample size. Reporting Limit is corrected for sample size;, dilation and moisture content if applicable. Qo lists qnafifien. Specific qualifiers are defined at the end of tbe report For moisture results, wet denotes rcsotl is not corrected for moisture and n/a denotes not applicable. 305149 J.aS.OO 16:41:00 f^^ace Analytical New Orleans Laboratory CUent ID: MW-3 Project: VIRGIN ISLAND Lab ID: 209592 Description: None Method: CLP VolatUe Organics Prep Factor: 1 Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l Services, Inc. 1000 Rivertiend Blvd. Suite F Saint Rose. LA 70087 Phone: 504.469.C333 Fax: 504.469.0555 Leached: n/a Client: ERTEC Site: None Project No.: 201156 Matrix: Water Prep Level: Water Units: ug/1 CoUected: 08-Mar-OO Prepared: Sample Qu: % Moisture: n/a Batch: 01745 Target List: SR615MVWAT Received: 10-Mar-OO Analyzed: 12-Mar-OO 12:18KCg CAS Number 67-64-1 67-66-3 100-41-4 75-09-2 108-88-3 1330-20-7 Parameter Acetone (2-Propanone, Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (total) Dilution Result ND ND ND -MO- ND ND Qu -J-U-AH- 1 c Reporting Limit 10.0 10.0 10.0 n 10.0 10.0 10.0 Reg. Limit 6 compound(s) reported 305150 ND denotes Not Detected at or above tbe adjusted reporting limit DF denotes Dilution Factor of extract The Prep Factor accounts for a non-roDtlnc sample size. Reporting Limit is corrected for sample size, dilution and moisture content If applicable. Qu lists qualifiers. Specific qualifiers are defined at the end of the report For moisture results, wet denotes resak is not corrected for moisture and n/a denotes not applicable. 3/28/00 16:41:0! f ^ " ^ ' ^ Report of Laboratory Analysis W ^ c e Analytical^ New Orleans Laboratory Single Sample - Inorganic Parameters P a c e A n a l y t i c a l Services, Inc. 1000 Rivertiend Blvd. Suite F Saint Rase. LA 7GCS 7 Phone: 504 469 0333 Fax: 504 469.0555 Client ID: MW-3 Project: VIRGIN ISLAND Lab ID: 209859 Description: None CUent: ERTEC Site: None Proiect No.: 201156 Matrix: Water CoUected: 3/8/00 %Moisture: n/a Received: 3/14/00 farameterName Method Batch DF Result Qu Reporting Units Limit Prep. Analysis Reg. Limit Sulfate EPA 375.2. 1 pannic<er(s) reponed 02155 194. mg/1 50.0 29-Mar-OO 12:03 LAK 305151 ND denotes Not Detected at or above the adjusted reportiog l i m i t DF denotes Dilution Factor of final sample. PF denotes sample Prep Factor which accounts for a noo-rootine sample stze. Reporting Limit is corrected for sample size, dilution and moistore content if applicable. Qu Uits qualifiers. Specific qualifiers are defined at the end of the report For moisture results, wet denotes resatt is not corrected for moisture and n/a denotes not applicable 3 3000 13:23:31 i j ^ ^ c e Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol CUent ID: MW-7 Project: VIRGIN ISLAND Lab ID: 209593 Description: None Method: CLP VolatUe Organics Pace Analytical Services, Inc. 1000 Rivertiend Blvd, Suite F Saint Rose. LA 70087 Phone: 504 469.0333 Fax: 504.469.0555 Prep Factor: 1_ Leached: n/a CUent: ERTEC Site: None Project No.: 201156 Matrix: Water Prep Level: Water Units: ug/1 CoUected: 08-Mar-OO Prepared: Sample Qu: % Moisture: n/a Batch: 01745 Target List: SR615MVWAT Received: 10-Mar-OO Analyzed: 11-Mar-OO 15:27KCB CAS Number 67-64-1 67-66-3 100-41-4 75-09-2 108-88-3 1330-20-7 Parameter Acetone (2-Propanone, Dimethyl keto Chlorofonn Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (total) Dilution Result Qu ND 1.50 J ND t-.40--H7All^ A ND ND Reporting Limit 10.0 10.0 10.0 J '-' 10.0 10.0 10.0 Reg. Limit 6 compouod(s) reported \Ki';-.n' 305152 ND dcDoMs Not Detected at or above the adjnstcd reporting l i m i t p F denotes Dilution Factor of extract The Prep Factor accounts for a non-routine sample size. Reporting Limit is corrected for sample size, dilation and moisture content if applicable Q u lists qnalifiers. Specific q o a l l f i c n are defined at the end of the report For moisture results, wet denotes rcsok b not corrected for moistore and i^a denotes sol applicable. 3':3'00 16:41:01 ^^J^ce Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Inorganic Parameters P a c e A n a l y t i c a l Services, Inc. 1000 Riverbend Blvd. Suite F Saint Rase. LA 700S7 Phone: 504 469 0333 Fax: 504 469 0555 ClientlD: MW-7 Project: VIRGIN ISLAND Lab ID: 209860 Description: None CUent: ERTEC Site: Project No.: Matrix: CoUected: None 201156 Water 3/8/00 ParameterName Method Batch DF Result Qu Reporting Units Limit "/oMoisture: n/a Received: 3/14/00 Prep. Analysis Reg. Limit Sulfate EPA 375.2 I paramelerfs) reported 02155 195. mg/1 50.0 29-Mar-OO 12:03 LAK 'k ND denotes Not Detected at or above the adjusted reporting limit DF denotes Dilution Factor of final sample. PF denotes sample Prep Factor which accounts for a non-routine sample size. Reporting Limit is corrcc«d for sample size, dilution and moistnre content if applicable. Qu Usts qnalifiers. Spcdfk: qualifiers are defined at the end of the report For moutnre results, wet denotes result is not corrected for moisture and n/a denotes not applicable. 305153 3 JO'00 13::3:31 /2. ' ^t^\Jew Orlea ^ace Analytical ^\lew Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l Services, Inc. 1000 Rivertiend Btvd. Suite F Saint R o s e . LA 7 0 0 8 7 P h o n e : 504 469.0333 F a x : 504 4 6 9 . 0 5 5 5 ClientlD: MW-10 Project: VIRGIN ISLAND Lab ID: 209594 Description: None Method: CLP VolatUe Organics Prep Factor: I Leached: n/a CUent: ERTEC Site: None Project No.: 201156 Matrix: Water Prep Level: Water Units: ug/1 CoUected: 07-Mar-OO Prepared: Sample Qu: % Moisture: n/a Batch: 01745 Target List: SR615MVWAT Received: 10-Mar-OO Analyzed: 11-Mar-OO 15:58 JJCB CAS Number 67-64-1 67-66-3 100-41-4 75-09-2 108-88-3 1330-20-7 Parameter Acetone (2-Propanone, Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (total) Dilution Result ND ND ND t:20 ND ND Qu -i-y-AM \ I Reporting Limit 10.0 . 10.0 10.0 'A \ 10.0 10.0 10.0 Reg. Limit 6 compound(s) reported .w -A. A 305154 ND denotes Not Detected at or above the adjusted reporting limit DF deaotes DUodoo Factor of extract Tbe Prep Factor accounu for a non-routine sample size. Reporting Limit is corrected for sample size, dilution and moistnre content if applicable. Qn lists qualifiers. Specific qoallficn are defined at the end of the report For moisture results, wet denotes rcsall is not corrected for moisture and n/a denotes not applicable. 3/28'00 16:41:01 Hy^^ ~y Report of Laboratory Analysis / ^ ^ c e Analytical^ ^rJew Orleans Laboratory Single Sample - Inorganic Parameters P a c e A n a l y t i c a l Services, Inc. 1000 Rivertiend Blvd. Suite F Saint Rose. LA 70087 Phone: 504.469.0333 Fax: 504.469.0555 ClientlD: MW-10 Project: VIRGIN ISLAND Lab ID: 209861 Description: None CUent: ERTEC Site: None Project No.: 201156 Matrix: Water CoUected: 3/7/00 farameterName Sulfate Method EPA 375.2 Batch 02155 DF Result Qu Reporting Units Limit %Moisture: n/a Received: 3/14/00 Prep. Analysis Reg. Limit 286. mg/1 50.0 29-Mar-OO 12:03 LAK 1 pmrmmetcr(s) reported ND dcnotn Not [)«tectcd •! or above the Idjostcd reporting UmiL DF denolca Dilution Factor of final lanplc. PF denotes sample Prep Factor whlcb accoonts for a oon-nHitine sampk sbc Reporting Limit is corrected for sample size dilation and moistnre content if applicable. Qu lisu qualifiers. Specific qualifiers are defined at tbe end of the report. For moisture results, wet denotes resnll b not corrected for moisture and n/a denotes not applicable 305155 :- :.oooi3::; ^J^ace Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s , Inc. 1000 Riverbend Btvd. Suite F Saint Rose. LA 70OS7 Phone: 504.469 0333 Fax: 504.469.0555 ClientlD: MW-2 Project: VIRGIN ISLAND Lab ID: 209595 Description: None Method: CLP Volatile Organics Prep Factor: 1. Leached: n/a CUent: ERTEC Site: None Project No.: 201156 Matrix: Water Prep Level: Water Units: ug/1 CoUected: 08-Mar-OO Prepared: Sample Qu: % Moisture: n/a Batch: 01745 Target List: SR615MVWAT Received: 10-Mar-OO Analyzed: 12-Mar-OO 12:49 KCB CAS Number 67-64-1 67-66-3 100-4M 75-09-2 108-88-3 1330-20-7 Parameter Acetone (2-Propanone, Dimethyl keto Chloroform Ethylbeiuene Methylene chloride (Dichloromethane Toluene Xylene (total) DUution Result Qu ND 37.0 ND •1:2&-J -i r A H - ;; ND ND Reporting Limit 10.0 10.0 10.0 .) U '00 10.0 10.0 Reg. Limit 6 compound(s) reported 305156 .\D denotes Not Detected at or above the adjusted reporting UmiL OF denotes Dilution Factor of extract The Prep Factor accounts for a nooHroutine sample size. Reporting Limit is corrected for sampk size, dilution and moisture content if applkable. Qo lists qoallflers. Specific qualifiers are defined at tbe end of the report For moisture results, wet denotes rcsotl b not corrected for moisture and n/a denotes not applicable. 3/28/00 16:41:01 ^ ' ^ / Report of Laboratory Analysis / ^ ^ ^ c e Analytical^ ^^4ew Orleans Laboratory Single Sample - Inorganic Parameters P a c e Analytical Services, Inc. 1000 Riverbend Blvd. Suite F Saint Rose. LA 70087 Phone: 504.469.0333 Fax: 504.469.0555 Client ID: MW-2 Project: VIRGIN ISLAND Lab ID: 209862 Description: None Client: ERTEC Site: None Project No.: 201156 Matrix: Water CoUected: 3/8/00 ParameterName Method Batch DF Result Qu Reporting Units Limit %Moisture: n/a Received: 3/14/00 Prep. Analysis Reg. Limit Sulfate EPA 375.2 1 parameter(s) reported 02155 151. mg/1 50.0 29-Mar-OO 12:03 L A K s o denotes Not Detected at or above die adjusted reporting HmfL . OF denotes Dilution Factor of final sample. PF denotes sample Prep Factor which accoonti for a non-routine sample size. Reporting Limit is corrected for sample size, dilution and moisture content If applicable. Qn lists qualifiers. Specific qualifiers are defined at the end of the report For moisture results, wet denotes result is not corrected for moistnre and n/a denotes not applicable. 305157 ?.30'00 13:23:3: /^J^ace Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol Pace Analytical Services, Inc. 1000 Rivertiend Blvd, Suite F Saint Rose. LA 70087 Phone: 504 469.0333 Fax: 504.469.0555 ClientlD: MW-8 Proiect: VIRGIN ISLAND Lab ID: 209596 Description: None Method: CLP VolatUe Organics Prep Factor: 1 Leached: n/a CAS Number Parameter 67-64-1 Acetone (2-Propanone, Dimethyl keto 67-66-3 Chloroform 100-41-4 Ethylbenzene 75-09-2 Methylene chloride (Dichloromethane 108-88-3 Toluene 1330-20-7 Xylene (total) 6 conipound(t) reponed CUent: ERTEC Site: None Proiect No.: 201156 Matrix: Water Prep Level: Water Units: ug/I CoUected: 08-Mar-OO Prepared: Dilution Result 1 ND 1 ND 1 ND 1 1.10-.1-i. 1 ND 1 ND Qu Uu Sample Qu: % Moisture: n/a Batch: 01745 Target List: SR615MVWAT Received: 10-Mar-OO Analyzed: 11-Mar-OO 17:28 »<^CB Reporting Reg. Limit Limit 10.0 10.0 10.0 \V) U 10.0 10.0 10.0 305158 ND denotes Not Detected at or above the adjusted reporting limit DF denotes DOution Factor of extract The Prep Factor accounts for a non-routine sample size. Reporting Limit is corrected for sample size, dilution and moisture content if applicable. Qn Ibu quaUflen. Specific qualifiers arc defined at the end of the report For noisture resulti. wet denotes resalt ti not corrected for moisture and n/a denotes not applicable. 3:100 16:-Jl;0: ^"^"j Report of Laboratory Analysis / ^ ^ c e Analytical^ . Jew Orleans Laboratory Single Sample - Inorganic Parameters P a c e A n a l y t i c a l . Services, inc. 1000 Riverb&nd Blvd. Suite F Saint Rose. LA 70087 Phone: 504.469.0333 Fax: 50^ 469.0555 ClientlD: MW-8 Project: VIRGIN ISLAND Lab ID: 209863 Description: None ParameterName CUent: ERTEC Site: None Project No.: 201156 Matrix: Water CoUected: 3/8/00 Method Batch DF Result Qu Reporting Units Limit VoMoisture: n/a Received: 3/14/00 Prep. Analysis Reg. Limit Sulfate EPA 375.2 1 parameCcrfs) reported 02155 74.6 mg/1 10.0 29-Mar-OO 12:03 LAK M) denotes Not Detected at or above the adjusted reporting limit DF denotes Dilution Factor of final sample. PF denotes sample Prep Factor which acconnts for a non-routine sample tUc. Reporting Limit is corrected for sample size, dilution and moisture content if applicable. Qu Usts qualifiers. Specific qualifiers are defined at the end of the report For moisture results. «ei denotes resuK is not corrected for moisture and n/a denotes not applicable. 305159 3'30'OO 1 3 : : J : 3 2 ^ ^ a c e Analytical f ^ ^ N e w Orleans Laboratory ^0 7Jp^ ..-,:,.' ClientlD: MW-80 ^^ Project: VIRGIN ISLAND Lab ID: 209597 Description: None Method: CLP VolatUe Organics Report of Laboratory Analysis Prep Factor: 1. Single Sample - Protocol CUent: ERTEC Site: None Project No.: 201156 Matrix: Water Prep Level: Water Units: ug/1 CoUected: 08-Mar-OO Leached: n/a Prepared: P a c e A n a l y t i c a l S e r v i c e s , Inc. 1000 Rivertiend Blvd. Suite F Saint Rose. LA 70087 Phone: 504.469.0333 Fax: 504.469.055S Sample Qu: % Moisture: n/a Batch: 01745 Target List: SR615MVWAT Received: 10-Mar-OO Analyzed: 11-Mar-OO 17:58 K£g CAS Number 67-64-1 67-66-3 100-41-4 75-09-2 108-88-3 1330-20-7 Parameter Acetone (2-Propanone, Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (total) Dilution Result ND ND ND ND ND ND Qu Reporting Limit lO.O 10.0 10.0 10.0 10.0 10.0 Reg. Limit 6 compound<s) reported 305160 M> denotes Not Detected at or above the adjusted reporting limit DF denotes Dilution Factor of extract The Prep Factor acconnts for a non-routine sample size. Reporting Limit is corrected for sample size. dDntion and moisture content if applicable. Qo lists quaUfien. Specific qualifiers are defined at the end of the report For moisture results, wet denotes result b not corrected for moisture and n/a denotes not applicable. 3'23 00 16:41:02 / ^ ^ c e Analytical^ ^Wew Orleans Laboratory 0'A. Client ID: EB030800 Project: VIRGIN ISLAND Lab ID: 209598 Description: None Method: CLP VolatUe Organics Prep Factor: \ Leached: n/a Report of Laboratory Analysis Single Sample - Protocol Pace Analytical Services. Inc. 1000 Riverbend Blvd, Suite F Saint Rose. LA 70087 Phone: 504.469.0333 Fax: 504.469.0555 ' CUent: ERTEC Site: None Project No.: 201156 Matrix: Water Prep Level: Water Units: ug/I CoUected: 08-Mar-OO Prepared: Sample Qu: % Moisture: n/a Batch: 01745 Target List: SR615MVWAT Received: 10-Mar-OO Analyzed: 11-Mar-OO 18:28 KCB CAS Number 67-64-1 67-66-3 100^1-4 75-09-2 108-88-3 1330-20-7 Parameter Acetone (2-Propanone, Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (total) Dilution Result ND ND ND 1.70 J ND ND Qu All Reporting Limit 10.0 10.0 10.0 10.0 10.0 lO.O Reg. Limit 6 compound(s) reported ND denotes Not Detected at or above the adjusted reporting limit DF denotes Dilution Factor of extract The Prep Factor accounts for a non-routine sample size. Reporting Limit is corrected for sample size;, dilution and moisture content if applicable. Qu lists qualifiers. Specific quaUficn arc defined at the end of the report For m0>sture results, wet denotes rcsall a not corrected for moisture and n/a denotes not applicable. 305161 3,'28'00 16:41:02 ^ J ^ c t ^ ^ ^ a c e Analytical ^ ^ N e w Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l Services, Inc. 1000 Riverbend Blvd, Suite F Sairtt Rose. LA 70087 Phone: 504 469.0333 Fax: 504.469.0555 Client ID: MW-6 Project: VIRGIN ISLAND Lab ID: 209599 Description: None Method: CLP VolatUe Organics Prep Factor: I Leached: n/a CUent: ERTEC Site: None Project No.: 201156 Matrix: Water Prep Level: Water Units: ug/I CoUected: 09-Mar-OO Prepared: Sample Qu: % Moisture: n/a Batch: 01745 Target List: SR615MVWAT Received: 10-Mar-OO Analyzed: 12-Mar-OO 13:19KCB CAS Number Parameter Dilution Result Qu Reporting Limit Reg. Limit 67-64-1 67-66-3 100-41-4 75-09-2 108-88-3 1330-20-7 Acetone (2-Propanone, Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (total) 6 conipouiid(s) reported 400 400 400 400 400 400 ND ND 1240O ND ND 60700 D6 D6 D6 D6 D6 D6 4000 40OO 4000 4000 4000 4000 ND denotes Not Detected at or above the adjusted reporting limit DF denotes DUution Fictor of extract The Prep Factor acconnts for a oon-roadne sample siz£. Reporting Limit is corrected for sample s"*. dilution and moisture content if applicable. Qu lists qualifiers. Specific qualifiers are defined al tbe end of the report For moisture results, wet denotes result is not corrected for moisture and n/a denotes not applicable. 