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LETTER REPORT DATA COMPARISON AND EVALUATION REPORT TUTU WELLFEELD SITE ST, THOMAS, U.S. VIRGIN ISLANDS Prepared for U.S. ENVIRONMENTAL PROTECTION AGENCY Office of Waste Programs Enforcement Washington, D.C. 20460 EPA Work Assignment No. EPA Region Site No. Contract No. CDM Federal Programs Corporation Document No. Prepared by Work Assignment Project Manager Telephone Number EPA Work Assignment Manager Telephone Number Data Prepared C02048 n 2P1D 68-W9-0002 TES5-C02048-LR-CXLH CDM Federal Sally Odland (212) 393-9634 Caroline Kwan (212) 264-0151 June 8, 1993 *64463* 64463 C O M F E D E R A L P R O G R A M S C O R P O R A T I O N a s u b s i d i a r y o f C a m p D r e s s e r & M c K e e I n c . June 8, 1993 Ms. Caroline Kwan U.S. Environmental Protection Agency 26 Federal Plaza New York, NY 10278 PROJECT: TES V, EPA Contract No. 68-W9-0002 Work Assignment: CO2048 Tutu Wellfield Site St. Thomas, U.S. Virgin Islands DOCUMENT NO. TES5-CO2048-LR-CXLH SUBJECT: Data Comparison and Evaluation Report Dear Ms. Kwan: Per your request CDM FEDERAL PROGRAMS CORPORATION (CDM Federal) has prepared this data comparison report for the Tutu Wellfield site in St. Thomas, U.S. Virgin Islands. As we discussed, one package of data is still outstanding. We will update this report upon receipt of the data. 1.0 INTRODUCTION CDM Federal received Work Assignment No. C02048 under TES V Contract No. 69-W9- 0002 to provide enforcement support for EPA Region JJ during the Remedial Investigation/Feasibility Study (RI/FS) at the Tutu Wellfield Site in St. Thomas, U.S. Virgin Islands. The purpose of this RI/FS is to delineate the potential sources, the horizontal and vertical extent, and potential migration pathways of petroleum hydrocarbon products and other organic and inorganic contamination in soil and groundwater at the Tutu Wellfield site. This report presents a comparison of the analytical data results presented by CDM Federal and the PRP contractor, Geraghty and Miller (G&M) from split sampling events which occurred from July 1992 to October 1992. Ill Fukon Saeet, Suite 710 New York, NY 10038 212 39J-96M hinted on Headed COM FEDERAL PROGRAMS CORPORATION a subsidiary ol Camp Dresser & McKee inc 2.0 SUMMARY OF SAMPLING ACTTVTnES In order to investigate the sources and delineate the contamination, subsurface borings were drilled and sampled, shallow and deep monitoring wells were installed and sampled, and surface samples were collected. To corroborate G&M's analytical results, CDM Federal split seven subsurface soil samples from borings and monitoring wells, seven surface soil samples, and four groundwater samples. Table 1 is a summary of those split samples taken on JuW22,_24* and 30, 1992.,Jk»festtrface soil samples were split with G&M, from well borings fbTMW-8^)MW-6D, from soil borings B-6 and B-l. On August 11, CDM Federal-personnel collected split subsurface soil samples from borings at locations MW-5 in the Tillet Garden Art Center area, and B-l 2 in the O'Henry Dry Cleaner area (Table 2). On August 19, CDM Federal personnel split 100% of the surface soil samples taken by G&M at the Tutu site (Table 3). Between September 29 and October 1 , CDM Federal split 5 aqueous samples (4 groundwater and 1 field blank) with G&M (Table 4). CDM Federal's samples were analyzed via Routine Analytical Services (RAS) for Target Compounds List (TCL) volatile organic compounds (VOC), TCL semivolatile organic compounds (SVOCs); and Target Analyte List (TAL) metals and cyanide. Subsurface soil and groundwater samples were also analyzed via Special Analytical Services (SAS) for methyl-tertiary-butyl-ether (MTBE), 1,2-dibromoethane, n-propylbenzene and total petroleum hydrocarbons (TPH). 3.0 DATA COMPARISON In general, the data presented in Tables 5,6, and 7 indicate that the analytical results of the CDM Federal split samples and the G&M samples are comparable. Two types of discrepancies were observed. These were cases where: 1) A G&M sample concentration was reported as not detected while the split sample concentration was above the contract required limit. 2) Both sample and split concentrations were detected but their concentrations differed by more than an order of magnitude. COM FEDERAL PROGRAMS CORPORATION a subsidiary of Camp Dresser & McKee inc In general these discrepancies constituted a small percentage of the total split samples compared. The following sections discuss the data, by contaminant group, where CDM Federal's and G&M's data differed. Volatile Oranic Comound (VOCs) Data In sample E-64-^ ft), acetone and 2-butanone were detected at 370 ug/kg and 59 ug/kg respectively by G&M but were undetected by CDM Federal. In sample SS-3, xylene was detected at 19 ug/kg by G&M but undetected by CDM Federal (Table 5). Semi-Volatile Organic Compounds (SVOCs) The discrepancies found were associated with common laboratory contaminants (Table 6). Total Petroleum Hydrocarbons fTPHs) \ ^ £AK'^c' !v Lf\ O^ j In sample B-l (4-8 ft) CDM Federal's data revealed a TPH concentration of 60.2 ug/kg while G&M's was undetected. (Table 5). Inorganics Split sample data revealed two inorganics, cadmium and mercury at concentrations of 2.0 ug/kg and 0.25 mg/kg in SS-6. Vanadium was detected in SS-1 and SS-4 at 151 ug/kg and 107 ug/kg respectively. All five of these concentrations were detected above the contract required detection limit in CDM Federal's samples but were undetected in G&M's samples. Cyanide was detected above the contract required limit in three of G&M's samples at concentrations of 1.1 ug/kg, 1.2, ug/kg, and 0.96 ug/kg and mercury was detected at 0.19 ug/kg in one of G&M's samples but were undetected in CDM Federal's samples (Table 7). There were numerous discrepancies between sample and split sample data for field blank sample SS-7 . Many of G&M's inorganic concentrations were at least two orders of magnitude higher than CDM Federal's. In summary, the analytical results from split samples generally compare well with results obtained by the PRP laboratory. Except for the data from a surface soil field blank, the analytical discrepancies noted were minor. The Geraghty and Miller analytical results appear therefore to be reliable. Attachment 1 presents the data validation qualifers used in Tables 5,6, and 7. COM FEDERAL PROGRAMS CORPORATION a subsidiary ot Camp Dresser & McKee Inc If you have any questions regarding this report, please do not hesitate to call