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SDMS Document m CbRPORATION pA Halliburton Company i .• ii •••• [SV. t-f-- • y ^•Ijl | ; ;• :•—ri...-, g •#;' '5r;asf> i- . ... .i_J COr-PDRArjij^s/ 115533 i i I ^^ i p I t FINAL DRAFT SITE l^MSPECTION REPORT Vi- VI CHEMICAL ST. CipSC. U.S. VIRGIN ISLANDS y \ VOLUME 2 OF 2 n • u f " C FIELD INVESTIGATION TEAM;^ UNCONTRQlLEfSsHAZARbOllS SU • • • . ; ' ' ^ y - j i-: r" I .VAS lita-.-w^-. .-^^.1^. v'^.^^r-f.: i « ft IL NUS CORPOR^ONKH .C SUPERFUND Divfiioiy- in-nn'v.::, m '.. t..'f : - ? fT r*i si v5 •••'S'^Ir" 'v„ 100573 02-9101-04-SI / ^ REV. NO. 0 FINAL DRAFT SITE INSPECTION REPORT VI CHEMICAL ST. CROIX, U.S. VIRGIN ISLANDS VOLUME 2 OF 2 PREPARED UNDER TECHNICALDIRECTIVE DOCUMENT NO. 02-9101-04 CONTRACT NO. 68-01 -7346 FOR THE ENVIRONMENTAL SERVICES DIVISION U.S. ENVIRONMENTAL PROTECTION AGENCY SEPTEMBER 4,1991 HALLIBURTON NUS ENVIRONMENTAL CORPORATION SUPERFUND DIVISION 100574 fi m REFERENCE NO. 9 100575 NUS CORPORATION II 0725 100576 VI CHEMICAL 02-9101-04 TDD MANAGER-R. 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SKINER Waltham MA 02254 Primary contact: Lab type: Comments: Antonia Benney INORGANICS (617)890-7200 1 0 0 6 0 7 NUS FIT SAMPLING # 0 lAF E R""ASF*""^OR' RMATiON m NLV yi: UhomAcn' ShippingDatc(s): Z ^ b h i i a f l U ^ ^ , [ ^ Laboratories: Organic V O m pU 0kj?,/>O Site Name Case No. TDD/BRICS k^Cl5^ SASNc n;^.qiQ|-o4/\/xz6j:^ SamplingDate(s) ' j p \c\hJiLahX\ TJR^ iQQl lnorganic^jm/Y\C,r^ ^StMrmoA. Field SMO' A Signature/Date (Jh/lAit(yvm fl • h x y k y ^blQ i Sample Type NUS Sample No. Organic CLP No. Inorganic CLP No. QC Information Comments ^ •Tiio^jLJYidijuatt.r V X 2 5 ' ^ ^ ^ 6GLc^ (YiaPAci mslmsD ^ l A n d i i i n t f £_ GuOZ- 6GL02- meTA o>i- GrDu/ndiiJotfl rz. G-UOS b 6 - L 0 3 m6FAo2> Du^p pr 6-toi. G^i^^(k?q1fir G U J 4 B6L04 fnfcF^o4 rrfPuyvYliPatr) n &UJ5 66L0S \1f\^fA05 rrmu/vTlUJa-tQr 6-UJb bALoio \^h^^ ^^ Sori^nu^gb Siidl e)6Lcq mbrA oq fjariimiq./- ^^^gAimcai: Scd2 B6-L10 m^FA 10 Sia^. B(jL.n y^ftPA II S^din^/l^ Sacl4 66-^12. mfeFAi:^ PULP oT^sdz^ SLC^imt n i - SlLdS BG-Ln AviiFAn Scd\mt ^F Sa.d(g 6G-HU, ]fV\ferftilg So\L ;:&k; s fe6-L.i3 rv\6PA '3 m5\n^ List samples in the toilowmg order: groundwater (GW). surfacewater (bW). sedimenf (bkti), soils (S). Rinsate ^ i i i J S - F i i j A M r t - M ^ G # RM....ON C r l i M l I I ' k t L <«tLi.Cr^^t. ! • « • 4^l%f>»lr^ « 9 ! » ^ « « «>^ • « ^ M \rx ('hpmi'ccO' Isite Name Case No TDD/BRICS SAS No Sampling Date(s) 4-j? k ^ UOJlU Z X ^ i g Q i Shipping Date(s): lido)^ i J O A U ^ 8 , W I Laboratories: Organic (Jm m ,p U ftl r? >^o Inorganic 5i,b/lr\/nfl ,r4-J^klt-Aa/]A^ Signature/bate rknxJlAyyW f\ £cu>tijl y ^'^^'^' Sample Type NUS Sample Ho. Organic CLP No. Inorganic CLP No. OC Information Comments Ro^fi UI25' SX farLH {(\t^A ^ ^ c % ^ . 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Deiivef To How ana Noirty Tetepnooe Numoer 2 L j Aooress Betow i \ j Company Name To (Consignee s Namei Sireet Aooress (No PO Box Numoeri Street Aooress Teiepnone No /TELEX No iimcxxiant) g^c Q/./y stale/Province ZIP/Postai Cooe City/Town Country Destination Customs BroKer ano Tetepnone No /TELHX No. loentiticaton Numoer tof Customs txjrposes (eg,. IN /VAT /E.l N. or as local^ required) "'( " " T W B I " V Ljl L' • - • ' • ' " ' " • - " ' - ' nt lority -I 36XLettef"/ i—i „ „ „ „ ,, J ^,,metope- '2 1—1 "^ECE^ '^^'^ I' " Oedared Value Umt U.S. S100 , Theu Aanoonai ServicM Avaaaon I BelvMen U.S. & Puerto Rico Only |jNot All Options Available To All Countries p *!) n Saturday Denver/ 9 d SaurOay PicR-Up ' 30 • Economy Oist. Svc. ! D • 80 Q Deterred Heavyvwighl I ". L 111 UJ U.1JI1 pn 11,41 J u IJ. 1,11 i i u i 1 IlJ 1.1 ,y^'?^#WM'f^.> iv>i 1 riiMiWOT Tn« g-rm laitt 4 ^ . . •r dtiatllB lntnmstinnnl-*ir UVBUMI PART 110191 Rnv 4/00 ->virnarfwv> » i -ir-^^t OL-9101 0-/ : r^-.i&.,Cre"' --ntiO >••& anc^^ Peoerai Express Account Nimoar -omoanv Name • " • - ' ' A T ^ ^rom I Senoer s Name Street Aooress (No P O Box Numberi Sireei Aooress Oily/Town T ^- ' • Country State/Province ZiP/Postal Cooe Senoer fieterences iit Neeaeo First 24 cnaraciers wiii appear on .nvoice.) loeniilicaiion Numoer tor Customsourooses teg. i N /VAT /El.N, or as locaity reouireoi Deifver To Hoto anO Notrty Tewofxxw Nurno^ 2 n Aooress Be«w i d Company Name To (Consignees Namei Street Aooress 'No PO Box Numoeri Telephone NO./TELDf No dmoonani) z ^ ^ ' 6iC^ Sireet Aooress City/Town Counirv y M State/Province ZIP/Postai Cooe DestinatKxi CusiorBs Broner ana Teiepnooe No./TELEX No lOentrticaiKyi Numt»r tor Customs purposes teg,. i.N./V AT/E.IN., or asiocairy requireol \ \ •-•.-M-o .•r-^r.\'.>.s- : ••-..-• .:• . 1 Q mn Priority .en^^^^^^-'tzDfEDexPaK D D 'Oeclarea Value Limn U.S. $100 | These Adouonai Servces Avaiiaoe SoMsanUS i Puerto Rco Only ^ "Fvlot All Options A^ l^iMui fAii Options Available To All Countries 1 ^ 1 d l Bill Sfnoer 5 C ] Cash/Check In Aovance X Q Economy Oist. Svc. a 80 L J Oetetred Heavyweignt iiij.m 1 I Mill m i ijnm.11111 .11 J.I I w^'^m^mz^-'^^^rm^^mssm- Not All OptJQos Available To All Countries S n Saturday Oattttwy 9 C I Saturday PicK-Up 4 L J Dangerous Goods as per attacned Shipper s Declaration C A C ] Cargo Areratt Only D nQ « 2 n Bill Consignee 3/ 13^Bi« ThiroPany 4 " n CiecitCaro Fill tn Fedex Account Numoer or Credit Card NumtDer Below :7myw>E:,-^!i-»m:. Not All Options Available To All Countries n BiJI Sender "" ' 7 D a t Conaghee-; 8 D a* Third Party Fi| In Fedex Aaxxxtl ^kiaioat Betowr. • I W 'OU neieoy d^ee lo tne canMora on me O*CK CX Tn Non-Nego&aoo A« Wayo* Vou warrant irwi tne tnortr—cn corvanea on tna A» WayW « ffuB arxl correct, T ^ Wartw Coowr^on may aocv (O t m w r T o m ana Km) ou iiatwty tor oamage. oss or oeiav. 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Sainula ) Ntjiabar 1 ; - Gc^iOb ^ 4 ^ ^ jai HI* iM d^ )45^ JSOt -*- \^fe^ t76fe |OK» \\oc Mk woo - 1ZJQ5 JO/a loZJ fe&U2L Mko. torP^ Jbfcki^ 1 2 ^ ^ : ^ > & ^ q ^ tcy-iiri ^<r^C^ feG^^U^ £^ckil £!6kl2^ 6 ^ 1 ^ fa;^ N « ^ ^ fiGikib. fi^ n r^^^ \^ g x ^ l ^ ) '^ I L Ponn ailO-1 (a^a) Raplaoaa EPA Form 207&A 100617 '2 "m E Z E ' ' • y i - CHAIN OF CUSTODY RECORD k\rQ\l\ U Q . ' t N V I I O N M E N T A l M0TECT10N AOENCT - I I O I O N II Environmental Services IHvlsion EDISON, NEW JEKSEY 01(17 0~L RiOl 04 Iu.i..«d*-d,.« K:?^^' - ' ^ f \ ^ ' o r ^ y ^ y :c,o -^N . . ^ •:^€-or ^ ::. ~?ca-i- K l , ^ u cen-:^Q,^ K J T 0 ^ 5 - 5 Nuabcr N u n b . r of C o n t . i n . r t D.tcripti.n • ( SoapUs toTT'C, UKAJ LOi')^. ^o-v<:;l rtU_"VqK M V y \ c y p O \ y O O ^ ' ^ , Lo>3c_^.n^^ h > ^ i /7^i<^iA^ u ^ o 1 ^ X LooO C2)nc P«rion Aisuoiing Ratponiibility for S O M B I K D^JUituu A • lixxfx r I G ^ Oal* Sample Number RellaqvUkaJ Ky K.c.lved t y t T i a * D a t . / - I . M P * * " i a i f i i a a t a ai Cuttedv Sample Number Relinquifk.d Byl R . c . i v . d >r: Tim. D a l . I . a i a a far C h a n t . «> Cuitodr Sample Numb.r Relinquished fty. It.t«i<r.d ftyt n a . O a l * ( • • • • « l.r C h a n * . •( Cvitedy Xelli«quish*d B y Received By; T i a . Dot* l . a f d a iat C h a n f • at CuOedy raa* Na. 100618 Z o i- T v^ \E\ Caoier- CHAIN OF CUSTODY RECORD INV1B0NMINTAL PBOTtCTION AOENCY - (EOION II Environmental Services IHvlsion IDISON, NEW JERSEY 01117 IUU" 0 2 , ^ ) 0 ' -UH N a m . ef Unif and Addreea \ y ^ < 'Y'orcL\^yy^r^ \OAZ> ^\rEA 'ZrtOfyAZ, P'^:^-^ ^-^ b - ^ . 1 : 0 . - ^ y j '^^^^2>~7 >U 1 K_ S a a p l * Nuabar N u « b * r •f CoRtainari 0«*cripH*fi •< S s a p U i 1 U'4^^'<^^ ^ ^ \ G ^ o I J ^ (-<^'^. ^^^'^^b,-to^^ »^f^ll |f\6fftU 3 12, Pvrsen A i i u n i n g Kaitfbiiflibility fer Sanpl*: Ofiysyji f^ ^y-yor lifcxy zJ Dale y\ SompU Nw«b*r Relinquished By: Received Byi D a l . R e a l * , l . r Ch.n«e o l Custody -ho }c(t) A ^ 0)^i^^)5 Sample Number Relinquish.^ Cft R.ceived By: Data Raaiaa iar Chang* ei Custody Sample Number Relinquished B y Received B y Time D a i * • a a f a a lar Chanf a oi Custody Sample Number Relinquished Byt Received By: TIaia Oal* l * a « * a l a t C h a n f * ai Cuslady 100619 M i * N*. l o t f r • ^ ^ m X. ^ * '"^ Looier rJ E L CHAIN OF CUSTODY RECORD INVHONHAENTAl. PROTECTION AOENCY - REOION II Environmental Services Division EDISON, NEW JERSEY 0(117 ro u 3 OZ qio]-o4 Nome of Unit and Addreta | N > - --^ 1 ^ ^ — ^ ' "v^ ' ) •y c^iSoo, MT o3s^-i S . a p l . Nuaber Number el Containeri 3 4 t4 Oescripti.a . i Saaplae 2. gi^^i^. J vV \s-. I ''^y)*L.y<i jici.-^-H ^•-^KiL?^, ^ LJt;-'Cjunk, Si£a.tou?.,3~" O z r U - ^ bCriJjE itibility < « Sai t!-lrvu<rt>>viL ft • ^^o^cou- Tim. Dale Soffpia ^ » b « r . Rellnwished B « C -6<x^y Rec.iv.d B y Data Raataa iar C h a n f . a ' Cuslady Somple N u m b . r R e l l n q i l l W ^ a y ^ , R . c . i v . d B y Tim. Oala (•aeaa i a r Chaiifa ei Custody Sample Namber Relinquished B y Received B y D a l * •aaeaa iar Chanf a .< Cuslady Sampl. Number Relinquished B y Received By: D a l * 1I*«*«« tea C l M P f . al Cust.dy 100620 i7T~r -^ V_ \o ou_> ®1 CHAIN OF CUSTODY RECORD ENVIRONMENTAL PROTECTION AOENCY - REOION II Environmental Services Division EDISON, NEW JERSEY 0BI17 ? oz. ^ IOI-oH. 1 of Unit and Addr.sa j s J \ X 3 C O f P O C C X T V ^ Q \ "^ Soaple Nuaber Nuaber el Containeri Detcrlplian ei Samples ^) bo ^^z-^(^bcr^^ raslmsOj CQ<XJ> caoc.^hl^o, £>s-h<^^f^b^s 2. \\A zr\\ ^ 0 ^ i/\c, Is J LOUJ CJOOL^ J Ss^^tW\V 10 3 '^L/t' ^ b^^L^'^ ex,-o:^> M 3 PvrioA Asiuming RsBpenitbllity fa&.Saapt«: ^VUW^UKQ. ft. 6a^"a r r&t Dal *VA Somple I ^ Relinquished Bv sample i ^ Relinquished B r xoo^.y bo^^K- ,n Received B y Time D o t . R.aiws far Chanf* ei Custody Sample Number Relinquished B y Received B y Time Oal* Raoea* fer Chanfa al Custody Sample Number Relinquished B y Received Byl D a l * laaeaa iar Chaafa ei Custody iemple lumber Relinquished By: Received By: Tiaa Oala # R * * M « l*r Chanf a ai Cuslady 100621 rata Ha. \-z\ r.K \ i O ^ Coj^^'' y CHAIN OF CUSTODY RECORD ENVIRONIWENTAL FROTICTION AOENCY - RIOION II Environmental Services Division EDISON, NEW JERSEY 0Sai7 i i Name of Unit and Seaple Nuaber ; ' • > ' - • * d y \ q '7/>u4 ft'CH-i'S ^ Number el Containers y G 3 2- i4 Person Assuming Ri Sample Number Sample Number Sample Number Sample Number Relinq C AZ Relinq Relini Relinq OL ^\]0\ • o y .ddres. \OUS yor\yzryy\,jY-^ 0««crlptl»n of SoapUs 2 .^. ,vt| uoft i;i6\5,u,>aSconL , J 0 ^ ^ ' ^ + ^ sponsibility lor Soapiai uished B y uisha4 t m > . • (Uished B y uished B y Received Byi Received B y Received Byt Received By: Time Time Time Tima 0 « l * 0 * 1 . D a l * 6*1* Time Date R . a M * i . r C h a n f . ai Cuitedy to ^ b -fer on^/vySi5 R*at*a iar Chanfa ai Custody R . a M a lar C h * n f • . i Cuslady R*a*«a lar C h a n f * ai Cuiladv 100622 ^•••Na. lL>f \ 3*^ . - ^ " r ' r S a E a g B a ' '-'-g^gt!*?-?'^''^.'-?'^-*-^"*• • ' ^ ^ - A . - « — e ~ ^ <!-«(!i»- RECEIPT FOR SAMPLES AND DOCUMENTS DATE OF SAMPLE COLLECTION NAME OF £ ^ I L I T Y VI AG Poe\3 FACILITY LOCATION 0 ) r r^X4*Q0 5+eci J S4-. Crc>\% RECEIPT OF THE DOCUMENT(S) ANO/OR SAMPLEIS) 0€SCfllB6D IS HEREBY ACKNOWLEDGED: NO. OESCRIPTION Mz 2oi \ SQrrLples TRANSFERRBD BV (SIgnatura) yZ. RE NAM A->^aPQ 'SeTTy'yt^Q OATE SIGNED i 2 ^ TITLE DATE/lQNrO 100623 REFERENCE NO. 10 100624 NUS CORPORATION AND SUBSIDIARIES TELECON NOTE 4 CONTROL NO.: ^ ^ ~ < ? / / 7 / - ^ y DATE: ra//^^^/ TIME: / SSo DISTRIBUTION: - yzT z y - - ^ '/y7( BETWEEN: / ^ g g S 7 ^ o^^e^ OF: \/T ^ y f F / 9 PHONE: (8c5?)77J-377^ AND: y ^ (NUS) DISCUSSION: ^ ^ ^ tt^ysS^-^^yascL ,J(^^Ay^ ^ . ^ ^ ^ ^«»>.>«< m^y/y^ '^d^r?f(l^ t ^ d ^ y ^ .^r^^^ - ^ E^AP y^ ^ ^ / ^ yJL^^y^ y=:&o - / ^ ^ d ^ ^ ^ ^ / ' z L w ^ : ^ ^ ^t<^/Af d^^y^^y^ ' ^ ! d X , ^ ^ y ( ^ / ^ - ^ J m ^ ^ r ^ £€yri^ A y t . ^ p j j y ^ <x.^iTEy/^ f=r 7^ — y ' r ^ e Z ^ Z ' ^ - ^— I I I •—irm lag-nr i r ^ a r r t ^ t -iri 1 — NUS 067 REVISED OMS REFERENCE NO. 11 100626 O^'9/Ol- o*/ DISTRIBUTION - \/x d / L , ^ y y BETWEEN: J^/fi/lh k)£'&7rfri OF: VZP/fG- F^coA PHONE ^ 6 7 3 AND: DISCUSSION: E Z Z ^ (NUS) f;/^4f<^fPrt^ T^^yJ A^^tA/^ /Z^iJ^ ^<yati <v>.<^d4iy!y^ ^ ^<aiuayagyiJ^- / ^ - ^ y d ^ ; ^ ^ ' ^ ^ a ^ . ^ ^ ^ ^ y ^ . / , f ^ ^>cyL " ^ Z ^ ^ '^M^m.^^yd^ s.<di Ait/irk^ ^ / Pt0^fy/!t4 i AOnyTTi^cdAinf otdf\ yffgyuA / f ^ /dP . ^ ' ^ ^ ^ his If A f i Dcuiccn ncac < • REFERENCE NO.12 100628 NUS PHOTO I.D. SITE KJAMP- Azr aimicAL LOCATION: ^r^ c/?Q\y, cAl^^'^v'^^''^^-, U'^- *^-< TDD *• pt-i'1l<^l~<^^l DATE: hlylA9 3-i,—«•,-----:.•.•;,/ CN VO O O REFERENCE NO. 13 100630 GOVERNMENT OF THE VIRGIN ISL.ANDS OF THE UNITED STATES DEPARTMENT OF PLANNING AND NATURAL RESOURCES DIVISION OF FISH AND WILDLIFE LAGOON STREET COMPLEX, ROOM 203, FREDERIKSTED ST. CROIX, U.S. VIRGIN ISLANDS 00840 14 February 1991 Mr. Richard M. Settino NUS Corporation 1090 King George Post Road Suite 1103 Edison, New Jersey 00837 Dear Mr. Settino: The coastline of the area of concern (one-mile radius around Latitude 17° 42' 35" N and Longitude 64° 47' 27" W) contains a fringing red mangrove/black mangrove wetland and three small ponds, collectively referred to as Manning Bay wetland. Under V.I. Code, Act #5665 - Protection of Indigenous, Endangered and Threatened Fish, Wildlife and Plants, it is the policy of the Territory to prevent a net loss of wet- lands and only the Commissioner of the Department of Planning and Natural Resources may issue a permit to cut, prune or remove mangroves. Fair Plain Gut, an intermittant drainage way which retains water and becomes naturally dammed by beach sediments deposited by longshore wind and wave energy, is located west and south of the sewage treatment plant. This gut receives the flow from an upland watershed of 6,574 acres. Flow rates have been detennined at 3.316 cfs (BC and E/CH2M Hill, 1979). Red mangroves line Fair Plain Gut from the Airport Road to the sea. Depending upon the salinity of the water. Fair Plain Gut and ad- jacent ponds may contain the following fish species: Talapia, white mullet, majarra, tarpon, snook and lady fish. Power failures at the sewage treatment plant result in the discharge of raw sewage into Fair Plain Gut and, subsequently. Manning Bay wetland and adjacent inshore waters. The resultant fish kill in Fair Plain Gut and Manning Bay wetland is significant. Discharges from the sewage treat- ment plant and seepage from the municipal landfill into inshore coastal waters adversely impact sensitive seagrass beds and other marine benthic communities, such as coral reefs and algal plains, located both within and seaward of the area of concern. 100631 The coastline in this area is a nesting area for the White-crowned Pigeon (Columba leucocephala), a species of local concern. Other local and migratory birds use this mangrove community. The endangered Brown Pelican (Pelecanus occidentalis) feeds offshore, as will the Least Tern (Sterna antillarum) and Royal Tern (Sterna maxima). Just outside the circle to the east is Ruth Cay, a nesting area for White- crowned Pigeons and Least Terns. Recently, the Division of Fish and Wild- life introduced the endangered St. Croix ground lizard (Ameiva polops) to this island in an attempt to establish a third population. Sandy Point Wildlife Refuge, critical habitat for the endangered leather- back seaturtle (as well as nesting habitat for endangered hawksbill and green seaturtles), is located outside the area of concern at St. Croix's extreme southwestern tip. I trust this information will be of assistance to you. Should you have any questions, please contact me directly. Sincerely, ^JJULC William Tobias Fisheries Biologist REFERENCE BC&E-CH2M Hill. 1979. A sediment reduction program. Government of the Virgin Islands GN 54000.74 . WT/cdc 100632 REFERENCE NO.14 100633 '•'.-"•• y Z ^ , - : Z y z . y z ^ : - ' - y - . . : • ; REFERENCE NO. 15 100635 ••"y:iZ-:-i, tyzy ZyAy'l -. Z r "•ss^ y [^EFEIREMOE *;. 100637 .GW6 VI CHEMICAL. LEGEND a SEPTIC TANK y/y//SJOHM DRAINS !.?r)V VEGETATION ^ GROUNDWATER SAMPLE • SEDIMENT SAMPLE • SOIL SAMPLE GW4l¥l SAMPLE LOCATION CROIX, U.S.V.l SEOI APPROX. 500 I L J CORPCDRATON T/-V C O A I 02-9101-04-STR Rev. Nc. 0 NUS Sample ID Number VI25-GW1*' CLP Organic Sample Number TABLE 1 SAMPLE DESCRIPTIONS VI CHEMICAL ST CROIX, U.S. VI CASE NO. 15933 CLP Inorganic Sample Coliection Sample Number Time Type BGL01 MBFA01 1027 Aqueous Sample Location Groundwater sample collected from the production well located in the southern corner of the site. Vi25-GW2 VI25-GW3'' BGL02 MBFA02 1414 BGL03 MBFA03 1414 Aqueous Groundwater sample collected from Fairplains No. 9 public supply well . Aqueous Duplicate groundwater sample collected at the same location as sample VI25-GW2. VI25-GW4 Vi25-GW5 VI25-GW6 VI25-SED1 BGL04 MBFA04 1430 BGL05 MBFAG5 1456 BGL06 MBFA06 1506 BGL09 MBFA09 1238 Aqueous Groundwater sample collected from Fairplains No. 8 public supply well . Aqueous Groundwater sample collected from VIPA No. 1 publicsupply well. Aqueous Groundwater sample collected from VIPA No. 2 publicsupply well. Sediment Downstream sediment sample collected from River Gut at a bearing of 19° and a distance of approximately 75 feet from the western corner of the bridge on Route 56 that spans River Gut. Duplicate- Indicates that a sample was collected as an environmental duplicate sample. MS/MSD - Indicates that additional sample volume was collected and shipped to the laboratory for matrix spike (MS) and matrix spike duplicate (MSD) analysis. 100639 TABLE I (CONT'D) SAMPLE DESCRIPTIONS VI CHEMICAL ST CROIX, U.S. VI CASE NO. 15933 02-9101-04-STR Rev. No. 0 CLP Organic Sample Number CLP Inorganic Sample Number Collection Time Sample Type NUS Sample ID Sample Sample Collection Sample Sample Number Number Number Time Type Location VI25-SED2 BGLIO MBFA10 1255 Sediment Sediment sample collected from River Gut on the northeastern side of the site at a distance of approximately 25 feet from the 55-gallon drum drain and approximately 75 feet from the 4-inch PVC discharge pipe. VI25-SED3 BGLII MBFA11 1347 Sediment Upstream sediment sample collected from River Gut at a bearing of 60° and a distance of approximately 30 feet from the fence post located at the north corner of the property. VI25-SED4* BGL12 MBFA12 1255 Sediment Duplicate sediment sample collected at the same location as sample VI25- SED2. VI25-SED5 BGL17 MBFA17 1205 Sediment Sediment sample collected from a storm drain located in the center of the concrete pad between the warehouse building and the maintenance building. VI25-SED6 8GL16 MBFA16 1148 Sediment Sediment sample collected from a storm drain located at a bearing of 250° and a distance of approximately 8 feet from the south corner of the maintenance building. * Duplicate - Indicates that a sample was designated collected as an environmental duplicate sample. 100640 TABLE I (CONT'D) SAMPLE DESCRIPTIONS VI CHEMICAL ST. CROIX, U.S. VI CASE NO. 15933 02-9101-04-STR Rev. No.o NUS Sample ID Number VI25-S1** CLP Organic Sample Number BGL13 CLP Inorganic Sample Number MBFA13 Collection Sample Time Type 1046 Soil Sample Location Surface soil sample collected from the loading dock area at a bearing of 255° and a distance of 30 feet from the northeast corner of the warehouse building. Sample depth: 0 to 6 inches. VI25-S2 BGLU MBFA14 1100 Soil VI25-S3 BGL15 MBFA15 1110 Soil Surface soil sample collected from directly below a gate valve at the north end of a pipe connecting the 14 tanks of the tank farm. Sample depth: 0-6 inches. Surface soil sample collected from an area of stained soil located approximately 2 feet west of the switch panels between tanks T-4 and T-5. Sample depth: 0 to 6 inches. VI25-S6 BGL23 MBFA22 1516 Soil Background surface soil sample collected at a bearing of 0° and a distance of 50 feet from the eastern corner of VIPA No. 2 pump house. Sample depth: 0 to 6 inches. MS/MSD - Indicates that additional sample volume was collected and shipped to the laboratory for matrix spike (MS) and matrix spike duplicate (MSD) analysis. 100641 02-9101-04-STR Rev. No. 0 TABLE I (CONT'D) SAMPLE DESCRIPTIONS VI CHEMICAL ST. CROIX, U.S. VI CASE NO. 15933 NUS Sample ID Number VI25-R1N1 VI25-RIN2 VI25-TBLK1 CLP Organic Sample Number BGL18 BGL19 BGL22 CLP Inorganic Sample Number MBFA18 MBFA19 Collection Time 1013 1028 1005 Sample Type Rinsate Blank Rinsate Blank Trip Blank Sample Location Trowel rinsate collected in the field. Bowl rinsate collected in the field. Trip blank; analytefree water obtained from NUS Corp. Region 2 FIT office, Edison, New Jersey. 100642 OP rata TraOdng IXjra 1 - Revalicaatian of Case « : I g q s : ^ revisicjn o Type : T E i r ^ o r r ^ ^ ^ . c . OOCT^WTTCR : P TT.' SEVHWER S-£jQ£j.S ^ r ^ < ^ - > ^ ^ TfP^ CF ER??CP (Crit,Signif,Tra5TS) : V^o xp^rrccs DEscRipna; : Tcrra: Ti-PT P- i?_^cc. (Crit.Sigrjif .Trans) DEScRipna: : 7>£na: Criticaa error* a significant error which effects 2 or iiore sanples Significa.nt error* categories identified cn the Functional Guidelines ^anscription error « can also be considered as major or minor TQI7»L ISRCRS - • GCTT : M F ' ^ # sicmr : « ISMC s tf XAXE : a|«4/9/ 100643 SIMCftRD OPESATING FWXEDURE Title: Evaluation of Metals Data for the Date: Tea. 1990 Contract Laboratory Program Nuirtaer: His-2 ARsndix A.l: Data Assessrent - contract Revision: lO Coipliance (*Itot:al Review - Inorganics) A.l.9.17 f^nn X. XI. XII (Veriflcatiicn of InstTtmrnt;*i Par^ret^rs). A. 1.9.17.1 Is verification report presait for: InstTLsnent Detection Limits (quarterly)? [ ICP Interelateit Correction Factors (annually)? C / ICP Linear Ranges (quarterly)? [ ] __ ^^lOtJ: If no, contact DPO of the lab. A.1-9.17.2 Form X (Tnstmn«nt Detection Limits) - (Note: IDL is not required for Cyanide.) / Are ULs present for: all the analytes? ^-—V - - all the instnanents used? [_/_] For both AA and ICP v«ien both are used for same analyte? I ] MHiUi If T» for any of the above, prepare Telephone Record Log and contact laboratory. Is ITL greater than ORDL for any analyte? If yes, is the ccncentration on Form I of the sanple analyzed on the instnsnent uhose UL exceeds CPDL, greater than 5 x IDL? [ 1 — — iCnOSt I ' na, flag as estiinated all values leeu than five times KL of the instrtjmnt %i]08e nz. exceeds CJSL.. 100644 S m i M D QPS»T3IC raOCnXIRE Title: Evaliaticn of Metals Data for the Date: Feb. 1990 Contract Laboratory Program fAjnber: HW-2 Appendix. A. 1: Data Assessment - contract Revision: 10 Cotpliance (Ttotal Review - Inorganics) A . l . 9 . 1 7 . 3 gVmn XT ft i n o a r Rflmf«^| :iS2 IS uzb Was any sanple result higher than h i ^ linear range / of ICP,. [_ i Vlas any sanple result higher than the highest / calibration standard for ncn-ICP parameters? ( 1 If yes for any of the above, was the sanple diluted to obtain the result on Form I? [ ] _ . aCUCCJ: If no, flag the result reported on Form I as estimated!J). / A . l . 9 . 1 8 t o r r e n t SOl^r^ rid f^aaA^yrdtryti Is soil conLgiL in sedijnent(s) less than 50\? [ ] _L. u m c t i ' . If yes, qualify as estimated all data not previously rejected or flagged due to other QC criteria. 100645 SWN»RD CPESAinc PRDCHXJRE Title: Evaluation of M»tais Data for the Contract Laboratory Program Appendix A. 2: Data Asse&snent .Narrative Page 27 c: 33 Date: Feb. 1990 ^XJnDer: rSv- Z Revision: :: Case« SUGt contractor /WJ msf'^'Oi h/oS-fsT Site /-r r/r^,ti?/: Lab 5^^^^rA^ Reviewer ^. Afrretu Matrix: Soil — Water g Other — A.2.1 ITie case description and exceptions, if any, are noted below with reason(s) for rejection or qualification as estimated value(s) J. ^ ^ ^ ^ AU ^^"^ Cf rn^ ujfto y o.9<f.c y^y>^iiuy .^^"fifro ysfi\' <?^3, ^ r,^ >^ yJ ^>. S..J.CU ^o ^7,^^^uy. ...Mjdiitil / ? , i<f C L C Cl ^ ^ ^ ^rnc(c / ^ n P f ^ ( ^ i ^ J 7)iti 2£i ^ r A /f^ 4(>^^ <9.TfT. TJt 'cUut ^tit^f^l^ /y^tid. La^ fl^^^'7 QO . ^ ^ - K A U ^ J . fir.I'usH-. —•» fsltMiLmJ •y y f n f ^ ' O f (^ ^ S Z f L f r ^ ca . s U i Q ^ ^nf>^^\^.->.k.i.(.^i9i^l^^ /let- ^ ) - ; ^ - o l ^ c > 3 / < ? ^ ^ / ' ^ 100646 p? ,/-i3f^^ _ c,l,e>Jii02iii^Hl^^^^l('^l^^ SWWRD CPERWBB FKXZDURE Page :3 cf 35 Ccntnct Laboratory Program t^Mxr: ;-w-2 AfpBTflix A.2: Data Assessment Narrative Revision.- .: A. 2.1 (cont inuat lean) lo(%J3 W TCP ^,7.L D-./l ^ > ^ j f Z | < r ^ t y i^Z^JULL ^rc -T/.^^.J ^ ^ ^:^li^,LmJ -for 4k. ^ U ^ ^ /OcI«<M — h^^r-iUA ^ ^ < i l / j - ^ t ^ a ^ A - o \ , OA^oi.oHioTi 0(i> (P IrAt^Qot-^C^ fi) fi<(Jl Oi>ft$ ^, ftWioVs Ovfr"*^^ W V u . ^ ^ C>k(U Oot^S. Cai W\/j Uses I'^'Z-i^ft^ t^ftJtoJ^^ ^o^K^tU tAoy W SP>t<lc Sn^plt lUt^vx/- cfvWn^ 100647 smwRD QPBovmc PROCBDURE Titit; EtfUuiticn of MKals Data for the Contract Ljtontoxy Progran Appflidlx A.2: Data Assasanent Narrative Date: Feb. 1990 Number: t«-2 Revision: lo A.2.1 (continuation) 100648 SIMCWD CPHlATiic TKXSDJKE Page 30 c: 33 Title: Evaluatien Of Metals Data for the Date: Feb ^990 Contract Laboratory Program .Number Appendix A.2: Data Assessment Narrative A.2.2 Contract-Problens/Nan-Ccnpiiance Revision: 13 >MB Reviewer: Detet. Signature contractor Reviewers ^ W V \ \ . D«tej__5j^L Signature varified byt »_«__ Detej. 100649 SIWCW© CPESAmc raOCEDURE Page 3i cf 35 Title: Evaluation of Metals Data for the Date: reL. :^90 Contract Laboratory Program Nurtoer: ' y - z Afpendix A.3: Contract Non-Carpliance Revision- • (SID Report) CONISWrr NOWXMPLIANCE (S^D REPCFT) Regional Review of Uncontrolled Hazarctous Waste Site Contract Laboratory Data Paclcage CfibSE ND. The hardcopied (laboratory name) Inorganic data pacJcage received at Region II has been reviewed and the quality" assurance perforroance data sunwarized. "DTe data reviewed included: SMD Sanple NO.:_ Cane. It Matrix: contract No. v^87-KQ2S .KOZS •KQ27(saM7a7) requires that specific analytical \«rX be done a that associated reports be provided by the contractor to tha Regions, EMSL-LV, and 3 0 . gsieral criteria used to determine the perfonnance were based on an examination of: - Data Conpleteness • Duplicate Analysis Results - Matrix ^ike Results - Blank Analysis Results - Calibration Standards Results - MSA Results Items of non-conpliance with the above contract are described below. COnnents: Reviewer's Initial Date 100650 SaNCMD CPn?ATIIC PROCOURE Title: Evaluation of Metals Data for the Contract Laboratory Program Affandix A. 7: CLP Data Assessment (3ieociist Inorganic Analysis Page 35 oi 35 Date: Feb. 1990 Nunber: HW-2 Revision: -0 QCRPWIC RB3I(2»L CA3A ASSESa^EOT Region a^ CASE ND. / T f I 3 y ± C(y,rc7L LABQRAICRY SX",^ >u<t\. SITE ND. CF SAMPLES/ Mvasix ^ /^^^^-> sow* ydllELzBL Jthl. VEJISiSS. (IF NDT ESD) yJ<JS--F-rT REVHWBR'S WME r - r j r ^ ^ IPO: A i m ^ FYI r^T& &.«vqr.«^«g^n^ "^ftfiRY Ca^JEnOH EAIE > I . HGLDDC TIMES 2. O^LIERAHOC 3. BLANKS 4. ICS 5. LCS 6. DUPLIC3ME A^»LYSIS 7. r«V3RDC SPIKE 8. MSA 9. . SERIAL DILOTICU 10. a w ^ z vsurroMicN II. OTHER QC 12. (MKKLl. ASSESgETT ICP AA Hg T J^ Jl. JL J2- 0 J2- _&. j;i. O « Data has ro problane/or qualified due to minor problons. M - Data qualified due to major problans. Z « Data unacceptable. X « Problcns, but do not affect data. /vA. CYANIDE xJA JCnOJ ITD6: AREAS GF CWCEBKt NOIABLE PEI^FO^mCE: 100651 CLP Data TtacJdng Form 1 - Revalidation of Case • : I ?<^3:^ revision 0 Type : ^nnff^nn^^ CCUISACICF : C" TTT- REVIEWER ; C-V->r\f) /V^*^<?^.-, - TypE ar P J O ^ (Crit,Sigm.f,Trans) : V^o ^ ^ r r o T S . DEsocpna: : Acrra: : TiTZ €}T T^pr^. (Crit,Sisr.if,Trans) : DEsocEPna; : Acna; : Critical error* a significant error which effects 2 or more sanples 'rnificant error* categories identified on the Functional Guidelines "-cription error « can also be considered as major or minor '»S - f G^rr : t SiaCF : t TOANS : 100652 SmOAD CSaKrnXi MCUUURE Title: EvaltatiBn of Metals Deta for the Date: Feb. 1990 Contract iatoratory Program NLmPer: Hiv-2 Appendix A.l: Data Assesanent - Contract Revision: 10 Conpiiance (Tbtal Review - Inorganics) A.l.9.17 Dxm X. XI. X n fVariflriWir^ ^ TnatrrMgit^ Parameters). A. 1.9.17.1 Is verification report prescrt for: ^ Instrunant Detecticn Limits (quarterly)? ( ^ 1 2CP Intarelem«it correction Factors (annually)? \.../j^ ICP Linear Rsiget (quarterly)? (_/l _ . 2CZZQ}: If TO, contact XFO of the lab. A.l.9.17.2 Form X fTnstrtamtt; D»fca«ian Liaita) - (Note: I£L i s not required for Cyanide.) Are IIX3 presflRt for; all the analytes? [_£j all the instrunantii used? (_L.1 For both M^ and 2 9 '^Jom. both are used for analyte? (jLI aCHQI: If no for any of the above, prepare Teli^cne Record Log and contact Is nx* graitar t h n QCL for any analyte? C— 1 — If y«*. i* tha concvitration oi Form I of the sample analyna on tha Instzuant vtiose nL vcceedi (3CL, ttan S X IDL? C 1 — - ^ If 10, flag as estimated all values ttan f Iva times nx. of the instnaant 100653 33MIMD QFE2AIZIC HI "I hllTRE Title: Evalnadih'M MKali Data for tha Date: Feb. 1990 Ccntract^ Xifeoratory Program NUnber: HK-2 Appendix A. 1: Data Assesanent - contrsict Revision: 10 Ccnpliance (Ttotal Review - Inorganics) A.i.9.17.3 BCBaJSLJIiiiBaL.£aDaGai YES {C U/h Has any sanple result higher than high linear range y a t ICP. [y_] Vlas any sanple result higher than tha highest y- calibration standard for ncn-ICP parameters? [ ^ 1 If yes for any of the above, was the aaqple diluted to obtain the result on Form I? [ 1 _ . aCZXOI: If no, flag the result reported on Form I as astimaced(J). i A.1.9.18 fiwcgit aotida of a Is soil cont«it in sedim«it(s) less than 50%? ijZ^ MTTiCK: If yas, qualify as estimsted all data * not previously rejected or f laggs^ due to other QC criteria. 100654 k*^^ — SWNCAHD CPERWDJB FIOCEZXiRE Title: Svaluatioref MKals Data for the Contract Uteratory Program Aiipendlx A.2: Data Assesanant Narrative Page 27 ot 35 Date: Feb. 1990 NUnber: hM-2 Revision: lo Caset aX3t ccntractor / r f 3 3 /^/T^A'tS'? y j L i i s - P j - r Site Lab Revi i y ^ * ' \ . Matrix: Soil /rr> Water C- 4r Other ^ A.2.1 TTM case description and vcce^ions, if any, are noted below with reaaon(s) for rejection or qualification as estimated value(a) J. / r ^ /:,^f <r n )L± U « ^ ^ J . ^ ^ ^ A-krmy . f f r ^ t f i ^ y i k y ) n P ^ - A ^ cja^ f / ^ f f d J Jk£. £ iihA2l'dJ. ^ ^ £ r _ ...iLilA Ic Cid L J c ^ y^^^o 4An-t^ . 9 ^ ^ - - <^Anr3/<.S • >^/;M IOrl'*>r l U . f C itdt n . c A m J ..^ r ^ i i t r ^ i h ^ ' ,J v ^ y ^^<' Hi-^\ ml^SZL pfdX »^ g-^lt,^^it.^ JU $:a,.tU —>>/0?^^ mffA> o\.to^u^{i^^(\m^/r^('Jh^^ 1 0 0 6 5 5 GRSAiXSC FRDCZSURE Page :a of 35 Title: Etfiii^BjofMitala Beta for the Date: Feb. ;990 c c n t r s r UBoratory Program Nunoer: t«-2 Afpandtsi A.2i Data Assesansit Narrative Revision: lo A.2.1 (ccntinuation) 6 SSR, - ^ ^^t"W<f''t1 Ck/^ .C.^ , A a .^^^ ii,A ?.