305162 3'28'00 16:41:0? ^ ^ ^ Report of Laboratory Analysis ^ J ^ c e Analytical^ New Orleans Laboratory Single Sample - Inorganic Parameters P a c e A n a l y t i c a l Services, Inc. 1000 Riverbend Blvd. Suite F Saint Rose. LA 70087 Phone: 504.469.0333 Fax: 504 469.0555 ClientlD: •MW-6 Project: VIRGIN ISLAND Lab ID: 209864 Description: None Client: ERTEC Site: Project No.: Matrix: CoUected: None 201156 Water 3/9/00 ParameterName Method Batch DF Result Qu Reporting Units Limit Prep. %Moisturc: n/a Received: 3/14/00 Analysis Reg. Limit Sulfate EPA 375-2 1 parametMls) reported 02155 47.4 mg/1 10.0 29-Mar-OO 12:03 LAK ND denotes Not Detected at or above dM adjusted reporting l i m i t DF denotes Dilution Factor of final sample. PF denotes sample Prep Factor which accounts for a non-roulinc sample size Reporting Limit is corrected for sample size, dilution and moistnre content if applicable. Qo Usts qualifiers. Specific qualiiicri arc defined at the end of tbe report For moisture results, wet denotes rcsnit is not corrected for moisture and n/a denotes not applicable. 305163 •ooo I 43. ace Analytical ew Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e Analytical Services, Inc. 1000 Riverbend Blvd, Suite F Saint Rose. LA 70O87 Phone: 504 469 0333 Fax: 504.469.0555 ClientlD: MW-1 Proiect: VIRGIN ISLA^a) Lab ID: 209600 Description: None Method: CLP VolatUe Oreanics Prep Factor: I CAS Number Parameter Leached: n/a CUent: ERTEC Site: None Proiect No.: 201156 Matrix: Water Prep Level: Water Units: ug/1 CoUected: 09-Mar-OO Prepared: Dilution Result Qu Sample Qu: % Moisture: n/a Batch: 01745 TareetList: SR615MVWAT Received: 10-Mar-OO Analyzed: 12-Mar-OO 14:20 KCB Reporting Reg. Limit Limit 67-64-1 67-66-3 100^1-4 75-09-2 108-88-3 1330-20-7 Acetone (2-Propanone, Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (total) 6 compound(%) rtponed 500 50O 500 500 500 500 ND D6 ND D6 19600 D6 sm-. -]-iJ~A:H' ND D6 89000 D6 5fex) 5000 5000 5000 •• 5000 50OO 5000 ...-^SV:' W VD denotes Not Detected at or above the adjusted reportiog limit OF denotes DUution Factor of extract The Prep Factor accounts for a non-routine sample size. Reporting Limit is corrected for sample size, dilution and moisture content if applicable. Qn lists qualifiers. Specific qnalifiers are defined at the end of the report For moisture results, wet denotes resalt is not corrected for moisture and n/a denotes not applicable. 305164 3.':800 16:41:03 T^^^ce Report of Laboratory Analysis ^ace Analytical^ "New Orleans Laboratory P a c e A n a l y t i c a l Sen/;ces, Inc. 1000 Riverbend Blvd. Suite F Saint Rose. LA 70037 ClientlD: MW-1 Project: VIRGIN ISLAND Lab ID: 209865 Description: None ParameterName Method Batch Single Sample - Inorganic Parameters CUent: ERTEC Site: None Project No.: 201156 Matrix: Water CoUected: 3/9/00 Reporting DF Result Qu Units Limit Prep. Phone: sO^ 469 03.J3 Fax: 504469.0555 %Moisture: n/a Received: 3/14/00 Reg. Analysis Limit Sulfate EPA 375.2 I panjne<er(s) reported 02155 ND mg/1 10.0 29-Mar-OO 12:03 LAK VD denotes Not Detected at or above the adjusted reporting limit DF denotes DUution Factor of final sample. PF denotes sample Prep Factor which accounts for a non-routine sample sb Reporting Limit is corrected for sample size, dilution and moisture content If applicable Qa lists qualifiers. Specific qualifiers arc defined at the end of the report For moisture results, wet denotes resatt is not corrected for moisture and n/a denotes not applicable. 305165 r.r.ooo 15::? T^jj^ce Analytical i^ew Orleans Laboratory ClientlD: FB030900 Project: VIRGIN ISLAND Lab ID: 209846 Description: None Method: CLP VolatUe Organics Prep Factor: 1 Report of Laboratory Analysis Single Sample - Protocol CUent: ERTEC Site: None Project No.: 201156 Matrix: Water Prep Level: Water Units: ug/1 CoUected: 09-Mar-OO Prepared: P a c e A n a l y t i c a l Services, Inc. 1000 Riverbend Blvd. Suite F Saint Rose. LA 70087 Phone 504 469.0333 Fax: 504.469.0555 Leached: n/a Sample Qu: % Moisture: n/a Batch: 01908 Target List: SR615MVWAT Received: 14-Mar-OO Analyzed: 14-Mar-OO 16:4220 CAS Number 67-64-1 67-66-3 lOO^M 75-09-2 108-88-3 1330-20-7 Parameter Acetone (2-Propanone, Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (total) Dilution Result ND ND ND 3.10 1 ND ND Qu Ail Reporting Limit 10.0 10.0 10.0 10.0 10.0 10.0 Reg. Limit 6 compound(s) reported ND denotes Not Detected at or above the adjusted reporting limit DF denotes DUution Factor of eitract The Prep Factor accounts for a non-routine sample size. Reporting Limit is corrected for sampte size, dilution and moistnre content If applicable. Qu lists qualifiers. Specific qualifiers arc defined al the end of the report For moisture results, wet denotes rcsalt is not corrected for moisture and o/a denotes not applicable. 305166 3:S.OO 16:41:03 JO Report of Laboratory Analysis A/i %^ace Analytical ew Orleans Laboratory CUentID: TB031000 Project: VIRGIN ISLAND Lab ID: 209848 Description: None Method: CLP VolatUe Organics Prep Factor: X Leached: n/a Single Sample - Protocol P a c e A n a l y t i c a l Services, Inc. 1000 Riverbend Blvd. Suite F Saint Rose. LA 70087 Phone: 504.469.0333 Fax: 504.469.0555 CUent: ERTEC Site: None Project No.: 201156 Matrix: Water Prep Level: Water Units: ug/I CoUected: 10-Mar-OO Prepared: Sample Qu: % Moisture: n/a Batch: 01908 Target List: SR615MVWAT Received: 14-Mar-OO Analyzed: 14-Mar-OO 17:14PEI CAS Number 67-64-1 67-66-3 100-41-4 75-09-2 108-88-3 1330-20-7 Parameter Acetone (2-Propanone, Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (total) Dilution Result ND ND ND 2.10 J ND ND Qu All Reporting Limit 10.0 10.0 10.0 10.0 10.0 10.0 Reg. Limit 6 compound(s) reported ND denotes Not Detected at or above the adjasted reporting l i m i t DF denotes DQution Factor of extract. Tbe Prep Factor accounts for a non-rootine sample size Reporting L i m i t is corrected for sample size, dilution and moisture content If applicable. Q n lists qaalifien. Specific qualifiers are defined at the end of the report For moisture results, wet denotes result is not corrected for moisture and n/a denotes not applicable. 305167 3/:S00 16:41:03 "^^^ce Analytical^ New Orleans Laboratory ClientlD: FB031000 Project: VIRGIN ISLAND Lab ID: 209849 Description: None Method: CLP VolatUe Organics Prep Factor: i Leached: n/a Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l Services, Inc. 1000 Riverbend Btvd. Suite F Saint Rose. LA 70087 Phone: 504 469.0333 Fax: 504.469.0555 CUent: ERTEC Site: None Project No.: 201156 Matrix; Water Prep Level: Water Units: ug/1 CoUected: 10-Mar-OO Prepared: Sample Qu: % Moisture: n/a Batch: 01908 Target List: SR615MVWAT Received: 14-Mar-OO Analyzed: 14-Mar-OO 17:45 M I CAS Number 67-64-1 67-66-3 100^1-4 75-09-2 108-88-3 1330-20-7 Parameter Acetone (2-Propanone, Dimethyl keto Chlorofonn Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (total) Dilution Result ND ND ND 2.40 J ND ND Qu All Reporting Limit 10.0 10.0 10.0 10.0 10.0 10.0 Reg. Limit 6 compound<s) reported ND denotes Not Detected at or above i W adjusted reporting l i m i t DF denotes Dilution Factor of extrao. The Prep Factor accounts for a non-routine sample l i z c Reporting Limit is corrected for samp4e size, dilution and moisture content If applicable. Qn lilts qualifiers. Specific qualifiers are defined at the end of the r e p o r t For moisture results, wet d e n o l s r c i n k b not corrected for mobturc and n/a denotes not applicable. 305168 } : 3 00 16:JI:04 /^^^ace Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol Pace Analytical Services, Inc. 1000 Riverbend Blvd. Suite F Saint Rose. LA 70087 Phone: 504.469.0333 Fax: 504.469.0555 CUent ID: MW-12 Project: VIRGIN ISLAND Lab ID: 209850 Description: None Method: CLP VolatUe Organics Prep Factor: I Leached: n/a Client: ERTEC Site: None Project No.: 201156 Matrix: Water Prep Level: Water Units: ug/1 CoUected: 10-Mar-OO Prepared: Sample Qu: % Moisture: n/a Batch: 01908 Target List: SR61SMVWAT Received: 14-Mar-OO Analyzed: 14-Mar-OO 16:11211 CAS Number 67-64-1 67-66-3 100-4M 75-09-2 108-88-3 1330-20-7 Parameter Acetone (2-Propanone, Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (total) Dilution Result ND ND ND 2:00-J.- ND ND Qu ^^All. it Reporting Limit 10.0 10.0 10.0 .\) 10.0 10.0 10.0 Reg. Limit 6 compound(s> r ^ w r t e d iMnA VD denota Not Detected at or above the adjusted reporting l i m i t DF denotes DUution Factor of estract The Prep Factor accounts for a non-rontlne u m p l e size. Reporting L i m i t is corrected for sample size, dilution and moisture content if applicable. Q« lists qualifiers. Specific qualifiers arc defined at the end of the report For moisture results, wet denotes rcsalt a not corrected for moisture and n/a denotes not appUcahlc. 305169 J/:S'0O 16:41:04 ^ ^ / Report of Laboratory Analysis /^^.^ce Analytical^ New Orleans Laboratory Single Sample - Inorganic Parameters P a c e A n a l y t i c a l Services. Inc. 1000 Rivertiend Blvd. Suite F Saint Rose. •_/» 70087 P.hone: 504 469 C333 Fax: 504.469 0555 ClientlD: MW-12 Proiect: VIRGIN ISLAND Lab ID: 209866 Description: None ParameterName Method Batch Sulfate • EPA 375.2 02155 1 pararaeter(t) reported DF 5 Result 194. Qu CUent: ERTEC Site: None Proiect No.: 201156 Matrix: Water CoUected: 3/10/00 Reporting Units Limit mg/1 50.0 Prep. %Moisture: n/a Received: 3/14/00 Analysis 29-Mar-OO 12:03 LAK Reg. Limit \ D denotes Not Detected at or above the adjusted reporting l i m i t DF denotes DUution Fictor of final sample. PF denotes sample Prep Factor which accounts for a noo-routinc s Reporting Limit is corrected for sample size dilution and moisture content if applicable. Qu lists qualifiers. Specific qualifiers are defined at the end of the report For moisture results, wet denotes result is not corrected for moisture and n/a denotes not applicable: n p l e t i z c 305170 3/3O0O 13::3:}. ^ ^ c e Analytical^ New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l Services, inc. 1000 Riverbend Blvd, Suite F Saint Rose. LA 7C0S7 Phone: 504 469 0333 Fax: 504.469.0555 ClientlD: MW-14 Proiect: VIRGIN ISLAND Lab ID: 209851 Description: None Method: CLP VolatUe Organics Prep Factor: 1 Leached: n/a CAS Number Parameter Client: ERTEC Site: None Proiect No.: 201156 Matrix: Water Prep Level: Water Units: ug/1 CoUected: 10-Mar-OO Prepared: Dilution Result Qu Sample Qu: % Moisture: n/a Batch: 01908 TareetList: SR615MVWAT Received: 14-Mar-OO Analyzed: 14-Mar-OO 18:16DET Reporting Reg. Limit Limit 67-64-1 Acetone (2-Propanone, Dimethyl keto 67-66-3 Chloroform 100-41-4 Ethylbenzene 75-09-2 Methylene chloride (Dichloromethane 108-88-3 Toluene 1330-20-7 Xylene (total) 6 compouad(9) reported ND ND ND '1:90--;—i-Al+ ND ND 10.0 10.0 10.0 10.0 lO.O 10.0 '• f\ Ai --., ND denotes Not Detected at or above the adjusted reporting l i m i t DF denotes Dilution Factor of e i t r a c t The Prep Factor accounts for a noo-routinc sample size. Reporting Limit is corrected for sample size, dilution and moisture content If applicable. Qn lists qualifiers. Specific qnallAcrs arc defined at the end of the report For moisture results, wet denotes resatt is not corrected for moisture and a/* denota not applicable. 305171 3.28'00 16:41:04 t^""*'^/ Report of Laboratory Analysis ^ ^ c e Analytical^ New Orleans Laboratory Single Sample - Inorganic Parameters P a c e A n a l y t i c a l Services, Inc. 1000 Rivertiend Blvd. Suite F Saint Rose. LA 70087 Phone. 504 469.0333 Fax: 504.469.0555 Client ID: MW-14 Project: VIRGIN ISLAND Lab ID: 209867 Description: None CUent: ERTEC Site: None Project No.: 201156 Matrix: Water CoUected: 3/10/00 ParameterName Sulfate Method Batch DF Result Qu Reporting Units Limit %Moisture: n/a Received: 3/14/00 Prep. Analysis Reg. Limit EPA 375-2 02155 207. mg'1 50.0 29-Mar-OO 12:03 LAK 1 p«nnicter(s) reported ND denotes Not Detected at or above the adjusted reponiDg IlmiL DF denotes Dflntion Factor of ftnal sample. PF denotes sampte Prep Factor whldi accounts for a aon-roatine sample sin Reporting Limit is corrccttd for sample size, dilution and moisture content if applicable. Qo lists qualifiers. Specifk qualifiers are defined at tfie end of (lie report. For moisture results, wet denotes rcsnit is not corrected for moisture and n/a denotes not applicable. 305172 t.'JOOO 1- New Ohei Report of Laboratory Analysis ace Analytical "w Orleans Laboratory ClientlD: ASTVMP4D Project: VIRGIN ISLAND Lab ID: 2011117 Description: None Method: CLP Volatile Organics Prep Factor: j , Leached: n/a Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s , Inc. 1000 Riverbend Btvd, Suite F Saint Rose. LA 70087 Phone: 504 469 0333 Fax: SO4.469.05SS Client: ERTEC Site: None Project No.: 201382 Matrix: Water Prep Level: Water Units: ug/I CoUected: 30-Mar-OO Prepared: Sample Qu: % Moisture: n/a Batch: 02231 Target List: SR615MVWAT Received: 31-Mar-OO Analyzed: 06-Apr-OO 18:16 ACA CAS .Number 67-64-1 67-66-3 100-4M 75-09-2 108-88-3 1330-20-7 Parameter Acetone (2-Propanone. Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (total) Dilution Result Qu ND 2.40 J 1.30 J r.40—rrjAir jr. ND ^-iM--4-J:~-' l O l Reporting Limit 10.0 10.0 10.0 ! : 10.0 . 10.0 10.0 Reg. Limit 6 compound(s) reported AiM I ND denotes .Not Detected at or above the adjusted reporting l i m i t DF denotes DQution Factor of e i t r a c t The Ptep Factor Kconnts for a non-rooflne sample size. Reporting Limit is corrected for sampk siz^ dUutloo and moisture content If applicable. Qn tbts qualifiers. Specific qualifiers arc d<fuie<l at the end of tbe r e p o r t For motstnre resalts, wet dedotes resoH b aot corrected for moisture and n/a denotes not applicable. 305173 4.14/00 14:10:29 J^^Ci ace Analytical w Orleans Laboratory Repoit of Laboratory Analysis Single Sample - Protocol Pace Analytical Services, Inc. 10OO Rivertiend Btvd. Suite F SaJnl R o s e , i ^ 70087 Phone: 504 469 0333 Fax: 504.469.0555 ClientlD: ASTVMPID Proiect: VIRGIN ISLAND Lab ID: 2011123 Description: None Method: CLP Volatile Organics Prep Factor: I Leached: n/a CAS Number Parameter CUent: ERTEC Site: None Proiect No.: 201382 Matrix: Water Prep Level: Water Units: ugA CoUected: 30-Mar-OO Prepared: Dilution Result Qn Sample Qu: % Mobture: n/a Batch: 02231 TareetList: SR615MVW.\T Received: 31-Mar-OO Analyzed: 08-Apr-OO 15:27 ACA Reporting Reg. Limit Limit 67-64-1 67-66-3 100-41-4 75-09-2 108-88-3 1330-20-7 Acetone (2-Propanonc. Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene itotal) 6 compound(i) reported 100 100 100 100 100 100 ND ND 11100 ND ND 34100 D6 D6 D6 D6 D6 D6 1000 1000 1000 1000 1000 1000 NT) denotes Not Defected at or above ilic adjnstcd reporting limit DF denotes Dilution Factor of extract Tht Prtp Factor acconnts for a oon-routloe sampk size. Reportlns Limit ts corrected for sample she. dilution and aM>istnrc content If applicable. Qn Usts quallflerL Spcctnc quaUfWn art defined at the end of the report For moisture results, wet denotes result is oot corrected for moisture and n/a denotes not applicable. 305174 4.14.00 14 10:30 _Ml^Ci ace Analytical 'w Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e Analytical Services, Inc. 1000 Rivertiend Blvd. Suite F Saint Rose. LA 70087 Phone: 504 469 0333 Fax: 504 469. 0555 ClientlD: ASTVMP2D Project: VIRGIN ISLAND Lab ID: 2011124 Description: None Method: CLP Volatile Organics Prep Factor: I Leached: n/a CUent: ERTEC Site: None Project No.: 201382 Matrix: Water Prep Level: Water Units: ug/1 CoUected: 30-Mar-OO Prepared: Sample Qu: % Moisture: n/a Batch: 02231 Target List: SR615MWVAT Received: 31-Mar-OO Analyzed: 08-Apr-OO 15:56 ACA CAS Number Parameter Dilution Result Qu Reporting Limit Res- Limit 67-64-1 67-66-3 lOO-tl-4 75-09-2 108-88-3 1330-20-7 6 compoundU) Acetone (2-Propanone, Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene 1 tout) reported 50 50 50 50 50 50 ND ND 3170 -9I-.0- ND 12600 D6 D6 D6 -i ti-AII- D6 D6 A A'.r- > 5 500. 50O- 500. 500. 500. 500. ND denotes Not Detected at or above the adjasted reporting limit DF denotes Dtludoo Factor of estract Tbe Prep Factor accoonts for a aon-roatine sample SIZCL Reportbf Limit is corrected for sample slxe, dUutJon aad moisture content If applicable. Qu lists qualifiers. Speafic qualifiers are dcOaed at tbe end of the report For mobture results, wet denotes resak is not corrected for moistnre and n/a denotes aot apptkablc. 