me at (212) 393-9634. Sincerely, CDM Federal Programs Corporation Ai.0 I Sally Odtand Work Assignment Manager TABLE 1 TUTU WELLFIELD SITE SUMMARY OF SPLIT SAMPLE INFORMATION July 22, 24 and 30, 1992 Shipments Subtle Location TU-MW-S TU-MW-6D MW-9 FB072992 B6 Bl Simpk Matrix Soil Soil Soil Aqueoui SoU Soil Volatile* BHR65 BHR64 BHR63 BHR69 BHR67 BHR66 BNA- Bitractablei BHR65 BHR64 BHR63 BHR69 BHR67 BHR66 Metah MBBS5S MBBS57 MBBS56 105429 105426 105427 Cyanide MBE55S MBB557 MBE556 105429 105426 105427 MTBB n-propy (benzene 1 ,2-dibromoethane 7382B-01-OI 73828-01-02 73S2B-01-03 7382B-01-04 7382B-01-06 732B-01-07 TPH 73S2B-02-01 7382B-02-02 7382B-02-03 73S2B-02-04 7382B-02-06 7382B-02-07 Date/Time of Sunpk Collection 7/20/92 9 1015 7/21/92 9 1500 7/24/92 ft 1030 7/29/92 9 0830 7/30/9290925 7/30/92 9 1300 Sample Rcmtiti 2-4' interval 0-2' interval 0-4' interval — 4-8' interval 4-8' interval QC Remarki — MS/MSD — Field Blank — — TABLE 2 TUTU WELLFIELD SITE SUMMARY OF SPLIT SAMPLE INFORMATION August 11, 1992 Shipments Sample Location Field Blank B-12 MW-5 Sample Matrix Rniatc Soil Soil Volatile! BHR60 BHR61 BHR62 BNA- Extnctabfei BHR60 BHR61 BHR62 Mculi MBES70 MBES71 MBES72 Cyanide MBE55S MBE571 MBE572 MTBE n-propy (benzene 1 ,2-dibromoetfaane 7382B-01-«0 73S2B-01-61 73S2B-01-62 TPH 7382B-02-60 73S2B-02-61 7382B-02-62 Dtlerrimeof Sample Collection 8/1 1/92 9 1400 8/11/929HOO 8/11/929 1700 Sample Remarki — 6-8' interval 1-4' interval QC Remarki Field Blank MS/MSD ... TABLES TUTU WELLFIELD SITE SUMMARY OF SURFACE SOIL SPLIT SAMPLES August 19, 1992 Shipments Sample Location SS-1 SS-2 SS-3 SS-4 SS-5 SS-6 SS-7 SS-S Sampling Date/Time 8/19/92 & 0930 8/19/92 @ 0945 8/19/92 @ 1030 8/19/92 <3> 1945 8/19/92® 1130 8/19/92 @ 1200 8/19/92 @ 1330 8/19/92 @ 1345 Sample Matrix Soil Soil Soil Soil Soil Soil R in sate Soil VOA Sample No. NA NA BFY-35 BFY-36 BFY-37 BFY-38 BFY-39 BFY-40 BNAs Sample No. BFY-NS BFY-NS BFY-35 BFY-36 BFY-37 BFY-38 BFY-39 BFY-40 Inorganic Sample No. MBXS-33 MBXS-34 MBXS-35 MBXS-36 MBXS-37 MBXS-38 MBXS-39 MBXS-40 c NA - Not Analyzed rj- TABLE 4 TUTU WELLFIELD SITE SUMMARY OF SPLIT SAMPLE INFORMATION August 11, 1992 Shipments Sample Location FB0929 RTB-01 MW6R RTB-02 MW4 MW5 MW14 Simple Matrix Rniale Aqueotu Aqueotu Aqueous Aqueoui Aqueoui Aqueoui Volatile. BHBS2 BHB5I BHB53 BHB54 BHB55 BHB56 BHB57 BNA- ExtncUbki BHB52 NA BHB53 NA BHB55 BHB56 BHB57 Metalt MB0061 NA MBOO60 NA MBOO59 MBOO5S MBOO57 Cyanide MB0061 NA MB0060 NA MBOO59 MB005I MBOO57 MTBE o-propylbcoxcoc 1,2-dibromoemanc 7511B-02-02 75! IB-02-01 75UB-02-03 751 IB-02-04 751 IB-02-05 751 IB-02-06 7511B-02-07 TPH 751 IB-01-01 NA 751 IB-01 -02 NA 751 IB-01 -03 751 IB-01-04 751 IB-0-05 Date/Time of Sample Collection 9/29/92 & 1040 9/29/92 0 0730 9/29/92 0 1315 9/30/92 A 1200 9/30/92 0 1330 10/1/92 & 1000 10/1/9291300 Sample Renuiti — _. ... — ~ — — QC Remarks Field Blank Trip Blank — Trip Blank MS/MSD — - NA - Not Analyzed TABLE 5 TUTU WELLFIELD WATER (ug/L). SOIL (ug/kg) CASE MO. 18S03 AND 7382B-01 VOLATILE DATE COLLECTED: CASE/SAS NO: SAMPLE LOCATION: SAMPLE NO: MATRIX: ChloroMethane BroMOMethane Vinyl Chloride Ch loroethane Methylene Chloride Acetone Carbon Disulf ide 1,1-Dichloroethene 1 , 1 -D i ch loroethane 1,2-Dichloroethene (total) Chloroform 1, 2 -Dich loroethane 2-Butanone 1,1,1-Trichloroethane Carbon Tetrachloride Bromodi ch I oromethane 1 , 2 - D i ch I oropr opane cis-1,3-Dichloropropene Trichloroethene D < bromoch loromethane 1 . 1 ,2- Trichloroethene Benzene t r ans - 1 , 3 - D i ch 1 oropr opene Bronof om 4-Methyl -2-Pentanone 2-Hexanone T et r ach I oroethene 1 , 1 ,2,2-Tetrachloroethane Toluene Chlorobenzene Ethylbenzene Styrene Xylene (total) 1,2-Dibo*oethane(EDB) Methyl Tertiary Butyl Ether N-Propy I benzene TOTAL PETROLEUM HYDROCARBONS 7/24/92 18S03 MU-9 (0-* ft) BHR-63 SOIL 10 U 10 U 10 U 10 U 25 UJ 70 UJ 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 J 10 U 10 U 10 U 10 U 10 UJ 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 11 U 11 U 11 U 163.0 7/24/92 MU-9 (0-4 ft) MU-9 PRP SOIL 11 U 11 U 11 U 11 U 18 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 5 U 10 U 5 u 230.0 D 7/21/92 18503 MU-6D BHR-64 SOIL 11 U 11 U 11 U 11 U 26 UJ 55 UJ 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 UJ 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 194.0 7/21/92 MU-6D MU-60 PRP SOIL ** 7/20/92 18503 MU-8 (2-4 ft) BHR-65 SOIL 11 U 11 U 11 U 11 U 25 UJ 53 UJ 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 UJ 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 69.3 7/20/92 MU-8 (2-4 ft) ME-8 PRP SOIL 11 U 11 U 11 U 11 U 25 27 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 2 J 11 U 1 J 11 U 11 U 11 U 11 U 5.6 U 11 UJ 5.6 UJ 22.0 U NOTE: ** - Location MU-6D was later abandoned and Geraghty and Miller did not provide the data TUTU UELLFIELD WATER (ug/L), SOIL (ug/kg) CASE MO.18544, 73828-01 AND 73828-02 VOLATILE TABLE 5 Continued DATE COLLECTED: CASE/SAS HO: SAMPLE LOCATION: SAMPLE HO: MATRIX: Chloromethana Bromonethane Vinyl Chloride Chloroethane Methylene Chloride Acetone Carbon Disulfide 1,1-Dfchloroethene 1 , 1 -0 i ch I oroethene 1,2-Dichloroethene (total) Chloroform 1,2-Dichloroethane 2-Butanone 1,1,1-Trichloroethane Carbon Tetrachloride Bronodi ch 1 oromethane 1 , 2-Dichloropropane cis-1,3-Dichloropropene Trichloroethene D i broMoch I orooe thane 1,1,2-Trichloroethane Benzene t rans • 1 , 3 - D i ch 1 oropropene BroMofor* 4-Methyl -2-Pentanone 2-Hexanone Tet rach I oroethene 1 , 1 ,2,2-Tetrachloroethane Toluene Chlorobenzene Ethyl benzene Styrene Xylene (total) 1,2-DiboiMethane(EDB) Methyl Tertiary Butyl Ether N-Propylbenzene TOTAL PETROL IUM HYDROCARBONS 7/30/92 18544 B-1 (4-8 ft) BHR-66 SOIL 11 U 11 U 11 U 11 U IB UJ 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 UJ 11 U 11 U 11 U 11 U 11 U 1 J 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 60.2 7/30/92 B-1 (4-8 ft) B-1 PRP SOIL 38 U 38 U 38 U 38 UJ 38 U 16 J 38 U 38 U 38 U 38 U 38 U 38 U 38 U 38 U 38 U 38 U 38 U 38 U 38 U 38 U 38 U 38 U 38 U 38 U 38 U 38 U 38 U 38 U 38 U 38 U 38 U 38 U 38 U 19 U 38 UJ 19 UJ 77.0 U 7/30/92 18544 B-6 (4-8 ft) BNR-67 SOIL 11 U 11 U 11 U 11 U 17 UJ 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 UJ 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 69.6 7/30/92 B-6 (4-8 ft) B-6 PRP SOIL 29 U 29 U 29 U 29 U 29 U 370 29 U 29 U 29 U 29 U 29 U 29 U 59 29 U 29 U 29 U 29 U 29 U 29 U 29 U 29 U 29 U 29 U 29 U 29 U 29 U 29 U 29 U 29 U 29 U 29 U 29 U 29 U 15 U 30 UJ 