^ t^*ra fi^{_ .fU-^^--^ \ ^ rrih^i)r,l r <r - mfKCfi, or /a, n. IM. U • /.^ i Q c l ^ y /JLAUA — ^ 5xL ^ ' - — ^ /^^uM Ij. /^f ir. i7i ^«3 ( H J /CIP ^e..lL OiJ^Xtst^o ^/^ O ^ C f t r t y f t f a t Cf . A J . ty(re ^ f t h U r Ht *^ / O V.i 4 ^ / ALLI yfii^A '-cy«^yi.n.nr/i^./r./6,n. J3 100656 Titia: ^nJjmjm of NRaiJ KfpmaS^Zi Deta I Dtta for the PiUyiM ABiewnnTiL Narrative 29 of 35 Date: Feb. 1990 Number: m-z Revision: lo A.2.1 (continuation) r- ^ \ \ \ \ \ ' \ \ \ \ \ X X 100657 S3SWARD OPBRAaTNG WXaOURE Page 30 ot 35 Title: EvaluaeSan of Morals nwa for the Date: Feb i990 contract Laboratory Program NijTper: HW-2 Appendix A.2: itota Assessment Narrative Revision: lo . ^ - i : : ^ A.2.2 Ccncract-PrQbl«ns4«n-Qaipliance ' ^ 9 — M J..u^i>.^^»J UUJK O VA)wg A. ^ . ^ ^ L y^/il^^-IO ^ r S^. - MtdiOi Z^ I t J i ^ ^ ^ J u f • ' ^ ^ " ^ ' * ' 1 ^ M L d r J i , ^ d U D . / . U . a ^ Lrmm -TX / i . P / . ^ M / S / ^ ^ ' / 9^ M^Bmrt. •"TvV^ OBtai iiijL 100658 SIMCMD UKMM'ING PROdlURE Title: S9alaai$» of HKals Oeta for the Oontraet Laboratory Progi'am AfpwTdix A.7: CLP Data Assesanant Qieoaist Inorganic Analysis Page 35 ot 35 Date: Feb. 1990 Number: HW-2 Revision: 10 QCRSttCC REZnOAL IKIA ASSESSGn* Region o? G^SENO. inn lABCBAICPy 5/V.> iL. SIIE OT CifAraf ND. c r 9VffUS/ WCBIX / O Tc.,- L ynflsff^'Cr<f 9^/t^ wnjoBk (IF lor Eg)) /t^o^ ^ r ? IFO: AmCM 1. 2. 3. 4. 5. 6. 7. 8. 9. » 10. 11. 12. HOLDCPC TDCS ^LXEBKIIGNS OMiCS ICS LCS CUFUCATE M J O S I 3 MKIPIX SPDCE M9^ sEPiAL D i z u n a i 9 « « Z VEPinOCtZCll OIHEP QC QNESKIa ASSESSCXir rn ajvusnxxt T9aL__A CA3A ASCTy»«g gBeaav ia> SL AA Hg £> i^ D . ^ O • Deta has no ytutil—/or qualified dua to ainar problans. M • Data qualified dua to aajor problsH. Z • Data unaocaptabla. X « Probi—, but do not affect ALlltll nSMSs ML 100659 J.S. EPA - CLP INORG^' :-PA -..Ai-IPLE NO 0. 0 c-rnti-ation Unit:. g /' :•• •-J dry w e i g h t ! : ^.! G ,•' L CAS No. Color Before: COLORLESS Color After: COLORLESS Itmments : Analy te Alum inum Ant imony Arsenic Bar ium Bery11ium Cadmium Calcium Chromium Cobalt Cooper Iron Lead Hagnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc Cyanide ; c :y :y Dncentration 31.S0 14. 00 4. 60 40.30 1.00 3.00 68800.00 4. 00 4.00 5.80 121.00 3. 10 43500.00 2.20 2.00 4. 00 2670.00 4.60 2.00 54S000.00 3. 00 30.00 13.70 C B U B 0 B : T u u u u B B U B T Ti^* Bjr+ u: u 3'NUJ B ^ B; I Before: CLEAR After: CLE/ i,R M P P F P P P P P P P P F P P CV P P F P P F P P NR Texture: Art :ifacts _is FORM I - IN 100660 3/90 I.J. S. EPA - CLP INORGA:- FPA -.AT '•Z\ ,.^ :-- t- : . + •'.ini t: •^•-5/''<•:? d r - '.vieiQht I JG/L CAS No. 742<^-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-41-7 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-7 7732-49-2 7440-22-4 74*©-23-5 744i»-28-0 74^ai»n62-2 74rtfl^6-6 Color Before: COLORLESS Color After: COLORLESS Comments; Analyte Aluminum Ant imony Arsenic Barium, Bery1lium Cadmium Calcium Chromium Cobalt Copoer Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc Cyanide Concentration 39. 14. 2. 45. 1. 3. 69900. 4. 4. 11. 26. 4. 48600. 383. 0. 4. 1520. 4 . 2. 7.63000. 3. 31. 9. 40 00 00 00 00 00 00 00 00 80 20 00 00 00 20 00 00 00 00 00 00 80 00 U BJT u u u B Ul UUTvlW B: Clarity Before: CLEAR Clarity After: CLEAR M P " P F P P P P P P P P F P P CV P P F P P F P P NR Texture: Artifacts; 100661 FORM I - IN 3 / 9 0 LJ.S. EPA - CLP INORGANIC i'NAi. /• •A -..HFE"^ EPA i.ANPLE '-M •. fc: ' • z . ' \ • y t ^ JG/L ; A S N O . 742'=»-90-5 7 4 4 0 - 3 6 - 0 7 4 4 0 - 3 3 - 2 7 4 4 0 - 3 9 - 3 7 4 4 0 - 4 1 - 7 7 4 4 0 - 4 1 - 7 7 4 4 0 - 7 0 - 2 7 4 4 0 - 4 7 - 3 7 4 4 0 - 4 8 - 4 7 4 4 0 - 5 0 - 8 7 4 3 9 - 8 9 - 6 7 4 3 9 - 9 2 - 1 7 4 3 9 - 9 5 - 4 7 4 3 9 - 9 6 - 5 7 4 3 9 - 9 7 - 6 7 4 4 0 - 0 2 - 0 7 4 4 0 - 0 9 - 7 7 7 3 2 - 4 9 - 2 7 4 4 0 - 2 2 - 4 7 4 4 0 - 2 3 - 5 744©--28-0 7 4 4 | t ^ 6 2 - 2 744fii^66-6 # Color Before: COLORLESS Color After: COLORLESS omments; Analyte Aluminum Antimony Arsenic Barium Bery11ium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc Cyanide Concentrat ion 45. 14. 2. 46. 1. 3. 74100. 4. 4. 13. 19. 4. 50500. 400. 3. 4. 1760. 4. 2. 374000. 3. 33. 21. 90 00 00 30 00 00 00 00 00 60 20 20 00 00 30 00 00 00 00 00 00 60 30 U Clarity Before: CLEAR Clarity After: CLEAR Texture: Artif.acts eii»B<»^ FORM I - I N 100662 Z / 9 ^ - INORGANIC ANALVSI'T; C'ATA •^HEET EPA ?Ai-1PLE NO, 0- 0 Lini t.^ .1.5/L 11 y / K' '.g d r^ y u e i. •^g h t 1 ;AS N O . 7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-41-7 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-7 7732-49-2 7440-22-4 7440-23-5 744B-28-0 74S|a-62-2 74*a-6<)-6 Analyte Aluminum Ant imony Arsenic Barium Bery11ium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thailium Vanadium Zinc Cyanide Concentration 44.60 14. 00 2. 00 68. 10 1, 3. 00 00 127000.00 4. 4. 4. 00 00 70 11. 20 3.90 71600.00 17. 70 0.20 4. 00 2760.00 4. 00 2.00 590000.00 3.00 32.30 6.20 Q c: I —' , Bl Ul Ul W QZT Ul Ul I Ul ul Bl Bl ul N* ul B: Ul T U l^NU B M P P F P P P P P P P P F P P CV P P F P P F P P NR Color Before: COLORLESS Color After: COLORLESS mments; # Clarity Before: CLEAR Clarity After: CLEAR Texture: Artifacts FORM I - IN 100663 ;/90' INORGANTC AM-v;.. >•-. I EPA SAMPLE NO, 'D <?, or iTr.3/K,a dr-y w^eightl: 'JG/L CAS No. 7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-41-7 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-7 7782-49-2 7440-22-4 7440-23-5 744^^28-0 7^igh>62-2 74iBf-66-6 Color Before: COLORLESS Color After: COLORLESS comments: Analyte Aluminum Ant imony Arsenic ' Barium 1 Beryllium 1 Cadmium Calcium ' Chromium 1 Cobalt Copper 1 Iron 1 Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc Cyanide Concentration 19. 14. 2. 34. 1. 3. 61300. 4. 4. 4. 13. 3. 40100. 1 . 1. 4. 2880. 4. 2. 572000. 3. 50. 6. 00 00 30 70 00 00 00 00 00 00 30 70 00 00 20 00 00 00 00 00 00 30 20 U u B Clarity Before: CLEAR Clarity After: CLEAR Texture: Artifacts: 100664 FORM I IN 3 / 9 0 U.S. EPA - CLP INORGANIC ANALYSIS DATA S H E E ' •,'—tr^r.yt /i J\i .,'A ''.- ~ -• - -'n.. p ' : S-' A-^, :!.;.. : EPA SAMPLE NO. Mo :.ol id; 0, 0 Concentr.3t ion Unit: '•3/ u mg/K-g dry weight!: UG/L CAS No, Color Before: COLORLESS Color After: COLORLESS mments: # Analyte Aluminum Antimony Arsenic ' Barium Beryllium' Cadmium ' Calcium Chromium 1 Cobalt 1 Copper 1 Iron ' Lead 1 Magnesium 1 Manganese 1 Mercury 1 Nickel Potassium 1 Selenium 1 Silver 1 Sodium ! Thallium 1 Vanadium 1 Zinc 1 Cyanide 1 Concentration 45 1^ 2 49 1 3 75800 4 4 15 50 5 56000 1 0 4 1200 4 2 237000 3 25 36 .20 00 ,00 20 00 00 00 00 00 80 30 90 00 30 72 00 00 00 00 00 00 10 90 B Clarity Before: CLEAR Clarity After: CLEAR Textur.e: Artifacts: FORM I - IN 100665 3/90 • = A y CAl Nc, . 7 4 2 9 - = < 0 - 5 " ^ 4 4 0 - 3 6 - 0 7 4 4 0 - 3 , 3 - 2 :'.i-,vT-;.9--3 7 4 A . 0 - 4 1 - 7 : : ^ 4 4 0 - 4 l - 7 • ^ 4 4 0 - 7 0 - , : ' -'z.u.i3-':i.?-Z- : ^ 4 4 0 - 4 3 - 4 7443-0^0-3 7439-3-^-.-. 743^^-92-1 74 ;,-^-'35-4 - ' ^ . 3 ^ - ^ 6 - 5 7 4 3 9 - Q 7 - 6 7 4 4 0 - 0 2 - 0 7 4 4 0 - 0 9 - 7 7 7 3 2 - 4 9 - 2 7<ii40-22-4 7 4 4 0 - 2 3 - 5 7 4 4 J K 2 8 - 0 7 4 ^ _ 6 2 - 2 7 4 4 f c - 6 6 - 6 o l o r B e f o r e : GREY o l o r A f t e r : GREY jmmenfcs ; STONES, ROOTS An^l-,-'- ' A lurn-. r;:.;,T. : ,Ar-;t iMV,:'r.y : Ar-5'=.;nic ' Sa.f-irjm 1 B e r / 1 1,: ijin ' C3dmi'.:,7-. Caio.v.ifT Chro:;;iuir. '. Cobalt CoDcer 1 Iron 1 Lead Magnes iumi ' Mangane.se ; Mercury : Nickel : PotassiLi.-n '. Selenium ' Silver '- Sodium Thallium 1 Vanadium 1 Zinc : Cyanide 1 . 2 7 '. IJ '. IJ I loo. r-^r:'-. - ,~ r 15 700 4. --> 90 0 0 45600 1 o 14 46 25700 15. 7660 •354. 0. 10 1300 0. 0 ^ , • ' - , ' 0 32 53 . •:'!-] 00 oO 00 30 27 27 00 70 70 40 00 10 1 00 00 12 30 00 OQ 54 00 74 40 90 Clarity Before Clarity After: BTjN T u; J' a I u: • J h p p CV p p p' NR T e x t u r e : MEDIiJf^ A r t i f a c t s : YES 100666 'ORM I IN i / 9 0 r \ \ D r >A SAMPL-I 5ntr.3ticr Units fug/L or mg/Kg dry weight!: MG/KG m CAI No. Color Before: SROUIN Color After: BROWN mments: Analyte Aluminum ,Ant imony Arsenic Barium Beryllium Cadmium ' Calcium Chromium Cobalt Copper Iron 1 Lead 1 Magnesium' Manganese 1 Mercury 1 Nickel Potassium' Selenium ' Silver Sodium Thallium Vanadium Zinc Cyanide Concentration 32400, 4, 3. 115. 0, 0. 74900, 16, 23. 60. 35300. 7. 10900. 1320. 0. 13, 1490, 0, 1640. 0. 62. 73. 00 30 20 00 25 25 00 30 70 50 00 50 00 00 14 60 00 51 00 30 10 50 Clarity Before; Clarity After: B U U Texture: FINE. Artifacts:.' 100667 c^nPNi T :=A ^3t•r 'A '-.Af 'jn: • ^ r , or nV:g/K',g dry weight KG CAS No. 7/^2^-90-5 •^440-36-0 •^440-33-2 7440-39-3 7440-41-7 7440-41-7 7440-70-2 •^440-47-3 7443-43-4 7440-50-3 74 39-39-6 7439_;32-l 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-7 7782-49-2 7440-22-4 7448-23-5 74^£a-2a-0 76.0-ti2-2 744a-66-6 Analyte Aluminum .•^nt imony Arsenic Barium Bery11ium Cadmium Calcium Chromium Cobalt Cooper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc Cyanide Concentration 30400.00 6.70 4. 10 111.00 0. 35 0. 32 79900.00 17. 60 24.80 62.00 39200.00 7. 50 11800.00 1400.00 0. 15 14. 60 1500.00 1.30 0. 64 1530.00 1.00 63. 20 82.30 C 1 Q Br^N ^ N 8 1 Ul \T- Ul X B: u rjNW U 1 B ^ u: 15N M 1 P 1 P 1 F 1 p ; p 1 p 1 P ! O 1 p 1 p 1 p : F 1 D 1 P 1 CVI p 1 p ; p I p : p 1 F ; p 1 p 1 NR 1 Color Before: BROWN Color After: BROWN (mments : ROOTS Clarity Before: Clarity After Texture: FINE Artifacts: 'YES " 0(100^ 100668 ;'U • i t r a t i o n '3/L '.ir-/ w e i ' 5 h t 1 : MG/KG CAS r 7429- 7440- 7440- 7440- 7440- 7440 7440- 7440- 7440 7440- 7439- 7439- 7439- 7439- 7439- 7440- 7440- 7732- 7440- ^ ^ ^ y i i m t 749 7 4 ^ Jo. -90- -36- -38- -39- -41- -41- -70- -47- -43- -50- -39- -92- -95- -96- -97- -02- -09- -49- -22- -23- -28- »«2- *66- -5 -0 -2 . -!• -7 -7 -2 -3 -4 -S -6 -1 -4 -5 -6 -0 -7 -2 -4 -5 -0 -2 -6 Analyte Aluminum Art irncioy Arsenic Barium Bery11ium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc Cyanide Concentrat ion 33600. 5 . -», 122. 0. 0. 32100. 16. 25. 64. 38400. 7. 11800. 1430. 0. 15. 1600. 1 . 0. I 7^50. 0, 64. 79, 00 00 60 00 29 29 00 80 40 30 00 30 00 00 12 20 00 20 59 30 87 30 90 :olor Before: BROWN :oior After: BROWN knments r ROOTS Clarity Before: Clarity After: U U M F~ P F P P P P P P P P tr I p p CV p F P P F P P NR T e x t u r e . : ' F I N E A r t i f a c t s : YES •ss^ 100669 FORM I - I N ; / 9 0 IPA IN 0 P G -^ ^ I : ,'- ^, -. i .. t -A -AilF' :AS N O . 7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-41-7 7440-70-2 7440-47-3 7440-43-4 7440-50-8 7439-39-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-7 7782-49-2 7440-22-4 7 4 4 ^ 2 3 - 5 7 4 ^ ^ 2 8 - 0 74jKrJ66-6 Color Before: BROWN Color After: BROWN Ipmments; STONES, ROOTS f . or •'-?/',<• ;ai9ht!: MG/KG Ana L Vte Aluminum Ant imony Arsenic Bar i',:m Bery11ium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magne.sium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc Cyanide Concentrat ior, 9400 26 8 48 0 0 51200 57 13 367 183000 466 4740 925 0 47 495 0 0 314 0 2 1500 00 60 00 60 23 23 00 60 30 00 00 00 00 00 11 80 00 87 46 00 65 20 , 00 Clarity Before Clarity After: M P P F P P P P P P P P F P P CV P P F P P F P P NR Texture: MEDIUM Artifacts: YES sm^^ FORM I IN 100670 3 / 9 0 1." .'^ - CLP T M n p 0, '.. M 'A -A f:i9/L ;/K-a dry :hfc ;1G/KG :AS No. Color Before: BROWN Color After: BROWN ^mments: STONES, ROOTS Analyte Aluminum Ant imony Arsenic Barium Eery 11ium Cadmium Calcium Ch."omium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thai1ium Vanadium Zinc Cyanide Concentration 10600. 15. 5. 95. 0. 4. 42100. 110. 17. 109. 121000. 137. 5000. 1420. 0. 49. 659. 1 , 0. 361 . 0. 14. 1710. 00 50 50 60 30 50 00 00 30 00 00 00 00 00 15 60 00 20 60 00 39 30 00 Clarity Before; Clarity After: U 1 • ^ * Texture: " MEDIUM Artifacts:"YES. FORM I IN 100671 3/90 E P .A - C L ? T M p p ;-. ,,*\' d 'r. : I Jit ? Concentr,3t ion Units Cug/L or mg/Kg dry weight!: MG/KG , # " ' ', CAS No. 17429-90-5 ; 7440-36-0 ;7440-33-2 17440-39-3 ;7440-41-7 17440-41-7 ;7440-70-2 :7440-47-3 1 7440-43-4 17440-50-8 17439-89-6 17439-92-1 :7439-95-4 1 7439-96-5 ',7439-97-6 1 7440-02-0 17440-09-7 17782-49-2 !7440-22-4 1 7/| itt23-5 1 '7^9R'2S'-0 ' '^^^^t^^"'^ ! 74l^e6-6 Analyte Aluminum Ant imony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Cooper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc Cyanide Concentration 1C1 0 13600.00 1 1 3. 90 IU IJT^I 1. 101BtTNW 103.001 1 0.23 1U1 0.231UI 69300.00 1 1 19.601 IX 13.40 1 y 58.701 1 21500.00 1 1 9.001 1 7630.00 1 1 735.00 1 1 0ji ^ e. iiL,"D: dld^i ' 10.70 1 ij- 2170.001 1 0. 91 IU a'NW 0.461UT 333.00 1 B ^ 0.6SIUI 74.701 1 142.001 I^N 1 1 M 1 P 1 P 1 F 1 P 1 P I P I P 1 P 1 P 1 P 1 P 1 F 1 P 1 P 1 CVI P 1 P 1 F 1 P 1 p : F 1 p 1 p 1 NR 1 Color Before: BROWN Color After: BROWN iments r STONES, ROOTS Clarity Before: Clarity After: Texture I MEDIUM Artifacts: YES Q^iieo# 100672 FORM I - IN ;/90 oP,^ - ,^fc z 3ht nG/KG 0 n r CAS No. ^429-^0--- 7A40-36-0 7440-33-2 "'440-39-3 7440-41-7 7440-4 1 -7 7440-70-2 7440-47-,!. 744 0-43-4 7440-50-3 7439-8='-6 "'439-'?2-l 7439-95-4 7139-06-5 7439-97-6 7440-02-0 7440-09-7 7732-49-2 7440-22-4 7440-23-5 7440-28-0 74^»-62-2 7448-66-6 Ana 1yte Aluminum Ar'i t i ;nO'ny Ar.seni •:; Barium Bery11ium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thai!ium Vanadium Zinc Cyanide Concentrat i on 21700.00 4 . 00 7. 60 135.00 0. 24 0. 24 23300.00 27.90 21. 10 99. 60 44100.00 35.30 7600.00 1050.00 0. 10 13. 30 2990.00 0. 90 0. 47 321.00 0. 67 97. 20 337.00 c; Q UlT^i irN U' Ul ^ 1 w U 1 ? U I^'NW Ul BiT U 1 : = ^ M 1 p 1 p 1 c ' p 1 p ' p 1 p 1 p 1 p 1 p 1 p 1 F 1 p 1 p : CV 1 p 1 p 1 F 1 p ; P ! p ' O 1 p 1 NR 1 Color Before: BROWN rolor After: BROWN iment s : ROOTS. STONES Clarity Before: Clarity After: Texture: MEDIUM Artifacts: YES 100673 FORM I IN 3 / 9 0 fug/L or mg/Kg weight): MG/KG - k ^ F olor Before: F olor After: E kmments r r ROOTS CAS No, T.ii29-90-5 "'440-36-0 7440-33-2 •'440-;,o_.3 7440-4 1-7 7440-4 1-7 7440-70-2 74.40-47-,3 7440-43-4 7440-50-3 7439-39-6 7439-^2-1 7439-05-4 7439-96-5 7439-97-6 7440-02-0 7440-09-7 7732-49-2 7440-22-4 7440-23-5 7<i4JP-28-0 7 4 ^ 6 2 - 2 744»-66-6 5R0WN 5R0WN Analyte Alumintim Ant imony Arsenic Barium Bery1lium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thai 1ium Vanadium Zinc Cyanide Clarit Claril Concentrat ion 21000.00 9. 20 9. 10 196.00 0. 24 0.24 43100.00 49. 00 22.30 73. 70 31700.00 322.00 7420.00 987.00 0. 11 33.50 2920.00 0. 97 0. 49 639.00 0. 73 63. 50 362.00 C B i„J U U u IJ B U 0 jN ^N r 3 f a T ;^NW f '^N ;y Before: :y After: M 0 P F P P P P P p P P p P P CV P P F P P F P P NR ,i r i Texture: • •. MEDIUM • Artifacjts: YES 100674 00000^ FORM I - IN 3/90 =.^ ]- N1 r^ p i' d / •- wei',3ht ! ; m 4::9-90-5 440-36-0 440-33-2 7^^40-39-3 -440-41-7 440-41-7 4 4 0-70-2 440-47-3 4 40-43-4 440-50-3 7439-39-6 7439-'-a2-l 7439-95-4 :"439-=>6-5 7439_g7_6 7440-02-0 7440-09-7 7732-49-2 7440-22-4 7440-23-5 7449-28-0 74«p-62-2 744*-66-6 ."olor Before: BROWN ::olor After: BROWN ment.s ; STONES. ROOTS ,An.alyte I Concentrat ion I C A i -..ur] i rum Ant imony .Ar senic Barium Beryl 1ium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thai1ium Vanadium Zinc Cyanide l'^200. 119 0 0 13000 20 19 43 25300 9 5160 1070 0 10 2500 0 0 0 34 44 00 50 90 00 21 21 00 00 50 70 00 g0 00 00 10 30 00 36 42 00 65 90 30 Clarity Before: Clarity After: U U U B' IJ P P C P o P p p p p p p p CV p p o F P P NR Texture: MEDIUM Artifacts: YES 100675 FORM I - I N i/90 U.S. EPA - CLP 1 INORGANIC ANALYSIS OA~A -HF 'A T.AMPLE N'-' ,in 1 weight 'd/L CAS No. 7429 7440 7440 7440 7440 7440 7440 7440 7440 7440 7439 7439 7439 7439 7439 7440 7440 7782 7440 7440 7440 744ft-: 7 4 j i ^ 90-5 36-0 38-2 39-3 41-7 41-7 70-2 47-3 43-4 50-3 89-6 92-1 95-4 96-5 97-6 02-0 09-7 49-2 22-4 23-5 28-0 62-2 66-6 € Color Before: COLORLESS Color After: COLORLESS omments: Ana A luminum Ant imony Arsenic Barium Bery11ium Cadmium Ca Icium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thailium Vanadium Zinc Cyanide Clarity Before: CLEAR Clarity After: CLEAR Texture: Artifacts: ' 100676 ..A.. oodoo*^ FORM I IN 3 / 9 0 U.S. EPA - CLP INORGANIC ANALYSIS DATA SHEET .EPA SAMPLE NO. •-J ,_ :3 ivi ; - {-^ ... -^ -I ,• > o i t;- :5 r •;, Nc i / K g d r y w e i g h t ! iG/L 7 4 2 9 - 9 0 - 5 7 4 4 0 - 3 6 - 0 7 4 4 0 - 3 8 - 2 7 4 4 0 - 3 9 - 3 7 4 4 0 - 4 1 - 7 7 4 4 0 - 4 1 - 7 7 4 4 0 - 7 0 - 2 7 4 4 0 - 4 7 - 3 7 4 4 0 - 4 3 - 4 7 4 4 0 - 5 0 - 8 7 4 3 9 - 8 9 - 6 7 4 3 9 - 9 2 - 1 7 4 3 9 - 9 5 - 4 7 4 3 9 - 9 6 - 5 7 4 3 9 - 9 7 - 6 7 4 4 0 - 0 2 - 0 7 4 4 0 - 0 9 - 7 7 7 3 2 - 4 9 - 2 7 4 4 0 - 2 2 - 4 7 4 4 0 - 2 3 - 5 7 4 4 » - 2 8 - 0 7 4 W P 6 6 - 6 # Color Before: COLORLESS Color After: COLORLESS omments; Analyte Aluminum Ant imony Arsenic Barium 1 Beryl1ium Cadmium Calcium Chromium J Cobalt Copper Iron Lead Magnesium Manganese. Mercury Nickel 1 Potassium 1 Selenium 1 Silver 1 Sodium 1 Thallium 1 Vanadium 1 Zinc 1 Cyanide I Concentration IC 51. 14, 2, 2. 1, 3, 84, 4, 4, 2, 47. 2, 77. 1, 0, 4. 268. 4. 2. 85. 3. 2. 19. 20 00 00 00 00 00 40 00 1 00 00 10 30 50 00 26 00 00 00 00 20 00 00 90 ^ ' U B uj7" Ul B I T ujjnsj Ul Bl Clarity Before: CLEAR Clarity After: CLEAR M P~ P F P P P P P P P P F P P CV P P F P P F P P NR Texture: Artif.acts: 100677 ^ s ^ H B B ^ FORM I - IN 3 / 9 0 ATTACHMENT 1 SOP NQ. HW-6 PAGE _or TOTAL REVIEW CLP DATA ASSESSMENT Functional Guidelines for Evaluating Organics Anaiysis Case No. I O / C Q SDG No.i^TriX)! LABORATORY r\yi jh}J SITE I / T L M ^ * ^ - ^ -DTKITK ASSESSMENT; . ] ^ \ 6.O.W. Documcn4 ^ 0 L m o \ . O CRecldL/qq) The ourront igunotional guidelines (1006) for evaluating organic data have been applied. All data are valid and acceptalile except those analytes which have been qualified with a "J" (estimated), "U" (non-detecqj), "R" (unusable),or "JN" (presumptive evidence for the presence 'of the material at an estimated value). All action is detailed on the attached sheets. Two facts should be noted by all data users. First, the "R" flag means that the associated value is unusable. In other words, due to significant QC problems the analysis is invalid and provides no information as to whether the compound is present or not. "R" values should not appear on data tables because they cannot be relied upon, even as a last resort. The second fact to keep in mind is that no compound concentration, even if it has passed all QC tests, is guaranteed to be accurate. Strict QC serves to increase confidence in data but any value potentially contains error. si^SSix ^:~P^^yy^^ ^^"^^-j^^yu^—Date -Lt/y^^l/ verified Bv: ^ . ^ . . . ^ ^-yi/J^^J DatetO?-/ l9 /19 ?J. 100678 ATTACHMEE3T 1 PAGE OF SOP NO. HM-6 DATA ASSESSMENT: 1. HOLDING TIME: The amount of an analyte in a sample can change with time due to chemical Instability, degradation, volatilization, etc. If the specified holding time is exceeded, the data may not be valid. Those analytes detected in the samples whose holding time has been exceeded will be qualified as estimated, "J". The non-detects (sample quantitation limits) will be flagged as estimated, "J", or unusable, "R", if the holding times are grossly exceeded. The following action was taJcen in the samples and analytes shown due to excessive holding time. ^c/lOa^Lu ijLMMjisljLi IJUifi, (^ ^-dfuj ckixiJUUi'-f7^mL (^\A^LnV^crash ^kud UZUAJL t ^ ^A^riAMy)Z^ ^^^t^'^^''>;?w^:^ A^\^^yY^i,vZ^)^tXJuyMJi^ l&trC6002. 04,DL, I^Hi'^'^i'O, /^/Z;;3,)Y,/r;/(.,/7,33jOS ZO$u - ftC-L 1S,U3^ ou-ail^iid ^yyinjCbclCzj), 100679 PAGE OF ATTACHMENT 1 SOP NO. HW-6 DATA ASSESSMENT: 2. BLANK CONTAMINATION: Quality assurance (QA) blanks, i.e., method, trip field, rinse and water blanks are prepared to identify any contamination which may have been introduced into the samples during sample preparation or field activity. Method blanks measure laboratory contamination. Trip blanks measure cross-contamination of samples during shipment. Field blanks measure cross- contamination of samples during field operations. If the concentration of the analyte is less than 5 times the blank contaminant level (10 times for the common contaminants), the analytes are qualified as non- detects, "U". The following analytes in the samples shown were qualified with "U" for these reasons: A) Method blank contamination , , i '/I ,. ' ?• A/C-i ?iLi)2.,/!)3,^/. ov.o^oqwo,i/,ii,i3|iHyi%iU)n,i'5. ^ , . , . y ^ ^(Xtyzh)ui_ •,j.)tyy>Cj^y.uU^zdn>^^:h^^ F>^L VijldjPjJZj3,0^^1^^ I^H, L5 B) Field 'or rinse blank contamination ("water blanks" or "distilled water blanks" are validated like any other sample) C) Trip blank contamination 100680 0 O ^ Jl.oJzy dTimiD^L is. lATJyj^. diedJ/AL. 100681 PAGE OF ATTACHMENT 1 SOP NO. HW-6 DATA ASSESSMENT: 3. MASS SPECTROMETER TUNING: Tuning and performance criteria are established to ensure adequate mass resolution, proper identification of compounds, and to some degree, sufficient instrximent sensitivity. These criteria are not sample specific. Instrument performance is determined using standard materials. Therefore, these criteria should be met in all circumstances. The tuning standard for volatile organics is bromofluorobenzene (BFB) and for semi-volatiles is decafluorotriphenyl- phosphine (DFTPP). If the mass calibration is in error, all associated data will be classified/ as unusable, "R". .-> , »« TB^Ldi^)>'^)i 100682 ATTACHMENT 1 PAGE OF SOP NO. HW-6 DATA ASSESSMENT: 4. CALIBRATION: Satisfactory instrument calibration is established to ensure that the instrument is capable of producing acceptable quantitative data. An initial calibration demonstrates that the instrument is capable of giving acceptable performance at the beginning of an experimental sequence. The continuing calibration checks document that the instrument is giving satisfactory daily performance. A) RESPONSE FACTOR: The response factor measures the instrument's response to specific chemical compotinds. The response factor ?P&t^^o'^fl?®^ compound List (TCL) mustAb^Tl^ T'p'&T^t^^^^V^He init^ial and continuing calibrations. A value '^'Sfesffii' \nilicates a sprious detection and quantitation problem (poor sensitivity). AMlytes detected in the sample will be qualified as estimated, "J".• All non-detects for that compound will be rtjietti ("P"). Jl)^^'^^ 100683 ATTACHMENT 1 SOP NO. HW-6 PAGE OF DATA ASSESSMENT: CALIBRATION: A) PERCENT RELATIVE STAND?JRD DEVIATION (%RSD) AND PERCENT DIFFERENCE (%D): Percent RSD is calculated from the initial calibration and is used to indicate the stability of the specific compound response factor over increasing concentration. Percent D compares the response factor of the continuing calibration check to the mean response factor (RRF) from the initial calibration. Percent D is a me^ure of the instrument's daily perfonnance. Percent RSD must be <^»^aid %D must be <25%. A value outside of these limits indicates potential detection and quantitation errors. For these reasons, all positive results are flagged asj.estimated, "J" and non-detects are flagged "UJ" (if %D or RSD >»«%). If the»B is a gross deviation of %RSD and %D, the non-detects may be rejected ("R"). >.For the'^B/P'fes:^CIDE f s ^ z i o r T , and^i4vbutylcni<irendai5.e must T I ^ exc ^>ij^in i5% on tnfe quantitation column colbmn. 100684 ATTACHMENT SOP NO. HW-6 PAGE OF DATA ASSESSMENT: 5. SURROGATES: All samples are spiked with preparation to evaluate '^"•'= effici to sample rmance and ith surrogate compounds prior preparation to evaluate overall laboratory perforin efficiency of the analytical technique. If the measured surrogate concentrations were outside contract specifications, qualifications were applied to the samples and analytes as shown below. - . n, cio ^ iu.ie KiaZ^ys ^ ^ y . , n 'FJ^./f/\'/Z^/K£^ O I ' y^ 10 Po^^^^"^^*^ ^ ^ • ,-tL i>eLOMM\ Lor 0^^^^ . _^ . -yM^-^"^yZi'yyi^yrt^ ^ C v x > ^ ^ vjso^ Q r T i yt i \ L A X J ^ rZlySJLAJ' 1 A 0 l ^ ~i ' ^ • / - r T ' K i i ^ 100685 ATTACHMENT 1 PAGE_OF SOP NQ. HW-6 DATA ASSESSMENT: 7. INTERNAL STANDARDS PERFORMANCE: Internal standard (IS) performance criteria ensure that the GC/MS sensitivity and response are stable during every experimental run. The internal standard area count must not vary by more than a. factor of 2 (-50% to +100%) from the associated continuing calibration standard. The retention time of the internal standard must not vary more than +30 seconds from the associated continuing calibration standard. If the area count is outside the (-50% to + 100%) range of the associated standard, all of the positive results for compounds quantitated using that IS are qualified as estimated, "J", and all non-detects as "UJ", or "R" if there is a severe loss of sensitivity. If an internal standard retention time varies by more tjian 30 seconds, the reviewer will use professional judgment to determine either partial or total rejection of the data for that sample 100686 ATTACHMENT 1 PAGE OF SOP NO. HW-6 DATA ASSESSMENT: 8. COMPOUND IDENTIFICATION: A) VOLATILE AND SEMI-VOLATILE FRACTIONS: TCL compounds are identified on the GC/MS by using the analyte's relative retention time (RRT) and by comparison to the ion spectra obtained from )cnown standards. For the results to be a positive hit, the sample peak must be within + 0.06 RRT units of the standard compound and have an ion spectra which has a ratio of the primary and secondary m/e intensities within 20% of that in the standard compound. For the tentatively identified compounds (TIC) the ion spectra must match accurately. In the cases where there is not an adequate ion spectrum match, the laboratory may have provided false positive identifications. B) PESTICIDE FRACTION: The retention times of reported compounds must fall within the calculated retention time windows for the two chromatographic columns and a GC/MS confirmation is required if the concentration exceeds 10 ng/mi in the final sample extract. M 100687 ATTACHMENT 1 PAGE_OF SOP NO« HW-6 DATA ASSESSMENT: 9. MATRIX SPIKE/SPIKE DUPLICATE, MS/MSD: The MS/MSD data are generated to determine the long-term precision and accuracy of the analytical method in various matrices. The MS/MSD may be used in conjunction with other QC criteria for some additional qualification of the data. p^^ ms i rosb Jhuj 4ny ^ v n - \ ^ ( L ^ ^ ^ ^ ^ ' - ^ ' ^ ^ 'i+Kji>jL^tU-FAy^ f, / f 100688 PAGE OF DATA ASSESSMENT: 10. OTHER QC DATA OUT OF SPECIFICATION: 11. SYSTEM PERFORMANCE AND OVERALL ASSESSMENT (continued Ol^next page if necessary): 12. CONTRACT PROBLZWS NOM-COHPLIAHCE: n / /i i . ^i * J - — 1 J. I ^ H H B M ^ contains re-extra Factlfte, re-analysis or n reviewing the QA results, tne following form :if ied to be used. W -y7Ln^ta.nZl t^Llb^Luo'dASf-'MJiJcluJiZiaAU 'UL^ Ah^ ts^j^ fi*^nz/ioJ>^ P ^ y y ^ ^ \^\Ah l)jMJi\<^^ )--LilJT)yLijiy>ayxi ir(du/yjJli^^'^f^'^-^ 100689 ATTACHMENT 1 PAGE OF SOP NO. HW-6 ~ DATA ASSESSMENT: 1 1 . SYSTEM PERFORMANCE AND OVERALL ASSESSMENT ( c o n t i n u e d ) : ^ 1 0 0 6 9 0 c3 non &yy^hlLnC^ (^CbO^n CI\JICJL\ \J)aJl ^^^XJ^ '^Uuii'\y? C^'llf^ I ij^^^ ^DdJjyULE} ITZUAUL (L&\yiZ7yzlz^ <i h n ^y,_yLj/.mxii^^: luMJL y^JLyCj-y^a/u_. y'm^.'-ty • 100691 i>roJcct: V X - C K j ) n \ ' ( c o j ) >A,.< « « ' >%«»>« ^ m i m g w d i e * r i iMto: ltcvle«er*e IwltUlet - y { \ l i l l i tlBee!LS)rW)/;L->vXp^i^ Ni««>er of 5i-.«i«,^9 f ^ / " 7 / ^ n f ^ ^ j p c j Atialf tee HelccUil ime to facewllwe He»lw» CrticrU; Swrrcaates itelds (m> liOLiOOL loiiWL lOM (I) iSi 50/) mtmmm^imammmmatt ttllbnitlBw ^l5 \«*^l>j^ f iNllM 11 a an| 2:y^ tMtlcM ^ ) ^ n % Mil nil) OUMMT TniUl f ftewplee j ^ JH J 2 n •teUI I Iff « l l 1—1» ii 1 ^ 1 Z)^"^ .0 r.v/ 4Z. -TD ^ ^ ^ii,^ / J 1 1 itoielf tee Esiliwiinl lnw to facewUsK Itewrlce Criteria for: Achin nn) iVN (COy »0» <»>•• I'EOT caoi !SLm_ TOltMn tU**' u -a . ^ £Z £ 2 ^ ^v^ / -^^ S 7 3 I ? > ^ 3 5 - / / . ^ < ,^^(^ /v5vn / ^ g ^ / ^ > ' ^ 100692 IA VOLATILE ORGANICS ANALYSIS DATA SHEET # Name: roMPTTCHat.ypp ,ab Code: COMPU Case No.: 15933 EPA SAMPLE NO. BGLOl Contract: 68D00159 SAS No.: SDG No.: BGLOl "Matrix: (soil/water) WATER oample wt/vol: 5.0 (g/mL) ML ivel: (low/med) LOW % Moisture: not dec. : '• Column: DB-6^4 ID: 0.530 (mm) Soil Extract Volume: (uL) 402859 CAS NO. COMPOUND Lab Sample ID Lab File ID: CN002859A53 Date Received: 03/04/91 Date Analyzed: 03/07/91 Dilution Factor: 1,0 Soil Aliquot Volume: (uL) CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q i w M i 74-87-3 Chloromethane 74-83-9 Bromomethane 75-01-4 Vinvl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1,1-Dichloroethene 75-34-3 1, l-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform 107-06-2 1,2-Dichloroethane 78-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 75-27-4 Bromodichloromethane 78-87-5 1,2-Dichloropropane 10061-01-5 cis-1,3-Dichloropropene 79-01-6 Trichloroethene 124-48-1 Dibromochloromethane 79-00-5 —1,1,2-Trichloroethane 71-43-2 —Benzene 10061-02-6 —Trans-l,3-Dichloropropene 75-25-2 Bromoform 108-10-1 4-Methvl-2-Pentanone 591-78-6 --2-Hexanone 127-18-4 Tetrachloroethene 79-34-5 1,1,2.2-Tetraehloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene 1^00-41-4 Ethylbenzene •100-42-5 Styrene 1330-20-7 Xylene (total) 10 10 10 10 10 10 10 10 31 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 U U U U u u u u u u u u u u u u u u u u u u u D u u u u u u FORM I VOA 1 0 0 6 9 3 3/90 y r^T"- / IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS EPA SAMPLE NO. BGLOl Name: COWP^CHHIiRTP Contract: 68D00159 Lab Code: COMPU Case No.: 15933 SAS No.: SEX3 No.: BGLOl Matrix: (soil/water) WATER Sample wt/vol: 5.0 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. GC Column: DB-624 ID: 0.530 (mm) Soil Extract Volume: (uL) Number TICs found: Lab Sample ID: 402859 Lab File ID: CN002859A53 Date Received: 03/04/91 Date Analyzed: 03/07/91 Dilution Factor: 1.0 Soil Aliquot Volxome: (uL) CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L I CAS NUMBER COMPOUND NAME RT EST. CONC, 100694 FORM I VOA-TIC 3/90 IA VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. Name: rnf^^TrwTm-,MP Lc»b Code: COMPU Case No.: 15933 BGL02 Contract: 68D00159 SAS No.: SDG No.: BGLOl • trix: (soil/water) WATER Sample wt/vol: 5.0 (g/mL) ML [ vel: (low/med) LOW '; Moisture: not dec. ^ Column: DB-624 ID: 0.530 (mm) 5 il Extract Volume: (uL) CAS NO. COMPOUND Lab Sample ID: 402866 Lab File ID: CN002866A53 Date Received: 03/04/91 Date Analyzed: 03/07/91 Dilution Factor: 1.0 Soil Aliquot Volume: (uL) CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q 74-87-3 Chloromethane 74-83-9 Bromomethane 75-01-4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1,1-Dichloroethene 75-34-3 1, l-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform 107-06-2 1,2-Dichloroethane 78-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 75-27-4 Bromodichloromethane 78-87-5 1,2-Dichloropropane 10061-01-5 cis-1,3-Dichloropropene 79-01-6 Trichloroethene 124-48-1 Dibromochloromethane 79-00-5 ——1,1,2-Trichloroethane 71-43-2 -r*-B«nzene 10061-02-6——?