305175 4.14 00|4:10-:.l ^ace Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l S e r ^ i c & s , Inc. 10OO Riverbend Blvd. Suite F Saint R o s e . LA 7 0 0 8 7 P h o n e : 5 0 4 . 4 6 9 . C333 Fax: 5 0 4 . 4 6 9 0S5S ClientlD: .\STVMP3D Proiect: VIRGIN ISLAND Lab ED: 2011125 Description: None Method: CLP VolatUe Organics Prep Factor: 1 Leached: n/a CAS Number Parameter CUent: ERTEC Site: None Project No.: 201382 Matrix: Water Prep Level: Water Units: ug/1 CoUected: 30-Mar-OO Prepared: Dilution Result Qu Sample Qu: % Mobture: n/a Batch: 02231 Target List: SR615MVWAT Received: 31-Mar-OO .Analyzed: 08-Apr-OO 16:55 ACA Reporting Reg. Limit . Limit 67-64-1 67-66-3 100^1-4 75-09-2 108-88-3 1330-20-7 Acetone (2-Propanone, Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene Itotal) 6 conipound(s) reported 100 100 100 100 100 100 ND ND 6850 r40r~ ND 35900 D6 D6 D6 •-J\7-At|- /,-;;• D6 D6 1000 1000 1000 D ( / 1000 1000 1000 .^A Al:f\ ND denotes Not Detected at or above the Mljastcd reporting limit DF denotes Dilution Factor of extract Tlw Prep Factor accoonts for a aon-rootine sample loe. Reportiat ^'^"^^ is corrected for sample she, dihitkia and mobmre content If applicable. Qu llsa qualificn. Specific qaalifien are defined at tfac end of [he report. For moisture resulti. wet denotes result a not cnrrected for oMistare and n/a denotes aot appikabie. 7 305176 4 14.00 14:10:31 J^4iCi Report of Laboratory Analysis ace Analytical fiv Orleans Laboratory ClientlD: FPPVMPID Project: VIRGIN ISLAND Lab ID: 2011237 Description: None Method: CLP VolatUe Organics Prep Factor: J[ Leached: n/a Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s , Inc. 1000 Riverbend Blvd. Suite F Saint Rose. LA 70087 Ftione: 504.469. 0333 Fax: 504.469.05SS CUent: ERTEC Site: None Project No.: 201382 Matrix: Water Prep Level: Water Units: ug/1 CoUected: 30-Mar-OO Prepared: Sample Qu: % Moistiu-e: n/a Batch: 02231 Target List: SR615MVWAT Received: 03-Apr-OO Analyzed: 10-Apr-OO 13:03 ACA CAS Number 67-64-1 67-66-3 100-41-4 75-09-2 108-88-3 1330-20-7 Parameter Acetone (2-Propanone, Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (total) Dilution Result Qu ND 25.6 ND ^A2<iy-i^7M\ it ND 2.10 J Reportiiig Limit 10.0 10.0 10.0 / I J 10.0 10.0 10.0 Reg. Limit 6 compouod(s) reported AtAA 7-A'l ND denotes Not Detected i t or above the adjusted reporting l i m i t DF denotes Dtlutioo Factor of extract Tbe 1 ^ - ^ Factor acconnts for a ooo-rootlac u m p l e size Rcportln( L i m i t is corrected for sample lixc. dUution and molstare content If apptlcable Qu Gsts qualifiers. Specific qoaUfien are defined at tfac end of tbe r e p o r t For moisture results, «rct denotes resnll b not corrected for mobture and n/a denotes not a p p l k a b k . 305177 4/14.00 14:10:33 J^ace Analytical i.rfw Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l Services. Inc 10OO Rivertiend Blvd. Suite F' SaJnt Rose. LA 70087 Phone: 504.469.0333 Fax: S04.469 05S5 7 ^ CUentID: FPPVMP5D Project: VIRGIN ISLAND Lab ID: 2011238 , - '''^- V i' ' A-., i } Description: None f ' ly'V ' i Method: CLP VolatUe Organics Prep Factor: 1 Leached: n/a CUent: ERTEC Site: None Project No.: 201382 Matrix: Water Prep Level: Water Units: ug/1 CoUected: 30-Mar-OO Prepared: Sample Qu: % Moisture: n/a Batch: 02231 Target List: SR615MVWAT Received: 03-Apr-OO Analyzed: 10-Apr-OO 13:33 ACA CAS Number 67-64-1 67-66-3 100^1-4 75-09-2 108-88-3 1330-20-7 Parameter Acetone (2-Propanone, Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene Itotal) Dilution Result Qu ND 25.5 ND .2^0—1.J AW ~ i i ND 3.10 J Reporting Limit 10.0 10.0 10.0 )(,; 10.0 10.0 10.0 Reg. Limit 6 compound<i) reported * i \ .ND denotes Not Detected at or above the adjusted reportinf Umlt DF denotes Dilutioo Factor of extract TW Prep Factor accannts for a aon-r««tia« sample size. Reportlnt Limit is corrected for saaaple dzx, dUndoo and iBobCare cootcnt If appOcablc Qu Ibis qualificn. Specific qnall5en are defined at the end of the report For mobture results, wet denotes rcs«ll b aot corrected for mobturc aad a/a denotes not applicable. 305178 4.14 00 14:10:.. .1 Report of Laboratory Analysis ^ace Analytical New Orleans Laboratory ClientlD: FPPV>tP4D Project: VIRGIN ISLAND Lab ID: 2011241 Description: None Method: CLP Volatile Organics Prep Factor: i Leached: n/a Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s , tnc. 10OQ FUverbend Btvd. Suite r Saint Rose, LA 70087 Phone: S04.469 0333 Fax: SO4.469.05SS CUent: ERTEC Site: None Project No.: 201382 Matrix: Water Prep Level: Water Units: ug/I CoUected: 31-Mar-OO Prepared: Sample Qu: % Moisture: n/a Batch: 02231 Target List: SR615MVWAT Received: 03-Apr-OO Analyzed: 10-Apr-OO 14:02ACA CAS Number Parmmeter Dilution Result Qu Reporting Limit Reg. Limit 67-64-1 67-66-3 100^1-4 75-09-2 108-88-3 1330-20-7 Acetone (2-Propanone, Dimethyl keto Chloroform Ethylbenzene .Methylene chloride (Dichloromethane Toluene Xylene (total) ND 19.8 ND 2 ^ " ' J u'A'i 1 - /; ND ND 10.0 10.0 10.0 •A) '0 0 10.0 10.0 6 compound{s) reported A, \ * Ai ND denotes Not Detected «t or above the adjusted reporting Umlt DF denotes DQution Factxw of extract. The Prep Factor accounts for a non-rontinc sample size Reporting Limit Is corrected for sampte tizc; dilution and moisture content If applkable. Qn Usts qualifiers. Specific qaaHfkn are defined at the end of tbe report For mobture results, wet denota resnM b not corrected for moisture and n^a denotes not appUcabIc 305179 i 14.00 14:10:34 Report of Laboratory Analysis ace/Analytical V/ Orleans Laboratory Client ID: FB032900 Project: VIRGIN ISLAND Lab ID: 2011119 Description: None Method: CLP VolatUe Organics Prep Factor: \ Leached: n/a Single Sample - Protocol CUent: ERTEC Site: None Project No.: 201382 Matrix: Water Prep Level: Water Units: ug/1 CoUected: 29-Mar-OO Prepared: P a c e A n a l y t i c a l S e r v i c e s , Inc. 1000 Riverbend Btvd. Sijlte F ' Saint Rose. LA 70087 Phone: S04 46 9 0333 Fax: 504.46 9.0555 Sample Qu: % Moisture: nTa Batch: 02231 Target List: SR61SMVW.AT Received: 31-Mar-OO •Analyzed: 06-Apr-OO 18:45 ACA CAS Number ~67-64-l~" 67-66-3 100-41-4 75-09-2 I08-8S-3 1330-20-? 6 conipound<s) reported Parameter Dilution Result Qu Reporting Limit Reg. Limit Acetone (2-Propanonc. Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene 1 total) ND ND ND 1.40 J ND ND All 10.0 10.0 10.0 10.0 10.0 10.0 ND deaotes Not Detected at or above tfac adjusted repoaing limit DF denotes Dilution Factor of extract Tbe Prep Factor accooars for a noa-roniJne sample size. Reportiat Limit Is corrected for sample size, dDntion and moismre conieni if appUcablc. Ql liscs qoalifien. Specific qualiflcri are defined at the end of the report For moature resolcs, wet deaotes result a aol corrected for moisture and n/a denotes ool appUcable. 305180 4-14.00 14:10:9 ^ ^ ^ c t ^ K / onec ace Analytical V Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s . Inc. 1000 Rivertiend Blvd, Suite F Saint Rose. LA 70037 Phone: 504.469.0333 Fax: 5O4.469.055S CUentID: MW-1/3-29 Proiect: VIRGIN ISLAND Lab ID: 2011120 Description: None Method: CLP VolatUe Organics Prep Factor: 1 Leached: n/a CAS Number Parameter CUent: ERTEC Site: None Project No.: 201382 Matrix: Water Prep Level: Water Units: ug/I CoUected: 29-Mar-OO Prepared: Dilution Result Qu Sample Qu: % Moisture: n/a Batch: 02231 Target List: SR615MVWAT Received: 31-Mar-OO Analyzed: 08-Apr-OO 12:59 ACA Reporting Reg. Limit Limit 67-64-1 67-66-3 100-41-4 75-09-2 108-88-3 1330-20-7 Acetone (2-Propanone, Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (total) 6 conipound(s) reported 250 250 250 250 250 250 ND ND 21600 -3^55:— 463. 108000 D6 D6 D6 •liJ-All.- J D6 D6 • ,-A^A-':A'; i , 2500 2500 2500 ' 2500 2500 2500 nrf ND desoces Not Detected i t or above the adjusted reporting limit DF desoces DDotion Factor of extract. Tbe fVep Factor nccooiits for a non-routine sample size Reportfaf Limit U corrected for sample size, dUntloo and aMbmre content if applicable. Qo Bsn qoaUfien. Specific qualMcn are defined at the ettd of tbe report For mobmre resnitv wet denotes resah u not corrected for moUlurc and n/a deaotes aot applicable. 305181 4.14-00 14:10:30 ^ ^ C i ^ K v Orle^ Report of Laboratory Analysis ace/Analytical W Orleans Laboratory ClientlD: MW-10/3-30 Project: VIRGEV ISLAND Lab ID: 2011121 Description: None Method: CLP VolatUe Organics Prep Factor: I Leached: n/a Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s , Inc 1000 Riverbend Btvd. Suite F Saint Rose. LA 70037 Phone: 504 469 0333 Fax: SO4.469.0555 Client: ERTEC Site: None Project No.: 201382 Matrix: Water Prep Level: Water Units: ug/I CoUected: 30-Mar-OO Prepared: Sample Qu: % Moisture: n/a Batch: 02231 Target List: SR615MVWAT Received: 31-Mar-OO Analyzed: 08-Apr-OO 19:23 ^CA CAS Number 67-64-1 67-66-3 100-41-4 75-09-2 108-88-3 1330-20-7 Parameter Acetone (2-Propanone, Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (total) Dilution Result ND ND ND — 1.60- ND -2:30- -J- - i Qu rj-An— i i ! Reporting Limit 10.0 10.0 10.0 0 0 100 10,0 V I : 10.0 Reg. Limit 6 compound(t) reported iVw ND deaotes Not Detected al or above the adjusted reporting Gmit. OF denotes DUution Factor of extract Th< Prep Factor accoonts for a non-routine sample size Reporting L i m i t b corrected for sample stia. dUution and mobttue cootent If applkable. Qn Usts quaUflers. Specific qualifiers arc defined at the end of tbe report For mobture results, wet denotes resak b oot corrected for mmaxmrt and o/i denotes oot applicable. 305182 4 14 00 14:10:30 j ^ a c e Analytical i,.^w Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s , Inc. 10OO Rivertiend Blvd. Suite F Saint Rose, LA 70087 Phone: 504 469 0333 Fax: S04.469.05SS CUentID: MW-8/3-29 Project: VIRGIN ISLAND Lab ID: 2011122 Description: None Method: CLP VolatUe Organics Prep Factor: I Leached: n/a Client: ERTEC Site: None Project No.: 201382 Matrix: Water Prep Level: Water Units: ug/1 CoUected: 29-Mar-OO Prepared: Sample Qu: % Moisture: n/a Batch: 02231 Target List: SR61SMVWAT Received: 31-Mar-OO Analyzed: 08-Apr-OO 20:22ACA CAS Number 67-64-1 67-66-3 I0O-41-4 75-09-2 108-88-3 1330-20-7 Parameter Acetone (2-Propanone, Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene iiotai) Dilution Result Qu ND ND 2.70 J h60-.j-U-Aij /;,: ND n.6 Reporting Limit 10.0 10.0 10.0 / ) 10.0 10.0 10.0 Reg. Limit 6 compoundisl reported .ND denotes .Not Detected at or above dK adjusted reporting limit OF denotes DQution Factor of eitract The pyep Factor accounts for a non-roottne sample size. Reportiat Limit b corrected for sample size, dilution and moisture content If applicable. Qu Ibu qoalifiert Specific qualificn arc defined at the end of the report For moisture results, wet denotes raaJi b aot corrected for moisture and a/a denotes not applicable. 305183 4.14.00 14:10:30 J f ^ c e Analytical .. «v Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol Pace Analytical Services. Inc. 10OO Riverbend Btvd. Suite F Saint Rose. LA 70087 Phone: 504 469 0333 Fax: S04.469. OSSS ClientlD: FB033000B Proiect: VIRGIN ISLAND Lab ID: 2011126 Description: None Method: CLP Voladle Organics Prep Factor: 1 Leached: n/a CAS Number Parameter 67-64-1 Acetone (2-Propanone, Dimethyl keto 67-66-3 Chloroform 100-41-4 Ethylbenzene 75-09-2 .Vlethylene chloride (Dichloromethane 108-88-3 Toluene 1330-20-7 Xylene Itotal) 6 campound(i) reponed CUent: Site: Project No.: Matrix: Prep Level: Units: CoUected: Prepared: ERTEC None 201382 Water Water ug/1 30-Mar-OO Dilution Result 18.7 7j ND ND 2.00 J ND 1.30 J Qn All A l l Sample Qu: •/• Moistiire: n/a Batch: 02231 Target List: SR615MVWAT Received: 31-Mar-OO Analyzed: 08-Aor-OO 17:54 ACA Reporting Reg. Limit Limit 10.0 10.0 10.0 10.0 10.0 10.0 ND denotes Not Detected at or above tW adjusted reportlnc l i m i t DF denotes Dilutioo Factor of extract T I M Prep Factor acconnti for a oon-routioc sample size. Reportiaf Limit b corrected for sample size dilation and aM>lsture content If applicable Qo I b a qnalifiers. Specific qualifiers are defined at the end of tbe r e p o r t For mobture results, wet denota reaak b aot corrected for mobture and n/a denotes aot applicable. 305184 4 1X00 14:10:31 ^^jf^Face Analytical , *ew Orleans Laboratory CUentID: TRIP BLANK Project: VIRGIN ISLAND Lab ID: 2011127 Description: None Method: CLP VolatUe Organics Prep Factor: J_ Leached: n/a Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s , Inc. 1000 Riverbend Blvd. Suite = Saint Rose. LA 70037 Phone: 504 469.0333 Fax: S04.469 0S55 CUent: ERTEC Site: None Project No.: 201382 Matrix: Water Prep Level: Water Units: ug/1 CoUected: 30-'Mar-00 Prepared: Sample Qu: % Moisture: n/a Batch: 02231 Target List: SR615MVWAT Received: 31-Mar-OO Analyzed: 06-Apr-OO I5:49ACA CAS Number 67-64-1 67-66-3 100-41-4 75-09-2 108-88-3 1330-20-7 Parameter Acetone (2-Propanone, Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (total) Dilution Result ND ND ND 1.40 J ND ND Qu All Reporting Limit 10.0 10.0 10.0 10.0 10.0 10.0 Reg. Limit 6 compound(s) reported VD denotes .Not Detected at or above tbe adjusted reporting limit DF denotes OQuUoa Factor of extract The Prep Factor accounts for a ooo-routioe sample size. Rrportlnt Limit is corrected for sample size, dilutioa and moismre cootent If applicable. Qu lists qnaUfiers. Specific qnalifiers are defined at the end of the report For mobture resulti, wet denotes rcsalt b tMt corrccied for moisture and o/a denotes not applicable. 305185 4/14,00 I4:10:.-l j^pace Analytical ivew Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s . Inc. 1000 Rivertiend Blvd. Suite F Saint Rose. LA 7 0 0 8 7 P h o n e : 504.469 -3333 F a x : 504.469.0555 CUentID: MW-6/3-29 Proiect: VIRGIN ISLAND Lab ID: 2011128 Description: None Method: CLP Voladle Organics Prep Factor: 1 Leached: n/a CAS Number Parameter CUent: Site: Project No.: Matrix: Prep Level: Units: CoUected: Prepared: ERTEC None 201382 Water Water ug/1 29-Mar-OO DitutioD Result Qu Sample Qu: % Moisture: n/a Batch: 02231 Target List: SR615MVWAT Received: 31-Mar-OO Analyzed: 08-Apr-OO 18:24 ACA Reporting Reg. Limit Limit 67-64-1 67-66-3 100^1-4 75-09-2 108-88-3 1330-20-7 Acetone (2-Propanone, Dimethyl keto Chloix)fonn Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene .total) 6 compound(l) reported 100 100 100 100 100 100 ND ND 13800 ND 146. J 76600 D6 D6 D6 D6 1 D6 D6 1000 1000 1000 1000 1000 1000 A\ \ V S-:A ND denotes Not Detected at or above tike adjaitcd reportiog limit. DF denotes DQution Factor of eitract Tbe Prep Factor accounts for a non-routine sample size. Reporting Limit is corrected for sampk mt. dlhitioa and moismre content If applicable. Qu Usts qualiflers. Specific qualifiers are defined at tbe end of the report For moisture results, wet denotes resalt b aot corrected for mobture and iVa denotes not applkable. 305186 4/14 00 |4:10:J2 jl^Pace Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol Pace Analytical Services, Inc. 1000 Riverbend Blvd. Suite F Saint Rose. LA 70087 Phone: S04.469 0333 Fax: S04.469.0SSS CUentID: MW-6/3-29 Proiect: VIRGIN ISLAND Lab ID: 2011128DL Description: None Method: CLP Volatile Organics Prep Factor: 1 Leached: n/a CAS Number Parameter CUent: ERTEC Site: None Project No.: 201382 Matrix: Water Prep Level: Water Units: ug/l CoUected: 29-Mar-OO Prepared: Dilution Result Qti Sample Qu: % Moisture: n/a Batch: 02231 TareetList: SR615MVWAT Received: 31-Mar-OO Analyzed: 10-Apr-OO 11:35 ACA Reporting Reg. Limit Limit 67-64-1 67-^6-3 100-41-4 75-09-2 108-88-3 1330-20-7 Acetone (2-Propanone. Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (total) 6 coaipouad^s) reported 250 250 250 250 250 250 ND ND 12400 938.* ND 6-5600 Dl Dl Dl - ^ / All. Dl Dl i 2500 2500 2500 2500 2500 2500 N - ; \ ' \ .\ V- ND denotes Not Detected at or above tJkc adjasted reportiog Umlt DF deaotes Dilation Factor of eitract The Prep Factor acconau for a noa-rouciac sampk size. Rcpartittg Limit b corrected for sampk 4xt, dOntioo and mobtnre coatent If applkabk. Qa Iscs qualifiers. Specifk quallfkrs are defined at the end of the report For mobtarc resold, wet denoto resatt b not corrected for mobture and n/a denotes aot ippUcabk. 