15 UJ 170.0 7/29/92 18544 FB 7/29 BHR-69 WATER 10 U 10 U 10 U 10 U 2 BJ 10 UJ 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 3.0 U 7/29/92 FB 7/29 FB 7/29 PRP WATER 10 U 10 U 10 U 10 U 1 J 10 UJ 5 J 10 U 10 U 10 U 10 U 10 U 10 UJ 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 u 10 U 10 U 10 U 5 U 10 U 5 UJ 0.5 U TUTU WELLFIELO UATER (ug/L), SOIL (ug/kg) CASE 18559 Volatile [DATEl ————————————————— CASE/SAS NO: SAMPLE LOCATION: SAMPLE NO: MATRIX: Chloromethane Bromomethane Vinyl Chloride Chloroethane Methylene Chloride Acetone Carbon DUulffde 1,1-Dichloroethene 1,1-Dichloroethane 1,2-Dichloroethene (total) Chlorofom 1.2-Oichloroethane 2-Butanone 1,1.1-Trichloroethane Carbon Tetrachloride Bromodi ch I oronethane 1,2-Dichloropropane ci»-1,3-0ichloropropene Trichloroethene D i bromoch I oronet hane 1.1,2-Trichloroethane Benzene trans- 1 ,3-Dichloropropene Bromofom 4 -Methyl -2-Pentanone 2-Nexanone Tetrachloroethene 1 , 1 ,2,2-Tetrachloroethane Toluene Chlorobenzene Ethyl benzene Styrene Xylene (total) 1,2-OibroMoethane (EDB) tern-Butyl methyl ether N-Propy I benzene TOTAL PETROLEUM HYDROCARBONS 18/11/92 ———— 18559 FB 8/11 BHR60 UATER 10 UJ 10 U 10 U 10 U 2 BJ 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 3.2 B7TT792 ——— FB 8/11 FB 8/11 PRP UATER 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 5 u 10 UJ 5 UJ 0.5 U ia/n/92 —— 18559 8-12(6-8 ft) BHR61 SOIL 12 U 12 U 12 U 12 U 28 UJ 25 UJ 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 11 U 11 U 11 U 26.4 o/11/« B-12(6-8ft) B-12 PRP SOIL 11 U 11 U 11 U 11 U 11 UJ 13 UJ 11 U 11 U 11 U 11 U 11 U 11 U 11 UJ 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 UJ 11 UJ 11 U 11 U 11 U 11 U 11 U 11 U 11 U 5.7 U 11 UJ 5.7 UJ 25.0 «/1 1/92 18559 MU-S(O-Aft) BHR62 SOIL 10 U 10 U 10 U 10 U 27 UJ 31 UJ 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 11 U 11 U 11 U 1210.0 8/11/92 MU-5(0-4ft) MU-5 PRP SOIL 11 U 11 U 11 U 11 U 11 UJ 11 UJ 11 U 11 U 11 U 11 U 11 U 11 U 11 UJ 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 UJ 11 UJ 11 U 11 U 11 U 11 U 11 U 11 U 11 U 5.3 U 11 UJ 5.3 UJ 590.0 D TUTU UELLFIELD VOLATILE ORGANIC DATA UATER (ug/L), SOIL (ug/kg) CASE NO. 18648 VOLATILE TABLE 5 Continued DATE COLLECTED: CASE/SAS NO: SAMPLE LOCATION: SAMPLE NO: MATRIX: Chloromethane BroMomethane Vinyl Chloride Chloroethane Methylene Chloride Acetone Carbon Disulfide 1,1-Dfchloroethene 1,1-Di chloroethane 1,2-D<chloroethene (total) Chlorofon* 1,2-Dichloroethane 2-Butanone 1,1, 1 -Tri chloroethane Carbon Tetrachloride BroModichloromethane 1 , 2-D i ch I oropropane cis-1,3-Dichloropropene Trichloroethene D i bromoch 1 oromethane 1,1,2-Trichloroethane Benzene t rans - 1 , 3 - D i ch I oropr opene BroMoform 4 - Methy 1 - 2 - Pentanone 2-Hexanone Tetrach 1 oroethene 1,1,2,2-Tetrachloroethane Toluene Chlorobenzene Ethylbenzene Styrene Xylene (total) 1,2-Dibomoethane(EDB) Methyl Tertiary Butyl Ether N-Propylbenzene 87T9755 ——— 18648 ss-3 BFY35 SOIL 65 U 65 U 65 U 65 U 84 UJ 91 UJ 65 U 65 U 65 U 65 U 7 J 65 UJ 54 J 65 U 65 U 65 U 65 U 65 U 65 J 65 U 65 U 65 U 65 U 65 U 65 U 65 U 65 U 65 U 65 U 65 U 65 U 65 U 65 U 8779792 SS-3 SS-3 PRP SOIL 13 U 13 U 13 U 13 U 22 13 U 13 U 13 U 13 U 13 U 13 U 13 U 35 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 13 U 4 J 13 U 3 J 13 U 19 6.4U 13 UJ 6.4UJ 8/19/92 18648 SS-4 BFT36 SOIL 11 U 11 U 11 U 11 U 22 UJ 14 UJ 11 U 11 U 11 U 11 U 2 J 11 UJ 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 87T9752 ——— SS-4 SS-4 PRP SOIL 11 U 11 U 11 U 11 U 8 J 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 UJ 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 5.5 U 11 UJ 5.5 UJ 87T9791 ——— 18648 SS-5 BFY37 SOIL 11 U 11 U 11 U 11 U 16 UJ 11 UJ 11 U 11 U 11 U 11 U 2 J 11 UJ 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 8/19/92 SS-5 SS-5 PRP SOIL 11 U 11 U 11 U 11 U 10 J 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 UJ 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 5.5 U 11 UJ 5.5 UJ 8/19/92 18648 SS-6 BFY38 SOIL 12 U 12 U 12 U 12 U 26 UJ 12 UJ 12 U 12 U 12 U 12 U 12 U 12 UJ 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 8/19/92 SS-6 SS-6 PRP SOIL 11 U 11 U 11 U 11 U 22 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 11 U 1 J 11 U 11 U 11 U 11 U 11 U 11 U 5.7 U 11 UJ 5.7 UJ 8/19/92 18648 SS-7 FB BFY-39 UATER 10 UJ 10 U 10 U 10 U 2 BJ 10 UJ 10 U 10 U 10 U 10 U 10 U 10 U 10 UJ 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 UJ 10 UJ 10 U 10 U 10 U 10 U 10 U 10 U 10 U 8/19/9* SS-7 FB SS-7 PRP UATER 12 U 12 U 12 U 12 U 20 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 12 U 5.8 U 12 UJ 5.8 UJ TUTU UELLFIELO WATER (ug/L), SOIL (ug/kg) CASE NO. 18810 VOLATILE DATE COLLECTED: CASE/SAS NO: SAMPLE LOCATION: SAMPLE NO: MATRIX: ChloroiMthane BroMMMthane Vinyl Chloride Chloroethane Methylene Chloride Acetone Carbon DUulfidt 1 , 1 -D i ch I oroethene 1.1-Dichloroethane 1,2-Dichloroethene (total) Chloroform 1,2-Dichloroethane 2-Butanone 1.1,1-Trichloroethane Carbon TetrachloMde Bromodi ch loromethane 1.2-Dichloropropane cis-1.3-Dichloropropene Trichloroethene D i bromoch I oronethane 1,1,2-Trichloroethane Benzene tr«ns-1,3-Dichloropropene Broanform 4-Methyl -2-Pentanone 2-Hexanone Tetrachloroethene 1 , 1 ,2.2-Tetrachloroethane Toluene Chlorobenzene Ethylbenzene Styrene Xylene (total) 1,2-DiboiK>ethane(EDB) Methyl Tertiary Butyl Ether N-Propylbenzene 9/29/92 18810 RTB-01 BHB-51 WATER 10 U 10 U 10 U 10 UJ 5 J 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 J 10 U 10 U 10 U 10 U 10 UJ 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 9/29/92 RTB-01 RTB-01 PRP WATER 10 U 10 U 10 U 10 U 3 BJ 7 J 10 U 10 U 10 U 10 U 10 U 10 U 10 UJ 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 UJ 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 5 U 10 U 5 UJ 9/29/92 18810 FB- 09/29 BHB-52 WATER 10 U 10 U ^ 10 TJ 10 UJ 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U . 