—Trans-1,3-Dichloropropene 75-25-2 Bromoform 108-10-1 4-Methvl-2-Pentanone 591-78-6 2-Hexanone 127-18-4 Tetrachloroethene 79-34-5 1.1.2.2-Tetrachloroethene 108-88-3—• Toluene 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene 100-42-5 styrene 1330-20-7 Xylene (total) 10 10 10 10 ' 10 10 10 10 10 12 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 u u u u u ^ u u u u u u u u u u u u u u u u u u u u u u u u u u FORM I VOA 100695 3/90 IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS me: COMPUCHEM.RTP Code: COMPU Case No.: 15933 •ix: (soil/water) WATER iple wt/vol: 5.0 (g/mL) ML tl: (low/med) LOW loisture: not dec. lolumn: DB-624 ID: 0.53 0 (mm) '' Extract Volume: (uL) EPA SAMPLE NO. BGL02 Contract: 68D00159 SAS No.: SDG No.: BGLOl Lab Sample ID: 402866 Lab File ID: CN002866A53 Date Received: 03/04/91 Date Analyzed: 03/07/91 Dilution Factor: 1.0 imber TICs found: Soil Aliquot Volume: CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L .(viL) CAS NUMBER COMPOUND NAME RT EST. CONC. Q - i FORM I VOA-TIC 100696 3/90 IA VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. (Name: COMPUCHEM.IgP b Code: COMPU Case No.: 15933 BGL03 Contract: 68D00159 SAS No.: SDG No.: BGLOl '='trix: (soil/water) WATER Sample wt/vol: 5.0 (g/mL) ML vel: (low/med) LOW Moisture: not dec. Column: DB-624 ID: 0.530 (mm) oil Extract Volume: (uL) CAS NO. COMPOUND Lab Sample ID: 402867 Lab File ID: CN002867A53 Date Received: 03/04/91 Date Analyzed: 03/07/91 Dilution Factor: 1. 0 Soil Aliquot Volume: (uL) CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q 74-87-3 74-83-9 75-01-4 75-00-3 75-09-2 67-64-1 75-15-0 75-35-4 75-34-3 540-59-0 67-66-3 107-06-2 78-93-3 71-55-6 56-23-5 75-27-4 78-87-5 10061-01-5- 79-01-6 124-48-1 79-00-5 71-43-2 10061-02-6- 75-25-2 108-10-1 591-78-6 127-18-4 79-34-5 108-88-3 108-90-7 100-41-4 100-42-5 1330-20-7— Chloromethane Bromomethane Vinyl Chloride, Chloroethane Methylene Chloride_ Acetone Carbon Disulfide 1,1-Dichloroethene 1,l-Dichloroethane 1,2-Dichloroethene (total) Chloroform 1,2-Dichloroethane_ 2-Butanone 1,1,l-Trichloroethane_ Carbon Tetrachloride_] Bromodichloromethane 1,2-Dichloropropane_ cis-1,3-Dichloropropene_ Trichloroethene —-—Dibromochloromethane •7^7-1,1,2-Trichloroethane_ "*--Benzene ••—*»-Trans-l, 3-Dichloropropene, -—Bromoform 4-Nethyl-2-Pentanone_ 2-Hexanona Tetrachloroethene •—^^-1,1,2,2-Tetrachl oroethane, Toluene Chlorobenzene, Ethylbenzene •'• Styrene, Xylene (total) FORM I VOA 100697 3/90 IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS EPA SAMPLE NO, BGL03 ^JP? Name: COMPUCHEM.RTP Contract: 68D00159 .ab Code: COMPU Case No.: 15933 SAS No.: ^______ SDG No.: BGLOl Matrix: (soil/water) WATER ...ample wt/vol: 5.0 (g/mL) ML evel: (low/med) LOW % Moisture: not dec. C Column: DB-624 ID: 0.530 (mm) Soil Extract Volume: (uL) Number TICs found: 0 Lab Sample ID: 402867 Lab File ID: CN002867A53 Date Received: 03/04/91 Date Analyzed: 03/07/91 Dilution Factor: 1.0 Soil Aliquot Volume: (uL) CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L CAS NUMBER COMPOUND NAME RT EST. CONC. FORM I VOA-TIC 100698 J/90 IA VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO, BGL04 Name: COMPUCHEM.jyp Contract: 68D00159 ab Code: COMPU Case No.: 15933 SAS No.: SDG No.: BGLOl ^'atrix: (soil/water) WATER Sample wt/vol: 5.0 (g/mL) ML evel: (low/med) LOW I Moisture: not dec. Z Column: DB-624 ID: 0.530 (mm) "oil Extract Volume: (uL) Lab Sample ID: 402868 Lab File ID: CN002868C53 Date Received: 03/04/91 Date Analyzed: 03/07/91 Dilution Factor: 1.0 CAS NO. COMPOUND Soil Aliquot Volume: CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L 74-87-3 74-83-9 75-01-4 75-00-3 75-09-2 67-64-1 75-15-0 75-35-4 75-34-3 540-59-0 67-66-3 107-06-2 78-93-3 71-55-6, 56-23-5 75-27-4 78-87-5 10061-01-5— 79-01-6 124-48-1 79-00-5 71-43-2 10061-02-6— 75-25-2 108-10-1 591-78-6 127-18-4 79-34-5 108-88-3 108-90-7 100-41-4 100-42-5 1330-20-7— —Chloromethane —Bromomethane — V i n y l Chloride, —Chloroethane —Methylene Chloride, —Acetone Carbon Disulfide —1,1-Dichloroethene —1,l-Dichloroethane —1,2-Dichloroethene (total) —Chloroform —1,2-Dichloroethane, —2-Butanone —1,1,1-Trichloroethane, —Carbon Tetrachloride_J —Bromodichloromethane_ —1,2-Dichloropropane, —cis-1,3-Dichloropropene_ —Trichloroethene Dibromochloromethane •1,1,2-Trichloroethane, inzene •^*"Trans-l, 3-Dichloropropene, •—Bromoform 4-Methyl-2-Pentanone, 2-Hexanone Tetrachloroethene 1,1,2,2-Tetrachloroethane_ Toluene Chlorobenzene, Ethylbenzene_ Styrene, Xylene (total) .(UL) FORM I VOA a IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS EPA SAMPLE NO, BGL04 Name: COMPUCHEK.RTP Contract: 68D00159 ab Code: COMPU Case No. : 15933 SAS No.: SDG No. : BGLOl latrix: (soil/water) WATER Sample wt/vol: 5.0 (g/mL) ML ^evel: (low/med) LOW % Moisture: not dec. ;c Column: DB-624 ID: 0.530 (mm) '"oil Extract Volume: (uL) Number TICs found: 0 Lab Sample ID: 402868 Lab File ID: CN002868C53 Date Received: 03/04/91 Date Analyzed: 03/07/91 Dilution Factor: 1.0 Soil Aliquot Volume: CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L .(UL) CAS NUMBER COMPOUND NAME RT EST. CONC. _J_ FORM I VOA-TIC 100700 3/90 IA VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. 'Name: roMPTTCWTtif.ffPP b Code: COMPU BGL05 Contract: 68D00159 Case No.: 15933 SAS No.: SDG No.: BGLOl ' trix: (soil/water) WATER Sample wt/vol: 5.0 (g/mL) ML - vel: (low/med) LOW \ Moisture: not dec. Column: DB-624 ID: 0.530 (mm) ^'•-il Extract Volume: (uL) Lab Sample ID: 402869 Lab File ID: CN002869C53 Date Received: 03/04/91 Date Analyzed: 03/07/91 Dilution Factor: 1.0 CAS NO. COMPOUND Soil Aliquot Volume: CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L .(UL) 74-87-3 74-83-9 75-01-4 75-00-3 75-09-2 67-64-1 75-15-0 75-35-4 75-34-3 540-59-0— 67-66-3 107-06-2 — 78-93-3 71-55-6 56-23-5 75-27-4 78-87-5 10061-01-5 79-01-6 124-48-1— 79-00-5 71-43-2 10061-02-6 75-25-2 108-10-1— 591-78-6— 127-18-4 — 79-34-5 108-88-3 — 108-90-7 — 100-41-4 — 100-42-5— 1330-20-7- -Chloromethane - Bromomethane -Vinyl Chloride, -Chloroethane -Methylene Chloride, -Acetone Carbon Disulfide -1,1-Dichloroethene -1,l-Dichloroethane -1,2-Dichloroethene (total) -Chloroform •1,2-Dichloroethane, •2-Butanone •1,1,l-Trichloroethane_ -Carbon Tetrachloride_ •Bromodichloromethane -1,2-Dichloropropane -cis-1,3-Dichloropropene_ -Trichloroethene ———Dibromochloromethane •1,1,2-Trichloroethane, "Benzene •Trans-1,3-Dichloropropene, -Bromoform • 4-Methyl-2-Pentanone, -2-Hexanone Tetrachloroethene -1,1,2,2-Tetrachloroethane_ -Toluene -Chlorobenzene, -Ethylbanzene_^ -Styrene, Xylene (total) FORM I VOA 100701 3/90 IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS EPA SAMPLE NO, BGL05 ^ P Name: COMPUCHEM^JgP Contract: 68D00159 ab Code: COMPU Case No.: 15933 SAS No.: SDG No.: BGLOl "atrix: (soil/water) WATER sample wt/vol: 5.0 (g/mL) ML 2vel: (low/med) LOW % Moisture: not dec. - Column: DB-624 ID: 0.530 (mm) .^^oil Extract Volume: (uL) Number TICs found: Q 402869 Lab Sample ID Lab File ID: CN002869C53 Date Received: 03/04/91 Date Analyzed: 03/07/91 Dilution Factor: 1.0 Soil Aliquot Volume: (uL) CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L CAS NUMBER COMPOUND NAME RT EST. CONC. A- FORM I VOA-TIC 100702 3/90 IA VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. ^ro BGL06 Name: rnMpTTP|f|g|^j^yp Contract: 68D00159 Lab Code: COMPU Case No.: 15933 SAS No.: SDG No.: BGLOl atrix: (soil/water) WATER Sample wt/vol: 5.0 (g/mL) ML evel: (low/med) LOW "' Moisture: not dec. GC Column: DB-624 ID; 0.530 (mm) oil Extract Volume: (uL) CAS NO. COMPOUND Lab Sample ID: 402870 Lab File ID: CN002870C53 Date Received: 03/04/91 Date Analyzed: 03/07/91 Dilution Factor: 1.0 Soil Aliquot Volume: (uL) CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q 74-87-3 Chloromethane 74-83-9 Bromomethane 75-01-4 Vinvl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1,1-Dichloroethene 75-34-3 1, l-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform 107-06-2 1.2-Dichloroethane 78-93-3 2-Butanone 71-55-6 1.1.1-Trichloroethane 56-23-5 Carbon Tetrachloride 75-27-4 Bromodichloromethane 78-87-5 1.2-Dichloropropane 10061-01-5 cis-1,3-Dichloropropene 79-01-6 Trichloroethene 124-48-1 -^-—Dibromochloromethane 79-00-5 *j—1,1,2-Trichloroethane 71-43-2 y' -Benzene 10061-02-6—-8^—Trans-1,3-Dichloropropene 75-25-2 Bromoform 108-10-1 4-Methyl-2-Pentanone 591-78-6 2-Hexanone 127-18-4 Tetrachloroethene 79-34-5 1,1.2,2-Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene 100-42-5 Styrene 1330-20-7 Xylene (total) 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u FORM I VOA 100703 3/90 ^ K > Ni IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS EPA SAMPLE NO. BGL06 Name: COMPUCHEM.RTP Contract: 68D00159 Lab Code: COMPU Case No.: 15933 SAS No.: ' SDG No.: BGLOl atrix: (soil/water) WATER Sample wt/vol: 5.0 (g/mL) ML ,evel: (low/med) LOW °' Moisture: not dec. 'ZC Column: DB-624 ID: 0.530 (mm) oil Extract Volume: (uL) Number TICs found: 0 Lab Sample ID: 402870 Lab File ID: CN002870C53 Date Received: 03/04/91 Date Analyzed: 03/07/91 Dilution Factor: 1. 0 Soil Aliquot Volume; CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L .(UL) CAS NUMBER COMPOUND NAME RT EST. CONC. FORM I VOA-TIC 1 0 0 7 0 4 3 / 9 0 IA VOIATIIM ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. " Name: C0MP€7CH«iaT*f* Contract: 68D00159 i.ab Code: COMPtJ Case No.: 1593!? SAS N o . : SDG BGL09 No.: BGL09 atrix: (soil/water) SOIL Lab Sample ID: 402874 Sample wt/vol: 5.0 (a/mL) G Lab File ID: GH002874A18 evel: (low/med) LOW Date Received: 03/04/91 3: Moisture: n o t dec. .2.7 Date Analyzed: 0i^0,8/.9.1 ^C Column: pB-624 ID: 0.530 (mm) Dilution Factor: l.Q 3il Extract Volume: _ . . . (uL) Soil Aliquot Volume: . ._(uL) CONCENTRATION UNITS: CAS N O . COMPOUND fua/L or ua/Ka) UG/KG 0 • • 74-87-3 Chloromethane 74-83 -9 Bromomethane 75-01-4 Vinyl Chloride 75-00-3 • Chloroethane 75-09-2 Methylene Chloride 6 7 - 6 4 -1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1,1-Dichloroethene 75-34-3 1. l-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform 107-06-2 1,2-Dichloroethane 78-93-3 2-Butanone 71-55-6 1,1.1-Trichloroethane 56-23-5 Carbon Tetrachloride 75-27 -4 Bromodichloromethane 78-87-5 1,2-Dichloropropane 10061-01-5 cis-l, 3-Dichloropropene 79-01-6 Trichloroethene 124-48 -1 •?»r-'Dibromochl oromethane 79-00-5 5 ^ ^ , 1.2-Trichloroethane ^ 71-43-2 wl'lenzene 10061-02-6— im"' Tians-1,3-Dichloropropene 75-25-2 Broaofora 108-10-1 4-Methvl-2-Pentanone 591-78-6 2-Hexanona___ 127-18-4 Tetrachloroethene 79-34-5 1,1,2,2-Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene 100-42-5 Styrene 1330-20-7 Xylene (total) FORM I VOA 14 14 14 14 72 58 14 14 14 14 14 14 14 14 14 14 14 14 14 14 14 14 14 14 14 14 14 14 14 14 14 14 14 100705 U at u u u u u u u u u u u u u u u D u u u u u u a u JJ u u 3i 4 1 1 * tm ^9Q ^ IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS EPA SAMPLE NO. Name: gOMPTTgffgif^^[TP _ab Code: COMPU Case N o . : 15933 i t r i x : ( s o i l / w a t e r ) SOIL Sample w t / v o l : 5.0 (g/mL) g ) jvel: (low/med) LOW % Moisture: not dec. 27 ; ; Column: DB-624 ID: 0.530 (mm) r dl Extract Volume: (uL) B6I.09 Contract: 68D00159 SAS No.: SDG No.: BGL09 Lab Sample ID: 402874 Lab File ID: GH002874A18 Date Received: 03/04/91 Date Analyzed: 03/08/91 Dilution Factor: 1.0 Mtunber TICs found: Soil Aliquot Volume: CONCENTRATION UNITS: (ug/L or ug/Kg) VG/KG .(UL) COMPOUND NAME LAB. ARTIFACT RT 3.85 EST. CONC. 14 ^ - ^ T » t . , ti;.- * •'•5 PORM I VOA-TIC 1 0 0 7 0 6 3/90 IA VOLATILI ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO; BGLIO ^ Name: COMPOCHEiri^iifc C o n t r a c t : 68D00159 .ab Code: COMPU Case No.: 15933 SAS No.: SDG No.: BGL09 i t r i x : (soil/water) SOIL sample wt/vol: 5.0 (g/mL) G ivel: (low/med) LOW Moisture: not dec. 33 sC Column: DB-624 ID: 0.530 (mm) )il Extract Volume: (uL) CAS NO. COMPOUND Lab Sample ID: 402881 Lab File ID: GH002881A18 Date Received: 03/04/91 Date Analyzed: 03/08/91 Dilution Factor: 1.0 Soil Aliquot Volume: (uL) CONCENTRATION UNITS: (ug/L or ug/Kg) HfiZKfi Q 74-87-3 Chloromethane 74-83 -9 Bromomethane 75-01-4 vinyl Chloride 75-00-3 Chloroetheme 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1.1-Dichloroethene 75-34-3 1, l-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform 107-06-2 1,2-Dichloroethane 78-93-3 2-Butanone 71-55-6 1.1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 75-27-4 Bromodichloromethane 78-87-5 1,2-Dichloropropane 10061-01-5 cis-l, 3-Dichloropropene 79-01-6 Trichloroethene 124-48-1 m.«" Pibroiaochloromethane 79-00-5 Jtfcil,!,2-Trichloroethane 71-43-2 -Vp^ivnzene 10061-02-6- W*»Trana-l, 3-Dichloropropene 75-2 5-2 Broeof o m 108-10-1 4-MethYl-2-Pentanone 591-78-6 2-Hexanone— 127-18-4 Tetrachloroethene 79-34-5 1.1,2,2-Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene 100-42-5- Styrene 1330-20-7 Xylene (total) 15 15 15 15 56 , 51 15 15 15 15 15 15 15 15 15 15 15 15 15 15 15 15 15 15 15 15 15 15 15 15 15 15 15 U u ?<^ u u u u u u D U U u u u u u u u D U U u u u « u n i FORM I VOA: 100707 3/S% IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS EPA SAMPLE NO. BGLIO I Name: SSXiSSSBnLMBt Contract: 68D00159 b Code: COMPU Case No.: 15933 SAS No.: SDG No.: BGL09 fltrix: (soil/water) SOIL v..j:iple wt/vol: 5.0 (g/mL) g rel: (low/med) LOW Moisture: not dec. 33 Column: PB-624 ID: 0,??9 (mm) >il Extract Volume: (uL) umber TICs found: 1 Lab Sample ID: 402881 Lab File ID: GH002881A18 Date Received: 03/04/91 Date Analyzed: 03/08/91 Dilution Factor: 1.0 Soil Aliquot Volume: (uL) CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG CAS NUMBER COMPOUND NAME LAB. ARTIFACT RT 3.83 EST. CONC. 19 ^ FORM I VOA-TIC 1 0 0 7 0 8 3/90 i IA VOLATIIA ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. i P a m e : coMPncmocMg' Contract: 68D00159 o Code: COMPU Case No.: 15933 SAS No.: SDG No.: BGL09 BGLII rix: (soil/water) SOIL raple wt/vol: 5.0 (g/mL) S el: (low/med) LOW Moisture: not dec. 43 Column: DB-624 ID: 0.530 (mm) 1 Extract Volume: (uL) CAS NO. COMPOUND Lab Seunple ID: 402882 Lab File ID: GH002882A18 Date Received: 03/04/91 Date Analyzed: 03/08/91 Dilution Factor: 1.0 Soil Aliquot Volume: (uL) CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG Q 74-87-3 74-83-9 75-01-4 75-00-3 •— 75-09-2 67-64-1 75-15-0—-— 75-35-4 75-34-3 540-59-0 67-66-3 107-06-2 78-93-3 71-55-6 56-23-5 75-27-4 78-87-5 10061-01-5— 79-01-6 124-48-1—— 79-00-5 71-43-2 10061-02-6— 75-25-2 108-10-1 591-78-6 127-18-4 79-34-5 108-88-3 108-90-7 100-41-4 100-42-5 1330-20-7 —Chloromethane —Bromomethane —Vinyl Chloride, —Chloroethane —Methylene Chloride, —Acetone ~ Carbon Disulfide —1,1-Dichloroethene —1,l-Dichloroethane —1,2-Dichloroethene (total). —Chloroform —1,2-Dichloroethane_ —2-Butanone —1,1,1-Tr ichloroethane, —Carbon Tetrachloride_[ —Bromodichloromethane_ —1,2-Dlchloropropane, —cis-l, 3-Dichloropropene, —Trichloroethene •Dibromochloromethane ^ - r 1,2-Trichloroethane, WlenTene Wtxans-l, 3-Dichloropropene_ -Broaofora —4 -Methyl-2 -Pent2Uione_ —2 -Hexsmone, ' Tetrachloroethene —1,1,2,2-Tetrachloroethane_ —Toluene —Chlorobenzene, —Ethylbenzene_j] —Styrene_ Xylene (total) FORM I VQA( 100709 3/90 IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS EPA SAMPLE NO. Name: SSSSSSSSSLXSt. _ab Code: COMPU Case No.: 15933 "'atrix: (soil/water) SOIL Sample wt/vol: 5.0 (g/mL) G 2vel: (low/med) LOW % Moisture: not dec. 43 : Column: DB-624 ID: 0.530 (mm) .^Til Extract Volume: (uL) B6L11 Contract: 68D00159 SAS No.: SDG No.: BGL09 Number TICs found: Lab Sample ID: 402882 Lab File ID: GH002882A18 Date Received: 03/04/91 Date Analyzed: 03/08/91 Dilution Factor: 1.0 Soil Aliquot Voliune: (uL) CONCENTRATION UNITS: (ug/L or ug/Kg) JIS/Kfi CAS NUMBER 1. COMPOUND NAME LAB. ARTIFACT RT 3.85 EST. COMC. 25 FORM I VOA-TIC 5 , 100710 3/90 LA VOLATILI ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. fpiame: coMPnrm^.^y 3 Code: COMPU Case No.: 15933 BGL12 Contract: 68D00159 SAS No.: SDG No.: BGL09 :rix: (soil/water) SOIL imple wt/vol: 5.0 (g/mL) g 'el: (low/med) LOW Moisture: not dec. 34 Column: DB-624 ID: 0.530 (mm) -1 Extract Volume: (uL) Lab Sample ID: 402883 Lab File ID: GH002883A18 Date Received: 03/04/91 Date Analyzed: 03/08/91 Dilution Factor: 1.0 CAS NO. COMPOUND Soil Aliquot Volxime: CONCENTRATION UNITS: (ug/L or ug/Kg) VG/KG .(UL) 74-87-3 Chloromethane 74-83 -9 Bromomethane 75-01-4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1.1-Dichloroethene 75-34-3 1. l-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chlorofora 107-06-2 1.2-Dichloroethane 78-93-3 2-Butanone 71-55-6 1.1.1-Trichloroethane 56-23-5 Carbon Tetrachloride 75-27-4 BroBodichloroaethane 78-87-5 1.2-Dichloropropane 10061-01-5 cis-1,3-Dichloropropene 79-01-6 Trichloroethene 124-48-1 --»4Mbroaochloromethane 79-00-5 jfct,!, 2-Trichloroethane 71-43-2 M i n i iene 10061-02-6 ^Sirens-l. 3-Dichloropropene 75-25-2 Broaofora 108-10-1 4-Methvl-2-Pentanone 591-78-6 2-Hexanone^ 127-18-4 Tetrachloroethene 79-34-5-, 1.1.2.2-Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene 1 100-41-4 Ethvlbenzcuie 1 100-42-5 Styrene 1330-20-7 Xylene (total) 15 15 15 15 68 55 ^ 15 15 15 15 15 15 15 15 15 15 15 15 15 15 15 15 15 15 15 15 15 15 15 IS 15 IS IS U u u u u u u u u u u u D u u D U U D U U U D U U U U n u 100711 FORM I VOA 3/90 / y W D Nam( IE VOLATIIl ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS EPA SANPLE NO. •};»v»i*:«- Name: ^tib Code: COMPU Case No.: 15933 ^ trix: (soil/water) SOIL Sample wt/vol: 5.0 (g/mL) fi '.I (/el: (low/med) LOW ; Moisture: not dec. 34 L Column: DB-624 ID: 0.53O (mm) c 1 Extract Volume: (uL) Ni"mber TICs foxind: 1 BGL12 Contract: 68D00159 SAS No.: SDG No.: BGL09 Lab Sample ID: 402883 Lab File ID: GH002883A18 Date Received: 03/04/91 Date Analyzed: 03/08/91 Dilution Factor: 1.0 Soil Aliquot Volume: (uL) CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG CAS NUMBER COMPOUND NAME LABORATORY ARTIFACT RT 3.82 EST. CONC. 15 : ^ i •J FORM I VOA-TIC I 100712 C d 3/«n VOIATZIB QBBARICS ANALYSIS DATA SHEET EPA SAMPLE NO. tl Name: COMPUCHEM.] o Code: COMPU Case No.: 15933 BGL17 contract: 68D00159 SAS No.: SDG No.: BGL09 :rix: (soil/water) SOIL imple wt/vol: 1.0 (g/mL) fi 'el: (low/med) LOW Moisture: not dec. 19 . Column: DB-624 ID: 0.530 (mm) 1 Extract Volume: (uL) CAS NO. COMPOUND Lab Sample ID: 4Q2888 Lab File ID: GR002888C18 Date Received: 03/04/91 Date Analyzed: 03/12/91 Dilution Factor: 1.0 Soil Aliquot Volume: (uL) CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG Q • • 74-87-3 Chloromethane 74-83 -9 Bromomethane 75-01-4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 carbon Disulfide 75-35-4 1.1-Dichloroethene 75-34-3 1, l-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chlorofora 107-06-2 l,2-Dichloroe(thane 78-93-3 2-Butanone 71-55-6 1,1,1-Tr ichloroethane 56-23-5 Carbon Tetrachloride 75-27-4 BroBodichloroaethane 78-87-5 1,2-Dichloropropane 10061-01-5 cis-1,3-Dichloropropene 79-01-6 --Trichloroethene 124-48-1 -ji^lbroaochloroaethane 79-00-5 "Vmr^^ 2-Trlchloroethane 71-43-2 —«|bksene 10061-02-6 •^Vmns-l. 3-Dichloropropene 7 5-2 5-2————laeoaof ora 108-10-1 4-l!ethyl-2-Pentanone 127-18-4 Tetrachloroethene 79-34-5 1,1,2,2-Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene 100-42-5 Styrene 1330-20-7 xylene (total) 62 62 62 62 240 J 180 ^ 62 62 62 62 62 62 85 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 9 6V 86 . <. U t U u U D U U U ' * _> " i ^ 1 ^ 1 ° D U D U U U U 0 a ii 0^ J FCBOI I VOA 1 0 0 7 1 3 3/90 IS ORCAKICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS EPA SAMPLE NO. y yik'. < CQWPP' BGL17 xib Code: COMPU Case No.: 15933 "atrix: (soil/water) SOIL sample wt/vol: 1.0 (g/mL) fi evel: (low/med) LOW % Moisture: not dec. 19 Z Column: DB-624 ID: 0.53Q (mm) •^oil Extract Volume: (uL) Number TICs found: 10 Contract: 68D00159 SAS No.: SDG No.: BGL09 Lab Sample ID: 402888 Lab File ID: GR002888C18 Date Received: 03/04/91 Date Analyzed: 03/12/91 Dilution Factor: 1.0 Soil Aliquot Volume: (uL) CONCENTRATION UNITS: (ug/L or ug/Kg) HS/fifi CAS NUMBER 1. 2. ii: 6. 7. 8. 124-18-5 9. 10. COMPOUND NAME LAB. ARTIFACT UNKNOWN HYDROCARBON UNKNOWN HYDROCARBON UNKNOWN SUBST. CYCLOHEXANE UNKNOWN ETHYLMETHYLBENZENE UNKNOWN DECANE ETRYIMETHYLBENZENE UNKNOWN HYDROCARBON RT 3.75 19.09 20.25 20.45 21.45 21.97 22.15 22.32 22.65 23.05 EST. CONC. -i 140 ^iT^ffa 99 74 49 140 62 120 990 86 740 J V J f J J ^ / JA/ JN / in FOOi I VOA-TIC 100714 i 3/90 IA VOIATIU aaCMKICS ANALYSIS DATA SHEET EPA SAMPLE NO. BGL16 T5b Naune: COMt^'J^UMmi* Contract: 68D00159 Lab Code: COMPU Case No.: 15933 SAS No.: SDG No.: BGL09 Matrix: (soil/water) SOIL Sample wt/vol: l.O (g/mL) G Level: (low/med) LOW \ Moisture: not dec. 42 GC Column: DB-624 ID: 0.530 (mm) Soil Extract Volume: (uL) CAS NO. COMPOUND Lab Sample ID: 402887 Lab File ID: GR002887B18 Date Received: 03/04/91 Date Analyzed: 03/11/91 Dilution Factor: 1.0 Soil Aliquot Volume: (uL) CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG Q 7 4 -87-3 Chloromethane 74-83-9 Bromomethane 75-01-4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1.1-Dichloroothene 75-34-3 1. l-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chlorofora 107-06-2 1.2-Dichloroethane 78-93-3 2-Butanone 71-55-6 1.1.1-Trichloroethane 56-23-5 Carbon Tetrachloride 75-27-4 Broaodichloromethzme 78-87-5 1.2-Dichloropropane 10061-01-5 cis-1.3-Dichloropropene 79-01-6 Trichloroethene 124-4 8-1—jMMi Dibromochloromethane 79-00-5—-^|*~1.1.2-Trichloroethane 71-43-2—Mffiv Benzene 1006l-02-«Wliii«—Trans-1,3-Dichloropropene 75-25-2 Broaofora 108-10-1 4-Methyl-2-Pentanone 591-78-6 -2-Hexanone 127-18-4 Tetrachloroethene 79-34-5 1.1.2.2-Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene 1 100-42-5 Styrene 1330-20-7 xylene (total) 86 86 86 86 370 ^ 370 ^ 86 86 86 86 86 86 - 150 86 86 86 86 86 86 86 86 86 86 86 86 86 86 86 86 86 8« , SS 18 u U U D U u u u D U 1 u ^ 0 U u U U U U ,U u u D u D U U U U n J FORM I VOK. 100715 3/»e zm IS VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVILY IDENTIFIED COMPOUNDS EPA SAMPLE NO. fame: COMPU' Code: COMPU BGL16 Case No.: 15933 rix: (soil/water) SOIL mple wt/vol: 1.0 (g/mL) fi el: (low/med) LOW Moisture: not dec. 42 Column: DB-624 ID: 0.530 (mm) 1 Extract Volume: (uL) ntnber TICs fovind: 10 Contract: 68D00159 SAS No.: SDG No.: BGL09 Lab Sample ID: 402887 GR002887B18 Q3/04/91 Lab File ID: Date Received: Date Analyzed: 03/11/91 Dilution Factor: 1.0 Soil Aliquot Volume: fuL) CONCENTRATION UNITS: (ug/L o r ug/Kg) HfiL^Kfi CAS NUMBER 1. 2. ^ m w. 6. 7. 8. 9. 0. COMPOUND NAME UNKNOWN HYDROCARBON UNKNOWN HYDROCARBON UNKNOWN CYCLIC HYDROCARBON UNKNOWN HYDROCARBON UNKNOWN HYDROCARBON UNKNOWN HYDROCARBON UNKNOWN CYCLIC HYDROCARBON UNKNOWN HYDROCARBON ETHYIMETHYLBENZENE UNKNOWN HYDROCARBON RT 19.09 20.25 20.45 20.57 21.15 21.45 22.15 22.35 22.65 23.05 EST. CONC. 1200 1300 770 830 5200 2900 2600 14000 1100 12000 Q 7 ^ J J J J J J J JAI • J FORM I VOA-TIC 1 0 0 7 1 6 1 3/90 IA VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. 9L «RTP b Name: COMPPi Lab Code: COMPU Case No.: 15933 Matrix: (soil/water) SOIL Sample wt/vol: 5.0 (g/mL) fi Level: (low/med) LOW % Moisture: not dec. 16 GC Column: DB-624 ID: 0.530 (mm) Soil Extract Volume: (uL) BGL13 Contract: 68D00159 SAS No,: SDG No.: BGL09 CAS NO. COMPOUND Lab Sample ID: 402884 Lab File ID: GH002884A18 Date Received: 03/04/91 Date Analyzed: 03/08/91 Dilution Factor: 1.0 Soil Aliquot Volume: (uL) CONCENTRATION UNITS: (ug/L or ug/Kg) Qfi/£fi Q 74-87-3 74-83-9 75-01-4 75-00-3 75-09-2 67-64-1 75-15-0 75-35-4 75-34-3 540-59-0 67-66-3 107-06-2 78-93-3 71-55-6 56-23-5 75-27-4 78-87-5 10061-01-5 79-01-6 « 124-48-1— 79-00-5 71-43-2 10061-02-6 -Chloromethane - Bromomethane -Vinyl Chloride, -Chloroethane -Hethylene Chloride, -Acetone Carbon Disulfide, 1,l-Dichloroethene_ 1,1-Dichloroethane' •1,2-Dichloroethene (total), -Chlorofora •1,2-Dichloroethane_ • 2 -Butemone -1,1, l-Trichloroethane_ -Carbon Tetrachloride_|] -Broaodichloroaethane_ •1,2-Dichloropropane_ -cis-1,3-Dichloropropene, -Trichloroethene " -Dibromochloromethane 1,1,2-Trichloroeth2me, Benzene Trans-l,3-Dichloropropene, Broaofora -4 -Methyl -2 -Pentemone, -2-Bexanone EEZE^^_ 75-25-2 108-10-1 591-78-6 127-18-4 Tetrachloroethene 79-34-5 108-88-3 108-90-7 100-41-4 100-42-5 1330-20-7 • Xylene (total) -1,1,2,2-Tetrachloroethane_ -Toluene " —Chlorobenzene, —Ethylbenzene^^ —Styrene, 12 12 12 12 66 47 12 12 12 12 12 12 12 12 12 12 12 12 12 12 12 12 12 12 12 12 12 12 13 12 13 12 U U u (u U D U U U U U U U u u U u u u D U O u u u n 9 u u a .11 FORK r VOSi 100717 2/90 IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS EPA SAMPLE NO. BGL13 Lab Code: COMPU Case No.: 15933 SAS No.: SDG No.: BGL09 latrix: (soil/water) SOIL Sample wt/vol: 5.0 (g/mL) fi .^vel: (low/med) LOW " Moisture: not dec. 1$ GC Column: DB-624 ID: 0.530 (mm) oil Extract Volume: (uL) lumber TICs found: 2 402994 Lab Sample ID: Lab File ID: GH002884A18 Date Received: 03/04/91 Date Analyzed: 03/08/91 Dilution Factor: 1.0 Soil Aliquot Volume: (uL) CONCENTRATION UNITS: (ug/L or ug/Kg) QfiZKfi CAS NUMBER 1. 2. COMPOUND NAME LABORATORY ARTIFACT UNKNOWN RT 3.82 5.65 EST. CONC. >NC. ^ i 11 .^sy ^ 9 . 5 J ^ " ^ •rr i FORM I VOA-TIC 1 0 0 7 1 8 lli *.m 3- 3/90 • ^ IA VOLATIIS ORGANICS ANALYSIS DATA SHEET EPA SAHPLS NO. Name: COMPUCHEM. lb Code: COMPU Case No.: 15933 itrix: (soil/water) SOIL sample wt/vol: 5.0 (g/mL) fi jvel: (low/med) LOW I Moisture: not dec. 16 ; Column: DB-624 ID: 0.530 (mm) ^^il Extract Volume: (uL) BGL14 Contract: 68D00159 SAS No.: SDG No.: BGL09 CAS NO. COMPOUND Lab Sample ID: 402885 Lab File ID: GH002885B18 Date Received: 03/04/91 Date Analyzed: 03/09/91 Dilution Factor: 1.0 Soil Aliquot Volume: (uL) CONCENTRATION UNITS: (ug/L or ug/Kg) JJfiZKfi Q 74-87-3 74-83-9 75-01-4 75-00-3—- 75-09-2 67-64-1 75-15-0 75-35-4 75-34-3 540-59-0 67-66-3 107-06-2— 78-93-3 71-55-6 56-23-5 75-27-4 78-87-5 10061-01-5 79-01-6 124-48-1— 79-00-5 71-43-2 10061-02-6 75-25-2 108-10-1— 591-78-6— 127-18-4— 79-34-5 108-88-3— 108-90-7— 100-41-4— 100-42-5— 1330-20-7- -Chloromethane -Bromomethane -Vinyl Chloride, -Chloroethane -Methylene Chloride, -Acetone Carbon Disulfide -1,1-Dichloroethene -1,l-Dichloroethane -1,2-Dichloroethene (total), -Chloroform -1,2-Dichloroethane, -2-Butanone -1,1,1-Tr ichloroethane, -Carbon Tetrachloride^^ -BroaodichloroiMthane_ >1,2-Dichloropropane -cis-l,3-Dichloropropene_ -Trichloroethene Dibroaochloromethane 1,1,2-Trichloroethane zene -1,3-Dichloropropene, Broaofora •4-Methyl-2-Pentanone, •2-Hexanone ' Tetrachloroethene -1,1,2,2-Tetrachloroethane, -Toluene ' -Chlorobenzene, -Ethylbenzene^] -Styrene_ Xylene (total). FORM TfOh'-*-' 100719 3/90 '.. i n IE EPA SAMPLE HO. VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS — BGL14 'Name: fiQMHISHZILiBI Contract: 68D00159 L_b code: COMPU Case No.: 15933 SAS No.: ______ SDG No.: BGL09 ^ trix: (soil/water) SOIL Sample wt/vol: 5.0 (g/mL) fi ii /el: (low/med) LOW ; Moisture: not dec. 16 T Column: DB-624 ID: 0.530 (mm) Jrii Extract Volume: (uL) N\imber TICs fo\ind: 1 Lab Sample ID: 402885 Lab File ID: gH0Q399?B19 Date Received: 03/04/91 Date Analyzed: 03/09/91 Dilution Factor: 1.0 Soil Aliquot Volume: (uL) CONCENTRATION UNITS: (ug/L or ug/Kg) HfiZKfi CAS NUHBER 1. COMPOUND NAME LABORATORY ARTIFACT RT 3.83 EST. CONC. 15 " ^ ^-* i 1 0 0 7 2 0 FORM I VOA-TIC i 1 i t i r i i t «^ d J *i i % . 3/90 ^ : - ^ lA ^« TOLMTILB OitGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. Name: .ab Code: COMPU Case No.: 15933 Contract: 68D00159 SAS No.: BGL15 SDG No.: BGL09 Matrix: (soil/water) SOIL sample wt/vol: 3.0 (g/mL) fi ifivel: (low/med) LOW % Moisture: not dec. 18 ;C Column: DB-624 ID: 0.530 (mm) Soil Extract Volume: (uL) CAS NO. COMPOUND Lab Sample ID: 402886 Lab File ID: G3R02886A18 Date Received: 03/04/91 Date Analyzed: 03/14/91 Dilution Factor: 1.0 Soil Aliquot Volume: (uL) CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG Q 74-87-3 Chloromethane 74-83-9 Bromomethane 75-01-4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1.1-Dichloroethene 75-34-3 1, l-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chlorofora 107-06-2 1,2-Dichloroethane 78-93-3 2-Butanone 71-55-6 1.1.1-Trichloroethane 56-23-5 Carbon Tetrachloride 75-27-4 Broaodichloromethane 78-87-5 1,2-Dichloropropane 10061-01-5 cis-1.3-Dichloropropene 79-01-6 Trichloroethene 79-00-5 Jjii, 1 -1.2-Trichloroethane 71-43-2—-HHsi-'Benzene 10061-02-6«Mflp^>-Trans-l, 3-Dichloropropene 75-25-2 Broaofora 108-10-1 4-Methyl-2-Pentanone 591-78-6 2-Hex2mone 127-18-4 Tetrachloroethene 79-34-5 1.1.2.2-Tetrachloroethane 108-88-3 Toluene 108-90-7———-Chlorobenzene 100-41-4 Ethylbenzene 100-42-5 Styrene 1330-20-7 Xylene (total) 20 20 20 20 88 35 a 20 20 20 20^ \-- 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 U J i ^ 1 ^ 1 u ^ , F i j U U U U u u u u u u u u u D u u o D U U U u r . TCBK I VOA 100721 3/90 IS VOLATILI OBfiAHICS ANALYSIS DATA SHEET TENTATIVIUr IDENTIFIED COMPOUNDS EPA SAMPLE NO. M e : COMPUCHEM.. Code: COMPU Case No.: 15933 BGL15 Contract: 68D00159 SAS No.: SDG No.: BGL09 '•rix: (soil/water) SOIL Tiple wt/vol: 3.0 (g/mL) fi 2l: (low/med) LOW 'Moisture: not dec. 18 Column: DB-624 ID: 0.530 (mm) ' 1 Extract Volume: (uL) amber TICs found: 10 Lab Sample ID: 402886 Lab File ID: G3R02886A18 Date Received: Q3/04/91 Date Analyzed: 03/14/91 Dilution Factor: 1.0 Soil Aliquot Volume: (uL) CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG CAS NUMBER .. 124-18-5 2. 1. 629-62-9 • w 6. 112-40-3 9. 