305187 4/1400 14:10:}: mPaci Report of Laboratory Analysis ace Analytical "w Orleans Laboratory CUent ED: TB033100 Project: VIRGIN ISLAiND Lab ID: 2011235 Description: None Method: CLP VolatUe Organics Prep Factor: J_ Leached: n/a Single Sample - Protocol P a c e Analytical Services, Inc. 1000 Rivertiend Btvd. Suite F Saint Rose, LA 7O087 Phone: 504.469.0333 Fax: 504.469.0555 CUent: ERTEC Site: None Project No.: 201382 Matrix: Water Prep Level: Water Units: ug/1 CoUected: 31-Mar-OO Prepared: Sample Qu: % Moisture: n/a Batch: 02231 Target List: SR615MVWAT Received: 03-Apr-OO Analyzed: 10-Apr-OO 12:04 ACA CAS Number 67-64-1 67-66-3 100-4M 75-09-2 108-88-3 1330-20-7 Parameter Acetone (2-Propanone. Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (total) Dilution 1 1 1 1 1 1 Result ND ND ND 4.30 J ND ND Qu All Reporting Limit 10.0 10.0 10.0 10.0 10.0 . 10.0 Reg. Limit 6 compound(s) reponed ND denotes Not Detected at or above the adjusted reporting Baalt DF denotes Dilution Factor of extract Tbe Prep Factor acconnfi for a uoo-rontine sampk size. Reporting Limit is corrcded for sampk size, dltotkn aad mobtarc coolent If appttcabk. QQ Ibti qoallfters. Spedflc qaallfkn are defined at the end of the report For moisture resnlts, wet denotes rcsaM b not corrected for mobtmrc and o/a denotes aol applkabk. 305188 4/14,00 14:10:3; Jl^ci ace Analytical w Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s . Inc. 1000 Riverbend Blvd. Suite F Saint Rose. LA 70087 Phone: S04.469.0333 Fax: 504.469. OSSS Client ID: FB033000A Project: VIRGIN ISLAND Lab ID: 2011236- Description: None Method: CLP VolatUe Organics Prep Factor: I Leached: n/a CUent: ERTEC Site: None Project No.: 201382 Matrii: Water Prep Level: Water Units: ug/1 CoUected: 30-Mar-OO Prepared: Sample Qu: % Moisture: n/a Batch: 02231 Target List: SR615MVWAT Received: 03-Apr-OO Analyzed: lO-Apr-00 12:34 ACA CAS Number 67-64-1 67-66-3 lOO^M 75-09-2 108-88-3 , 1330-20-7 Parameter Acetone (2-Propanone, Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (tout) Dilution Result 16.3 rr ND ND 3.60 J ND ND Qu All All Reporting Limit 10.0 10.0 10.0 10.0 10.0 10.0 Reg. Limit 6 compouad<s) reported ND denotes Not Detected at or above the adjusted reporting l i m i t DF denotes Dilutioo Fsctor of extract Tbe IVep Factor accounts for a oo»-roaiine sampk size. Reporting Limit b corrected for sample size, dlhitton and m o l s a r e content If oppHcabk. Qu Ibts qoalifkrs. Specific quallfkrs arc defined at tbe end of the r e p o r t For mobture results wet denota result b oot corrected for mobture and o/a denotes not a p p l i c a b k 305189 4/14/00 14:10:32 "jmf^ci ace Analytical w Orleans Laboratory Report of Laboratory Analysis Single Sample - ProttKol P a c e A n a l y t i c a l S e r v i c e s . Inc. 1000 Riverbend Blvd. Suite F Saint Rose. LA 70087 Phone: 504.469.0333 Fax: 504.469. OSSS ClientlD: MW2/33IA Project: VIRGIN ISLAND Lab ID: 2011239 Description: None Method: CLP VolatUe Organics Prep Factor: i Leached: n/a CUent: ERTEC Site: None Project No.: 201382 Matrii: Water Prep Level: Water Units: ug/1 CoUected: 31-Mar-OO Prepared: Sample Qu: % Moisture: n/a Batch: 02231 Target List: SR61SMVWAT Received: 03-Apr-OO Analyzed: 10-Apr-OO 15:31ACA CAS Number 67-64-1 67-66-3 I0O-4M 75-09-2 108-88-3 1330-20-7 Parameter Acetone (2-Propanone, Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (toUl) Dilution Resalt ND 40.7 ND • 3 : 2 0 - n ND 1.40 J Qu -All"" Reporting Limit 10.0 10.0 10.0 /,•);>' 10.0 10.0 10.0 Reg. Limit 6 compound(s) reported :"\ / ND denotes .Not Detected it or above iW adjusted reporting limit DF denotes DUntk>o Factor of eitract The Prep Factor accounts for a noo-roatlnc sampk slxe. Reporting Limit Is corrected for sampk lizc, dDntkn and mobtnre content If appScabk. Qn Ibts qualifkrs. Specifk qna&lkrs are defined at the end of tbe report For mobtnre results, wet denotes resnJi b not corrected for mobturc and n/a desotn am applkabk. 305190 4/14,00 14:10:33 Report of Laboratory i<Viialysis ^ace Analytical New Orleans Laboratory ClientlD: MW2/33I Project: VIRGIN ISLAND Lab ID: 2011240 Description: None Method: CLP VolatUe Organics Prep Factor: _1 Leached: n/a Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s . Inc. 1000 Riverbend Blvd. Suite F Saint Rose. LA 70087 Phone: 504.469. C333 Fax: 504.469.0555 CUent: ERTEC Site: None Project No.: 201382 Matrii: Water Prep Level: Water Units: ug/I CoUected: 31-Mar-OO Prepared: Sample Qu: % Moisture: n/a Batch: 02231 Target List: SR615MVWAT Received: 03-Apr-OO Analyzed: lO-Apr-00 16:00 ACA CAS Number Parameter Dilution Result Qu Reporting Limit Reg. Limit 67-64-1 67-66-3 100-4M 75-09-2 108-88-3 1330-20-7 Acetooe (2-Propanone, Dimethyl keto Chloroform Ethylbenzene -Methylene chloride (Dichloromethane Toluene Xylene (total) ND 38.6 ND 10.0 10.0 10.0 2:40" ; t ; All- jf;,!^: 10.0 ND ND lO.O 10.0 6 compound(s) reported •ifH % .\D denotes Not Detected at or above tht adjusted reporting limit DF denotes Dilution Factor of citr«ct TW Prep Factor accoonts for a oon-rontinc sampk size. Reportlttg Limit Is corrected for sampk size, dOntkn and moisture content if applkabk. Qu Ibts qualifiers. Spcdfk quaUfkn tre deflned at the end of the report iilt« m/mt A^^Mt^ •r•m*^»^^ fnr mnt«*nn nil ni» dMlOtet nat annllrahl* 305191 4/14.00 14:10:33 <7 ^^ace Analytical Naw Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s . Inc. 10OO Rivertiend Btvd, Suite F ' Saint Rose, LA 70087 Phone: S04.469 0333 Fax: 504.469. OSSS Client ID: MW7/331 Project: VIRGIN ISLATQ) Lab ID: 2011242 Description: None Method: CLP VolatUe Organics Prep Factor: \_ Leached: n/a CUent: ERTEC Site: None Project No.: 201382 . Matrix: Water Prep Level: Water Units: ug/1 CoUected: 31-Mar-OO Prepared: Sample Qu: •/• Moisture: n/a Batch: 02231 Target List: SR615MVWAT Received: 03-Apr-OO Analyzed: 10-Apr-OO 16:30 ACA CAS Number 67-64-1 67-66-3 100-41-4 75-09-2 108-88-3 1330-20-7 Parameter Acetone (2-Propanone, Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (total) IMhition Result Qn ND 1.90 J ND J : 8 0 - - t y A i 1 ;-0 ND ND Reporting Limit 10.0 10.0 10.0 0 10.0 10.0 lO.O Reg. Limit 6 compound(i) reported \i\r ,Anf} ND denotes Not Detected it or above tbe adjusted reporting Umlt DF denotes DUuUoa Factor of eztnct Tbe Prep Factor accooaCs for a aon-roatine sampk size. ReponJog Limit Is corrected for sampk sine, dilution and moUiure coatent If applkai>k. Qo Usts quallfkrs. Spedfk quallfkrs are defined at Ibc end of the report For mobtnre results, wet denotes rcsall b aot corrected for mobture aad ofa dcnotea aoC applkabk. 305192 4 1400 14:10:34 j^pace Analytical • .aw Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol Pace Analytical Services. Inc. 10OO Rivertiend Blvd, Suite F Saint Rose. LA 70087 Phone: 504.469 0333 Fax: S04.469.0555 CUentID: FB033100B Proiect: VIRGIN ISLAND Lab ID: 2011243 Description: None Method: CLP VolatUe Organics Prep Factor: 1 Leached: n/a CAS Number Parameter 67-64-1 Acetone (2-Propanone, Dimethyl keto 67-66-3 Chloroform lOO-JM Ethylbenzene 75-09-2 Methylene chloride (Dichloromethane 108-88-3 Toluene 1330-20-7 Xylene (total) & conipouad(t) reported CUent: ERTEC Site: None Project No.: 201382 Matrii: Water Prep Level: Water Units: ug/1 CoUected: 31-Mar-OO Prepared: Dilution Result I 19.8 T I ND 1 ND 1 2.80 J 1 ND 1 ND Qu All All Sample Qu: % Moisture: n/a Batch: 02231 TareetList: SR615MVWAT Received: 03-Apr-OO Analyzed: 10-Apr-OO 14:32 ACA Reporting Reg. Limit Limit 10.0 10.0 10.0 10.0 10.0 10.0 ND d<so(a Not OMetlol il or ibovt lk< tdjaitcd rcfMnln( UmiL DF dtfwUi DDalioa Factor of extract. r W Prep Factor accounts for a aoa-raattnc umpte she. Reportiat Limit a corrected for sampte liie. dihidon aiMJ noisliin coBlent ifippUaUc Qo &sts qnalifiers. Specific qnalifiers arc deflned at liie end of tfac report For atoisrare resulti, wet denola resalt is not corrected for moistart and n/a denotes not applicable. 305193 4/1400 14:10:34 j^^Ci ^ ^ ^ / v Orlei Report of Laboratory Analysis aceAnaJytlcal W Orleans Lat>oratory Client ID: MW3 Project: VIRGIN ISLAgNfD Lab ID: 2011244 Description: None .VIethod: CLP VolatUe Organics Prep Factor: I Leached: n/a Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s . Inc. 10O0 Riverbend Blvd. Suite F Saint Rose. LA 70087 Phone: S04.469.0333 Fax: 504.469.0555 CUent: ERTEC Site: None Project No.: 201382 Matrii: Water Prep Level: Water Units: ug/1 CoUected: 31-iMar-OO Prepared: Sample Qu: % Moisture: n/a Batch: 02231 Target List: SR61SMVWAT Received: 03-Apr-OO Analyzed: lO-Apr-00 16:59 ACA CAS Number 67-64-1 67-66-3 100-41-4 75-09-2 108-88-3 • 1330-20-7 Parameter ACOODC (2-Propanone, Dimethyl keto Chlotoform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (total) Dilation Result ND ND ND i6ft ND ND Qu -JUVM-l iOl Reporting Limit 10.0 10.0 10.0 10.0 10.0 10.0 Reg. Limit 6 cofflpoundls) reported t. ,1 305193A ND d^HKcs Not Detected at or above (he adjusted reporting Kadt DF denotes DQution Factor of extract. Tbe Prep Factor accoaats for a noo-rondnc sampk size. Reporting U n i t U corrected for s a ^ p k dae, dOutloa and osotstire cootent if appScabk. Q« b o q a a U f k r v Specific qnalifkrs arc defined at tbe end of t k t r e p o r t Far aocstttre resulti, wet denota r o n A is not corrected for BobQu-c and o/a denotes not applkabk. -tl4 00 14:10:34 "^^^Pace Analytical . .aw Orleans Laboratory Report of Laboratory Analysis Smgle Sample - Protocol P a c e A n a l y t i c a l Services. Inc. 1000 Rivertiend Btvd. Suite F Saint Rose, LA 70087 Phone: 504 469.0333 Fax: 504.469.0555 ClientlD: FB033100A Project: VIRGIN ISLAND Lab ID: 2011245 Description: None Method: CLP VolatUe Organics Prep Factor: I Leached: n/a CUent: ERTEC Site: None Project No.: 201382 Matrix: Water Prep Level: Water Units: ug/1 CoUected: 31-Mar-OO Prepared: Sample Qu: % Moisture: n/a Batch: 02231 Target List: SR615xVrVW.AT Received: 03-Apr-OO Analyzed: lO-Apr-OO 1S:01ACA CAS Number Parameter Dilution Result Qu Reporting Limit Reg. Limit 67-64-1 67-66-3 100-41-4 75-09-2 108-88-3 1330-20-7 Acetone (2-Propan6ne. Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (total) 20.0 J ND ND 3.00 J ND ND A l l All 10.0 10.0 10.0 10.0 10.0 lO.O 6 compoundfs) reported ;VD denotes Not Ektectcd at or above tke adjnstcd reporting Umlt DF denotes Dilation Factor of extract. T>c Prep Factor accounts for a non-rontlne saaipk slxe. Reporting Limit U corrected for sampk itae, dilutioa and nioisture cootcat If applkabk. Qu Usts qnailflen. Specific qnaU6ers t n defined at the end of tbe report For moisttire results, wet denota result is not corrected for mobtnre and n/a denotes not applkabk. 305194 4/14,00 14:10:35 Jff^ce Analytical New Orleans Laboratory Report of Batch Surrogate Recovery Organic Protocol - Single Batch P a c e A n a l y t i c a l S e r v i c e s , Inc. 1000 Rivertiend Btvd. Suite F Saint Rose. LA 7O087 Phone: S04.469.0333 Fax: 504.469.0555 Method: Water GC/MS Volatile Organics Lab ID 0223IBIK05 02231B1K08 02231BIK10 02231 MS 0223IMSD 0223 ISA 10 2011115 201II17 2011119 2011120 2011121 2011122 2011123 1 2011124 2011125 2011126 2011127 2011128DL 2011235 2011236 2011237 20I123S 2011239 2011240 2011241 2011242 2011243 2011244 2011245 QC limits: BLANK BLANK BLANK MS MSD LGS DLT Surl: Toluene-<18 (S) Surl %Rec 105 104 109 99 103 ' • ^ 106 110 107 100 96 104 97 103 104 101 106 104 106 109 108 110 110 104 109 107 105 104 107 88-110 Sur 2: 4-Bromonuorobenzene (S) Sur3: 1,2-Dichloroeth iane-d4 (S) Sur 2 %Rec 104 97 93 .89 91 85 102 108 104 106 95 104 105 101 111 100 97 106 98 100 97 97 94 91 101 94 95 .93 94 86-115 Sur 3 %Rec 96 90 98 106 101 97 96 99 92 93 90 90 94 92 95 94 99 103 104 102 102 100 100 98 95 lOl 95 99 95 76-114 Report: Batch: Sur 4 %Rec 201382 02231 SurS %Rec Sur 6 %Rec Sur 7 %Rec Surg y.Rec • denotes torrogate recovery outside of QC liraiti. D denotes forrofafe recovery i i outside o f Q C Umia doe lo t a m p k dOucko. aad it aot conildcred an ezairska. A Lab Q) cooststinc of a batdi number with a B infllx b a method b k a k . A Lab a> coosbtBi| of a batch number with a S sufllz is an LCS. A Lab (D n i t h a MS satTb is a m a t r i i spike. A Lab ID with a MSD tafftt b a matrix spike dopUcate. 4/14/00 l4:I0-.36 305195 j f ^ c e Analytical New Orleans Laboratory Report of Quality Control Organic Protocol - Single Batch P a c e A n a l y t i c a l S e r v i c e s . Inc. 1000 Rivertiend Blvd. Suite F Saint Rose. LA 70087 Phone: 504.469.0333 Fax: 504.469.OSSS Method: Water GC/MS Volatile Organics ParameterName LCS LCS LCSD LCS Spike %Rec %Rec RPD Project No.: 201382 Batch: 02231 MS MS MSD (1)MS DUP Spike V.Rec %Rec RPD RPD Units: ug/1 QC Limits LCS MS/MSD Max RPD Qu 1,1 -Dichloroethene (Dichloroethylene) Trichloroethene (Trichloroethylene) Benzene Toluene Chloro benzene 5 rampoQaiKi) reported 50.00 50.00 50.00 50.00 50.00 131 116 110 121 112 50.00 50.00 50.00 50.00 50.00 127 117 116 121 117 127 122 119 129 121 0 4 3 6 3 0 4 3 6 3 61- 71 - 76- 76- 75- • 145 • 120 • 127 •125. •130 61- 71- 76- 76- 75- •145 •120 •127 •125 •130 14 14 Ql 11 13 Ql 13 * denotes recovery outside of QC limiiL MS ipike concentrations are not comctcd for mobture cootent of the ipQced sampk. (1) .MS RPD is calculated via SW-«4« rvks: on the basb of spiked sampk canccntrailoni radicr ihaa ipifce recoverks. 305196 4114.00 14:10:36 INSTRUMENT RUNLOG i.^i£ m 4- MS. VGA Q4Q6Q0 7:^16^ Iistrament: R Cohimn: RTX 30X2 60m Injector: 250C Initial oven Temp: 40C/6mn Tamp ramp: 8^3C/nun Final ovea toap: t J S ^ O C Carrier. Hs 30nil/mn Tuno Standard: B F e > - 3 4 ' 7 - 1 < - 6 f 1^10 MS t o n range: 35.300amu EM Voltage: Trap: Tenax/Silica gel Forge: 30ml/min I Imin Dcwrb: 180C 4iiiin Bake: 180C 7min C»librxtioa Standard: ifT'2.C^CLfSV [ W ^ FUc Lab ID Batdt QF DF DaU Tbne Conunenlj 6 / « 0406K02 2 0406K03 3 0406K04 * 0406K05 J 0406K07 6 0406K09 7 0406K11 « 0406K12 0406K13 0406K14 0406K15 0406K16 0406K17 0406K18 0406K19 6 0406K20 7 0406K21 8 0406K22 9 0406K23 20 0406K24 21 0406K25 22 0406K26 23 0406K27 24 0406K28 25 0406K29 BFB VST-DOIO VST-D020 VST-D050 VST-DIOO VST-D200 02231BK05 02231BK05 2011127 t / 02331SK06 2011115-^ 0223 IMS 0223 IMSD 20111171^ 2011119 FLU-SH 2011120' 2011121 2011122 2011123 FLU-SH 2011124 2011125 2011126 2011128 / " 02231 02231 02331 02231 02231 02231 02231 02231 02231 02231 02231 -(v^» 02231 Qjr 02231 02231 02231 06-Apr.OO 06-Apr-OO 06-/>qpr-00 06-Apr-OO 06-Apr-OO 06-Api-OQ 06-Apr-OO 06-Apr-OO 06-.Apr-00 06-Apr-OO 06-Apr-OO 06-Apr-OO 06-Apr-OO 06-Apr-OO 06-Apr-OO 06-Apr-OO 06-Apr-OO 06-Apr-OO 06-Apr-OO 06-Apr-OO 06-Apr-OO 06-Apr-OO 06-Apr-OO 06-Apr-OO 06-/>Lpr-OO 9:57 10:27 10:56 11:25 12:24 13:23 14:43 15:13 15:49 16:18 16:48 17:17 17:46 18:16 18:45 19:15 19:44 20:13 20:43 21:12 21:42 22:11 22:40 23:10 23:39 OK r^ ff / f < • 5f7tJx^ Loa^/'^c^ ^ e - S^'dixf uJCiHCfr- i- ^ ^ 1'. g'w 6 CO CO. / ^ ^ I ' T M C Co P.R. l-s'ftw C^aci< ft.H t-yTTT^ Go Ct3 4- -p.^ 305197 PlaOui>lu> V. 2 H\Vt» 1104:13 INSTRUMENT RUNLOG * ^m. J^IS. VOA Q4Q80Q ni^M^i Instrument: K Cohuno: RTXJ02.2 60m Injector 150C Initial OVCD Temp: 40C/6mn Tanp ramp: 8^C/n>in FouJ area temp: I 3 5 ^ 0 C Ourier: Ho 30nil/mn Tunc Standard: R F B ^ 3 l 7 - i C - g / n B (O MS scan range: 35-300ama EM Voltage: Trap: Tenax/Silica gel Forge: 30ml/inin llmin Dcaorfa: 180C 4min Bake: ISOCTmin Calibration Standard: " S y i ' Z ^ - C C P S O \.5b6(fi FUc U b I D Batch QF DF Date Time Commentj ^ » 0408K01 BFB 2 0408K02 VST-D050 02331 3 0408K03 02231BK08 02231 * 0408K04 /b2231BK08 02231 3 0408K05 v/2011120X*<*^ 02231 « 0408K06 X F L U - S H 7 0408K07 i/2011l21—f 10 02231 8 0408K08 /2011122-/=«^ 02231 9 0408K09 FLU-SH 0 0408K10/20111231/ 02231 1 0408K11 2011124»/ 02231 2 0408K:12 FLU-SH- 3 0408K13 2011125'^ 02231 4 0408K14 FLU-SH^ 3 0408K15 2011126v^ 02231 6 0408K16 2011128/X^^ 02231 7 0408K17 F L U - S H ^ ' * / / ^ 8 0408K18 2011121;^ 02231 9 0408K:i9 FLU-SH 20 0408K20 2011122-/ 02231 10l> I V 1 1 1 1 250 "^ 250 1 1 lOOX^lOO 2 5 0 / 250 1 1 100*^ 100 5 0 " ^ 50 1 / 1 lOO^C/^OO 1 n U ^ 1 1 100 "^uAOO 1 1 l A 1 1 I A 08-Apr-OO 08-AprrOO 08-Apr-OO 08-Apr-OO 08-Apr-OO 08-Apr-OO 08-Apr-OO 08-Apr-OO 08-Apr-OO 08-Apr-OO 08-Apr-OO 08-Apr-OO 08-Apr-OO 08-Apr-OO 08-Apr-OO 08-Apr-OO 08-Apr-OO 08-Apr-OO 08-Apr-OO 08-Apr-OO 10:52 11:24 12:00 12:29 12:59 13:28 13:58 14:27 14:57 15:27 15:56 16:26 16.55 17:25 17:54 18:24 18:53 19:23 19:52 20:22 •7^^93o.(, >r Cfi-r.i . H ^ A l . fce/oij helouj OK. /if~ O K H i . - 3Y/.3 75/. 