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 u 10 U 9/29/92 FB- 09/29 FB-09/29 PRP WATER 10 U 10 U 10 U 10 U 4 BJ 6 J 10 U 10 U 10 U 10 U 10 U 10 U 10 UJ 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 uj 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 u 10 U S U 10 U s uj 9/29/92 18810 MW-6R BHB-53 WATER 10 U 10 U 10 U 10 UJ 10 U 10 U 10 U 10 U 10 U 34 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 4 J 10 U 10 U 10 U 10 U 10 U 10 U 10 U 14 10 U 10 U 10 U 10 U 10 U 10 U 10 U 2 J 10 U 9/29/92 MW-6R MW-6R PRP WATER 10 U 10 U 10 U 10 U 10 U 10 UJ 10 U 10 U 10 U 39 10 U 10 U 10 UJ 10 U 10 U 10 U 10 U 10 U 3 J 10 U 10 U 10 U 10 U 10 UJ 10 U 10 U 13 10 U 10 U 10 U 10 U 10 U 10 U 5 u 10 U 5 UJ 9/30/92 18810 RTB-02 BHB-S4 WATER 0 R 0 R 0 R 0 R 1 J 0 0 0 0 0 0 0 0 0 0 0 0 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 10 U 10 U 10 U 9/30/92 RTB-02 RTB-02 PRP WATER 10 U 10 U 10 U 10 U 4 BJ 7 J 1 J 10 U 10 U 10 U 10 U 10 U 10 UJ 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 UJ 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U s u 10 U 5 UJ TUTU UELLFIELD WATER (ug/L), SOIL (ug/kg) CASE MO. 18810 VOLATILE TABLE 5 Continued DATE COLLECTED: CASE/SAS NO: SAMPLE LOCATION: SAMPLE NO: MATRIX: Chloronethane Broamethane Vinyl Chloride Chloroethane Methylene Chloride Acetone Carbon Disulfide 1.1-Dichloroethene 1 , 1 -D f ch I oroethane 1,2-Dfchloroethene (total) Chlorofon* 1 ,2-Dichloroethane 2-Butanone 1,1,1-Trichloroethane Carbon Tetrachloride Broandi eh I oroiaethane 1 ,2-Dichloropropane ci«-1,3-Dichloropropene Trichloroethene D i broMOch I oroiaethane 1 , 1 ,2-Tri chloroethane Benzene trans-1,3-Dichloropropene Bromoform 4-Methyl -2-Pentanone 2-Hexanone Tetrachloroethene 1,1,2,2-Tetrachloroethane Toluene Chlorobenzene Ethylbenzene Styrene Xylene (total) 1,2-DiboMoethane(EDB) Methyl Tertiary Butyl Ether N-Propylbenzene 9/30/92 18810 MU-4 BHB-55 WATER 0 00 0 0 0 0 0 0 780 0 0 00 0 0 0 7 0 0 0 0 0 0 0 27 0 0 0 0 R 0 R 0 R 10 U 10 U 10 U 9/30/92 MU-4 MU-4 PRP WATER 10 U 10 U 10 U 10 U 10 U 10 UJ 10 U 10 U 10 U 86 10 U 10 U 10 UJ 10 U 10 U 10 U 10 U 10 U a j 10 U 10 U 10 U 10 U 10 UJ 10 U 10 U 25 10 U 10 U 10 U 10 U 10 U 10 U 5 U 1.2 J 5 UJ 10/1/92 18810 MW-5 BHB-S6 WATER 0 R 0 R 0 R 0 R 64 J 0 R 0 R 0 R 0 R 30 J 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 1200 J 0 R 0 R 0 R 0 R 0 R 0 R 180 J 0 R 1100 J 0 R 1600 J 10 U 7700 D 270 DJ 10/1/92 MW-S MW-5 PRP WATER 500 Uu 500 U 500 U 500 U 500 U 500 UJ 500 U 500 U 500 U 500 U 500 U 500 U 500 UJ 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U 1000 U 500 U 500 UJ 500 U 500 U 500 U 500 U 180 J 500 U 930 500 U 1600 250 U 6200 180 J 10/1/92 18810 MU-14 BHB-57 WATER 0 R 0 R 18 J 0 R 1 J 0 R 0 R 0 R 0 R 38 J 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 0 0 0 0 0 0 R 1 J 0 R 0 R 0 R 0 R 0 R 0 R 10 U 10 U 10 U 10/1/92 MU-14 MW-14 PRP WATER 10 U 10 U 17 10 U 10 U 10 UJ 3 J 10 U 10 U 44 10 U 10 U 10 UJ 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 uj 10 U 10 U 1 J 10 U 10 U 10 U 10 U 10 U 10 U 5 U 10 U 5 U TABLE 6 TUTU UELLFIELD SENIVOLATILE DATA (ug/kg) CASE 18S03 SEN. SOIL DATE: CASE/SAS NO: SAMPLE LOCATION: SAMPLE NO: MATRIX: Phenol bis(2-Chloroethyl)ether 2-Chlorophenol 1,3-Dichlorobenzene 1 , 4 -0 i ch I orobenzen* 1.2-Dichlorobenzene 2-Methylphenot 2.2' -Oxybis(l-Chloropropanc) 4-Methylphenol N-Nltroso-di-n-propylamine Hexach I oroethane Nitrobenzene 1 sophorone 2-Nitrophenol 2.4-Dimethylphenol bi s ( 2 - Ch I oroethoxy )Methane 2,4-Dichlorophenol 1,2,4-TMchlorobenzene Naphthalene 4-Chloroaniline Hexach 1 orobut adi ene 4-Chloro-3-methylphenol 2-Methylnaphthalene Hexach I orocyc lopentadi ene 2,4.6-Trichlorophenol 2,4,5-Trichlorophenol 2-Chloronaphthalene 2-Nitroaniline Dimethyl Phtalate Acenaphthylene 2,6-0 initrotoluene 3-NitroaniMne Acenaphthene 2,4-Dinitrophenol 4-Nitrophenol Dibenzofuran 7/24/92 18503 MU-9 (0-4 ft) BHR-63 SOIL 340 U 340 U 340 U 340 U 340 U 340 U 340 U 340 U 340 U 340 U 340 U 340 U 340 U 340 U 340 U 340 U 340 U 340 U 340 U 340 UJ 340 U 340 U 340 U 340 U 340 U 830 U 340 U 830 U 340 U 340 U 340 U 0 R 340 U 830 U 830 UJ 340 U 7/24/92 MU-9 (0-4 ft) MU-9 PRP SOIL 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 860 U 350 U 860 U 350 U 350 U 350 U 860 U 350 U 860 U 860 U 350 U 7/21/92 18503 MU-60 (0-2ft) BHR-64 SOIL 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 870 UJ 360 UJ 870 UJ 360 UJ 360 UJ 360 UJ 0 R 360 UJ 870 UJ 870 UJ 360 UJ 7/21/92 MW-60 (0-2ft) MU-60 PRP SOIL ** 7/20/92 18503 MW-8 (0-4ft) BHR-65 SOIL 370 UJ 370 UJ 370 UJ 370 UJ 370 UJ 370 UJ 370 UJ 370 UJ 370 UJ 370 UJ 370 UJ 370 UJ 370 UJ 370 UJ 370 UJ 370 UJ 370 UJ 370 UJ 370 UJ 370 UJ 370 UJ 370 UJ 370 UJ 370 UJ 370 UJ 370 UJ 370 UJ 890 UJ 370 UJ 370 UJ 370 UJ 0 R 370 UJ 890 UJ 890 UJ 370 UJ 7/20/92 MW-8 (0-4ft) MW-8 PRP SOIL 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 900 U 370 U 900 U 370 U 370 U 370 U 900 U 370 U 900 U 900 U 370 U TUTU UELLFIELO SEMIVOLATILE DATA (ug/kg) CASE NO. 18810 SEN. WATER TABLE 6 Continued DATE: CASE/SAS NO: SAMPLE LOCATION: SAMPLE NO: MATRIX: 2.4-Dinftrotoluene Diethytphthalate 4-Chlorophenyl -phenylether Fluorene 4-Hitroaniline 4t6-Dinitro-2-methylphenol N-Nitrosod<phenylMine (1) 4-Bromophenyl -phenylether Nexach I orobenzene Pentachlorophenol Phenanthrene Anthracene Carbazole Di-n-Butylphthalate F luoranthene Pyrene Butylbenzylptithalate 3.3'-Dichlorobenzidine Benzo( a )anth racene Chrysene bis(2-Ethylhexyl)phthalate Di-n-octylphthalate Benzo(b)f luoranthene Benzo(k )f luoranthene Benzo(a)pyrene lndeno( 1 , 2,3-cd)pyrene D i benz( a, h ) anthracene Benzo(g,h, i )perylen« 19/29/92 —— i 18810 FB-09/29 BHB-52 WATER 10 U 10 U 10 U 10 U 25 U 25 UJ 10 U 10 U 10 U 25 UJ 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 UJ 10 U 10 U 10 U 10 U 10 U 10 U 9729792 ——— FB-09/29 FB-09/29 PRP WATER 10 U 10 U 10 U 10 U 25 U 25 U 10 U 10 U 10 U 25 UJ 10 U 10 U 10 U 10 U 10 U 10 U 10 UJ 10 U 10 U 10 U 50 BJ 10 UJ 10 U 10 U 10 U 10 U 10 U 10 U 9/29/92 ———— 18810 MU-6R BHB-53 WATER 10 U 10 U 10 U 10 U 25 U 25 UJ 10 U 10 U 10 U 25 UJ 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 2 JXXX 10 UJ 10 U 10 U 10 U 10 U 10 U 10 U 9729792 ——— MW-6R MW-6K PRP WATER 10 U 10 U 10 U 10 U 25 U 25 U 10 U 10 U 10 U 25 UJ 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 64 U 1 J 10 U 10 U 10 U 10 U 10 U 10 U 97515792 ——— 1 18810 MW-4 BHB-55 WATER 10 U 10 U 10 U 10 U 25 U 25 U 10 U 10 U 10 U 25 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 UJ 10 U 10 U 10 U 10 U 10 U 10 U 9735792 ——— MW-4 MW-4 PRP WATER 10 U 10 U 10 U 10 U 25 U 25 U 10 U 10 U 10 UJ 25 U 10 U 10 U 10 U 10 U 10 U 10 U 10 UJ 10 U 10 U 10 U 56 UJ 10 UJ 10 U 10 U 10 U 10 U 10 U 10 U 10/1/92 18810 MW-5 BNB-56 WATER 40 U 40 U 40 U 40 U 100 U 100 U 40 U 40 U 40 U 100 U 40 U 40 U 40 U 40 U 40 U 40 U 40 U 40 U 40 U 40 U 40 U 40 UJ 40 U 40 U 40 U 40 U 40 U 40 U 10/1/92 MW-5 MW-5 PRP WATER 10 U 10 U 10 U 10 U 25 U 25 U 10 U 10 U 10 UJ 25 U 10 U 10 U 10 U 10 U 10 U 10 U 10 UJ 10 U 10 U 10 U 22 UJ 10 UJ 10 U 10 U 10 U 10 U 10 U 10 U 16/1/92 18810 MW-14 BNB-57 WATER 10 U 10 U 10 U 10 U 25 U 25 U . 