1'^. COMPOUND NAME DECANE UNKNOWN HYDROCARBON PENTADECANE UNKNOWN HYDROCARBON UNKNOWN HYDROCARBON DODECANE DIMETHYL UNDECANE UNKNOWN HYDROCARBON UNKNOWN HYDROCARBON UNKNOWN HYDROCARBON RT 22.44 23.17 25.46 26.29 27.02 28.26 28.66 29.71 , 30.21 30.91 EST. CONC. 260 200 900 200 330 1200 570 330 530 1300 Q JN J JN J -J JN J J J J FORM I VOA-TIC 1 0 0 7 2 2 r z ,••» -4-5 -:&«-j 3 / f « ^ IA: EPA SAMPLE NO. VOLXACStf ORBANICS ANALYSIS DATA SHEET • ab Na Lab Cc [atri> "Sample Level: ; Mois GC Col ioil i 41k ' w m w ™«. rnnPTTrmnlS^K' Contract: 68D00159 )de: COMPU Case No.: 15933 SAS No.: SDG BGL23 No.: BGL09 :: fsoil/water) SOIL Lab Sample ID: 402989 ! wt/vol: 5.0 (q/mL) G Lab File ID: GR002889C riow/med) LOW Date Received: 03/04/91 .ture: not dec. _?, Date Analyzed: 0.3/12/91 .umn: DB-624 ID: 0.530 (mm) Dilution Factor: 1,0 :xtract Volume: (uL) Soil Aliquot Volume: CONCENTRATION UNITS: CAS NO. COMPOUND fua/L or ua/Ka) DC/KG Q 74-87-3 Chloromethane 74-83-9 Bromomethane 75-01-4 Vlnvl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1.1-Dichloroethene 75-34-3 1. l-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform 107-06-2 1.2-Dichloroethane 71-55-6 •^S^rrTTT-Trichloroethane 56-23-5 Carbon Tetrachloride 75-27-4 Broaodichloromethane 78-87-5 1,2-Dichloropropane 10061-01-5 cis-1,3-Dichloropropene 79-01-6 —r-—Trichloroethene 124-48-1—•^MJB^tfibroaochloromeSiarie 79-00-5 •^•Bfc-l.l. 2-Trichloroethane 71-43-2 «9ppiNenzene 10061-02-6-^ir 'lians-1,3-Dichloropropene 75-25-2 Broaofora 108-10-1 4-Methvl-2-Pentanone 591-78-6 2-Hexahone 127-18-4 Tetrachloroethene 79-34-5 1.1.2.2-Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene 100-42-5 styrene 1330-20-7 xylene (total) "^ FORM I VOJi- 11 11 11 11 51 J 32 11 11 11 11 11 11 18 11 11 11 11 11 210 11 11 11 11 11 11 11 11 . 11 11 11 11 11 11 100723 D ^ U U U U u u u u u u u u u u u u u u u u D u u 0 3 la. _(uL) i 1 1 V ^ . --' 1 t* 790 IS VOLATILS ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS EPA SAMPLE NO. BGL23 'Name: COMPUCHEM.ff» Contract: 68D00159 _ab Code: COMPU Case No.: 15933 SAS No.: ; SDG No.: BGL09 : ttrix: (soil/water) SOIL Sample wt/vol: 5.0 (g/mL) fi 1 '.vel: (low/med) LOW % Moisture: not dec. ^ : : Column: DB-624 ID: 0.530 (mm) f )il Extract Volume: (uL) Number TICs found: 1 Lab Sample ID: 402889 Lab File ID: GR002889C18 Date Received: 03/04/91 Date Analyzed: 03/12/91 Dilution Factor: 1.0 Soil Aliquot Volume: CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG .(uL) CAS NUMBER 1. COMPOUND NAME LABORATORY ARTIFACT RT 3.77 EST. CONC. 15 * FORM I VOA-TIC 100724 3 S 3/90 N. V IA . y j s y ^ A'^ I <^ %. A SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET lb Name: COMPUCH^.RTP Contract: 68D00159 Lab Code: COMPU Case No.: 15933 SAS No.: SDG No.: BGLOl Matrix: (soil/water) WATER Sample wt/vol: 5.0 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. GC Column: DB-624 ID: 0.530 fmm) Soil Extract Volume: (uL) Lab Sample ID: 402871 Lab File ID: CN002871B53 Date Received: 03/04/91 Date Analyzed: 03/07/91 Dilution Factor: 1.0 CAS NO. COMPOUND Soil Aliquot Volume: CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L .(UL) 74-87-3 Chloromethane 74-83-9 Bromomethane 75-01-4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 carbon Disulfide 75-35-4 1,1-Dichloroethene 75-34-3 1, l-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform 107-06-2 1,2-Dichloroethane 78-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 75-27-4 Bromodichloromethane 7 8-87-5 1,2-Dichloropropane 10061-01-5 cis-1,3-Dichloropropene 79-01-6 Trichloroethene 124-48-1— Dibromochloromethane 79-00-5—i^" 1,1,2-Trichloroethane 71-43-2—^'•'-—Benzene 10061-02-g*-- Trans-1,3-Dichloropropene 75-25-2 Bromoform 108-10-1 4-Methyl-2-Pentanone 591-78-6 2-Hexanone 127-18-4 Tetrachloroethene 79-34-5 1,1,2,2-Tetrachloroethane 108-88-3 Toluene 108-90-7 —Chlorobenzene 100-41-4 Ethylbenzene 100-42-5 Styrene 1330-20-7 Xylene (total) 10 10 10 10 3 10 10 10 10 10 10 10 10 3 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 u u , u u BJ u u u u u u u u J u u u u u u u u u u u u u u u u u u u FORM I VOA 1 0 0 7 2 5 3/90 • ^ IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS EPA SAMPLE NO. BGL18 Name: COMPUCHEM.RTP Contract: 68D00159 db Code: COMPU Case No.: 15933 SAS No.: SDG No.: BGLOl itrix: (soil/water) WATER Sample wt/vol: 5.0 (g/mL) ML i ivel: (low/med) LOW ^Moisture: not dec. JO Column: DB-624 ID: 0.530 (mm) ; lil Extract Volxome: (uL) "Tumber TICs found: 0 Lab Sample ID: 402871 Lab File ID: CN002871B53 Date Received: 03/04/91 Date Analyzed: 03/07/91 Dilution Factor: 1.0 Soil Aliquot Volume: CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L .(UL) CAS NUMBER COMPOUND NAME RT EST. CONC. Qt ^««^:. 100726 FORM I VOA-TIC 3/90 IA VOLATILE ORGANICS ANALYSIS DATA SHEET m -- ''ly^z EPA SAMPLE NO. / Name: COMPUCHEM.IffP 3D Code: COMPU Case No.: 15933 :rix: (soil/water) WATER ample wt/vol: 5.0 (g/mL) ML ( r e l : (low/med) LOW Moisture: not dec. i. Column: DB-624 ID: 0.530 (mm) c .1 Extract Volume: (uL) BGL19 Contract: 68D00159 SAS No.: SDG No.: BGLOl Lab Sample ID: 402872 Lab File ID: CN002872B53 Date Received: 03/04/91 Date Analyzed: 03/07/91 Dilution Factor: 1.0 CAS NO. COMPOUND Soil Aliquot Volume: CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L .(UL) 74-87-3 Chloromethane 74-83-9 Bromomethane 75-01-4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1,1-Dichloroethene 75-34-3 1, l-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform 107-06-2 1,2-Dichloroethane 78-93-3 • 2-Butanone 71-55-6 1 ,i.J^r2richloroethane 56-23-5 Carbon Tetrachloride 75-27-4 Bromodichloromethane 78-87-5 1,2-Dichloropropane 10061-01-5 cis-1,3-Dichloropropene 79-01-6 Trichloroethene 124-48-1 -*•-Dibromochloromethane 79-00-5 -'--i'-l, 1,2-Trichloroethane 71-43-2 •Bj-Benzene 10061-02-6 --Trana-1,3-Dichloropropene 75-25-2 Bromoform 108-10-1 4-Methy 1-2-Pentanone 591-78-6 2-Hexanone 127-18-4 Tetrachloroethene 79-34-5 -1,1,2,2-Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene 100-42-5 Styrene 1330-20-7 Xylene (total) 10 10 10 10 4 10 10 10 10 10 10 10 10 2 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 u u u u BJ u u u u u u u u J u u u u u u u u u u u u u u u D u u u FORM I VOA 100727 3/90 f, IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS Name: COMPUCHEM.RTP _ab Code: COMPU Case No.: 15933 : trix: (soil/water) WATER sample wt/vol: 5.0 (g/mL) ML 1 vel: (low/med) LOW \ Moisture: not dec. "^s. Column: DB-624 ID: 0.530 (mm) r il Extract Volume: (uL) "umber TICs found: 0 EPA SAMPLE NO, BGL19 Contract: 68D00159 SAS No.: SDG No.: BGLOl Lab Sample ID: 402872 Lab File ID: CN002872B53 Date Received: 03/04/91 Date Analyzed: 03/07/91 Dilution Factor: 1.0 Soil Aliquot Volume: (uL) CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L CAS NUMBER COMPOUND NAME RT EST. CONC. Qf FORM I VOA-TIC 100728 3/90 IA C^lcp - VOLATILE ORGANICS ANALYSIS DATA SHEET A/y EPA SAMPLE NO. BGL22 'Name: COMPUCHEM.^P Contract: 68D00159 b Code: COMPU Case No.: 15933 SAS No.: SDG No.: BGLOl "trix: (soil/water) WATER ample wt/vol: 5.0 (g/mL) ML vel: (low/med) LOW s Moisture: not dec. Column: DB-624 ID: 0.530 (mm) •'^il Extract Volume: (uL) CAS NO. COMPOUND Lab Sample ID: 402873 Lab File ID: CN002873B53 Date Received: 03/04/91 Date Analyzed: 03/07/91 Dilution Factor: 1.0 Soil Aliquot Volume: (uL) CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q 74-87-3 74-83-9 75-01-4 75-00-3—— 75-09-2 67-64-1 75-15-0 75-35-4 75-34-3 540-59-0 67-66-3 107-06-2 78-93-3 71-55-6 56-23-5 75-27-4 78-87-5 10061-01-5- 79-01-6 124-48-1 79-00-5 71-43-2 10061-02-6- 75-25-2 108-10-1 591-78-6 127-18-4 79-34-5 108-88-3 108-90-7 100-41-4 100-42-5 1330-20-7— Chloromethane Bromomethane Vinyl Chloride, Chloroethane Methylene Chloride, Acetone Carbon Disulfide 1,1-Dichloroethene 1,l-Dichloroethane 1,2-Dichloroethene (total) Chloroform 1,2-Dichloroethane, 2-Butanone 1,1,1-Trichloroethane, ^-Carbon Tetrachloride_ Bromodichloromethane 1,2-Dlchloropropane, cis-1,3-Dichloropropene, —Trichloroethene —-—Dibromochloromethane -1,1,2-Trichloroethane, nzene .Jfe.-Trans-l,3-Dichloropropene, Bromoform 4-Methyl-2-Pentanone, 2-Hexanone Tetrachloroethene 1,1,2,2-Tetrachloroethane, Toluene Chlorobenzene, Ethylbenzene_ Styrene, Xylene (total). FORM I VOA 100729 3/90 ^ IB VOLATILB ORGANICS ANALYSIS DATA SHEET TENTATIVELI IDENTIFIED COMPOUNDS >Name: COMPUCHEM.»P b Code: COMPU Case No.: 15933 "trix: (soil/water) WATER ;ample wt/vol: 5.0 (g/mL) ML . /el: (low/med) LOW Moisture: not dec. Column: DB-624 ID: 0.530 (mm) o\l Extract Volume: (uL) Number TICs found: 0 EPA SAMPLE NO. BGL22 Contract: 68D00159 SAS No.: SDG No.: BGLOl Lab Sample ID: 402873 Lab File ID: CN002873B53 Date Received: Date Analyzed: 03/04/91 03/07/91 Dilution Factor: 1.0 Soil Aliquot Volume; CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L .(UL) CAS NUMBER COMPOUND NAME RT EST. CONC. 4 1 0 0 7 3 0 FORM I VOA-TIC 3/90 IB ORGANICS ANALYSIS DATA SHEET Xab Name: Q^SESSmmStSS-^ Contract: 68D00159 Lab Code: COMPU Case No.: 15933 SAS No. : Matrix: (soil/water) WATER Sample wt/vol: 1000 (g/mL) ML Level: (low/med) LOW % Moisture: decanted: (Y/N) Concentrated Extract Volume: 1000 fuL) EPA SAMPLE NO. BGLOl Lab Sample Lab File ID: SDG No.: BGLOl ID: 402859 Injection Volume: 2.0(uL) GPC Cleanup: (Y/N) li pH: CAS NO. COMPOUND GR002859B05 Date Received: 03/04/91 Date Extracted: 03/19/91 Date Analyzed: 03/26/91 Dilution Factor: 1.0 CONCENTRATION UNITS: (ug/L or ug/Kg) |VG/L 108-95-2 111-44-4 95-57-8- 541-73-1 106-46-7 95-50-1- 95-48-7- 108-60-1 106-44-5 621-64-7 67-72-1- 98-95-3- 78-59-1- 88-75-5- 105-67-9 111-91-1 120-83-2 120-82-1 91-20-3- 106-47-8- 87-68-3- 59-50-7- 91-57-6- 77-47-4- 88-06-2- 95-95-4- 91-58-7- 88-74-4- 131-11-3 208-96-8 606-20-2 99-09-2- 83-32-9- Phenol -bis(2-Chloroethy1)Ether, -2-Chlorophenol_ •1,3-Dichlorobenzene, •1,4-Dichlorobenzene~ •1,2-Dichlorobenzene^ •2-Methy Iphenol, -2,2'-Oxybis(1-Chloropropane) •4-Methylphenol -N-Nitroso-Di-n-Propyl«unine -Hexachloroethane -Nitrobenzene •Isophorone 2-Nitrophenol, 2,4-Dimethylphenol_ -bis(2-Chloroethoxy)Methane •2,4-Dichloropheno1 - '*ti -! 1,2,4-Trichlorobenzene, N«^thalene, -•HSiloroaniline Hexachlorobutadiene 4-Chloro-J-Methylphenol_ 2-MethyInaphtha1ene. -Hexachlorocyclopentadiene •2,4,6-Triehlorophenol -2,4,5-Trichlorophenol - 2-Chioronaphtha1ene -2-Nitroaniline -Diaethyl Phthalate, -Acenaphthylene, •2,6-Dinitrotoluene, —3-Nitroaniline ]^ —Acenaphthene FORM I SV-1 n o o H 3/90 IC 5EMIV0LATII2' ORCAKICS ANALYSIS DATA SHEET EPA SAMPLE NO. ^ame: COMPUCHEM. b code: COMPU Case No.: 15933 BGLOl Contract: 68D00159 SAS No.: SDG No.: BGLOl : ix: (soil/water) WATER iDle wt/vol: 1000 (g/mL) ML, /--I: (low/med) LOW 1 i s t u r e : d e c a n t e d : (Y/N) i c e n t r a t e d E x t r a c t Volume: 1000 i c t i o n Volume: 2 .0 fuL) : Cleanup: (Y/N) M pH: _ CAS NO. COMPOUND GR002859B05 03/04/91 .(UL) Lab Sample ID: 402859 Lab File ID: Date Received: Date Extracted: Date Analyzed: Dilution Factor: li 03/19/91 03/26/91 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L IxiL 51-28-5 100-02-7 132-64-9 121-14-2 84-66-2 7005-72-3— 86-73-7 100-01-6 534-52-1 86-30-6 101-55-3 118-74-1 87-86-5 85-01-8 120-12-7 86-74-8 84-74-2 206-44-0 129-00-0 85-68-7 91-94-1 56-55-3 218-01-9 117-81-7 117-84-0 205-99-2 207-08-9 50-32-8 193-39-5 53-70-3 191-24-2 2,4-Dinitrophenol, 4-Nitrophenol Dibenzofuran 2,4-Dinitrotoluene, Diethylphthalate, 4-Chlorophenyl-phenylether_ Fluorene 4-Nitroaniline 4,6-Dinitro-2-MethyIphenol, N-Nitrosodiphenylamine (1)^ 4-Bromophenyl-phenylether_j| Hexachlorobenzene Pentachlorophenol Phenanthrene Anthracene Carbazole Di-n-Butylphthalate, -Fluoranthene^ '_ —^-fyrane. ylbenzylphthalate. L3 ' -Dichlorobenzidine, kzo (a) Anthracene ^ -Chrysene, bis(2-Ethylhexyl)Phthalate Di-n-Octyl Phthalate '_ Benzo(b)Fluoranthene Benzo ()c) Fluoranthene Benzo (a) Pyrene, Indeno(1,2,3-cd)Pyrene, Dibenz (a, h) Anthracene_[| Benz o(g,h,i)Pery lene 1) - Cannot be separated from Diphenyleusine FORM I SV-2 3/90 IF SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS 'Name: COMPUCHEM.RgP Contract: 68D00159 _b Code: COMPU Case No.: 15933 SAS No.: SDG trix: (soil/water) WATER ample wt/vol: 1000 (g/mL) ML rel: (low/med) LOW Moisture: decanted: (Y/N) icentrated Extract Volume: 1000 (uL) EPA SAMPLE NO, BGLOl No.: BGLOl 402859 Lab Sample ID: Lab File ID: GR002859B05 Date Received: 03/04/91 Date Extracted: 03/19/91 Date Analyzed: ~ection Volume: ^C Cleanup: (Y/N) E. 2.0fuL) 03/26/91 Dilution Factor: 1.0 pH: CONCENTRATION UNITS: ;.j3er TICs found: i CAS NUMBER 4. (ug/L or ug/Kg] COMPOUND NAME UNKNOWN UNKNOWN UNKNOWN DIO-PYRENE RT 4.97 6.30 8.17 13.62 UG/L 1 EST. CONC. 6.0 10 2.0 64 / J FORM I SV-TIC 1 0 0 7 3 3 3/90 IB SEMIVOUkTILE ORGANICS ANALYSIS DATA SHEET ^b Name: ^f^MF^CIBKjBTF Contract: 68D00159 Lab Code: COMPU Case No.: 15933 SAS No.: SDG No.: BGLOl Matrix: (soil/water) WATER Sample wt/vol: 1000 (g/mL) ML Level: (low/med) LOW % Moisture: decanted: (Y/N) Concentrated Extract Volume: 1000 fuL) Injection Volume: 2.0fuL) GPC Cleanup: (Y/N) H pH: CAS NO. COMPOUND Lab Sample ID: 402866 Lab File ID: GH002866A08 Date Received: 03/04/91 Date Extracted: 03/08/91 Date Analyzed: 03/12/91 Dilution Factor: 1.0 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L 108-95-2 111-44-4 95-57-8 541-73-1 106-46-7 95-50-1 95-48-7 108-60-1 106-44-5 621-64-7 67-72-1 98-95-3 78-59-1 — 88-75-5 105-67-9 111-91-1 120-83-2 120-82-1 91-20-3 106-47-8-'- 87-68-3— 59-50-7— 91-57-6—-« 77-47-4: 88-06-2 95-95-4 91-58-7 88-74-4-r 131-11-3 208-96-8^ 606-20-2 99-09-2 83-32-9 Phenol -bis (2-Chloroethy 1) Ether_ -2-Chlorophenol_ •1,3-Dichlorobenzene, •1,4-Dichlorobenzene^ •1,2-Dichlorobenzene' •2-Methy Iphenol, •2,2'-Oxybis(1-Chloropropane) -4-Methylphenol, -N-Nitroso-Di-n-Propylamine, -Hexachloroethane '_ -Nitrobenzene -Isophorone, 2-Nitrophenol, 2,4-Diaethy Iphenol, -bis(2-Chloroethoxy)Methane, •2,4-Dichlorophenol_ 1> 2,4-Trichlorobenzene, Naphthalene, Chloroaniline Hexachlorobutadiene .oro-3 -Methy Iphenol, 2i*itethylnaphthalene, -Hexachlorocyclopentadiene, •2', 4,6-<rrichlorophenol '_ -2,4,5-Trichlorophenol -2-Chloronaphthalene - 2 - N i t r o a n i l i n e -Dimethyl Phthalate, -Acenaphthylene, •2,6-Dinitrotoluene -3-Nitroaniline '_ -Acenaphthene FORM I SV-1 3/90 IC SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BGL02 ^ R j Name: mMPTTrw^.BTP Contract: 68D00159 Lab Code: COMPU Case No.: 15933 SAS No.: SDG No.: BGLOl EPA SAMPLE NO. M a t r i x : ( s o i l / w a t e r ) WATER Sample w t / v o l : 1000 (g/mL) ML L e v e l : (low/med) LOW % M o i s t u r e : d e c a n t e d : (Y/N) C o n c e n t r a t e d E x t r a c t Volume: 1000 fuL) C n j e c t i o n Volvime: 2 . 0 f u L ) GPC C l e a n u p : (Y/N) JH pH: CAS NO. COMPOUND Lab S a m p l e I D : 402866 Lab File ID: GH002866A08 Date Received: 03/04/91 Date Extracted: 03/08/91 Date Analyzed: 03/12/91 Dilution Factor: 1.0 CONCENTRATION UNITS: ( u g / L o r u g / K g ) iZfiZL. 5 1 - 2 8 - 5 1 0 0 - 0 2 - 7 1 3 2 - 6 4 - 9 1 2 1 - 1 4 - 2 8 4 - 6 6 - 2 7 0 0 5 - 7 2 - 3 8 6 - 7 3 - 7 1 0 0 - 0 1 - 6 5 3 4 - 5 2 - 1 8 6 - 3 0 - 6 1 0 1 - 5 5 - 3 1 1 8 - 7 4 - 1 8 7 - 8 6 - 5 8 5 - 0 1 - 8 1 2 0 - 1 2 - 7 8 6 - 7 4 - 8 8 4 - 7 4 - 2 2 0 6 - 4 4 - 0 1 2 9 - 0 0 - 0 — 8 5 - 6 8 - 7 — 9 1 - 9 4 - 1 — 5 6 - 5 5 - 3 — 2 1 8 - 0 1 - 9 1 1 7 - 8 1 - 7 1 1 7 - 8 4 - 0 2 0 5 - 9 9 - 2 2 0 7 - 0 8 - 9 5 0 - 3 2 - 8 1 9 3 - 3 9 - 5 5 3 - 7 0 - 3 1 9 1 - 2 4 - 2 2,4-Dinitrophenol, 4-N itrophenol '_ Dibenzofuran 2,4-Dinitrotoluene, Diethylphthalate, 4-Chlorophenyl-phenylether_ Fluorene 4-Nitroaniline 4,6-Dinitro-2^MethyIphenol, N-Nitrosodiphenylamine (1)' 4-Bromopheny1-pheny1ether_^ Hexachlorobenzene Pentachlorophenol Phenanthrene Anthracene Carbazole Di-n-Butylphthalate_ —Fluoranthene -—Pyrene, -—Butylbenzylphthalate -3,3'-Dichlorobenzidine, —Benzo (a) Anthracene '_ —Chrysene, bis(2-Ethylhexyl)Phthalate Di-n-Octy]^ Phthalate Benzo(b)Fluoranthene — — B e n z o (Ic) Fluoranthene Benzo(a)Pyrene, ——Indeno(1,2,3-cd)Pyrene_ Dibenz(a,h)Anthracene_^ Benzo(g,h,i)Perylene ;i) - cannot be separated from Diphenylaaine FORM I SV-2 100735 3/90 IF SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS EPA SAMPLE NO. BGL02 ^ b Name: CQiSSSSBBLXSE. C o n t r a c t : 68D00159 Lab Code: COMPU Case No.: 15933 SAS N o . : SDG No.: BGLOl Matrix: ( s o i l / w a t e r ) WATER Sample w t / v o l : 1000 (g/mL) ML. Level: (low/med) LOW % Moisture: d e c a n t e d : (Y/N) Concentrated E x t r a c t Volume: 1000 I n j e c t i o n Volume: 2.0fuL) GPC Cleanup: (Y/N) N pH: _ .(UL) Lab Sample ID: 402866 Lab File ID: GH002866A08 Date Received: 03/04/91 Date Extracted: 03/08/91 Date Analyzed: 03/12/91 Dilution Factor: 1.0 Number TICs found: CONCENTRATION UNITS: (ug/L or ug/Kg) Vfi/L CAS NUMBER k 1. 624-73-7 f 2. 3. 4. COMPOUND NAME ETHANE, 1,2-DIIODO- UNKNOWN UNKNOWN DIO PYRENE RT 5.90 6.18 6.45 13.24 EST. CONC. 6.0 390 10 42 Q JN, 3 * 100736 FORM I SV-TIC 3/90 IB SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET • Lab Name: COSSSSStlt^SE- Lab Code: COMPU Case No.: 15933 Matrix: (soil/water) WATER Sample wt/vol: 1000 (g/mL) ML Level: (low/med) LOW % Moisture: decanted: (Y/N) Concentrated Extract Volume: 1000 (uL) Injection Volume: 2.0(uL) GPC Cleanup: (Y/N) H pH: CAS NO. COMPOUND Contract: 68D00159 SAS No.: SDG No.: BGLOl Lab Sample ID: 402867 Lab File ID: GH002867A08 Date Received: 03/04/91 Date Extracted: 03/08/91 Date Analyzed: 03/12/91 Dilution Factor: 1.0 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L 108-95-2 Phenol 111-44-4 • bis(2-Chloroethyl)Ether . 95-57-8 2-ChloroDhenol 541-73-1 1,3-Dichlorobenzene 106-46-7 1.4-Dichlorobenzene 95-50-1 1,2-Dichlorobenzene 95-48-7 2-Methylohenol 108-60-1 2,2'-Oxybis(l-Chloropropane) 106-44-5 4-MethylDhenol 621-64-7 N-Nitro80-Di-n-Propylaaine 67-72-1 Hexachloroethane 98-95-3 Nitrobenzene 78-59-1 Isophorone 88-75-5 2-NitroDhenol 105-67-9 2.4-DiaethylDhenol 111-91-1 bis (2-Chloroethoxy) Methane 120-83-2 2,4-DichloroDhenol 120-82-1—-——1,2,4-Trichlorobenzene 91-20-3—Mu. —Naphthalene 106-47-0 mmr —4-Chloroaniline 87-68-3 'pij^' —Hexachlorobutadiene 91-57-6 2-MethYlnaDhthalene 77-47-4 ^Hexachlorocyclopentadiene 88-06-2 • 2.4.6»-Trichl<MroDhenol O R — O K ^ . 4 — — — . . O A R—(F*.-t .^h1 M V A n k A n n l S D — y ^ — 4 — — — * > 4, J—'irxcnxoropnenox 91-58-7 2-Chloronai^thalene 88-74-4 -2Hlitroaniline 131-11-3 Diaethyl Phthalate — 208-96-8 Acenaphthylene 606-20-2 2.6-Dinitr6toluene ;_ 99-09-2 3-Nitroaniline 83-32-9 -Acenaphthene 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 50 10 50 10 lb lb 50 u ^ < u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u ^ FORM I SV-1 100737 3/90 na IC SEMrVOLKFIlE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. • Name: COM: BGL03 uab Code: COMPU Case No.: 15933 atrix: (soil/water) WATER Sample wt/vol: 1000 (g/mL) ML jevel: (low/med) LOW % Moisture: decanted: (Y/N) Concentrated Extract Volume: loOO Injection Volume: 2.0fuL) GPC Cleanup: (Y/N) N pH: _ CAS NO. COMPOUND Contract: 68D00159 SAS No.: SDG No.: BGLOl .(uL) Lab Sample ID: 402867 Lab File ID: GH002867A08 Date Received: 03/04/91 Date Extracted: 03/08/91 Date Analyzed: 03/12/91 Dilution Factor: 1.0 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L 51-28-5 2.4-Dinitroohenol 100-02-7 4-Nitrophenol 132-64-9 Dibenzofuran 121-14-2 2,4-Dinitrotoluene 84-66-2 Diethylphthalate 7005-72-3 4-Chlorophenyl-phenylether 86-73-7 Fluorene 100-01-6 4-Nitroaniline 534-52-1 4,6-Dinitro-2-Methy Iphenol oo—ju—o—————N—WitrosociipnenYi.amine (ij 101-55-3 • 4-Bromophenyl-phenylether 118-74-1 Hexachlorobenzene 87-86-5 Pentachlorophenol 85-01-8 Phenanthrene 120-12-7 Anthracene 86-74-8 Carbazole 84-74-2 Di-n-Butylphthalate 206-44-0— Fluoranthene 129-00-0 jp^.. -Pyrene 85-68-7 ^Sk*—Butylloenzylphthalate 11 III Bit 1,3 • -Dichlorobenzidine 56-55-3— w T —Benzo (a) Anthracene 218-01-9 Chrysene 117-81-7 bis (2-Ethylhexyl) Phthalate 117-84-0 Di-n-Octvl Phthalate 205-99-2 Benzo (b) Fluoranthene 207-0 8-9 Benzo (K) Fluoranthene 50-32-8 Benzo (a) Pyrene 193-39-5 Indeno (1.2.3-cd) Pyrene 53-70-3 Dibenz (a, h) Anthracene 191-24-2 Benzo(a.h. i) Perylene 50 50 10 10 10 10 10 50 50 10 10 10 50 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 a-?-: u u u u u u u u u u u u u u u u « u u u u u u u u u u u u 0 X i ^ 1) - Cannot be separated from Diphenylaaine FORM I SV-2 100738 3/90 IF SEMTVOLATILB ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS EPA SAMPLE NO. Name: CQMPUCHEMfTP BGL03 _ab Code: COMPU Case No.: 15933 atrix: (soil/water) WATER Sample wt/vol: 1000 (g/mL) ML, evel: (low/med) LOW % Moisture: decanted: (Y/N) oncentrated Extract Volume: 1000 "njection Volume: 2.0fuL) GPC Cleanup: (Y/N) H pH: _ Contract: 68D00159 SAS No.: SDG No.: BGLOl .(UL) Lab Sample ID: 402867 Lab File ID: GH002867A08 Date Received: 03/04/91 Date Extracted: 03/08/91 Date Analyzed: 03/12/91 Dilution Factor: 1.0 ..umber TICs found: CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L CAS NUMBER ^ 1 . 624-73-7 COMPOUND NAME ETHANE, 1,2-DIIODO- DIO PYRENE^ RT 5.92 13.29 EST. CONC. 8.0 42 ci JN J •JI-: 1 ' J : FORM I SV-TIC 1 0 0 7 3 9 3/90 r^K IB SEMIVOUkTILI OBGANICS ANALYSIS DATA SHEET ame: C^MFJCHg"tMff: Contract: 68D00159 EPA SAMPLE NO. 1 BGL04 ab Code: COMPU Case No.: 15933 SAS No. SDG No.: BGLOl :rix: (soil/water) WATER Lab Sample ID: 402868 ample wt/vol: 1000 (g/mL) ML. Lab File ID: GR002868B05 '•el: (low/med) LOW Moisture: decanted: (Y/N) oncentrated Extract Volume: 1000 1 lection Volume: 2.0(uL) ;PC Cleanup: (Y/N) U. pH: CAS NO. COMPOUND .(UL) Date Received: 03/04/91 Date Extracted: 03/19/91 Date Analyzed: 03/26/91 Dilution Factor: 1.0 CONCENTRATION UNITS: (ug/L or ug/Kg) Ug/L 108-95-2 Phenol 111-44-4 bis (2-Chlaroethyl) Ether 95-57-8 2-Chloroohenol . 541-73-1 1,3-Dichlorobenzene 106-46-7 1,4-Dichlorobenzene 95-50-1 1,2-Dichlorobenzene 95-48-7 2-Methy Iphenol 108-60-1 2,2' -Oxybis (1-Chloropropane) 106-44-5 4-Methylphenol 621-64-7 N-Nitroso-Di-n-Propylamine 67-72-1 Hexachloroethane 98-9 5-3 Nitrobenzene 78-59-1 Isophorone 88-75-5 2-Nitroohenol 105-67-9 2.4-Diaethy Iphenol 111-91-1 bis (2-Chloroethoxy) Methane 120-83-2 • 2.4-Diohlorophenol 120-82-1 ••-•t«7l, 2 •4-Trichlorobenzene 91-20-3 • 1 MiBiiyyghthalene 106-47-8—•i^^Bi^brChloroaniline 87-68-3 ;4iHlil£nachlerobutadiene 5 9-5 0-7—^•^•Es^Uc^loro-a-Methy Iphenol 91-57-6 --M-E^-Methvlnaphthalene 77-47-4 —s'^Kexaehlerocvclopentadiene 88-06-2 2.4r6>-Tylchl«rophenol 95-95-4 2.4.5-CrichloroK>henol ^ 91-58-7 2-ChloronaDhthalene « 88-74-4 2-Nitjreaniline 131-11-3 Diaethvl Phthalate 208-96-8 AceBsehthvleae 606-20-2 2.6-Dinitrotolttene 99-09-2 3-Nitroaniline 83-32 -9 Acenaohthene - 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 IQ 10 50 10 50 10 10 10 50 ~ 10" u^r u u u u u u u u u u u u u u u u u D D tJ u u u ^ d / 1^3 v*/ I FORM I SV-1 3/90 1 0 0 7 4 0 IC SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. BGL04 6ie: CQlSJSSlSSSaftJBSi Contract: 68D00159 / c o d e : COMPU Case No.: 15933 SAS No.: SDG No. : BGLOl j(fatrix: (soil/water) WATER sample wt/vol: 1000 (g/mL) ML_ Level: (low/med) LOW % Moisture: decanted: (Y/N) Concentrated Extract Volume: 1000 injection Volume: 2.0fuL) GPC Cleanup: (Y/N) H pH: _ CAS NO. COMPOUND .(UL) Lab Sample ID: 402868 Lab File ID: GR002868B05 Date Received: 03/04/91 Date Extracted: 03/19/91 Date Analyzed: 03/26/91 Dilution Factor: 1.0 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L 51-28-5 100-02-7- 132-64-9 121-14-2 84-66-2- 7005-72-3 86-73-7 100-01-6 534-52-1 86-30-6 101-55-3 118-74-1 87-86-5 85-01-8 120-12-7 86-74-8 84-74-2 206-44-0 129-00-0 85-68-7 91-94-1 56-55-3 218-01-9 117-81-7 117-84-0 205-99-2 207-08-9 50-32-8 193-39-5 •' 53-70-3 191-24-2 2,4-Dinitrophenol_ 4-Nitrophenol '_ Dibenzofuran 2,4-Dinitrotoluene, Diethylphthalate 4-Chlorophenyl-phenylether Fluorene 4-Nitroaniline 4,6-Dinitro-2-MethyIphenol N-Nitrosodiphenyleuaine (1) 4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol Phenanthrene Anthracene Carbazole —-Di-n-Butylphthalate, ——Fluoranthene '_ •Pyrene, Butylbenzylphthalate, 9» 3'-Dichlorobenzidine, Benzo (a) Anthracene '_ —Chrysene, bis(2-Ethylhexyl)Phthalate D i - n - O c t y r P h t h a l a t e \ Benzo(b)Fluorzmthene Benzo(X)Fluoranthene Benzo (a) Pyr ene Indeno (1,2 ,.3-cd) Pyrene_ Dibenz(a,h)Anthracene^^ Benzo(g,h,i)Perylene (1) - Cannot be separated froa Diphenylaaine FORM I SV-2 100741 3/90 IF SEMTVOLATILB ORGANICS ANALYSIS DATA SHEET TENTATIVBLX IDENTIFIED COMPOUNDS EPA SAMPLE NO. J D code: COMPU Contract: 68D00159 BGL04 Case No.: 15933 SAS No. atrix: (soil/water) WATER Sample wt/vol: 1000 (g/mL) ML evel: (low/med) LOW 3- Moisture: decanted: (Y/N) ^ concentrated Extract Volume: 1000 fuL) SDG No.: BGLOl ijection Volume: 2.0(uL) GPC Cleanup: (Y/N) li " Number TICs found: 3 Lab Sample ID: 402868 Lab File ID: GR002868B05 Date Received: 03/04/91 Date Extracted: 03/19/91 Date Analyzed: 03/26/91 Dilution Factor: l.Q pH: CONCENTRATION UNITS: (ug/L or ug/Kg) Vg/L CAS NUMBER i: 3. COMPOUND NAME UNKNOWN UNKNOWN DIO-PYRENE RT 5.00 6.32 13.65 EST. CONC. 7.0 6.0 61 i J \ • - i • I y\\ FORM I SV-TIC 1 0 0 7 4 2 3/90 IB SEMTVOLATILB (AOANICS ANALYSIS DATA SHEET m Name: COMPUCHEM. Contract: 68D00159 EPA SAMPLE NO. BGL06 ..ab Code: COMPU Case No.: 15933 SAS No.: atrix: (soil/water) WATER sample wt/vol: 1000 (g/mL) ML ivel: (low/med) LOW Moisture: decanted: (Y/N) -oncentrated Extract Voliime: 1000 fuL) / SDG No.: BGLOl ijection Volume: 2.0(uL) ;PC Cleanup: (Y/N) Ji pH: CAS NO. COMPOUND Lab Sample ID: 402870 Lab File ID: GH0Q2870A08 Date Received: 03/04/91 Date Extracted: 03/08/91 Date Analyzed: 03/12/91 Dilution Factor: 1.0 CONCENTRATION UNITS: (ug/L or ug/Kg) yg/L 108-95-2 111-44-4 95-57-8- 541-73-1 106-46-7 95-50-1- 95-48-7- 108-60-1 106-44-5 621-64-7 67-72-1- 98-95-3- 78-59-1- 88-75-5- 105-67-9 111-91-1- 120-83-2- 120-82-1- 91-20-3- 106-47-8- 87-68-3- 59-50-7- 91-57-6- 77-47-4- 88-06-2- 95-95-4- 91-58-7- 88-74-4- 131-11-3 208-96-8 606-20-2 99-09-2- 83-32-9- Phenol —bis(2-Chloroethy1)Ether, —2-Chlorophenol, —1,3-Dichlorobenzene, —1,4-Dichlorobenzene^ —1,2-Dichlorobenzene~ —2-Methy Iphenol, —2,2'-Oxybis(1-Chloropropane) —4-Methylphenol, —N-Nitroso-Di-n-Propylamine, —Hexachloroethane '_ —Nitrobenzene —Isophorone^, 2-Nitvophenol 2,4-Diaethylphenol, — b i s (2-€liloroethoxy) Methane, —^2,4-Diefaiorophenol_ "^•l, a ? 4-Ttlchlorobenzene_ lalene oroaniline lorobutadiene Lorc»i^3 -Methy Iphenol, —3>>>Methylna|phthal ene. —Heicaehlorocyclopentadiene, — 2 , 4 , 6 ' Tl ichlerephenol I — 2 , 4 , SrTriebilorophenol —2-Chloronaphthalene —2!-Nitroaniline — D i a e t h y l Phthalate, —Ace>ttiphthylen«. — 2 , 6 - O l a i t r o t o l u e n e — 3 - N i t r o a n i l i n e '_ —Acenaphthene__ FORM I SV-1 . ' • • S I 100743 3/90 ^ IC SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET y ^Name: COMTOCHBM.gP ao Code: COMPU Case No.: 15933 SAS No.: c -.rix: (soil/water) WATER ample wt/vol: 1000 (g/mL) JH^. contract: 68D00159 EPA SAMPLE NO. BGL06 SDG No.: BGLOl E el: (low/med) LOW Moisture: decanted: (Y/N) :)..centrated Extract Volume: 1000 TuL) 1 action Volume: 2.0(uL) 'C Cleanup: (Y/N) H pH: CAS NO. COMPOUND Lab Sample ID: 402870 Lab File ID: GH002870A08 Date Received: 03/04/91 Date Extracted: 03/08/91 Date Analyzed: Q?/13/?l Dilution Factor: 1.0 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L i i 51-28-5 2.4-Dinitrophenol 100-02-7— 4-Nitrophenol 132-64-9 Dibenzofuran k 121-14-2 2.4-Dinitrotoluene f 84-66-2 Diethylphthalate 7005-72-3 4-Chlorophenyl-phenylether 86-73-7 Fluorene 100-01-6 4-Nitroaniline 534-52-1 4,6-Dinitro-2-Methylphenol 86-30-6 N-Nitrosodiphenylamine (1) 101-55-3— 4-Bromophenyl-phenYlether 118-74-1 Hexachlorobenzene 87-86-5 Pentachlorophenol 85-01-8 -Phenanthrene 120-12-7 Anthracene 86-74-8 Carbazole 84-74-2 Di-n-Butvlphthalate 206-44-0 —Fluoranthene 129-00-0 Mgpi'ene 85-68-7 «e|B*Ylbenzylphthalate 91-94-1 —^•|S3»-Dichlorobenzidine 56-55-3 ^ e n z o (a) Anthracene 218-01-9 -Chrysene . 117-81-7 bis( 2-Ethylhexyl) Phthalate 117-84-0 —Di-n-Octyl Phthalate 205-99-2 Benzo (b) Fluoranthene 207-08-9 Benzo (k) Fluoranthene 50-32-8 Benzo (a) Pyrene 193-39-5 Indeno (1.2,3-cd) Pyrene •53-70-3 Dibenz (a, h) Anthracene ^191-24-2 Benzo (q,h,i) Perylene 50 50 10 10 10 10 10 50 50 10 10 10 50 10 10 10 10 10 4 10 10 10 10 10 6 10 10 10 io 10 10 10 u u u u ) i y l ^ • « * r 1^ (1) - Cannot be separated froa Diphenylaaine FORM I SV-2 100744 MMUft IF SEMIVOLATILB ORGANICS ANALYSIS DATA SHEET TEHTATTVBLY IDENTIFIED COMPOUNDS EPA SAMPLE NO. Name: COMPy Lab Code: COMPU BGL06 Case No.: 15933 Matrix: (soil/water) WATER Sample wt/vol: 1000 (g/mL) ML ..evel: (low/med) ' LOW % Moisture: decanted: (Y/N) :oncentrated Extract Volume: 1000 fuL) Contract: 68D00159 SAS No.: SDG No.: BGLOl Cnjection Volxime: 2.0fuL) PC Cleanup: (Y/N) JI imber TICs found: 1 Lab Sample ID: 402870 Lab File ID: GH002870A08 Date Received: 03/04/91 Date Extracted: 03/08/91 Date Analyzed: 03/12/91 Dilution Factor: 1.0 pH: CONCENTRATION UNITS: (ug/L or ug/Kg) yg/L CAS NUMBER 1. COMPOUND NAME DIO-PYRENE RT 1 3 . 4 4 EST. CONC. 44 - \ a Q ZT "* \ A \ .-, -y- ^ -.^ -r. rf\ .... ... N J ' - • ; —. - '••.» o - ityz • ' % E : FORM I SV-TIC 100745 3/90 « IB SEMTVOLATILB OBGANICS ANALYSIS DATA SHEET EPA SAMPLE HO/ BGL09 Name: coMPUCHg^JTf Contract: 68D00159 Lab Code: COMPU Case No.: 15933 SAS No.: SDG No.: BGL09 atrix: (soil/water) SOIL Sample wt/vol: 30.6 (g/mL) fi evel: (low/med) LOW " Moisture: 27 decanted: (Y/N) JI Concentrated Extract Volume: 500.0 fuL) ijection Volume: 2.0(uL) GPC Cleanup: (Y/N) X pH: 7.3 CAS NO. COMPOUND Lab Sample ID: 402874 Lab File ID: GR002874B52 Date Received: 03/04/91 Date Extracted: 03/15/91 Date Analyzed: 03/20/91 Dilution Factor: 1.00 CONCENTRATION UNITS: (ug/L or ug/Kg) Vg/Kg 108-95-2- 111-44-4- 95-57-8— 541-73-1- 106-46-7- 95-50-1— 95-48-7— 108-60-1- 106-44-5- 621-64-7- 67-72-1— 98-95-3— 78-59-1— 88-75-5— 105-67-9- 111-91-1- 120-83-2- 120-82-1- 91-20-3— 106-47-8- 87-68-3— 59-50-7— 91-57-6— 77-47-4— 88-06-2— 95-95-4— 91-58-7— 88-74-4— 131-11-3- 208-96-8- 606-20-2- 99-09-2— 83-12-9— Phenol bis(2-Chloroethyl)Ether, 2 -Chlorophenol ' 1,3-Dichlorobenzene, 1,4-Dichlorobenzene' -1,2-Dichlorobenzene 2-MethyIphenol 2,2'-Oxybis(1-Chloropropane) 4-Methylphenol, N-Nitroao-Di-n-Propylamine, —-—Hexachloroethane ^ Nitrobenzene Isophorone_ -2-Nitrophenol. 