6 o ^ / / j -559.3 O K H-. _- /.3s ^fl i : 2 s o /K^745"S- t^(La> o < A6--Q.^ o ^ ^ ^ / / • ^ c 2^1> 305198 PnOwPba V. : VI lAU V H i S I INSTRUMENT RUNLOG '•MlS J^IS_ VOA 041QQO M (0(1 loxtnimcnt: K Column: RTX 302.2 60m Injector. 250C Initial oven Temp: 40C/6mn Temp ramp: 8^5C/mxn Fiiul oven temp: IS 5^S0C Carrier: He 30ml/nin Tune Standard: B F B / 3 > < ; T - / (, - feFQ/p Calibtation Standard: 3<? 7 - ' ^ " ^ C / ^ S D MS scan range: 35-300amii EM Voltage: Trap: Teoax/Silica gel Purge: 30ml/min 1 Imin Dootb: 180C4niin Bake: I80C 7min 3^ol F^ LablD Batdi QF DF Date Time Commmti 1 0410K01 V / B F B 2 0410K02 VST-D050 02331 3 G410K03 02231BK10 02231 4 0410K04 ^02231BK10 02231 J 0410K05 ^011128 tTu 02231 6 0410K06 -^2011235 02231 7 0410K07 /2011236 02231 « 0410K.08 /2011237 02231 9 0410K09 /2011238 02231 10 0410K10 /2011241 02231 11 0410K11 /2011243 02231 12 0410K12 /2011245 02231 13 0410K13 '2011239 02231 14 0410K14 /2011240 02231 15 0410K15 /^011242 02231 16 0410K:16 /2011244 02231 I'' 0410K17 02231SA10 02231 1* 0410K18 02231MS 02231 19 0410K19 02231MSi) 02231 250 250 10-Apr-OO •10-Apr-OO lO-.Apr-OO lO-Apr-OO 10-Apr-OO 10-Apr-OO lO-.-^pr-OO 10-.-\pr-00 li3-.\pr-00 10-Apr-OO 10-Apr-OO lO-.Apr-OO lO-Apr-OO lO-.Jipr-OO 10-Apr-OO 10-.-\pr-00 10-.-\pr-00 10-.\pr-00 lO-Apr-OO 9:33 10:02 10:36 11:05 11:35 12:04 12:34 13:03 13:33 14:02 14:32 15:01 15:31 16:00 16:30 16:59 17:29 17:58 18:23 t i < /f-:: 271.3 f7~ 2.c<> ^ _ - ? . / ; 0^--/.V -y--1% - y / y - - / ^ ^ ^^7 305199 i>roD.lPtM ». 2 VVtm »J»<* J^f^ce Analytical i\(iw Orleans Laboratory Report of Method Blank Organic Protocol - Single Batch Lab ID: 02231B1K05 Description: Water Method Blank Method: Water GC/MS Volatile Organics Project No.: 201382 Batch: 02231 P a c e A n a l y t i c a l Services, Inc. 10OO Rivertiend Blvd. Suite F Saint Rose. LA 70087 Phone: S04.469.0333 Fax: 504.469.0555 Units: ug/1 Prep Factor: j[ Leached: Prepared: Analyzed: 06-Apr-OO 15:13 ACA Reporting CAS Number 74^87^3' 67.^-1 74-83-9 67-66-3 100-41-4 75-01.4 75-09-2 -5-00-3 108-88-3 1330-20-7 75-15-0 75-35-4 75-34-3 540-59-0 107-O6-2 :'8-93-3 71-55-6 56-23-5 -5-27-4 7S-87-5 10061-01-5 79-01-6 12448-1 79-00-5 71-43-2 10061-02-6 -5-25-2 108-10-1 591-78-6 127-18-4 79-34-5 108-90-7 10042-4 J3 compoond(s) reported Parameter Dilution Chloromethane (Methyl chloride) 1 Acetone (2-Propanone. Dimethyl keto 1 Bromomethane (Methyl bromide) 1 Chlorofonn 1 Ethylbenzene 1 Vinyl chloride (Chloroethene) 1 Methylene chloride (Dichloromelhane 1 Chloroechane 1 Toluene 1 Xylene (total) 1 Carbon disulfide 1 1:1-Dichloroethene (Dichloroethylen 1 l.l-Dichloroelhane 1 1,2-Dichloroethene (total) I 1,2-Dichloroethane (Ethylene dichio 1 2-Butanone (Methyl ethyl ketone) 1.1,1-Trichloroethane (Methyl chlor Carbon tetrachloride Bromodichloromethanc 1.2-Dichloropropane cis-1.3-Dichloropropene Trichloroethene (Trichloroethylene) Dibromochloromcthane 1,1.2-Trichloroethane Benzene trans-1,3-Dichloropropene Bromofonm 4-Mcthyl-2-pentanone (VIIBK) 2-He.xanone Tetrachloroethene (Perchloroethylen 1.1.2 J-Tetrachloroelhane Chlorobenzene Stwene Result Qu ND ND ND ND ND ND ND J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Nb ND ND ND ND 1 ND I ND 1 ND I ND 1 ND 1 ND Limit 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 ND denotes .Not Delected i t or above Cbe reporting UmiL DF deaotes Daabon Factor. RJL denotes u m p l e Reporting LimJL Q« &sts qoallAen. Spetific quaU6<n t r e defined i t the end of tfac reporL 305200 4/1400 I4:10:3T JW^ce/Analytical New Orleans Laboratory Report of Method Blank Organic Protocol - Single Batch P a c e A n a l y t i c a l Services. Inc. 10OO Rivertiend Btvd, Suite F Saint Rose, LA 70087 Phone: 504.469.0333 Fax: S04.469.05SS Lab ED: 02231B1K08 Description: Water Method Blank Method: Water GC/MS Volatile Organics Prep Factor: 1 Leached: CAS Number Parameter Project No.: 201382 Batch: 02231 Prepared: Dilution Result Units: ug/1 Analyzed: 08-ADr-OO 12:29 Reporting Qu Limit ACA 67-64-1 Acetone (2-Propanone. Dimethyl keto 67-66-3 Chloroform 100414 Ethylbenzene 75-09-2 Methylene chloride (Dichloromethane 108-88-3 Toluene 1330-20-7 Xylene (total) 6 compound(s) r t p o n t d ND ND ND ND ND ND 10.0 10.0 10.0 10.0 10.0 10.0 305201 ND denotes Not Detected t l or above tbe reporting limit. DF denotes DOation Ftctor. RX, denotes sample Reporting LimlL 4'HOO 14:10:38 "j^Pace Analytical . .tew Orleans Laboratory Report of Method Blank Organic Protocol - Single Batch P a c e A n a l y t i c a l S e n / i c e s . Inc. 10O0 Riverbend Blvd. Suite F Saint Rose. LA 70087 Phone: 504 469.0333 Fax: 504.469.0555 Lab ID: 02231B1K10 Description: Water -Method Blank Method: Water GC/MS Volatile Organics Project No.: 201382 Batch: 02231 Units: ug/1 Prep Factor: I Leached: Prepared: Analyzed: 10-.\pr-00 11:05 ACA Reporting CAS .Number 74-87-3 67-M-l 74-83-9 67-66-3 75-01-4 100414 75-09-2 75.00-3 108-88-3 1330-20-7 ^ 75-15-0 P 75-35-4 75-34-3 540-59-0 107-06-2 78-93-3 71-55-6 56-23-5 •5-2:-* , 78-8--5 10061-01-5 79-01-6 12448-1 79-00-5 7143-2 10061-02-6 75-25-2 108-10-1 591-78-6 127-18-4 79-34-5 108-90-7 100-424 Parameter Dilution Chloromethane (Methyl chloride) Acetone (2-Propanone, Dimethyl keto Bromomethane (Methyl bromide) Chloroform Vinyl chloride (Chloroethene) Ethylbenzene Methylene chloride (Dichloromethane Chloroethane Toluene Xylene (total) 1 Carbon disulfide 1,1 -Dichloroethene (Dichloroethylen 1 1,1-Dichloro ethane I.2-Dichloroethcne (total) 1.2-Dichloroethane (Ethylene dichio 2-Butanone (Methyl ethyl ketone) 1,1,1 -Trichloroethane (Methyl chlor Carbon tetrachloride Bromodichloromeihane 1.2-Dichloropropane cis-l.3-Dichloropropene Trichloroethene (Trichloroethylene) Dibromochloromethane 1,1,2-Trichloroethane Benzene trans-1,3-Dichloropropene Bromoform 4-Methyl-2-pcntanone (MIBK.) 2-Hexanone Tetrachloroethene (Perchloroethylen 1,1.2.2-Tetrachloroethane Chlorobeiuene Styrene Result Qu ND ND ND ND ND ND ND J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Limit , 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 ' 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 33 conipound(s) reported ND denotes Not Detected at or above * e reporting llmlL DF deaotes D i n t i o n Factor. R L denotes tnmpic Reporting LimiL Q n Usts qn&Iiaen. Specific quaUfien t r e defined at the end of the report. 305202 4.14,00 14:10:38 ^^F^ceAnalyticaf Sample Data Summary Package SDG: 201708 Proiect(s): 201708, 201721, 201765 Presented to: Norma Eichlin McLaren Hart 25 Independence Boulevard Wairen, NJ 07059 Presented By: Pace Analytical Sennces, Inc. 1000 Riverbend Blvd. Suite F St. Rose, Louisiana 70087 Pace Analytical Services, Inc. 1000 Riverbend Blvd, Suite F SI. Rose LA 70087 Phone: 504.469.0333 Fax: 504.469.0555 May 30, 2000 305203 Pace Analytical Services, Inc. SDG:201708 McLaren Hart Narrative The McLaren Hart project consisted of thirty-four (34) water samples which were received by Pace Analytical Services, Inc. on May 2, 3 and 8, 2000 and logged in as Projects 201708.201721, and 201765. The samples were identified on the attached Sample Cross Reference report. The samples were analysed for volatile organics according to CLP methodology and sulfate according to Methods for Chemical Analysis of Water and Wastes Sample Management/Login Narrative Temperatures for the samples included in this report were 1.0. 16, and 24°C upon receipt. Client was notified about the elevated temperamre and the laboratory was instructed to go ahead and analyze the samples. No Qthef problems were encountered with the login process. ai2c '(7iA.i-<U^ Cindy Olavesen Date Project Manager Volatiles Manual integrations for volatile organics are occasionally necessar. due to co-elution, interferences and/or inadequacies of the software; these integrations are indicated by an "m" on the quantitation list and the inclusion of an extracted ion current profile indicating the integration of the target. Samples20l4006.2014007. 2014130. 201413L 2014457. 2014458. 2014459, 201446L 2014462. and 2014465 were diluted prior to analysis based upon screening information. Sample 2014462 required further dilution. Methylene chloride and acetone are common solvents; their presence in field samples may be an artifact of sample collection, transport, or analysis. No problems were encountered with these analyses. The pH measurement for each of these water samples was 1. Shelley ^ntoine Date Operation Manager Conventional Parameters No problems were encountered with the analyses. Lori Kelly J ^ ^ Date Water (^ualitx' Supervisor 305204 Quality Aasarance This data package has been reviewed for both completeness and technical specifications. The data were reviewed for overall QA/QC requirements of precision, accuracy, and consistency in data presentation. The data were evaluated for compliance against the CLP Method and Methods for Chemical Analysis of Water and Wastes. These guidelines were used in the preparation of our technical narratives. The release of this data package has therefore been authorized bv the Laboratory Manager through Quality Assurance review. Gary Newon QA Reviewer Date 305205 ^ ^ J ^ c t ^ace/knalytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s , Inc. 1000 Riverbend Blvd, Suite F Saint Rose. LA 70087 Phone: 504.469.0333 Fax: 5O4.469.0S55 ClientlD: MW-1 Proiect: VIRGIN ISLAND Lab ID: 2014006 Description: None Method: CLP Volatile Oreanics Prep Factor: 1 Leached: n/a CAS Number Par«meter 67-64-1 .Acetone (2-Propanone, Dimethyl keto 67-66-3 Chloroform 100-41-4 Ethylbenzene 75-0<)-2 Methylene chloride (Dichloromethane 10.S-S8-3 Toluene 1330-20-7 .Xylene (total) j^compoundO) reponed Dilution 50 50 50 50 50 50 Client: ERTEC Site: None Project No.: 201708 Matrix: Water Prep Level: Water Units: ug/1 Collected: 29-Apr-( Prepared: Result ND ND 1040 ND ND 8700 90 Qu D6 D6 D6 D6 D6 D6 Sample Qu: % Moisture: n/a Batch: 02732 TareetList: SR615MVWAT Received: 02-Mav-OO Analyzed: 04-Mav-OO 18:06 ACA Reporting Reg. Limit Limit 500. 500. 500. 500. 500. 500. 305206 ND denotes Not Detected at or above the adjusted reporting limit DF denotes DUution Factor of extract. T^e Prep Factor accounts for a non-routine sample size. Reportiog Limit Is corrected for sample size, dilation and moistnre content if applicable. Qa lists qnaliflcrv Specific qnaliflen arc defined at tbe end of the report For moistBre resatt*. w*< d#«n»« r*«iti» u »•«• *.»——»_,* *• '— -• - ' - -• 5/12/2000 10:52:38 ^ace Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s . Inc. 1000 Rivertiend Blvd. Suite F Saint Rose. LA 70097 Phone: 504.469.0333 Fax: S04.469.0SSS ClientlD: AST-VMP-ID Proiect: VIRGIN ISLAND Lab ID: 2014007 Description: None Method: CLP Volatile Oreanics Prep Factor: 1 Leached: o/a CAS Number Parameter 67-64-1 Acetone (2-Propanone. Dimethyl keto 67-66-3 Chloroform IOO-;i-> Ethylbenzene 75-09-2 Methylene chloride (Dichloromethane 108-88-3 Toluene 1330-20-7 Xylene (total) 6 compoundd) reported Dilution 100 100 100 100 100 100 Client: ERTEC Site: None Proiect xNo.:- 201708 Matrix: Water Prep Level: Water Units: ug/1 CoUected: 29-Apr-( Prepared: Result ND ND 6150 :s4. J ND 26300 OO Qu D6 D6 D6 All D6 06 Sample Qu: % Mobture: n/a Batch: 02732 TareetList: SR615MVWAT Received: 02-Mav-OO Analyzed: 09-Mav-OO 18:17 ACA Reporting Reg. Limit Limit 1000 ' 1000 1000 1000 1000 1000 305207 ND denotes Not Detected at or above ttie adjusted reporting l i m i t DF denotes DOotion Factor of extract Tbe Prep Factor accounts for a non-rootine sample size. Reporting L i m i t Is corrected for saaple size, dllotioo and moUtvre content if applicable. Qn Ihts qualiHers. Specific quatificrt arc defined at tbe end of the report For moisture results, wet denotes rtsolt b not corrected for moKtorc and n/a deootn nnt • n n i i r ^ w * 5/12/2000 10:52:39 W^^ct ^ace Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s . Inc. 10OO RIverbendBlvd. Suite F Saint Rose. LA 70087 Phone: 504.469.0333 Fax: S04.469.0SS5 CUentID: TB042900 Proiect: VIRGIN ISLAND Lab ID: 2014008 Description: None Method: CLP Volatile Oreanics Prep Factor: 1 Leached: n/a CAS Number Parameter 67-64-1 Acetone (2-Propanone. Dimethyl keto 67-66-3 Chloroform 100-11-4 Ethylbenzene 75-09-2 Methylene chloride (Dichloromethane 108-88-3 Toluene 1330-20-7 Xylene (total) ^ corapound<i} reponed CUent: ERTEC Site: None Project No.: 201708 Matrix: Water Prep Level: Water Units: ug/1 CoUected: 29-Apr-OO Prepared: Dilution Result Qu 1 ND 1 ND 1 ND 1 ND 1 ND Sample Qu: % Moisture: n/a Batch: 02732 Target List: SR615MVWAT Received: 02-Mav-OO .Analvzed: 04-Mav-OO 12:31 ACA Reporting Reg. Limit Limit 10.0 10.0 lO.O 100 10.0 10.0 305208 ,ND dcnaia Not Deucted u or >l>ovt iht tdjusted reporting limit DF denotet DQalioa Factor of extract. The Prep Factor aceoonci for a non-routine sample site. Reporting Limit U corrected for tampW lizc. dilution and moistnre content if applicable^ Qn listi quaUflcrs. Spwillc qaaimen art defined al tbe end or the report. 5/12/2000 10:52:3') Vtir tna,\<t%tr» r**til** ^ ^ J ^ c t ^ace/\nalytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s . Inc. 10OO RiverbetKi Btvd, Suite F Saint Rose. LA 70087 Phone: S04.469.0333 Fax: S04.469.0SS5 CUentID: FPP-VMP-4D Proiect: VIRGIN ISLAND Lab ID: 2014009 Description: None Method: CLP VolatUe Oreanics Prep Factor: 1 Leached: n/a CAS Number Parameter 67-64-1 Acetone (2-Propanone. Dimethyl keto 67-66-3 Chloroform 100-11-4 Ethylbenzene 75-09-2 Methylene chloride (Dichloromethane 108-88-3 Toluene 1330-20-7 .Xylene (toul) |4coropouod(s) reported CUent: ERTEC Site: None Proiect No.: 201708 Matru: Water Prep Level: Water Units: ug/I CoUected: 30-Apr-( Prepared: Dilution Result 1 ND 1 12.1 1 ND 1 ND 1 ND 1 ND )0 Qu Sample Qu: % Moisture: n/a Batch: 02732 TareetList: SR615MVWAT Received: 02-Mav-OO Analvzed: 04-Mav-OO 20:37 ACA Reporting Reg. Limit Limit 10.0 10.0 10.0 10.0 10.0 10.0 305209 ND denotes Not Detected at or above the adjusted reporting limit DF denotes DDotion Factor of estract The Prep Factor accounts for a noo-roatinc umple size: Reporting Limit a corrected for satnptc uztj dilation and moistnre content if appUcabic. Qu lists quaUflen. Specific qualfflers are defined at tbe end of the report For moitfnre r^tnll*. w»t *!•""»—'*•"*•'—-~* " — - - ' - ^ ' . . . 5/12/2000 10:52:40 ^[^J^ct I New Orlea Report of Laboratory Analysis ^ace/\nalytical New Orleans Laboratory CUentID: FPP-VMP-ID Project: VIRGIN ISLAND Lab ID: 2014010 Description: None Method: CLP Volatile Oreanics Prep Factor: 1, Leached: n/a Single Sample - Protocol P a c e Analytical Services, Inc. 1000 RIverbendBlvd. Suite F Saint Rose, LA 70O87 Phone: 504.469.0333 Fax: 504.469.0S55 CUent: ERTEC Site: None Project No.: 201708 Matrix: Water Prep Level: Water Units: ug/1 CoUected: 30-Apr-OO Prepared: Sample Qu: % Moisture: n/a Batch: 02732 Target List: SR615MVWAT Received: 02-MaY-00 Analyzed: 08-Mav-00 16:32 dgA CAS .Number 67-64-'l 67-66-3 100-41-4 75-09-2 105-SS-3 i:.;-o-2o-7 Parameter Dilution Acetone (2-Propanone. Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (total 1 Result ^ND" 81.6 ND ND ND ND Qu Reporting Limit " T o ^ 10.0 10.0 10.0 10.0 10.0 Reg. Limit - 6 cooipoand<i) reported 305210 \ D denotes Not Detected at or above t ^ adjusted reporting limit DF denotes DQatioa Factor of extract. The Prep Factor accounts for a non-routine sample size. Rqiorting Limit is corrected for sampk size, dilutioa and moistnrt coatent If applicable. Qn fiixs qoalifien. Specific qualifien are defined at tbe end of tbe report For aiotsture resulti, wet denotes resvit is not corrected for moisture and n/» denatM noi sonlirAhi^ 5/12/2000 10:52.41 ^ J ^ c t ^ace Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s , Inc. 100Q Riverbend Blvd. Suite F Saint Rose, LA 70087 Phone: 504.469.0333 Fax: SO4.469.0SS5 Client ID Project. Lab ID: Description: Method: Prep Factor: CAS Number 67-W-l 67-66-3 I0<j-ll-l 75-Jj9-2 lOS-iS-3 1330-20-7 FPP-VMP-2D VIRGIN ISLAND 2014011 None CLP Volatile Organics 1 Leached: n/a Parameter Dilutior Acetone (2-Propanone, Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (total) ^om(>ound(s) reported CUent: ERTEC Site: None Proiect No.: 201708 Sample Ou: Matrut: Water % Moisture: n/a Preo Level: Water Batch: 02732 Units: ue/1 TareetList: SR615MVWAT CoUected: 01-Mav-OO Received: 02-Mav-OO Prepared: Analyzed: 09-Mav-OO 20:21--^CA Reporting Reg. Result Qu Limit Limit ND 10.0 3.70 J 10.0 ND 10.0 2 50 J All 10.0 ND 10.0 1.20 J 10.0 305211 ND denotes Not Delected at or above tbe adjusted reporting l i m i t OF denotes DDntion Factor of extract. Tbe Prep Factor accounts for a non-roudine sample size. Reporting L i m i t ia corrected for sample size, dilution and moisture content i f applicable. Q u txsti qualifiers. Specific qnaUfiers are defined at the end of the report. For moisture results, wet denotes remit ii nat rAm^eit^ fnr mni<Hir* • « - ! «/- -*—-.»