10 U 10 U 10 U 25 U 1 J 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 2 J 10 UJ 10 U 10 U 10 U 10 U 10 U 10 U 10/1/92 MW-14 MW-14 PRP WATER 10 U 10 U 10 U 10 U 25 U 25 U 10 U 10 U 10 UJ 25 U 2 J 10 U 10 U 10 U 10 U 10 U 10 UJ 10 U 10 U 10 U 10 UJ 10 UJ 10 U 10 U 10 U 10 U 10 U 10 U TUTU UELLFIELD SEMIVOLATILE DATA (ug/kg) CASE 18503 SEN. SOIL TABLE 6 Continued DATE: CASE/SAS NO: SAMPLE LOCATION: SAMPLE NO: MATRIX: 2,4-Dinitrotoluene Diethylphthalate 4- Ch 1 orophenyl -phenylether Fluorene 4-NitroaniUne 4,6-D<n<tro-2-Mthylphenol N-Nitrosodiphenylanine (1) 4-BroMOphenyl -phenylether Hexach I orobenzene Pentach t orophenol Phenanthrene Anthracene Carbazote Di -n-Butylphthalate Fluor ant hene Pyrene Butylbenzylphthalate 3.3'-Dichlorobenzidine Benzo(a)anthracene Chrysene bis(2-Ethylhexyt)phthalate D<-n-octylphthalate Benzo(b)f luoranthene BenzoC k ) f I uoranthene Benzo(a)pyrene Indeno(1,2>3-cd)pyrene Dibenz(a,h)anthracene Benzo(g,h, < )perylene 7/24/92 18503 MW-9 (0-4 ft) BHR-63 SOIL 340 U 340 U 340 U 340 U 830 U 830 UJ 340 UJ 340 UJ 340 UJ 830 U 340 U 340 U 340 U 340 U 340 U 340 U 340 UJ 0 R 340 U 340 U 340 UJ 340 UJ 340 U 340 U 340 U 340 U 340 U 340 U 7/24/92 MU-9 (0-4 ft) MW-9 PRP SOIL 350 U 350 U 350 U 350 U 860 U 860 U 350 U 350 U 350 U 660 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 46 J 350 U 350 U 350 U 350 U 350 U 350 U 350 U 7/21/92 18503 MW-6D (0-2ft) BHR-64 SOIL 360 UJ 360 UJ 360 UJ 360 UJ 870 UJ 870 UJ 360 UJ 360 UJ 360 UJ 870 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 0 R 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 7/21/92 MU-6D (0-2ft) MW-60 PRP SOIL ** 7/20/92 18503 MU-8 (0-4ft) BHR-65 SOIL 370 UJ 370 UJ 370 UJ 370 UJ 890 UJ 890 UJ 370 UJ 370 UJ 370 UJ 890 UJ 370 UJ 370 UJ 370 UJ 370 UJ 370 UJ 370 UJ 370 UJ 0 R 370 UJ 370 UJ 370 UJ 370 UJ 370 UJ 370 UJ 370 UJ 370 UJ 370 UJ 370 UJ 7/20/92 MW-8 (0-4ft) MU-8 PRP SOIL 370 U 370 U 370 U 370 U 900 U 900 U 370 U 370 U 370 U 900 U 370 U 370 U 370 U 730 B 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U NOTE: *• - Location MW-60 was later abandoned and Geraghty and Miller did not provide the data. TABLE 6 Continued TUTU WELLFIELO SOIL ORGANIC DATA DATA (ug/l), (ug/kg) CASE NO. 18544 SEMIVOL DATE: CASE/SAS NO: SAMPLE LOCATION: SAMPLE NO: MATRIX: Phenol bis(2-Chloroethyt)ether 2-Chlorophenol 1.3-Dichlorobenzene 1,4-D<chlorobenzene 1 ,2-Dlchlorobenzen* 2-Methylphenol 2.2'-Oxybis(1-Chloropropane) 4-Methylphenol N-N1troso-d1-n-propylam1ne Nexach I oroethane Nitrobenzene I •ophorone 2-Nitrophenol 2,4-DlMethylphenol bi *(2-Ch I oroethoxy )methane 2,4-Dichlorophenol 1,2.4-Trlchlorobenzene Naphthalene 4-Chloroanillne Hexach lorobutadiene 4-Chloro-3-»ethylphenol 2-Methylnaphthalene Hexach 1 orocyc I opentadi ene 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2-Chloronaphthalene 2-Nltroaniline Di*ethylphthalate Acenaphthylene 2,6-Ointtrotoluene 3-Nitroanlline Acenaphthene 2,4-Dlnltrophenol 4-Nitrophenol Oibenzofuran 7/30/92 18544 B-1 (4-8 ft) BHR-66 SOIL 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 350 U 860 U 350 U 860 UJ 350 U 350 U 350 U 860 U 350 U 860 UJ 860 UJ 350 U 7/30/92 B-1 (4-8 ft) B-1 PRP SOIL 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 3100 U 1300 U 3100 U 1300 U 1300 U 1300 U 3100 U 1300 U 3100 U 3100 U 1300 U 7/30/92 18544 B-6 (4-8 ft) BHR-67 SOIL 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 870 UJ 360 UJ 870 UJ 360 UJ 360 UJ 360 UJ 870 UJ 360 UJ 870 UJ 870 UJ 360 UJ 7/30/92 B-6 (4-8 ft) B-6 PRP SOIL 820 U 820 U 820 U 820 U 820 U 820 U 820 U 820 U 820 U 820 U 820 U 820 U 820 U 820 U 820 U 820 U 820 U 820 U 820 U 820 U 820 U 820 U 820 U 820 U 820 U 2000 U 820 U 2000 U 820 U 820 U 820 U 2000 U 820 U 2000 U 2000 U 820 U 7/29/92 18544 FB 7/29 BHR-69 WATER 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 25 UJ 10 UJ 25 UJ 10 UJ 10 UJ 10 UJ 25 UJ 10 UJ 25 UJ 25 UJ 10 UJ 7/29/92 FB 7/29 FB PRP WATER 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 25 U 10 U 25 U 10 U 10 U 10 U 25 U 10 U 10 U 25 U 10 U TABLE 6 Continued TUTU UELLFIELD SOIL ORGANIC DATA DATA (ug/l), (ug/kg) CASE NO. 18544 SEMIVOL DATE: CASE/SAS NO: SAMPLE LOCATION: SAMPLE NO: MATRIX: 2,4-Dinitrotoluene Diethylphthalate 4-Chlorophenyl -phenylether f luorene 4-NitroaniUne 4,6-Dfnltro-2-Methylphanol N-Nitro«odiphenylaM<ne (1) 4 - BroMopheny I - pheny I ether Hexach t orobenzene Pent ach t oropheno I Phenanthrene Anthracene Carbozole D<-n-Butylphthalate Fluoranthene Pyrene Butylbenzylphthalate 3,3'-Dichlorobenztdine Benzo(a)anthracene Chrysene bis(2-Ethylhexyl)phthalate Di-n-octylphthalate Benzo(b)f luoranthene Benzo( k ) f I uoranthene Benzo(a)pyrene I ndeno( 1 , 2 , 3- ed)pyrene D i benz(a, h ) anthracene Benzo(g,h, 1 )perylene 7/30/92 18544 B-1 (4-8 ft) BHR-66 SOIL 350 U 350 U 350 U 350 U 860 UJ 860 U 350 U 350 U 350 U 860 U 350 U 350 U 350 U 350 U 350 U 350 U 350 UJ 350 U 350 U 350 U 49 J 350 UJ 350 U 350 UJ 350 U 350 U 350 U 350 U 7/30/92 B-1 (4-8 ft) B-1 PRP SOIL 1300 U 1300 U 1300 U 1300 U 3100 U 3100 U 1300 U 1300 U 1300 U 3100 U 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 1300 U 7/30/92 18544 B-6 (4-8 ft) BHR-67 SOIL 360 UJ 360 UJ 360 UJ 360 UJ 870 UJ 870 UJ 360 UJ 360 UJ 360 UJ 870 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 360 UJ 7/30/92 B-6 (4-8 ft) B-6 PRP SOIL 820 U 820 U 820 U 820 U 2000 U 2000 U 820 U 820 U 820 U 2000 U 820 U 820 U 820 U 820 U 820 U 820 U 820 U 820 U 820 U 820 U 820 U 820 U 820 U 820 U 820 U 820 U 820 U 820 U 7/29/92 18544 FB 7/29 BHR-69 WATER 10 UJ 1 BJ 10 UJ 10 UJ 25 UJ 25 UJ 10 UJ 10 UJ 10 UJ 25 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 9 BJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 7/29/92 FB 7/29 FB PRP WATER 10 U 10 U 10 U 10 U 25 U 25 U 10 U 10 U 10 U 25 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U TABLE 6 Continued TUTU UELLFIELD DATA (ug/L), (ug/kg) CASE MO.18559 SEHIVOL DATE: CASE/SAS NO: SAMPLE LOCATION: SAMPLE HO: MATRIX: Phenol bf»(2-Chloro«thyl)eth«r 2-Chlorophenol 1 ,3-Dichlorobenzene 1,4-Dichlorobenzen* 1 , 2-0 i ch lorobtnzene 2-Methylphenol 2.2'-Oxybis(1-Chloropropane) 4-Methylphenol N-Ni troso-di -n-propylMiine Hexach I oroethane Nitrobenzene 1 sophorone 2-Nitrophenol 2,4-Dimethylphenol bis(2-Chloroethoxy)Methane 2.4-Dichlorophenol 1,2,4-Trichlorobenzene Naphthalene 4-Chloroaniline Hexach lorobutadi ene A-Chloro-3-Methylphenol 2 -Me thy I naphthalene Hexach 1 or ocyc I opent adi ene 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2-Chloronaphthalene 