2,4-Diaethylphenol, —bis (2-Chloroethoxy) Methane, —2,4-Dichlorophenol, — - l »2,4-Trichlorobenzene, - *<|wi«Bephtbalene '_ lloroaniline ehlorobutadiene loro-3-MethyIphenol, ZHfethylnaphthalene, —Hexachlorocyclopentadiene, ———2,4,6-Triehlerophenol ^ ——-2,4,5-Trichlerophenol -2-Ghloronapbthalene a-Nitroaniline Dimethyl Phthalate, Acenaphthylene, 2,6-Dinitrotoluene 3 -Nitroanil ine ^ Acenaphthene^ FORM I SV-1 3/90 IC SEMIV<KATIIE ORGANICS ANALYSIS DATA SHEST EPA SAMPLE NO. Name: SSSSSSSSlttJBX. Lab Code: COMPU Case No.: 1$9?3 BGL09 Contract: 68D00159 SAS No.: SDG No.: BGL09 Matrix: (soil/water) SOIL Sample wt/vol: 30.6 (g/mL) fi Level: (low/med) LOW % Moisture: 27 decanted: (Y/N) li Concentrated Extract Volume: 500.0 Injection Volume: 2.0(uL) (UL) Lab Sample ID: 402874 Lab File ID: GR002874B52 Date Received: 03/04/91 Date Extracted: 03/15/91 Date Analyzed: 03/20/91 Dilution Factor: l.OO GPC Cleanup: (Y/N) CAS NO. pH: 7.3 COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) gg/Kg 51-28-5 100-02-7— 132-64-9— 121-14-2— 84-66-2 7005-72-3- 86-73-7 100-01-6— 534-52-1— 8 6 - 3 0 - 6 — 101-55-3— 118-74-1— 87-86-5 85-01-8 120-12-7— 86-74-8 84-74-2 206-44-0— 129-00-0— 85-68-7 91-94-1 56-55-3 218-01-9— 117-81-7— 117-84-0— 205-99-2— 207-08-9— 50-32-8 193-39-5— 53-70-3 191-24-2— 2,4-Dinitrophenol, 4-Nitrophenol ~_ Dibenzofuran 2,4-Dinitrotoluene, Diethylphthalate, 4-chlorophenyl-phenylether, Fluorene 4-Nitroaniline 4,6-Dinitro-2-Methylphenol, N-Nitrosodiphenyl2UBine (1)] 4-Bromophenyl-phenylether_^ Hexachlorobenzene • Pentachlorophenol Phenanthrene Anthracene Carbazole -Di-n-Butylphthalate, Fluoranthene '_ lyrene. (^Butylbenzylphthalate .3'-Dichlorobenzidine^ to( a)Anthracene •-«***attysene_ —~-bis(2-Ethylhexyl)Phthalate, Di-n-Octyt"Phthalate ——Benzo (b) Fluoranthene ——Benzo (X) Fluoranthene —Benzo(a)Pyrene, — I n d e n o (1,2^3 -cd) PyreiM. Dib«tz C* t h) Anthracene J] -Benzo(g,h,i)Perylene ; i (1) - Cannot be separated froa Diphenylaaine • o 0 7 i> • •i 2300 2300 440 440 440 440 440 2300 2300 440 440 440 2300 440 440 440 440 440 440 440 440 440 440 94- 440 44» 440^ 440 440 440 440 D O U D U U U D U U U D 0 D D U D U U D O U U 4 I JX' " * 100747 FORM I 3V-2 •* / O A ^gb Name: Lab Code: COMPU IF SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TBHTATIVBLY IDENTIFIED COMPOUNDS .•Jy«VW««-^ — ""? EPA SAMPLE NO. BGL09 Case No.: 15933 atrix: (soil/water) SOIL Sample wt/vol: 30.6 (g/mL) fi; evel: (low/med) LOW "" Moisture: \ 22. decanted: (Y/N) H Contract: 68D00159 SAS No.: SDG No.: BGL09 concentrated Extract Volume: 500.0 fuL) ijection Volume: 2.0(uL) GPC Cleanup: (Y/N) X pH: 7.3 Number TICs foxind: 29 Lab Sample ID: 402874 Lab File ID: gRQQ2974B?2 Date Received: 03/04/91 Date Extracted: 03/15/91 Date Analyzed: 03/20/91 Dilution Factor: 1.00 CONCENTRATION UNITS: (ug/L or ug/Kg) IZSZUfi CAS NUMBER 3. 4. 5. 6. 7. 8. 9. 10. 11. L2. 13. 14. L5. 16. 17. .8. .9. 20. ^1. :2. 23. 24. 5. « 9. COMPOUND NAME UNKNOWN UNKNOWN SOLVENT CONTAMINANT ALDOL UNKNOWN AMIDE SOLVENT CONTAMINANT BLANK CONTAMINANT ALDOL ALDOL UNKNOWN BLANK CONTAMINANT UNKNOWN SILOXANE UNKNOWN HYDROCARBON UMBNOWM HYDitOCARBON HYDROCARBON HYDROCARBON ACID HYCROCARBON UNUKNIM UNXNONN ALDOL ; ~ UNKNOWN UNKNOWN UNKNOWN UNXNONN UNKNOWN HYDROCARBON UNKNOWN UNKNOWN FORM I SV-TIC 100748 3/90 ^ t Name: IB SBIEEVOIATZLB ORGANICS ANALYSIS DATA SHBBT Contract: 68D00159 6 PA SAMPLE MO. BG: £r fe-- Lab Code: COMPU Case No.: 15933 SAS No.: SDG No.: BGL09 atrix: (soil/water) SOIL Lab Sample ID: 402881 Sample wt/vol: 30.2 (g/mL) G evel: (low/med) LOW " Moisture: 33 decanted: (Y/N) H Concentrated Extract Volxime: 500.0 njection Volume: 2.0(uL) .(UL) Lab File ID: GR002881B52 Date Received: 03/04/91 Date Extracted: 03/15/91 Date Analyzed: 03/20/91 Dilution Factor: 1.00 GPC Cleanup: (Y/N) CAS NO. pH: 9T? COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) Vg/Kg 108-95-2 111-44-4 95-57-8 541-73-1 106-46-7 95-50-1 95-48-7 108-60-1^ 106-44-5 621-64-7 67-72-1 98-95-3 78-59-1 88-75-5 105-67-9 111-91-1 120-83-2—-r 120-82-1- 91-20-3-^1 106-47-81 87-68-3" 59-50-7-- 91-57-6- ^ 77-47-4 88-06-2—— 95-95^4 91-58-7- 88^74^4^-"^ 131-11^3*-^ 208-96-8 606-20-2^— 99-09-2 83^32)r9r Phenol —bis(2-Chloroethy1)Ether, —2-Chlorophenol, —1,3-Dichlorobenzene, —1,4-Dichlorobenzene, —1,2-Dichlorobenzene, —2-MethyIphenol, —2,2•-Oxybis(1-Chloropropane)_ —4-Methylphenol —H-Nitroso-Di-n-Propylaaine —Hexachloroethane —Nitrobenzene —Iso|^roQe-_ •—2<-NitroBhenol_, 2 r4!^Diaethy Iphenol, --=—bieiS-Chloroethoxy) Methane, <—a, 4rr0iichlorophenol, (Za4-Trichlorobenzene, thaiene e r o a n i l i n e ehlorobutadiene oro-3-MethyIphenol, ^p^2-Nethylnaphthalene, !-9-H9e3Mu:hlorocyclopentadIene_ •^'!%, 4 « &-Trichiorophenol ^ —2^4»5-Trichlorophenol _ _ —r2HghIoronaphtbalene^ -a.-TNitreeniline -^^Diaethyl Phthalate^ •-!—Aceaaphthylen*. "^-2«6-Dinitrotoluene —3-Nitroaniline '_ —Acenaphthene FORM I SV-1 1 0 0 7 4 9 3/90 ••iM IC OLATIXJI OMBANICS ANALYSIS DATA SHEET •BX.2 ^ - - he: rnMPtTCHgM.RJg b Code: coMPU Case No.: 15933 EPA SAMPLE NO. BGLIO Contract: 68D00159 SAS No.: SDG No.: BGL09 t ix: (soil/water) SOIL PDle wt/vol: 30.2 (g/mL) fi .--l: (low/med) LOW ^ i s t u r e : 23. decanted: (Y/N) M icentrated Extract Volume: 500.0 fuL) i ction Volume: 2.0 fuL) : Cleanup: (Y/N) X pH: 8.5 Lab Sample ID: 402881 Lab File ID: gR002991B52 Date Received: 03/04/91 Date Extracted: 03/15/91 Date Analyzed: 03/20/91 Dilution Factor: 1.00 CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG IN 51-28-5 100-02-7— 132-64-9— 121-14-2— 84-66-2 7005-72-3- 86-73-7 100-01-6— 534-52-1— 86-30-6 101-55-3— 118-74-1— 87-86-5 85-01-8 120-12-7— 86-74-8 84-74-2 206-44-0— 129-00-0— 85-68-7 91-94-1 56-55-3 218-01-9— 117-81-7— 117-84-0— 205-99-2— 207-08-9— 50-32-8 193-39-5— 3-70-3 191-24-2— 2,4-Dinitrophenol, 4 -Nitrophenol ~_ Dibenzofuran 2,4-Dinitrotoluene, Diethylphthalate, 4-Chlorophenyl-phenylether, Fluorene 4-Nitroaniline 4,6-Dinitro-2-MethyIphenol, N-Nitrosodiphenyleusine (1)] — 4-Broaophenyl-phenylether_^ Hexachlorobenzene Pentachlerophenol ——Kienanthrene Anthracene ——CM:besoIe_ —^adi-n-Btttylphthalate, >ranthene 'Ibenzylphthalate, -Dichlorobenz idine, > Anthracene '_ b i t f f ^ E t h y l h e x y l x a i t h a l a t e •Dl-n-Octyl Phthalate '_ -Benzo(b)Fluoranthene •Benzo(k)Fluoranthene •Benzo (a) Pyrene, -indeno (1,2,3-cd) Pyrene, •Dibenz(a,h)Anthracene_^ •Benzo(9r>&,i) Perylene ;i) - Cannot be separated froa Diphenylaaine FORM I SV-2 I <, '• 100750 l.: 3 / 9 0 i IF OLATILK OBGANICS ANALYSIS DATA SHEET TENTATITiar IDENTIFIED COMPOUNDS EPA SAMPLE NO, ,: rpMPUCHEM. code: COMPU Case No.: 15933 BGLIO Contract: 68D00159 SAS No.: SDG No.: BGL09 trix: (soil/water) SOIL pie wt/vol: 30.2 (g/mL) G vel: (low/med) LOW loisture: 21 decanted: (Y/N) li )ncentrated Extract Volume: 500.0 (uL) .J ect ion Volume: 2.0(uL) ~Z Cleanup: (Y/N) X pH: 8.5 imber TICs found: 28 Lab Sample ID: 402991 Lab File ID: GR002881B52 Date Received: 03/04/91 Date Extracted: 03/15/91 Date Analyzed: 03/20/91 Dilution Factor: 1.00 CONCENTRATION UNITS: (ug/L or ug/Kg) Vg/Kg CAS NUMBER « 2. 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 5. 6. 7. 28. COMPOUND NAME SOLVENT CONTAMINANT ALDOL SOLVENT CONTAMINANT SOLVENT CONTAMINANT BLANK CONTAMINANT UNKNOWN ALDOL ALDOL UNKNOW UNKNOWN HYI»OCARBON UNKNOWN UNKNOWN UNXNOWN HYDROCARBON HYDROCARBON HYDROCARBON DIO-FYRXNE UNXNONN UNXNONN UNXNONN ALOOL UNXNOWN UNXNONN UNKNOWN HYDROCARBON RT 5.32 5.55 5.78 5.87 6.68 6.78 7.12 7.50 8.35 12.99 14.24 14.69 15.47 15.54 16.24 16.52 16.64 16.94 17.64 18.27 18.35 22.47 25.69 30.87 6.97 8.15 10.69 13.87 EST. CONC. FORM I SV-TIC 100751 3/90 IB SBKXV0UI9XU OlttyilCS ANALYSIS DATA SHEET EPA SAMPLE NO. iRb Naune: Lab Code: COMPU BGLII Case No.: 15933 Matrix: (soil/water) SOIL Sample wt/vol: 30.1 (g/mL) fi Level: (low/med) LOW % Moisture: 41 decanted: (Y/N) H Concentrated Extract Volume: 500.0 (uL) Injection Volume: 2.0fuL) GPC Cleanup: (Y/N) X pH: 7.4 CAS NO. COMPOUND Contract: $9P9015? SAS No.: SDG No.: BGL09 Lab Sample ID: 402882 Lab File ID: GRJ02882B07 Date Received: 03/04/91 Date Extracted: 03/28/91 Date Analyzed: 04/09/91 Dilution Factor: 1.0 CONCENTRATION UNITS: (ug/L or ug/Kg) HSZKfi 108-95-2 111-44-4 95-57-8- 541-73-1 106-46-7 95-50-1- 95-48-7- 108-60-1 106-44-5 621-64-7 67-72-1- 98-95-3- 78-59-1- 88-75-5- 105-67-9 111-91-1 120-83-2 120-82-1 91-20-3- 106-47-8 87-68-3- 59-50-7- 91-57-6- 77-47-4- 88-06-2- 95-95-4- 91-58-7- 88-74-4- 131-11-3 208-96-8 606-20-2 99-09-2- 83-32-9- Phenol -bis (2-Chloroethy 1) Ether, •2-Chlorophenol, 1,3-Dichlorobenzene, 1,4-Dichlorobenzene~ 1,2-Dichlorobenzene' 2-MethyIphenol, •2,2' -Oxybis (1-Chloropropane) _ -4 -MethQflphenol -N-Nitroeo-Di-n-Propylaaine -Hexachloroetheme -Nitrobensen«_ -Iscqphoro^ne 2r-||Ma9Bhsnol 2g#»;niaet^hylphenol_ -bi»4J|f-Chloroethoxy) Methane '2^0 4jSli9hlorophenol :flif a«dHI!riGhlorobenzene •Waphtlialene, oroanillne chlcHPobutadiene 'ro-3'-Methy Iphenol, jy.ljjIethKlimphthalene, -------S9?^ll^c|kienoeyclopentadlena_ r^li^i^ 4»<Brirfilorophenol -r-214^ •ifrTriffhlor<^>hem>l' •=r2irC>aeronephthalen» -2a|tttjroehWins£ - D i n e a w l i rtithalater,-,.: *^^VT1^^JWE*^ T*^^* w ^ ^ ^ * ^ ^ 'ip^ —2 a<yftMiiityotoluene>- a —3-Nitroaniline -Acensimthene^ 580 580 580 580 580 580 580 580 580 580 580 580 580 580 580 580 58& 580 580 580 580 58<^ 580^ 5 9 ^ 5«V^ 300*0 5B«0 30B«0 5W6' :l. j a s O i ^ M 500 u ^ u u D U D U U U U O D O O O D U U U U xy D \ ^ w w I? ,y A FORM I SV-1 100752 3/90 hii> IC Qixvoxamz ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. BGLII ^ b Code: COMPU Case No.: 15933 Matrix: (soil/water) SOIL Sample wt/vol: 30.1 (g/mL) fi Level: (low/med) LOW % Moisture: 42 decanted: (Y/N) H Concentrated Extract Volume: 500.0 fuL) Injection Volume: 2.0fuL) GPC Cleanup: (Y/N) X pH: 7.4 CAS NO. COMPOUND Contract: 68D00159 SAS No. : SDG No. : BGL09 Lab Sample ID: 402882 Lab File ID: GRJ02882B07 Date Received: 03/04/91 Date Extracted: 03/28/91 Date Analyzed: 04/09/91 Dilution Factor: 1.0 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG 51-28-5 100-02-7 132-64-9 121-14-2 84-66-2 7005-72-3— 86-73-7 100-01-6 534-52-1 86-30-6 101-55-3 118-74-1 87-86-5 85-01-8 120-12-7 86-74-8 84-74-2 206-44-0— 129-00-0 85-68-7- 91-94-1— 56-55-3— 218-01-9— 117-81-7— 117-84-0 205-99-2 207-08-9 50-32-8 193-39-5 53-70-3 191-24-2 —2,4-Dinitrophenol. —4-Nitrophenol '_ -..—Dibenzofuram —2,4-Dinitrotoluene_ —Diethylphthalate, —4-Chloropheny1-phenylether, —Fluorene ' 4-Nitroaniline —4,6-Dinitro-2-MethyIphenol —N-Nitrosodiphenylaaine (1) —4-Broaophenyl-phenylether —Hexachlorobenzene —Pentachlorophenol —iFhenanthrene —Anthracene —Carbaxole Od-B^Butylphthalate, Fiueranthene '_ Pyrene_ .tylbenzy Iphthal ate. , 3' -Didllorobenz idine, »( a ) Anthracene ~_ M.s(2-Bthylhexyl) Phthalate, •Bi^a-Octyl Phthalate, •—Benzo(b)Fluoranthene_ —Benso(]c) Fluoranthene" — B e n z o (a) Pyrene, —Indeno (1,2,3-cd) Pyrene, —Dibenz(a,h)Anthracene__ —Benzo(g,h,1)Perylene (1) - Cannot be separated froa Diphenylaaine FORM I SV-2 3000 3000 580 580 580 580 580 3000 3000 580 580 580 3000 580 580 580 580 580 580 580 580 580 580 58 O- 580 580^ 5807 580 5 W ~ 580 580 u *^^ u u u u u u u u u u u u u D u u u u u D U u D U U U u 100753 3/90 I F SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TSKSATIVEL!; IDENTIFIED COMPOUNDS EPA SAMPLE NO. y ^ m e : gSSSESSS^SOL BGLll Lab Code: COMPU Case No.: 15933 Matrix: (soil/water) SOIL Sample wt/vol: 30.1 (g/mL) fi Level: (low/med) LOW % Moisture: 41 decanted: (Y/N) Ji Concentrated Extract Volume: 500.0 (uL) [njection Volume: 2^Q(uL) GPC Cleanup: (Y/N) X pH: 7.4 Number TICs found: 24 Contract: 68D00159 SAS No.: SDG No.: BGL09 Lab Sample ID: 402882 Lab File ID: GRJ02882B07 Date Received: 03/04/91 Date Extracted: 03/28/91 Date Analyzed: 04/09/91 Dilution Factor: 1.0 CONCENTRATION UNITS: (ug/L o r ug/Kg) VG/KG i CAS NUMBER Jk^' W2. 3 . 4 . 5 . 6 . 7 . 8 . 9 . 1 0 . 1 1 . 1 2 . 1 3 . 1 4 . 1 5 . 1 6 . 1 7 . 1 8 . 1 9 . 2 0 . 2 1 . 2 2 . 2 3 . 2 4 . COMPOUND NAME SOLVENT CONTAMINANT UNKNOWN UNKNOWN ALDOL UNKNOWN ALDOL UNKNOWN HYDROCARBON UNKNOWN HYDROCARBON UNKNOWN HYDROCARBON UNKNOWN HYDROCARBON UNKNOWN RTOROCARBON UNXNOWN HYDROCARBON UNKNOWN HYDROCARBON UNXNONN HYDROCARBON inaBKNIN HYDROCARBON igJpONB HYDROCARBON • ^ B n m HYDROCARBON • ^ P — HYI2ROCARBON ^MStSfm HYDROCARBON UNXNOini HYDROCARBON UNXNOWN HYDitOCARBON UNKNOWN HYDROCARBON" DIO PYRBNB UNKNOWN HYDROCARBON RT 4 . 6 7 5 . 1 3 5 . 3 0 5 . 4 0 5 . 4 7 5 . 7 5 8 . 9 4 9 . 1 7 9 . 5 2 9 . 7 2 9 . 9 5 1 0 . 2 4 1 0 . 4 4 1 0 . 4 7 1 0 . 7 5 1 1 . 1 4 1 1 . 1 9 1 1 . 5 2 1 1 . 6 2 1 1 . 9 2 1 2 . 0 4 1 2 . 4 5 1 2 . 5 7 1 2 . 8 5 EST. CONC. 350 700 870 1300 1200 700 870 760 470 9 3 0 1400 7000 7 0 0 640 6400 1300 1200 1400 1500 1100 8 2 0 700 2 4 0 0 i 7 0 0 4 « ^ ftft JA^ J J J J J J J J J J j i j l j l Ji|... Jfz. S ^ * M ^ 3 1 0 0 7 5 4 FORM I SV-TIC 3/90 IB SAMP^^O. 1 SEMTVOLATILB O R G A N I C S ANALYSIS DATA SHEET Name: coMPTTrgr^jye Contract: 68D00159 ab code: COMPU Case No.: 15933 SAS No.: SDG No.: BGL09 itrix: (soil/water) SOIL Lab Sample ID: 402883 Sample wt/vol: 30.6 (g/mL) G_ Lab File ID: GR002883B52 i ivel: (low/med) LOW I Moisture: 14 decanted: (Y/N) Ji . incentrated Extract Volume: 500.0 r-j ect ion Volume: 2.0(uL) .(UL) sfC Cleanup: (Y/N) ,CAS NO. pH: 8.2 COMPOUND Date Received: 03/04/91 Date Extracted: 03/15/91 Date Analyzed: 03/20/91 Dilution Factor: 1.0 CONCENTRATION UNITS: (ug/L or ug/Kg) Vg/KG 108-95-2— 111-44-4— 95-57-8 541-73-1— 106-46-7— 95-50-1 95-48-7 108-60-1— 106-44-5— 621-64-7— 67-72-1 98-95-3 78-59-1 88-75-5 105-67-9— 111-91-1 120-83-2 120-82-1 91-20-3 106-47-8— 87-68-3 59-50-7 91-57-6 77-47-4 88-06-2 95-95-4 91-58-7 88-74-4 131-11-3— 208-96-8— 606-20-2— 99-09-2 83-32-9 Phenol bis(2-Chloroethyl)Ether, 2-Chlorophenol, 1,3-Dichlorobenzene, 1,4-Dichlorobenzene' 1,2-Dichlorobenzene~ — — 2 - M e t h y Iphenol, 2,2•-Oxybis(1-Chloropropeme) 4-Methylphenol, N-Nitroso-Di-n-Propyleunine, Hexachloroethane '_ Nitrobenzene Isophoxime^ 2-NitroidMnol 2,4-Diaethylphenol_ bis (2-Chloroethoxy) Methane, ——2,4-Oictklorophenol, —»—1,2,4r-Trlchlorobenzene, ilene oroanillne ehlorobutadiene )ro-3-Methy Iphenol, —«««.2^i4tothylnaphthalene. ——Bsxachlorocyclopentadiene, 2 ,4,6-Trichlorophenol '_ 2,4,5-Trichlorophenol ——2-Chloronaphthalene ._ 2-Nitroaniline Diaethyl Phthalate, Acenaphthylene, 2,6-Diaitrotoluene 3-Nitroaniline 2 Acenaphthene_ FORM I SV-1 100755 3/90 m^^ IC SEMIV<C»JITIIJB ORGANICS ANALYSIS DATA SHEET ^ Name: £QHEEflBB*KIE Contract: 68D00159 EPA SAMPLE NO. BGL12 Lab Code: COMPU Case No.: 15933 SAS No.: SDG No.: BGL09 Matrix: (soil/water) SOIL Sample wt/vol: 30.6 (g/mL) fi. Level (low/med) LOW % Moisture: 2ZL decanted: (Y/N) U Concentrated Extract Voliome: 500.0 Injection Volume: 2.0(uL) .(UL) GPC Cleanup: (Y/N) CAS NO. pH: 8.2 COMPOUND Lab Sample ID: 402883 Lab File ID: GR002883B52 Date Received: 03/04/91 Date Extracted: 03/15/91 Date Analyzed: Q3/20/?! Dilution Factor: 1.0 CONCENTRATION UNITS: (ug/L or ug/Kg) fiSZKfi 51-28-5 100-02-7 132-64-9 121-14-2 84-66-2 7005-72-3— 86-73-7 100-01-6 534-52-1 86-30-6 101-55-3 118-74-1 87-86-5 85-01-8 120-12-7 86-74-8 84-74-2 206-44-0 129-00-0 85-68-7 91-94-1 56-55-3 218-01-9 117-81-7 117-84-0 205-99-2 207-08-9 50-32-8 193-39-5 53-70-3 191-24-2 —2,4-Dinitrophenol, —4-Nitrophenol '_ —Dibenzofxiran —2,4-Dinitrotoluene_ —Diethylphthalate, — ? 4-Chlorophenyl-phenylether, —Fluorene '_ —4-Nitroanillne 4,6-Dinitro-2-MethyIphenol, N-Nitrosodiphenyl2UBine (1)] 4-Broaophenyl-phenylether_^ Hexachlorobenzene Pentachlorophenol —Phenanthrene ^Anthracene —Carbazole Dl-n-Butylphthalate, ranthene ylbenzylphthalate '-Dichlorobenzidine, ZO (a) Anthracene '_ -"•^aim (2 -Ethy Ihexyl) Phthalate —Dr-»-Octyl Phthalate \ — B e n z o (b) Fluoranthene^^ — B e n z o (Jc) Fluoranthene — B e n z o (a) Pyrene_ —Indeno(1,2,3-cd)Pyrene, —Dibenz(a,h)Anthracene_2 —Benzo(9,h,i)Perylene (1) - Cannot be separated froa Diphenylaaine' 2500 2500 490 490 490 490 490 2500 2500 490 490 490 2500 490 490 490 490 490 490 490 490 490 490 73 490 490^ 490 490 490 490 490 D U U D U U U U U U U ,U U U U U U U U U U u u 6 100756 irrvDv T rv. IF SEMIVOLATILB ORGANICS ANALYSIS DATA SHEET TSRTAXI7I9<1 IDENTIFIED COMPOUNDS EPA SAMPLE NO. Name: ^ab c o d e : COMPU BGL12 Case No.: 15933 itrix: (soil/water) SOIL sample wt/vol: 30.6 (g/mL) fi !vel: (low/med) LOW Moisture: 34 decanted: (Y/N) H ncentrated Extract Volume: 500.0 (uL) ejection Volume: 2.0(uL) fC Cleanup: (Y/N) X pH: 8.2 iber TICs found: 22 Contract: 68D00159 SAS No.: SDG No.: BGL09 Lab Sample ID: 402883 Lab File ID: GR002883B52 Date Received: 03/04/91 Date Extracted: 03/15/91 Date Analyzed: 03/20/91 Dilution Factor: 1.0 CONCENTRATION UNITS: (ug/L or ug/Kg) Vg/KG CAS NUMBER 4 4 5 S 7 » 10 Ll .7 o u 1 COMPOUND NAME SOLVENT CONTAMINANT UNKNOWN ALDOL UNKNOWN SOLVENT CONTAMINANT SOLVENT CONTAMINANT BLANK CONTAMINANT ALDOL UNKNOWN ALDOL V ALDOL ALDOL UNKNOWN -^ UNXNONN DIO-PYRENB RT 5.32 5.87 5.53 5.63 5.77 5.87 6.68 6.78 6.80 6.98 7.10 7.50 8.35 14.69 15.47 15.54 16.25 16.52 16.64 16.94 17.62 18.35 EST. CONC. FORM I SV-TIC 100757 3/90 IB SEMPl^XUaiUi ORGANICS ANALYSIS DATA SHEET • . EPA SAMPLE NO. BGL17RE b Name: i ii|||!l! IMg^ HI I . Contract: 68D00159 Lab Code: COMPU Case No.: 15933 SAS No.: SDG No.: BGL09 Matrix: (soil/water) SOIL Sample wt/vol: 30.2 (g/mL) G Level: (low/med) LOW % Moisture: 1£ decanted: (Y/N) Ji Concentrated Extract Volume: 500.0 fuL) Injection Volume: 2.0(uL) GPC Cleanup: (Y/N) X pH: 8.0 CAS NO. COMPOUND Lab Sample ID: 402888 Lab File ID: G2R02888B08 Date Received: 03/04/91 Date Extracted: 04/03/91 Date Analyzed: 04/06/91 Dilution Factor: 1.00 CONCENTRATION UNITS: (ug/L or ug/Kg) VG/Kg 108-95-2— 111-44-4— 95-57-8-— 541-73-1— 106-46-7— 95-50-1 95-48-7 108-60-1— 106-44-5— 621-64-7— 67-72-1 98-95-3 78-59-1 88-75-5— 105-67-9- 111-91-1- 120-83-2- 120-82-1- 91-20-3— 106-47-8- 87-68-3— 59-50-7— 91-57-6— 77-47-4— 88-06-2— 95-95-4— 91-58^7— 88-74-4— 131-11-a^ 208-96-8- 606-20-2- 99-09-2— 83-32-9— Phenol bis(2-Chloroethyl)Ether, 2-Chlorophenol, 1,3-Dichlorobenzene_ 1,4-Dichlorobenzene~ 1,2-Dichlorobenzene~ 2-Methy Iphenol, 2,2'-Oxybis(1-Chloropropane)_ 4-Methylphenol ~ N-Nitroso-Di-n-Propyleuaine, Hexachloroethane ]^ — — N i t r o b e n z e n e Isophorone, 2 -Nitrophenol, -2,4-DiaethyIphenol — — b i s (2-Chloroethoxy) Methane, 2,4-Dichlorophenol, --?—1,2,4-Trichlorobenzene_ —aii^rrNaphthalene, s^'^Chloroanil ine_ Hexachlorobutadiene riA,"<!hloro-3 -Methylphenol, ——2--Methylnaphthalene ——Hexachlorocyclopentadiene, 2,4,6-Trichlorophenol ^ 2,4,5-Trichlorophenol ; 2-ChlorcNiaphthalene 2-Nitroaniline Diaethyl Phthalate^ Acenaphthylene, 2,6-Dinitrotoluene 3-Nitroaniline '_ Acenaphthene FORM I SV-1 100758 3/90 IC ORGANICS ANALYSIS DATA SHEET Contract: 68D00159 EPA SANPLE NO. BGL17RE Code: CQMPU Case No.: 15933 SAS No.: SDG No.: BGL09 'Matrix: (soil/water) SOIL Lcib Sample ID: 402888 sample wt/vol: 30.2 (g/mL) fi Lab File ID: G2R02888B08 Level: (low/med) LOW Date Received: 03/04/91 % Moisture: 19 decanted: (Y/N) Ji Concentrated Extract Volume: 500.0 Injection Volume: 2.0(uL) .(UL) Date Extracted: 04/03/91 Date Analyzed: 04/06/91 Dilution Factor: 1.00 GPC Cleanup: (Y/N) CAS NO. pH: 8.0 COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) VG/Kg 51-28-5 100-02-7— 132-64-9— 121-14-2— 84-66-2 7005-72-3- 86-73-7 100-01-6— 534-52-1 86-30-6 101-55-3 118-74-1 87-86-5 85-01-8 120-12-7 86-74-8 84-74-2 206-44-0 129-00-0— 85-68-7 91-94-1 56-55-3 218-01-9— 117-81-7— 117-84-0— 205-99-2— 207-08-9— 50-32-8 193-39-5— 53-70-3 191-24-2— 2,4-Dinitrophenol, 4-Nitrophenol '_ -Dibenzofuran 2,4-Dinitrotoluene, Diethylphthalate, — 4-Chloropheny1-phenylether, Fluorene " 4-Nitroaniline 4,6-Dinitro-2-MethyIphenol • N-Nitrosodiphenylamine (1)" ——4-Broaophenyl-phenylether_^ Hexachlorobenzene -Pentachlorophenol ——Wienanthrene Anthracene ——carhezole_____ •—^-Oi-n-Botylphthalate, >?«fcr»B]iUorenthene '_ :ene ylbenzylphthalate 3 *:«Dtahlorobenz idine, ae(a)Anthracene bis(2-Ethylh^xylIPhthalate Di-h-Octyl Phthalate Benzo(b)Fluoranthene Benzo(k)Fluoranthene Benzo(a)Pyrene, Indimo (1,2,3-cd) Pyrene, Dibenz(a,h)Anthracene^] Benzo(g,h,i)Perylene (1) - Cannot be separated froa Diphenylaaine 100759 .,:> P O R M T <!-w_-v IF SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS EPA SAMPLE NO. BGL17RE fame: COmnyCHaFiRTP Contract: 68D00159 {b code: COMPU Case No.: 15933 SAS No.: SDG No.: BGL09 Matrix: (soil/water) SOIL sample wt/vol: 30.2 (g/mL) G Level: (low/med) LOW % Moisture: H decanted: (Y/N) H Concentrated Extract Volume: 500.0 fuL) tnjection Volume: 2.0(uL) GPC Cleanup: (Y/N) X pH: 8.0 Number TICs found: 20 Lab Sample ID: 402888 Lab File ID: G2R02888B08 Date Received: 03/04/91 Date Extracted: 04/03/91 Date Analyzed: 04/06/91 Dilution Factor: 1.00 CONCENTRATION UNITS: (ug/L or ug/Kg) IZfiZKfi CAS NUMBER ^ i ^ . 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. 13. 14. 15. 16. 17. 18. 19. 20. COMPOUND NAME UNKNOWN HYDROCARBON UNKNOWN ALKYL CYCLOHEXANE UNKNOWN HYDROCARBON UNKNOWN HYDROCARBON 1-METHYLNAPHTHALENE & UNKNOW UNKNOWN UNKNOWN HYDROCARBON UNKNOWN HYDROCARBON UNKNOWN HYintOCARBON UNKNOWN HYDROCARBON UNXNOWN UNKNOWN HYDROCARBON UNXNOWN^HYDROCARBON UNKWDWN HYOBOCARBON HYDROCARBON HYDROCARBON HYDROCARBON HYOSIOCARBON HYDROCARBON UNKNOWN HYDROCARBON RT 7.27 7.62 7.73 7.92 8.22 8.27 8.39 8.54 8.87 9.10 9.45 9.65 9.89 10.19 10.69 10.72 11.19 11.67 12.17 13.15 EST. CONC. 7400 3500 3900 11000 3900 2300 5700 4900 5300 6100 2000 6500 4000 8200 4900 2800 4100 4500 3500 49O0 * ' t 100760 / i FORM I SV-TIC 3/«o IB SEKIVOLAZXLB OBGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. BGL17 / Name: roMPTTCWTat^ifyy Contract: 68D00159 ab Code: COMPU Case No.: 15933 SAS No.: SDG No.: BGr:69 y E X "atrix: (soil/water) SOIL sample wt/vol: 30.4 (g/mL) G^ evel: (low/med) LOW % Moisture: 19 decanted: (Y/N) JL oncentrated Extract Volume: 500.0 Tnjection Volvuae: 2.0(uL) v:»PC Cleanup: (Y/N) X pH: 8.0 CAS NO. COMPOUND Lab Sample ID: 402^88X' Lab File ID: GRD02888B52 Date Received/.- 03/04/91 Date Extrac^d: 03/15/91 Date AnaWzed: 03/24/91 Dilutv^ Factor: 1.0 108-95-2 Phenol_ 111-44-4 bis(2-ClAoroethyl)BCl>er 95-57-8 2-ChloreiUien61 541-73-1 l,3-DichlbD6benz; 106-46-7 1,4-Dichlijtoben/ene 95-50-1 T i , 2-Dical^obeh5fene" 95-48-7 4 2-Methyi|pAi« 108-60-1 Y 2,2 • yONj^ia^l/Chloropropane) 106-44-5 -^ 4-Me4:htIph6n6l 621-64-7 + N-NitrowApl-n-Propylamine, 67-72-1 y—HexachLor^thane 98-95-3 \—lIT^robensene 78-59-1 Hv'fe- 88-75-5 HW-^-Kl^c'bphBnol 105-67-9 \ijf2yl5Olaethylphenol, 111-91-1 ba8rf2-Chloroethoxy') Methane, 120-83-2 'f^KrliiKltZlor^b.Wio\ 120-82-1 -^jfeij i, 4.-Trichlorobenzene, 91-20-3 -afe^t^Naphthalene 106-47-8—-rdHmfc<?b^oroaniline, 87-68-3 -qiJ^^Htarachlorobutadiene 59-50-7—-TAflBp^ej^ll^oro-S^Methylphenol, 91-5 7 -6—yy^'JBay^f jfclthylnaphthalene^^ 77-4 7 -4 --A'- !• • yeararh ] orocyclopentadiene, 88-O6-2// a r AiJ6-Trichlorophenol. 95-95-Vj/ 2,4r4^-inficia:orophenol^ 91-5a;«r 2-Qilogonftpbthalene 88-74^4 ^-—2-Nitroeailine, " l 3 l ? ^ l - 3 ^ Dlj^thyl i»hthalate._ 208/96-8 A q s p a p h | A y l e n e _ ^ ' 606-20-2 2« ^Dinitrotoluene 99-09-2 3-Nitroanil ine, 83-32-9 Acenaphthene FORM I SV-1 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 740 400 400 2100 400 2100 4O0 400 *<M) 2100 40O-" u i a u u u u u u u u u u u u u 1 u u u u u " 1 u 1 u D u u u u tr TH ^ 1 U yt tr-> 3/90 100761 IC LtflLB ORGANICS ANALYSIS DATA SHEET Contract: 69PQ9X5? EPA SAMPLE NO. BGL17 Lab Code: COMPU Case No.: 15933 SAS No, Matrix: (soil/water) SOIL Sample wt/vol: 30.4 (g/mL) fi Level: (low/med) LOW % Moisture: 12 decanted: (Y/N) Ji Concentrated Extract Volume: 500.0 SDG No.: BGL09 Injection Volume: GPC Cleanup: (Y/N) CAS NO. JL^(uL) COMPOUND CENTRATION UNITS: (/g/L or ug/Kg) Vg/Kg 51-28-5 100-02-7 132-64-9 121-14-2 84-66-2 7005-72-3 86-73-7 100-01-^6 534-52-1 86-30-6 101-55-3 118-74-1 87-86-5 85-01-8 120-12-7 86-74-8 84-74-2 206-44-0 129-00-0 85-68-7 91-94-1 56-55-3 218-01-9— 117-81-7— 117-84-0- 205-99-: 207-08-* 50-32- 193-: 53-7( 1913 yl-phenyl ether. Lab Sample ID: 40288J^ Lab File ID: GI(DO2888B52 y Date Received': 03/04/91 Date Ex^acted: 03/15/91 alyzed: 03/24/91 Factor: 1.0 -2,4-Dinitri -4-Nitroph -Dibenzofu: -2,4-Dinit -Die -4-ChJLo -Fluorenl •4-Nitro iDi trp-2-MethyIphenol, iphenylamine (1)~ :<inyl-phenylether_J obenz ene bropkenol Ltylphthalate cyIbenzylphthalate > ^-Dichlorobenzidine, ^1^ Anthracene \ bis(2-Ethylhexyl)Phthalate Dt=^nK?ctyr: PhtheLlate Benzo(b)Fluoranthene Benzo (Ic) Fluoranthene Benzo (a) pyrene. Indeno(1,2,3-cd)Pyrene, Dibenz (a, h) Anthracene^] Benzo(g,h,i)Perylene :9 ;i) - Cannot be separated froa Diphenylaaine FORM I SV-2 100762 3/90 IF >LATII.B ORGANICS ANALYSIS DATA SHEET TElfTATTVEUr IDENTIFIED COMPOUNDS EPA SAMPLE NO. lP<ame: COMPUCHEM.H^^^ Contract: 68D00159 jb code: COMPU Case No.: 15933 SAS No.: SDG No.: BGL09 BGL17 t r i x : ( s o i l / w a t e r ) SOIL imple w t / v o l : 30.4 (g/mL) fi, v e l : (low/med) LOW Moisture: li decanted: (Y/N) Ji ncentrated Extract Volume: 500.0 -j ect ion Volume: 2.0 (uL) r'C Cleanup: (Y/N) X pH: 8.0 jnber TICs found: 20 100763 FORM I SV-TIC 3/90 IB SEMTVOLATIIA ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. BGL16RE Name: COMPUCHSynf** Contract: 68D00159 ab Code: COMPU Case No.: 15933 SAS No.: SDG No.: BGL09 trix: (soil/water) SOIL •ample wt/vol: 1.? (g/mL) G vel: (low/med) MED Moisture: 42 decanted: (Y/N) Ji .-icentrated Extract Volume: 500.0 ^uL) ; I ect ion Volume: 2.0fuL) Lab Sample ID: 402887 =C Cleanup: (Y/N) CAS NO. pH: 7,9 COMPOUND Lab File ID: GRPP2987ft07 Date Received: 03/04/91 Date Extracted: 04/17/91 Date Analyzed: 04/26/91 Dilution Factor: 4.0 CONCENTRATION UNITS: (ug/L or ug/Kg) Vg/Kg •i 108-95-2- 111-44-4 95-57-8 541-73-1 106-46-7 95-50-1 95-48-7 108-60-1 106-44-5 621-64-7 67-72-1 98-95-3 — 78-59-1 88-75-5 105-67-9 111-91-1 120-83-2 120-82-1 91-20-3 106-47-8 87-68-3 59-50-7 91-57-6 77-47-4 88-06-2 95-95-4 - 91-58-7 88-74-4 131-11-3 08-96-8 06-20-2 99-09-2 83-32-9 Phenol —bis(2-Chloroethyl)Ether, —2-Chlorophenol, —1,3-Dichlorobenzene, —1,4-Dichlorobenzene]| —1,2-Dichlorobenzene, —2-Methylphenol_ — 2 , 2 • -Oxybis (1-Chloropropane) __ —4-MethyIphenol —N-Nitroso-Di-n-Propylaaiine_ —Hexachloroethane 1 —Nitrobenzene —Isophorone^ ^2-Nitrophenol, 2,4-DiaethyIphenol, — b i s (2-<hloroethoxy} Methane, —2,4-Dichlorophenol_ —1,2,4-Trichlorobenzene_ ithalener '_ toroaniline Ibrobutadiene Fdro-3-Methy Iphenol, • "t-«»thyinaphthalene. —Hexachlorocyclopentadiene, —2,4,6-TrichX^opRenol " —2,4,5-TrichIorophenol —2-Chloronapbthalene —2-Nitroaniline^ —Diaethyl Phthalate —Acenaphthylene, —2,6-Dinltrotoluene —3-Nitroaniline •—Acenaphthene, FORM I SV-1 53000 53600 53000 53000 53000 53000 53000 53000 53000 53000 53000 53000 53000 53000 53000 53000 53000 53000 53000 5300O 53000 53000 53000 53000 53000 270000, 53000 270000 i 53000 53000 B309» 270000 53000 U u u u u u u u u u u u u u u u u D u u u o- Xh ^ - r- o o 3/90 IC LATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. BGL16RE ySSiiSSlSSMLBSS. Contract: 68D00159 j o d e : COMPU Case No.: 15933 SAS No.: SDG No.: BGL09 ^trix: (soil/water) SOIL Sample wt/vol: 1.3 (g/mL) G Level: (low/med) MED % Moisture: 42 decanted: (Y/N) H Concentrated Extract Volume: 500.0 fuL) Injection Volume: 2.0(uL) GPC Cleanup: (Y/N) X pH: 7.8 CAS NO. COMPOUND Lab Sample ID: 402887 Lab File ID: GRD02887A07 Date Received: 03/04/91 Date Extracted: 04/17/91 Date Analyzed: 04/26/91 Dilution Factor: 4.0 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG 51-28-5 100-02-7 132-64-9 121-14-2 84-66-2 7005-72-3 86-73-7 100-01-6 534-52-1 86-30-6 101-55-3 118-74-1 87-86-5 85-01-8 120-12-7 86-74-8 84-74-2 206-44-0- 129-00- 85-68-7- 91-94-1 56-55-3—i**|i 218-01-9—*- —2,4-Dinitrophenol_ —4-Nitrophenol —Dibenzofuran —2,4-Dinitrotoluene, —Diethylphthalate, —4-Chlorophenyl-phenylether, —Fluorene —4-Nitroaniline —4,6-Dinitro-2-MethyIphenol, —N-Nitrosodiphenylamine (1)' —4-Broaopheny1-phenylether_ —Hexachlorobenzene —Pentachlorophenol —Phenamthrene —Anthracene -Carbazole —Di-n-Butylphthalate, -Fluoranthene Pyrene_ Butylbenzylphthalate, 117-81-7 117-84-0 205-99-2 207-08-9 50-32-8 193-39-5 53-70-3 191-24-2 3,3*-Dichlorobenz idine, "—Benzo (a) Anthracene '_ Chrysene, —bis(2-Ethylhexyl)Phthalate —Di-n-OetyX Phthalate —Benzo(b)Fluoranthene —Benzo (Ic) Fluoranthene —Benzo (a) Pyrene, —Indeno(1,2,3-cd)Pyrene, —Dibenz(a,h)Anthracene^^ —Benzo(g,h,i)Perylene (1) - Czmnot be separated from Diphenylaaine FORM I SV-2 270000 270000 53000 53000 53000 53000 53000 270000 27000O 53000 53000 53000 270000 53000 53000 53000 53000 53000 5500 53000 53000 53000 53000 6300 . 51000 53000 53000 53000 5300a 5300O 53000 D 100765 3/! IF EMTVOLATILB ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS EPA SAMPLE NO. BGL16RE Name: COMPUCHEM.RTP Contract: 68D00159 Lab Code: COMPU Case No.: 15933 SAS No.: SDG No.: BGL09 latrix: (soil/water) SOIL Sample wt/vol: 1.3 (g/mL) G uevel: (low/med) MED Moisture: 42 decanted: (Y/N) Ji Concentrated Extract Volume: 500.0 (nL) njection Volume: 2.0fuL) GPC Cleanup: (Y/N) X pH: 7.8 Number TICs found: 20 402887 Lab Sample ID: Lab File ID: GRD02887A07 Date Received: 03/04/91 Date Extracted: 04/17/91 Date Analyzed: 04/26/91 Dilution Factor: 4.0 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG RT 6.85 7.55 8.22 8.57 8.69 8.82 9.19 9.40 9.74 9.94 10.19 10.45 10.94 10.99 11.40 11.84 12,25 12.67 13.12 13.62 EST. CONC. 390000 420000 580000 390000 290000 690000 440000 640000 320000 800000 360000 1100000 580000 290000 580000 470000 420000 330000 230000 340000 N ,±J Tp jfr J 1 J 1 ^ 1 ^ 1 ^ } J J J J J J ^ I J 1 ^ I ^ I ^ l i ^J> jfl CAS NUMBER 1. 2. 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. 13. 14. 15. 16. 17. 18. 19. 20. COMPOUND NAME UNKNOWN UNKNOWN UNKNOWN UNKNOWN UNKNOWN UNKNOWN UNKNOWN UNKNOWN UNKNOWN UNKNOWN UNKNOWN UNKNOWN UNKNOWN UUSOHN HYDROCARBON HYDROCARBON HYDROCARBON HYDROCARBON HYDROCARBON HYDROCARBON HYDROCARBON HYDROCARBON HYDROCARBON HYDROCARBON HYDROCARBON HYDROCARBON HYDROCARBON HYDROCARBON HYDROCARBON HYDROCARBON HYDROCARBON HYDROCARBON UNXNONN 100766 ?^ FORM I SV-TIC 3/90 ^ i IB EPA SAMPLE NO ^Rb SEISVQ^a^^^ OBGANICS ANALYSIS DATA SHEET Name: ' ' iMI'lHilUJfcMfl' C o n t r a c t : 68D00159 BGIJ;6 y T PLE Lab Code: COMPU Case No.: 15933 SAS No. SDG NO.: i>2_ Matrix: (soil/water) SOIL Sample wt/vol: 30.0 (g/mL) G. Level: (low/med) LOW % Moisture: 41 decanted: (Y/N) Ji Concentrated Extract Volume: 500.0 fuL) Injection Volume: 2.0fuL) GPC Cleanup: (Y/N) X pH: 7.8 CAS NO. COMPOUND ^ Lab Sample ID: 4Qg887 Lab File ID: /GH002887B08 Date Repeivea: 03/04/91 r" ••' y ^Extpacted: 0 4 / 0 2 / 9 1 a l y z e d : 0 4 / 0 6 / 9 1 SiSL Driljtftion F a c t o r : i j :xilU£NTRATION UNITS: 4 i ^ / L o r ug/xg) UG/KG / / 108-95-2 111-44-4 9 5 - 5 7 - 8 - 541-73-1 106-46-7 9 5 - 5 0 - 1 - 9 5 - 4 8 - 7 - 108-60-1 106-44-5 621-64-7 6 7 - 7 2 - 1 - 9 8 - 9 5 - 3 - 7 8 - 5 9 - 1 - 88-75-5- 105-67-9 1 1 1 - 9 1 - 1 120-83-2 1 2 0 - 8 2 - 1 9 1 - 2 0 - 3 - 106-47-8 8 7 - 6 8 - 3 - 5 9 - 5 0 - 7 - 9 1 - 5 7 - 6 - 7 7 - 4 7 - 4 - 8 8 - 0 6 - 2 - 9 5 - 9 5 - 4 - 91-58-7 88-74- 131-11/3 208-98-8 606-20-2 9 9 - 0 9 - 2 - 83-32-9-r Phenol ' E t h e r :ene, izene' snzene' —bi8(2-Chloi —2-Chloroph« —1,3-Dichl< —1,4-Dij —1,2-Dichl^ —2-Methylph\ ^-2,2 ' -^(^cybjw( 1-Chloropropane)_ t4-MethvlNWenol —>I-N —Hex. f-Di - n - P r o p y l amine, roethane izene, m e — V l ^ | | ( e B h e n o l —2yffl6j^aethylphenol •-bzsilgjtOLloroethoxy) Methane ff^Oiffhlorophenoi. I%{)k *4«ffrichlorobenzene, i p l ^ i ^ l e n e . L p r o a n i l i n e i l o r o b u t a d i e n e ^9X9"- 3 -Methy Ipheno 1, »i?