— —• - — " - * 512/2000 10:52:41 ^T^A^ce ^ ^ace/Knalytical { New Orleans Laboratory Report of Lal>oratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l Services, Inc. 10OO Rivertiend Btvd. Suite F Saint Rose. LA 70087 Phone: 504.469.0333 Fax: S04.469.0SS5 CUentID: FPP-VMP-4D Proiect: VIRGIN ISLAND Lab ID: 2014013 Description: None Method: CLP Volatile Organics Prep Factor: I Leached: n/a CAS Number Parameter 67-64-1 Acetone (2-Propanone, Dimethyl keto 67-66-3 Chloroform 100^1-4 Ethylbenzene 75-09-2 Methylene chloride (Dichloromethane 108-88-3 Toluene 1330-20-7 Xylene (total! 6 coinpound(4) rep«rt«l CUent: ERTEC Site: None - Project No.: 201708 Matrix: Water Prep Level: Water Units: ug/I CoUected: 01-Mav-OO Prepared: Dilution Result Qu 1 ND 1 20.2 1 ND 1 1.90 J All 1 ND 1 ND Sample Qu: % Moisture: n/a Batch: 02732 Target List: SR615MVWAT Received: 02-Mav-OO Analvzed: 08-Mav-OO 17:02 ACA Reporting Reg. Limit Limit 10.0 10.0 10,0 10.0 10.0 10.0 305212 \ D denotes Not Detected at or above tbe adjusted reporting l i m i t DF denotes DOnHon Factor of extract Tbe Prep Factor acconnts Tor a ooo-routine sample size; Reporting L i m i t is corrected for sample size, dilution and moistnre content if applicable. Qu lists qoaliflers. Specific qaaliners are defined at tbe end of the report For moistnrt results, wet denotes resoB is aot corrected for mobture and n/a denotes not applicable. 5/12/2000 \0;5:;A2 ^ g ^ ^ c t ^ace/Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s , Inc. 1000 Riverbend Blvd. Suite F Saint Rose, LA 70087 Phone: 504.469 0333 Fax: 504.469.0SS5 CUent ID Project Lab ID Description- Method: Prep Factor: CAS Number 67-64-1 67-66-3 lOO-tl-4 75-09-2 108-83-3 1330-20-7 FPP-VMP-ID VIRGIN ISLAND 2014014 None CLP VolatUe Organics 1 Leached: n/a Parameter Dilution Acetone (2-Propanone. Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene -Xylene (total) 6 conipouad(>) reported CUent: ERTEC Site: None Project No.: 201708 Matrix: Water PrepLievel: Water Units: ug/1 CoUected: Ol-Mav- Prepared: Result ND 137. ND 3.20 J ND ND 00 Qu All Sample Qu: % Moisture: n/a Batch: 02732 TareetList: SR615MVWAT Received: 02-Mav-OO Analvzed: 09-Mav-OO 17:45 ACA Reporting Reg. Limit Limit 10.0 10.0 10.0 10.0 10.0 10.0 305213 ND denotes Not Detected at or above the adjusted reporting l i m i t DF denotes DQoCion Factor of e i t r a c t The Prep Factor acconnti for a noo-routine sample size. Reporttzig L i m i t Is corrected for sample size, dilutioa and moisture content i f applicable. Qn lists qaallflcnL Specific qualifiers are defined at the end of tbe r e p o r t For moisture results, wet denotes resolt b not corrected for moisture and n/a denotes oot anoUcable. 5/12.-2000 10:52:42 / 'ace Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s , Inc. 10OO Rivertiend Blvd, Suite F Saint Rose, LA 70087 Phone: 504.469.0333 Fax: SO4.469.05S5 CUentID: FPP-VMP-3D Proiect: VIRGIN ISLAND Lab ED: 2014015 Description: None Method: CLP Volatile Organics Prep Factor: 1 Leached: n/a CAS Number Parameter 67-64-1 Acetone (2-Propanone. Dimethyl kelo 67-66-3 Chloroform i 00-41-4 Ethylbenzene 75-09-2 Methylene chloride (Dichloromethane IOS-88-3 Toluene 1330-20-7 Xylene (total) 6 compound<sl reported CUent: Site: Project No^ Matrix: Prep Level: Units: CoUected: Prepared: Dilution Resu ERTEC None 201708 Water Water ue/1 01-Mav-OO It ND 9.80 J ND 1.90 J ND ND Qu All Sample Qu: % Moisture: n/a Batch: 02732 Target List: SR615MVWAT Received: 02-Mav-OO Analvzed: 08-iMav-OO 18:32-^CA Reporting Reg. Limit Limit 10.0 10.0 10.0 10.0 10.0 10.0 305214 ND denotes Not Detected at or above the adjusted reporting timit DF denotes Dilution Factor of extract The Prep Factor accoonts for a non-rootine sample size. Reporting L i m i t Is corrected for sample size, dilution and vwstnrc content if applicable. Qu lists qualifiers. Specific qoaUfien arc defined at the end «f the report For moisture results, wet denotes result is not corrected for a o n t u r c and o/a denotes not apoUcablc. 5/12/2000 10:52:43 W^^^ce I New Orlea ^ce/Analytical New Orleans Laboratory ClientlD: FB050100 Project: VIRGIN ISLAND Lab ID: 2014129 Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s , Inc. 1000 Rivertiend Blvd. Suite F Saint Rose, LA 70087 Phone: 504.469.0333 Fax: 504.469.0555 Description Method Prep Factor CAS Number 67"-64-l 67-66-3 100-Jl-l "5-09-2 108-88-3 1330-20-7 None . CLP VolatUe Oreanics 1 Parameter Leached: n/a Acetone (2-Propanone, Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichic Toluene .Xylene (total) i compoundtit reported 5romethane Dilution CUent: Site: Project No.: Matrix: Prep Level: Units: CoUected: Prepared: ERTEC None 201721 Water Water \xsA 01-Mav-OO Result _..___ ND 1.90 J 2.00 J ND 7.70 J Qu All Sample Qu: % Moisture: n/a Batch: 02732 TareetList: SR615MVWAT Received: 03-Mav-OO Analvzed: 08-Mav-OO 20:03 ACA Reporting Reg. Limit Limit 10.0 10.0 10.0 10.0 10.0 10.0 305215 \ D denotes Not Detected at or atwvc tbe adjusted reportiog Omit DF denotes DQotioo Factor of extract The Prep Factor accounts for a aon-rootiac sample size. Reporting Limit is corrected for sunple size, dilutioa and moisture content if appUcable. Qo lists qualifiers. Specific qoaliflers are defined at the end of tbe report For moisture resalts, wet denotes rcsalt is not corrected Tor moisture and n/a denotes not applicable. 5/12/2000 10:51:3-1 ace Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s . Inc. 1000 Riverbend Btvd, Suite F Saint Rose, LA 70087 Phone: 504.469.0333 Fax: S04.469.0SS5 CUentID: AST-VMP-ID Proiect: VIRGIN ISLAND Lab ID: 2014130 Description: None Method: CLP VolatUe Oreanics Prep Factor: I Leached: CAS Number Parameter 67-64-1 Acetone (2-Propanone, Dimethyl keto 67-66-3 Chloroform 100-41-4 Ethylbenzene 75-09-2 Methylene chloride (Dichloromethane 108-88-3 Toluene 1330-20-7 Xylene (total) 6 canipound(s) reported n/a Dilution 100 100 100 100 100 100 Client: ERTEC Site: None Proiect No.: 201721 Matrix: Water Prep Level: Water Units: ug/1 CoUected: 01-Mav- Prepared: Result ND ND 4290 309 i ND 15300 00 .Qo D6 D6 D6 All D6 D6 Sample Qu: % Moisture: n/a Batch: 02732 TareetList: SR615MVWAT Received: 03-Mav-OO Analvzed: 09-Mav-OO 19:50 ACA Reporting Reg. Limit Limit lOOO lOOO 1000 1000 iOOO 1000 305216 VD denotes Not Detected at or above the adjusted reporting limit DF denotes DQution Factor of eitract T^e Prep Ftctor Kcoontt for t aoa-rontine sample fize. Reporting Limit is corrected for sample size, dilution and moisture cootent if applicsblcL Qu lists qualifiers. Spedflc qualifiers are defined at Che end of Che report For mobture results, wet denotes resatt is not corrected for moisture and n/a denotes oot applicable. 5/12^2000 10:51:35 ^ace Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample • Protocol P a c e A n a l y t i c a l S e r v i c e s . Inc. IOOO Rivertiend Blvd. Suite F Saint Rose, LA 70087 Phone: 504.469.0333 Fax: 504.469.05SS CUentID: AST-VMP-3D Proiect: VIRGIN ISLAND Lab ED: 2014131 Description: None Method: CLP VolatUe Oreanics Prep Factor: \ Leached: C A S Number Parameter 67-64-1 Acetone (2-Propanone, Dimethyl keto 67-66-3 Chlorofomi 100^1-4 Ethylbenzene 75-09-2 Methylene chloride (Dichloiomethane 108-88-3 Toluene 1330-20-7 Xylene (toul) k6 compounddt reported n/a Dilution 100 100 100 100 100 100 CUent: Site: Project No.: Matrii: Prep Level: Units: CoUected: Prepared: ERTEC None 201721 Water Water uen 01-Mav- Result .- ND ND 6750 242( 2IS. J ND M 00 Qu " D 6 " D6 D6 All D6 D6 Sample Qu: % Moisture: n/a Batch: 02732 TareetList: SR615MVWAT Received: 03-Mav-OO Analvzed: 08-Mav-OO 21:03 ACA Reporting Reg. Limit Limit iooo"^ IOOO 1000 IOOO [OOO 1000 305217 fro denota Not Detected %t or ilMve the adiusted rep«rtin{ limit. DF denotes Daatioo Factor of extract. The Prep Factor accounts for a noa-roatine sample size. Reporting Limit b corrected for saapk size, dilution and moisture content if applicable. Qn lists qnaliflers. Spedflc (jnaliflers are dellned at tbe end of the report. 5/12/2000 10:51 J 7 For RiAivrnr^ r^*ntt* iw*f rf*- Al«riir* • n d n/a H H ^^J^ct ^ace/Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s . Inc. i ooo Filvertiend Blvd. Suits F Saint Rase. LA 70087 Phone: S04.469.0333 Fax: SO4.469.0SSS CUentID: AST-VMP-4D Proiect: VIRGIN ISLAND Lab ID: 2014132 Description: None Method: CLP VolatUe Oreanics Prep Factor: 1 Leached: n/a CAS Number Parameter Dilution 67-64-1 Acetone (2-Propanonc, Dimethyl keto 67-66-3 ChloiDform 100-41-4 Ethylbenzene 75-09-2 Methylene chloride (Dichloromethane 108-88-3 Toluene 1330-20-7 Xylene (total) &cooipound(s) reported CUent: Site: Project No.: Matrix: Prep Level: Units: CoUected: Prepared; ERTEC None 201721 Water Water u ^ 01-Mav-OO Result Qu ND 2.10 J 35.5 2.70 ; All ND 307. Sample Qu: % Moisture: n/a Batch: 02732 TareetList: SR61SMVWAT Received: 03-Mav-OO Analvzed: 09-Mav-OO 19:18ACA Reporting Reg. Limit Limit 10.0 10.0 10,0 10.0 10.0 10.0 305218 ND denotes Not Detected at or above tbe adjusted reporting limit DF denotes DOndon Factor of eitract The Prep Factor accounts for a noo-rootiae sample size. Reporting Limit b corrected for (ample size; dilution and moisture content if applicable. Q Q SSCS qualifien. Specific qoatifien are dellned at the end of the report For moisture results, wet denotes resolt is not rorr»rt#rf fnr tnnWUxr^ and n/« HrnntM nnt annlir*! 5/i:i/2000I0:SI;-J0 ^ ^ J ^ c t ^ace/Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol F ^ c e A n a l y t i c a l S e r v i c e s . I n c . iOOO Rh/erberHj Blvd. Suite F Saint Roae. LA 70087 Phone: SO4.469.0333 Fax: S04.469.OSSS CUentID: TB050200 Proiect: VIRGIN ISLAND Lab ID: 2014133 Description: None Method: CLP VolatUe Organics Prep Factor: 1 Leached: n/a CAS Number Parameter Dilution 67-64-1 Acetone (2-Propanonc, Dimethyl keto 67-66-3 Chloroform 100-41-4 Ethylbenzene 75-09-2 Methylene chloride (Dichloiomethane 108-88-3 Toluene 1330-20-7 Xylene (total) 6 conipound<i) reported CUent: Site: Project No.: Matrix: Prep Level: Units: CoUected: Prepared: Resu ERTEC None 201721 Water Water ug/I 02rMav-00 It ND ND ND 1 80 J ND ND Qu All Sample Qu: % Moisture: n/a Batch: 02732 TareetList: SR615MVWAT Received: 03-Mav-OO Analvzed: 08-Mav-OO 20:33 ACA Reporting Reg. Limit Limit 10.0 10.0 10.0 100 10.0 10.0 305219 ND denotes Not Detected at or above the adjusted reporting l i m i t DF denotes DDntion Factor of extract The Prep Factor acconnts for a non-rontine sample size Reporting L i m i t is corrected for sample size, dUndon and moistare cootent i f applicable. Qn ttsa qnaUfiers. Spedflc qnatlftcrs are defined at the end of the report 5/12/2000 10:51:43 ^ l ^ ^ c t I New Orlea ^ace/Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l Services. Inc. IOOO Riverbend Blvd. Suite F Saint Rase, LA 70087 Phone: 504.469.0333 Fax: S04.469.0S55 CUentID: M W l Project: VIRGIN ISLAND Lab ID: 2014461 Description: None Method: CLP VolatUe Organics Prep Factor: I Leached: CAS .Number Parameter 67-64-1 .Acetone (2-PrDpanone. Dimethyl keto 67-66-3 Chlorofonn 100-41-4 Ethylbenzene 75-09-2 Methylene chlonde (Dichloromethane 108-8S-3 Toluene 1330-20-7 Xylene (total/ 6 compoondts) reported n/a Dilution 100 100 100 100 100 100 CUent: ERTEC Site: iNone Proiect No.: 201765 Matrix: Water Prep Level: Water Units: ug/1 CoUected: 03-Mav-OO Prepared: Result ND ND 7680 141 J 155 J 40100 Qu D6 D6 D6 All D6 D6 Sample Qu: % iMoisture: n/a Batch: 02851 Target List: SR615MVWAT Received: 08-Mav-OO Analyzed: 17-Mav-OO 14:37 KCB Reporting Reg. Limit Limit 1000 1000 1000 1000 1 ooo IOOO 305220 ND denotes Not Detected at or above the adjusted reportiog limit DF denotes DQation Factor of exd-act Tbe i*rep Factor accoonts for a non-routine sample size. Reportiog Limit it corrected for sample size, dUution and moisture content if applicable. Qn lisu qaaUflcrs. Spedflc qualifiers arc defined at the end of the report For moisture results, wet denotes resalt b not corrected for moiiture «n(i n/« rf»nnt»* n«t .nnCi—hi. S/2Z'2000 14:26:23 ^ J ^ C i ace Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Inorganic Parameters P a c e A n a l y t i c a l S e r v i c e s . Inc. IOOO Riverbend Blvd, Suite F Saint Rose. LA 70087 Phone: 504.469.0333 Fax: SQ4.469.0SS5 CUentID: MWl Project: VIRGIN ISLAND Lab ID: 2014461 Description: None CUent: ERTEC Site: None Project No.: 201765 Matrix: Water CoUected: 5/3/2000 %Moisture: n/a Received: 5/8/2000 ParameterName Method Batch DF Result Qu Reporting Units Limit Prep. Analysis Reg. Limit Sulfate EPA 375.2 I paramctcrtl) reported 02967 25.0 mg/1 10.0 19-May-OO 11.35 ELO 305221 ND denotes Not Detected i t or above the adjusted reporting l i m i t DF denotes DQution Factor of final sample PF denotes sample Prep Factor which accoonts for a uon-routtne sample size Reporting L i m i t u corrected for sampte size, dilution and moismre content if applicable. Qn tbts qnalifiers. Specific qualifiers are defined at the end of the report For moisture results, wet denotes resah is not corrected for moisture and n/a denotes not applicable. 5/22/2000 14:26:54 /^Z/^£ ^ace/Analytical New Orleans Laboratory Report of Laboratory Analysis Suigle Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s , tnc. IOOO Riverbend Blvd. Suite F Saint Rose, LA 70087 Phone: 504.469.0333 Fax: SO4.469.0S5S CUent ID: Project: Lab ID: Description: Method: Prep Factor: CAS .Number 67-64-1 67-66-3 100-41-4 75-09-2 I08-.SX-3 1350-20-7 ; MW6 VIRGIN ISLAND : 2014462 None CLP VolatUe Organics 1 Leached: n/a Parameter Acetone (2-Propanone, Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene .Xylene {total! k compound<i| reported CUent: ERTEC Site: None Project No.: 201765 Matrix: Water Prep Level: Water Units: ug/1 CoUected: 03-Mav- Prepared: Dilution Result 100 ND 100 ND 100 14500 100 150. J 100 131. J 200 63000 00 Qu D6 D6 D6 All D6 Dl Sample Qu: % Moisture: n/a Batch: 02851 Target List: SR615MVWAT Received: 08-Mav-OO Analvzed: 17-Mav-OO 15:38 KCB Reporting Reg. Limit Limit 1000 1000 1000 1000 IOOO 2000 ND denotes Not Detected at or above the adjusted reportiot Omit DF denotes DQution Factor of extract The Prep Factor accoonts for a non-routine sample sUe. Reporting Limit is corrected for sample size, dilution and moisture content if applicable. Qn lists qualifiers. Specific qoaliners are defined at the end of the report. 305222 S/22/;(XX) 14::6:25 ^ ^ ^ c e Report of Laboratory Analysis / z^^ce Analytical New Orleans Laboratory Single Sample - Inorganic Parameters P a c e A n a l y t i c a l S e r v i c e s . I n c . IOOO Rivertiend Blvd. Suite F Saint Rose, LA 70087 Phone: 504.469.0333 Fax- SO4.469.0SSS ClientlD: MW6 Proiect: VIRGIN ISLAND Lab ID: 2014462 Description: None ParameterName Method Batch Sulfate EPA 375.2 02967 1 puueter(s) reported DF 1 Result 66.3 Qu Client: ERTEC Site: None Proiect No.: 201765 Matrix: Water CoUected: 5/3/2000 Reporting Units Limit mg/1 10.0 Prep. %Moisture: n/a Received: 5/8/2000 Analysis 19-May-OO 11:35 ELO . Reg. Limit 305223 ND denotes Not Detected at or above tbe adjusted reportinf limit DF denotes DDntion Factor of final sample. PF denoto sample Prep Factor which accounts for a non-rootine sample size. Reporting Limit is corrected for sample size, dilution and moisture cootent if applicable. Qn fists qoaliners. Specific qoaliflers are defined at the end of the report. For mobture results, wet denotes result b not corrected for moisture aod n/a denotes not aoolicable. 