2-Nftroantline Dimethylphthalate Acenaphthylene 2,6-Dinitrotoluene 3-Nitroanilfne Acenaphthene 2,4-Dinitrophenol 4-Nitrophenol Dibenzofuran 2,4-Dlnitrotoluene Diethylphthalate 4-Chlorophenyl -phenylether Fluorene 4-Nitroanilfne 4,6-Dinitro-2-wethylphenol N-Nitrosodlphenylamine (1) 8/11/92 18SS9 FB-8/11 BHR60 UATER 10 U 10 U 10 U 10 U 10 JU 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 25 U 10 U 25 U 10 U 10 U 10 U 25 UJ 10 U 25 U 25 UJ 10 U 10 U 10 U 10 U 10 U 25 UJ 25 U 10 U 8/11/92 FB-8/11 FB-8/11 PRP UATER 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 25 U 10 U 25 U 10 U 10 U 10 U 25 U 10 U 25 U 25 U 10 U 10 U 10 U 10 U 10 U 25 U 25 U 10 U 8/11/92 18559 B-12 (6-8 ft) BHR61 SOIL 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 940 U 390 U 940 U 390 U 390 U 390 U 940 U 390 U 940 U 940 UJ 390 U 390 U 390 U 390 U 390 U 940 U 940 U 390 U 8/11/92 B-12 (6-8 ft) B-12 PRP SOIL 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 920 U 380 U 920 U 380 U 380 U 380 U 920 U 380 U 920 U 920 U 380 U 380 U 380 U 380 U 380 U 920 U 920 U 920 U 8/11/92 18559 MW-5 (0-4 ft) BHR62 SOIL 340 U 340 U 340 U 340 U 340 U 340 U 340 U 340 U 340 U 340 UJ 340 U 340 U 340 U 340 U 340 U 340 U 340 U 340 U 340 U 340 U 340 U 340 U 340 U 340 U 340 U 820 U 340 U 820 U 340 U 340 U 340 U 820 U 340 U 820 UJ 820 UJ 340 U 340 U 340 U 340 U 340 U 820 UJ 820 U 340 U 8/11/92 MW-5 (0-4 ft) MW-5 PRP SOIL 350 UJ 350 UJ 350 UJ 350 UJ 350 UJ 350 UJ 350 UJ 350 UJ 350 UJ 350 UJ 350 UJ 350 UJ 350 UJ 350 UJ 350 UJ 350 UJ 350 UJ 350 UJ 350 UJ 350 UJ 350 UJ 350 UJ 350 UJ 350 UJ 350 UJ 860 UJ 350 UJ 860 UJ 350 UJ 350 UJ 350 UJ 860 UJ 350 UJ 860 UJ 860 UJ 350 UJ 350 UJ 350 UJ 350 UJ 350 UJ 860 UJ 860 UJ 350 UJ TABLE 6 Continued TUTU WEILFIELD DATA (ug/L). (ug/kg) CASE MO.18559 SENIVOL DATE: CASE/SAS NO: SAMPLE LOCATION: SAMPLE NO: MATRIX: 4-BroMophenyl -phtnylether Hexach ( orobenzene Pentach I orophenol Phenanthrene Anthracene Carbazole Di-n-Butylphthalate F luoranthene Pyrene Butylbenzylptithalate 3,3'-D<chtorobenzidine Benzo( • ) anthracene Chrysene b<s(2-Ethylhexyl)phthalate Di-n-octylphthalate Benzo(b)f luoranthene Benzo(k)f luoranthene Benzo(a)pyrene lndeno{ 1 ,2,3-ed)pyrene 0 i benz( a,h ) anthracene Benzo(g,h, i )perylene 8/11/92 18559 FB-8/11 BHR60 WATER 10 U 10 U 25 U 10 U 10 U 10 U 10 U 10 U 10 UJ 10 UJ 10 U 10 U 10 U 3 BJ 10 UJ 10 U 10 U 10 U 10 U 10 U 10 U 8/11/92 FB-8/11 FB-8/11 PRP WATER 10 U 10 U 25 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 8/11/92 18559 B-12 (6-8 ft) BHR61 SOIL 390 U 390 U 940 U 390 U 390 U 390 U 390 U 390 U 390 U 390 UJ 390 U 390 U 390 U 390 UJ 390 UJ 390 U 390 U 390 U 390 U 390 U 390 U 8/11/92 B-12 (6-8 ft) B-12 PRP SOIL 380 U 380 U 920 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 380 U 8/11/92 18559 NW-5 (0-4 ft) BHR62 SOIL 340 U 340 U 820 U 340 U 340 U 340 0 340 U 340 U 340 U 340 UJ 340 U 340 U 340 U 340 UJ 340 UJ 340 U 340 U 340 U 340 U 340 U 340 U 8/11/92 MW-5 (0-4 ft) MW-5 PRP SOIL 350 UJ 350 UJ 860 UJ 350 UJ 350 UJ 350 UJ 350 UJ 350 UJ 350 UJ 350 UJ 350 UJ 350 UJ 350 UJ 45 J 350 UJ 350 UJ 350 UJ 350 UJ 350 UJ 350 UJ 350 UJ TUTU WELLFIELD SOIL ORGANIC DATA DATA (ug/l), (ug/kg) CASE NO. 18648 SEMIVOL TABLE 6 Continued DATE: CASE/SAS NO: SAMPLE LOCATION: SAMPLE NO: MATRIX: 4-Chlorophenyl-phenylether Fluorene 4-NitroanlUne 4,6-Dinitro-2-Methylphenol N-NftrosodiphenylM<ne (1) 4-Bromophenyl -phenylether Hexach 1 orobenzene Pentachlorophenol Phenanthrene Anthracene Carbazole Di-n-Butylphthalate Ftuoranthen* Pyrene Butylbenzytphthalate 3,3'-Dichlorobenzidine Benzo(a)anthracene Chrysene bis(2-Ethylhexyl)phthalate Di-n-octylphthalate Benzo(b)f luoranthene Benzo( k ) f I uoranthene Benzo(a)pyrene Indenod ,2,3-cd)pyrene Dibenz(a,h)anthracene Benzo(g,h, i )perylene 8/19/92 18648 SS-3 BFY3S SOIL 13000 UJ 13000 UJ 32000 UJ 0 R 13000 UJ 13000 UJ 13000 UJ 0 R 13000 UJ 13000 UJ 13000 UJ 9400 J 13000 UJ 13000 UJ 13000 UJ 13000 UJ 13000 UJ 13000 UJ 13000 UJ 13000 UJ 13000 UJ 13000 UJ 13000 UJ 13000 UJ 13000 UJ 13000 UJ 8/19/92 SS-3 SS-3 PRP SOIL 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 3400 J 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 8/19/92 18648 SS-4 BFT36 SOIL 11000 UJ 11000 UJ 28000 UJ 28000 UJ 11000 UJ 11000 UJ 11000 UJ 28000 UJ 11000 UJ 11000 UJ 11000 UJ 1800 J 11000 UJ 11000 UJ 11000 UJ 11000 UJ 11000 UJ 11000 UJ 11000 UJ 11000 UJ 11000 UJ 11000 UJ 11000 UJ 11000 UJ 11000 UJ 11000 UJ 8/19/92 SS-4 SS-4 PRP SOIL 0 0 00 0 0 0 R 0 R 0 R 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 R 8/19/92 18648 SS-5 BFY37 SOIL 370 U 370 U 900 UJ 900 U 370 U 370 U 370 U 900 U 370 U 370 U 370 U 370 U 370 U 370 U 78 J 370 U 370 U 370 U 370 U 370 UJ 370 U 370 U 370 U 370 U 370 U 370 U 8/19/92 SS-5 SS-5 PRP SOIL 390 U 390 U 950 U 950 U 390 U 390 U 390 U 950 U 390 U 390 U 390 U 55 J 100 J 76 J 190 J 390 U 390 U 59 J 430 390 U 84 J 390 U 390 U 390 U 390 U 82 J 8/19/92 18648 SS-6 BFY38 SOIL 390 U 390 U 940 UJ 940 U 390 U 390 U 390 U 940 UJ 390 U 390 U 390 U 390 U 390 U 390 U 64 J 390 U 390 U 390 U 390 UJ 390 UJ 390 U 390 U 390 U 390 U 390 U 390 U 8/19/92 SS-6 SS-6 PRP SOIL 0 0 0 0 0 0 0 0 0 0 R 0 R 0 R 0 R 0 R 58 J 0 R 0 R 0 R 290 J 0 R 0 R 0 R 0 R 0 R 0 R 0 R 8/19/92 18648 SS-7 FB BFY-39 WATER 10 UJ 10 UJ 25 UJ 25 UJ 10 UJ 10 UJ 10 UJ 25 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 0 R 10 UJ 10 UJ 2 BJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 8/19/92 SS-7 FB SS-7 PRP SOIL 370 U 370 U 910 U 910 U 370 U 370 U 370 U 910 U 370 U 370 U 370 U 62 J 370 U 370 U 75 J 370 U 370 U 370 U 270 J 370 U 370 U 370 U 370 U 370 U 370 U 370 U TUTU UELLF1ELD SOIL ORGANIC DATA DATA (ug/l), (ug/kg) CASE NO. 18648 SEMIVOL TABLE 6 Continued DATE: CASE/SAS NO: SAMPLE LOCATION: SAMPLE NO: MATRIX: Phenol bU(2-Chloroethyl )ether 2-CMorophenot 1,3-Dichlorobenzene 1 ,4-Dichlorobenzene 1 ,2-Dichlorobenzene 2-Hethylphenol 2,2'-OxybU(1-Chloropropane) 4-Methylphenol N-Nitroso-di-n-propylaMine Hexach I oroethane Nitrobenzene I sophorone 2-Nitrophenol 2,4-Dimethylphenol bis-(2-Chloroethoxy)Methane 2,4-Dichlorophenol 1,2,4-Trichlorobenzene Naphthalene 4-CMoroaniline Hexach 1 orobutadi ene 4-Chloro-3-methylphenol 2-Methylnaphthalene Hexach I orocyc I opentadi ene 2.4,6-THchlorophenol 2,4.5-Trichlorophenol 2- Ch 1 oronaphthal ene 2-Nitroaniline Dimethylphthalate Acenaphthylene 2,6-Dinitrotoluene 3-Nltroaniline Acenaphthene 2,4-Dinitrophenol 4-N!trophenol Dibenzofuran 2,4-Dinitrotoluene Diethylphthalate [S719/55 ——— I 18648 SS-3 BFY35 SOIL 0 R 13000 