*ll^1S]|Xl>naphthalene^ '-*Be¥SOhlerocYclopeatadienej ^-A«4 a 6 c g g i e h l e g e » h e n o l —2r4 tSrtJf iohloroBhenol T-arqMovenaBhthalenei -Dl^B^iyr. fhthalate - •--•=--~A?«»M»>^»l«Be. —2c.4''9aiiiitretoluene — 3 - N i t r o a n i l i n e \ —AiqfliSjphthene 570 570 570 570 570 570 570 570 570 570 570 570 570 570 570 570 570 570 570 570 570 570 S70 170 570 2S00 S70 3S0O » » • D U U U U U U V u u u D U u u u u u U u n D D 0 FORM I SV-1 100767 3/90 IC LATILB ORGANICS ANALYSIS DATA SHEET i: fiOMBIQiQBMSE lab Code: COMPU EPA SAMPLE NO. BGL16 Contract: 68D00159 Case No.: 15933 SAS No.: SDG No.: BGL09 Matrix: (soil/water) SOIL Sample wt/vol: 30.0 (g/mL) G Level: (low/med) LOW % Moisture: 42. decanted: (Y/N) Ji Concentrated Extract Volume: 500.0 fuL) Injection Volume: 2.0(uL) Lab Sample ID: 402887 Lab File IP<^''^ GH002887B08 Date Rec/^ived: 03/04/91 Date^.^^racted: 04/02/91 Dab6 Analyzed: 04/06/91 Dilutioii Factor: l.OO GPC Cleanup: (Y/N) CAS NO. pH: 7.9 COMPOUND 51-28-5 100-02-7 132-64-9 121-14-2 84-66-2 7005-72-3— 86-73-7 100-01-6 534-52-1 86-30-6 101-55-3 118-74-1 87^86-5 85-01-8 120-12-7 86-74-8 84-74-2 206-44-0 129-00-0 85-68-7 91-94-1 56-55-3 218-01-9 117-81-7 117-84-0 205-99-2 207-08-9 50-32-8 193-39-5 53-70-3 191-24-2 -2,4-Dinitrophen -4 -Nitrophenol ^v -Dibenzof urztir^ ^ -2,4-pinitrdtoluene -Diethylphthalate -4-Chl -Fluor -4-NitftoAiCline -4,6-Duk/tro-2-OCethy Iphenol -N-Ni*^odipMnylamine (1) •4 -Broapphen^-pheny 1 ether_ -Hexacnlorobiinz ene nyl-phaftylether. -Pentaobl -Phenanth: -Antbr. enol ONCENTRATItfN tJNITS: (ug/L Or>^/Kg) UG/KG rlphthalate, ithene z y l p h t h a l a t e 'v-Dlchlorobenz i d i n e , ISO Ca) Anthracene ' \ (2-EthylhexylJ^Phthalate L-n-Octyi Phthalate '_ -Benzo(b)Fluoranthene -—Benzo (Ic) Fluoranthene ^ Benzo(a)Pyrene, • Indeno(1,2,3-cd)Pyrene, Dibenz(a,h)Anthracene_[ Benzo(g,h,i)Perylene (1) - Cannot be separated from Diphenylamine FORM I SV-2 2900 2900 570 570 570 570 570 2900 2900 570 570 570 2900 570 570 570 570 570 570 570 570 570 440 400 570 570 570 570 570 570 570 u Py u u u u u u u u u u u u u u u u u u u u D J J u u u u n ILy 100768 f '• J IF EPA SAMPLE NO. JLB ORGANICS ANALYSIS DATA SHEET ""TBriATIVELY IDENTIFIED COMPOUNDS ff^e: GsasssssmdXSS. roMPU Case No.: 15933 Contract: 68D00159 BGL16 Lai) code Matrix: (soil/water) S O U ^ sample wt/vol: 30,Q (g/mL) G^ Level: (low/med) LOW % Moisture: 42 decanted: (Y/N) Jl Concentrated Extract Volxune: 500.0 Injection Volume: 2jii(uL) GPC Cleanup: (Y/N) X pH: Number TICs found: 20 SAS No.: SDG No.: BGL09 / Lab Sample ID: 402887^ Lab File ID: GH002887B08 Date Receivedc^ 03/04/91 Date Ext^^ted: Q4/02/91 100769 FORM I SV-TIC 3/90 IB SEIBVOUOIU ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. 9L Nfl Lab Cc 1 a t r i > Sample L e v e l : % Mois Concer Cnject GPC Cl A 9 n mA- fTOMPnrKBjfepp C o n t r a c t : 68p00159 >de: COMPU C a s e N o . : 15933 SAS N o . : SDG BGL13 N o . : BGL09 :: ( s o i l / w a t e r ) SOIL Lab Seunole I D : 402884 i w t / v o l : 3.0.7 (a/mL) G Lab F i l e I D : GR002884B52 (low/med) LOW D a t e R e c e i v e d : 9 3 / 0 4 / 9 1 j t u r e : 16 d e c a n t e d : (Y/N) N D a t e E x t r a c t e d : 0 3 / 1 5 / 9 1 i t r a t e d E x t r a c t Volume: 5 0 0 . 0 fuL) D a t e A n a l y z e d : 0 3 / 1 9 / 9 1 : i o n Volume: 2 , 0 ( u L ) D i l u t i o n F a c t o r : 1.0 . e a n u p : (Y/N) Y pH: 6 . 9 CONCENTRATION UNITS: CAS NO. COMPOUND f u a / L o r u g / K a ) UG/KG 0 1 0 8 - 9 5 - 2 P h e n o l 1 1 1 - 4 4 - 4 - b i s ( 2 - C h l o r o e t h y l ) E t h e r 9 5 - 5 7 - 8 - 2 - C h l o r o p h e n o l 5 4 1 - 7 3 - 1 1 . 3 - D i c h l o r o b e n z e r i e 1 0 6 - 4 6 - 7 1 , 4 - D i c h l o r o b e n z e n e 9 5 - 5 0 - 1 1 , 2 - D i c h l o r o b e n z e n e 9 5 - 4 8 - 7 2 - M e t h y l p h e n o l 1 0 8 - 6 0 - 1 2 , 2 • - O x y b i s ( 1 - C h l o r o p r o p a n e ) 1 0 6 - 4 4 - 5 4 - M e t h y i p h e n o l 6 2 1 - 6 4 - 7 N - N i t r o s o - D i - n - P r o p y l a m i n e 6 7 - 7 2 - 1 H e x a c h l o r o e t h a n e 9 8 - 9 5 - 3 N i t r o b e n z e n e 7 8 - 5 9 - 1 I s o p h o r o n e 8 8 - 7 5 - 5 — 2 - N i t r o p h e n o l 1 0 5 - 6 7 - 9 2 . 4 - D i a e t h y l p h e n o l 1 1 1 - 9 1 - 1 b i s ( 2 - C h l o r o e t h o x y ) M e t h a n e 1 2 0 - 8 3 - 2 2 . 4 - D i c h l o r o p h e n o l 1 2 0 - 8 2 - 1 - — ~ : r r . — 1 . 2 ^ 4 : - T r i c h l o r o b e n z e n e 9 1 - 2 0 - 3 — • = 3 H B ! ^ - H a f d i t h a l e n e 1 0 6 - 4 7 - 8 — = ^ H i i | i f ^ 4 - C h l o r o a n i l i n e 8 7 - 6 8 - 3 - - r ? d H | | | f r H e x a c h l o r o b u t a d i e n e 5 9 - 5 0 - 7 - — = f l H K 5 ^ - C h l O r o - 3 - M e t h y l p h e n o l 9 1 - 5 7 - 6 : r ~ ~ p « 2 ^ H e t h y l n a p h t h a l e n e 7 7 - 4 7 - 4 — r - r - - H e x a c h l o r o c y c l o p e n t a d i e n e 8 8 - 0 6 - 2 2 ^ 4 . 6 - ^ T r i c h l o r o p h e n o l 9 5 - 9 5 - 4 - 2 . 4 . 5 - T r i c h l o r o p h e n o l 9 1 - 5 8 - 7 • 2 - C h I o r o n a p h t h a l e n e 8 8 - 7 4 - 4 2 - H i t r o a n i l i n e 1 3 1 - 1 1 - 3 D i a e t h v l P h t h a l a t e 2 0 8 - 9 6 - 8 — ^ A c e n a p h t h y l e n e 606^20-2.-r— 2 . 6 - D l n i t r o t o l u e n e ._, 9 9 - 0 9 - 2 3 - N i t r o a n i l i n e _ , 8 3 - 3 2 - 9 A c e n a p h t h e n e FORM I SV-1 380 380 380 380 380 380 380 380 380 380 . 380 380 380 380 380 380 380 380 380 380 380 380 380 380 3 8 0 aooo ^ 3 3 8 0 ( 1 ; 2 0 0 0 1 ' ^ O 3 8 0 j " <a38Ciu ri^sois ^^oor^ ?o^ - 1 0 0 7 7 0 uy ul ul u 1 u 1 u 1 ujT u u D O u u u u u u u u u Xf o u u taa 3/ • ' 9 0 IC tLATXLX ORGANICS ANALYSIS DATA SHEET EPA SAMPLE UOm (me: S^SSSSS^JPSt ^ b Code: coMPU Case No.: 15933 BGL13 C o n t r a c t : 68D00159 SAS No.: SDG No.: BGL09 Matrix: (soil/water) SOIL Sample wt/vol: 30.7 (g/mL) fi Level: (low/med) LOW %^ Moisture: 1& decanted: (Y/N) Ji Concentrated Extract Volume: 500.0 fuL) Injection Volume: 2.0fuL) GPC Cleanup: (Y/N) X pH: 6.9 CAS NO. COMPOUND Lab Sample ID: 402884 Lab File ID: GR002884B52 Date Received: 03/04/91 Date Extracted: 03/15/91 Date Analyzed: 03/19/91 Dilution Factor: . 1.0 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG 51-28-5— 100-02-7- 132-64-9- 121-14-2- 84-66-2 7005-72-3 86-73-7— 100-01-6- 534-52-1- 86-30-6— 101-55-3- 118-74-1- 87-86-5— 85-01-8— 120-12-7- 86-74-8— 84-74-2— 206-44-0- 129-00-0 85-68-7- 91-94-1- 56-55-3 — 218-01-9- 117-81-7- 117-84-0- 205-99-2- 207-08-9- 50-32-8— 193-39-5- 53-70-3— 191-24-2- 2,4-Dinitrophenol, 4-Nitrophenol '_ Dibenzofurem 2,4-Dinitrotoluene, Diethylphthalate, 4-Chlorophenyl-phenylether_ Fluorene 4 - N i t r o e u i i l i n e 4,6-Dinitro-2-Methylphenol, N-Nitrosodiphenyleuaine (1)^ 4 -Broaophenyl -pheny lether_]| Hexachlorobenzene — Pentachlorophenol —Phenanthrene ———Anthracene Carbazole —rrr——Di-n-Butylphthal ate, ••riffwrr-Fluoranthene ]] r.-Pyrene_ tyIbenzylphthalate, 3,3'-Dichlorobenzidine, Benzo (a) Anthracene '_ Chrysene, .-.,^—bis (2-Ethylhexyl) Phthalate Di-n-Octyl-Phthalate I — — Benzo(b)Fluoranthene — — — B e n z o (k) Fluoranthene _, — — B e n z o (a) Pyrene, -Indeno(1,2,3-cd)Pyrene_ — — D i b e n z (a, h) Anthracene^^ Benzo(g,h,i)Perylene (1) - Cannot be separated froa Diphenylaaine FORM I SV^2 100771 3/90 _^ ANALYSIS DATA SHEET IDENTIFIED COMPOUNDS EPA SAMPLE NO. BGL13 15933 contract: $SDQQ159 SAS No.: SDG No.: BGL09 sample wt/vol: 3Q-7 (g/mL) G Level: (low/med) LOW % Moisture: Ifi decanted: (Y/N) Ji Concentrated Extract Volume: 500.0 fuL) Injection Volume: 2JLII(UL) GPC Cleanup: (Y/N) X pH: 6.9 Number TICs found: 27 Lab Sample ID: 402884 Lab File ID: GR002884B52 Date Received: 03/04/91 Date Extracted: 03/15/91 Date Analyzed: 03/19/91 Dilution Factor: 1.0 CONCENTRATION UNITS: (ug/L or ug/Kg) VG/Kg 4 4 CAS NUMBER 1. 2. 3. .4. 5. 6. 7. 8. 9. 10. 11. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. COMPOUND NAME UNKNOWN SOLVENT CONTAMINANT SOLVENT CONTAMINANT SOLVENT CONTAMINANT UNKNOWN UNKNOWN BLANK CONTAMINANT ALDOL ALDOL ALDOL UNKNOWN UNKNOWN DIO-PYRENE- UNXNOWN UNKNOWN HYDROCARBON HYDROCARBON UNXNONN UNKNOWN UNKNOWN UNKNOWN UNKNOWN UNKNOWN UNKNOWN HYDROCARBON UNKNOWN RT 5.22 5.43 5.52 5.62 5.72 6.53 6.75 6.98 7.17 7.53 8.40 16.69 18.39 18.62 19.75 20.14 20.37 21.64 27.14 29.56 30.92 33.77 8.22 9.62 15.14 25.81 29.07 EST. CONC. 500 14000 120 540 540 890 620 540 620 660. 390 230 1100 700 470 230 190 120 970 2300 1300 1200 350 230 120 470 660 II • f g ' ' ^ l: J J J J J J J I 1 0 0 7 7 2 FORM I SV-TIC 3/90 IB SEMIVOLATILB ORGANICS ANALYSIS DATA SHEET Contract: 68D00159 EPA SAMPLE NO. Name: SSJSSSSSJEEJBt i.ab Code: COMPU Case No.: 15933 SAS No.: itrix: (soil/water) SOIL Sample wt/vol: 30.4 (g/mL) fi. BGL14 SDG No.: BGL09 •vel; (low/med) LOW Moisture: .!§. decanted: (Y/N) Ji v^ncentrated Extract Volume: 500.0 (uL) jection Volume: 2.0(uL) Lab Sample ID: 402885 Lab File ID: GR002885B52 Date Received: 03/04/91 Date Extracted: 03/15/91 Date Analyzed: 03/20/91 Dilution Factor: 1.0 PC Cleanup: (Y/N) I pH: 9,1 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-95-2 111-44-4 95-57-8 541-73-1 106-46-7 9 5 - 5 0 - 1 95-48-7 108-60-1 106-44-5 621-64-7 67-72-1 98-95-3 7 8 - 5 9 - 1 88-75-5 105-67-9 111-91-1 120-83-2 120-82-1 91-20-3 106-47-8 87-68-3 59-50-7 91-57-6 77-47-4 88-06-2 95-95-4 91-58-7 88-74-4 131-11-3 |2 08-96-8 606-20-2 99-09-2 83-32-9 ——Phenol -bis(2-Chloroethyl)Ether, •2-Chlorophenol, 1,3-Dichlorobenzene, —1,4-Dichlorobenzene' —1,2-Dichlorobenzene' —2-Methylphenol, -2,2' -Oxybis (l-Chloroprop«me) _ -4-Methylphenol "2 -N-Nitroso-Di-n-Propylamine -Hexachloroethane -Nitrobenzene •Isophorone, 2-Nitrophenol 2,4-Diaethylphenol, -bis(2-Chloroethoxy)Methane, -2,4-Dichlorophenol_ ,2r4-Trichlorobenzene, lene oroanillne it^ilOrobutadiene oro-3-MethyIphenol, 3?4fethylnaphthal ene. -Hexachlorocyclopentadiene_ -2,4,6-Triciilor0phenol_ 1 -2,4,5-Trichlorophenol -2-Chl<Mronaphthalene__ -2-Nitroaniline -Diaethyl Phthalate, -Acenai^thylene. •2,6-Dinitrotoluene, —3-Nitroaniline —Acenaphthene, m o o FORM I SV-1 3/90 IC ^EMIVOUkTILE GSGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. Lab Name: SSiSSSSS^LXSS. il Lab Code: COMPU Case N o . : 15933 BGL14 Contract: 69P901?9 SAS No.: SDG No.: BGL09 Matrix: (soil/water) SOIL Sample wt/vol: 30.4 (g/mL) fi. Level: (low/med) LOW % Moisture: _1£ decanted: (Y/N) Ji Concentrated Extract Volume: 500.0 fuL) Injection Volume: 2.Q(uL) GPC Cleanup: (Y/N) CAS NO. pH: 8.1 COMPOUND Lab Sample ID: 402885 Lab File ID: GR002885B52 Date Received: 03/04/91 Date Extracted: 03/15/91 Date Analyzed: 03/20/91 Dilution Factor: 1.0 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG 51-28-5 100-02-7 — 132-64-9— 121-14-2 — 84-66-2 7005-72-3- 86-73-7 100-01-6— 534-52-1 86-30-6 101-55-3— 118-74-1— 87-86-5 85-01-8 120-12-7— 86-74-8 84-74-2 206-44-0— 129-00-0— 85-68-7 91-94-1 56-55-3 218-01-9— 117-81-7— 117-84-0— 205-99-2— 207-08-9— 50-32-8 193-39-5— 53-70-3 191-24-2— 2,4-Dinitrophenol 4-Nitrophenol [ Dibenzofuran 2,4-Dinitrotoluene. Diethylphthalate, 4-Chlorophenyl-phenylether, Fluorene 4 - H i t r o a n i l i n e 4 ^ 6-Dinitro-2-MethyIphenol. N-Nitrosodiphenylauaine (1)" 4-Broaophenyl-phenylether_^ ——Hexachlorobenzene Pentachlorophenol ^ e n a n t h r e n e Anthracene — Carbazole •—Di-n-Butylphthalate, •TTts^r-Fluoranthene ~_ •Byrene, tty Ibenzylphthalate, 3'-Dichlorobenz idine, "Mmzo (a) Anthracene '_ -Chrysene, bi«U-Ethy Ihexyl) Phthalate Dt-n-Octyar-a>tfaalate Benzo(b)Fluoranthene —Benzo (k) Fluoranthene —Benso CalPyrene, Indeno(1,2,3-cd)Pyrene, Dibenz (a,h) Anthracene_J| Benzo(g,h, i) Perylene 1) - Cannot be separated.froa DiphenylaainiT FORM I SV-2 100774 IF SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS EPA SAMPLE NO. BGL14 Name: fiOlffinfflBLSTE Contract: 68D00159 Lab code: COMPU Case No.: 15933 SAS No.: SDG No.: BGL09 Matrix: (soil/water) SOIL Sample wt/vol: 30.4 (g/mL) fi Level: (low/med) LOW % Moisture: l§, decanted: (Y/N) N Concentrated Extract Volume: 500.0 (xxL) Injection Volume: 2.0(uL) GPC Cleanup: (Y/N) X pH: 8.1 Number TICs found: 25 Lab Sample ID: 402885 Lab File ID: GR002885B52 Date Received: 03/04/91 Date Extracted: 03/15/91 Date Analyzed: 03/20/91 Dilution Factor: 1.0 CONCENTRATION UNITS: (ug/L or ug/Kg) VG/Kg CAS NUMBER f 2. 5. 6. 7. 8. 9. 10. 11. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. w COMPOUND NAME SOLVENT CONTAMINANT ALDOL UNKNOWN OXYGENATED ALKANE SOLVENT CONTAMINANT BLANK CONTAMINANT UNKNOWN ALDOL UNKNOWN UNKNOWN UNKNOWN UNKNOWN UNKNOWN UNKNOWN UNXNOWN UNXNOWN UNXNONN DIO-PYRENB- UNKNOWN ^ UNKNOWN UNKNOWN HYDROCARBONS UNKNOWN HYDROCARBONS RT 5.30 5.53 5.63 5.77 6.70 6.78 6.9T 8.39 11.10 11.14 12.09 13.02 14.27 14.72 15.50 15.57 16.67 16.97 17.65 18.32 ia.39- 24.97 25.16 13.87 16.24 100775 FORM I SV-TIC 3/90 IB J U K I V O L A T I I B ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. • > Name: SS^SSSSaSSUBl. Lab Code: COMPU BGL15 Contract: 68D00159 Case No.: 15933 SAS No.: SDG No.: BGL09 iatrix: (soil/water) SOIL Lab Sample ID: 402886 Sample wt/vol: 1.1 (g/mL) G_ Lab F i l e ID: G2R02886A21 iCvel: (low/med) MED i Moisture: IS. decanted: (Y/N) M oncentrated Extract Volume: 500.0 "njection Volume: 2.0(uL) .(UL) Date Received: 03/04/91 Date Extracted: 04/18/91 Date Analyzed: 04/25/91 Dilution Factor: 1.00 ;PC Cleanup: (Y/N) CAS NO. pH: 8.1 COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) VG/KG 108-95-2 111-44-4 95-57-8 541-73-1 106-46-7 95-50-1 95-48-7 108-60-1 106-44-5 621-64-7 67-72-1 98-95-3 78-59-1 88-75-5 105-67-9 111-91-1 120-83-2 120-82-1 91-20-3 106-47-8 87-68-3 59-50-7 91-57-6 77-47-4 88-06-2 95-95-4 91-5S-7 88-74-4— 131-11-3^- 208-^0*6 606- 99-09-2 83-32-9- — P h e n o l -bis(2-Chloroethyl)Ether. -2-Chlorophenol. -1,3-Dichlorobenzene -1,4-Dichlorobenzene -1,2-Dichlorobenzene -2-MethyIphenol 2,2'-Oxybis(1-Chloropropane)_ 4-Methylphenol -N-Nitroso-Di-n-Propylamine. -Hexachloroethane ] -N itrobenzene -Isophorone, 2-N^roi)hMtol 2,4-H}iBet^lphenol. -bis(2'-€hloroethoxy) Methane -2, 4H)icML«urophenol. ', 24 4«'^nrii^lorobenzena, ithalene oroaniline iShlorobutadiene _ ioro-3-Methylphenol -t-iihthylnaphthalene -HeaaehloroOyelopentadiene -2,4,.6<'«T)riekl«rophettol_ '_ -2,4 rO-Trichlerephenol 2-Gblerona|^tiM&lene 2-Ntt«eeniti'n» ^ -DiaetHyP Phthalaga -Acen^pfi«hy<liM» 11000 11000 11000 11000 11000 11000 11000 11000 11000 11000 11000 11000 11000> 11000 11000 11000 ' 11000 11000 11000 llOOOr^ 11000 11000 iiopo 11000on 55044: —2,6-D£»£tretoluene —3-Nitroanillna —Acenaphthene^. S ^ U D D U U U a u u u TJ O! XT Ui U' O O u; u ut 11000 a rj 9 ^1 If I tr- FORM I SV-1 1 0 0 7 7 6 2/m 1 IC SBNIVOLATILB OBGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. r name: Lab Code: COMPU iKXP Case No.: 15933 Matrix: (soil/water) SOIL Sample wt/vol: 1.1 (g/mL) G Level: (low/med) MED % Moisture: 13, decanted: (Y/N) N Concentrated Extract Volume: 500.0 (uL) Injection Volume: 2.0fuL) GPC Cleanup: (Y/N) i pH: 8.1 CAS NO. COMPOUND BGL15 Contract: $9D0Q159 SAS No.: SDG No.: BGL09 Lab Sample ID: 402886 Lab File ID: G2R92996A23. Date Received: 03/04/91 Date Extracted: 04/18/91 Date Analyzed: 04/25/91 Dilution Factor: 1.00 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG 51-28-5 100-02-7 132-64-9 121-14-2 84-66-2 7005-72-3 86-73-7 100-01-6 534-52-1 86-30-6 101-55-3 118-74-1 87-86-5 85-01-8 120-12-7 86-74-8 84-74-2 206-44-0—-- 129-00-0 85-68-7 91-94-1- 56-55-3- 218-01-9- 117-81-7 117-84-0 205-99-2 207-08-9 50-32-8 193-39-5 53-70-3 191-24-2 —2,4-Dinitrophenol. —4 -Nitrophenol [ —Dibenzofuran —2,4-Dinitrotoluene, —Diethylphthalate, —4-Chlorophenyl-phenylether, —Fluorene ' 4-Nitroaniline —4,6-Dinitro-2-Methy Iphenol —N-Nitrosodiphenylaaine (1) —4-BroBopfaenyl-phenylether —Hexachlorobenzene —Pentachlorophenol —Fhenan4^b;¥«ne —Anthracene —GarlMSole «i-'«i-Butylphthalate, ->ra.a0ranthene ^ •fVrene_ Ibenzylphthalate, [, 3;* 'Hdichlerobenzidine, (a) Anthracene '_ -bis(2-Ethylhexyl)Phthalate -ffl-^hr-OCt^L_Bithalate -Benzo(b)Fluoranthene -Benzo(k) Fluoranthene -Benzo (a) Pyrene, —Indeno (1,2,3-cd) Pyrene, —Dibenz (a ^ h) Anthracene_^ —Benzo (g, h, i) Perylene (1) - Cannot be separated froa Diphenylaaine FORM I SV-2 55000 55000 11000 llOOO 11000 11000 11000 55000 55000 11000 11000 11000 55000 11000 11000 11000 11000 11000 11000 11000 11000 11000 IIQOO 1100 11000 11000 11000 11000 llOOO 11000 llOOO ^ 100777 '6M IF SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVBLY IDENTIFIED COMPOUNDS EPA SAMPLE NO. Name: Lab Code: COMPU BGL15 Case No.: 15933 latrix: (soil/water) SOIL Sample wt/vol: 1.1 (g/mL) fi evel: (low/med) MED \ Moisture: 18. decanted: (Y/N) Ji oncentrated Extract Volume: 500.0 fuL) ejection Volume: 2.0(uL) PC Cleanup: (Y/N) X pH: 8.1 -mber TICs found: 20 Contract: 68D00159 SAS No.: SDG No.: BGL09 Lab Sample ID: 402896 Lab File ID: G2RQ2886A21 Date Received: 03/04/91 Date Extracted: 04/18/91 Date Analyzed: 04/25/91 Dilution Factor: 1.00 CONCENTRATION UNITS: (ug/L or ug/Kg) VG/Kg 100778 CAS NUMBER 3 ^ ' m 4. 5. 6. 7. 8. 9. 10. 11. >. .3. L4. i . i . .7. • u. COMPOUND NAME UNKNOWN HYDROCARBON UNKNOWN HYDROCARBON UNKNOWN HYDROCARBON UNKNOWN HYDROCARBON UNKNOWN HYDROCARBON UNKNOWN HYDROCARBON UNKNOWN HYDROCARBON UNKNOWN HYDROCARBON UNKNOWN HYIWOeARBON UNKNOWN HYDROCARBON UNKNOWN HYDROCARBON UNKNOWN HYOftOCARiSON UNKNOWN HYDROCARBON TnncMQim: Hvnaor^PBnM UNXHam HYDROCARBON UNB^HP^ HYl»OCARBON UNBJ^HlPBnFBKOCARBON U ^ ^ K nrOROCARBON UKQHPKLHTHIOCARBON UNXMONK HYOBOCARBON RT 7.12 7.98 8.55 8.79 9.35 9.54 9.95 10.24 10.67 10.92 11.20 11.55 12.15 12.19 12.65 12.72 13.27 13.80 14.32 14.80 EST. CONC. 100000 130000 72000 170000 91000 180000 120000 200000 58000 210000 110000 310000 190000 120000 47000 170000 400000 350000 270000 140000 ( = f JA/ ^ \ J J J J J J J J ^ J J J J J J J J J , i ; . . C • ^ FORM I SV-TIC 1 1 { -^1 '^ ^,~- « /A 3/90 IB SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. BGL23 Lab Name: '"'^MFTOnKiFT^ Contract: 68D00159 Lab Code: COMPU Case No.: 15933 SAS No.: SDG No.: BGL09 Matrix: (soil/water) SOIL Sample wt/vol: 30.3 (g/mL) fii Level: (low/med) LOW % Moisture: 9 decanted: (Y/N) H Concentrated Extract Volume: 500.0 Injection Volume: 2.Q(uL) .(UL) GPC Cleanup: (Y/N) CAS NO. pH: 7,$ COMPOUND Lab Sample ID: 402889 Lab File ID: GRJ02389B07 Date Received: 03/04/91 Date Extracted: 03/28/91 Date Analyzed: 04/08/91 Dilution Factor: 1.0 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG 108-95-2 Phenol 111-44-4 bis (2-Chloroethyl) Ether 95-57-8 2-Chlorophenol 541-73-1 1,3-Dichlorobenzene 106-46-7 1,4-Dichlorobenzene 95-50-1 1,2-Dichlorobenzene 95-48-7 2-Methylphenol 108-60-1 2,2'-Oxybis (1-Chloropropane) 106-44-5 : 4-Methylphenol 621-64-7 N-Nitroso-Di-n-Propylamine 67-72-1 Hexachloroethane 98-95-3 Nitrobenzene 78-59-1 Isophorone 88-75-5 2-Nitrophenol 105-67-9 2,4-Diaiethy Iphenol 111-91-1 bis (1-Chloroethoxy) Methane 120-83-2 2,4-Dlchlorophenol 120-82-1 •^-—1,2,4-Trichlorobenzene 91-20-3 JgT^-Naphthalene 1 0 6 - 4 7 - 8 — « : 4-Chloroaniline 87-68-3 ' y ' -Hexachlorobutadiene 59-50-7 - — 4-Chloro-3-Methy Iphenol 91-57-6 2-MethYlnaphthalene 77-47-4 Hexachlorocyclopentadiene 88-06-2 2,4,6-Trichlorophenol 95-95-4 2.4,5-Trichlorophenol 91-58-7 2-Chloronapbthalene 88-74-4 2-Nitroanillna 131-11-3 Diaethvl Phthalate 208-96-8 Acenaphthylene 606-20-2 2,6-Dinitrotoluene 99-09-2 3-Nitroaniline 83-32-9 Acenaphthene 360 360 360 360 360 360 360 360 360 360 360 360 360 360 360 360 360 360 360 360 360 360 360 360 360 1800 360 1800 360 .. 360 360 1800 360 U p u ^ 1 u u u u u u u u u u u u u u u u u u 1 u u u u u 0 D D 0 0 u di u £> r^ r-- Ol r- o o H FORM I SV-1 3/90 IC ^ ^ V O L A T I L B OBGANICS ANALYSIS DATA SHEET y Aat&e: COMPUCHEM.RTP Contract: 68D00159 EPA SAMPLE NO. BGL23 3 Code: COMPU Case No.: 15933 SAS No.: SDG No.: BGL09 itrix: (soil/water) SOIL Lab Sample ID: 402889 iple wt/vol: 30,3 (g/mL) fi_ Lab File ID: GRJ02889B07 i v e l : (low/med) LOW l o i s t u r e : d e c a n t e d : (Y/N) Ji -icentrated E x t r a c t Volume: 500.0 I j e c t i o n Volume: 2.0(uL) .(UL) Cleanup: (Y/N) CAS NO. pH: 7.5 COMPOUND Date Received: 0 3 / 0 4 / 9 1 Date E x t r a c t e d : 0 3 / 2 8 / 9 1 Date Analyzed: 0 4 / 0 8 / 9 1 D i l u t i o n F a c t o r : 1.0 CONCENTRATION UNITS: (ug/L o r ug/Kg) Jlfi/KS 51-28-5 2,4-Dinitrophenol 100-02-7 4-Nitrophenol 132-64-9 Dibenzofuran 121-14-2 2,4-Dinitrotoluene 84-66-2 Diethylphthalate 7005-72-3 4-Chlorophenyl-phenylether 86-73 -7 Fluorene 100-01-6 4-Nitroaniline 534-52-1 4,6-Dinitro-2-Methylphenol 86-30-6 N-Nitrosodiphenylamine (1) 101-55-3 4-Broaopheny 1-pheny lether 118-74-1 -^ Hexachlorobenzene 87-86-5 Pentachlorophenol 85-01-8 ^enanthrene 120-12-7 Anthracene 86-74-8 -Carbazole 84-74-2 «r;Oi-n-Butylphthalate 206-44-0 -ii£^nuoranthene 129-00-0 ^^feAvrene 85-68-7 -^IpBBatvlbenzylphthalate 91-94-1 -^';f»B«3 • -Dichlorobenzidine 56-55-3 —Benso (a) Anthracene 218-01-9 Chrysene 117-81-7 bis (2-Bthy Ihexyl) Phthalate 117-84-0 Di-n-Octyl Phthalate 205-99-2 Benzo (b) Fluoranthene 207-08-9 —Benzo (k) Fluorsuithene 50-32-8 — B e n z o (al Pyrene 193-39-5 Indeno (1.2,3-cd) Pyrene 53-70-3 Dibenz (a,h) Anthracene 191-24-2 Benzo (a.h.i) Perylene (1) - Cannot be separated froa Diphenylamine 1800 1800 360 360 360 360 360 1800 1800 360 360 360 660 360 360 360 360 360 360 ' 360 360 360 360 360 360- : 360s 2 360c, i 360-: i 360£7 360 ~ 360 u Z^ u ' u u u u u u u u l\y u ^ u u u u u u u u u a ,u y . TrfU z. 100780 IF yivOLATILE ORGANICS ANALYSIS DATA SHEET y/^TENTATTTOJf IDENTIFIED COMPOUNDS / • ^n^f^jcHEM.RTP C o n t r a c t : 68D00159 EPA SAMPLE NO. BGL23 ^ode: COMPU Case N o . : 15933 SAS N o . : i t r i x : ( s o i l / w a t e r ) SOIL iple w t / v o l : 30.3 (g/mL) fi ivel: (low/med) LOW . l o i s t u r e : 2 d e c a n t e d : (Y/N) fi i c e n t r a t e d E x t r a c t Volume: 500.0 fuL) i j e c t i o n Volume: 2JJ1(UL) : Cleanup: (Y/N) X pH: 7.5 b e r TICs found: 26 SDG No.: BGL09 Lab Sample ID: 402889 Lab File ID: GRJ02889B07 Date Received: 03/04/91 Date Extracted: 03/28/91 Date Analyzed: 04/08/91 Dilution Factor: 1.0 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG ^ A S NUMBER w~ 2 . 3 . 4 . 5 . 6 . 7 . 8 . 9 . 0 . x l . 1 2 . 3 . 4 . 1 5 . r6. 7 . 1 8 . 1 9 . 0 . - 1 . 2 2 . : 3 . ;4. • COMPOUND NAME SOLVENT CONTAMINANT UNKNOWN UNKNOWN ALDOL ALDOL UNKNOWN ALDOL ALDOL UNKNOWN UNKNOWN UNKNOWN UNKNOWN UNKNOWN UNXNONN UIQUBMN uifl(fipBl UlolpiBi UNXJiblRI DIO PYRENE UNKNOWN UNKNOWN HYDROCARBON- UNKNOWN UNKNOWN UNKNOWN UNKNOWN UNKNOWN RT 4.67 5.22 5.28 5.38 5.48 5.53 5.75 5.88 5.95 6.98 7.88 7 . 9 5 8.62 9.42 9.45 9.57 10.12 11.19 12.57 14.95 16.82 19.42 23.12 26.32 26.42 2 7 . 4 1 EST. CONC. 510 510 760 290 760 - 330 760 ^ 440 . 400 330 290 180 150 290 330 730 400 l l O 1500 . 800 250 7 3 0 870 1000 360 870 Q - ^ it SS ^ jy A J J J J ^ h ^hJ ^ j j ' J ^' J J J J J / J N t r* " • ' • 1 0 0 7 8 1 FORM I SV-TIC 3/90 IB SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. lb Name: cowpnCHEM.WTP .ab Code: COMPU Case No.: 15933 BGL18 C o n t r a c t : 68D00159 SAS No.: SDG No.: BGLOl I t r i x : ( s o i l / w a t e r ) WATER Sample w t / v o l : 1000 (g/mL) JfL. - ^ v e l : (low/med) LOW M o i s t u r e : ' d e c a n t e d : (Y/N) Concentrated E x t r a c t Volume: 1000 i j e c t i o n Volume: 2.0(uL) 3PC Cleanup: (Y/N) Ji pH: _ CAS NO. COMPOUND .(UL) Lab Sample ID: 402871 Lab File ID: GH002871A08 Date Received: 03/04/91 Date Extracted: 03/08/91 Date Analyzed: 03/12/91 Dilution Factor: 1.0 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L 108-95-2 111-44-4 95-57-8 541-73-1 106-46-7 95-50-1 95-48-7 108-60-1 106-44-5 621-64-7 67-72-1 98-95-3 78-59-1 88-75-5 105-67-9 111-91-1 120-83-2 120-82-1 91-20-3 106-47-8 87-68-3 59-50-7 91-57-6 77-47-4 88-06-2 95-95-4 91-58-7 88-74-4 131-11-3 208-96-a 606-20-2 99-09-2 • 83-32-9 Phenol —bis (2-Chloroethyl) Ether, —2-Chlorophenol —1,3-Dichlorobenzene_ —1,4-Dichlorobenzene] —1,2-Dichlorobenzene] —2-Methylphenol. —2,2•-Oxybis(1-Chloropropane) —4-Methylphenol —N-Nitroso-Di-n-Propyleunine, —Hexachloroethane —Nitrobenzene —Isophorone, 2-Nitrophenol 2,4-Diaethylphenol. -bis (2'!*Chloroethoxy) Methane, -2,4-Dichlorophenol. -1,2,4-Trichlorobenzene Naphthalene 4-Chloroaniline achlorobutadiene 4-€toloro-3-HethyIphenol —2-Hethylnaphthalene -Hexachlorocyclopentadiene, -2,4, fr-Tr^chlerephenol '_ -2,4,5-Trichlorophenol -2-€hlwronaBa>thalene - 2 - N i t x o a n i l i n * —Diaethyl F&thalate, —Acena^thylene; — 2 , S-Dliiitrotoluene — 3 -Nitroaniline [ —Acenaphthsne,2 FORM I SV-1 ; . 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 50 10 50 10 10 10 50 10 100782 1 3/90 *• - IC SEMIV0LATII2 ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. BGL18 &b Name: COMPUCHEM.gfP Contract: 68D00159 Lab Code: COMPU Case No.: 15933 SAS No.: . SDG No.: BGLOl atrix: (soil/water) WATER Sample wt/vol: 1000 (g/mL) MJi, ,evel: (low/med) LOW " Moisture: decanted: (Y/N) Concentrated Extract Volume: 1000 Injection Volume: 2.0(uL) GPC Cleanup: (Y/N) Ji pH: _ CAS NO. COMPOUND .(UL) Lab Sample ID: 402871 Lab File ID: GH002871A08 Date Received: 03/04/91 Date Extracted: 03/08/91 Date Analyzed: 03/12/91 Dilution Factor: 1.0 CONCENTRATION UNITS: (ug/L or ug/Kg) Vg/L 51-28-5 100-02-7 132-64-9 121-14-2 84-66-2 7005-72-3 86-73-7 100-01-6 534-52-1 86-30-6 101-55-3 118-74-1 87-86-5 85-01-8 120-12-7 86-74-8 84-74-2 206-44-0 129-00-0— 85-68-7— 91-94-1— 56-55-3 218-01-9 117-81-7 117-84-0 205-99-2 207-08-9 50-32-8 193-39-5 53-70-3 191-24-2 2,4-Dinitrophenol, 4-Nitrophenol Dibenzofuran 2,4-Dinitrotoluene, —-Diethylphthalate, 4-Chlorophenyl-phenylether, Fluorene ] 4-Nitroaniline 4,6-Dinitro-2-Methylphenol. N-Nitrosodiphenylamine (1)[ 4-Bromopheny1-phenylether_ Hexachlorobenzene ___; Pentachlorophenol Phenanthrene Anthracene Carbazole Di-n-Butylphthalate, —Fluoranthene . —Pyrene, -Butylbenzylphthalate, 3,3'-Dichlorobenz idine, Benzo(a)Anthracene -—Chrysene, bis(2-Ethylhexyl)Phthalate, Di-n-Octyl^Phthalate Benzo(b)Fluoranthenej Benzo (k) Fluoranthene .__ Benzo (a) Pyrene, Indeno(1,2,3-cd)Pyrene, Dibenz(a,h)Anthracene_ Benzo (g,h,i)Pe]::ylene (1) - Cannot be separated froa Diphenyl2unine FORM I SV-2 100783 Q 3/90 -n EPA SAMPLE NO. — - If SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS BGL18 Name: f^OMFTHTTW• B ? Contract: 68D00159 .ab Code: COMPU Case No.: 15933 SAS No.-J SDG No.: BGLOl itrix: (soil/water) WATER ;ample wt/vol: 1000 (g/mL) J!Ii_ svel: (low/med) LOW Moisture: decanted: (Y/N) roncentrated Extract Volume: 1000 ijection Volume: 2.0(uL) sFC Cleanup: (Y/N) Ji pH: _ :(UL) Lab Sample ID: 402871 Lab File ID: GH002871A08 Date Received: 03/04/91 Date Extracted: 03/08/91 Date Analyzed: 03/12/91 Dilution Factor: X.0 - dumber TICs found: CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L CAS NUMBER 0- COMPOUND NAME DIO-PYRENE RT 13.39 EST. CONC. 48 Q ; ^'^ ^ FORM I SV-TIC *A 1007S4 :^A 3/90 IB I ^ — SEMTVOLATILB ORGANICS ANALYSIS DATA SHEET ^Rc EPA SAMPLE NO. BGL19 lame: COMPTTCHKM.lag Contract: 68D00159 ID Code: COMPU Case No.: 15933 SAS No.: SDG No.: BGLOl crix: (soil/water) WATER ample wt/vol: 1000 (g/mL) ML • / e l : (low/med) LOW Moisture: decanted: (Y/N) -.ncentrated Extract Volume: 1000 jection Volume: 2.0fuL) PC Cleanup: (Y/N) N pH: _ CAS NO. COMPOUND .(UL) Lab Sample ID: 402872 Lab File ID: GH002872A08 Date Received: 03/04/91 Date Extracted: 03/08/91 Date Analyzed: 03/12/91 Dilution Factor: 1.0 CONCENTRATION UNITS: (ug/L or ug/Kg). UG/L 108-95-2 111-44-4 9 5 - 5 7 - 8 — — 541-73-1 106-46-7 95-50-1 95-48-7 108-60-1 - 106-44-5 621-64-7 67-72-1 98-95-3 78-59-1—r— 88-75-5 105-67-9 111-91-1 120-83-2 120-82-1 91-20-3 106-47-8 87-68-3 59-50-7 91-57-6 77-47-4 88-06-2 95-95-4 91-58-7 88-74-4 131-11-3 208-96-8 606-20-2 99-09-2 83-32-9 — P h e n o 1 — b i s (2-Chloroethyl) Ether, 2-Chlorophenol, —1,3-Dichlorobenzene, —1,4-Dichlorobenzene, —1,2-Dichlorobenzene' —2-Methylphenol. —2,2'-Oxybis(l-Chloropropzme)_ —4-Methylphenol —N-Nitroso-Di-n-Propylamine —Hexachloroethane —Nitrobenzene • —Isophorone 2 -Nitrophenol. 2,4-Diaethylphenol. — b i s (SljHChloroethoxy) Methane —2,4-Oichlorophenol rr~*l# 2,4-Trichlorobenzene ithtalene rChloroaniline orobutadiene f^f5>^« >ro-3 -Methy Iphenol. "^^-M^C^Inaphthalene, ---J^exac&Lorocyclopentadiene, •—2,4r€-TlriclilQrophenol_] I —2,4,$-Trichlerophenol —2-ChIoronaphthalene — 2 - N i t r o a n t l l n e .. - —Dimethyl Phthalate, —Acenaphthylene, — 2 , 6 - D i n i t r o t o l u e n e — 3 - N i t r o a n i l i n e '_ —Acenaphth<sne_ FORM I SV-1 3/90 100785 IC SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET >ab Name: COMpy Lab Code: COMPU tKTF Case No.: 15933 EPA SAMPLE NO. BGL19 Contract: 68D00159 SAS No.: SDG No.: BGLOl Matrix: (soil/water) WATER sample wt/vol: 1000 (g/mL) ML Level: (low/med) LOW % Moisture: decanted: (Y/N) Concentrated Extract Volume: 1000 fuL) Lab Sample ID: 402872 Lab File ID: Date Received: GH002872A08 03/04/91 Injection Volume: 2.oruL^ Date Extracted: 03/08/91 Date Analyzed: 03/12/91 Dilution Factor: 1.0 GPC Cleanup: (Y/N) Ji pH: CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) HfiZL. Q 51-28-5 2,4-Dinitrophenol 100-02-7 4-Nitrophenol 132-64-9 Dibenzofuran 121-14-2 2,4-Dinitrotoluene - 84-66-2 Diethylphthalate 7005-72-3 4-Chlorophenyl-phenylether 86-73-7 Fluorene 100-01-6 4-Nitroaniline 534-52-1 4,6-Dinitro-2-Methy Iphenol 86-30-6 N-Nitrosodiphenylamine (1) , 101-55-3 4-Bromophenyl-phenylether 118-74-1 Hexachlorobenzene 87-86-5 Pentachlorophenol' 85-01-8 Phenanthrene 120-12-7 Anthracene 86-74-8 Carbazole 84-74-2 "—Di-n-Buty Iphthal ate 206-44-0—^y-—Fluoranthene 1 2 9 - 0 0 - 0 — ^ Pyrene 85-68-7— fc.. -Butylbenzylphthalate 91-94-1 »•-—3,3'-Dichlorobenzidine 56-55-3 Benzo (a) Anthracene 218-01-9 Chrysene 117-81-7 bis (2-Ethylhexyl) Phthalate 117-84-0 Di-n-Octyl Phthalate 205-99-2 Benzo (b) Fluoranthene 207-08-9 Benzo (k) Fluoranthene 50-32-8-r Benzo(a) Pyrene ' 193-39-5 Indeno (1.2.3-cd) Pyrene 53-70-3 Dibenz (a, h) Anthracene 191-24-2 Benzo(a.h.i) Perylene 50 50 10 10 10 10 10 50 50 10 10 10 50 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 u -r ur 1 u u u u u u u u u u u u u u u u 1 il "^ 1) - Cannot be separated from Diphenylaaine 100786 •prwsiA T a t r — t IF SEMTVOLATILB ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS EPA SAMPLE NO. BGL19 Naae: <'!'