5/22/2000 14:26:56 g2c. ^ace/Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s . I n c . IOOO Rivertiend Blvd. Suite F Saint Rose, LA 70037 Phone: 504.469.0333 Fax: 5O4.469.0SS5 # CUent ID. Project. Lab ID: Description: Method: Prep Factor: CAS Number 67-64-1 67-66-3 I0<j-4l-t -5-09-2 10^88-3 1330-20-7 MW8 VIRGIN ISLAND 2014463 None CLP VolatUe Organics 1 Leached: n/a Parameter Acetone (2-Propanone. Dimethvl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (lotaji ^compoundts) reported CUent: Site: Project No.: Matrix: Prep Level: Units: CoUected: Prepared: Dilution Resu ERTEC None 201765 Water Water ug/1 03-Mav-OO It Qu "ND ND ND 1.60 J All ND 1.30 J Sample Qu: % Moisture: n/a Batch: 02851 Target List: SR615MVWAT Received: 08-Mav-OO Analvzed: 17-Mav-OO 16:36 KCB Reporting Reg. Limit Limit 10.6 10.0 10.0 10.0 11.1.0 10.ij 305224 ND denotes Not Detected at or above the adjusted reporting limit DF denotes DQution Factor of extract The Prep Factor accooaD for a non-routine sample size. Repordng Limit Is corrected for sample size, dDutlon and moisture content if applicable. Qo Usts qualifiers. Specific qualifiers are defined al the end of the report For moisture results, wet denotes resatt a aot corrected for moistore and n/a denotes not applicable. 5/22/2000 14-.26:27 J2. Report of Laboratory Analysis /^J^ace/Analytical^ New Orleans Laboratory Single Sample - Inorganic Parameters P a c e Analytical Services, Inc. 1000 Rtverbertd Bh/d. Suite F Saint Rose. LA 70087 Phone: 504469.0333 Fax: SO4.469.0SS5 ClientlD: MW8 Proiect: VIRGIN ISLAND Lab ID: 2014463 Description: None 'arameterName Method Batch Sulfate EPA 375.2 02967. 1 paramcter(s) reported OF 1 Result 84.9 Qu CUent: ERTEC Site: None Proiect No.: 201765 Matrii: Water CoUected: 5/3/2000 Reporting Units Limit mg/1 10.0 %Moisture: n/a Received: 5/8/2000 Prep. Analysis 19-May-OO ll:35 ELO Reg. Limit 305225 ND denotes Not Detected al or above the adjusted reporting limit DF denotes DQution Factor of final sample. PF denotes sampte Prep Factor which acconnts for a non-routine sample size. Reporting Limit b corrected for sample size, dllutiott and moisture content if appUcablc Qn lists qaaliflerv Specific qoalifien are defined at the end of tbe report For moutnre results, wet denotes resatt U not corrected for moisture and n/a denotes not applicable. 5/22/2000 14:26:57 /5-^^£ ^ace/Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s , Inc. 1000 Rivertiend Blvd. Suite F Saint Rose, LA 70087 Phone: S04.469.0333 Fax: 504.469.0555 CUentID: MW7 Project: VIRGIN ISLAND Lab ID: 2014464 Description: None Method: CLP VolatUe Organics Prep Factor: I Leached: n/a C.AS Number Parameter 67-64-1 Acetone (2-Propanone, Dimethyl keto 67-66-3 Chloroform 100-41-4 Ethylbenzene 75-09-2 Methylene chloride (Dichloromethane I0^.'IS-3 Toluene 1330-20-7 Xylene (total) ^ compoundO) reponciJ Dilution CUent: Site: Project No.: Matrix: Prep Level: Units: CoUected: Prepared: ERTEC None 201765 Water Water ug/1 03-Mav-OO Result Qu ND 1.40 1 ND 1.50 J All ND 2.50 1 Sample Qu: % Moisture: n/a Batch: 02851 TareetList: SR615MVWAT Received: 08-Mav-OO Analvzed: 17-Mav-OO 17:05 KCB Reporting Reg. Limit Limit fo^o" '""" 10.0 10.0 lO.O 10.0 10.0 305226 ND denotes Not Detected at or above the adjusted reporting limit DF denotes DOntioa Factor of eitract The Prep Factor acconnts for a non-routine sample size. Reporting Limit b corrected for sample size, dilution and moistore content If applicable. Qu Osts qnaliflen. Spedflc qualificn are defined at the end of the report For mobtnre resalts, wet denotes rtsak b oot corrected for mobtnre and n/a denotes not applicable. 5/22/2000 14:26:23 ml4^ct ace Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Inorganic Parameters P a c e A n a l y t i c a l S e r v i c e s , I n c . IOOO Riverbend Blvd. Suite F Saint Rose, LA 70087 Phone: 504469.0333 Fax: 604.469.0555 CUentID: MW7 Project: VIRGIN ISLAND Lab ID: 2014464 Description: None CUent: ERTEC Site: None Project No.: 201765 Matrix: Water CoUected: 5/3/2000 ParameterName Method Sulfate EPA 375.2 I pamnetcrti) reported Batch 02967 DF Result Qu Reportiog Units Limit %Moisture: n/a Received: 5/8/2000 Prep. Analysis Reg. Limit 206. mg/1 50.0 19-May-OO 11:35 ELO 305227 ND denotes Not Detected at or above tht adjusted reporting limit DF denotes DQution Factor of final sample. PF denotes sample Prep Factor which accoonts for a non-rontine sample size. Reporting Limit b corrected for sample size; dUution and moistnre cootent if appUcablc Qu Usts quaUflen. Specific quaUflers are defined at tbe end of the report For moisture results, wet denotes resalt b not corrected for moutore and o/a denotes not applicable. 5/2Z'2O0O 14:26i5S ^ . ^ c e / 'T>f^ce/Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s , I n c . IOOO Rivertiend Blvd. Suite F Saint Rose, LA 70087 Phone: SO4.469.0333 Fax: 504.469.0555 Client ID: Project: Lab ID: Description: Method: Prep Factor: ASTVMP2D VIRGIN ISLAND 2014465 None CLP VolatUe Organics 1 Leached: n/a CUent: Site: Project No.: Matrix: Prep Level: Units: CoUected: Prepared: ERTEC None 201765 Water Water UR/1 03-Mav-OO Sample Qu: % Moisture: Batch: Target Lbt: Received: Analyzed: n/a 02851 SR61SMVWAT 08-Mav-OO 17-Mav-OO 18:32 KCB ^ ^ ^ ^ c CAS Number Parameter 67-64-1 Acetone (2-Propanone, Dimethyl keto 67-66-3 Chloroform 100-4 M Ethylbenzene 75-09-2 Methylene chlonde(Dichloromethane 108-38-3 Toluene 1330-20-7 Xylene {total/ conipaund(s) reported Dilution 4 4 4 4 4 4 Result 401. ND ND 1. 6.00 I ND 907. Qu " D6 D6 D6 All D6 D6 Reporting Limit 46.0" 40.0 40.0 40.0 40.0 40.0 Reg. Limit 305228 ND denotes Not Detected at or above the adjusted reporting limit DF denotes DOntion Factor of extract n « Prep Factor acconnts for a uon-rouUne sample sixe. Reporting Limit Is corrected for sampk size, dilution aod moisture cootent if appUcable Qn lists quaUfiers. Specific qnaUfiers are defined at the end of the report. For moisture results, wet denotes result b not corrected for moisture and n/a denotes not applicable. 5/22/2000 14:26:30 W^J^ct Report of Laboratory Analysis _ ^ . ^ace Analytical I New Orleans Laboratory Single Sample - Inorganic Parameters P a c e A n a l y t i c a l Services, I n c . IOOO R t v e r b e r t d B l v d . Suite F S a i n t R o s e , LA 7 0 0 8 7 P h o n e : 504.469.0333 F a x : 504.469.0555 CUentID: ASTVMT2D Project: VIRGIN ISLAND Lab ID: 2014465 Description: None Client: ERTEC Site: None Project No.: 201765 Matrii: Water CoUected: 5/3/2000 ParameterName Method Batch DF Result Qu Reporting Units Limit %Moisture: n/a Received: 5/8/2000 Prep. Analysis Reg. Limit Sulfate EPA 375.2 1 parunctefts) reported 02967 119. mg/1 20.0 19-May-OO 11:35 ELO 305229 ND denotes Not Detected at or above tbe sdjuited reporting l i m i t DF dcat»(es Dilution Factor of final sample. PF denotes sample Prep Factor which accooots for a noo-rootine t Reporting L i m i t is corrected for sample size, dUution and moisture content if applicable. Qn lists quaUflers. Specific quaUflers arc defined at the end of the report For moisture resulti, wcC denotes result s not corrected for mobture and o/a denotes not appUcable. npte size. 5/2Z'20O0 14:26:59 ^ ^ J ^ c e ^ace Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l Services. Inc. IOOO Riverbend Blvd. Suite F Saint Rose, LA 70087 Phone: SO4.469.0333 Fax: SO4.469.0SS5 m CUentID: FB050300 Proiect: VIRGIN ISLAND Lab ID: 2014466 Description: None Method: CLP VolatUe Organics Prep Factor: 1 Leached: n/a C.XS Number Parameter 67-64-1 Acetone (2-Propanone. Dimethyl keto 67-66-3 Chloroform 100-41-4 Ethylbenzene 75-09-2 Methylene ;hloride (Dichloromethane 108-8S-3 Toluene 1330-20-7 Xylene (toui;, A compoundtt) reported CUent: Site: Project No.: Matrix: Prep Level: Units: CoUected: Prepared: ERTEC None 201765 Water Water ug/1 03-Mav-OO Dilution Result Qu ND ~ " ND ND 1.60 i All ND 4.20 J Sample Qu: % Moisture: n/a Batch: 02851 Target List: SR615MVWAT Received: 08-Mav-OO Analvzed: 17-Mav-OO 17:34 KCB Reporting Reg. Limit Limit i0.b" ~ ' 10.0 10.0 10.0 10.0 10.0 305230 .ND denotes Not Detected at or above the adjasted reporting l i m i t DF denotes DOntion Factor of extract X\kt Prep Factor accounts for a aon-rontine sample size. Reporting L i m i t b corrected for sample six£, dilutioo and moistnre content if applicable. Q n Usts quaUflers Specific quaUfWn art defined at the end of the report For moisture results, wet denotes resak b not corrected for moisture and n/a denotes not applicable. 5/22/2000 14:26:32 wl^^ct ' t^f^vu Ortega ^ace Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e Analytical Services. Inc. 1000 Rivertiend Blvd. Suite F Saint Rose, LA 70087 Phone: 504.469.0333 Fax: SO4.469.0SS5 CUent ID: Project: Lab ID: Description: Method: Prep Factor: TB050400 VIRGIN ISLAND 2014467 None CLP VolatUe Organics 1 Leached: n/a CUent: Site: Project No.: Matrii: Prep Level: Units: CoUected: Prepared: ERTEC None 201765 Water Water ue/1 04-Mav-OO Sample Qu: % Moisture: Batch: Target List: Received: Analyzed: n/a 02851 SR615MVWAT 08-Mav-OO 15-Mav-OO 20:33 ACA CAS Number Parameter 67-64-1 Acetone (2-Propanone. Dimethyl keto 67-66-3 Chloroform 100-4M Ethylbenzene 75 -09-2 Methylene chloride (Dichloromethane IO.S-iS-3 Toluene 1330-20-7 Xylene (total) 6 compound(i) reported Dilution I I I Result ND ND ND 1.60 J ND ND Qu All Reporting Limit 10.0 10.0 10.0 lO.O 10.0 10.0 Reg. Limit 305231 ND deaotes Not Detected at or above the adjasted reporting Umit DF denotes DQution Factor of extract The Prep Factor accoonts for a non-routine sample size. Reporting limit b corrected for sample slic, dllodon and moisture content If appUcable. Qn lists qoallflcrt. Spedflc quaUflers are defined at the end of the report For moUtorc resalts, wet doiotes result b not corrected for moisture and n/a denotes not appUcable. 5/72/2000 14:26:33 /flM^( ace/Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s . Inc. IOOO Rtvertiertd Blvd. Suite F Saint Rose. LA 70087 Phone: S04.469.0333 Fax: SO4.469.0SS5 CUentID: FB050400 Proiect: VIRGIN ISLAND Lab ID: 2014468 Description: None Method: CLP VolatUe Oreanics Prep Factor: I Leached: n/a C.AS Number Parameter 67-64-1 Acetone (2-Propanone. Dimethyl keto 67-66-3 Chloroform |(X)-4l-4 Ethylbenzene 75-09-2 Methylene chloride (Dichlonomethane lO.S-?S-3 Toluene 1330-20-7 Xylene (total) 6 cQnip<iund(i) reported CUent: ERTEC Site: None Project No.: 201765 Matrix: Water Prep Level: Water Units: ug/I CoUected: 04-Mav-OO Prepared: Dilution Result Qu 1 ^ "'ND 1 ND 1 ND 1 120 J All 1 ND 1 4.70 J Sample Qu: % Moisture: n/a Batch: 02851 Target List: SR615MVWAT Received: 08-Mav-OO Analvzed: 15-Mav-OO 21:03 ACA Reporting Reg. Limit Limit 10.0 10.0 10.0 10.0 10.0 10.0 305232 ND denotes Not Detected at or above the adjusted reporting limit DF denotes DUudon Factor of extract The Prep Factor accounts for a non-routine sample size. Reporting Limit b corrected for sampk size, dUntlon and moisture content if applicable Qo Usts qualifien. Spedflc quaUflers are defined at the end of the report. For mobture results, wet denotes result b not corrected for moisture and n/a denotes not applicable. 5/22/2000 14:26:35 ^^^F^ct ^ace/Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol Pace Analytical Services. Inc. 1000 Rh/erbend Blvd. Suite F Saint Rose, LA 70087 Phone: 504.469.0333 Fax: SO4.469.0SS5 CUent ID: Project; Lab ID: Description: Method: Prep Factor: CAS Number 6'-64-l 67-66-3 1 i/j-i 1 - i ''5-39-2 !0v*i-3 1330-20-7 ; MW-2 ; VIRGIN ISLAND ; 2014469 ; None CLP VolatUe Organics 1 Leached: n/a Parameter Acetone (2-Propanone. Dimethyl keto Chloroform Ethylberuene Methylene chloride (Dichloromethane Toluene .Xylene (total) A coapoand(s) reported CUent: ERTEC Site: None Proiect No.: 201765 Matrix: Water Prep Level: Water Units: ug/1 CoUected: 04-Mav- Prepared: Dilution Result 1 ND 1 16.7 1 ND 1 1.70 I 1 ND 1 ND 00 Qu All Sample Qu: % Moisture: n/a Batch: 02851 TareetList: SR615MVWAT Received: 08-Mav-OO Analvzed: 15-Mav-OO 21:32 ACA Reporting Reg. Limit Limit io,o" 10.0 10,0 10.0 10 0 10.0 305233 NT) deaotes Not Detected at or above the adjasted repordog l i m i t DF denotes Dflntlon factor of extract The Prep Factor accoonts for a noo-roudne sample size. Reporttag L i m i t b corrected for sample size, dilution and moisture content i f applicable. Qu Sscs qnaUflcn. Specific qualifiers are defined at the end of the report For aabrnrff r»<alt«. w*< Amntmm r n i t ia n A t r ^ t r r ^ ^ t ^ t t t u t w,A w,l<m A^wtntm^ nni 5'22/2000 U;26:36 •>/^£ _ ^ . ^ace/Analytical I New Orleans Laboratory Report of Laboratory Analysis Single Sample - Inorganic Parameters P a c e A n a l y t i c a l Services, Inc. IOOO Rivertiend Blvd. Suite F Saint Rose, LA 70087 Phone: 504.469.0333 Fax: 504.469.0SS5 CUentID: MW-2 Project: VERGIMSLAND Lab ID: 2014469 Description: None ParameterName Method Batch Sulfate EPA 375:2 02967 1 paramctcrt^) reported DF 5 Result 149. Qu CUent: ERTEC Site: None Proiect No.: 201765 Matrix: Water CoUected: 5/4/2000 Reporting Units Limit mg/1 50.0 Prep. %Moisture: n/a Received: 5/8/2000 Analysis 19-May-OO II;3S ELO Reg. Limit 305234 ND denotes Not Delected at or above iW adjasted reporting Umit DF denotes DQatioa Factor of final sample. PF denotes sample Prep Factor which accounts for a non-rontiac sample size Reporting Umit b corrected for sampte sixe. dilution and moisture cootent if appUcable. Qu lists qualificn. Specific qaaUfWn are defined at the end of the report. For motstnre results, wet denotes resalt is not corrected for mobture and ti/a denotes uot applicable. 5'22>^000 14:27:00 ^^J^ct ^ace Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e Analytical Services, Inc. 1000 Riverbend Btvd. Suite F Saint Rose, LA 70087 Phone: 504.469.0333 Fax: 504.469.0555 CUentID: DUPLICATE Project: VIRGIN ISLAND Lab ID: 2014470 Description: None Method: CLP VolatUe Organics Prep Factor: 1 Leached: n/a CAS Number Parameter 67-64-1 Acetone (2-Propanone, Dimethyl keto 67-66-3 Chloroform 100-41^ Ethylbenzene 75-09-2 Methylene chloride (Dichloromethane lO.S-SS-3 Toluene 1330-20-7 Xylene (total) ( compoand(i) reported CUent: ERTEC Site: None Project No.: 201765 Matrix: Water Prep Level: Water Units: ug/1 Collected: 04-Mav-OO Prepared: Dilution Result Qu 1 ND 1 21.1 1 ND 1 2.00 J All 1 ND 1 l.iO J Sample Qu: % Moistnre: n/a Batch: 02851 TareetList: SR615MVWAT Received: 08-Mav-OO Analvzed: 15-Mav-OO 17:06 ACA Reporting Reg. Limit Limit 10.0 10.0 10.0 10.0 10.0 10.0 305235 ND denotes Not Detected al or above the adjusted reporting limit DF denotes DDntion Factor of estract The Prep Factor accounts for a non-routine sample size. Reporting Limit is corrected for sample size. dUution and moistare content if appUcablc. Qu fists quaUfien. Specifk qualifiers are defined at the end of the report For maitrure rMiilf<_ w K d r t i a t s r e a h is not corrM!lMl for m o b t u r e a n d n/a denotes QOt aDoUcablc. 5/22/2000 14:26:39 W^J^ce Report of Laboratory Analysis __ ^ace Analytical^ f New Orleans Laboratory Single Sample - Inorganic Parameters F ^ c e A n a l y t i c a l S e r v i c e s , Inc. IOOO Rivertiend Blvd. Suite F Saint Rose. LA 70087 Phone: 504.469.0333 Fax: 504.469.0555 CUentID: DUPLICATE Project: VIRGIN ISLAND Lab ID: 2014470 Description: None CUent: ERTEC Site: None Project No.: 201765 Matrix: Water CoUected: 5/4/2000 %Moisture: n/a Received: 5/8/2000 ParameterName Method Batch DF Result Qu Reporting Units Limit Prep. Analysis Reg. Limit Sulfate EPA 375.2 1 parameterfs) reported 02967 179. mg/1 50.0 19-May-OO 11:35 ELO 305236 ND denotes Not Detected at or above the adjasted reporting limit DF denota DUution Factor of final sample. PF denotes sample Prep Factor which acconnts for a non-routine sample size. Reporting Limit b corrected for sample size, dilutioa and moisture coatent if appUcable. Qa Usts quaUfien. Specific quaUfiers are defined at the end of the report For moistnre results, wet denotes resalt b not corrected for oiobture and n/a denotes oot applicable. 