UJ 0 R 13000 UJ 13000 UJ 13000 UJ 0 R 13000 UJ 0 R 13000 UJ 13000 UJ 13000 UJ 13000 UJ 0 R 0 R 13000 UJ 0 R 13000 UJ 13000 UJ 13000 UJ 13000 UJ 0 R 13000 UJ 13000 UJ 0 R 0 R 13000 UJ 32000 UJ 13000 UJ 13000 UJ 13000 UJ 32000 UJ 13000 UJ 0 R 0 R 13000 UJ 13000 UJ 13000 UJ S7TC755 ——— SS-3 SS-3 PRP SOIL 0 R 0 00 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R 0 R [8719791 ———— 18648 SS-4 BFY36 SOIL 11000 UJ 11000 UJ 11000 UJ 11000 UJ 11000 UJ 11000 UJ 11000 UJ 11000 UJ 11000 UJ 11000 UJ 11000 UJ 11000 UJ 11000 UJ 11000 UJ 11000 UJ 11000 UJ 11000 uj 11000 UJ 11000 UJ 11000 UJ 11000 UJ 11000 UJ 11000 UJ 11000 UJ 11000 UJ 28000 UJ 11000 UJ 28000 UJ 11000 UJ 11000 UJ 11000 UJ 28000 UJ 11000 UJ 28000 UJ 28000 UJ 11000 UJ 11000 UJ 11000 UJ 8719/95 ———— SS-4 SS-4 PRP SOIL 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 R 0 R 0 R 8/19/92 18648 ss-5 BFY37 SOIL 370 UJ 370 UJ 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 900 U 370 U 900 UJ 370 U 370 U 370 U 900 UJ 370 U 900 UJ 900 U 370 U 370 U 370 U 8/19/92 SS-S SS-S PRP SOIL 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 950 U 390 U 950 U 390 U 390 U 390 U 950 U 390 U 950 U 950 U 390 U 390 U 390 U 8/19/92 18648 SS-6 BFY38 SOIL 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 390 U 940 U 390 U 940 UJ 390 U 390 U 390 U 940 UJ 390 U 940 U 940 U 390 U 390 U 390 U 8/19/92 SS-6 SS-6 PRP SOIL 0 R 0 R 0 R 0 R 0 0 0 0 0 0 0 0 0 0 0 0 0 0 00 0 0 0 0 0 0 0 0 0 0 0 0 0 R 0 R 0 R 0 R 0 R 0 R 8/19/92 18648 SS-7 FB BFY-39 WATER 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 10 UJ 25 UJ 10 UJ 25 UJ 10 UJ 10 UJ 10 UJ 25 UJ 10 uj 25 UJ 25 UJ 10 UJ 10 UJ 10 UJ 8/19/92 SS-7 FB SS-7 PRP SOIL 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 370 U 910 U 370 U 910 U 370 U 370 U 370 U 910 U 370 U 910 U 910 U 370 U 370 U 370 U TABLE 6 Continued TUTU UELLFIELD SEMI VOLATILE DATA (ug/kg) CASE NO. 18810 SEN. WATER DATE: CASE/SAS NO: SAMPLE LOCATION: SAMPLE NO: MATRIX: Phenol bis(2-Chloroethyl)ether 2-Chlorophenol 1 ,3-Dichlorobenzene 1 . 4 -D i eh I orobenzene 1 ,2-Dichlorobenzene 2-Methylphenol 2,2'-Oxybis(1-Chloropropane) 4-Methylphenol N-Nitroso-di-n-propylaM<ne Hexach I oroethane Nitrobenzene I sophorone 2-Nitrophenol 2.4-Dimethylphenol bi s( 2 - Ch loroethoxy )methane 2,4-Dichlorophenol 1,2,4-Trichlorobenzene Naphthalene 4-Chloroaniline Hexach I orobutad i ene 4-Chloro-3-methylphenol 2-Methylnaphthalene Hexachlorocyclopentadiene 2.4,6-Trichlorophenol 2,4,5-Trichlorophenol 2-Chloronaphthalene 2-Nitroaniline Dinethylphthalate Acenaphthylene 2,6-Dinitrotoluene 3-Nitroaniline Acenaphthene 2.4-D<nitrophenol 4-Nitrophenol Dibenzofuran 9/29/92 18810 FB-09/29 BHB-52 UATER 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 25 U 10 U 25 U 10 U 10 U 10 U 25 U 10 U 25 UJ 25 U 10 U 9/29/92 F8-09/29 FB-09/29 PRP WATER 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 25 U 10 U 10 U 10 U 10 UJ 10 U 10 U 10 U 10 U 25 U 10 U 25 U 10 U 10 U 10 u 25 U 10 U 25 U 25 UJ 10 U 9/29/92 18810 MW-6R BHB-53 WATER 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 25 U 10 U 25 U 10 U 10 U 10 U 25 U 10 U 25 UJ 25 U 10 U 9/29/92 MW-6R MW-6R PRP WATER 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 25 U 10 U 25 U 10 U 10 U 10 U 25 U 10 U 25 U 25 U 10 U 9/30/92 18810 MW-4 BHB-55 WATER 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 25 U 10 U 25 U 10 U 10 U 10 U 25 U 10 U 25 UJ 25 U 10 U 9/30/92 MW-4 MW-4 PRP WATER 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 25 U 10 U 25 U 10 U 10 U 10 U 25 U 10 U 25 U 25 U 10 U 10/1/92 18810 MW-5 BHB-56 WATER 39 BJ 40 U 40 U 40 U 40 U 40 U 40 U 40 U 40 U 40 U 40 U 40 U 40 U 40 U 19 J 40 U 40 U 40 U 160 40 U 40 U 40 U 58 40 U 40 U 100 U 40 U 100 U 40 U 40 U 40 U 100 U 40 U 100 UJ 100 U 40 U 10/1/92 MW-5 MW-5 PRP WATER 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 UJ 3 J 10 U 10 U 10 U 10 U 10 U 7 J 10 U 10 U 10 U 310 D 10 U 10 U 10 U 130 D 10 U 10 U 25 U 10 U 25 U 10 U 10 U 10 U 25 U 10 U 25 U 25 U 10 U 10/1/92 18810 MW-14 BHB-57 WATER 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 25 U 10 U 25 U 10 U 10 U 10 U 25 U 10 U 25 UJ 25 U 1 J 10/1/92 MW-14 MW-14 PRP WATER 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 UJ 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 u 10 U 10 U 10 U 10 U 25 U 10 U 25 U 10 U 10 U 10 U 25 U 10 U 25 U 25 U 2 J TABLE 7 TUTU UELLFIELD WATER (ug/L), SOIL (ug/kg). CASE MO.18503 METALS DATE COLLECTED: CASE/SAS NO: SAMPLE LOCATION: SAMPLE NO: MATRIX: AluniniM Antimony Arsenic BariuM Beryl 1 inn CadMiun Calciun ChroMiua Cobalt Copper Iron Lead Magnesium ManganUe Mercury Nickel PotasciiM Sel-eniuM Silver SodiuM ThalliuM VanadiiM Zinc Cyanide 7/24/92 18503 MW-9 (0-4 ft) MBES-56 SOIL 33600.00 3.40 UJ 0.46 UJ 25.00 B 0.15 U 0.31 U 43900.00 25.40 26.80 J 67.00 39200.00 4.40 J 22000.00 920.00 0.05 U 18.90 J 264.00 B 0.0 R 1.80 B 1010.00 B 0.90 U 90.60 51.70 0.52 U 7/24/92 MW-9 (0-4 ft) MW-9 PRP SOIL 22400.00 6.00 B 0.7 B 18.7 B 0.21 U 0.64 U 31600.00 15.6 18.9 50.7 25700.00 3.2 J 15100.00 631.00 0.05 U 12.4 205.00 B 0.43 U 0.64 U 654.00 B 0.64 U 56.3 32.4 0.53 U 7/21/92 18503 MW-60 (0-2 ft MBES-57 SOIL 24200.00 3.70 UJ 0.0 R 81.90 0.28 B 0.34 U 38700.00 28.90 23.10 J 68.40 40700.00 11.80 J 16700.00 794.00 0.06 U 17.20 J 897.00 B 00 R 1.70 B 717.00 B 0.94 U 114.00 84.70 0.53 U 7/21/92 MU-6D (0-2ft) MW-60 PRP SOIL ** 7/20/92 18503 MW-8 (2-4 ft) MBES-58 SOIL 33000.00 3.40 UJ 0.46 UJ 23.80 B 0.21 B 0.32 U 39000.00 20.80 24.50 J 57.10 37500.00 1.90 J 20600.00 859.00 0.05 U 15.70 J 201.00 B 0.0 R 1.70 B 843.00 B 0.90 U 85.60 45.10 0.55 U 7/20/92 MW-8 (2-4 ft) MW-8 PRP SOIL 22500.00 5.6 B 0.44 U 21.7 B 0.22 U 0.65 U 28400.00 15.3 J 19.00 49.7 26500.00 0.48 BJ 15400.00 688.00 0.05 U 11.3 204.00 B 0.44 UWJ 0.65 U 491.00 B 0.65 U 59.5 31.8 0.55 NOTE: ** - Location MW-6D Mas later abandoned and Geraghty and Miller did not provide the data. TABLE 7 Continued TUTU UELLFIELD WATER (ug/L), SOIL (ug/kg) CASE NO. 18559 CYANIDE DATE: CASE/SAS NO: SAMPLE LOCATION: SAMPLE NO: MATRIX: Cyanide 8/11/92 18559 FB 8/11 M8ES-70 UATER 10 U 8/11/92 FB 8/11 FB PRP UATER 10 U 8/11/92 18559 B-12 (6-8 ft) MBES-71 SOIL 0.56 U 8/11/92 B-12 (6-8 ft) B-12 PRP SOIL 0.57 U 8/11/92 18559 MU-5 (0-4 ft) MBES-72 SOIL 0.50 U I\J *• e c a 01 c m c « toe -» ui *• >< Ul O Ul -« -» C OB OB C 09 C c. X C C 09 COB M C C COB OBC C. Z C. Z C C OB C Ul — Ul -• O -« - • * « 09 M -^ M C C 09 OBC c. COB C A CASE/ LE LE IX COLLEC SAS NO E LOCA S L NO a 3 in in V><A JO PJ x to -• « S « r- to o< h -O ijj rf ui ix M UI OBC C CC OB. -• M Ul -« 09 Ul -. *• -• >4ui _• o ui ui -• -»o-»o-Mrjwp <r> C COBOBCC. C CC OBC C CC..C. C ^ « is* -^ ftj -^ O- O <O *» M — o -« -• U O M O a X J W O 4 O O O M -* -o JK ""xl^ C «C. C CC > U> </> OB ft/I M W ssa 8 Z <n -• OB 09 (A 09 *v ? «/> Ul ? U> M Ul U> 1- UIUI 555 m m c • 5 S m o S TUTU UELLFIELD UATER (ug/L), SOIL (ug/kg). CASE NO. 18648 NETALS TABLE 7 Continued DATE COLLECTED: CASE/SAS NO: SAMPLE LOCATION: SAMPLE NO: MATRIX: Aluminum Antimony Arsenic Bar i in Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganise Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc Cyanide 8/19/92 18648 SS-6 MBXS-38 SOIL 30800.00 3.8 U 8.2 84.9 0.52 B 2.0 34100.00 21.5 22.7 96.2 42300.00 75.2 17700.00 817.00 0.25 10.5 4540.00 J 0.0 R 3.2 366.00 B 0.20 UJ 131.00 170.00 0.59 U 8/19/92 SS-6 SS-6 PRP SOIL 14300.00 J 7.4 BNJ 17.3 J 89.00 J 0.23 UJ 0.68 UJ 59200.00 J 23.3 NJ 14.00 J 55.4 NJ 39500.00 J 14.4 J 9960.00 J 662.00 J 0.06 U 14.1 J 1910.00 J 0.46 UJ 1.6 BJ 340.00 BJ 0.68 UJ 71.3 NJ 91.7 J 0.57 U 8/19/92 18648 SS-8 MBXS-40 SOIL 31000.00 3.2 U 0.67 BJ 30.4 B 0.27 B 0.30 U 100000.00 20.4 20.00 56.1 33100.00 0.0 R 23800.00 911.00 0.09 U 10.3 520.00 B 0.70 UJ 0.95 U 184.00 B 0.18 UJ 108.00 51.3 0.51 U 8/19/92 SS-8 ss-a PRP SOIL 21500.00 J 14.7 BNJ 0.99 BJ 29.3 BJ 0.41 UJ 1.2 UJ 144000.00 J 16.2 NJ 16.9 BJ 43.1 NJ 25400.00 J 2.5 SJ 21400.00 J 888.00 J 0.05 U 12.9 BJ 325.00 BJ 0.41 UJ 1.7 UJ 187.00 BJ 0.62 UJ 82.1 NJ 43.8 J 1.1 8/19/92 18648 FB SS-7 MBXS39 UATER 48.2 BJ 16.3 UJ 2.4 UJ 4.6 UJ 0.70 UJ 1.5 UJ 64.4 BJ 4.9 UJ 3.5 UJ 3.8 UJ 7.6 UJ 3.2 J 40.1 UJ 4.4 UJ 0.31 J 3.9 UJ 266.00 UJ 3.6 UJ 4.8 UJ 148.00 BJ 0.90 UJ 2.4 UJ 10.5 BJ 10.0 U 8/19/92 FB SS-7 FB SS-7 PRP UATER 13800.00 J 6.00 BNJ 19.1 J 90.9 J 0.23 UJ 0.7 UJ 30700.00 J 18.8 NJ 13.8 J 54.8 NJ 23800.00 J 11.4 J 9670.00 J 672.00 J 0.06 U 10.7 J 2070.00 J 0.47 UJ 0.93 UJ 251.00 BJ 0.7 UJ 73.1 NJ 97.1 J 1.3 TUTU UELLFIELD WATER (ug/L), SOIL (ug/kg). CASE NO. 18810 METALS TABLE 7 Continued DATE COLLECTED: CASE/SAS NO: SAMPLE LOCATION: SAMPLE NO: MATRIX: AluMinuM Antimony Arsenic Barium Beryl HIM Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Mangani se Mercury Nickel Potassium Selenium Silver Sodium Thai liun Vanadium Zinc Cyanide 10/1/92 18810 MU-14 MBGG-57 WATER 4370.00 11.00 U 3.00 UJ 125.00 B 1.00 U 2.00 U 87000.00 16.40 6.70 B 27.40 6340.00 1.30 BJ 40900.00 2550.00 0.20 U 23.40 B 1340.00 B 1.00 UJ 1.00 U 128000.00 3.00 U 18.10 B 44.90 10.00 UJ 10/1/92 MU-14 MU-14 PRP WATER 5280.00 20.00 U 2.00 UW 123.00 B 1.00 U 3.00 U 89800.00 13.9 7.3 B 20.3 B 7160.00 1.8 B 42300.00 2480.00 0.1 U 14.6 B 1300.00 B 2.00 UJ 4.00 U 131000.00 3.00 U 21.00 B 34.9 J 10.00 UJ 10/1/92 18810 MU-5 MBGG58 WATER 1790.00 11.00 U 4.20 BJ 168.00 B 1.00 U 2.00 U 38000.00 14.90 5.60 B 14.20 B 2520.00 5.00 UJ 19600.00 378.00 0.20 U 50.40 9040.00 1.00 UJ 1.00 U 199000.00 3.00 U 5.80 B 30.50 10.00 UJ 10/1/92 MU-5 MBGG-58 PRP WATER 1490.00 20.00 U 3.9 B 167.00 B 1.00 U 3.00 U 40100.00 15.7 6.9 B 9.2 B 2280.00 1.00 U 21700.00 407.00 0.1 U 54.3 9310.00 2.00 U 4.00 U 214000.00 3.00 U 6.4 B 26.1 J 10.00 UJ 9/30/92 18810 MU-4 MBGG-59 WATER 11200.00 11.00 U 3.00 UJ 77.80 B 1.00 U 2.00 U 46000.00 30.50 13.20 B 40.80 16000.00 1.00 BJ 36800.00 1180.00 0.20 U 34.80 B 2270.00 B 1.00 UJ 1.00 U 238000.00 3.00 U 78.70 41.10 10.00 UJ 9/30/92 MU-4 MU-4 PRP WATER 6790.00 20.00 U 2.00 UU 61.8 B 1.00 U 3.00 U 44700.00 19.00 10.2 B 28.00 10700.00 2.4 BJ 36500.00 1020.00 0.1 U 15.2 B 2810.00 B 2.6 B 4.00 U 256000.00 3.00 UJ 64.9 27.00 10.00 UJ 9/29/92 18810 MU-6R MBGG60 WATER 22000.00 11.00 U 3.00 UJ 118.00 B 1.00 U 2.00 U 72200.00 39.60 19.70 B 79.60 28500.00 5.00 UJ 44100.00 401.00 0.20 U 38.00 B 3550.00 B 1.00 UJ 1.00 U 217000.00 3.00 U 135.00 72.30 10.00 UJ 9/29/92 MW-6R MU-6R PRP WATER 16600.00 20.00 U 2.00 UW 110.00 B 1.00 U 3.00 U 64600.00 22.5 12.3 B 56.4 21400.00 4.7 S 41700.00 314.00 0.1 U 17.1 B 3540.00 B 3.5 BJ 4.00 U 229000.00 3.00 UJ 110.00 47.00 0.00 R 9/29/92 18810 FB 9/29 MBGG-61 WATER 38.60 B 11.00 U 3.00 UJ 2.00 U 1.00 U 2.00 U 302.00 B 2.00 B 2.00 U 6.60 B 137.00 1.00 BJ 81.20 B 2.60 B 0.20 U 14.10 B 409.00 U 1 .00 UJ 1.00 U 500.00 B 3.00 U 2.00 U 6.10 B 10.00 UJ 9/29/92 FB 9/29 FB 9/29 PRP WATER 32.00 U 20.00 U 2.00 U 1.00 U 1.00 U 3.00 U 46.1 B 4 00 U 4.00 U 4.00 U 14.9 B 1.00 U 44.3 B 1.00 U 0.1 U 8.00 U 560.00 U 2.00 U 4.00 U 379.00 B 3.00 U 4.00 U 2.00 U 10.00 UJ ATTACHMENT 1 EPA SAMPLE ANALYSIS QUALIFIERS 1. EPA defined qualifiers for organic compounds U - Compound was analyzed but not detected. J - estimated value N - Presumptive evidence of a compound P - The difference for detected concentration of a pesticide/Aroclor target analyte is greater than 25% between the two GC columns. C - Identification of pesticide results was confirmed by GC/MS B - Analyte is found in the associated blank as well as in the sample E - Compounds concentrations exceed the calibration range of the GC/MS instrument for that specific analysis D • Compounds identified in an analysis at a secondary dilution factor. A - TIC is a suspected aldol - condensation product. R - Data Rejected 2. EPA defined qualifier for inorganic compounds, (a) C (concentration) qualifier B - Reported value was obtained from a reading that was less than the Contract Required Detection Limit (CRDL) but greater than or equal to the Instrument Detection Limit (IDL) U - Analyte was analyzed for but not detected. 2 I of/ (11075) (b) Q (Quality Control) qualifier E • The reported value is estimated because of the presence of interference. M - Duplicate injection precision not met. N • Sample recovery not within control limits S - The reported value was determined by the Method of Standard Additions (MSA) W - Post-digestion spike for Furnace AA analysis is out of control limits (85 - 115%), while sample absorbance is less than 50% of «pike absorbance R - Data Rejected * - Duplicate analysis not within control limits + - Correlation coefficient for the MSA is less than 0.995 (c) M (method) qualifier P - for ICP A - for Flame AA F - for Furnace AA PM • for ICP when Microwave Digestion is used AM - for Flame AA when Microwave Digestion is used FM - for Furnace AA when Microwave Digestion is used CV - for Manual Cold Vapor AA AV - for Automated Cold Vapor AA CA - for Midi-Distillation spectrophotometric AS - for semi-Automated Spectrophotometric C - for manual Spectrophotometric T - for Titrimetric NR - If the analyte is not required to be analyzed. 2 2 of/ (11075)