^*fP^7Qni*1iir^ Contract: 68D00159 ^ab Code: COMPU Case No.: 15933 SAS No.: SDG No.: BGLOl atrix: (soil/water) WATER 5ample wt/vol: 1000 (g/mL) ML evel: (low/med) LOW 'i Moisture: decanted: (Y/N) oncentrated Extract Volume: 1000 fuL) 'njection Volume: 2.0 (uL) ;PC Cleanup: (Y/N) Ji .amber TICs found: 1 Lab Sample ID: 402872 Lab File ID: GH002872A08 Date Received: 03/04/91 Date Extracted: 03/08/91 Date Analyzed: 03/12/91 Dilution Factor: 1.0 pH: CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L CAS NUMBER Wi- COMPOUND NAME DIO-PYRENE RT 13.30 EST. CONC. 52 _ Q ; J • : • • * '--i. • -4i _4 — FORM I SV-TIC 100787 3/90 ID PESTICIDE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. BGLOl Lab Name:COMPUi LABORATORIES Contract;SAS5849HO I. Lab Code: COMPU Case No.; 15933 SAS No.: 5849HO SDG No.: BGLOl Matrix: (soil/water)WATER Sample wt/vol: 1000(Q/ml^ML % Moisture: decanted: (Y/N) Extraction: (SepF/Cont/Sonc) SEPF Concentrated Extract Volume: lOOOOfuL) Injection Volume: 1.0(uL) GPC Cleanup: (Y/N)Ji pH: Lab Sample ID: 402938 Lab File ID: Date Received: 03/04/91 Date Extracted:0 3/0 6/91 Date Analyzed: 03/11/91 Dilution Factor: 1 Sulfur Cleanup: (Y/N) N CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg)I2S;ili 319-84-6 319-85-7 319-86-8 58-89-9 76-44-8 309-00-2 1024-57-3 959-98-8 60-57-1 72-55-9 72-20-8 33213-65-9 72-54-8 1031-07-8 50-29-3 . 72-43-5 -<-— 53494-70-5'ti»*i.i 7421-36-3—*••— 5103-71-9 5103-74-2 8001-35-2 12674-11-2 11104-28-2 11141-16-5 534(69-21-9 12672-29-6 11097-69-1 11096-82-5 •alpha-BHC. •beta-BHC_ -delta-BHC •gamma-BHC (Lindane). -Heptachlor •Aldrin •Heptachlor epoxide. •Endosulfan I ^ •Dieldrin •4,4' -DDE •Endrin •Endosulfan II •4,4'-DDD •Endosulfan sulfate •4,4* -DDT -Hethoxychlor ••Endrin ketone •Endrin aldehyde. •alpha-Chlordane. •gamma-Chlordane, •Toxaphene, •Aroclor-1016. -Aroclor-1221_ •Aroclor-1232. -Aroclor-1242. •Aroclor-1248. -Aroclor-1254. •Aroclor-1260. OtPSOIV'd' OrOSQIIL 0 - 0 5 Q I I L QrOSOIIL Q-05QIIL OtQSOilL OtOSQIIL O t l O f l L O t l O I I L Q,1QIIL O T I Q I I L 0.10|U O t l O I I L Q , 1 0 I I L OiSQIIL O T I Q I I L OtIQISL OrQSOtIL QtOSOIIL .S^ilL JuxilllL X L H I I L JLLAIIL juxjaiii ZLJL\IL juLaiu .1 FORM I PEST 100738 ID PESTICIDE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. .Jib M^mo.rnMPnrwPM TABQRATORIES Contract:SAS5849HO BGL02 lb Code: COMPU Case No.: 15933 SAS No.: 5849HO SDG No.: BGLOl -Matrix: (soil /water) WATER ; unple wt/vol: lOOOfq/mllML % Moisture: decanted: (Y/N) l-.ctraction: (SepF/Cont/Sonc) SEPF r )ncentrated Extract Volume: lOOOOfuL) Injection Volume: 1.0(uL) ( ?C Cleanup: (Y/N)li pH: Lab Sample ID: 402939 Lab File ID: Date Received: 03/04/91 Date Extracted;03/06/91 Date Analyzed: 03/11/91 Dilution Factor; X Sulfur Cleanup: (Y/N) Ji CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg)HS/L 319-84-6— 319-85-7 — 319-86-8— 58-89-9 76-44-8 309-00-2 — 1024-57-3- 959-98-8— 60-57-1 72-55-9 72-20-8 33213-65-9 72-54-8 1031-07-8- 50-29-3 72-43-5 53494-70-5 7421-36-3- 5103-71-9- 5103-74-2- 8001-35-2- 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 alpha-BHC. beta-BHC_ delta-BHC •gamma-BHC (Lindane). -Heptachlor -Aldrin •Heptachlor epoxide. •Endosulfan I • D i e l d r i n • 4 , 4 ' -DDE •Endrin •Endosulfan I I -4,4'-ODD Endosulfan s u l f a t e 4 r4•-DDT -Hethoxychlor i n k e t o n e Endrin aldehyde. alpha-Chlordane, gaaoM-Chlordane, Toxaphene^ -Aroclor-1016 -Aroclor-1221, -Aroclor-1232, -Aroclor-1242, -Aroclor-1248, -Aroclor-1254, -Aroclor-1260. I 0,05QIIL 0.050IU 0-050|U 0.050|U 0.050|U 0.050IU O T Q S Q I I L 0.050IU 0-10|U 0.10|U QtlQIIL 0-10|U OtlQIIL QtlQilL 0.10|U 0.50IU OtlQIIL OtlQIIL QTOSQIIL 0-05Q|U JLLSLIU. XJLllL XJilJL juim J^l FORM I PEST 1 0 0 7 8 9 3/90 ID PESTICIDE ORGANICS ANALYSIS DATA SHEET ^ a b M^H'o^rnMPTirwKW IJBORATQRIES Contract:SAS5849HO EPA SAMPLE NO. BGL03 I. ab Code: COMPU Case No.; 15933 SAS No. : 5849HO SDG No.: BGLOl Matrix: (soil/water)WATER ample wt/vol: 1000^g/ml)ML % Moisture: decanted: (Y/N) extraction; (SepF/Cont/Sonc) SEPF oncentrated Extract Volume; lOOOOfuL) Injection Volume; l.Q(uL) PC Cleanup: (Y/N)H pH: Lab Sample ID: 402940 Lab File ID: Date Received: 03/04/91 Date Extracted:03/Q6/91 Date Analyzed: 03/11/91 Dilution Factor: JL Sulfur Cleanup: (Y/N) U CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg)UG/L 319-84-6— 319-85-7— 319-86-8— 58-89-9 76-44-8 309-00-2— 1024-57-3- 959-98-8— 60-57-1 72-55-9 72-20-8 33213-65-9 72-54-8 1031-07-8- 50-29-3 72-43-5 53494-70- 7421-36-3- 5103-71-9- 5103-74-2- 8001-35-2- 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 alpha-BHC. beta-BHC_ delta-BHC —gamma-BHC (Lindane). —Heptachlor —Aldrin —Heptachlor epoxide, —Endosulfan I —Dieldrin —4,4'-DDE —ExMlrin —Endosulfan I I —4,4'-ODD -Endosulfan s u l f a t e -4,4'-DDT -Hethoxychlor idrin ketone -Endrin aldehyde, -alpha-Chlordane, -gasBsa-Chlordane, -Toxaphene. —Aroclor-1016. —Aroclor-1221, —Aroclor-1232, —Aroclor-1242, —Aroclor-1248. —Aroclor-1254, —Aroclor-1260_ Q.Q50I 0.05QIIL 0.050|U 0.050|U O T Q S Q I I L 0-050|U 0.10|D 0.10|U 0.50|U QtlOilL O-lOjU 0.050|U 0-050|U miJilJL XJL\JL ZLJLIJL 2yS.\JL J ^ I I L J^iU O T O S O I I L O T O S O I I L OtlOIIL O T I Q I I L OilQlfl- O.IQIIL O.IOIIL J ^ l J ^ l S FORM I PEST 1 0 0 7 9 0 3/90 ID PESTICIDE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. Lab Name;COMPUCHRMnABORATORIES Contract:SAS5849HO BGL04 I. Lab Code: COMPU Case No.: 15933 SAS No.; 5849HO SDG No.: BGLOl Matrix: (soil/water)WATER Sample wt/vol: lOOOfq/ml^ML % Moisture: decanted; (Y/N) Extraction; (SepF/Cont/Sonc) SEPF Concentrateid Extract Volume: lOOOO(uL) Injection Volume: l.Q(uL) GPC Cleanup; (Y/N)Ii pH: Lab Sample ID: 402941 Lab File ID: Date Received: 03/04/91 Date Extracted;03/06/91 Date Analyzed; 03/12/91 Dilution Factor: X Sulfur Cleanup; (Y/N) fi CAS NO. COMPOUND CONCENTRATION UNITS; (ug/L or ug/Kg)afi/L Qf 319-84-6— 319-85-7— 319-86-8— 58-89-9 76-44-8 309-00-2— 1024-57-3- 959-98-8— 60-57-1 72-55-9 72-20-8 33213-65-9 72-54-8 1031-07-8- 50-29-3 72-43-5- 53494-70- 7421-36- 5103-71-9 5103-74-2- 8001-35-2- 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 alpha-BHC. beta-BHC_ delta-BHC. -gamma-BHC (Lindane). -Heptachlor -Aldrin -Heptachlor epoxide. -Endosulfan I -Dieldrin •4,4' -DDE •Endrin •Endosulfan I I . •4,4'-ODD -Endosulfan s u l f a t e -4,4* -DDT -Hethoxychlor -Endrin ketone Badrin aldehyde. alpha-Chlordane. gaasMi-Chlordane. Toxaphene. -Aroclor=101fr_ -Aroclor-1221_ -Aroclor-1232. -Aroclor-1242_ -Aroclor-1248_ -Aroclor-1254, -Aroclor-1260_ FORM I PEST 100791 3/90 ID PESTICIDE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. BGL06 Lab M«n.oTrnMpTTf;HB]t ji^ftOP^'r^pTRS Contract:SAS5849HQ Lab Code: CQMPU Case No.: 15933 SAS No.: 5849HO SDG No.: BGLOl Matrix: (soil/water)WATER Sample wt/vol: 1000(q/ml)ML % Moisture; decanted; (Y/N) Extraction; (SepF/Cont/Sonc) SEPF Concentrated Extract Volume: lOOOO(uL) Injection Volume: JLiJl(uL) GPC Cleanup; (Y/N)H pH: Lab Sample ID; 402942 Lab File ID: Date Received: 03/04/91 Date Extracted:03/06/91 Date Analyzed: 03/11/91 Dilution Factor: JL Sulfur Cleanup; (Y/N) fi CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg)UG/L 319-84-6— 319-85-7— 319-86-8— 58-89-9 76-44-8 309-00-2— 1024-57-3- 959-98-8— 60-57-1 72-55-9 72-20-8— 33213-65-9 72-54-8 1031-07-8- 50-29-3 72-43-5— 53494-70- 7421-36-3 5103-71-9 5103-74-2- 8001-35-2- 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 alpha-BHC. beta-BHC_ delta-BHC gamma-BHC (Lindane). Heptachlor Aldrin Heptachlor epoxide, Endosulfan I Dieldrin 4,4•-DDE • Endrin Endosulfan II 4,4•-DDD ——Endosulfan sulfate, -4,4'-DDT —Methoxychlor__ ^^-Endrin ketone. -Endrin aldehyde, r^s^fi^-aXpha-Chlordane. ——gaaaa-Chlordane, —Toxaphene, Aroc lor-^10^t6_ Aroclor-1221_ Aroclor-1232_ Aroclor-1242_ Aroclor-1248_ Aroclor-1254_ Aroclor-1260_ O T O S O O T Q S O O T O S Q 0.050 O T O S Q Q T O S O O T O S O O T O S O O T I O O T I Q 0.10 0.10 0.10 0.10 0.10 0.50 0.10 0.10 0.050 0.050 JLJi. U i . J ^ J L J A J ^ JLJJL UL mldJi ui: IL IL m FORM I PEST 1 0 0 7 9 2 3/90 ID PESTICIDE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. Lab Name:COMPUCHiy LABORATORIES Contract:SAS5849HQ BGL09 Lab Code: COMPU Case No.: 15933 SAS No.: 5849HO SDG No.: BGL09 Matrix: (soil/water)SOIL Sample wt/vol: 30.50fq/ml)G % Moisture: 21 decanted: (Y/N)N Extraction: (SepF/Cont/Sonc) SONC Concentrated Extract Volxime; 2000^uL) Injection Volume: 1.0(uL) GPC Cleanup; (Y/N)l pH;7.3 Lab Sample ID: 402945 Lab File ID: Date Received: 03/04/91 Date Extracted:03/11/91 Date Analyzed; 03/14/91 Dilution Factor; i Sulfur Cleanup: (Y/N) fi CAS NO. COMPOUND- CONCENTRATION UNITS; (ug/L or ug/Kg)VG/Kg 319-84-6 alpha-BHC 319-85-7 beta-BHC 319-86-8 delta-BHC 58-89-9 gamma-BHC (Lindane). 76-44-8 Heptachlor 309-00-2 Aldrin 1024-57-3 Heptachlor epoxide_ 959-98-8 Endosulfan I 60-57-1 Dieldrin. 72-55-9 4.4' -DDE 72-20-8 Endrin 33213-65-9 Endosulfan II 72-54-8 4,4'-DDD 1031-07-8 Endosulfan aulfate_ 50-29-3 4,4'-DDT 72-43-5 egffc' -Hethoxychlor 53494-70^ j^i —Endrin ketone 7421-36-j[PaBr Endrin aldehyde 5103-71-^^— alpha-Chlordane 5103-74-2 gaaaa-Chlordane 8001-35-2 Toxaphene 12674-11-2 Aroclor-1016. 11104-28-2 Aroclor-1221_ ^ 1141-16-5 Aroclor-1232 L-9 Aroclor-1242 ^ Aroclor-1248 (C' Aroclor-1254 ^ , Aroclor-1260 V^ JLZL l y L i j . ZL7L l y j L l y L 1 ^ X t l Qt90 JLI JLH -ixl _t»l . I x i 0T61 22L JLI 4.4 XJL JLI 2 ^ AL AL AL yi'X u u u u IL IL IL FORM I PEST 100793 3/90 ID PESTICIDE ORGANICS ANALYSIS DATA SHEET Contract:SAS5849HQ EPA SAMPLE NO. BGLIO Lab NameiC9T^P^JC"^]|f MkPORATORIES Lab Code: COMPU Case No.: 15933 SAS No.: 5849HQ SDG No.: BGL09 Matrix: (soil/water)£2IL Sample wt/vol: 30.70(Q/ml^G % Moisture; 21 decanted: (Y/N)N Extraction; (SepF/Cont/Sonc) SONC Concentrated Extract Volume: 2000(uL) Injection Volume; l.O(uL) GPC Cleanup; (Y/N)! pH:8.5 Lab Sample ID: 402946 Lab File ID: Date Received: 03/04/91 Date Extracted;03/11/91 Date Analyzed: 03/14/91 Dilution Factor: i Sulfur Cleanup; (Y/N) fi CAS NO. COMPOUND CONCENTRATION UNITSJ (ug/L or ug/Kg)IiaZKfi 319-84-6— 319-85-7— 319-86-8— 58-89-9 76-44-8 309-00-2— 1024-57-3- 959-98-8— 60-57-1 72-55-9 72-20-8 33213-65-9 72-54-8 1031-07-8- 50-29-3 72-43-5 53494-70-5 7421-36-3- 5103-71-9- 5103-74-2- 8001-35-2- 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 alpha-BHC, beta-BHC__ delta-BHC_ •gamma-BHC (Lindane). -Heptachlor -Aldrin 'Heptachlor epoxide, •Endosulfan I -Dieldrin •4,4' -DDE •Endrin -Endosulfan I I . •4,4' -DDD •Endosulfan s u l f a t e •4,4' -DDT -Hethoxychlor Endrin ketone. Bndrin aldehyde, alpha-Chlordane, gaaaa-Chlordane, Toxaphene, -Aroclor-1016 .Aroclor-1221, -Aroclor-1232 -Aroclor-1242. -Aroclor-1248. -Aroclor-1254. .Aroclor-1260. i ^ ZL^\ Ati 2.5 ZL1\ jLtA 2 ^ JL3.\ J L i ! JLII J ^ l 4 . 8 i JLll JLil JLll .2^1 jUft! X t l l Axil -2LSI 2SSi\ A3.\ A3.\ JiAl AS.\ All All All inX-i IU I 1 IU IU IU IU |U lUjI 1 IU IU iU IU IU IU IU IU IU IU IU IU IU m^ IU IU IU IU i£ 1— ri FORM I PEST 100794 3/90 ID PESTICIDE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. Lab Name;rr)MPUCHBy LABORATORIES BGLII Contract:SAS5849HQ Lab Code: COMPU Case No.: 15933 SAS No.: 5849HO SDG No.: BGL09 Matrix: (soil/water)SfiIL Sample wt/vol: 30.30(a/ml)G % Moisture: H decanted: (Y/N)fi Extraction: (SepF/Cont/Sonc) SONC Concentrated Extract Volume: 2000(uL) Injection Volume; l.OfuL) GPC Cleanup: (Y/N)l pH;7.4 Lab Sample ID; 402947 Lab File ID; Date Received: 03/04/91 Date Extracted:03/ll/91 Date Analyzed: 03/14/91 Dilution Factor; i Sulfur Cleanup: (Y/N) fi CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg)IIS/Efi 319-84-6 319-85-7 319-86-8 58-89-9- 76-44-8- 309-00-2 1024-57- 959-98-8 60-57-1- 72-55-9- 72-20-8- 33213-65 72-54-8- 1031-07- 50-29-3- 72-43-5- 53494-70 7421-36- 5103-71- 5103-74- 8001-35- 12674-11 11104-28 11141-16 53469-21 12672-29 11097-69 11096-82 alpha-BHC. beta-BHC_ delta-BHC gamma-BHC (Lindane). Heptachlor Aldrin 3 Heptachlor epoxide. Endosulfaui I Dieldrin -4,4•-DDE Endrin -9 Endosulfan II. 4,4 • -DDD, 8———Endosulfan sulfate 4,4'-DDT. —Hethoxychlor, -9a||jp!«»-Endrin ketone 3 - eiTi —Endrin aldehyde, 9^.ki^;2ur.HBipha-Chlordane, 2 —gaaaa-Chlordane, 2 —Toxaphene, -2 Aroclor-TrOlrfi -2 Aroclor-1221 -5 Aroclor-1232 -9 Aroclor-1242, -6 Aroclor-1248 -1 Aroclor-1254, -5 .—Aroclor-1260 ULl U l l l L L l ^ l l L ItJillL Ui.\JL 1ASL\]L -UlilL -LvHIIL i t l l l L iLllIL ixllIL i*llIL ^ L I I I L iuZIIL itlllL ^ I I L ixllIL JLuIIIL -LJailL -LLHIIL -2IUIIIL illlL -azifl. 12SL\JL j a m -SHU, jsiiiflXI _51IML_ FORM I PEST 100795 3/90 ID PESTICIDE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. BGL12 Lab Name;COMPUCHEM LABORATORIES Contract:SAS5849HQ 1. Lab Code: COMPU Case No.: 15933 SAS No.: 5849HO SDG No.; BGL09 Matrix: (soil/water)SOIL Sample wt/vol: 30.40fa/ml)G % Moisture; 2A decanted; (Y/N)N Extraction: (SepF/Cont/Sonc) SONC Concentrated Extract Volume; 2000(uL) Injection Volume; 1.0(uL) GPC Cleanup; (Y/N)X pH;8.2 Lab Sample ID: 402948 Lab File ID: Date Received: 03/04/91 Date Extracted;03/11/91 Date Analyzed; 03/14/91 Dilution Factor; JL Sulfur Cleanup: (Y/N) fi P CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg)IIS/Kfi Qi 319-84-6 319-85-7 319-86-8 58-89-9 76-44-8 309-00-2 1024-57-3 959-98-8 60-57-1 72-55-9 72-20-8 33213-65-9— 72-54-8 1031-07-8 50-29-3 72-43-5- 53494-70 7421-36- 5103-71-9«»— 5103-74-2 8001-35-2 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 —alpha-BHC. —beta-BHC_ delta-BHC -gamma-BHC (Lindane). -Heptachlor -Aldrin -Heptachlor epoxide, •Endosulfan I •Dieldrin •4,4* -DDE •Endrin -Endosulfan I I •4,4'-DDD, -Endosulfan s u l f a t e •4,4' -DDT. —Methoxychlor_ -—Endrin ketone •Endrin aldehyde, •alpha-Chlordane, •gaaaa-Chlordane, -Toxaphene, -Aroclor-ii^lfi, -Aroclor-1221, -Aroclor-1232 -Aroclor-1242. -Aroclor-1248. -Aroclor-1254. -Aroclor-1260. FORM I PEST 100796 3/90 ID PESTICIDE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. BGL17 Lab Name:£QlIE Lab Code; COMPU RATQRIES Contract:SAS5849HQ Case No.: 15933 SAS No.: 5849HO SDG No.: BGL09 Matrix; (soil/water)SOIL Sample wt/vol: 30.50fa/ml)G % Moisture: 11 decanted; (Y/N)N Extraction: (SepF/Cont/Sone) SONC Concentrated Extract Volume: 2000(uL) Injection Volume: l.O(uL) GPC Cleanup: (Y/N)l pH:fl.Jl Lab Sample ID: 402956 Lab File ID: Date Received: 03/04/91 Date Extracted:0 3/11/91 Date Analyzed: 03/14/91 Dilution Factor: i Sulfur Cleanup: (Y/N) fi CAS NO. COMPOUND CONCENTRATION UNITS; (ug/L or ug/Kg)US/lSfi 319-84-6— 319-85-7— 319-86-8— 58-89-9 76-44-8 309-00-2— 1024-57-3- 959-98-8— 60-57-1 72-55-9 72-20-8 33213-65-9 72-54-8 1031-07-8- 50-29-3 72-43-5- 53494-70- 7421-36- 5103-71-9- 5103-74-2- 8001-35-2- 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 -alpha-BHC -beta-BHC_ -delta-BHC, - gamma—BHC -Heptachlor, -Aldrin (Lindane). -Heptachlor epoxide, -Endosulfan I -Dieldrin -4,4' -DDE -Endrin •Endosulfan •4,4' -DDD II •Endosulfan s u l f a t e , -4,4' -DDT Hethoxychlor_ —Endrin ketone. 'Endfin aldehyde, -alpha-Chlordane, •gaama-Chlordane, -Toxaphene -Aroclor*10^1& -Aroclor-1221 .Aroclor-1232 -Aroclor-1242 -Aroclor-1248 -Aroclor-1254 -Aroclor-1260 FORM I PEST 100797 3/90 ID PESTICIDE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. BGL16 Lab Name. f-QWPiyt-Kf:^ - T.^qgp^T9R TF,? Contract:SAS5849HQ Lab Code: COMPU Case No.: 15933 SAS No.: 5849HQ SDG No.: BGL09 Matrix: (soil/water)SOIL Sample wt/vol: 30.60(Q/ml)G % Moisture: 41 decanted: (Y/N)N Extraction: (SepF/Cont/Sonc) SONC Concentrated Extract Volume; 2000(uL) Injection Volume; 1.0(\iL) GPC Cleanup: (Y/N)I pH:7.8 Lab Sample ID: 402955 Lab File ID: Date Received: 03/04/91 Date Extracted:03/I1/91 Date Analyzed; 03/14/91 Dilution Factor; 1 Sulfxir Cleanup; (Y/N) fi CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg)IIS/Ka Q ^ 1 319-84-6 alpha-BHC 1 1 319-85-7 beta-BHC | 1 319-86-8 delta-BHC | 1 58-89-9 qamma-BHC (Lindane) | 1 76-44-8 Heptachlor | 1 309-00-2 Aldrin - | 1 1024-57-3 Heptachlor epoxide | 1 959-98-8 Endosulfan I | 1 60-57-1 Dieldrin 1 1 72-55-9 4.4'-DDE | 1 72-20-8 Endrin | 1 33213-65-9 Endosulfan II | 1 72-54-8 4.4'-DDD | 1 1031-07-8 Endosulfan sulfate | 1 50-29-3 4.4'-DDT I 72-43-5™^^jN- Hethoxychlor | 1 53494-70-5^^ Endrin ketone 1 1 7421-36-3^e<pE»i^-Endrin aldehyde 1 5103-71-9-^^i*—-alpha-Chlordane 1 5103-74-2 gaaaa-Chlordane | 1 8001-35-2 Toxaphene 1 12674-11-2 Aroclor-1016 1 11104-28-2 Aroclor-1221 1 11141-16-5 Aroclor-1232 | 1 53469-21-9 Aroclor-1242 1 1 12672-29-6 Aroclor-1248 1 11097-69-1 Aroclor-1254 1 11096-82-5 Aroclor-1260 1 -< 1 2.9(U •* I 2.9|U 1 7.7( 2.9|y 2.9IU 20 |I^ 2.9IU 2.9|U lOIP 24IP 5.6|U 9.5|P 5.6|U 5.6rU' 5.6(U w 15|JP 5.6IU > 5.6(U " J— 1 HI ^1 2.9|U 1 1 16IP 1 1 290|U 1 1 56|U J } Sfr^U P • IIOID 56IU 58 in f a«^n - 5fi|D^ 1 ^ _ l - I _ ^ FORM I PEST 100798 3/90 ID PESTICIDE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. BGL13 Lab MAmoTrnvpTirwryu LABORATORIES Contract:SAS5849HO Lab Code: COMPU Case No.: 15933 SAS No.: 5849HO SDG No.; BGL09 Matrix: (soil/water)SOIL Sample wt/vol: 30.50fa/ml^G % Moisture: ii decanted: (Y/N)N Extraction: (SepF/Cont/Sonc) SONC Concentrated Extract Volume: 2000(uL) Injection Volume: 1.0(uL) GPC Cleanup; (Y/N)X pH:6.9 Lab Sample ID: 402952 Lab File ID: Date Received: 03/04/91 Date Extracted:03/11/91 Date Analyzed: 03/14/91 Dilution Factor: X. Sulfur Cleanup: (Y/N) fi CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg)lia/isa 319-84-6 — 319-85-7— 319-86-8— 58-89-9 76-44-8 309-00-2— 1024-57-3- 959-98-8— 60-57-1 72-55-9 72-20-8 33213-65-9 72-54-8 1031-07-8- 50-29-3 72-43-5 53494-70-5 7421-36-3- 5103-71-9- 5103-74-2- 8001-35-2- 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 alpha-BHC. beta-BHC_ delta-BHC •gamma-BHC (Lindane). -Heptachlor •Aldrin -Heptachlor epoxide. •Endosulfan I -Dieldrin -4,4' -DDE -Endrin -Endosulfan I I -4,4' -DDD, -Endosulfan s u l f a t e -4,4' -DDT •»-Hethoxychlor —Endrin ketone -Endrin aldehyde, -alpha-Chlordane, -gaama-Chlordane, -Toxaphene, -Aroc lor-10^16:_ -Aroclor-1221_ -Aroclor-1232_ -Aroclor-124 2_ -Aroclor-1248_ -Aroclor-1254_ -Aroclor-1260_ I JUi.\ iJHU- i J l l H . UllIL a ^ 0.t7 .UdlU iJIIIL .LJL\IL 1^\IL l ^ l l L -ILIIIL _2Liin_ J^ia_ -i^lIL -ULIU. 2Si.\lL __2illH . X L I I I L I J . L L I I U Z J JLAl .1^1 ,2MIIL mJlilL J l i l L J14Q- ^ I S - JU»Il j a i FORM I PEST 100799 3/90 ID PESTICIDE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO, BGL14 Lab Name:COMPUCHEM LABORATORIES Contract:SAS5849HQ Lab Code: COMPU Case No.: 15933 SAS No.: 5849HO SDG No.: BGL09 Matrix: (soil/water)SfiIL Sample wt/vol: 30.60(a/ml)G % Moisture: ii decanted: (Y/N)N Extraction: (SepF/Cont/Sonc) SONC Concentrated Extract Volume; 200Q(uL) Injection Volume: l.O(uL) GPC Cleanup: (Y/N)I pH:8.1 Lab Sample ID: 402953 Lab File ID: Date Received: 03/04/91 Date Extracted;03/11/91 Date Analyzed: 03/14/91 Dilution Factor: i Sulfur Cleanup; (Y/N) fi CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg)IIS/KS 319-84-6 319-85-7 319-86-8 58-89-9 76-44-8 309-00-2 1024-57-3 959-98-8 60-57-1 72-55-9 72-20-8 33213-65-9 72-54-8 1031-07-8 50-29-3 72-43-5 53494-70-5-^ 7421-36-3--^ 5103-71-9 5103-74-2 8001-35-2 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 -alpha-BHC. •beta-BHC__ delta-BHC -gamma-BHC (Lindane). -Heptachlor •Aldrin •Heptachlor epoxide, •Endosulfan I_ -Dieldrin -4,4' -DDE -Endrin -Endosulfan I I -4,4' -DDD, •Endosulfan s u l f a t e •4,4' -DDT, -Methoxychlor_ •—Endrin ketone -Bndrin aldehyde, -alpha-Chlordane, -gajona-Chlordane, -Toxaphene, -Aroclor-1016_ -Aroclor-1221. -Aroclor-1232, -Aroclor-1242, -Aroclor-1248. -Aroclor-1254, -Aroc lor-12 6 p. JUL JLH AJL Q T 3 5 I 2.JL\ 0-48 _Luil 1 ^ JLiii llfl- IIIL FORM I PEST 100800 3/90 ID PESTICIDE ORGANICS ANALYSIS DATA SHEET Contract;SAS5849HO EPA SAMPLE NO. BGL15 Lab WainPi^9^py(;;ffBlff LABORATORIES Lab Code: COMPU Case No.: 15933 SAS No.; 5849HO SDG No.: BGL09 Matrix: (soil/water)SOIL Sample wt/vol: 30.40fQ/ml^G % Moisture; ifi. decanted; (Y/N)N Extraction; (SepF/Cont/Sonc) SONC Concentrated Extract Volxime: 2000(uL) Injection Volume: l.O(uL) GPC Cleanup; (Y/N)I pH:!^! Lab Sample ID: 402954 Lab File ID: Date Received: 03/04/91 Date Extracted:03/11/91 Date Analyzed; 03/14/91 Dilution Factor; i Sulfur Cleanup: (Y/N) fi CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg)SIS/KS 319-84-6 319-85-7 319-86-8 58-89-9 76-44-8 309-00-2 1024-57-3 959-98-8 60-57-1 72-55-9 72-20-8 33213-65-9 72-54-8 1031-07-8 50-29-3 72-43-5 -sy^ 53494-70-5- 7421-36-3-d^-"- 5103-71-9 ' — 5103-74-2 8001-35-2 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 -alpha-BHC. -beta-BHC_ —delta-BHC. -gamma-BHC (Lindane). -Heptachlor -Aldrin^ -Heptachlor epoxide. -Endosulfan I - D i e l d r i n -4,4" -DDE -Endrin -Endosulfan I I . • 4 , 4 ' -DDD -Endosulfan s u l f a t e , • 4 , 4 ' -DDT. — M e t h o x y c h l o r _ — E n d r i n k e t o n e . -Endrin a l d e h y d e , -alpha-Chlordane, -gaimna-Chlordane, -Toxaphene, -Aroclor-1016, -Aroclor-1221, -Aroclor-1232. -Aroclor-1242. -Aroclor-1248. -Aroclor-1254. -Aroclor-1260. I ^ JLLHIIL :UL\IL ^SJS- JLJIIU. -ifllE. -IfllE ^ J L I I J P ^ 0 . 3 3 I J P JL^IJP --. - Z H I I L Z X A ^ \ 2m\]L -IflllL Ak\lL .MIIL JLHIU- JLAIIL ^ 1 0 . JfillL l_ FORM I PEST 1 0 0 8 0 1 3/90 ID PESTICIDE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. .ab Name:£QK£I2CiffiHJiiBQB&2QEIES Contract;SAS5849HQ BGL23 Lab Code: COMPU Case No.: 15933 SAS No.: 5849HQ SDG No.: BGL09 latrix: (soil/water)SfiIL Sample wt/vol: 30.60fa/ml)G i Moisture: 2, decanted: (Y/N)N extraction: (SepF/Cont/Sonc) SONC Concentrated Extract Volume: 2000fuL) injection Volume: 1.0(uL) ';PC Cleanup; (Y/N)2 pH:7.5 Lab Sample ID: 402957 Lab File ID: Date Received; 03/04/91 Date Extracted;03/11/91 Date Analyzed; 03/14/91 Dilution Factor; i Sulfur Cleanup: (Y/N) fi CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg)US/SS 1 319-84-6 alpha-BHC 1 1 319-85-7 beta-BHC 1 1 319-86-8 delta-BHC | 1 58-89-9 gamma-BHC (Lindane) | 1 76-44-8 Heptachlor | 1 309-00-2 Aldrin | 1 1024-57-3 Heptachlor epoxide , | 1 959-98-8 Endosulfan I | 1 60-57-1 Dieldrin 1 72-55-9 4,4'-DDE | 1 72-20-8 Endrin 1 33213-65-9 Endosulfan I I | 1 72-54-8 4f4'-DDD 1 1031-07-8 Endosulfan s u l f a t e 1 50-29-3 4,4'-DDT 1 72-4 3-5 mmm—Methoxychlor j 53494-70-5^^»—Endrin ketone i 7421-36-3—^^^SiT-Endrin aldehyde i 5103-71-9—-«*«w.-^pha-Chlordane 1 5103-74-2 gamma-Chlordane 1 8001-35-2 Toxaphene 1 12674-11-2 Aroclor^lGlfr 1 11104-28-2 Aroclor-1221 1 11141-16-5 Aroclor-1232 1 53469-21-9 Aroclor-1242 1 12672-29-6 Aroclor-1248 j 11097-69-1 Aroclor-1254 1 11096-82-5 Aroclor-1260 1 . 1.8IU- 1.8|U 1.8|U 1.8|U 1.81U 1.8IU 1.8IU 1.8IU 3.6IU 3.6IU Tl k 1 3 . 6 | U f 1 3 . 6 | U | 1 3.6IU 1 1 3.61U 3.6|U 18IU 3.6IU 3.6IU 1 1.8IU 1 i.aiu 1 180IU 1 36IU 1 36r^U 1 72ID , 1 1 36tOtt 1 1 36|Oll 1 1 3 6 I D I 1 36IUJ 1 1 tl FORH I PEST 100802 3/90 ID PESTICIDE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO, BGL18 Lab Hane'.QQlSSWSSLJLbSQMSmiSS. Contract:SAS5849HQ Lab Code: COMPU Case No.: 15933 SAS No.: 5849HQ SDG No.: BGLOl Matrix: (soil/water)WATER Sample wt/vol: i(2fljQ.(g/ml)Jat % Moisture: decanted: (Y/N) Extraction: (SepF/Cont/Sone) SEPF Concentrated Extract Volxune: lOOOOfuL) Injection Volxime: l.O(xiL) GPC Cleanup; (Y/N)fi pH: Lab Sample ID: 402943 Lab File ID; Date Received: 03/04/91 Date Extracted:03/06/91 Date Analyzed: 03/11/91 Dilution Factor; i Sulfur Cleanup: (Y/N) fi CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg)IIS/L Qi» 319-84-6 319-85-7 319-86-8 58-89-9 76-44-8 309-00-2 1024-57-3 959-98-8 60-57-1 72-55-9 72-20-8 33213-65-9 72-54-8 1031-07-8 50-29-3 ^- 72-43-5 ««» 53494-70 -*" 7421-36-3 5103-71-9 5103-74-2 8001-35-2 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 —alpha-BHC, —beta-BHC__ delta-BHC. —gamma-BHC (Lindane). —Heptachlor —Aldrin —Heptachlor epoxide, —Endosulfan I —Dieldrin —4,4'-DDE —Endrin —Endosulfan I I . —4,4'-DDD —Endosulfan s u l f a t e . —4,4'-DDT —Methoxychlor_ -Endrin ketone. -Endrin aldehyde. -alpha-Chlordane, -ganma-Chlordane, -Toxaphene, —Aroclor-tOlff, —Aroclor-1221_ —Aroclor-1232. —Aroclor-1242, —Aroc lor-12 48. —Aroclor-1254. —Aroclor-1260, O t O S O l U ^ QTOSOiuTr O T O S Q I I L " OTOSOIBL OTOSOIIL 0.050IU OTOSQIIL OTOSQIIL QTXOIIL O T I O I I L Q.IQIIL QtlQIH- QTXQIIL QtlOIU- O . I O I U OTSOIU- QtlOIIL o . i o i u 0.0501U OtQSQIIL JUL\JL JLH^IL J^IIL UL\JL mULlJL JLAin. JuJUt XJII FORM I PEST 1 0 0 8 0 3 3/90 ID PESTICIDE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. BGL19 Lab M^mr>.rni^p^Q^ T.Annp&TnPTF.g Contract:SAS5849HO Lab Code: COMPU Case No.: 15933 SAS No.: 5849HQ SDG No.: BGLOl Matrix: (soil/water)WATER Sample wt/vol: lOOOfq/mDML % Moisture; decanted; (Y/N) Extraction; (SepF/Cont/Sonc) SEPF Concentrated Extract Volxime; lOOOO(xiL) Injection Volxime: l.O(xiL) GPC Cleanup: (Y/N)fi pH: Lab Sample ID; 402944 Lab File ID; Date Received; 03/04/91 Date Extracted;03/06/91 Date Analyzed: 03/11/91 Dilution Factor; i Sulfur Cleanups (Y/N) fi CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg)UG/L t 319-84-6— 319-85-7— 319-86-8— 58-89-9 76-44-8 309-00-2— 1024-57-3- 959-98-8— 60-57-1 72-55-9 72-20-8 33213-65-9 72-54-8— 1031-07-8- 50-29-3-— 72-43-5 53494-7 7421-36 5103-71 5103-74-2— 8001-35-2— 12674-11-2- 11104-28-2- 11141-16-5- 53469-21-9- 12672-29-6- 11097-69-1- 11096-82-5- —-alpha-BHC beta-BHC_ delta-BHC -gamma-BHC (Lindane). -Heptachlor -Aldrin -Heptachlor epoxide. -Endosulfan I -Dieldrin -4,4'-DDE -Endrin •Endosulfan II •4,4'-DDD, -Endosulfan sulfate -4,4' -DDT i*. Hethoxychlor_ —Endrin ketone •Endrin aldehyde, -alpha-Chlordane, -gamma-Chlordane, -Toxaphene, -Aroclor-t016, -Aroclor-1221, -Aroclor-1232, -Aroclor-1242, -Aroclor-1248. -Aroclor-1254, -Aroclor-1260, O T O S O 0.050 O T O S O 0.050 O T O S O O T O S O 0.050 0.050 0.10 0.10 0,10 0.10 0,10 OTIO 0,10 0.50 0-10 O T I O 0.050 0,Q5Q ±JL ±JL JUL m Z . ^ J ^ J ^ J ^ mUL V V 1 u 1 u u u u u u u u u u u u u u u u u u u IL U l u l §v FORM I PEST 1 0 0 8 0 4 3/90 REFERENCE NO. 17 100805 NUS CORPORA TION ___, , „ _ .,-___ SUPERFUND DIVISION PROJECT NOTES ^°- l 7 ^ { % ^ J /^y^ °-^- Z F A ^ 7?7 FROM: ^ " " ^ ^ y ^ ^ ^ / y y S 5 ^ y ^ SUBJECT: REFERENCE 'T^.e^^' /^.xy^^^yLyL V-^.A'y.y..y^.yy Vyjz-y^^^AdJ^ Sc^ <£3y^y'y' yi,^dZi!£^tyymy y ^ /^2<^yfi^^ey^ A m yytyJ^ y ^ y y p d d y y y y i y ^ / L a > m y ^gS>^ S e ^ cX, A J ^ Z / yc2i£yaiiAyJy / < ^ ^ C ^ / ^ 7/.yJ "Pr^yTZS^y/yary.. yZ.. J ^ y A 79S.^ y . ^ y ^ J ^ ' ' T J O T ^ y^7^*yr*^ea*dy^ y ^ L a y j L yTZS^j' ^ y A Z Z A . ^ > L ^ S/8^^£*^ " ,:<yta<l ^^rLy,^y:J^. ' T Z ^ haiOA,y y ^ y ^ ^ ^ ^ y J / ^ y ^ y y t y A y . ^ y ^ yyZ^e / i ^ ^ y A r y t ^ . y ^ ^ ^ y^y^yeA '^^yxyyyjp . y L y ^ L - ^ ^ ^ ^z?^ ^Z^f^iJTy g ^ ^ ^ / L > y ^ . / / < Z i ^ y > / y f ! ^ ^ y f i ^ y f t ^ ZZd^U A/^l6*<£jP.. y ^ y y ^ . l y Z T Z ^ ^ y ^ y y l y y ^ j j ^ .^itZ^lmy^yf^ yiJ2ay.^.yA.^^ yr:£r SgT^ ^ ^ v y^..ytAfi ^ ^ ^ yiS^ y^y^yf^^y^i^ y^i^trfC ^r^^^i y^y^ ^ y / A y P y ^ i f ^ fi'ytr^y^a^ ( > » ^ y j y : ^ f -TT^^r?- / ( y ^ ^ Z ^ m * ^ . ^ y<yA^ ^rzdiray j ^ t ^ yiOys^zy^yy^ ^.^p;s€<y ^f^y^yy y^^y^J^ ^<y^ZZ^ yS^yi^ ^ A ^ ^ y^^^^diy^^^jC A y . . ^ ^ ^ . ^ " T Z ^ y L r ^yyrAy^.y^ yfyi a y i j U y f r y ^ y > ^ y y Z ! ^ rctyy^^yil^ed^ J2. T y y / ^ y j ^ ^ y i ^ / y y T s Z JZy^yZar'^yii:^^^^yt^(P .^c.:^.^ t y t ^ & y , ^ . ~^ 1 '^t.*<^y y ^ y.^jay .yy^atyeyy^jAyrA^. T J .^<^KVfe^>- .yfZ/^y yLgyty ^ ^ r - ^ < y . y ^ '=^,cy>^yyj> a-/i/^ C^y/cry^ ' H ^ j ^ ^ ^ , ^ ^ y " - ^ ^^^'^ " ^ ^ 6 i i i r s i<^fiy qy^j^oyeJ 15=; ayty*><J) /Zrt^..,^u^. -yjrf.^j,^^7se / U Z Z T F "a " Z ^ / y ? a ^ > r y y r / ^ A/J^yryjf- y?.Ays- < ^ ^ j f c ^ > f ^ ^ ^ ^ y j a ^ ^ y t c £ y £ > ^ ^.14 y ^ y Z h^JjUiJlMJtJL. NUS443A58 1182 1008Q6 NUS CORPORATION AND SUBSIDIARIES STANDARD CALCULATION SHEET CUENT: yry. rtj^rrr/yfC FILE NO.: cZfcZi' 9/y>y-cz. ^ BY: yf"s^. y y y y Q O PAGE /y_ SUBJECT: " ^ ^''•syy^^/f^jy t5j>ti^^77an) ^ - ^ ^ y ^ ~ y ^ - 3 CHECKED BY: DATE ^y^/^7 j3>i<7'^]/^T 'TatViyfTlfnt'i / s 7 //j7?^ S 7 5 ^ - r ^ d i - :2 r^J/yrty-rr^ JA <>-» ^ r - ^ 7 3<^ y(Z>y "oftmtjiyf Cki^O /ts CtuixyfTS TO. ^ - ? D J - ^ T ^ J A T - 1 / 3 ^ S 7 ^ ^ /o ^fi-T-JOfO (SF Z^S/XV^T- /A) \ 'y^r. o o o o o 70 o o y^m, o o o o o / 6 o o u o o o o o w ^ y o ^ / f f , s o 0 o -^f S1< S S ^ l7/<s77tAZC£nyy3yim yiytf cy^7 ^o c ^ 7 S G7 / / 75 yyr 1 VH ^ 1 -^7 ? ^ (oO Z S C7 y y . ^ FOr (yi)iiai2.e: 7^ =• /oTm. iTAtsr^cr l^>ptkyf77&r*i "f^p - ''^oufT^ea,) dff: jZ>d iytttcry^ cy/u^rs 7)>'«^ /^-7— / S ¥ S 7 ^ ? 7 0 'TZZr-y^i. '^POtyniui (M'un-'utT^l^ 1 ^r/yrf/f72F];x —. ioPUcyi77ryy> O F DyfJX ! ^ m o o o o o 7 S 7 o ^ o ) A S ? ^ ^ o O o O 0 t ^ S / o o c9S/ I M 1 O o o o 0 (^9o -^3^ o /tSZiG 0/c.r ' T ^ T j o * * ) <^yrt y ^ o o 0 y ^ s y -sy^ 1 t ^ ^ c ^ 1 o y ^ / 9 tSrar -77 ^ 7 c ^ SV 5 7 7'SYS 7 Z 3 cZ2S^3 .P05 7G73 LF^opt^ i^ <Z23 3<^/ 7-^5 ^ 3 9(Z>S o cPSPt :^93 7S-V(^ 1 .) 01 NUS 155A REVISED 0285 Kris Buros FINAL REPORT-FINAL w~-^ '0 WATER MANAGEMENT PLAN FOR THE ~ PUBUG WATER SYSTEM Prepared for THE DEPARTMENT OF CONSERVATION AND CULTURAL AFFAIRS GOVERNMENT OF THE VIRGIN ISLANDS Prepared by CH2M HILL SOUTHEAST, INC Project No. CN14325w\0 July.1983. 100808 0 s.ooo 10,000 r»«« 0 ~ I.MO 3.000 Mrictt Sri vice D i i l n c l i «i0 N i i m l i e i r i l demand of the service FIGURE 3-4. djslrlcis on SI. CroJx for Ifie year 1980. DEMOGRAPHIC Table 3-3 DATA FOR THE U.S VIRGIN ISLANDS C"»t«!gOflf S t . Jtiliii t 3 I, i STJ TOTALS S t . Ilitiaiut SIT imALS St. Clull C O 00 |-» o 1 J ) I , i fc 7 I 1 10 11 11 1} 14 1} U I) la I I J 5 i 1 « t la II 11 11 14 IS U 11 IS I t 10 SIX TUtAI.S T01U.S i*u|Hll«tiU« 1.011 041 l i l I U IS TJ.B6 l i s iifc sss l . S l ) ),4Sfc 4,S»9 l . M S 1.622 a.ISS no Sfc4 2,111 I . I S J fct; l.ISS I I UO iizjn lis l.SSI 11,110 H I sn (•04 4.9fc4 l . U O 1,012 2,OSS 1,4«> ) , S ) t l.SSI S04 4IS S4t 101 4 i I I I . 4 J 4 1 4t,2S0 «S,910 Uurk~>orc* 410 I 41fc I I Zv, 11 t 4S 10 * , f c l f I I SS 440 IJO 1 114 ISS 11 400 fc.tOS S.OII IS 20,95{ 111 S i l 111 U S IS IS I , O t l l . S I t 4.011 l O i i H s.m 411 )S2 UO ?w 10 l . } 4 1 l O . J l t 41.J4S 19B0 l)«t« Sclioolf 4J» S I iii 40 ifcO l . O b l 114 2,608 ISS 4«6 1,061 164 11 4,21S S.S6S uTiii 11 2.U1S 2.812 9 1,9)9 1.200 1,169 440 6S 1,169 J99 40 1.168 I S , l i s 1S.SI8 Uotttli I ^ 41 10 l i p m S I 4 » I M R c i t w i r a n t < t » b U p ) IS K 4P 30 !^ IS lop 10 110 110 ISS 10 SJ 10 Id 1} 10 10 IS IS 190 IS IS SS 10 S9S 1.41S i'opulatinn ^ g r — 1,24S 1,071 l a i 116 40 17ns 141 19S 6)S 1,741 2.810 4,S1S 1,881 l , 7 S I 9,01s 1,214 6S6 2,986 4,191 797 1,114 1,911 4,881 11 160 SO,SIO 4 ) 1 4,S62 I4,42S 100 610 S09 6,674 * , » I S 1,940 i.n* ) , I 4 S 3,880 1,410 SSS S2I 688 401 S I 4IS S . l l l 62,14S IIS.610 1990 r t o l t i t t t i l t>»t» Uork Fofca ScEooTi I t o l e l t jftstima) SIO SO 4S0 11 I I s so 11 1,110 IS 600 4S1 SIS 1 III 266 11 411 I.IOS t . l S t 71 429 100 B) sri 48 260 1.117 114 794 2.608 SSS 996 1.067 164 12 4.11s S.S7S 84 10 )S8 « 1 10 81 41) 110 114 661 167 194 1S4 111 Sett^ufailt J t i b U O Fu|Mlal Ion urtotisl 100 IS m so 10 us 4$ IS 12s 70 110 10 l i s 190 21,100 190 914 199 199 IS S9 1.141 I.6S1 6,091 MS 601 9.106 SIS 10 181 U S )74 11 10 I,I1S 11.6)0 iS.f»i 18.408 1) 2.09S . l . B l l ----9 l , ) ) t 1.149 J1169 440 6S 1,)69 800 .