5/22/2000 14:27:01 9^J^ce ' NeuM Orle^a ^ace/Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l Services, I n c 1000 Rivertiend Blvd. Suite F Saint Rose, LA 70O87 Phone: 504.469.0333 Fax: 504.469.0555 CUentID: TB050400 Proiect: VIRGIN ISLAND Lab ID: 2014471 Description: None Method: CLP VolatUe Organics Prep Factor: 1 Leached: n/a CAS Number Parameter Dilution 67-64-1 Acetone (2-Propanone. Dimethyl keto 67-66-3 Chloroform IO0-4M Ethylbenzene 75-09-2 Methylene chloride (Dichloromethane IOS-88-3 Toluene 1330-20-7 Xylene (total) 6 compoundts) reported CUent: Site: Project No.: Matrix: Prep Level: Units: CoUected: Prepared: ERTEC None 201765 Water Water nWl 04-Mav-OO Result • "ND" " ND ND 1.90 J ND ND Qti All Sample Qu: % Moisture: n/a Batch: 02851 TareetList: SR615MVWAT Received: 08-May-OO Analvzed: 15-Mav-OO 16:36 ACA Reporting Reg. Limit Limit 10.0 10.0 10.0 10.0 10-0 10.0 305237 .ND denotes Not I>etectcd at or above the adjusted reporting Umit DF denotes Dflotion Factor of extract The Prep Factor accounts for a non-routine sample size. Reporting Umit b corrected for sample size, dUution and moisture content If appUcable. Qu Usts quaUfiers. Specifk quaUficn are defined at the end of the report For moisture resalts, wet denotes resah b oot corrected for moisture and n/a denotes not applicable. 5'22'20OO 14:26:41 W ^ ^ c t ^^ ^ace Analytical / New Orleans Laboratory Report of Method Blank Ot;ganic Protocol - Single Batch P a c e Analytical Services, Inc. 1000 Riverbend Blvd. Suite F Saint Rose, LA 70087 Phone: 504.469.0333 Fax: 504.469.0555 Lab ID: 02732B1K04 Description: Method: Prep Factor: Water Method Blank Water GC/MS VolatUe Organics 1^ Leached: CAS Number Parameter 74.87l3~ 67-64-1 67-66-3 74-83-9 75-01-4 100-41-4 75-00-3 75-09-2 108-88-3 1330-20-7 75-15-0 75-35-4 75-34-3 540-59-0 107-06-2 78-93-3 71-55-6 56-23-5 75-27-4 78-87-5 10061-01-5 79-01-6 124-48-1 79-00-5 71-43-2 10061-02-6 75-25-2 108-10-1 591-78-6 127-18-4 79-34-5 108-90-7 100-42-4 Chloromethane (Methyl chloride) Acetone (2-Propanone, Dimethyl keto Chloroform Bromomethane (Methyl bromide) Vinyl chloride (Chloroethene) Ethylbenzene Chloroethane Methylene chloride (Dichloromethane Toluene Xylene (total) Carbon disulfide 1,1 -Dichloroethene (Dichloroethylen 1,1-Dichloroethane 1,2-Dichloroethene (total) 1,2-Dichloroethane (Ethylene dichio 2-Butanone (Methyl ethyl ketone) l,l,l-Trichloroethane(Methyl chlor Cathon tetrachloride Bromodichloromeihane 1,2-Dichloropropane cis-l ,3-Dichloropropene Trichloroethene (Trichloroethylene) Dibromochloromethane 1,1,2-Trichloroethane Benzene trans-1,3-Dichloropropene Bromoform 4-Melhy!-2-pentanone (MIBK.) 2-Hex3none Tetrachloroethene (Perchloroethylen 1,1,2,2-Tetrachloroethane Chlorobenzene Styrene 33 compound(s) reported Project No.: 201708 Batch: 02732 Prepared: Units: ug/1 Analyzed: 04-Mav-OO 11:58 ACA Dilution Result ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Qu Reporting Limit 16.6' 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 lO.O 10.0 10.0 10.0 10.0 10.0 305238 M> denotes Not Detected at or above the reporting limit OF denotes Dilution Factor. RL denotes sample Reporting Limit Qu lists qualifiers. Specific qualifien are defined at the end of the report 5/l2-'20OO 10:52:54 ^'Z^oe _^. ^ace Analytical I New Orleans Laboratory Report of Method Blank Organic Protocol - Single Batch P a c e A n a l y t i c a l S e r v i c e s , Inc. IOOO RIverbendBlvd, Suite F Saint Rose, LA 70087 Phone: 504.469.0333 Fax: 504.469.0555 Lab ID: Description: Method: Prep Factor: CAS Numb 67"-"64-"|~ ' 74-87-3 74-83-9 67-66-3 100-41-4 75-01-4 75-09-2 75-00-3 108-88-3 1330-20-7 75-15-0 75-35-4 75-34-3 540-59-0 107-06-2 78-93-3 71-55-6 56-23-5 75-27-4 78-87-5 10061-01-5 79-01-6 124^8-1 79-00-5 7M3-2 10061-02-6 75-25-2 108-10-1 591-78-6 127-18-4 79-34-5 108-90-7 100-42-4 02732B1K08 Water Method Blank Water GC/MS VolatUe Organics I Leached: er Parameter Acetone (2-Propanone, Dimethyl keto Chloromethane (Methyl chloride) Bromomethane (Methyl bromide) Chlorofonm Ethylbenzene Vinyl chloride (Chloroethene) Methylene chloride (Dichloromethane Chloroethane Toluene Xylene (total) Carbon disulfide 1,1-Dichloroethene (Dichloroethylen 1,1 -Dichloroethane 1,2-Dichloroethene (total) 1,2-Dichioroethane (Ethylene dichio 2-Butanone (Methyl ethyl ketone) l,l,l-Trichloroethane(Methyl chlor Carbon tetrachloride Bromodichloromethanc 1,2-Dichloropropane cis-l,3-Dichloropropene Trichloroethene (Trichloroethylene) Dibromochloromethane 1,1,2-Trichloroethane Benzene trans-1,3-Dichloropropene Bromoform 4-Methyl-2-pentanone(MIBK) 2-Hexanone Tetrachloroethene (Perchloroethylen 1,1,2,2-Tetrachloroethane Chlorobenzene Styrene Proiect No.: 201708 Batch: 02732 Prepared: Dilution Result Q 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND J 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND Units: ug/I Analvzed: 08-Mav-OO 14:58 Reporting u Limit 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 lO.O 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 ACA 33 compound(s) reported 305239 NT) denotes .Not Detected st or above the reporting Umit DF denotes Dilution Factor. RL denotes sample Reporting L i m i t Qu Usts qualifiers. Speciflc qualifiers are defined at the end of the report 5/12/2000 10:52:55 ^[^J^ct _/. ^ace Analytical ! New Orleans Laboratory Report of Method Blank Organic Protocol - Single Batch P a c e A n a l y t i c a l S e r v i c e s , Inc. 1000 Riverbend Blvd. Suite F Saint Rose, LA 70087 Phone: 504.469.0333 Fax: 504.469.0555 Lab ID: 02732B1K10 Description: Water Method Blank Method: Water GC/MS VolatUe Organics Prep Factor: 1 Leached: CAS Number Parameter 67-64-1 Acetone (2-Propanone, Dimethyl keto 67-66-3 Chloroform 100-41-4 Ethylbenzene 75-09-2 Methylene chloride (Dichloromethane 108-88-3 Toluene 1330-20-7 Xylene (total) 6 cocnpaund(s) reported Project No.: 201708 Batch: 02732 Prepared: Dilution Result Qu " " ' T " ~ ND 1 ND 1 ND 1 ND i 1 ND 1 ND Units: ug/1 Analvzed: 09-Mav-OO 16:12 Reporting Limit 10.0 10.0 10.0 10.0 10.0 10.0 ACA 305240 VD denotes Not Detected at or above the reporting Umit DF denotes Dilution Factor. RL denotes sample Reporting L i m i t Qo lists qualifiers. Specific qualifiers are defined at the end of the report 5 12 2000 10:52:56 /_^, ^ace Analytical f New Orleans Laboratory Report of Method Blank Organic Protocol - Single Batch Lab ID: 02851BK15 Description: Water Method Blank Method: Water GC/MS VolatUe Organics Project No.: 201765 Batch: 02851 P a c e Analytical Services, Inc. 1000 Riverbend Btvd, Suite F Saint Rose, LA 70087 Pfione: 504.469.0333 Fax: SO4.469.0S55 Units: ug/1 Prep Factor: 1 Leached: Prepared: Analyzed: 15-Mav-OO 16:06 ACA CAS Number 67~64-~i 67-66-3 100-41-4 75-09-2 108-88-3 1330-20-7 Parameter Dilution Result Qu Reporting Limit Acetone (2-Propanone, Dimethyl keto Chloroform Ethylbeiuene Meth> lene chloride (Dichloromethane Toluene Xylece (total) 6 compound(s) reported ND ND ND ND ND ND 10.0 10.0 10.0 10.0 10.0 10.0 305241 ND denotes Not Detected at or abo> e die reporting limit DF denotes Dilution Factor. RL denotes sample Reporting Limit Qu lisis qualifiers. Specific qualifiers are defined at the end of the report 5:2:000 14:27:15 ^if^^Ci ace Analytical I New Orleans Laboratory Report of Method Blank Organic Protocol - Single Batch Pace AnalyticarServices, Inc 1000 Riverbend Blvd. Suite F Saint Rose, LA 70087 Phone: 504.469.0333 Fax: S04.469.0SS5 Lab ID: Description: Method: Prep Factor: 02851B1L17 Water Method Blank Water GC/MS VolatUe Organics J, Leached: CAS Number Parameter 67-64-1 74-87-3 67-66-3 74-83-9 100-41-4 75-01-1 75-00-3 75-09-2 108-88-3 1330-20-7 75-15-0 75-35-» 75-34-3 540-59-0 107-06-2 78-93-3 71-55-6 56-23-5 75-27-4 78-87-5 I006I-01-S 79-01-6 124-48-1 79-00-5 71-43-2 10061-02-6 75-25-2 108-10-1 591-78-6 127-18-4 79-34-5 108-90-7 100^2-4 Acetone (2-Propanone, Dimethyl keto Chloromethane (Methyl chloride) Chloroform Bromomethane (Methyl bromide) Ethylbenzene Vinyl chloride (Chloroethene) Chloroethane Methylene chloride (Dichloromethane Toluene Xylene (toul) Carbon disulfide 1,1-Dichloroethene (Dichloroethylen I.I-Dichloroethane 1.2-Dichloroethene (total) 1,2-Dichloroethane (Ethylene dichio 2-Buianone (Methyl ethyl ketone) 1,1,1-Trichloroethane (Methyl chlor Carbon tetrachloride Bromodichloromethane 1,2-Dichloropropane cis-1,3-Dichloropropene Trichloroethene (Trichloroethylene) Dibromochloromethane 1,1,2-Trichloroethane Benzene trans-1.3-Dichloropropene Bromoform 4-MethyI-2-pentanone (MIBK) 2-Hexanone Tetrachloroethene (Perchloroethylen 1,1,2,2-Tetrachloroethane Chlorobenzene Styrene 33 CQmpaa[id<s) reported Project No.: 201765 Batch: 02851 Prepared: Dilution Result 1 .ND 1 ND 1 ND 1 ND 1 ND 1 ND I ND 1 ND 1 ND 1 ND 1 ND I ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 ND Units: ug/I Analvzed: 17-Mav-OO 09:31 Reporting Qu Limit 10.0 . 10.0 10.0 10.0 10.0 10.0 10.0 J 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 lO.Q 10.0 10.0 10.0 10.0 KCB 305242 ND denotes Not Detected at or above iht reportiiig limit DF denotes Dilution Factor. RL denotes sample Reporting Limit Qu lists qualifleri. Specific qoalifien are defined at tbe end of the report. 5/2Z'2000 14:27:14 / ^ace Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s , Inc. 100O Rivertiend Blvd. Suite F Saint Rose. LA 70087 Phone: 504.469.0333 Fax: S04.469.0SSS ClientlD: WCASTWB Proiect: VIRGIN ISLAND Lab ID: 2014458 Description: None Method: CLP VolatUe Organics Prep Factor: 1 Leached: n/a CAS Number Parameter 67-64-1 Acetone (2-Propanone, Dimethyl keto 67-66-3 Chlorofonn lOO^M Ethylbenzene 75-09-2 Methylene chloride (Dichloromethane 108-88-3 Toluene 1330-20-7 Xylene (total) 6 conipound(s) reponed Dilution 20 20 20 20 20 20 CUent: ERTEC Site: None Project No.: 201765 Matrii: Water Prep Level: Water Units: ug/1 CoUected: 03-Mav- Prepared: Result ND ND 68.4 J 27.4 J ND 3140 00 Qu D6 D6 D6 All D6 D6 Sample Qu: % Moisture: n/a Batch: 02851 Target List: SR615MVWAT Received: 08-Mav-OO Analvzed: 17-Mav-OO 11:59 KCB Reporting Reg. Limit Limit 200. 200. 200. 200. 200. 200. 305243 SD denotes Not Detected at or above the adjusted reportiog limit DF denotes DflutJon Factor of extract The Prep Factor accounts for a non-routine sample sizeu Reporting Limit b corrected for umple size, dllodon and moisture coatent if applicable. Qa lists qualifiers. Specific qualificn are deflned al the end of the report. For moisture results, wet denotes result is not corrected for mobture and n/t denotes not applicable. 5/22/2000 14:26:14 gz ^ace/Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s , I n c . IOOO Rh/erbend Blvd. Suite F Saint Rose, LA 70087 Phone: 504.469.0333 Fax: 5O4.469.0SS5 CUentID: WCASTWC Project: VIRGIN ISLAND Lab ID: 2014459 Description: None Method: CLP VolatUe Organics Prep Factor: 1 Leached: n/a C.AS .Number Parameter 6"-64-l .Acetone (2-Propanone. Dimethyl keto 67-66-3 Chloroform 100-11-4 Ethylbenzene 75-09-2 Methylene chloride (Dichloromethane I')'i-S8-3 Toluene 1330-20-7 .Xylene (total.) 4a)mpound()) rvponcd Dilution 200 200 200 200 200 200 CUent: ERTEC Site: None Proiect No.: 201765 Matrix: Water Prep Level: Water Units: ug/1 CoUected: 03-Mav-OO Prepared: Result ND ND 19300 234. J 4|i). J 96600 Qu D6 D6 D6 .All D^ D6 Sample Qu: % Moisture: n/a Batch: 02851 Target List: SR615MVWAT Received: 08-Mav-OO Analyzed: 17-Mav-OO 12:31 KCB Reporting Reg. Limit Limit 2000 2000 2000 2000 2l)(")(! 2000 305244 .ND denotes Not Detected at or above tbe adjusted reporting limit. DF denotes Dfludoo Factor of estract. Tbe Prep Factor accounts for a noo-routlne sample size. Reportiog Limit b corrected for sample size, dilution aod moisture content if applicable. Qu Usts quaUflers. Specific qualiflers are deflned at the end of the report 5/21'2000 14:26:18 Report of Laboratory Analysis P a c e A n a l y t i c a l Services, Inc. IOOO Rtverbertd Btvd, Suite F Saint Rose. LA 70087 Veiv O r l e a n s Laboratory Suigle Sample - Protocol CUent: CUentID: WCASTWD Site: Proiect: VIRGIN ISLAND Project No.: Lab ID: 2014460 Matrix: Description: None Prep Level: Method: CLP VolatUe Organics Units: Collected: Prep Factor: 1 Leached: n/a Prepared: CAS Number Parameter Dilution Resu 67-64-1 Acetone {2-Propanone, Dimethyl keto 1 67-66-3 Chloroform 1 100-11-4 Ethylbenzene 1 75-09-2 Methylene chlondel Dichloromethane 1 108-88-3 Toluene ! 1330-20-7 Xylene (toul) 1 .6 cofnpound(s) rrporttd ERTEC None 201765 Water Water ug/1 03-MaY-OO It Qu ND ND ND 1.40 J All ND 3.80 J P h o n e : S04.469.0't3-i Fax- S04.469. OSSS Sample Qu: % Moisture: n/a Batch: 02851 TareetList: SR615MVWAT Received: 08-Mav-OO Analvzed: 17-Mav-OO 18:03 KCB Reporting Reg. Limit Limit 10.0 10.0 10.0 10.0 10-0 10.0 305245 ND denotes Not Detected at or above tbe adjusted reporting UmiL DF denotes Dilution Factor of eitract The I*rep Factor accounts for a noo-routioe sample size. Reporting Limit b corrected for sample size, dilutioo and moisture content if applicable. Qu Usts qaaliners. Spedflc qoalifiers are deflned at the end of the report. 5 22.2000 14:26:20 ^ l ^ c t /_^^ace/Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol Pace Analytical Services, Inc. 1000 Rivertiend Btvd, Suite F Saint Rose, LA 70087 Phone: 504.469.0333 Fax: SO4.469.0SS5 CUentID: WCFPPWA Proiect: VIRGIN ISLAND Lab ID: 2014473 Description: None iMethod: CLP VolatUe Oreanics Prep Factor: 1 Leached: n/a C.AS Number Parameter Dilution 67-64-1 Acetone (2-Propanone, Dimethyl keto 67-66-3 Chloroform 100-11-4 Ethylbenzene 75-139-2 Methylene chloride (Dichloromethane lOS-SS-3 Toluene 1330-20-7 Xylene (toul.i |ct>iiipound(i) reporwd CUent: Site: Project No.: Matrix: Prep Level: Units: CoUected: Prepared: Resu ERTEC None 201765 Water Water ugn 04-Mav- It ND 3.80 J ND 2.30 J ND ND 00 Qu All Sample Qu: % Moisture: n/a Batch: 02851 TareetList: SR615MVWAT Received: 08-Mav-OO Analvzed: 15-Mav-OO 17:35 ACA Reporting Reg. Limit Limit 10.0 10.0 10.0 10.0 10.0 10.0 305246 ND denotes Not Detected at or at>ove tb< adjusted repordog limit. DF denotes DQotioo Factor of extracL Tbe Prep Factor accounts for a non-roodne sample size. Reportiag Limit b corrected for sampte size, dilution and moisture content If applicable. Qn &sts qualiflers. Speclflc qoaliflers tre deflned at the end of tbe report 5/22/2000 14:26:42 ^[^J^ce ^ace/Analytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s , Inc. 1000 Rivertiend Blvd. Suite F Saint Rose, LA 70087 Phone: 504.469.0333 Fax: 504.469.0555 Client ID Project. Lab ED: Description: Method: Prep Factor: CAS Number 67-64-1 67-66-3 lOO-tl-4 75-09-2 108-88-3 1330-20-7 WCFPPWB 8 VIRGIN ISLAND 2014474 None CLP VolatUe Organics 1 Leached: n/a Parameter Dilution Acetone (2-Propanone, Dimethyl keto Chloroform Ethylbenzene Methylene chloride (Dichloromethane Toluene Xylene (total) 6 compound(t) reported CUent: Site: Project No.: Matrix: Prep Level: Units: CoUected: Prepared: ERTEC None 201765 Water Water ue/1 04-Mav-OO Result Qu ND ND ND 2.10 1 All ND ND SampleQu: % Moisture: n/a Batch: 02851 TareetList: SR615MVWAT Received: 08-Mav-OO Analyzed: 15-Mav-OO 18:05 ACA Reporting Reg. Limit Limit 10.0 10.0 10.0 10.0 10.0 10.0 305247 ND denotes Not Detected at or above tbe adjusted reporting limiL DF denotes DDntion Factor of eitract Tbe Prep Factor accimots for a oon-rootiae sample size. Reporting Limit b corrected for sample size, dllodon and moisture content if applicable. Qa Ibts qualiflers. Spedflc qualifiers are deflned at tbe end of the report For moistore results, wet denotes resalt b not corrected for moisture and n/a denotes not applicable. 5'22/200O 14:26:4? ^ ^ ^ c t ^ace Anaiytical New Orleans Laboratory Report of Laboratory Analysis Single Sample - Protocol P a c e A n a l y t i c a l S e r v i c e s , Inc. IOOO Rtverbertd Btvd, Suite F Saint Rose, LA 70087 Phone: S04.469.0333 Fax: 504.469.0555 CUentID: WCFPPWC Project: VIRGIN ISLAND Lab ID: 2014475 Description: None Method: CLP VolatUe Oreanics Prep Factor: 1 Leached: n/a CAS Number Parameter Dilution 67-64-1 Acetone (2-Piopanone. Dimethyl keto 67-66-3 Chloroform I00-4M Ethylbenzene 75-09-2 .Methylene chloride (Dichloromethane 108-88-3 Toluene 1330-20-7 Xylene (toul) 6 compound{s) reported CUent: ERTEC Site: None Proiect No.: 201765 Matrix: Water Prep Level: Water Units: ug/I CoUected: 04-Mav- Prepared: Result ND 17.6 ND 1.80 1 ND ND 00 Qu All Sample Qu: % Moisture: n/a Batch: 02851 TareetList: SR615MVW.AT Received: 08-Mav-OO Analvzed: 15-Mav-OO 18:35 ACA Reporting Reg. Limit Limit 10.0 10.0 10.0 10.0 10.0 10.0 305248 ND denotes Not Detected at or abo^e the adjusted reportiag lifflit OF denotes Dflntion Factor of extract Tbe Prep Factor accoonts for a non-routine sample me. Reporting limit b corrected for sampte size, dUndoo and aoisture content if applicable. Qn Ibts qualiflers. Spedflc qnalifkrs are defined at tbe csid of the report 5/22/2000 U:;6:45 ^ This page was intentionally left blank for pagination purposes. 305249