- 199 40 — ---- l.lfcS 10,8)) 19.89J 1,1)7 160 6S 110 ---- 91 -- S6 -- 81 200 181 100 — 161 100 1S4 --.. 180 1,841 i l i i i 91S SS SS 10 10 -- IS -- 10 10 IS 4S 190 --.' )S IS SS " -' 10 640 1,680 I .4)4 1.110 198 IS) 46 i:iJ5 148 410 I I S 1,961 1,164 S.OIO 2, ISS 1.916 9.192 I.SIS 961 1,7)1 4.814 89) 1,449 S.91I S.0]6 IS _ 180 S6;87S SbS S,19S i 7 . 4 ) l ' S16 I S l 608 ),9)S S . l l l 10,66) 3.141 3,161 4,617 4,099 6)0 81? 486 61 49S 6.140 •4,240 I 1 4 A 9 0 2UUU I'l uK*: I t'l U»l« Uork FutLC Scliuiilf l l o t e l a (t>tr»uin) ( p x p l l * ) ( r o a * » ) - ^ f - m Tim d l l H I I M I ( t » l i U « ) SSI. 60 4S0 10 i,~o«i; kV9 lis 8 ) iSfi 10 1»S 60 iV. 110 IS US 1 ] 9 S) IS ).S4) 16 6)6 460 SSO 1 124 ISO 24 469 ) . S ) I 6 . I I S 46 120 24.740 4".) 1,040 957 226 11 101 1,411 1,9IS 4,6SS 196 691 10,164 611 I I 111 14) 4)6 1) 11 J^Z5 IS,198 SI.611 48 -- 260 -- ) , 5 I 4 1)4 1,194 2,608 SSS -- 1,699 1,06) 164 12 4,1)S l . S i S -- 19,688 72) J,09S 2.811 -' .. 9 1,4)0 ) , ) 1 7 1 . U 9 440 64 1,169 800 .. 799 4U --.. - • i . i t a )),4S6 41,944 -- ',0 )U 81 4 ) 1 1 ) 1 .. -- 6)1 -- 144 IBS .. 267 1)4 194 100 111 r.m 16U IIS 110 .. -- ISi. .. S6 .* 62 200 M l 100 161 181 ISi. .- 180 1,1)8 6,4S1 .. IS 10 6S IIS 6S 10 IS l i s 10 160 .. 10 160 I I S IS IS r.m SS 6S 10 10 SU -. 10 10 IS so 190 .. .. IS IS SS is 680 i.Qou Mutai SILS - r c « l d c n l U I | WKV CN»8S6 walk i i i r c « | SQI - . t l i o o l i TUR • t o u r l a t t i r l c n l c i l . A P P E N i i m I AVERAGE AHIWIAC n A I N T A L L lAULE A H B I t E V I A I ltlM& USEU I O I & I H I C I Nil. I 1 i 6 I M t 10 II 12 I ) I* IS 16 I r ID IV 20 i l . IIUIHAS its I S 1 0 »» *s « 0 4 0 « 0 4 0 I S 4 0 1 9 I S 4 0 * 0 4 S • s • 0 4 0 0 0 S I . C R U M J S SI . JOHN 40 4S SO *s so 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 ISL AMIS l i * . J - S I . JOIIH I - S I . lltUMAS • - S I . CRum CAiEConv CAI L K C M E O O I H R E S S C L l U R m t f - . ---- L t AKACC MEUICAL O f l l E n H E S I U E N I I A L SCIIOUL l U H I S I •onnroHc E I I I H I H-s u l O l b l S U B O I S I C P O K f . A l . / O I D S f l i _ - - ---- UNI 1 U I S I X I C 1 s u i i o i S I N K : 1 GALLONS l - t H IIAV IOOO t . A l l U N S ><EN IIAV l O I A l O l S S U L V t O SUt 111 suuAut r t E i MON-(>ai«ai.c HAIER SOURCES BKI) - ORACKISM MELL VAICR ORN - RAINOAIER COLLCCIEO FROM A OHIVEMAV OR OIMCH SlMIAlLS r a w - r i L I C R E O SECONOARV M A S I E M A I I R a m - niHER Pmtt - PMIMARV I R E A I t O M A S I E H A I E R SEA - S C A a A l f R — O I R E C I I N I A A E SEH - SEAMAIER — MELL SUR - SURFACE HAIER SUCH AS A PONII SDK - SECUNOAN* I R E A I E I t H A S I E a A I E H SAL I H A I t U I S CUHSIOEREO I O BE A L L H A I E R B i l l ! A l U I A L n i S S U L V E U S U L I O S l U S ll» l O . O U O H C / L OH G R t A I L I I . O E S A L I N A I I O N U N I I S l i t SCR I I M I UN <» I TRE O l - O I S I I L L A I I f l N EO - CLECIM1M>|ALV..|S RO - D E v r R S t (ISMIISIS SS - MM All S I I L L E E E O H A I E R OHH - UMACKISM HELL H A I E R O I M - O I I I E R S H I - S E A H A I E R - - I N I A K E S H H - SEAHAIER - - HLLL o o 00 V A N U F A l I I M E H AUC - AUUA C M £ M S A I - I I A S I C l E C l m U L U G I t S CUL - C U L L I G A N CN« - E N V I H O G E N I C S • IVO - IIVURANAUI I C S lOE - ISRAEL DE^AL I N A I ION I N C I r i t C I I S IUN - I O N I L S MEC - M L L I I A N I C A l L I I I I I P H E N I Slll>l*L T NEC - N d ' l U N L M I C H I H I U C I I I I I - I I I K E I I PEM - M E H H U I I I I'l » - PCll » « t IR l ( •> HCC - UtSUIIUCE CIINSLHVAI I I I N ( I I M I ' A N * SRS - S I MEANS ROGERS UOP - E L U I U SVSICMS HE > - Mt S I I N C I I O U S E H S A - a A l E R S l R V I C t r ll> A M t R | ( . REFERENCE NO. 18 100812 LEVEL: SELECTION: SEQUENCE: EVENTS: REG u2 REGION, STATE, SITE NAHE ALL U.S. EPA SUPERFUND PROGRAM ** C E R C L 1 S ** LIST-8: SITE/EVENT LISTING EPA ID NO. VID988266177 VID988266185 VID980530984 VID988266U4 VID118157866 VID988266193 VID988266151 SITE NAME STREET CITY COUNTY CODE AND NAME STATE ZIP CONG DIST. CRUZ BAY TEXACO CENTERLINE ROAD ST. JOHN VI 00830 020 ST. JOHN DOMINO OIL SERVICE STATION CENTERLINE ROAO ST. JOHN VI 00830 020 ST. JOHN ESSO FREDERIKSTED PLANT RD TO SANDY POINT FREDERIKSTED VI 00840 010 ST CROIX FISH HAWK MARINA ROUTE 32 AT BENNER BAY ST. THOMAS VI 00801 030 ST. THOMAS FOUR STAR AIR CARGO CYRIL E. KING AIRPORT, HARWOOO ST. THOMAS 030 ST. THOMAS GASSETT MOTORS ROUTE 384 TUTU DISTRICT ST. THOMAS 030 ST. THOMAS INDEPENDENT BOATYARD ROUTE 32 AT BENNER BAY ST. THOMAS 030 ST. THOMAS VID98065109S ISLAND CHEMICAL CORP MELVIN-EVANS HUY (RT 66) CHRISTIANSTED 010 ST. CROIX VI 00801 VI 00801 VI 00801 VI 00820 NFA. FLAG NFA NFA NFA NFA NFA OPRBLE UNIT 00 00 00 00 00 00 00 EVENT TYPE DS1 PA1 DS1 PA1 DS1 PA1 DS1 PA1 DS1 PA1 DS1 PA1 DS1 PA1 01 RVI 09/13/89 PAGE: 457 RUN DATE: 05/01/91 RUN TIME: 15:33:40 VERSION: 1 ACTUAL ACTUAL START COMPL CURRENT DATE DATE EVENT LEAD 03/03/89 EPA (FUND) 02/28/89 03/31/89 EPA (FUND) 03/03/89 EPA (FUND) 02/28/89 03/31/89 EPA (FUND) 06/01/81 EPA (FUND) 04/17/86 EPA (FUND) 03/03/89 EPA (FUND) 02/28/89 03/31/89 EPA (FUND) 03/03/89 EPA (FUND) 02/28/89 03/31/89 EPA (FUND) 03/03/89 EPA (FUND) 02/28/89 03/31/89 EPA (FUND) 03/03/89 EPA (FUND) 02/28/89 03/31/89 EPA (FUND) EPA (FUND) O O 00 H» CO LEVEL: SELECTION: SEQUENCE: EVENTS: REG .,1 REGION, STATE, SITE NAME ALL U.S. EPA SUPERFUND PROGRAM • • C E R C L I S ** LlST-8: SITE/EVENT LISTING PAGE: 459 RUN DATE: 05/01/91 RUN TIME: 15:33:40 EPA ID NO. VID982272569 VID090544958 VID980780589 VID988267431 VID9aa26626a VID988267449 VID988266102 VID988266235 SITE NAME STREET CITY COUNTY CODE AND NAME STATE ZIP CONG DIST. TU TU UELLFIELD ANN'S RET REDT ST. THOMAS VI 00801 030 ST. THOMAS TUTU ESSO ROUTE 384 TUTU DISTRICT ST. THOMAS VI 00801 030 ST. THOMAS TUTU TEXACO ROUTE 38 AND ROUTE 384 ST. THOMAS VI 00801 030 ST. THOMAS UNIVERSITY OF VI CHRISTINSTEN ST. CROIX VI 00820 010 ST. CROIX _yi.XHEMlCAL.,.. ROUTE 66 ST. CROIX VI 00820 010 CHRISTIANSTED VI DEPT OF AGRICULTURE FREDERICKSTED ST. CROIX VI 00820 010 ST. CROIX VI GOVERNMENT MOTOR POOL ROUTE 304 ST. THOMAS VI 00801 030 ST. THOMAS VIRGIN AIR CYRIL E. KING AIRPORT, HARWOQD ST. THOMAS VI 00801 030 ST. THOMAS NFA. FLAG NFA OPRBLE UNIT 00 01 00 00 EVENT TYPE RVI RV2 RV3 C01 DS1 PAl 0S1 PAl 00 00 00 00 00 RVI DSI PAl RVI DSI PAl DSI PAl ACTUAL START DATE 09/02/87 03/22/90 09/24/90 10/02/87 02/28/89 02/28/89 03/08/90 VERSION ACTUAL COMPL DATE 03/22/90 05/31/90 03/03/89 03/31/89 03/03/89 03/31/89 : 1 CURRENT EVENT LEAD EPA (FUND) RESP. PARTY RESP. PARTY RESP. PARTY EPA (FUND) EPA (FUND) EPA (FUND) EPA (FUND) EPA (FUND) 02/05/87 EPA (FUND) 02/10/89 EPA (FUND) 03/08/90 07/17/90 EPA (FUND) 03/31/89 EPA (FUND) 02/28/89 03/31/89 EPA (FUND) 03/03/89 EPA (FUND) 02/28/89 03/31/89 EPA (FUND) O O 00 l-> LEVEL: SELECTION: SEQUENCE: REGION: 02 EPA ID REGtO.. o2 INTEGRATED REG, ST, SITE NAHE SITE/ALIAS NAHE STREET CITY COUNTY NAME VID988266144 VID118157866 U.S. EPA SUPERFUND PROGRAH ** C E R C L I S •* LIST-4: SITE ALIAS LOCATION LISTING PAGE: 536 RUN DATE: 04/01/91 RUN TIME: 09:01:45 VERSION: 1 STATE COUNTY ZIP COOE FISH HAWK HARINA ROUTE 32 AT BENNER BAY ST. THOMAS VI ST. THOMAS 030 FOUR STAR AIR CARGO CYRIL E. KING AIRPORT, HARUOOD ST. THOMAS VI ST. THOMAS 030 FOUR STAR AIR CARGO ST. THOMAS 00801 00801 ALIAS SEQ. NAHE 0 SOURCE FED FAC 01 VI VID988266193 GASSETT MOTORS ROUTE 384 TUTU DISTRICT VID988266151 y!P?8065io?§. VID988266219 M O O 00 tn ST. THOMAS ST. THOMAS INDEPENDENT BOATYARD ROUTE 32 AT BENNER BAY ST. THOMAS ST. THOMAS ISLAND CHEHICAL CORP MELVIN-EVANS HUY (RT 66) CHRISTIANSTED ST. CROIX MCKESSON ENVIRO-SYSTEMS SAFETY CLEAN ISLAND CHEMICAL CORP ST. CROIX LAGA BUILDING ROUTE 38 TUTU DISTRICT ST. THOMAS ST. THOMAS VI 030 VI 030 VI 010 VI VI 030 00801 00801 00820 00801 01 02 03 REGI EPA ID REGIOit u2 INTEGRATED REG, ST, SITE NAHE SITE/ALIAS NAHE STREET CITY COUNTY NAHE VID988266268 VID988267449 VI CHEHICAL ROUTE 66 ST. CROIX CHRISTIANSTED VI CHEHICAL VI DEPT OF AGRICULTURE FREDERICKSTED ST. CROIX ST. CROIX VI DEPT OF AGRICULTURE U.S. EPA SUPERFUND PROGRAH ** C E R C L I S ** LIST-4: SITE ALl.r LOCATION LISTING PAGE: 539 RUN DATE: 04/01/91 RUN TIME: 09:01:45 VERSION: 1 STATE ZIP COUNTY COOE VI 010 VI VI 010 VI 00820 00820 ALIAS SEQ. NAHE FED n SOURCE FAC 01 01 V1D988266102 VI GOVERNMENT MOTOR POOL ROUTE 304 ST. THOMAS ST. THOMAS VI 030 VI GOVERNMENT MOTOR POOL ST. THOMAS VI 00801 01 VID988266235 VIRGIN AIR CYRIL E. KING AIRPORT, HARWOOO ST. THOMAS VI ST. THOMAS 030 VIRGIN AIR ST. THOMAS VI 00801 01 VID988266250 VIRGIN ISLAND CHEMICAL ESTATE 130 ESTATE BETHLEHEM VI ST CROIX 010 00820 H O O 00 REFERENCE NO. 19 100817 NUS CORPORATION AND SUBSIDIARIES TELECON NOTE m CONTROL NO.: ^•^^^ ?//?/ - o 4 RIBIITinM- / DATE: DISTRIBUTION: ^// n/ TIME: cz^y^o - l / r (^%dd^ y^y^ BETWEEN: / ^ . UykAiei^ OF I/ZIZ^^ PHONE: ( ^ 9 ) 7 7 g ' - ^ - > ^ ^ AND: ^^""T^cyzy^^f}^ ^ ^ ^ ^ r y y . 'yOo (NUS) DISCUSSION: ^ y - ^ = ^ J L / P y ^ . ^ . t ^ A d , 'Cj^^ddz/ ^i<yA^^yiy:dy ^ / d ^ ^ ^ t S ' . ^ ^ k ^ . . ^ . . . . P ^ ^ l / Z 7 y ^ .<y^M r ^ ^ i ^ ^ > a ^ ^ ^Bty^Z/dj dc^fcyy^y/ g y ^ i o / y z ^ ^yitScr^^ ^g^^az^ ^.yus^yyP y ^ (zZrTiyg^y/ ^ ^ ^ r y , ^ . t . d y 7 a ( y ^ T ^ £ < y € ^ ^z^^c^y ^ i s ^ y ^ ^ ^ g g ^ ^ g ^ ^ ^ ^ A ^ T ^ ^ ^ ^ d c y j y y ^ .^^74>iy j : z r ^ y3yy>AyyyZ^ ^ 2 f e ^ ^ < . g . i ^ . . g ^ ykycye^etcZt' yZ^F ^ ^ 2 ^ ' ) ^ g ^ ^ / ' i^<i^hJ^ - - ^ = ^ r ^ ' ^ y ^ . ^ : f ^ y ^ < y ^ ' ^ d y r ^ / ^ y ^ A I<y7!«yy^ ^ye^^tyO^ ysrz. ..^.^yr^. <f<^€. NUS 0«7 REVISED 068S REFERENCE NO. 20 100819 NUS CORPORATION AND SUBSIDIARIES TELECON NOTE CONTROL NO.: DATE: rS /7/?/ TIME: /3V5' DISTRIBUTION: ~ \ y Z ^ Cy/tXLyyd/caJ/ r^cy< BETWEEN: AND: OF: MX 0()/?Pyi PHONE: (Fo?):^75"-5S73 ^^ygy/ffiet^ 5 v g -y^yy>o (NUS) DISCUSSION: yjAJ^o^ (5r ^ A ^ : / z ^ y2Ai£d/i ^ujzt^jtJ i ^ e a ^ £^=L - ^ *y€7l>ea^ yAjt/y) ^djry/;^ .^e»<J^JLay( ^y.iy^^4^^7lky^. X .^fet^g^ .j^>r-r - ir-tTrt-V y / Q O > f & ^ g ^^^C-gf^ ' ^ / ^ < ^ r ^ - ^ ^ ^ J e A l d f W T d ^ ' ^ ^ ^»eS?€> yuytx^J 7fidf>^ / L A ^ ^ & ^fyCnfryjf ' S / . Ul^TrZ/ A a y / r ^ • . ^ . ^ ^ rUner^Jj/yL^ ^ ^ ' ^ l i f - t d d ^ ^ - ^rjr)?p7:>-'^^^5 NUS 067 REVISED 068S i% ,-<^ > " t ' ' .... ^ 1 , f > _ y eEFEeiMOE M©.- 22 100822 NUS CORPORA TION /./^.TXTC SUPERFUND DIVISION PROJECT NOTES ^°- i / Z /)?eyyy^ / ^ °"^^- s / ^ < y A y . . . „ . „ . y T ^ 9 i O l A : y y Z P < ^ - ^ , COPIES SUBJECT '. T^ky^yZdryf -^s^.i^gg.^g^^«^ -^y3^.^^^^u^y7y REFERENCE 7^£teT>7 "cyp. '• FZ/^rUmy 7Z^a*<^^t,L^Uy, r : z ^ J ) /T^ S g ^ f c o .^/-^/g/ y/y/Zryy/ ^ ^ a ^ / ^ y(A9yA>'y^iiyi>^ S.yCUzF'/'// ^ y ^ ts2yiyi^.^y2^ygcyj y>-prr ' ^ , (y^^>-/y '^^^»^ .-^d^uy/ yJ^s^yAyy^ . y / r z : ^ ^ ^ ^ ^ Z^ <? y Z r /JmZ^y y z y a ^ T ^ ' T * - " - ^ ^ , 1 ^ y^^d^Zy yay^..i£E,^yf:y ^ ^ ^ 3 ^ d:t:^eyf^ZLyr y^i^zy^sZy <^^Z^ . J o y ^ ^ ^ ^ T^y.^.^Ajf ^ - ^ /yzA^^ATLP) Sg^fc^^ ^ g ? ^ .rg^^^ <:iyid4Sc.am^,&y7 7 ^ ^ ( ^ <ifdYya£yP y ^ ^^^4^*,,y.a.^.yZ^yrj. ~ 7 Z ^ Z^?^^y^.y/^^y^yrs^ ^ ; r - ^ . ^ . ^ X / l ^ ^ ItrH^d ^2y>^o^y^iy^ .a^s^ ^ a ^ ^c:^.^^^^ ^ 7^77y^y>^ y / y ^ . y^^^y..^ 7 " ' T Z ^ / ^ ^ ^ ^ ^ . . ^ x f e ^ yji/jy^z;/ //^'y!^. yOa. G)^.^yyey&r >C^.-^^*«feg^ / o & 7 ^ ^ A ^ Z / y ^ y Z ^ ^y;yty!^^JTZ/^ ^ ^ / Z / Z T ^ Z ^ < ? ^ , 9 . . ^ . %^ryy . ^ z ^ yfZAy^y/ y ^ J ? ^.^^-Sy:yayidi ^ ^ ^ a ^ * ^ .^^d^y^ay^ a ^ yexr^^^^a^ ^ r^y^yyiy^ 77)0 y2e.^yi/jp. y ^ ^J2u ^ . .yT^T^Jd^t^^j? ^.ra^a^A,yydy •St=^,^ua^kzP . ^ . .eay/f o / j y ^ ^ .g^^y dic^ts^ yg/^ z ^ ^ ^ / z s g ^ y ^ y t ^ ^^^^ y^-./y^.Z^y/ y ^ ^ ^ Ory^ - ^ o Y ^ a ^ ^ ^ ^ y > ^ 2 ^ ^ A ! ^ y M ^ ^ z r ^ . - ^ ^ . ^ ^ . y ^ o 7 .i^yyy^ yjr^y y^yy*Myy y u p ^ Z ^ 'y,^y>T>y ^y^yTZ^yaCU 7 \ y y t ^ . NUS443A58 1182 100823 (I s.ooo 10.000 f M i 0 I.soo 3.O0O Mr lei t Sriwice OistiicU am Niiinli«ieit demand of the service FIGURE 3^. districts on St. Croix for the year 1980 ai2M CSHIII L_ DEMOGRAPHIC Table 3 3 DATA FOR THE U.S. VIRGIN ISLANDS 1 '•IwMl U l a l l Catr-tott i t . i i * m • I t 1UIAI8 :>l. IlMs^a £Tt lUIJkU 8>. C i u l « f \ \ I m T u i u . f l o t u j J i i "^^- I I i l M Y t i ^ l a t t i m 1,011 8 « l » l I M n T.in i » I H SJS I , $ } 1 >,«V» « . } * * i , H a i . t i i S,I8S UO i ^ l , l » i , m t t i I.I18 t . t u « . t « « I I UO 11} 1,881 11,110 i l l S U «0« « , t M I . U O • , • 1 1 l . O M 1.^11 l . i H t . i U MM 4 I ( M t M l W 111 S I M «*,180 «S,«10 Uuik r a t e * « I 0 1 <.u I I «. m .. I I • « i M k . k i t I I M U O 1)0 1 I U !$• >I «00 t . t O i t . o i i -- IS I l l 811 111 U S IS l ( i . o t i l . k i t » , 0 I ) M t S«t • . I H t n • - - )S> no 1*0 I * - U i i l O . S I t U.ViJ i t a o n « t . ' I c l ^ i i : i f | | > i l l «>« --•) .. m -- «» -• JtO .. I . O t I JJt -- ] , t O * I S * — » « t I . M ' J t t ) I I.,11S s.sts .. i T . l i i 11 l.UtS l . t l l .' .. » l . v l f 1.100 S.M« t t * t s I . M I ---- >•» t o — • • -- J . I t t 10. » • » * 2 i ! H o l a U ^ 5 - 1 t l 1 * m .. 171 -- • 1 t » I M ---- 111 •- I S t • t l — U l I H 111 *- I I I t o t s •10 ---- t l -- IS — •1 I0« M l ---- I t i 100 I M .. .. m l . S I l •.>l> l U t t M i r w l U»M«») t u .- I S -- IS .. .. .. t « I f n »• IS >9^ 10 ua .. -- no ISS .. «i i f SS I t IA n 10 10 IS » I M .. IS » •s -. 10 SIS >.*n r o f u l a t l o n I , I t s I . O I l M l l i t t s r*M U l MS t i s l . l t l I.OIO t . * M • . • • I I . I S I • .OlS l . l l t i S t l . M t t . l t l M l l . S I t l . t l l t . t t i 11 I t a sio;«5 t i l t . S t l I t . t l S 100 t M so* t . t l t « . 1 M • , « t o l , i l « l . m !,••• l l t M SSS S i l t l 8 t o i S) t i s i.m t l . l t S JlS.tJO l « M r f o l . l K i l D«( i^lff*) SIO so tso 11 • - KBJI -- I I a sa 11 I . I M IS t a a t s i »'! 1 I'J I t i 11 t n I.IOS •.1st -• I I n.loo I M • I t l t « I H la •* l . l t l I . U I t . a t i »• t a i t . i o t SM la M l I I S l i t I I la M i l l i i . t i a t t . l M 100 -- 81 -- m -- t t -- i t o •- 1.111 l i t I M i . t o a ast -- « 9 t I . O t I M t 11 t . l l S l . S I S --•- l a . t o a 11 i . o t s . i . a i i ----t l . l l t S . I t t l . M t t t a t s l . M t aoo -- i t t t a — .. .. .h\iS l o . a i i n.fM I l l o l c l * lifS^ • t 10 ISO -• -- a i -- ---- 10 • 1 t n 110 ---- t t i -- I M t t l -- I t l I t t 1st I I I I t o t s 110 ---- «1 -* St -- 81 100 M l 100 -- I t l 100 I S t ---- 180 i . a t i s . s i i ftcttauiMit 100 -- n -- -- i n ' ---- so M IIS t s -- IS l i s -• 10 ua .- 10 l i s I M -- tls SS SS 10 10 •- i s -- 10 10 IS t s I M ---- IS IS t s " -- | 0 t t o i ^ t t o Fu|Nil*i i o n 1 ••)<. 1,110 I M I S l t t y . m U 8 t i o I I S l , « t l l . I t t S.OIO i . i s a i , t u t . i t i l,8>S I t l 1,111 t t u 1*1 ) , t t t • , t ] l s . a i t IS 180 St . i l i i t s S,IS8 > i , t t i • l i t I S l t o i l , t l S s . l l l l a . t t i l . l t l i . i t i t . t i i t . o t t H ) t M •11 t t t t l t t s _»»2i2 ; t , u o I j t . t l l O UtiiiTt^olic ( U C I . U I I S ) t o JiSO 10 I , u » l l « S I IS l , » t l I t t i t t t o Sio 1 l i t 1^0 I t t t t I,S1I t . n s t t 1)0 I t . U O t J . ! I,0<.0 t i l l i t 11 101 l , t l l l . t I S titst I « t t t l 1 0 , l i t i l l I I 1)1 U ) t i t 11 11 _ 1 J ) I 0 I S . I t t SJL.*»1 r i u j i i i ^ c d Ul !;cruH>is tJV • M -- 81 -- iSO t t •- )60 -- l . S I t l i t l , l t t i . t o a •)• .. I , t 9 t l , O t ) U t 11 t . l l S l . S i S .. 19,881 111 i,o»s ) , 8 I ) ---. » 1,<.)0 1,111 I , I k t t t o t s i , i t t 800 -- i t t t o . } . m )),<.St t i . t u l a — U i l i i i — •u. 10 )!• Ml -. SW -. -- i o 10 • 1 t i l 111 .. -- t M .. I t t H S .. I t l l i t I t t 100 I I I I t u I I S 110 l%<. St i l 700 M l 100 .. I t l M l ISl. .- _ 11? 1 , 1 1 * t . t S J b a t IMI M l t u t i « » > 110 -- IS ---. H I .. IS l a t s I I S t s l a IS us l a I t a 10 I t a l i s IS IS r.m SS t s l a l a su IS 10 IS sa I M .. IS IS 8S .. .- la aaa 1.000 Mutai tliS • • c a l 4 * l i l l a l | MIf * Hoik l u i c a i GCU - . i l u M i l ( TUa - t o v d a t i>rlaal*4. aa«SA o o 00 to Ol • . ' y . ' - . ' " . ' t ;• '•'- V '• I^EFE^EINIOE IN3©„ 23 100827 DATE: # JECT: FROM: TO: UNITED STATES ENVIRONMENTAL PROTECTION AGENCY OCT 18 1990 REGION II Virgin Island Chemical Co. CVIChem) - Well Water Data John Higgins, P.E., On-Scene Coordinator Response & Prevention Branch c;).^j^f4^^ Sherrel Henry, Remedial Project Manager Eastern New York/Caribbean Remedial Action Branch Please find attached the, "Compendium of Well Water Data Collected at the Virgin Island Chemical Co. by the USEPA (1986-1990)." Thank you for reviewing the draft version. As we agreed, I am sending this report to Ms. Yvette Canegatta of the Virgin Island Department of Natural Resources. This repon vrill also be appended to the VIChem OSC Report. I can be contacted at (FTS) 340-6194, should you have any questions regarding the removal action at VIChem. Attachment cc: Yvette Canegatta, VIDPNR 100828 REGION II FORM 1320-1 (9/85) COMPENDIUM OF WELL WATER DATA COLLECTED AT THE VIRGIN ISLAND CHEMICAL CO. BY THE USEPA (1986-1990) FOREWORD The purpose of this report is to summarize pertinent sampling data and information regarding the volatile organic, well water data collected by the United States Envirormiental Protection Agency (EPA) during various sampling events at, and in the vicinity of the Virgin Island Chemical Co. (VIChem) Hazardous Waste Site in St. Croix during and prior to the 1990 Superfund Removal Action. Summary reports of each of these sampling events are included in the VIChem Removal Action Site Files. A review of the data indicates that Chloroform was consistently the dominant contaminant during each of the sampling events. For this reason, Chloroform results are included herein and are plotted in the attached graph, "Chloroform Contamination in Well Water - Virgin Island Chemical Co. Site, St. Croix". Since the purpose of this report is to merely assemble pertinent data, and not to interpret the data or make recommendations based on the data, all analyzed data, including qualified and rejected data, are included in this report. It should be pointed out that the Drinking Water Maximum Contaminant Level for total trihalomethanes is 100 ug/l (See 40 CFR §141.12) and the 1980 Federal Water Quality Criteria for Chloroform (as revised), based on a carcinogenicity of 10"*, is 5.70 ug/l for human exposure from contaminated water and fish. COMPENDIUM 1. RCRA Enforcement (3/13/86) The Environmental Services Division (ESD) of Region 2 conducted a RCRA Enforcement Inspection of the VIChem facility, then known as Berlex Laboratories, on March 13, 1986. The inspection included 3 soil samples taken from the intermittent stream, or "gut", on the site perimeter, 2 soil samples obtained from the laboratory water drainage pit, and one sample taken from the production well in the northwest comer of the property. The results of the organic analysis from the production well indicated Chloroform contamination at a level of 130 ug/l. 2. St. Croix Well Survey Phase I (3/7/88-3/10/88) The Response and Prevention Branch (RPB) conducted well sampling for volatile organic constituents at 21 locations in St. Croix, including four wells in the vicinity of the VIChem Site. The data was rejected by the Monitoring Management Branch (MMB) due to excessive holding times. Chloroform contamination was indicated in the October 25, 1988 repon, "St. Croix Well Survey", prepared by Weston - TAT, as shovm below: Well Name Fairplains #6 Fairplains #9 VIPA #1 VIPA #2 Chloroform (ug/l) 24 75 &70 11.5 11.3 3. St. Croix Well Survey Phase I (10/31/88-11/2/88) RPB resampled wells at eight locations, including four wells in the vicinity of the VIChem Site. Chloroform contamination was indicated as shown below: Well Name Fairplains #6 Fairplains #9 Fairplains #8 VIPA #2 Chloroform (ug/l) 35.9 10.4 & 9.7 12.4 1.6U* * Chloroform was not detected at the detection level of 1.6 ug/l. 100829 4. VIChem Removal Action Phase 1 (1/17/90) During Phase I removal action activities at VIChem, three off-site wells and the on-site water tank were sampled for volatile organic contamination. Analytical services were provided by a private laboratory procured by the TAT. In addition to the routine QJVQC required for Level 2 Removal Program sampling, two performance evaluation samples and one blind duplicate sample were analyzed. TAT validated the data and, although QJVQC discrepansies were slight and few, liie data was qualified as estimated. Once again, Chloroform was the most dominant compoimd in each sample; the data for this contaminant are shown below: Well Name Fairplains #6 Fairplains #9 Fairplains #8 Water Tank Chloroform (ug/l) 39.0 25.0 5.0 23.9* * This is an average of Chloroform contamination in the three tank samples (Water tank sample = 23.9 ug/l, Water tank drain sample = 22.7 ug/l. Water tank pump sample = 25.0 ug/l). 5. VIChem Removal Action Phase I (6/25/90) During Phase II removal action activities at VIChem, four off-site welis were sampled and analyzed for volatile organic contaminants. When detected, Chloroform was the most dominant compovmd in each sample and in 3 out of 4 samples the only VOC detected. Analytical services were provided by the Contract Laboratory Program and the data was validated by MMB. The only data qualified was for a QA/QC sample for a single compound. The Chloroform data for this sampling event are shown below. Well Name Fairplains #6 Fairplains #9 VIPA #1 VIPA #2 Chloroform (ug/l) 11 39 2J* 5U** * An estimated value of 2 ug/l was reported. Chlorofoim was not detected at the detection level of 5 ug/l. «« 100830 Chloroform Contamination (ug/l) in Well M e r °%y^.yi< H O O 00 LO wy Virgin Island Chemical Site, St Croix O o c» w to iiikiiti/^^His tiiak exceea w mg/i; ana (4) wWidverse health effects shall result. f40 FB 59570. Dec. 24, 1975, as amended at 45 FR 57342. Aug. 27, 19B0; 47 FR 10998, Mar. 12, 1982: 51 FR 11410, Apr. 2, 1986] § 141.12 Maximum contaminant leveU for organic chemicals. The following are the maximum con- taminant levels for organic chemicals. The maximum contaminant levels for organic chemicals in paragraphs (a) and (b) of this section apply to all community water systems. Compliance with the maximum contaminant levels in paragraphs (a) and (b) of this sec- tion, is calculated pursuant to § 141.24. The maximum comtaminant level for total trihalomethanes in paragraph (c) of this section applies only to commu- nity water systems which serve a pop- ulation of 10,000 or more individuals and which add a disinfectant (oxidant) to the water in any part of the drinlt- Ing water treatment process. Compli- ance with the maximum contaminant level for total trihalomethanes is cal- culated pursuant to { 141.30. (a) CMorinated hydrocwbora: EndHn (1,2,3,4,10, lO-heiachkxo-a. 7- epoxy-1.4. 4a,5.6.7,B,81.octahydro-1,4- en*), «ndo-5.8-drmeltiano naphthalene)... Lindane (1,2,3.4,5.6-hexachkxocyclo- hexane. gamma isomer) Methoxychlor (l.l.t-Trichloro-Z, 2-bl» [p- methoxyphenyl) ethane) Toxaphene (C,.H,.Cl,'TechnJcal chlorinated camphene. 67-69 percent ehloflne) (b) Chlofophenoxys: 2,4-D, |2,4-Dichloropherx)xyacetic add) 2,4.S-TP Silvex (2,4,5-TrichlorophefX>xypro- pionic acid) (c) Total trihalomethar^ea (the sum of the co(v centrations of txomodichlorofnelhane, dibro- mochloromethane, tribromomettiane (tiromo- lorm) and thchloromethane (chloroform)) Level, milligrama per Uter 0.0002 0.004 0.1 0.005 0.1 0.01 0.10 mg/l. [40 FR 59570, Dec. 24. 1975. as amended at 44 FR 68641, Nov. 29. 1979] § 141.13 Maximum contaminant levels for turbidity. The maximum contaminant levels for turbidity are applicable to both community water, systems and non- ihe maximum contaminant levels turbidity in driniting water, measured at a representative entry point(s) to the distribution system, are: (a) One turbidity unit (TU), as deter mined by a monthly average pursuant to § 141.22, except that five or fewer turbidity units may be allowed if the supplier of water can demonstrate lo the State that the higher turbidity does not do any of the following: (1) Interfere with disinfection; (2) Prevent maintenance of an effec tlve disinfectant agent throughout tiie distribution system; or (3) Interfere with microbiological de- terminations. (b) Five turbidity units based on an average for two consecutive days pur- suant to { 141.22. 140 FR 59570, Dec. 24, 1975] EFTECTIVE DATE NOTE: At 54 FR 27527. June 29, 1988, i 141.13 was amended, adding Introductory text, effective December 31. 1990. This section already contains an intro- ductory text. EPA will publish a document at a later date clarlfylnK the status of tht current introductory text. Por the conven- ience of the user, the added material fol lows. S 141.13 Maximum conlamlnant levela for tur- blditr. The requirements in this section apply to unfiltered systems until December 30, 1991. unless the State has detennined prior to that date. In writing pursuant to { 1412(b)(7)(C)(lll), that filtration is re quired. The requirements in this section apply to filtered systems until June 29, 1993. The requirements in this section apply to unfiltered systems that the State has de- termined, in writing pursuant to i 1412(b)(7)(C)(lli), must Install filtration, until June 29. 1993. or until filtration Is In stalled, whichever is later. § 141.14 Maximum microbiological con- taminant levels. The maximum contaminant levels for col iform bacteria, applicable to community water systems and non- community water systems, are as fol- lows: (a) When the membrane filter tecli nique pursuant to S 141.21(a) is used. 560 (1) Ope per 100 milliliters as the arithmetic mean of all samples exam- ined per compliance period pursuant to § 141.21(b) or (c), except that, at the primacy Agency's discretion sys- tems required to taice 10 or fewer sam- ples per month may be authorized to exclude one positive routine sample per month from the monthly calcula- tion If: (i) As approved on a case-by-case basis the State determines and Indi- cates In writing to the public water system that no imreasonable rlsls to lieallh existed under the conditions of this modification. This determination sliould be based upon a number of fac- tors not limited to the following: (A) The system provided and had maintained an active disinfectant re- sidual In the distribution system, (B) the potential for contamination as in- dicated by a s-nitary survey, and (C) the history of tne water quality at the public water system (e.g. MCL or mon- itoring violations); (ii) the supplier ini- tiates a check sample on each of two consecutive days from the same sam- pling point within 24 hours after noti- fication that the routine sample is positive, and each of these check sam- ples Is negative; and (ill) the original posKlve routine sample is reported and recorded by the supplier pursuant to 55141.31(a) and 141.33(a). The suppli- er shall report to the State its compli- ance with the conditions specified in this paragraph and a summary of the corrective action taken to resolve the prior positive sample result. If a posi- tive routine sample is not used for the monthly calculation, another routine sample must be antdyzed for compli- ance purposes. This provision may be used only once during two consecutive compliance periods. (2) Pour per 100 milliliters In more than one sample when less than 20 are examined per month; or (3) Four per 100 milliliters iri more than five percent of the samples when 20 or more are examined per month. (b) (1) When the fermentation tube method and 10 milliliter standard por- tions pursuant to i 141.21(a) are used, conform bacteria shall not be present In any of the following: o ^ ^ ant to 8141.21 (b) oWc) except that, at the State's discretion, systems re- quired to take 10 or fewer samples per month may be authorized to exclude one positive routine sample resulting in one or more positive tubes per month from the monthly calculation If: (A) As approved on a case-by-case basis the State determines and indi- cates In writing to the public water system that no unreasonable risk to health existed under the conditions of this modification. This determination should be based upon a number of fac- tors not limited to the following: (1) The system provided and had main- tained an active disinfectant residual in the distribution system, (2) the po- tential for contamination as indicated by a sanitary survey, and (J) the histo- ry of the water quality at the public water system (e.g. MCL or monitoring violations); (B) The supplier initiates a check sample on each of two consecutive days from the sampling point within 24 hours after notification that the routine sample Is positive, and each of these check samples is negative; and (C) The original positive routine sample Is reported and recorded by the supplier pursuant to { 141.31(a) and S 141.33(a). The supplier shall report to the State its compliance with the conditions specified In this para- graph and report the action taken to resolve the prior positive sample result. If a positive routine sample is not used for the monthly calculation, another routine sample must be ana- lyzed for compliance purposes. This provision may be used only once during two consecutive compliance pe- riods. (ID Three or more portions in more than one sample when less than 20 samples are examined per month; or (lil) Three or more portions in more than five percent of the samples when 20 or more samples are examined per month. (2) When the fermentation tube method and 100 milliliter standard portions pursuant to { 141.21(a) are used, collform bacteria shall not be present In any of the following: 661 BEFEREMCE MO. 24 r 100833 NUS CORPORATION AND SUBSIDIARIES TELECON NOTE CONTROL NO.: 0^-9707' o¥ DATE: -7/70/9/ TilWE: 0?70 DISTRIBUTION: ^ i / j : //;Addy:cyJ^ / - ^ BETWEEN: ^ j - 6 y J y y y ^ ^ 7 ^ « A K ^ /7(yy7raii(7^ OF: PHONE: ['S0^]77S--5y7S ANO: yfydyyyj^lZ ' ^ ^ 7 7 7 ^ 0 (NUS) DISCUSSION: < £ Z ^ » g o / 5 < ^ i ^ ^y.*y7kS/y (y-^r3y' 2 ^ r ^ y yy*>^^yy*^cyf^ y t ^ ^ U ^ ^ y?r. ^2y^^76A ' ^ r ^ y O ^ ^ - - " 7 ^ ^yJyy^tAe/ y^yjj/ y ^ ^ Z ^ ^ < ^ yjZ7iS^*d^^^*cyp — ^jy^t^y^j^ -yyj y-TTyr y O ^ ytlrZZzS - s / y ^ ^ . ^ r ^ . . i ^ ^ t ^ U ^ ' - t ( y ^ . y / Z:d^.-yy .-/^.tyyfcyj- j^yytyAr yCZ^<^y.^!ZZ^:^ "sg;^:-.^^^^. NUS 067 REVISED 06SS